WQ0010689_Annual Report_20170222

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9l01� DRY � t� SP
Annual Report Review Class A Distribution
1. Class A Annual Distribution and Marketing/Surface Disposal Certification Form
o Was a certification form submitted? Y
e Was distribution conducted during the reported year?
© How many dry tons were distributed? -%91, IGIR
a Were the distributions within the permitted amount? y P� ►�m i-� L+�^� " �� 2 T
a Were recipients information listed?Y
o Did it indicate compliance?y
® Was form complete?
® Was it signed by the ppropriate people`?�r
2. -Monitoring J
e Were the analyses conducted at the required frequency?'�" �PO�S �o�lzce�j any �i��e�
o Were the metals analyses reported on the Residual. Sampling Summary Form? }� O
a Were the results reported in mg/kg? /
e Were the metals within ceiling concentration permit limits? Y
® Were the metals within monthly average concentration permit limits?o�
® If no, were the lab analyses attached?
0 Were all the required parameters tested?
o .Was TCLP analysis conducted? As & I C4 Cr S,_ Aj I(oKr.6,
e Were the TCLP contaminants within regulatory limits? y
3. Pathogen and Vector Attraction Reduction, N I
e Was a signed copy of the Pathogen and Vector Attraction Reduction Form submitted?
o Did the form indicate the od of coverage, the residual class, and the pathogen reduction alternative and the
vector attraction red on option used?
o Was the approppafe documentation to show pathogen and vector attraction reduction included in.the report?
e Was pathogpfand vector attraction reduction demonstrated according to 40 CFR Part 503 or 2T?
4. General
® Was the report in the proper format?y
a Were any parts of the annual report missing?t1
® Was the report submitted on time?�
PstLi� C E��

2/22/2017
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
RE: 2016 Annual Ash Report
Permit No. WQ0010689
Wood Boiler — North Cove, NC
RECEIVED
;t;ct�.raR:iyc:� 1'r�fi.� lr tjn
it
L CR,..ir-i Gcryry�,,����gqrU
� d � QiYJhV/L
Enclosed is the 2016 Annual Ash Distribution Report fo using the forms provided by NCDENR-
DWQ. Included in this report is the following information:
- Class A Annual DMSDF and Supplemental Information
- Annual Residual Sampling Summary Form and Form-B
- Lab Sheets
- Ash Receiver Signature Sheets
There were no permit deviations noted during the 2016 Reporting Year.
If you have any questions or require additional information, please contact Mike Pisarik at 828-
756-6017 or michael pisarik@,baxter.com.
I certify, under penalty of law that the above information is, to the best of my knowledge and
belief, true, accurate and complete. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
Sincerely,
Jon Rushford
VP Manufacturing- North Cove
MAR - 6 2017
Attachments: Annual Ash Report (3 copies)
Water Qualtty Regional Operdons
Cc: Ricky Styles I AsheVlltB Realonai Office
Baxter Healthcare Corporation
PO Box 1390. Marion, NC 28752
T 828.756.4161

Section 1 Form DMSDF
Class A Annual DMSDF
and Supplemental
Information
RECEIVED
Division of Water FWourm
MAR - 6 2017 3'
Water Quality Regional Operations
Asheville Regional Office

CLASS . A ANNUAL. DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL 'CERTIFICATION AND SUMMARY FORM
Supplemental Information.
WQ PERMIT #: WQ0010689 FACILITY NAMEE:F Baxter Healthcare Corporation North Cove SteamGeneration Plant Ash
PHONE: [phone]=6809 COUNTY:. I McDowell OPERATOR: 4 Baxter Healthcare
FACILITY TYPE .(please check one). [ Surface:Disposal.(complete. Part A - "Month"., ".Source(s)" and. "Residual In!' columns only)
fvo Distribution. and Marketing (complete Parts A. and B)
Part. A*:
Part B*:
Month
Sources(s) (include NPDES #. if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry •
tons)
Intended use(s) .
ApriLMay
WQ0010689
56.49
175.16
131.65.
Bob Brackett
231.65
Land Aoplication
April/May
WQ0010689
53.51
-165.94
219.46
Kenneth Hughes
219.46
Land Application
July
WQ0010689
15:63
121:90
137.52
Paul Boone
137.52
Land Application
July
WQ0010689
24.22
188.94
213.16
Hughes
213.16
Land Application
July
WQ0010689
7.03
54.85
61..88
Phillips
61..88
Land Application
July
WQ0010689
3.13. ..
- 24.38
27.50
Young
27.50
Land Application
Totals:
Annual d tons :
16Q
731.168'
-891.168
.:vim• : -x: :..v.: ,v::..., ..v.: ,.:: ::: ...::: •-::. v::;• .n. .:. w : v
.•...n...... n:4!•i':;•:iv-'%::?�U,;;♦..-... ..�.. ...v.t ,y.. ...k,.: v.:u..w..,
>:;:::>::�.:«�;;:<�::;::y<,�,:.�:;v,;-.,i<:;.v:m:n.:.,..:.,.,f,+..,,.:.x,..�...
89-1.1,68
4'{.. .ii:vvv�;•:;:?;.:v'.i.:
•:,:1-•::.::5•::: vv:: n;:,::;:;:�..,•,
Amendments used: Bulking Agent(s) used: Dry Wood Chips
*-If more space. is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (SUPPA 1
DFKIR FORM DMSDF (Sunn) (12/2006) ,

CLASS.A.ANNUAI.,,DISTRIBUTION AND MAR MTING/ SURFACE DISPOSAL CERTIFICATIONAND SUMMARY FORM
WQ PERMIT.#: WQ0010689 FACILITYNAME: Baxter Healthcare, Corporation North Cove. Steam GenerationTlant Ash
PHONE: [phone] COUNTY:, McDowell OPERATOR: 'Baxter Healthcare
FACILITY- TYPE (please check one): El. Surface Disposal. (complete Part A (Source(s) and "Residual In"' Volume only) and, Part C)
2 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in oneration'during.the bast calendar vear? Yes 0 No ® =► If No skip carts A. B. C and certify form'below
Part A*:
Part B*:
Month
=
Sources(s) (include NPDES #'if
applicable)
Volume (dry tons)
Reci Tent Information
Amendment/
Bulking Agent
Residual In
. Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January.
See DMSDF sheet
February -
supplemental for, -
Marche
breakdown,
April
May
June
July
August
September
October,
November
December
Total from FORM DMSDF (sup)
160
731 16Zd .,,,
„8911�68: -,,
891:1;6.8
X..,
Totals:
Annual d tons):
1'60
; 731 I68,
894 16>i
`,;+,3 `.:.7„: sa " {{ >
891.168
:...
Amendments used: Bulking Agent(s) used: Dry Wood Chips
*'If more: space is required; attach additional information sheets (FORM. DMSDF (supp)):. Total Number of Form DMSDF. (Supp) 1 .
Part C:. .
Facility was compliant during thepast calendar year with all conditions of the land application permit . R ;Yes
(includingbut not limited to items 1-3below) issued, by the Division of Water Quality: ® No -► If -No, Explain in Narritive.
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. -All operation and maintenance requirements were compiled withor, in the case of a. deviation, prior.authorization was received from the Division of Water Quality.
3.:No contravention of Ground Water Quality Standards occurred at a monitoring well:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and'.belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing -violations."
Sign tare of Permittee Date Signature of Preparer** Date
(if different from Permittee)
**Preparer is. defined in 40 CFR Part 503.9(r) and 15A NCAC 2TA102 (26)
nFNR FORM nmgnF tigo ng)

Section 2 Form RSSF
Annual Residual
Sampling Summary
Form and Form B

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0010689 Laboratory:
Baxter Healthcare Corporation North Cove
Facility Name: Steam Generation Plant Ash
Residual Source WQ # or
NPDES #:
WQ0010689
WWTP Name: NA
Residual Analvsis Data
1) Pace Analytical Services
2)
3)
4)
5)
Parameter
(mg g)
Conc.
Limit
m a
Sample or Com osite Date
NP33116A
NP33116B
SP61516A
SP61516B
Percent Moisture (%)
NA
48.5
49.9 . ✓
42.7 v
49
Arsenic
75
ND �-tl,
NDc
11.6 b-`
14.1 v
Cadmium
85
ND z- 1,1
ND zq jt
1.9 v
2.1 ,/
Copper
4,300
260 ✓
74.8 ,/
83.5 v
113 v
Chromium
NA
30.7
27.4
21.0
24.4 v
Lead
846
25.8 ✓
56.3 V
27 V
31.9 e/
Mercury
57
ND-,-.aao
ND4, a0.3
0.005 v
ND-�,a,
Molybdenum
75
ND C, q
ND z-?, 1
1.9 .
2
Nickel
420
26.3 a/
22.9 ,/
19.4 ✓
23.1 ✓
Selenium
100
ND
ND /-Iy,
-ND z- i •
ND I-f, 4
Zinc
7,500
259 .
170
227 ✓
270
Total Phosphorus
NA
941 1V
1200 ,/
1720 ✓
1360
Barium
NA
1680 y/
1340 v'
1400 ✓
1830 ,✓
Calcium
NA
89200 ✓
75100 V
78400 `$
102000✓
Iron
NA
16800
,, ----19800
1 10300
11900 ✓
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with,,a system designed
to assure that qualified. personnel properly gathered and evaluated the information submitted. I am aware that there are significant -
penalties for sutting false information, including the possibility of fines and imprisonment for knowing violations."
Signatdre'of Preparer
4?k /Z Z
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0010689
Baxter Healthcare Corporation North Cove
Facility Name: Steam Generation Plant Ash
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analvsis Data
WQ0010689
NA
Laboratory: 1) Pace Analytical Services
2)
3)
4)
5)
Parameter
(mg/kg)
Sample or Composite Date
NP33116A
NP33116B
SP61516A
SP61516B
Magnesium
15600 V
12500 ,/
12500 v
17300
-
Manganese
2930 V
2380 ✓
2930
3460 ✓
pH
11.6 V
11.3 ✓
8.4 v
8.4 ✓
Potassium
22900 ✓
20000 ✓
21800
25000 ✓
Silver
ND -5.01
ND4-1e1
ND/-o,-14
ND ,71
Sodium
6280 V
ND
5310 ✓
6230 e.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
,0/7
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

Section 3 Lab Sheets

/41cei21�ltll al cefebAcwrr
a
April 14, 2016
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
Pace Analytical Services, Inc.
9800 KlnceyAve. Suite 100
Huntersville. NC 28078
[phone]
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on March 31, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 24

