WQ0010689_Annual Report_20160227

Annual Report Review Class A 4stribution
1. Class A Annual Distribution and(Marketing/Surface Disposal Certification Form
® Was a certification form submitted? Ye�5
® Was distribution conducted during the reported year? y z r
® How many dry tons were- distributed? j 1 S 70 VZ
e Were. the distributions within the permitted amount? ye r
e Were recipients information listed? je
® Did it indicate compliance? yO_S
® Was form complete? Ye
® Was it signed by the appropriate people? Ya
2. 1Monitoring -
® Were the analyses conducted at the required frequency?Y e5
® Were the metals analyses reported on the Residual. Sampling'Summary Form? Y�
m Were the results reported in mg/kg?
® Were the metals within ceiling concentration permit limits? � &5
® Were the metals within monthly average concentration permit limits).a
® If no, were the lab analyses. attached?
m Were all the required parameters tested? yeS
® Was TCLP analysis conducted? too V'nV V414 Of-w-& T"PLr fvt+-A�'.t
Were the TCLP contaminants within regulatory limits? Nik
3. Pathogen and Vector Attr on Reduction
Was a signed cop the Pathogen and Vector Attraction Reduction Form submitted?
® Did the form ' crate the period of coverage, the residual class, and the pathogen reduction alternative and the
a li
vector on reduction option used?
® Was t appropriate documentation to show pathogen and vector attraction reduction included in the report?
® W pathogen and vector attraction reduction demonstrated according to 40 CFR Part 503 or 2T?
4. General
Was the report in the proper format? j"_5
o Were any parts of the annual report missing? NQ .
® Was the report submitted on time? 110-5
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Baxter
2/17/2016
NCDENR - DWQ
Aquifer Protection Section
Land Application Unit
1636 Mail Service
Raleigh, NC 27699
RE: 2015 Annual Ash Report
Permit No. WQ0010689
Wood Boiler - North Cove, NC
Enclosed is the annual ash distribution report for the calendar year 2015, using the forms
provided by NCDENR-DWQ.
If you have any questions or require additional .information, please contact Amanda Richcreek at
828.756.6809.
I certify, under penalty of law that the above information is, to the best of my knowledge and
belief, true, accurate and complete. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
Sincerely,
J. � an1WP--e-i11`e1-r-
Plant Manager
f tE.0 1 ., _i_J
Division of Water Resources
MAR - 1 .2016
Water Quality Regional Operations
Asheville Regional Off,:(;
Cc: NC Division of Water Quality (3 additional- copies with enclosures)
Ricky Styles
Baxter Healthcare Corporation
PO Box 1390, Marion, NC 28752
T 828.756.4151

Section 1:Fo.rm DM:-S.D`F

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0010689 FACILITY NAME: Baxter Healthcare Corporation North Cove Steam Generation Plant Ash
PHONE: [phone] , COUNTY:: McDowell OPERATOR:. Baxter Healthcare
FACILITY TYPE (please check one): � ❑ ''Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
0 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 0 No ❑ --► If No slap parts A B C and certify f b 1
Part A*:
rt
orm a ow
t
B*:Par
Sources s include NPDES # if Volume, (dry tons)
O C.
Recipient Information
Month Amendment/
applicable) Residual In Product Out
Bulking Agent
Names)
Volume (dry tons )
Intended use s
O
January.
..See DMSDF sheet
February
supplemental for
March
breakdown
April.
May.
June
DivislE
, M M.,
Jul
August
_ 1 201
September
October
November
Water Qu
llhf Regions
a 1
December.
As,
vu;e t------
. Total from.FORM DMSDF. (sup) = 23547 i 1r251 1"4 70 <>
.r 8 2` v
-
.. ,.
Totals. -� z��- �.. - w
Annual �` , `b ,, r - t. st :> Y:rx>v v az. - r
• 23'S 47
( 1251 55. -1487 02. x<; << s<;< v< t>, _ r z
d tons d - s, c,w fy �' 1?4 sfik€"''$ tf
. _ `.. s :. 87.02'
Amendments used: Bulkin A gent(s) s used: Dry Wood' Chi s
* If more space is required, attach additional information sheets (FORM DMSDF (supp)). Total Number of Form DMSDF (Supp) 1
P C�
a
Facility was compliant during the past calendar year with all conditions of the land application permit p Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No —�: If No, Explain in Narrative
1: All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received.from the Division of Water Quality.
3. No contravention of Ground Water Quality. Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Z lM/
Signature Permittee Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature of Preparer** Date
(if different from.Permittee)
DENR FORM DMSDF (12/2006)

Section 2 Form RSSF
Annual Residual
Sampling Summary
Form and Form. B:

CLASS A ANNUAL DISTRIBUTION. AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0010689 FACILITY.NAME:�� Baxter Healthcare Corporation:.North Comae Steam Generation Plant Ash
PHONE: [phone] COUNTY: , McIDow,ell OPERATOR• J,B_ axter Healthcare
FACILITY TYPE (please check one): :0 Surface Disposal (complete Part A - "Month", '-'Source(s)" and "Residual In" columns only)
Distribution and, Marketing (complete Parts
Part A*: .
A, and B)
Part B*:
Month
Sources(s) (include NPDES:# if.
applicable)
Volume'(dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Names
Volume (dry.
-tons)
Intended uses)
March.
WQ0010689.
49.47,
313.38
392.85..
Dean McClure
362.85
Land Application
March.
WQ0010699
0.53
3.39
3.92
Frankie Marlowe
3.02
Land Application
April
WQ0010689
10.00
34.25
44.25
Terry English
44.25
'Lan dd Application
April
WQ0010689
10.00
34.25
44.25
Daniel Ray
44.25
Land Application
July...
WQ0010689
33.60
382.20
415.80
Dean McClure
415.80.
Land Application
August
WQ0010689-
6.40
72.80 ,
79.20
Emily McFalls
79.20,
Land Application
Dec
Dec
WQ0010689
WQ0010689
70.00 .
55:47
229.45
18.1.93
299.45
231.30'
Paul Boone
Dean McClure
299.45
237.30
Land Application
Land.Application
Totals:
Annua1 (dton
354,
12.1 -
.< � 'Wood
Amendments used: Bulkin 'A ent s used: D Chips
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 1
DENR FORM DMSDF (Supp). (12/2006)