Pace Analytical Services, Inc.
/Ice
A apical9800 Kincey Ave. Suite 100
WAWA &WM Huntersville, NC 28078
# VO4)875-9092
i
CERTIFICATIONS
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
Pennsylvania Certification IDS
Georgia Certification #: C040
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
L-A-B DOD-ELAPAccred-Ration #: L2417
Alabama Certification #: 41590
Arizona Certification #: AZ0734
Arkansas Certification
Califomia Certification #: 04222CA
Colorado Certification
Connecticut Certification #: PH-0694
Delaware Certification
Florida/TNI Certification #: E87683
Georgia Certification #: C040
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification #: 391
,Kansas/rNl Certification #: E-10358
Kentucky Certification # 90133
Louisiana DHH/rNI Certification #: LA140008
Louisiana DEQ/rNI Certification #: 4086
Maine Certification #: PA00091
Maryland Certification #: 308
Massachusetts Certification #: M-PA1457
Michigan/PADEP Certification
Missouri Certification #: 235
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersviile, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Montana Certification #: Cert 0082
Nebraska Certification #: NE-05-29-14
Nevada Certification #: PA014572015-1
New Hampshire/rNi Certification #: 2976
New Jersey/rNI Certification #: PA 051
New Mexico Certification #: PA01457
New York/rNI Certification #: 10888
North Carolina Certification #: 42706
North Dakota Certification #: R-190
Oregon/rNI Certification #: PA200002
Pennsylvania/rNI Certification #: 65-00282
Puerto Rico Certification #: PA01457
Rhode Island Certification #: 65-00282
South Dakota Certification
Tennessee Certification #: TN2867
Texas/TNI Certification #: Ti 04704188-14-8
Utah/rNI Certification #: PA014572015-5
USDA Soil Permit #: P330-14-00213
Vermont Dept. of Health: ID# VT-0282
Virgin Island/PADEP Certification
Virginia/VELAP Certification #: 460198
Washington Certification #: C868
West Virginia DEP Certification #:143
West Virginia DHHR Certification #: 9964C
Wisconsin Certification
Wyoming Certification #: 8TMS-L
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 24

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SAMPLE ANALYTE COUNT
Project: Wood Boiler Ash 3131
Pace Project No.: 92292040
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytts
Lab ID Sample ID Method
Analysts
Reported
Laboratory
92292040001 NP33116A EPA 6010
CDF
17
PASI-A
EPA 6010
CDF
7
PASI-A
EPA 7470
HVK
1
PASI-A
EPA 7471 '
HVK
1
PASI-A
ASTM D2974-87
CLW
1
PASI-C
EPA 1010
MLS
1
PASI-A
EPA 9045.
TEP
1
PASI-A
EPA 365.1
BRJ
1
PASI-A
SW-846 7.3.3.2
PAS
1
PASI-PA
SW-846 7.3.4.2
PAS
1
PASI-PA
92292040002 NP33116B EPA 6010
CDF
17
PASI-A
EPA 6010
JMW
7
PASI-A
EPA 7470
HVK
1
PASI-A
EPA 7471
HVK
1
PASI-A
ASTM D2974-87
CLW
1
PASI-C
EPA 1010
MLS
1
PASI-A
EPA 9045
TEP
1
PASI-A
EPA 365.1
BRJ
1
PASI-A
SW-846 7.3.3.2
PAS
1
PASI-PA
SW-846 7.3.4.2
PAS
1
PASI-PA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 24

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ANALYTICAL RESULTS
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NP33116A Lab ID: 92292040001 Collected: 03/31/16 09:45 Received: 03/31/1611:18 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
ND
mg/kg
11.7
10
04/05/16 20:00 04/07/16 13:17 7440-38-2
Barium
1680
mg/kg
5.9
10
04/05/16 20:00 04/07/16 13:17 7440-39-3
Cadmium
ND
mg/kg
1.2
10
04/05/16 20:00 04/07/1613:17 7440-43-9
Calcium
89200
mg/kg
117
10
04/05/16 20:00 04/07/1613:17 7440-70-2
Chromium
30.7
mg/kg
5.9
10
04/05/16 20:00 04/07/16 13:17 7440-47-3
Copper
260
mg/kg
5.9
10
04/05/16 20:00 04/07/1613:17 7440-50-8
iron
16800
mg/kg
117
10
04/05/16 20:00 04/07/1613:17 7439-89-6
Lead
25.8
mg/kg
5.9
10
04/05/16 20:00 04/07/1613:17 7439-92-1
Magnesium
15600
mg/kg
117
10
04/05/16 20:00 04/07/1613:17 7439-95-4
Manganese
2930
mg/kg
5.9
10
04/05/16 20:00 04/07/16 13:17 7439-96-5
Molybdenum
ND
mg/kg
5.9
10
04/05/16 20:00 04/07/16 13:17 7439-98-7
Nickel
26.3
mg/kg
5.9
10
04/05/16 20:00 04/07/1613:17 7440-02-0
Potassium
22900
mg/kg
5850
10
04/05/16 20:00 04/07/16 13:17 7440-09-7
Selenium
ND
mg/kg
11.7
10
04/05/16 20:00. 04/07/1613:17 7782-49-2
Silver
ND
mg/kg
5.9
10
04/05/16 20:00 04/07/1613:17 7440-22-4
Sodium
6280
mg/kg
5850
10
04/05/16 20:00 04/07/16 13:17 7440.23.5
Zinc
259
mg/kg
11.7
10
04/05/16 20:00 04/07/16 13:17 7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 04/02/16 05:30 Initial pH:11.2; Final pH: 4.9
Arsenic
ND t,
mg/L
0.050
1
04/05/16 02:20 04/05/16 13:32 7440-38-2
Barium
2.6 ✓
mg/L
0.25
1
04/05/16 02:20 04/05/1613:32 7440-39-3
Cadmium
0.014✓
mg/L
0.0050
1
04/05/16 02:20 04/05/1613:32 7440-43-9
Chromium
0.052 1✓
mg/L
0.025
1
04/05/16 02:20 04/05/1613:32 7440-47-3
Lead
0.039
mg/L
0.025
1
04/05/16 02:20 04/05/16 13:32 7439-92-1
Selenium
ND
mg/L
0.10
04/05/16 02:20 04/05/1613:32 7782-49-2
Silver
ND
mg/L
0.025
V 1
04/05/16 02:20 04/05/1613:32 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 04/02/16 05:30 Initial pH: 11.2; Final pH: 4.9
Mercury
ND
mg/L
0.00020
1
04/05/1613:30 04/05/1616:59 7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
ND
mg/kg
0.0069
1
04/08/1615:45 04/09/1618:14 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
48.5
%
0.10
1
0.4/04/16 07:08
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint >200 deg F V 70.0 1 04/11/1611:20
9045 pH Soil Analytical Method. EPA 9045
pH at 25 Degrees C 11.6 Std. Units v 0.10 1 04/01/1615:15 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 24

/+ 0 Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
wwrvpeyew com Huntersvllle, NC28078
s [phone]
ANALYTICAL RESULTS
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
Sample: NP33116A , Lab ID: 92292040001 Collected: '03/31/1609:45 Received: 63/31/16 11:18 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dlluffons.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
365.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus '941 mg/kg 29.0 10 04/05/16 02:23 7723-14-0
733C S Reactive Cyanide Analylicaf Method: SW-846 7.3.3.2
Cyanide, Reactive ND ✓ mg/kg 1.9 1 04/04/16 19:23
735S Reactive Sulfide Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive ND ✓ mg/kg 19.3 1 04/04/1614:15
Date: 04/14/2016 05:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 24

?CeAnaocal
www.peceJebe cam
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ANALYTICAL RESULTS
Project: Wood Boiler Ash 3/31
Pace Project No:: 92292040
Pace Analytical Services; Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: NP33116B
Lab ID: 92292040002 Collected: 03/31/1609:45
Received: 03/31/1611:18 Matrix: Solid
Results reported on a "dry weight-
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Qua]
6010 MET ICP
Analytical Method: EPA 6010
Preparation Method: EPA 3050
Arsenic
ND mg/kg
14.3 10
04/05/16 20:00 04/07/1.613:20 7440-38-2
Barium
1340 mg/kg
7.1 10
04/05/16 20:00. 04107/1613:20 7440-39-3
Cadmium
ND mg/kg
1.4 10
04/05/16 20:00 04/07/16 13:20 7440-43-9
Calcium
75100 mg/kg
143 10
04/05/16 20:00 04/07/1613:20 7440-70-2
Chromium
27.4 mg/kg
7.1 10
04/05/16 20:00 04/07/1613:20 7440-47-3
Copper
74.8 mg/kg
7.1 10
04/05/16 20:00 04/07/16 13:20 7440-50-8
Iron
19800 mg/kg
143 10
04/05/16 20:00 04/07/1613:20 7439-89-6
Lead
56.3 mg/kg
7.1 10
04/05/16 20:00 04/07/1613:20 7439-92-1
Magnesium
12500 mg/kg
143 10
04/05/16 20:00 04/07/16 13:20 7439-95-4
Manganese
2380 mg/kg
7.1 10
04/05/16 20:00 04/07/1613:20 7439-96-5
Molybdenum
ND mg/kg
7.1 10
04/05/16 20:00 04/07/16 13:20 7439-98-7
Nickel
22.9 mg/kg
7.1 10
04/05/16 20:00 04/07/1613:20 7440-02-0
Potassium
20000 mg/kg
7130 10
04/05/16 20:00 04/07/1613:20 7440-09-7
Selenium
ND mg/kg
14.3 10
04/05/16 20`:00 04/07/16 13:20 7782-49-2
Silver
ND mg/kg
7.1 10
04/05/16 20:00 04/07/16 13:20 7440-22-4
�5odlu
ND mg/kg
7130 10
04/05/16 20:00 04/07/16 13:20 7440-23-5
Zinc
170 mg/kg
14.3 10
04/05/16 20:00 04/07/16 13:20 7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010
Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311;
04/02/16 05:30 Initial pH: 11.2; Final pH: 5
Arsenic
ND mg/L
0.050 V 1
04/07/16 03:45 04/07/16 23:18 7440-38-2
Barium
2.5 V mg/L
0.25 1
04/07/16 03:45 04/07/16 23:18 7440-39-3
Cadmium
0.0063 V mg/L
0.0050 1
04/07/16 03:45 04/07/16 23:18 7440-43-9
Chromium
ND mg/L
0.025 ✓ 1
04/07/16 03:45 04/07/16 23:18 7440-47-3
Lead
0.049 ✓ mg/L
0.025 1
04/07/16 03:45 04/07/16 23:18 7439-92-1
Selenium
ND mg/L
0.101/ 1
04/07/16 03:45 04/07/16 23:18 7782-49-2
Silver
ND mg/L
0.025 1
04/07/16 03:45 04/07/16 23:18 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470
Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311;
04/02/16 05:30 Initial pH: 11.2; Final pH: 5
Mercury
ND mg/L
0.00020 1
04/08/16 01':15 04/08/1613:13 7439-97-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Mercury
ND mg/kg
0.0083 1
04/08/1615:45 04/09/1618:21 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
49.9 %
0.10 1
04/04/16 07:07
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0 1
04/11/1611:20
9045 pH Soil
EPA 9045
Analytical MaYStd.
pH at 25 Degrees C
11.3 Units
0.10 1
04/01/1615:15 H6
REPORT OF LABORATORY ANALYSIS'
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 24

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•www.pacsiebs-cam.
ANALYTICAL RESULTS,
Project: Wood Boiler Ash 3/31
Pace Project No,: 92292040
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: NP33116B
Lab ID: 92292040002 Collected: 03/31/16 09:45
Received: 03/31/1611:18 Matrix: Solid
Results reported on a °dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
1200 mg/kg 57.8 20
04/05/16 02:27 7723-14-0
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND ✓ mg/kg 2.0 1
04/04/16 19:23
735S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND ✓ mg/kg 19.9 1
04/04/1614:15
Date: 04/14/2016 05:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 24

aceMaVbgl
WMEPeowaftcom
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
QC Batch: MERP/9203
QC Batch Method: EPA 7470
Associated Lab Samples: 92292040001
METHOD BLANK: 1701931
Associated Lab Samples: 92292040001
Parameter Units
mg/L
Mercury
LABORATORY CONTROL SAMPLE: 1701932
Parameter Units
Mercury mg/L
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
Matrix: Water
EPA 7470
7470 Mercury TCLP
Blank Reporting
Result Limit Analyzed Qualrfiers
ND 0.00020 04/05/1616:02
Spike LCS LCS % Rec
Cone. Result % Rec Limits
.0025 0.0025 99 80-120
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1701933 1701934
MS MSD
92291659001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND .0025 .0025 0.0027 0.0027 106 107 75-125 0
Results presented on this page are In the units Indicated by the 'Units' column except where an alternate unit Is presented to the right of the resutL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 24

c?CL�ICc�®
i
QUALITY CONTROL DATA
Project: Wood Boiler Ash 3/31
Pace Project No.: 92202040
QC Batch: MERP/9223 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92292040002
METHOD BLANK: 1704980 Matrix: Water
Associated Lab Samples: 92292640002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/L ND 0.00020 04108/1612:57
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1704981
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury mg/L .0025 0.0028 11.0 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1704982 1704983
MS MSD
92292325001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Resuft Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND .0025 .0025 0.0030 0.0028 121 112 75-125 8
Results presented on this page are In the units Indicated by the'Units' column except whore an aiternato unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical' Services, Inc..
Page 9 of 24

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t
QUALITY CONTROL DATA
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
UG Batch: MERP/9221 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92292040001, 92292040002
METHOD BLANK: 1704003
Associated Lab Samples: 92292040001. 92292040002
Parameter . Units
Mercury mg/kg
Matrix: Solid'
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0050 04/09/1617:52
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1704004
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg .067 0.068 102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1704005
1704006
MS
MSD
92292257001 Spike
Spike
MS
MSD MS MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.012 .05
.074
0.056
0.085 87 97 75-125 40 R1
Results presented on this page are In the unite indicated by the 'Unite' column except where an alternate unit Is presented to the right of the rosutt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 24

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WA+t'•paoeteiY OM
s
i
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
Pace Analytical Services; Inc.
9800 KinceyAve. Suite 100
j Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
ut., tsatcn: MPRP/21248 Analysis Method: EPA 6010
QC Batch Method: EPA3050 Analysis Description: 60.10 MET
Associated Lab Samples: 92292040001, 92292040002
METHOD BLANK. 1702146
Associated Lab Samples: 92292040001, 92292040002
Parameter
Units
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Iron
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Manganese
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Matrix: Solid
Blank
Result
Reporting
Limit
Analyzed Qualifiers
ND
1.0
04/07/1612:40
ND
0.50
04107/1612:40
ND
0.10
04/07/1612:40
ND
10.0
04/07/1612:40
ND
0.50
04/07/1612:40
ND
0.50
04/07/1612:40
ND
10.0
04107/1612:40
ND
0.50
04/07/1612:40
ND
10.0
04/07/1612:40
ND
0.50
04101/1612:40
ND
0.50
04/07/1612:40
ND
0.50
04/07/1612:40
ND
500
04/07/1612:40
ND
1.0
04/07/1612:40
ND
0.50
04/07/1612:40
ND
500
04/07/1612:40
ND
1.0
04/07/1612:40
LABORATORY CONTROL SAMPLE:
Parameter
1702147
Units
Spike
Cone.
LCS
Result
LCS
% Rae
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
49.0
98
80-120
Barium
mg/kg
50
49.6
99
80-120
Cadmium
mg/kg
50
50.1
100
80-120
Calcium
mg/kg
500
496
99
80-120
Chromium
mg/kg
50
48.9
98
80-120
Copper
mg/kg
50
49.5
99
80-120
Iron
mg/kg
500
502
100
80-120
Lead
mg/kg
50
49.2
98
80-120
Magnesium
mg/kg
50Q
488
98
80-120
Manganese
mg/kg
50
48.2
96
80-120
Molybdenum
mg/kg
50
51.8
104
80-120
Nickel
mg/kg
50
49.9
1.00
80-120
Potassium
mg/kg
500
ND
100
80-120
Selenium
mg/kg
50
50.6
101
80-120
Silver
mg/kg
25
25.0
100
80-120
Sodium
mg/kg
500
497J
99
80-120
Zinc
mg/kg
50
49.6
99
80-120
Results presentod on this page are In the units Indicated by the "Unite' column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 24

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QUALITY CONTROL DATA
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1702148
1702149
MS
MSD
92292325001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result .
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
ND
48.3
50
55.7
56.6
98
97
75-125
2
Barium
mg/kg
96.6
48.3
50
157
174
125
155
75-125
10 M6
Cadmium
mg/kg
ND
48.3
50
52.8
53.3
409
107
75-125
1
Calcium
mg/kg
1160
483
500
1380
1460
58
71
75-125
5 M6
Chromium
mg/kg
31.4
48.3
50
136
101
216
139
75-125
29 M6, R1
Copper
mg/kg
38.5
48:3
50
86.4
87.5
99
98
75-125
1
Iron
mg/kg
32600
483
500
40500
38600
1630
1190
75-125
5 M6
Lead
mg/kg
17.9
48.3
50
•77.8
85.5
124
135
75-125
10 M6
Magnesium
mg/kg
3910
483
500
4580
4550
138
128
75-125
1 M6
Manganese
mg/kg
499
48.3
50
610
760
230
521
75-125
22 M6, R1'
Molybdenum
mg/kg
ND
48.3
50
50.7
50.4
102
98
75-125
0
Nickel
mg/kg
28.0
48.3
50
97.2
102
143
149
75-125
5 M6
Potassium
mg/kg
ND
483
500
ND
ND
79
88
75-125
Selenium
mg/kg
ND
48.3
50
41.8
46.9
86
94
75-125
11
Silver -
mg/kg
ND
24.2
24.9
22.4
23.7
93
95
75-125
6
Sodium
mg/kg
ND
483
500
ND
ND
88
.88
75-125
Zinc
mg/kg
68.2
48.3
50
117
125
102
114
75-125
6
Results presented on this page are In the units Indicated by the 'Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc..
Page 12 of 24

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Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
QC Batch: MPRP/21241
QC Batch Method: EPA 301 CA
Associated Lab Samples: 92292040001
METHOD BLANK: 1701563
Associated Lab Samples: 92292040001
QUALITY CONTROL DATA
Analysis Method: EPA 6016
Analysis Description: 6010 MET TCLP
Matrix: Water
Blank
Parameter
Units
Result
Arsenic
mg/L
ND
Barium
mg/L
ND
Cadmium
mg/L
ND
Chromium
mg/L
ND
Lead
mg/L
ND
Selenium
mg/L
ND
Silver
mg/L
ND
LABORATORY CONTROL SAMPLE:
1701564'
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Reporting
Limit Analyzed •
0.050 04/05/1612:05
0.25 04/05/1612:05
0.0050 04/05/1612:05
0.025 04105/1612:05
0.025 04/05/1612:05
0.10 04/05/1612:05
0.025 04/05/1612:05
Spike
LCS
LCS
Conc.
Result
% Rec
2.5
2.7
109
2.5
2.6
104
2.5
2.7
107
2.5
2.7
107
2.5
2.5
101
2.5
2.8
110
1.2
1.2
98
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
% Rec
Limits Qualifiers
80-120
80-120
80-120
80-120
80-120
80-120
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1701565
1701566
MS
MSD
92291659001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units.
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.9
2.8
116
113
75-125
2
Barium
mg/L
ND
2.5
2.5
2.9
2.8
111
107
75-125
4
Cadmium
mg/L
ND
2.5
2.5
2.9
2.8
115
112
75-125
2
Chromium
mg/L
ND
2.5
2.5
42.9
2.8
114
111
75-125
3
Lead
mg/L
ND
2.5
2.5
2.7
2.7
109
106
75-125
3
Selenium
mg/L
NO
2.5
2.5
3.0
2.9
119
116
75-125
3
Silver
mg/L
ND
1.2
1.2
1.3
1.3
106
103
75-125
4
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Dater 04/14/2016 05:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 24

2ceAnWicai"
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t
QUALITY CONTROL DATA
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
QC Batch: MPRP/21270
QC Batch Method: EPA 3010A
Associated Lab Samples: 92292040002
Analysis Method:
Analysis Description:
EPA6010
6010 MET TCLP
METHOD BLANK: 1703626
Matrix: Water
Associated Lab Samples: 922292040002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Arsenic
mg/L
ND
0.050
04/07/16 23:11
Barium
mg/L
ND
0.25
04/07/16 23:11
Cadmium
mg/L
ND
0.0050
04/07/16 23:11
Chromium
mg/L
ND
0.025
04/07/16 23:11
Lead
mg/L
ND
0.025
04/07/16 23:11
Selenium
mg/L
ND
0.10
04/07/16 23:11
Silver
mg/L
ND
0.025
04/07/16 23:11
LABORATORY CONTROL SAMPLE:
1703627
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2.5
2.6
103
80-120
2.5
2.3
93
80-120
2.5
2.4
96
80-120
2.5
2.4
97
80-120
2.5
2.2
90
80-120
2.5
2.7
109
80-120
1.2
1.3
104
80-120
n
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1703628
1703629
MS
MSD
92292040002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.8
2.6
112
106
75-125
5
Barium
mg/L
2.5
2.5
2.5
4.9
4.6
95
85
75-125
5
Cadmium
mg/L
0.0063
2.5
2.5
2.6
2.5
102
98
75-125
4
Chromium
mg/L
ND
2.5
2.5
2.6
2.5
105,
100
75-125
4
Lead
mg/L
0.049
2.5
2.5
2.5
2.4
100
96
75-125
4
Selenium
mg/L
ND
2.5
2.5
3.0
2.8
117
109
75-125
7
Silver
mg/L
ND
1.2
1.2
1.4
1.3
111
105
75-125
6
Results presented an this page are In the units Indicated by the 'Units' column except where an alternate unit Is presented to the right at the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc..
Page 14 of 24