ANNUAL RESIDUAL SAMPLING* SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in F.ORM RSSF - B
WQ Permit Number: WQ0010689 Laboratory:
Baxter Healthcare Corporation North Cove
Facility Name: Steam Generation Plant Ash
Residual Source WQ # or WQ0010689
NPDES.#e '
WWTP Name: NA
Residnal Annlvcic Data
1) Pace Analytical Services.
Cone.
Sample:or Composite Date
Parameter
Limit
(mg/kg)
a:
SP22615A
SP22615B
NP61615A
NP61615B
SP i029 i SA
SP 102915B
m
Percent Moisture (%)
NA
32.9
31.7 V1.
40.6
39.9 ✓
41.4 V:
39.4
Arsenic
75 ;
4.1
3..0 +/ ...:
4.5 -.
4.4 d
4 v ...
3
Cadmium
85
1.2 ✓
0.95 ✓.
2.2 ✓
1.4
0.78
0.7v
Copper.
4,300
66.6
61.19 �1
77.4
59..3 ✓
72 ✓
68.4 v
Chromium
NA
18.6 ✓
16.2 ✓
14.2 ✓
14.6 v
20.1 V:
21:1 V. .
Lead.
840.
18.3 v
16.4 ✓
27 V
19.4 ✓:
13.9 ✓
15.1
Mercury.
57
ND V
ND V..
NDweND
V
ND ✓
ND ✓
Molybdenum.
75
1.3 V
1.1 ..
2
1.6 V
0.51 V'
0.45 ✓
Nickel
.420,
20.5 ',✓
17.4 V
16:9 k/
16 V18.1
✓
17.5
Selenium
100 -
ND 4/
ND
ND
ND
1 3 .
Zinc.
7,500
173 ;�
152 %e
2 10 ✓'
1 93 V
1 47 ✓
1 29 +✓:
Total Phosphorus
NA
1960 ,/
1630V :
2700 -1
2750✓
1370.✓
1430
Barium .
NA _
1380 R°
142.0 V
128.0d
1220 ✓
815 V. .
765 V. .
Calcium . .
NA
82700
69200. ✓ .
74900 ..
7160.0 ✓
. 4570.Of _
37400 ✓
Iron :
a,.
NA.
130.00
.. -
12200 �''.: _
...
9160.
..
9620 if..
9T20` .
8730 ✓'
i_vi buiiauc UlbpUbai iacuiuca Luc cenmg concentration nnuts ustea in mis Corm_ are not applicable. Reference the individual permit for metals. limits.. ('Cl certify, under penalty of law, that this document was prepared. under my direction: or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted.. I am aware that there are significant
penalties for submitting false information, including the possibility .of fines and imprisonment for knowing violations."
.4_
cam.
2/1�zb6
Signa \ e of Prepares * Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters 'not listed in FORM RSSF that are part of the. WQ permit or were analyzed for over the past
calendar year: Use additional forms as needed.
WQ Permit Number: WQ0010689 Laboratory: 1) Pace Analytical Services .
Baxter Healthcare Corporation North Cove
Facility Name: Steam Generation Plant Ash 2)
Residual Source WQ0010689 3)
NPOES # or WQ#: 4)
WWTP Name: NA 5)
Residual Analvsis Data
Parameter
Sample or .Composite
Date
�m1g)
SP22615A
SP22615B
NP616115A
NP61615B
SP102915A
SP102915B
Magnesium .
20100 `/
17600
14400 ;�
14800 �
11400
6990 ✓`
Manganese .
2810'�
2440v
2480 V .
2480 'A
1360 1(
1.3 90 %
pH'..
Potassium ...
11.8 '� ..
N a' 0
1.1.8.E
17000 V
9.2. %e
1950.67
19400
ND ✓
ND
Silver
2:4 . rs .
2: `�
1.5 .
1.5,
1. v'
2.
Sodium
4540 V
37801/..
4030.V
4160.E
63 40
64 20
6GI, certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel_ properly gathered and evaluated the information submitted. I ani aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signs r of Preparer *, Date
*Preparer is defined in 40 CFR Part 503.:9(r) and 15ANCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

F--ebrvary'2�0�15:.

Pace Analytical Services, Inc.
® KinceyAve. Suite 100
�+ 9
�Ce a�yt�Ca� 800Huntersville, NC 28078
www.paeelabaoom
(704)e75-9092
ANALYTICAL RESULTS
Project: Wood Boiler.Ash 2/26
Pace Project No.: 92238940
sample: SP22615A
Lab ID: 92238940001 Collected: 02/26/15 09:45 Received: 02/26/15 11:59 Matrix: Solid
:Results reported on a ' dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units-
Report Limit DF
Prepared Analyzed CAS No. Qual
6010 MET=ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
4.1' mg/kg
1.4 .1
02/27/1516*50 02/27/15 2066 7440-38-2
Barium
1380 mg/kg
0.70 1
02/27/15 15:50 02/27/15 20:16 7440-39-3
Cadmium
1.2 mg/kg
0.14 1
02127/1515:50 02/27/15 20:16 7440-43-9
Calcium
82700 mg/kg
141 10
02/27/1515.50 03/02/1513:30 7440-70-2
Chromium
18.6 mg/kg
0.70 1
02/27/15 15:50 02/27/15 20:16 7440-47-3
Copper
66.6 mg/kg
0.70 1
02/27/15 15:50 02/27/15 20:16 7440-50-8
Iron
13000 mg/kg
14.1 1
02/27/15 15:50 02/27/15 20:16 7439-89-6
Lead
18.3 mg/kg.
0.70 1
02/27/15 15:50 02/27/15 20:16 7439-92-1
Magnesium
20100 mg/kg
141 10
02127/1515:50 03/0211513:30 7439-95-4
Manganese
2810 mg/kg
7.0 10
02127/1515:50 0310211513:30 7439-96-5
Molybdenum
1.3- mg/kg
0.70 1
02/27/151&50 02/27/1520:16 7439-98-7
.Nickel
20.5 mg/kg
0.70 1
02127/1515:50 02/27/15 20:16 7440-02-0
Potassium
20400 mg/kg
7030 10
02127/1515:50 03/0211513:30 7440-09-7
Selenium
ND mg/kg
1.4 1
02/27/1515:50 02/27/15 20:16 778249-2
Silver
- 2.4 mg/kg
0.70 1
02/27/15 15:50 02/27/15 20:16 7440-22-4
Sodium
4540 mg/kg
-703 1
02/27/15 15:50 02127/1520:16 7440-29-5
Zinc
173 mg/kg
1.4 1
02/27/15 15:50 02/27/15 20:16 7440-66-6
6010 MET ICP, .TCLP
Analytical -Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311;
03/02/15 15:30
Arsenic
ND mg/L
0.050 1
03/03/1513:05 03/03/15 20:16 7440-38-2
Barium
3.1 mg/L
0.25 1
03/03/15 13:05 03/03/15 20:16 7440-39-3
Cadmium
-ND mg/L.
0.0050 1
03/03/15 13.05 03/03/15 20:16 7440-43-9
'Chromium
ND mg/L
0.025 1
03/03/15 13:05 03/03/15 20:16 7440-47-3
Lead
ND mg/L
0:025 1
03/03/15 13:05 03/03/15 20:16 7439-92-1
Selenium
ND mg/L
0.10 1
03/03/15 13:05 03/03/15 20:16 7782-49-2
.Silver
ND mg/L
0.025 1
03/03/15 13:05 03/03/15 20:16 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 03/02/15 15:30
Mercury
'ND mg/L
0.00020 1
03%03/15 15:30 03/04/15 12:14 7439-97-6
7471 •Mercury
Analytical Method: EPA 7471 Preparation Method:, EPA 1471 .
Mercury.
ND mg/kg
0.0056 1
03/03/1518:00 03104/1513:26 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
32.9 %
0.10 1
03/02/15 10:13
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
11.8 Std. Units
0.10 1
03/03/15 11:15
365.1-Phosphorus, Total-
Analytical Method: EPA 365.1
Phosphorus
1960 mg/kg
186 25
03/03/15-11:07 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/05/2015 12:11 PM without the written consent of Pace Analytical Services; Inc..
Page 4 of 27