QUALITY CONTROL DATA
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
QC Batch: PMST/8933 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92292040001, 92292040002
SAMPLE DUPLICATE: 1699973
92292011001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 98.2 98.2 0
SAMPLE DUPLICATE: 1699974
92292040002 Dup
Parameter Units Result Result
Percent Moisture ' % 49.9 50.7
RPD Qualifiers
N
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the 'Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc..
Page 15 of 24

;aceAnaykal
1 tMYYIK(tgt:e�bB.CMn
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
QC Batch: WET/44147
QC Batch Method: EPA 1010
Associated Lab Samples: 92292040001, 92292040002
SAMPLE DUPLICATE: 1706537
Parameter Units
Flashpoint deg F
QUALITY CONTROL DATA
Analysis Method: EPA 1010
Analysis Description: 1010 Flash Point, Closed Cup
92292040001 Dup
Result Result RPD Qualifiers
>200 >200
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the 'Units' column except whore an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc..
Page 16 of 24

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Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
QC Batch: WET/43937
QC Batch Method: EPA 9045
Associated Lab Samples: 92292040001, 92292040002
SAMPLE DUPLICATE: 1699261
Parameter Units
pH at 25 Degrees C Std, Units
QUALITY CONTROL DATA
Analysis. Method: EPA 9045
Analysis Description 9045 pH
92291687002 Dup
Result Result RPD Qualifiers
12.9 12.9 0 H6
Pace Analytical Services, Inc:
9800KInceyAve. Suite100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the 'Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 24

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QUALITY CONTROL DATA
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
OC Batch: WETA/27059 Analysis Method: EPA365.1
QC Batch Method: EPA 365.1 Analysis Description: - 365.1 Phosphorus, Total
Associated Lab Samples: 92292040001, 92292040002
METHOD BLANK: 1701429 - Matrix: Solid
Associated Lab Samples: 92292040001, 92292040002
Blank Reporting
Parameter Units Result Limit Analyzed
Phosphorus mg/kg ND 2.0 04/05/16 02:07
LABORATORY CONTROL SAMPLE: 1701430
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Phosphorus mg/kg 50 50.2 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1701431 1701432
MS MSD
92291687001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 83.3 79.4 79.4 138 139 68 70 90-110 1 M1
Results presorded on this page are In the units Indicated by the 'Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 24

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QUALITY CONTROL DATA
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
ut; daicn: WETA/23166 Analysis Method: SW-846 7.3.3.2
QC Batch Method: SW-846 7.3.3.2 Analysis Description: 733C Reactive Cyanide
Associated Lab Samples: 92292040001, 92292040002
METHOD BLANK: 1052580 Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide, Reactive mg/kg ND 1.0 04/04/1619:14
SAMPLE DUPLICATE: 1052581
30178281001 Dup
Parameter Units Result Result RPD Qualifiers
Cyanide, Reactive mg/kg ND ND
Pace Analytical Services, Inc.
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units, column except where an alternate unit Is presented to the right of the resulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc..
Page 19 of 24

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DUALITY CONTROL DATA
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
OC Batch: WETA/23167
Analysis Method:
SW-846 7.3.4.2
QC Batch Method: SW-846 7.3.4.2
Analysis Description:
734S Reactive Sulfide
Associated Lab Samples: 92292040001, 92292040002
METHOD BLANK: 1052582
Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Sulfide, Reactive
mg/kg
ND
10 04104/1614:15
SAMPLE DUPLICATE: 1052583
30178281001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Sulfide, Reactive
mg/kg
ND
NO
Pace Analytical Services, Inc.
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the 'Units' column except where an altemato unit Is presented to the right of the resutL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc..
Page 20 of 24

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i
QUALIFIERS
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL- Reporting Limit.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW646 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-PA Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA required holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/14/2016 05:09 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 24

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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Wood Boiler Ash 3/31
Pace Project No.: 92292040
Pace Analytical Services, Inc.
9800 ICrncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
OC Batch
Analytical Method
Batch
92292040001
NP33116A
EPA3050
MPRP/21248
EPA6010
ICP/19102
92292040002
NP331168
EPA 3050
MPRP/21248
EPA6010
ICP/19102
92292040001
NP33116A
EPA 3010A
MPRP/21241
EPA 6010
ICP/19087
92292040002
NP33116B
EPA 301DA
MPRP/21270
EPA6010
ICP/19118
92292040001
NP33116A
EPA 7470
MERP/9203
EPA 7470
MERC/8835
92292040002
NP33116B
EPA 7470
MERP/9223
EPA 7470
MERC/8858
92292040001
NP33116A
EPA 7471
MERP/9221
EPA 7471
MERC/8862
92292040002
NP33116B
EPA 7471
MERP/9221
EPA 7471
MERC/8862
92292040001
NP33116A
ASTM D2974-87
PMST/8933
92292040002
NP331165
ASTM D2974-87
PMST/8933
92292040001
NP33116A
EPA 1010
WET/44147
92292040002
NP331168
EPA1010
WE17/44147
92292040001
NP33116A
EPA 9045
WET/43937
92292040002
NP33116B
EPA 9045
WE17/43937
92292040001
NP33116A
EPA365.1
WETA/27059
92292040002
NP33116B
EPA 365.1.
WETA127059
92292040001
NP33116A
SW-846 7.3.3.2"
WETA/23166
92292040002
NP331168
SW-846 7.3.3.2
WETA/23166
92292040001
NP33116A
SW-846 7.3.42
WETN23167
92292040002
NP331168
SW-846 7.3.4.2
WETA/23167
Date: 04/14/2016 05:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Wdhout the written consent of Pace Analytical Services, Inc..
Page 22 of 24

Document Naive Document Revised:18FES2016
aG�arlalytbf Sample Condition upon Recei t(SCUR Page 1 of:2
Document No,: Issuing Authority:
F-CHR-CS-003-rev,18 Pace Huntersville Quality Office
Sample Page 2 of 2 for internal Use ONLY
Condition Upon Client Name: r Project { WO VZO0
D4� (aOQS
Courier: OFPd Ex ❑UPS USPS ent
❑ Commercial QPace ❑Other: 92292040 1 1
Custody Seal Present? E]Yes Q o Seals Intact? (]Yes []No
��'"'' Date/initials person Examining Contents:� 3'!
Parking Material: []Bubble Wrap {Bubble Bags (]None __60 hen: )p
Thermometer: [] IR Gun #S-SN:15527198 ❑ T oflee: QWet []Blue 'e ❑samples on fee, cooling process has bin, J
Correction Factor: 0:0'C Cooler Temp Corrected BiologfcatTissue Frozen? Oyes ❑No 2ti/A
Temp. should be above freezing to 6'C
USDA Regulatdd 11( C] N/A, water sample)
Did samples or' hate in a quarantine lone within the United States: CA, NY,.orSC (check maps)? Did samples originate from a foreign source (Internationally,
[]Yes o d �'
in uding Hawarl and Puerto Rim}? ❑Yes o
COMMENTS:
Chain bf Custody Present?
es
❑No
[]N/A
1.
Chain Of Custody Filled Out?
es
[]No
[IN/A
2
Chain -of CustodyRelinquished?
es
[]No
❑N A
3.
Sampler Name.and/or S nature on COC?
s
QNo
❑M/A
4.
Samples Arrived within Hold Time?
es
QNo
N/A
5.
Short Hold Time Analysis f c72 hr.)?
Yes.
No
N .A
6.
Rush Turn Around Time 'Requested?
QYes
o
ON/A:
7.
SufhclentVolume?.
es
QNo
N A
8.
Correct Containers Used?
es
K NSA
=Pace Containers Used?
QY
o
'ON/A
Containers Intact?
Y s
No
QN/A.
10.
Filtered Volume Recelved•for Dissolved Tests?
9Yes
❑No
N/A
11. Note If sediment is visible In the dissolved container
Sample Ubels.MatchCOC?
L.3'res
ON,
EqN/A
12.
-Mcludes Date/Time iD/Anal is Matrix:
All containers needing acid/base preservation have been
checked?
[]Yes
[]No
��,,�
►- KJA'
*-�'^
13.
All.containers needing preservation are found to be In
compllance with EPA recornrnendation?
(HNO3, H2SO4, H042; NaOli >9 Sulfide, NaOH>12 Cyanide)
E]Yea
E]No.
N/A
Exceptions: VQA, Collform, TOC; Oil and Grease,
D90/801S (water) DOC.0 Hg ...
❑Yes
ONO
111NIX
Samples checkedfordechlorination
(]No
A
14.
Head ace in VOA Vials >5-6mm ?
❑Yes
❑No
iS.
Trip Blank Present?
Oyes
QNo
N/
16,
Trip Blank Custody Seals Present?
Oyes
ON.
/A
-Pace Trip Blank Lot#(if urchased :
CLIENT NOTIMATION/RESOWTION
Person Contacted: Date/Time;
Comments/Resolution:
Field.Data Required? OYes ❑No
Project Manager. SCURF Review; Date:
'r'f /V%�
Project Manager SRF Review: //r Dale:
Note: Whenever there is a discrepancy affecting North Car— olI- ompiiante satrapies, a copy, of this form will beaent to the North Carolina
Out of hold, incorrect preservative; outof temp, incorrect container66
edification Office (i.e.
Page 23 of 24

Pon
Please- test the sample(s) for the parameters as,.
listed: below.
Send'original resultsUn. efnail: ricky_.styleS9baxt6r.com, & amanda richcreek@baxter..com,
Send invoice and, copy of restift to: email:: ([e-mail]
R16ky. Styles,
..:Baxter Biomass Purchas4 Ord 1.08107.
2859 iOld Linville, Rd.
Marlon, NC 28752
[phone]
A I I--
2,e 21. &74
tieqUeSteCl UUe
Sample 1)
date:
Sampkii
Sample. Date(s)
Grab or
Total Metals -
TCLP Metals -
I nitability,:
pH,
Total -Arsenic,
Nil I TCLP
Description
land time sample
Composite
As, B8, Cd,
As-, Baj Cd,
Reactivity
:CorrosiVity
collected -
Ca,,Cn Cu, Fei
�Cr, Pb, Hq,
:Pb, 09, Ng,
Sey Ag
Mnj Mo,,Nii K,.
Se, Aq,.Na,
Zn,IDtal
Phosphorus
NP3'3116A'
ASH,
-3-31-16 9:45AM.
OSITE-
COMPOSITE-
YES
'YES,
YES
YES
NP33116B
ASH •3-31
-I 6,9.45AM,
:COMPOSITE POSITE
YES
YES'
YES
.'.'YES.
Sample sent to:: Pace, Analytical Services,
2225'Riverside Drive
Asheville, NC 28804
'828-:254-7176
'Chain of Custody
Project Manager: Toni Williams
0806 Kincey,,Avenue, . Suite I OC
HUntersville,.'SIC ,28078
(704) 875- 9092 ext. 233
5t. 1.4

Baxter Biomass -Wood Boiler Ash - Ricky Styles
Please test the sample(s) for the parameters as
listed below.
Send -original results to: email: [e-mail] &[e-mail]
Send invoice and copy of results to: email: [e-mail]
Ricky Styles
Baxter Biomass Purchase Order # 108107
2859 Old Linville Rd.
Marion, NC 28752
[phone]
Reauested Due Date:
Ctamnlo Al 1 1 ICTR11
Sample #
Sample
Sample Date(s)
Grab or
Total Metals -
TCLP Metals
Ignitability,
pH
Total -Arsenic
Full TCLP
Description
and time sample
Composite
As, Ba, Cd,
As, Ba, Cd,
Reactivity
Corrosivity
collected
Ca, Cr, Cu, Fe,
Cr, Pb, Hg,
Pb, Mg, Hg,
Se, Ag
Mn, Mo, Ni, K,
Se, Ag, Na,
Zn, total
Phos horus
NP33116A
ASH
3-31-16 9:45AM
COMPOSITE
YES
YES
YES
YES
NP33116B
ASH
3-31-16 9:45AM
COMPOSITE
YES
YES
YES
YES
Sample sent to: Pace Analytical Services,
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Chain of Custody
Project Manager: Tom Williams
9800 Kincey Avenue, Suite 10C
Huntersville, NC 28078
(704) 875 - 9092 ext. 233
ti,►5

aceAnapical
►o wpacelabs.cam
July 06, 2016
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on June 15, 2016. The
results relate only to the samples included -in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample_analyte
.page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me. --
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
.' This. report shall, not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 1 of 22

aceAnalyiical
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E
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
Pennsylvania Certification IDs
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
L-A-B DOD-ELAP Accreditation #: L2417
Alabama Certification #: 41596
Arizona Certification #: AZ0734
Arkansas Certification
California Certification #: 04222CA
Colorado Certification
Connecticut Certification #: PH-0694
Delaware Certification
Florida/TNI Certification M E87683
Georgia Certification #: C040
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification #: 391
Kansas/TNI Certification #: E-10358
Kentucky Certification #: 90133
Louisiana DHH/TNI Certification #: LA140008
Louisiana DEQfrNI Certification #: 4086
Maine Certification #: PA00091
Maryland Certification #: 308
Massachusetts Certification #: M-PA1457
Michigan/PADEP Certification
Missouri Certification #: 235
CERTIFICATIONS
Montana Certification M Cert 0082
Nebraska Certification #: NE-05-29-14
Nevada Certification #: PA014572015-1
New Hampshire/TNI Certification #: 2976
New Jersey/TNI Certification #: PA 051
New Mexico Certification #: PA01457
New York/TNI Certification M 10888
North Carolina Certification #: 42706
North Dakota Certification #: R-190
Oregon/TNI Certification #: PA200002
Pennsylvania/TNI Certification #: 65-00282
Puerto Rico Certification #: PA01457
Rhode Island Certification #: 65-00282
South Dakota Certification
Tennessee Certification #: TN2867
Texas/TNI Certification #: T104704188-14-8
UtahfTNI Certification M PA014572015-5
USDA Soil Permit #: P330-14-00213
Vermont Dept. of Health: ID# VT-0282
Virgin Island/PADEP Certification
Virginia/VELAP Certification #: 460198
Washington Certification #: C868
West Virginia DEP Certification M 143
West Virginia DHHR Certification #: 9964C
Wisconsin Certification
Wyoming Certification M 8TMS-L
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification M E87627
North Carolina Field Services Certification M 5342
Kentucky UST Certification M 84
North Carolina Wastewater Certification #: 12
Virginia/VELAP Certification M 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification M 40
Florida/NELAP Certification M E87648
South Carolina Certification M 99030001
Massachusetts Certification M M-NCO30
Virginia/VELAP Certification M 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 22

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F
SAMPLE ANALYTE COUNT
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID
Method
Analysts
Analytts
Reported
Laboratory
92301490001 SP61516A
EPA6010
JMW, SH1
17
PASI-A
EPA6010
SH1
7
PASI-A
EPA 7470
SER
1
PASI-A
EPA 7471
WAB
1
PASI-A
ASTM D2974-87,
KDF
1
PASI-C
EPA 1010
MLS
1
PASI-A
EPA 9045
MLS
1
PASI-A
EPA365A
WRC
1
PASI-A
SW-846 7.3.3.2
PAS
1
PASI-PA
SW-846 7.3.4.2
PAS
1
PASI-PA
92301490002 SP615168
EPA6010
JMW, SH1
17
PASI-A
EPA6010
SH1
7
PASI-A
EPA 7470
SER
1
PASI-A
EPA 7471
WAB
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 1010
MLS
1
PASI-A
EPA 9045
MLS
1
PASI-A
EPA365.1
WRC
1
PASI-A
SW-846 7.3.3.2
PAS
1
PASI-PA
SW-846 7.3.4.2
PAS
1
PASI-PA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 22

;alce A nalXica I
7 WWW.P&DftbS.COM
ANALYTICAL RESULTS
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP61516A I Lab ID: 92301490001 Collected: 06/15/16 09:45 Received: 06/15/16 11:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
11.6
mg/kg
1.5
1
06/17/1619:20 06/19/1615:01
7440-38-2
Barium
1400
mg/kg
0.74
1
06/1711619:20 06/19/1615:01
7440-39-3
Cadmium
1.9
mg/kg
0.15
1
06/17/1619:20 06/19/1615:01
7440-43-9
Calcium
78400
mg/kg
148
10
06/17/1619:20 06/20/1618:37
7440-70-2
Chromium
21.0
mg/kg
0.74
1
06/17/1619:20 06/19/1615:01
7440-47-3
Copper
83.5
mg/kg
0.74
1
06/17/1619:20 06/19/1615:01
7440-50-8
Iron
10300
mg/kg
14.8
1
06/17/1619:20 06/19/1615.01
7439-89-6
Lead
27.0
mg/kg
0.74
1
06/17/1619:20 06/19/1615:01
7439-92-1
Magnesium
12500
mg/kg
14.8
1
06117/1619:20 06/19/1615:01
7439-95-4
Manganese
2930
mg/kg
7.4
10
06117/1619:20 06/2011618:37
7439-96-5
Molybdenum
1.9
mg/kg
0.74
1
06/17/1619:20 06/19/1615:01
7439-98-7
Nickel
19.4
mg/kg
0.74
1
06/17/1619:20 06119/1615:01
7440-02-0
Potassium
21 SW
mg/kg
7400
10
06/17/1619:20 06/20/16 18:37
7440-09-7
Selenium
ND
mg/kg
1.5
1
06/17/1619:20 06/19/1615:01
7782-49-2
Silver
ND
mg/kg
0.74
1
06/17/1619:20 06/19/1615:01
7440-22-4
Sodium
6310
mg/kg
740
1
06/17/1619:20 06/19/1615:01
7440-23-5
Zinc
227
mg/kg
1.5
1
06/17/1619:20 06/19/1615:01
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 06/20/16 23:13 Initial pH: 9.2; Final pH: 5.2
Arsenic
ND mg/L 0.050 V 1 06/21/1618:38 06/23/1616:08 7440-38-2
Barium
5.8 ✓ mg/L 0.25 1 06/21/1618:38 06/22/16,21:31 7440-39-3
Cadmium
0.023 ✓ mg/L 0.0050 1 06/21/1618:38 06/22/16 21:31 7440-43-9
Chromium
ND mg/L 0.025 / 1 06/21/1618:38 06/22/16 21:31 7440-47-3
Lead
ND mg/L 0.025 `� 1 06/21/1618:38 06/22/16 21:31 7439-92-1
Selenium
Silver
ND mg/L 0.10 ✓ 1 06/21/1618:38 06/22/16 21:31 7782-49-2
✓
ND mg/L 0.025 1 06/21/16 18:38 06/22/16 21:31 7440-22.4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 06/20/16 23:13 Initial pH: 9.2; Final pH: 5.2
Mercury
ND mg/L 0.00020 1 06/23/16 21:56 06/24/1613:05 7439-97-6
7471 Mercury
Analytical Method; EPA 7471 Preparation Method: EPA 7471
Mercury
0.0050 mg/kg 0.0042 1 06/17/16 22:00 06/21/16 13:28 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
42.7 % 0.10 1 06/17/16 09:12
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 J deg F 70.0 1 07/06/16 09:45
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
8.4 � Sid. Units 0.10 1 06/28/16 16:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 22

Wceftljdcale
www.pacetetiscmn
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i
ANALYTICAL RESULTS
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
oampre: oroloibA
Lab ID: 92301490001 Collected: 06/15/16 09:45
Received: 06/15/16 11:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
1720 mg/kg 34.9 10
06/17/1619:19 7723-14-0'
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND V mg/kg 1.7 1
06/22/16 00:19
735S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND V mg/kg 17.4 1 .
06/21/16 18:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 22