.c .
S
dl I I�.71C L P,22��615-.B-

aceAnalytical
www.Pw*bs.cwe
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, 'NC28078
[phone]
Project: Wood Boiler Ash 2/26
Pace Project No.: 92238940
Sample: SP22615B
LabID: 92238940002
Collected: 02/26/15 09:45 Received: 02126/1511:59 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Parameters
Results
Units
Report Limit DF
Prepared Analyzed CAS No. Qual
6010•MET ICP
Analytical Method: EPA6010 Preparation Method: EPA3050
Arsenic
3.0
mg/kg
1.0 1
02/27/15 15:50 02/27/15 20:20 7440-38-2
Barium
1420
mg/kg
5.2 10
02/27/15 15:50 03/0211513:33 7440-39-3
Cadmium
0.95
mg/kg
0.10 1
02127/15.15:50 02/27/15 20:20 7440-43-9
Calcium
69200
mg/kg
105 10
02/27/15 15:50 03/02/1513:33 7440-70-2
Chromium
16.2
mg/kg
0.52 1
02/27/15 15:50 02/27/15 20:20 7440-47-3
Copper
61.9'
mg/kg
0.52 1
02/27/1515:50 02/27/15 20:20 7440-50-8 .
Iron
12200
mg/kg
105 10
02/27/15 15:50 03/02/1513:33 7439-89-6
Lead:
16.4
mg/kg
0.52 1
02/27/1515:50 02/27/15 20:20 7439-92-1
Magnesium
17600
mg/kg
105 10
.02/27/1515:50 03/02/1513:33 7439-95-4
Manganese
2"0
mg/kg
5.2 10
02/27/1515:50 03/02/1513:33 7439-96-5
Molybdenum
1.1
mg/kg
0.52 1
02/27/15 15:50 02/27/15 20:20 7439-98-7
Nickel
17.4
mg/kg
0.52 1
02/27/15 15:50 02/27/15 20:20 7440-02=0
Potassium .
17000
mg/kg
5230 10
.02/27/15 15:50 03/02/1513:33 7440-09-7
Selenium .
ND
mg/kg
1.0 1
02/27/1515:50 02/27/15 20:20 7782-49-2
Silver
2.0
mg/kg.
0.52 1
02/27/1515c50 02/27/15 20:20 7440-22-4
Sodium
3780
mg/kg
523 1
02127/1515:50 02/27/15 20:20 7440-23-5
Zinc
152
mg/kg
1.0 1
02/27/15 15:50 02/27/15 20:20 7440-66-6
6016 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA
1311; 03/02/15 15:30
Arsenic
ND
mg/L
0.050 1 .
03/03/15 13:05 03/03/15 20:19 7440-38-2,
Barium
2.9
mg/L
0.25 1
03/03/15 13:05 03/63/1520:19 7440-39-3
Cadmium
ND
mg/L
0.0050 1
03/03/1513:05 03/03/15 20:19 7440-43-9
Chromium
ND
mg/L
0.025 1
03103/151T05 03/03/15 20:19 7440=47-3
Lead
ND
mg/L
0.025 1
03/03/15 13:05 03/03/15 20:19 7439-92-1
Selenium
ND
mg/L
0.10 1
03/03/15 13:05 03/03/15 20:19 7782-49-2
Silver
ND
mg/L
0.025 1
03/03/15 13:05 03/03/15 20:19 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470
Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 03/02/15 15:30
Mercury
ND
mg/L
0.00020 1
03/03/15 15:30. 03104/15 12:16. 7439-97-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Mercury
ND
mg/kg
0.0054 1
03/03/1518:00 03/04/1513:29 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
31.7
%
0.10 1
03/02/15 10:13 .
9045 pH Soil
Analytical Method: EPA 9045
PH at 25 Degrees C
11.8
Std. Units
0.10 1
03/03/15 11:15
365.1 Phosphorus, Total-
Analytical:Method: EPA365.1
Phosphorus
1630
mg/kg.
118 25
03/03/1511:09 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 03/05/2015 12:11 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of27

Quality Control Data for
S.P,226-15-A
SP226156
February .2-0:1 5

Pace Analytical Services, Inc. .
/��, �+
' 9800 KinceyAve. Suite 100
aceAnalX cal Huntersville, NC 26078
wwx:pacaisbacom [phone]'
QUALITY•CONTROL DATA
Project: Wood Boller Ash 2/26.
Pace Project:No.:.92238940
QC Batch: .. MERP/7630 Analysis Method: EPA.7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92238940001, 92238940002
METHOD BLANK: 1401323 Matrix: Water
Associated Lab. Samples: 92238940001, 92238940002 -
Blank. Reporting
Parameter Units Result. Limit Analyzed Qualifiers
Mercury mg/L ND 0M020 03/04/1511:37
LABORATORY CONTROL SAMPLE:. 1401324
Spike LCS. LCS %'Rec
Parameter Units Conc. Result % Rec Limits: Qualifiers
Mercury
mg/L .0025 .0.0026 ..: 105 807120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:: ,' 1401325 1401326
MS . MSD
92239123009 Spike Spike MS MSD MS' MSD % Rec .
Parameter Units Result Conc. Conc. .'Result Result % Rec : ' % Rec Limits RPD Qual
Mercury mg/L ND '.0025 .0025 0.00.27' 0.0027 109' 108. 75-125 1 :.
i
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unitls'presented to the right of the result.
z� REPORT .OF.LABORATORY ANALYSIS
This report shall not be.reproduced, except in full,
Date: 03/05/2015.12:11 PM .. without the written consent of Pace Analytical Services; Inc.. Page 6-of 27 . .

Pace Analytical, Services, Inc:.
e
aceAr�alytica!
9800-KinceyAve. Suite.100
Huntersville, NC28078
www.pamtbscom
.
704)875- 092
( 9
QUALITY .CONTROL DATA
Project: Wood Boiler Ash 2/26
Pace Project No.: 92238940
QC Batch: MERP/7631 Analysis Method: EPA 7471
''QC Batch:Method: EPA 7471 Analysis Description: - 7471 Mercury
Associated Lab Samples:, 92238940001, 92238940002
METHOD BLANK:. 1401521 Matrix: Solid.
Associated Lab Samples: ..92218940001, 92238940002
Blank. Reporting.
Parameter Units Result Limit Analyzed.. Qualifiers
Mercury. mg/kg '. ND 0.0060• 03/04/1512:37
LABORATORY CONTROL SAMPLE: 1401522
'Spike :LCS.. LCS. %Rec
Parameter Units Conc. Result % Rec Limits Qualifiers . .
- Mercury mg/kg :067 0.068 102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1401523 1401524:
MS MSD
.92239002001 Spike . Spike. MS MSDMS' MSD
% Rec
Parameter - Units Result Conc. Conc.' Result Result %•Rec: %Rec
Limits RPD Qual
Mercury mg/kg 0.'017 .064 ..063 0.076 0.076.. :.93 95
75=125 :1 .
i
Results. presented on this page aretn the units Indicated by the "Units" column except wherem aaltemate unit Is presented to.the right:of the result
Qo"
:REPORT OF LABORATORY ANALYSIS ..
This report shall not be reproduced, except in full;
Dater 03./05/201512:11 `PM without the written consent of Pace Analytical Services; Inc.:
Page 7 of.27 .

Pace Analytical Services, Inc.._
®
�Vy/71IQIIVG/
9800 Kincey Ave. 'Suite 100
HunterSville,:NC28078 .'
www paeefabs.com,
. [phone]
QUALITY CONTROL -DATA -
Project: Wood Boiler Ash 2/26
Pace Project .92238940
QC Batch: MPRP/17978
Analysis Method:
EPA6010
QC Batch Method: EPA 3060
Analysis Description:
6010 MET
Associated'Lab Samples: 92238940001, 92238940002
:METHOD.BLANK: 1399665
Matrix: Solid, .
Associated Lab Samples:, 92238940001; 92238940002
Blank Reporting . . '...
Parameter
Units:.
Result, Limit.' Analyied ,
.':Qualifiers'
Arsenic ".
mg/kg
ND
1.0. 02/27/1519:16
Barium
mg/kg
ND
0.5b 02/27/1519.16
Cadmium
mg/kg
..ND .
0.10.: 02/27/15 19:16
Calcium
mg/kg'
ND
10.0..02/27/1.519:16
Chromium
mg/kg
ND
.0.50 02/27/1519:16
Copper
mg/kg
ND
0.50-02127/1519:16
-Iron
mg/kg
ND
1.0.0-02127/1519:16
Lead
mg/kg
ND
-0.50 02/27/15 1516 -
Magnesium
mg/kg
ND
10.0 02/27/1519:18
Manganese'
mg/kg
ND
0.50 02127/1519:16
Molybdenum
mg/kg
ND
0.50 02127/1519:16
Nickel
mg/kg
-ND-
6.50 02/27/1519:16
Potassium
mg/kg
ND
500 02/27/15,19:16
Selenium
mg/kg
ND
1.0 02/27/1519:18
Silver.,
mg/kg
ND
0.50 02127/1519:16
Sodium
mg/kg
ND
500. 02127/1519:16
.
Zinc:mg/kg
ND
1.0:.02127/1519:16
LABORATORY CONTROL SAMPLE:
1399.686 .
Spike LCS
LCS %
Rec
Parameter
Units'
Conc. Result
% Rec Limits Qualifiers.
Arsenic
mgAg
-50 48.7
97
80-120 ... .
Barium
mg/kg
50 47.3"
95
80-120
Cadmium
mg/kg
50 -49.6
99
80-120
Calcium
mg/kg
500 486
97
80-120
Chromium
mg/kg
50 47.T
95
80-120.
Copper'
mg/kg
50 49.8
100 .80-120..
Iron
mg/kg
Soo 481
96
80-120
Lead
mg/kg
50 49.6
99
80-120
Magnesium
mg/kg
.500 491.
98
80-120
Manganese..
mg/kg
50 48.1
96
80-120 .
Molybdenum
mg/kg.
50 51.4
103..
60-120
Nickel
mg/kg.
50 49.4
99
80-120
-Potassium
mg/kg .
500 ND
96
80-120
Selenium
mg/kg.
50 49.6
99
80-120
:Silver
mg/kg
25 24.8
99
80-120
Sodium
mg/kg
500 475J
95
'80-120
Zinc
mg/kg
50 49.2
98:
80-120
Results presented on this page are In the units Indicated by the "Units''column except'Where an alternate unit.Is'pre sented to the right of the resuk.'
REPORT.OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 03/05/2015 12:11 PM. -
without the
written consent of Pace Analytical Services; Inc..
Page 8 of 27 ;