raceAnapcal e
www.pecslabs.com
s
i
ANALYTICAL RESULTS
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
Pace Analytical Services, Inc.
9800-KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
zampie: SP615160 Lab ID: 92301490002 Collected: 06/15/16 09:45 Received: 06/15/16 11:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
Barium
14.1
mg/kg
1.4
1
06/17/1619:20 06/19/1615:04 7440-38-2
Cadmium
1830
mg/kg
7.1
10
06/17/1619:20 06/20/1618:40 7440-39-3
Calcium
2.1
mg/kg
0.14
1
06/17/1619:20 06/19/1615:04 7440-43-9
Chromium
102000
mg/kg
142
10
06/17/1619:20 06/20/1618:40 7440-70-2
Copper
24.4
mg/kg
0.71
1
06/17/1619:20 06/19/1615:04 7440-47-3
Iron
113
mg/kg
0.71
1
06/17/1619:20 06/19/1615:04 7440-50-8
11900
mg/kg
14.2
1
06/1711619:20 06/19/1615:04 7439-89-6
Lead
31.9
mg/kg
0.71
1
06117/1619:20 06/19/1615:04 7439-92-1
Magnesium
17300
mg/kg
142
10
06/17/1619:20 06/20/1618:40 7439-95-4
Manganese
3460
mg/kg
7.1
10
06/17/1619:20 06/20/1618:40 7439-96-5
Molybdenum
2.0
mg/kg
0.71
1
06/17/161.9:20 06/19/1615:04 7439-98-7
Nickel
Potassium
23.1
mg/kg
0.71
1
06/17/1619:20 06/19/1615:04 7440-02-0
Selenium
25000
mg/kg
7110
10
06/1711619:20 06/20/1618:40 7440-09-7
ND
mg/kg
1.4
1
06/17/1619:20 06/19/1615:04 7782-49-2
Silver
ND
6230
mg/kg
0.71
1
06/17/1619:20 06/19/1615:04 7440-22-4
mg/kg
711
1
06/17/1619:20 06/19/1615:04 7440-23-5
Zinc
270
mg/kg
1.4
1
06/17/1619:20 06/19/1615:04 7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 06/20/16 23:13 Initial pH: 9.3; Final pH: 5.1
Arsenic
ND mg/L 0.050 / 1 06/21/1618:38 06/22/16 21:34 7440-38-2
Barium
7.8 -/ mg/L 0.25 1 06/21/16 18:38 06/22/16 21:34 7440-39-3
Cadmium
0.026 v' mg/L 0.0050 1 06/21/1618:38 06/22/16 21:34 7440-43-9
Chromium
ND mg/L 0.0251� 1 06/21/16 18:38 06/22/16 21:34 7440-47-3
Lead
Selenium
ND mg/L 0.025 ✓ 1 06/21/1618:38 06/22/16 21:34 7439-92-1
✓
Silver
ND mg/L 0.10 1 06/21/16 18:38 06/22/16 21:34 7782-49-2
ND ✓
mg/L 0.025 1 06/21/1618:38 06/22/16 21:34 7,440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 06/20/16 23:13 Initial pH: 9.3; Final pH: 5.1
Mercury
ND mg/L 0.00020 1 06/23/16 21:56 06/24/16 13:07 7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
ND mg/kg 0.0070 1 06/17/16 22:00 06/21/16 13:31 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
49.0 % 0.10 1 06/17/16 09:12
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F 70.0 1 07/06/16 09:45
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
8.4 Std. Units 0.10 1 06/28/1616:08
Date: 07/06/2016 05:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 22

lCeAnapical
:pawaba.com
i
i
ANALYTICAL RESULTS
Project: Wood BoilerAsh 6/15
Pace Project No.: 92301490
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP61516B Lab ID: 92301490002 Collected: 06/15/16 09:45 Received: 06/15/1611:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
365.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus 1360 mg/kg 39.2 10 06/17/1619:20 7723-14-0
733C S Reactive Cyanide Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive ND mg/kg 2.0 1
06/22/16 00:19
735S Reactive Sulfide Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive . ND I/ mg/kg 19.6 1 06/21/16 18:15
Date: 07/06/2016 05:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 22

aceAnalytical
t ww++:pacefabs.cam
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
QC Batch: MERP/9682 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92301490001, 92301490002
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1763243
Matrix: Water
Associated Lab Samples: 92301490001, 92301490002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
mg/L
ND 0.00020
06/24/1612:20
LABORATORY CONTROL SAMPLE:
1763244
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
mg/L
.0025
0.0023
94 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1763245 1763246
MS MSD
92301816005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND .0025 .0025 0.0024 0.0024 96 94 75-125 2
Results presented on this page are In the units Indicated by the 'Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 22

aceAna/Xical
WWW-Pscabbs.can
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
QC Batch: MERP/9614 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92301490001, 92301490002
METHOD BLANK: 1756887 Matrix: Solid
Associated Lab Samples: 92301490001, 92301490002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0050 06/21/1612:22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)B75.9092
LABORATORY CONTROL SAMPLE: 1756888
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury mg/kg .083 0.078 94 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1756889 1756890
MS MSD
92301372001 Spike Spike MS MSD. MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg ND .049 .048 0.032 .0025J 66 5 75-125 M1
Results presented on this page are in the units indicated by the 'Unite" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dater 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 22

aceAnalytical
ttww..pacdau.com
f
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
QC Batch: MPRP/22075 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 92301490001, 92301490002
METHOD BLANK: 1758321
Associated Lab Samples: 92301490001, 92301490002
Parameter
Units
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Iron
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Manganese
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Matrix: Solid
Blank
Result
Reporting
Limit
Analyzed
ND
1.0
06119/1614:25
ND
0.50
06/19/1614:25
NO
0.10
06/19/1614:25
ND
10.0
06/20/1618:06
ND
0.50
06/19/1614:25
ND
0.50
06/19/1614:25
NO
10.0
06/19/1614:25
NO
0.50
06/19/1614:25
ND
10.0
06/1911614:25
ND
0.50
06/19/1614:25
ND
0.50
06/19/1614:25
ND
0.50
06/19/1614:25
NO
500
06/19/1614:25
ND
1.0
06/19/1614:25
ND
0.50
06/19/1614:25
ND
500
06/19/1614:25
ND
1.0
06119/1614:25
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1758322
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Arsenic
mg/kg
50
50.8
102
80-120
Barium
mg/kg
50
51.0
102
80-120
Cadmium
mg/kg
50
52.0
104
80-120
Calcium
mg/kg
500
537
107
80-120
Chromium
mg/kg
50
51.4
103
80-120
Copper
mg/kg
50
51.4
103
80-120
Iron
mg/kg
500
516
103
80-120
Lead
mg/kg
50
51.5
103
80-120
Magnesium
mg/kg
500
511
102
80-120
Manganese
mg/kg
50
51.0
102
80-120
Molybdenum
mg/kg
50
54.3
109
80-120
Nickel
mg/kg
50
51.8
104
80-120
Potassium
mg/kg
500
511
102
80-120
Selenium
mg/kg
50
52.3
105
80-120
Silver
mg/kg
25
25.7
103
80-120
Sodium
mg/kg
500
515
103
80-120
Zinc
mg/kg
50
52.9
106
80-120
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units Indicated by the 'Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 22

aceAnc?6 cal
ww,ypaceiabs.cam
1
QUALITY CONTROL DATA
Project Wood Boiler Ash 6/15
Pace Project No.: 92301490
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1758323
MS
92298500001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1758324
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qua]
Arsenic
mg/kg
39.8
41.7
36.2
75.4
73.0
85
92
75-125
3
Barium
Cadmium
mg/kg
474
41.7
36.2
464
490
-24
43
75-125
5 M1
Calcium
mg/kg
226
41.7
36.2
228
256
3
82
75-125
12 M1
Chromium
mg/kg
149000
417
362
136000
.140000
-3130
-2570
75-125
3 M6
Copper
mg/kg
223
41.7
36.2
230
243
15
53
75-125
5 M1
Iron
mg/kg
758
41.7
36.2
694
785
-153
74
75-125
12 M1, M6
Lead
mg/kg
65500
417
362
64500
70000
-236
1250
75-125
8 M6
mg/kg
25300
41.7
36.2
31500
29600
14900
12000
75-125
6 M6
Magnesium
mg/kg
6990.
417
362
6640
6820
-85
-48
75-125
3 M1
Manganese
mg/kg
8370
41.7
36.2
13500
14000
12300
15500
75-125
3 M6
Molybdenum
mg/kg
16.9
41.7
36.2
52.1
49.7
84
90
75-125
5
Nickel
mg/kg
48.7
41.7
36.2
74.9
74.1
63
70
75-125
1 M1
Potassium
mg/kg
13000
417
362
ND
ND
-64
-7
75-125
M6
Selenium
mg/kg
4.2
41.7
36.2
41.2
37.8
89
93
75-125
8
Silver
mg/kg
35.4
20.8
18.1
50.5
52.9
72
97
75-125
5 M1
Sodium
mg/kg
9000
417
362
ND
ND
-206
-184
75-125
M6
Zinc
mg/kg
31500
41.7
36.2
132000
140000
242000
300000
75-125
6
Results presented on this page are In the units Indicated by the 'Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 22

aceAffiVical
/ W*WPBCei $.00M
i
QUALITY CONTROL DATA
Project:. Wood Boiler Ash 6/15
Pace Project No.: 92301490
Pace Analytical Services, Inc.
9800 KlnceyAve. Sufte 10o
Huntersville, NC 28078
[phone]
QC Batch: MPRP/22129
Analysis Method: EPA 6010
OC Batch Method: EPA 3010A
Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92301490001, 92301490002
METHOD BLANK: 1761146
Matrix: Water
Associated Lab Samples: 92301490001, 92301490002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Arsenic
mg/L
ND 0.050
06/22/16 20:37
Barium
mg/L
ND 0.25
06/22/16 20:37
Cadmium
mg/L
ND 0.0050
06/22/16 20:37
Chromium
mg/L
ND 0.025
06/22/16 20:37
Lead
mg/L
ND 0.025
06/22/16 20:37
Selenium
mg/L
ND 0.10
06/22/16 20:37
Silver
mg/L
ND 0.025
06/22/16 20:37
LABORATORY CONTROL SAMPLE:
1761147
Spike
LCS
LCS % Rec
Parameter
Units
Cone.
Result
% Rec Limits
Qualifiers
Arsenic
mg/L
2.5
2.5
100
80-120
Barium
mg/L
2.5
2.4
94
80-120
Cadmium
mg/L
2.5
2.5
98
80-120
Chromium
mg/L
2.5
2.4
94
80-120
Lead
mg/L
2.5
2.3
93
80-120
Selenium
mg/L
2.5
2.5
99
80-120
Silver
mg/L
1.2
1.2
98
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1761148
1761149
MS
MSD
92301920001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter
Units Result
Cone.
Cone. Result
Result % Rec %
Rec
Limits
RPD Qual
Arsenic
mg/L ND
2.5
2.5 2.6
2.7
105
106
75-125
1
Barium
mg/L ND
2.5
2.5 2.5
2.4
98
98
75-125
0
Cadmium
mg/L ND
2.5
2.5 2.6
2.6
103
103
75-125
1
Chromium
mg/L ND
2.5
2.5 2.5
2.5
97
98
75-125
1
Lead
mg/L 0.18
2.5
2.5 2.6
2.6
97
97
75-125
0
Selenium
mg/L ND
2.5
2.5 2.8
2.8
110
111
75-125
0
Silver
mg/L ND
1.2
1.2 1.3
1.3
102
102
75-125
0
Results presented on this page are In the units Indicated by the 'Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc..
Page 12 of 22