. Pace Analytical Services, Inc.
®
ce I�I cal
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pscebbs cem
[phone]
QUALITY
CONTROL.DATA•
Project: Wood Boiler
Ash 2/26
Pace Project No.: 92238940
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:.
1399687 .
1399688.
.
MS
MSD.
92238583001
Spike
Spike
MS
MSD
MS
MSD
% Red
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
N.D.
69.1
68.1
69:5..
' . 69.1
. 100
101
75-125
1
Barium
mg/kg
40.1
'69.1
68.1:.
132.'
108
133.
100
75-125
20:M1
Cadmium
mg/kg,
ND
69:1
68.1
69.4
68.4
100
1.00
75-125
2
Calcium
mg/kg
3450
691
681-
5060
2820
'233
-91
75-125
57 M1,R1
Chromium
mg/kg ..
0.77
69.1
68.1
68A.
66.0
98
96
75-125
..4
Copper
mg/kg ..
2.8'
69.1.
68.1
.73.6
.72.0
102
102
.75-125
..2
Iron
mg/kg..
387
691
, .681
1260
960
126 -
. 84.
. 75-125 ..
27 M1,R1
Lead
mg/kg..
17..5
69.1
68.1
.69.6
71.6
75-
80
.75-125
..3
Magnesium
mg/kg
.457
691
081
1310-
'1110
123
96.
.75-125
.16 .
Manganese .:.
mg/kg :
194
69.1
_ . 68.1..
306
233
162 .
. 58.
75-125.
- :27 M1, R1
Molybdenum
mg/kg--
ND .
'69'1
68.1
68.3 .
70.2
99'
103
75-125
3
Nickel
mg/kg_
0.97 -
69.1
68.1.
69.8
- 68.9
100
100
75-125
1
Potassium
mg/kg
1380
661
681
2370
1970
144 .
87
75A25.
-18 M1
Selenium
mg/kg
ND
69.1
:68.1
73.1
71.5
105
104. -
75-125
2
Silver ..
mg/kg
ND
34.6
33.9
'34.4.
33.8
100•
99
75-125
2
Sodium,
mg/kg
ND,
691
681
726
692
95.
91
75-125_
5
Zinc.
mg/kg
13.1
69.1
68.1
85.6
79.3
105
97.
75-125
8
Results presented on this page are In the
units Indicated Oy the "Units" column except where an alternate unlUs presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,',
'Date: 03/05/2015 12:11 PM
without the
written consent of Pace Analytical.Seirvices, Inc.:
Page 9 of27

Pace Analytical Services, Inc.. .
�n� ®
.. /yll Nical
9800 Kincey Ave. Suite 100 ' .. .
HuntersvII16,'NC 28078' : .
www.Pacelebs.cafi
[phone]
QUALITY CONTROL -DATA
Project: Wood Boiler. Ash 2/26
Pace Project No.; ..92238940
QC Batch: MPRP/1.7989
Analysis Method:. .... EPA 60.10 .
Oil; Batch Method: EPA 3010
Analysis Description: °, 6010 METTCLP. .
Associated Lab Samples: 92238940001,
92238940002
-METHOD BLANK: 1401070
Matrix: Water
Associated Lab Samples:. " 92238940001,
92238940002
Blank Reporting_
Parameter
Units:
Result Limit.'
Analyzed Qualifiers
Arsenic
mg/L
.ND 0.050.
03/03/1519:29
Barium
mg/L
ND 0.25
03/03/1519:29
Cadmium.
mg/L
ND 0.0050
.03/03/1519:29 .
Chromium.
mg/L
ND 0.025
03/63/1519:29
Lead
mg/L
ND 0.025
-03/03/1519.29
Selenium .
mg/L
NO 0.10
-03/03/15 19:29 -
Silver
mg/L
ND 0.025
03/03/15-19:29
LABORATORY CONTROL SAMPLE: 1401071
Spike LCS
LCS %. Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Arsenic
mg/L .
2.5 : 2.4
96 80A20.
I` Barium.
mg/L .
2.5. 2.3
91 80 120
4. Cadmium
mg/L
..2.5 2.4
97 80-120
.'Chromium
mg/L
2.5 . 2.4 .
94 80=120
Lead
mg/L
2.5 2.3
92 80-12.0
Selenium
mg/L
2.5' 2.4.
97 80-120.
Silver
mg/L
1.2 1.2
97 80-120
i
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1401072
1401073
MS MSD
92238935001 Spike Spike MS
MSD MS MSD
"/e Rec
Parameter Units
Result Conc. Conc. Result
Result % Rec % Rec
Limits
RPD Qua[
Arsenic mg/L
.,ND'
2.5 2.5 2.4
2.4 96 95
75-125
1.
Barium mg/L
0.43
2.5 2.5 2.7
.2.7 92 .92
75-125
0
Cadmium ing/L
ND .
2.5 2.5 2.4
2.4 98 97
,75-125
-.1
Chromium mg/L
ND
2.5 2.5 2.3
2.3 93 -92-
75-125
1
Lead mg/L
ND
2.5 .2.5- 2.3
2.2 90 90
75-125
-1
Selenium mg/L...
ND:.
2:5 • 2:5. .. ..2.4
2.4 97 96
75-125
1
Silver mg/L
ND
1.2. 1.2 1.2
1.21 98. 97
75-125
1
Result presented on this page are In the units Indicated by the 'Units" column except where an alternate unit Is presented to the right of theyesult.
REPORT OF LABORATORY ANALYSIS
This report shall not be,reproduced, except in full,
Date: 03/05/2015 12:11 PM without the written consent of Pace Analytical Services, Inc..
Page :10-of 27

aceAnalytical
www.pacelebs.com
QUALITY CONTROL DATA
Project: Wood Boiler Ash 2/26
Pace Project No.: 92238940
QC Batch: WET/35961 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92238940001, 92238940002
SAMPLE DUPLICATE: 1400641
Parameter
pH at 25 Degrees C
92238611001
Units Result
Std. Units 5.5
Dup
Result RPD
5.5
0
Qualifiers
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville,'NC 28078
[phone]
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/05/2015 12:11 PM without the written consent of Pace Analytical Services, Inc..
Page 12 of 27

Pace Analytical Services, Inc.
aC� /I„aIi/
I
800•KinceyAve. Suite 100 .. .
Huntersville, NC 28078
wwa:pa Abacom
-
(704)8759092'
QUALITY .CONTROL DATA
Project: Wood Boiler Ash 2/26
Pace Project No.: 92238940
QC Batch: WETA/22063 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 .. Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92238940001, 92238940002 -.
METHOD BLANK: 1399264 Matrix: Solid
Associated Lab Samples: ". 92238940001-, 92238940002
Blank Reporting
Parameter Units- Result Limit Analyzed Qualifiers
Phosphorus rig/kg ND 2.0.: 03/03/15 10:42 -
LABORATORY CONTROL SAMPLE:..'1399265
Spike LCS .. LCS' °%a Rec'
Parameter Units Conc. Result , %-Rec . Limits Qualifiers
Phosphorus mg/kg 50 . . 49:1 98 . 90-110
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1399266 1399267:: .
MS. MSD . .
.0238157001 Spike Spike MS MSD MS' : MSD
% Rec
Parameter Units _ Result Conc:. Conc:. Result Result .% Rec % Rec
Limits RPD . 'Qual'
Phosphorus mg/kg 162 193 193 424 417 137. 133
90-110 - :2 M1
Results presented on this page are In the units Indicated by.the "Units" column except where an alternate unit Is presented to the right of the result.
:REPORT OF.LABORATORYANALYSIS -. .
This report shall not be.reproduced, except in full,
Date: 03/05/2015 .12:1.1 PM - without the written consent of Pace Analytical Services, Inc:..
i Page 13-of27

Section 3Lab: -Sheets
June . 2015

Pace Analytical Services,.inc.
®
9800 KinceyAve. Suite 100
/+ ddlt+� /r+��
wceAIaljdic l
Huntersville,'NC28078'
wxwp9oe1a6S0wn
[phone]
ANALYTICAL RESULTS
.
Project:. Wood Boiler Ash 6/16
Pace Project No.: 92255112
Sample:. NP61615A
Lab ID: 92255112061 Collected: 06/16/15 12:45" Received: 06/18/15 10:30 Matrix: Solid
Results reported on a"dry weight"basis and are adjusted.forpercent moisture, sample
size and any dilutions..
Parameters.
Results Units Report Limit DF
Prepared . Analyzed CAS No. QuAl
6010 MET:ICIP
Analytical Method:-EPA6010. Preparation Method:. EPA3050_
Arsenic
4.5 mg/kg - . 1.6: 1-
06/23/15 17:30 - 06/26/1517:37 7440-38-2
Barium
1280 mg/kg 0.81 1
'06/23/1517:30 06/2611517:37 7440-39-3
Cadmium
2.2 - mg/kg 6.16 1
06/23115 17:30 06/26/15 17:37 7440-43-9 .
Calcium
74900 mg/kg 162 .. 10
06/23/15,17:30 06/29/1515:00 7440 70-2
Chromium
14.2 mg/kg 0.81 1
"06/23/1517:30.:06126/1517:37 7440-47-3 ..
77.4" mg/kg 0:81 . 1.
06/23/15 17:30 06/2611517:37 7440 50 8
.Copper
Iron .
9160 mg/kg 16.2 1
06/23./16'17:80 06/26/15 17:37 7439-89-6:
Lead
27.0 mg/kg 0.81: 1
06123/15 1:7:30.06/26/1517:37 7439-92-1
Magnesium
14400: mg/kg . 115.2. 1.:
06/23/15 17:30 06/26/15 17:37 7439.954.
Manganese
24.80 mg/kg.'_ 8.1 10.
. 06/23/1517:30. 06/29/15.15:00 7439=96-5.
'Molybdenum
2.0: mg/kg":. 0.81 1
06/23/1517:30. 06/26M5.17:37 7439-98-7
Nickel
16.9 mg/kg 0.81 1.
06/23/15 17:30 06/26/15-17:37 7440-02-0
Potassium
19500 mg/kg 8090. 10
06/23/15 17:30 06/29/1515:00 7440-09-7.
p
Selenium
ND.. mg/kg 1.6 1
06/23/15 17:30- 06/26/1517:37 77.82-49-2 : -
Silver
4.5 mg/kg. 0.81 ` 1
06/23/15 17 W 06/26/1517:37 7440-22-4
Sodium
4030: mg/kg 809 1
06/23/1.517:30 06/2611517:37 7440-23-5
Zinc
210 mg/kg- 1.6 1'
06/23/1517:30 06/2611517:37 7440-66-6
i.
6010 MET ICP, TCLP
Analytical Method: EPA 6010. Preparation Method: EPA 3010 .
Leachate Method/Date: EPA 1311; 06/26/15 03:10
Arsenio
ND mg/L . 0.050 . . 1 .
06/29/15 20:00 06/30/15 15:06..7440-38-2
Barium
3.8 mg/L 0.25: 1
06/29/15 20:00 06/30115 15:06 7440-39-3
Cadmium
ND mg/L 0.0050 1
06/29/15.20:00 06/30/1515:06 7440-43-9
Chromium
ND mg/L 0.025 1
06/29/15-20.00. 06/30/1515:06 7440-47-3
Lead
ND mg/L : .0.025 '1
06/29/15 20:00 .06/30/1515:06 7439-92:4 ,
Selenium
ND mg/L 0:10 1 ;
06/29/1.5 26:00 06/36/1515:06.7782=49-2
:Silver " .
ND mg/L . 0.025 1
06/29/15 20:00 .06/30/15 15:06 7440-22 4
7470 Mercury; TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470'
Leachate Method/Date: EPA 1311; 06/26/15 03:10
Mercury.
ND mg/L 0.00020 1
06/30/1510:20 06/30/1517:19: 7439-97-6
7471 Mercury.
Analytical Method: EPA'7471 Preparation Method: EPA 7471
Mercury..
-ND. mg/kg . 0.0079 -' 1
06/26/15 16:00. 06/27/15.17:10 7439.97 6 M1
Peccent.Moisture
Analytical Method: ASTM D2974187
Percent Moisture
40.6 % 0.10 1
07/0211510:11 '. .
9045'pH Soil -
Analytical Method: EPA 9045,
pH at 25 Degrees C
.0.9 Sid. Units 0.10 1'
06/25/15 10:05 . .
365.1. Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
2700. mg/kg . 96.2 20
06/30/1510:28 7723-14-0
REPORT OF LABORATORY ANALYSIS .:
This report shall not be reproduced, except in full,
Date: 07/02/2015 06:18 PM :
without the written consent:ofPace Analytical Services; Inc.. Page 4 of 27