1-!;a1CeA178yb1
wwW-Poodabs.cem
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i
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
r,rc: tiatcn; PMST/9131 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92301490001, 92301490002
SAMPLE DUPLICATE: 1757883
Parameter
Percent. Moisture
SAMPLE DUPLICATE: 1757884
Parameter
Percent Moisture
92301559001 Dup
Units Result Result RPD Qualifiers
% 792 79.1 0
92301741013 Dup
Units Result Result RPD Qualifiers
% 23.4 23.0 2.
Pace Analytical Services, Inc.
9B00 Kincey Ave., Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc..
Page 18 of 22

ace Analytical"
_., tttnvp8celabs.com
i
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
QC Batch: WET/46042 Analysis Method: EPA 1010
QC Batch Method: EPA 1010 Analysis Description: 1010 Flash Point, Closed Cup
Associated Lab Samples: 92301490001, 92301490002
SAMPLE DUPLICATE: 1773189
92301490001 -Dup
Parameter Units Result Result RPD Qualifiers
Flashpoint deg F >200 >200
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented an this page are in the units indicated by the 'Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc..
Page 14 of 22

/--!;a1CeA17a1Xb1
i
w+vw.pei»labs.cam
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
QC Batch: WET/45856 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92301490001, 92301490002
SAMPLE DUPLICATE: 1767178
92301490001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 8.4 8.4 0
Pace Analytical Services, Itic.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc..
Page 15 of 22

ac,Mnalydical
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QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
QC Batch: WETA/27979 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92301490001, 92301490002
Pace Analytical Services, Inc.
9800 KlnceyAve. Suite 100
Huntersville, NO 28078
[phone]
METHOD BLANK: 1757161
Matrix: Solid
Associated Lab Samples: 92301490001, 92301490002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Phosphorus
mg/kg
ND 2.0
06/17/1618:50
LABORATORY CONTROL SAMPLE:
1757162
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Phosphorus
mg/kg
50 50.2
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1757163 1757164
MS MSD
92300323001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 1220 6600 6600 2980 3000 -3 -3 90-110 1 M6
Results presented on this page are In the units Indicated by the 'Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc..
Page 16 of 22

aceAnalyAcal
tvamxpacetebs.com
i
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
QC Batch: WETA/23970 Analysis Method: SW-846 7.3.3.2
QC Batch Method: SW-846 7.3.3.2 Analysis Description: 733C Reactive Cyanide
Associated tab Samples: 92301490001, 92301490002
METHOD BLANK: 1095809
Associated Lab Samples:
Parameter
Cyanide, Reactive
SAMPLE DUPLICATE: 1095810
Parameter
Cyanide, Reactive
Matrix: Solid
Blank
Reporting
Units
Result
Limit Analyzed Qualifiers
mg/kg
ND
0.99 06/22/16 00:19
30186859005
Dup
Units
Result
Result RPD Qualifiers
mg/kg
ND
ND
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the: result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc..
Page 17 of 22

.,!;aceAnalytical
t 1v44g1:�8C818bS.COm
i
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
QC Batch: WETA/23973 Analysis Method: SW-846 7.3.4.2
QC Batch Method: SW-846 7.3.4.2 Analysis Description: 734S Reactive Sulfide
Associated Lab Samples: 92301490001, 92301490002
METHOD BLANK: 1095817 Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfide, Reactive mg/kg ND 9.9 06121/1618:15
SAMPLE DUPLICATE: 1095818
30186859005 Dup
Parameter Units Result Result RPD Qualifiers
Sulfide, Reactive mg/kg ND ND
Pace Analytical Services, Inc.
9860 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the unite indicated by the 'Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/06/2016 05:48 PM without the written consent of Pace Analytical Services, Inc..
Page 18 of 22

aceft ytical
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QUALIFIERS
Project:. Wood Boiler Ash 6/15
Pace Project No.: 92301490
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite too
Huntersville, NC 28078.
[phone]
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-PA Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
Mi Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
Date: 07/06/2016 05:48 PM
REPORT OF LABORATORY. ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 22

!2ceAnayical
r www.p Wabs.can
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Wood Boiler Ash 6/15
Pace Project No.: 92301490
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92301490001
SP61516A
EPA 3050
MPRP/22075
EPA 6010
ICP/19745
92301490002
SP61516B
EPA 3050
MPRP/22075
EPA 6010
ICP/19745
92301490001
SP61516A
EPA 3010A
MPRP/22129
EPA 6010
ICP/19768
92301490002
SP61516B
EPA 3010A
MPRP/22129
EPA 6010
ICP/19768
92301490001
SP61516A
EPA 7470
MERP/9682
EPA 7470
MERC/9313
92301490002
SP61516B
EPA 7470
MERP/9682
EPA 7470
MERC/9313
92301490001
SP61516A
EPA 7471
MERP/9614
EPA 7471
MERC/9252
92301490002
SP61516B
EPA 7471
MERP/9614
EPA 7471
MERC/9252
92301490001
SP61516A
ASTM D2974-87
PMST/9131
92301490002
SP61516B
ASTM D2974-B7
PMST/9131
92301490001
SP61516A
EPA 1010
WET/46042
92301490002
SP615168
EPA 1010
WET/46042
92301490001
SP61516A
EPA 9045
WET/45856
92301490002
SP61516B
EPA 9045
WET/45856
92301490001
SP61516A
EPA365.1
WETA/27979
92301490002
SP61516B
EPA365.1
WETA/27979
92301490001
SP61516A
SW-6467.3.3.2
WETA/23970
92301490002
SP61516B
SW-846 7.3.3.2
WETA/23970
92301490001
SP61516A
SW-846 7.3.4.2
WETA/23973
92301490002
SP61516B
SW-846 7.3.4.2
WETN23973
Date: 07/06/2016 05:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 20 of 22

� Document Name: Document Revised: May 24, 2016
aeeAna�ytfcal Sample Condition Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-ASV-CS-003•Rev.20 Pace Asheville Quality Office
Condition Uporim Client blame:
6— Receipt Projec
Courier: ❑Fed Ex DUPS ❑LISPS
❑ Commercial ❑Pace ❑Other:
Custody Seal Present? ❑Yes pfdo Seals Intact? QYes
P
Page 2 of 2 for Internal Use ONLY
W0#:92301490
111111011111111111111
92301490
iDate/initials Person Examining Contents:
ac g Material: ❑Bubble Wrap ❑Bubble Bags None ❑.Other:
T rmometer: •-
IRGun #S SN:15527198 Type of Ice: ❑tNet ❑Blue one ❑Samples on ice, cooling process has begun
Correction Factor: 0.01C Cooler Temp Corrected (•C): ( Biological Tissue Frozen? ❑Yes ❑No N/A
Temp should be above freezing to 6°C
USDA Regula d Soil (❑ N/A, water sample)
Did sampleoriginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Aid samples originate from a foreign source (intern 'Wally,
❑Yes NO _
_
moumrtg ndwa!i and ruerio {ocofr uyes WNo
Comments/Discrepancy:
Chain of Custody Present?
es
[]No
❑N/A
1.
j Samples Arrived within Hold Time?
0<s
[IN., N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
No
,,.(_]N/A
3.
Rush Turn Around'Tfine Requested?
❑Yes..
6o
❑N/A
4.
Sufficient Volume?
©Yes
[]No.
❑N/A
5.
Correct Containers Used?
Yes'
[]No
❑NIA
6.
-Pace Containers Used?
(7J�', s"..
❑No
❑N/A
Containers Intact?
Yes
[]No
❑N/A,.
7.
, Samples Field Filtered?
❑Yes
❑No
NJA
B. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
VYes
[]No
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix: 145 L'
All containers needing acid/base preservation have been
10. H�{p3
checked?
❑Yes
[]No
N/A
pH<t
All containers needing preservation are found to be in
HOpH<z
compliance with EPA recommendation?
HzswpH<:
(HNO3, HZS04, HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide)
❑Yes
❑No
gIINIIA
Exceptions: VOA, Coliform, TOC Oil and Grease,
eraatpwtz
ORO/8015 (water) 0OC,LLHg
❑Yes
[]No
I H
t"'DH/Zn0k pH>9
Samples checked for dechlorination?
❑Yes
[]No
/:a-
11.
Headspace in VOA Vials (>5-6mm)?
❑Yes
allo
NIA.
12.
Trip Blank Present?
❑Yes
[]No
/1C"
13.
Trip Blank [ustodySeals Present?
QYes
[]NO.
N/A
Pace Trip Blank Lot # (if purchased):
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:,
Project Manager SCURF Review:
Field Data Required? ❑Yes []No
Date/Time:
Date: G/&/ram
Project Manager SRF Review: �^— Date. ( d t: /
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Car Una OEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 21 of 22

Baxter Biomass - Wood Boiler Ash. - Ricky Styles
Pleasetest the sample(s) for the .parameters as
listed below.
Send original results to. email: [e-mail]
Send invoice and copy of results to: email: [e-mail]
Ricky Styles
Baxter Biomass Purchase Order # 113488
2859 Old Linville Rd.
Marion, NC 28752
[phone]
q;. 30 1 'fq o
N
N
O
N
N
N
cm
0—
Requested Due
Sample #
Date:
Sample
Description
Sample Date(s)
and time sample
collected
aam
Grab or
Composite
le ALL L,O r
Total Metals -
As, Ba, Cd,
Ca, Cr, Cu, Fe,
w
TCLP Metals
As, Ba, Cd,
Cr, Pb, Hg,
Ignitability,
Reactivity
pH
Corrosivity
Total -Arsenic
Full TCLP
Pb, Mg, Hg,
Se, Ag
Mn, Mo, NI, K,
Se, Ag, Na,
Zn, total
Phos horns
SP61516A
ASH
6-15-16 9:45AM
COMPOSITE
YES
YES
YES
YES
COMPOSITE
YES
YES
YES
YES
SP61516B
ASH
6-15-16 9:45AM
Sample sent to: Pace Analytical Services,
2225 Riverside Drive
Asheville, NC-28804
828-254-7176
Chain of Custody
Project Manager: Tom Williams
980o Kincey Avenue, Suite 10(
Huntersville, NC 28078
(704) 875 - 9092 ext. 233
0 15
►0
M

Section 4 Ash Receiver
Signature Sheets
Signed Ash Distribution
Information Sheets