Secteion-.3 -.:La,.'b:.-She.ets

Pace Analytical: Services, Inc..
A ®
�C�AI If�I ICI
9800 Kincey Aye. -Suite 100 _
Huntersville, NC 28078
rr www.pacalabs.tom
[phone]
ANALYTICAL. RESULTS
Project: Wood Boiler Ash 6/16
Pace Project -No.: 92255112
Sample: NP6161SS
Lab ID: 92255112002 Collected: 06/16/1512:45 -Received: 06/18/1510:30 Matrix: Solid
Results reported on a dry weight" basis and are adjusted for percent moisture, sample
size' and any dilutions.
Parameters
Results Units Report Limit DF
Prepared Analyzed, .. CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA
3050
Arsenic
4.4 mg/kg 1A. 1
06/23M517:30 06/26M.17140 7440-38-2
Barium
1220' mg/kg 0.68 1 .:.06/23/1517:30
.06/26/1517:40 7440-3973
Cadmium
1:4 mg/kg 0.14. 1:.
06/23/15'17:30.06/26/1517:40 7440-43-9
Calcium'
71600- 'mg/kg 1.361.10
06/23/1517:30 06/29/1515:13 7440-70-9
Chromium _
14.6 mg/kg 0.68 1
06/23/15 17:30 06126/1517:40 7440-47-3
Copper
59.3 mg/kg 0.68 1
06/23/1517:30. 06/26/1517:40 7440-50-8
Iron
9620 mg/kg .:. .13.6 1
06/23/1517:30 .O6/26/1517:40.7439-89-6
Lead
. 19.4 mg/kg: .0.68, .. 1
MOM 17;30. `06126/15 17:40 7439-92A
Magnesium
14800 ' mg/kg 136 - 10
O6/23115-17:30 06/29/1515:13. 7439-95-4
Manganese_
2480 mg/kg 6.8 10'
06/23/1517:30 06/29/1515:13'.7439-96.5
Molybdenum
1.6 mg/kg. 0.68 - -1
.06/23/15 17:30 06/26/15 17:40 7439-98-7
Nickel
'16.0 mg/kg 0.68 1
O6/23/1517:30 06/26/1517:40 7440-02-0
Potassium
19400 mg/kg 6810 10
06/23/15 17:30:06/29/15 15:13 7440-09-7
Selenium
ND mg/kg 1.4 1
06/23/1517:30- 06/26/1517:40 7782-49-2.
Silver
1.5 mg/kg 0.68 1'
06/23/15.17:30 06/26/1517:40 7440-22-4
Sodium
4160, mg/kg 681 1
06/23/15 IT30 06/26/1517AO 7440-23-5-
Zinc
'193 mg/kg. 1.4-. 1
0.6/2311517:30 .06/26/15-17AO 7440-66-6
6010 MET'ICP, TCLP
Analytical Method: EPA6010 Preparation Method::EPA3010.
Leachate-Method/Date: EPA 1311; 06/28/15 20:20 .
Arsenic
ND mg/L. -0.050 .. 1
06/29/15-22:40 ' .06/30/1512:53 7440-38-2
Barium
9:0 mg/L 0.25 1
O6/29/15 22:40 06/30/1.512:53 7440-39-3 .
Cadmium
0:013 mg/L 0.0060 1
06/29/15 22:40 06/30/15.12:53 7440-43-9
'Chromium_
ND mg/L 0.025 1
06/29/15 22:40 06/30/16 12:53 7440-47-3 :
Lead
ND mg/L 0.025 : 1
00/29/15 22:40 .06/30115 12:53 7439-92-1
Selenium
ND mg/L' 0.10 1
06/29/15 22:40 06/30/15 12:53 7782-49-2
:Silver ..
ND mg/L 0.025 1
06/29/15 22:40 06/30/15 12:53 7440-22-4 •
7470 Mercury, TCLP.
Analytical Method: EPA 7470. Preparation Method: EPA 7470
Leachate •Method/Date: EPA 1311; 06/28/15 20:20 .
Mercury
ND mg/L 0.00020 1-
WWI 06%30/15 17:21 7439-97-6
7471'Mercury
Analytical Method: EPA:7471 Preparation Method: EPA'7471
Mercury
ND mg/kg 0.0076 1
06/26M516:00 '06/27/1517:17 7439-97-6 .
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture _ :.
39.9 % 6.10 _ 1
07/02/15 10:12 _ .. .
9045'pH'Soil
Analytical'Method: EPA9045
pH at-25 Degrees C
9.1 Std..Units 0:10 1:
: 06/25/15 1,0:05'
366.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
2750 mg/kg 64.01 10
06/30%1510:20.7723-14:0. .
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, .
Date: 07/02/2015 06:18 PM .
without the written consent of Pace Analytical Services, anc.. ' Page 5 of 27 '

Quality Control Data for
N�.�P61-6:15-A
P-61-615-B
June 20
15

aceAnalyticai®
mrw.pecelebscom
I'
QUALITY'CONTROL. DATA
Pace Analytical.Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Wood Boiler Ash 6/16
Pace Project:No.: 92255112
QC Batch: MERP/7984
Analysis Method:
EPA 7470
QC Batch Method: EPA 7470
Analysis Description-
7.470 Mercury TCLP
Associated Lab Samples: 92255112001, 92255112002
METHOD BLANK: 1497247
Matrix: Water
Associated Lab Samples: 92255112001, 92255112002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mg/L
ND 0.00020 06/30/1516:35
LABORATORY CONTROL SAMPLE: 1497248 -
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury mg/L
.0025 0.0025
100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1497249 1497250
MS MSD
- 92254472001
Spike Spike. MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec . Limits RPD :. Qua[
Mercury mg/L ND
.0025 .0025 0.0024
0.0018 95 70 75-125 30 M1,R1
Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
1�
REPORT OF LABORATORY ANALYSIS .
This report shall not be reproduced, except in full,
Date: 07/02/2015 06:18 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 27

Pace Analytical Services, Inc.
/s,/e 9800 Kincey Ave. Suite 100
a/+
VeAnaly IKal Huntersville, NC 28678' . .
www.pacelabi.com [phone]
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/16 .
Pace Project No.: 92255112
QC Batch: MERP/7975 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92255112001, 92255112002
:METHOD BLANK:.. 1495730: Matrix: Solid,
Associated Lab Samples: 92255112001, 92255112002
Blank, Reporting
Parameter. Units Result. Limit Analyied .. Qualifiers
Mercury' mg/kg ND 0.0050 06/27/1517:03
LABORATORY CONTROL SAMPLE: 1495731
Spike CCS CCS %-Rec
Parameter. Units' Conc. Result %,Rae Limits" ' Qualifiers
Mercury mg/kg .-067 0.079 . 119 80 120
'MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1.495732 1495733 .
MS MSD
92255112001 Spike Spike MS MSD MS . MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rae -% Rec Limits RPD Qual
Mercury, mg/kg ND .086 .096 0.064 0.057 74 59 75-125: 12 M1
i
Results presented on this page are In the units Indicated by the "Units" -column except wherean alternate unit Is presented to the right of the result.
REPORT.OF. LABORATORY.ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/02/2015 06:18 PM without the written consent of PaceAnalytical Services; Inc.. Page 7 of 27 .

-Pace Analytical Services, Inc. .
®
/�
a{jeA IA aljdic 1.
9800 Kincey Avg. Suite 100 .
Huntersvi11e;:NC28078
www.peGel umn
[phone]
g
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/16
Pace Project No.: 92255112
QC Batch: MPRP/18815
Analysis Method:
EPA 6010
QC Batch Method: EPA3050 -
Analysis Description:
6010 MET
Associated Lab Samples: 92255112001,
92255112002
METHOD: BLANK: 1492328
Matrix: Solid:
Associated Lab Samples: 92255112001,
92255112002
Blank Reporting
Parameter
Units
Result Limit
Analyzed .
Qualifiers:
Arsenic
mg/kg
ND
1.0
- 06/26/15 17:13
Barium
mg/kg
ND
0.50
06/26/1517:13
Cadmium
mg/kg
ND .
0.10
06/26/16 17:13
Calcium .,
mg/kg
ND
10.0
06/26/1517:13
Chromium
mg/kg
ND
-0.50
-06/26/1517:13
Copper.
mg/kg:
ND
0.50
'06/26/1517:13
Iron
mg/kg
ND
10.0
00/26/1517:13
'Lead
mg/kg
ND
0.60
06/26/1517:13
Magnesium
mg/kg
ND
.10.0
06/26/1517`13
Manganese
mg/kg.
ND.
0.50
06/26/15 17:13 _ _
-
Molybdenum .
mg/kg
ND
0.50
06/26/1517:13
Nickel
mg/kg
ND
0:50
06/2611517:13
Potassium
mg/kg
ND
500
06/26/151713
Selenium
mg/kg
ND
1.0
06/26/1517*13 ,
.
Silver
mg/kg
ND_
0.50
06/2611517:13
Sodium
mg/kg.
ND'
500
06/26/1517:13,
Zinc
mg/kg
ND
1.0
06/26/1517:13 ...
.
LABORATORY CONTROL SAMPLE:
1492329
Spike LCS LCS
.%,Rec
Parameter
Units.
Conc. Result % Rec
Limits Qualifiers
Arsenic...
mg/kg
50 .47.4• 95
80-120
Barium.
mg/kg.
50. 48.5 97
80-120.
Cadmium
mg/kg
50 47.8 96
80-120
Calcium
mg/kg
500 563 101
.80-120. .
Chromium
mg/kg
50: 48,2. 96
80-120
Copper .
mg/kg
50 .48.8. 98
80-120'
Iron
mg/kg :
500 485.' 97
80-120
Lead
mg/kg'
50 .. 49.1 98
80-120
Magnesium.
mg/kg..'.
500 ... 471. 94,
80A20
Manganese_ _
mg/kg .:.
.50 47.4 95
80-120
Molybdenum
mg/kg
50 50.7 101.
80-120
Nickel-
mg/kg
50 47.7 95
80420
-Potassium
mg/kg ..
500 ND 97
80-120
Selenium
mg/kg
50 47:1 94
80-120'
Silver
mg/kg
25 21.5 86
80-120
Sodium
mg/kg
500 578' 116
80-120
Zinc
mg/kg
50 48.0 - 96
80-120
i
Results presented on this,page are In the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except'in full,
Date: 07/02/2015 06:18 PM
without the written consent of Pace Analytical Services; Inc..
Page 8 of 27 .

PaceAnalytical'Services, Inc.
9800 Kinsey -Ave: Suite 100
Huntersville, NC 28078
[phone]-.
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/16.
Pace Project No.: 922W12
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1492330
1492331
MS
MSD
92255417001- Spike
Spike'.
MS
MSD..
'MS
MSD
% Rec
Parameter
Units
Result Cone.
Cone..'
Result
Result
% Rec
% Rec
Limits .
RPD Qual
Arsenic
mg/kg
ND 39.1
39.7
37.6
38.6.
96.
.97
75425.
3
Barium
mg/kg
12.5 39.1
39.7'
- 47.9
49.0
91
92.
75-125
2'
Ug/g
Cadmium ..
mg/kg
"ND 39.1
39.7
381
.. 39.1 ..
98
98
75-125
2
Calcium
mg/kg
27.4 391
397
400.
408.
95
96
75-125.
2
Ug/g
Chromium
rrig/kg
ND 39.1
39.7
38.5
39.3.
98
99
75-125
.2
Copper
mg/kg
0.559 39.1
39.7
'39.7
40.8
100
101
75-125
3
ug/g
Iron
mg/kg
21.9 . 391.
397
407
414
98.
99
75-125
2
..
Ug/9
Lead
mg/kg.
.
ND 39.1.
39.7
.38.9
39.8
.98
99 :.
75-125
2.
Magnesium
mg/kg
ND 391
397.
377 '
' 387
96'
97
75-1.25
3.
• ..
Manganese "
mg/kg , .
ND 39.1.
39.7
37.8
38.8
96
97
75 125
3
-Molybdenum -
mg/kg
ND 39.1
39.7.
40.3
41A
103
104
75-125
.3
Nickel
mg/kg
ND 39A
39.7..
37.'9
39.0
97
.98'
7&125.
3
Potassium
mg/kg
ND. 391
397.
466
479
81
83,
75-125
3
Selenium
mg/kg
ND 39.1
39.7
37.8-
38.4
.96
96
75.125
2.
Silver
mg/kg.
ND 19.5.
19.8
17.2
17.7
88
89
'75-125
3
Sodium
mg/kg
ND 391
.397
399
409
94
95
757125
3
�. Zinc ,
mg/kg
6.78 39.1
39.7
44.3
45.7
96
98
.75-125
3'
Ug/g
i
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unitis presented to the fight of the result.
F
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full, .
Date: 07/62/2015 06:18 PM
without the written consent of Pace Analytical. Services, Inc..
Page 9, of.27

Pace Analytical Services, Inc.
d J �g ®
�{7t�/'InalXical
9800 Kincey Ave. Suite1.00
Huntersville,:NC'28078"
www.pecelebleam
[phone]
QUALITY CONTROL -DATA
Project: Wood Boiler Ash 6/16
Pace ProjectNo.: 92255112
QC'Batch: MPRP/18854
Analysis Method:. EPA6010 -.
QC Batch Method: EPA 3010
Analysis Description: 6010 MET TCLR
Associated Lab Samples: 92255112001
METHOD BLANK: 1496691
Matrix: Water -
Associated Lab. Samples: 92255112001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers:.
Arsenic
mg/L
ND 0.050 06/30/1513:43
Barium
mg/L
ND 0.25 06/30/1513:43
Cadmium
mg/L
ND 0.0050 06/30/1.513:43
Chromium.
mg/L
ND 0.025 06/30/1513:43
Lead
mg/L
ND 0.025 06/30/1513:43
Selenium
mg/L
ND 0.10 06/30/1513.43
Silver
mg/L
ND 0.025 06/30/1513:43
LABORATORY CONTROL SAMPLE: . 1496692
Spike, LCS. LCS %. Rec . .
Parameter
Units
Conc. Result % Rec Limits . Qualifiers
Arsenic
mg/L
2.5 2.4 96 80-120
Barium "
f
mg/L
2.5 2.2 .. 88 80-120
Cadmium
mg/l.
2.5 2.3. 91 80-120
Chromium
mg/L "
. 2.5 . 2.3 92 80-120
Lead
mg/L
2.5 2.2 87 80-120
Selenium
mg/L
2.5 2.4 96 80120
Silver
mg/L
1.2 1.2 97 80-120
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 1496693 1496694
'MS :MSD
.92254472001
Spike Spike MS , . MSD. MS. , . MSD.
% Rec
Parameter Units
Result
Conc. Conc. Result Result %•Rec % Rec
Limits RPD Qual
Arsenic mg/L
ND
.2.5 2.5 2.5 2.5: 1.01: 99.
75-125
2
Barium mg/L
67.OJ
2.5: 2.5 2.4 .2.4 .93 .92
75-1215
2
ug/L
Cadmium mg/L
ND
.2.5 2:5 .2.4 2.3 96 . '.94.
'75-125
2
.Chromium . mg/L
ND
2.5 2.5 2.4 2.4 98 96.,
75-1.25
2
Lead mg/L
ND
2.5 2.5 2.3 2.3 93 90
75-125
3
Selenium mg/L
ND
2.5 2.5 2.5 2.4 100 97
75-125
3
Silver mg/L
2.08J
1.2 1.2 1.3 1.2 100 99
75-125
1
ug/L
Results presented on this page are In the units Indicated by the "Units" column except Where an alternate unit Is presented to the right
of the result.
:REPORT OF.LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/02/2015 06:18'PM
without the written consent of Pace Analytical Services, Inc..
Page 10 of 27