Baiter Healthcare,,,or
.2859 Old Linville Load:
M anion; l�Tortli Carolina 28752
Ash I;itiPibution Utilization Agreement -(Valid: thru .11/307.1:9) Baxter Copy-
Baxter, Healthcare Corp.,
, is the generator of the ash .provided"to (Recipient)..
Application of the. aforementioned ash is prohibited' except -in accordance with the instructions on this sheet.
Transport:_ Adequate provisions shall be taken to ensure.that the transportation.of ash does not cause,nuisances and
hazards to public health.andaafety;or.othervvise cause an adverse impact (e.g. transport wet. ash ,in leak:proof.truchs
or cover dry. ash).._M5
Storage: The ash shall be adequately stored" to prevent wind' erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash ,slightly moistened will accomplish this objective ,under normal .conditions.
However, berms, barriers; or tarps,'may be necessary under windy or rainy conditions.or if erosion or runoff cannot
be controlled.
Application When using ash,,the following shall. apply-:° _
• The ash application rates shall be limited to those that canbe agronomically justified (i.e., liriiited to .that needed
to:meet the liming.requirements of the -crops be_ ing grown pn theaand)..:: .
• Ash 'shallnot be placed within one:foot'of:the'seasonal high water table: .
• Ash shall not -be placed within 1.00 feet of any water supply'well or spring unless underlain and:overlain by,a =
liner -with a maximum hydraulic* conductivity of 10"6 centimeters per second. If such a liner/cover is .provided,
ash shall not be placed within 25 feet of any supply well or spring. .
„ Y
• The. ash shallnot be applied to any. site. that -is flooded; frozen; or snow-covered.
A .summary of the ash chemical analyses is located- on page 2 of the information sheet.. Detailed laboratory, results .
are available upon request:
-Title to the ash will transfer from Baxter Healthcare,. Corp .to Recipient upon delivery thereof. Thereafter; Baxter
-Healthcare, Corp will have no responsibility and shall notbe-held.liable by Recipient or any third.partyfor any spill,
misuse, misapplication or other: mishandling of the: ash.. Recipient acknowledges and agrees that the ash is -being
delivered by Baxter -Healthcare, Corp to Recipient..as.an accommodation to Recipient.:: In exchange 'therefore,
Recipient agrees to indemnify, save and :hold .Baxter Healthcare; Corp harmless from and against any and all.: =
liability,' damage; loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery .
asserted against Baxter Healthcare, Corp by any third: party, including: any governmental authority, whether for
bodily injury (including death) or damage to property,' arising from or in connection with Recipient's receipt, "
transportation, handling or other use of the.ash.
Signed (Ash Recipient): Date::
Ash Recipient's Address:
T.
Intended Use of Ash: -J f
lea"
Expected Qty/Yr: Acres of Land:
Baxter Representative Signature:
Pago2of 3,...
Updated: .11-07.14 .

Baxtep Healthcare; Corp,
2859 Old -Linville Load.
MarioniAorth Carolina 287.52
_ Ash Distribution Utilization Agreement (Valid thru-11/30119), Baxter.Copy
Baxter Healthcare- Corp., is the generator of the ash:providedao 4,.6w� . _ O n L . (Recipient).. -
Application of the aforementioned.ash is prohibited except in.accordance with the instructions on this sheet:
Trans
port:.Adequate provisions shall;be taken to ensure that the'transportation of ash does not cause nuisances and
hazards to public health and. safety. or. otherwise_.cause an :adverse impact (e:g:; transport wet ash In. le trucks
= or cover dry: ash).. ^ k �ti .1 • iS ^i
Storage._ The ash shall be adequately stored -to prevent: wind erosion'or surface runoff from carrying ash into any .
surface waters. Keeping the ash. slightly moistened, Will accomplish this - objective under normal . conditions.
However, berms; barriers; or tarps, may be'necessary under windy or rainy -conditions -or if erosion or runoff cannot
be controlled.
q.
Application: When using ash,.the.following shall apply:
t The ash application rates shall be hmited'to those that can be Agronomically' -justified (i.e., limited to that needed
to: meet the liming requirementstof the clops being grown_ on the.land)..
o : Ash shall not be placed within one foot of the seasonal high water table:
o Ash_ shall not: be placed within 100 feet of any water supply well or spring unless underlain and: overlain. by a
linei with a'maximum hydraulic.conductiyity of 10-6 centimeters per second. If alines/cover is provided,
ash shall not -be laced within 25. feet of an ,water-s- 1 well or spring.
P Y uPp Y. P. .g
o The: ash shall not be a d to an site: that is flooded frozen, . _ .. PP �lieY � en; or snow-covered.::.
A summary of the ash chemical analyses is located on page 2' of the information sheet. Detailed laboratoryresults -
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon .delivery thereof. Thereafter,- Baxter.
Healthcare, Corp will• have no responsibility and shall not held liable by -Recipient or any thir_ d-party for any.spill,
misuse, ."misapplication or other- mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to .Recipient as -an. accommodation to Recipient: In exchange therefore, .
Recipient a ees to - indemnify" save - and .hold .Baxter Healthcare;*. . Corp
p gr , , _ harmless from and against: any. and all.
liability, dama a loss cost ex ease. uicludin ' attorrie s' fees 'claim;. demand. suit; action; judgment or recovery
g , , P, (� g Y )'
asserted against Baxter- Healthcare; .Corp by any third party, including any _governmental authority, whether for
bodily injury (including death) or damage to. property, arising from or in connection with Recipient's receipt,
transportation, handling or other -use of the.ash.
Si ed Ash Rep i ient : _� ; : Date
-Ash Recipient's Address: 1 1 - aIf
Intended Use of Ash::. p
Expected Qty/Yr: Acres -of Land::
e�
-Baxter Representative Signature::
Page 2 of . 3
... • . .Updated; a l 07.14 . - .

'Baxter Healthcare for. o
p
ill - -. 2859 -Old Lin v.. , e Road:
Marion, North- Carolina 28752=
Ash Distribution Utilization Agreement (Valid thru 11/30/19); Baxter Copy =
Baxter Healthcare, Corp.; is. the generator of the=ash provided to hV�y (Recipient).. -.
Application of the. aforementioned ash is prohibited except in accordance with -instructions on thus sheet.
Transport:. Adequate provisions shall be taken to ensure: that the transportation.of ash does not cause nuisances and
"hazards to public.health:and:safety.or.otherwise.cause an adverse.impact(e.g.; transport wet. ash.in.leak-proof trucks.
or "cover dry: ash)...
Storage: The ash shall be adequately stored to prevent wind erosion or surface .runoff from carrying ash into any
surface-waters..Keeping the ash "slightly moistened will accomplish this objective under normal .conditions.
However, -berms, barriers, of tarps; may be necessary under windy or rainy conditions or if erosion or runoff cannot-
be'controlled.
Applicatiori:.When using ash,.the-following shall apply:
• The ash application rates shall be limited to those that can.be agronomically justified (i.e., limited to.thatneeded
to:meet the liming requirements -of the crops -being grown on theaand):.:
ft
MEMO
• Ash shall not be placed within one:foot.of the seasonal high water table. .
• Ash. shall -not be placed within 100 feet of any water supply well or spring unless underlain and -overlain by.a'..
liner.with a maximum. hydraulic_ conductivity of 10"6 centimeters per second: If -such a liner/cover is .provided,
ash shall not be -placed within 25. feet of any water'supply well or spring. .
• _ The ash shall not be applied to any site_ that is flooded; frozen, or snow=covered:
-A summary of the ash chemical analyses is located on page 2 of the information sheet Detailed laboratory results
are available upon request.
Title -to -the -ash will transfer from -Baxter Healthcare, Corp to Recipient upon delivery thereof Thereafter, Baxter
Healthcare, Corp will"have no responsibility and shall'not be held liable.by Recipient or any third partyfor. any spill,
misuse, :misapplication or other mishandling of the ash.. Recipient acknowledges and agrees that the ash is being '
delivered by Baxter. Healthcare, Coip to Recipient. as: an- accommodation to Recipient: In exchange 'therefore. -
Recipient agrees to -indemnify, . save: and .hold . Baxter Healthcare; .Corp harmless ,from and, against any and all
liabil#y,'dama e, loss, cost, expense (including attorneys'' fees), `claim,. demand, sui action ud ent of reco'
g_ j very
asserted. against Baxter Healthcare,. Corp by any third party; :including any governmental authority, whether for
bodily injury (including death) or damage to properly, arising from. or in connection with Recipient's receipt,
transportation, :handling a or.other
�use f the ash. .
Signed (Ash Recipient): �J a 1 I �S "Date:
®`� /' /� / Ash Recipient's'Address: - I ./ . �{ J (. -�W
Intended tJse"of Ash: FOI�����.®/ .1(: �!1 /��
Expected' Qty/Yr: �60 Acres of Land:
Baxter Representative Signature:
page 2 of 3
1
Updated: 1-07-14 _

Baxter Healthcare, Corpe
2859 Old Linville road
Marion, North Carolina 28752
Ash Dicta ibutIlon Utilization Ag'eeMi o'nt (Valid thru 11/30/19), -Baxter Copy
Baxter Healthcare, Corp.; is the generator of the ash provided to
Application of the aforementioned ash is prohibited except in Reci :
®sir d� )
accordance with the instructions on this sh(. P lenteet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and'
hazards to public health and safety or otherwise cause an adverse impact (e g ,transport wet ash in leak -proof trucks
f. .. „ .a... f or cover (Iry ash).
Anv=m�tit.��,•,,Ma..:::a::ee .�.:.. __�_ . _ . .
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from, carrying ash into any
surface waters. Keeping the ash slightly moistened will -accomplish this objective under normal conditions.
However, .berms, barriers, or tarps, may be necessary under windy or rainy, conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (Le.; limited to that needed
to meet the limingrequirements of the crops being grown on the land).rt� `
> 11ot be stoc algid for more Chant ' � -,
< �. .,,� t�i days prspr to las►d appheattoti
:Atihlic�tion'.af.Bulk:recte3�iaiYc`chall�:i;i,,,Y...r�.,st,;;.aiins ...._c_ _�, •,.,1 --"�' �:�-'. , . ---.
.; � •»,,Y� �u• ,�, vsa�,�.auvn.eesment�sltatt^ auauntalned_at they -land appl%atlora sateen btu �esttl�ls;_ate
,gn�apphedt
• Ash shall not be placed witlifin one foot of the seasona111igh, water table.
+ Ash shall not be placed within 100 feet of any water supply well or spring unles
liner with a maximum hydraulic s underlain and overlain by a
capductivity of 10� centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is looted on page 2 of the information sheet, Detailed_laboratory results'
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not beheld liable by Recipient or any third party for any spill;
misuse, .misapplication or other mishandling of the ash. Recipient acknowledges and agrm that the ash is being
delivered by Baxter Healthcare, Corp to Recipient- as an accommodation to Recipient.. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, 'suit, 'action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, "including any governmental authority; whether for
bodily injury (including death) or damage to property; arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient): „��, / Date:/p--/�
Ash Recipient's Address:��} ..«� .
js
Intended Use of Ash: L
Expected Qty/Yr: J
2,LA9F_eoaf Land:
Baxter Representative Signature:
Page of -3
Updated: 11-07=14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to >on' YdWA (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instruct'ons on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash) Any spill occurring white ash ts;in transport or -on the application, Jelds is,"the°responsibility of t} e.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient):
Ash Recipient's Address:
Intended Use of Ash: k'_/t
Date: �-
Expected Qty/Yr: �(� `�o.� Acres of Land:
Baxter Representative Signature: ?�'
a
Page 2 of 3
Updated: 11-07-14