Pace Analytical Services, Inc.
9800-I0ncey Ave: Suite 100
QV�i'l7/ 1�I�VR1
Huntersville: NC 28078
xmw.peoelabsoam
[phone]
QUALITY CONTROL -DATA,
Project:. Wood Boiler Ash 6/16.
Pace Project No.: 92255112
QC Batch: MPRP/18868
Analysis Method: EPA 6010
QC Batch Method: EPA 3016
Analysis Description: 6010 MET TCLP.
Associated Lab Samples: 92255112002
METHOD BLANK: 1497701
-Matrix: Water
Associated Lab Samples: 92255112002
Blank Reporting
Parameter
Units,
Result Limit Analyzed
Qualifiers
Arsenic
mg/L
ND 0.050. .06/30/15 12:15
Barium
mg/L
ND 0:25 06130/1512`:15
Cadmium
mg/L
ND 0.0050 06/30/1512:15
Chromium
mg/L
ND 0.025 06/30/15 12:15
Lead
mg/L
ND' 0.025 66/30/1512:15 '
Selenium
mg/L
ND 0.10 06/30/1512:15
/L
ND 0 025 06/30/15-12.16
Silver,
mg
-LABORATORY CONTROL SAMPLE: 1497702
Spike
LCS
LCS
% Rec
Parameter
Units Conc.'
Result
%Rec
Limits Qualifiers
Arsenic
mg/L 2.5
2.5
100
80-120
.
is Barium
mg/L 2.5,
2.4
96
80-126
Cadmium
mg/L 2.5
2.5
98
80-120
Chromium
mg/L = 2.5
.2.4
98
80-120
Lead
mg/L 2.5
2:4
94
80-120
Selenium
mg/L 2:5
2.5
99
80-120'
Silver .
mg/L 1 2
1;2
99
80-120
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 1497703
1497704
MS
MSD
92254473001 Spike
Spike MS
MSD .
MS MSD
% Rec
Parameter
Units
Result Conc:
-Conc. Result
Result
6/6-Rec . % Rec
Limits RPD Qual
Arsenic'
mg/L
ND 2.5
2.5 2.6
2.6
1104 . 105
75-125..
.0
Barium
mg/L:
ND Z5
: 2.5- 2.5
2.5
99.: 100
75-125,
1
Cadmium
mg/L
ND 2.5
2.5- 2.6
2:6
103 103-
75-125
0,
.Chromium
mg/L
. 4.98J. 2.5
2.5 2.5
2.5.
100 10.1•
75-125. •
2
.
ug/L
Lead.:
mg/L
86.8 ' 2.5
2.6- - . 2.6
2.6
99 99
75-125
0
ug/L.
Selenium
mg/L
ND 2:5
2.5 2.6
2.6
103 104
' 75-125
1
Sliver.
mg/L
ND . 1.2
1.2• 1.3
1.3
103 104.
, 75-125
1
I
i
Results presented on this page am
in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT.OF LABORATORY_ ANALYSIS
_. .
This report shall not be reproduced, except in full,
Date: 07/02/2015 06:18 PM
without the written consent of Pace Analytical
Services, Inc..
Page 11. of 27

Pace Analytical- Services, Inc..
dn,I /�' ® 9800 KinceyAve. Suite 100
(?CeNIGUiUill. Huntersville, NC28078''
www.paWab&wm [phone]-
y „
F
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/16
.Pace Project No.': = 92255112
QC Batch: PMST/8054- Analysis.Method: - ASTM 1)2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92255112001, 92255112002
SAMPLE LE -DUPLICATE: .1499501
Parameter
Percent.Moisture
SAMPLE DUPLICATE: 1499502
Parameter
Percent Moisture

Pace:Analytical Services, Inc.
IaceAnalXi /+RI
9800 KinceyAve. Suite100
Huntersville, NC 28078
wwwpeeelebsoom
/�
[phone]
t
QUALITY CONTROL DATA
Project: Wood Boiler Ash 6/16.
Pace Project No.: 9225511.2,
QC Batch: WET/38342
Analysis Method:. EPA 9645 -
QC.Batch Method:. EPA9045" .
Analysis Description: 9045 pH
Associated Lab Samples:" 92255112001,
92255112002
SAMPLE DUPLICATE: 1492936
92255522008 Dup
Parameter
Units Result Result RPD" Qualifiers
OH at 25.Degrees C
Std. Units 7.2 7.2 0
SAMPLE DUPLICATE: 1492837
92255561001 Dup
Parameter :
Units Result Result. RPD Qualifies
pH at25 Degrees C
Std. Units 6:8" 6.8 0
Results' presented on this page are In the units Indicated by the ,"Units"'column except where an alternate unit is presented to the right of the result.
REPORT" OF "LABORATORY ANALYSIS . -
This'reportshall not be reproduced, except in'full, .
Date: 07/02/2015 06:18 PM
without the written consent of Pace Analytical Services, Inc..
Page 13"of 27 "

-Pace Analytical Services, Inc. "
®.
aceAnalytica!
.91100-KinceyAve. Suite100' .
Huntersville; NC 28078 '
www.paceiabloom
[phone]
QUALITY CONTROL" DATA
Project: Wood Boiler Ash 6/1li
Pace Project No.: 92255112
QC Batch: WETA123516 Analysis Method: . - . EPA 365.1
QC. Batch Method: " EPA 365:1 Analysis_ Description: 366.1 Phosphorus, 'Total
Associated Lab Samples, 922551120,01, 92255112002
METHOD:BLANK: 1496978 Matrix: Solid
Associated Lab Samples:. 9225511200.1, 92255112002
Blank Reporting .. ... .
Parameter Units Result Limit, Analyzed . Qualifiers
Phosphorus mg/kg -ND 2.0.06/30/15;09:59
LABORATORY CONTROL SAMPLE: 1496979
Spike LCS LCS % Rec
Parameter Units :. Conc. Result : , %Rec Limits Qualifiers
Phosphorus mg/kg. 50 52.3 105 ..907110,
MATRIX SPIKE &-M ATRIX SPIKE DUPLICATE: 1496980 1496981
MS MSD
92255606001, Spike Spike MS MSD MS MSD
% Rec "
Parameter Units Result Conc. Conc. Result Result % Rec % Rec
Limits .RPD Qual
�. Phosphorus mg/kg 120 .237 261, 371 290 106 84 "
90-110 25 M1,R1
Results presented on this page are In the units Indicated by the "Units". column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced„ except in full,
Date: 07/02/2015 06:18 PM . without the written consent of Pace Analytical Services; Inc.:
Page 14 of 27

Pace Analyticat Services, Inc.
®
9000 Kincey Ave. Suite 100 .
aceAnalyiical
-Huntersville; NO 28078 :. .
wwwpsoe/s6s.00m
[phone]
ANALYTICAL. RESULTS
Project: Ash 10/29
Pace Project:No;:. 92274113
Sample:-$P102s15A'
Lab ID: 02274113001 Collected: '10/29/15 09:45 Received:.10/29/15 13:38 'Matrix:
Solid
Results reported on a "dry weight ". basis and are adjusted for percent moisture, sample
size and any dilutions. • "
Parameters.
Results Units .. Report Limit DF
Prepared
Analyzed .
CAS No. Qual.
6010 MET ICP
Analytical Method: EPA 6010 .Preparation Method: EPA 3050
Arsenic
4.0 . mg/kg, 1.0 , 1
11/04/15 21:00
1.1/06/15 14:00 7440-38-2
Barium
.815 mg/kg 2561 . 50
11/04/15 21:00
11/06/15 .15*19
.7440-39-3
Cadmium
0.78.. mg/kg 0.10 1
11/04/15 21:00
11/06/15 14:00
7440-43-9
Calcium
45700. mg/kg 502 50
11/04/15 21:60.
11/06/15 15:19
7440-70-2 .
Chromium
20.1 mg/kg 0.50 1
11/04/15 21:00
11/06/15 -14:00
7440-47-3
Copper
72:0 mg/kg 0.50 1
11/04/1521,00-
11/06/1514:00
7440-50=8
Iron
9120 mg/kg 502 50
11/04/1521:00
11106/1515:19
7439-89-6
Lead:
.13.9 mg/kg 0.50: 1.
11/04/15 21:00.
11/06/15 14:00
7439-92-1
Magnesium .
11400 mg/kg 502' 50:
11/04/15 21:00
.:11/06/15.15:1,9
7439-95-4
Manganese.
1360 mg/kg . 25.1 .50
11/04/15 21,40.0.
11/06/15 15:19
7439-96-5.
Molybdenum
0.51 mg/kg ..0.50 1:
11/04/15 21:00..11/06/15
14:00
7439-98-7
Nickel
18.1 171,19" .0.56. 1.
11/04/15 21:60,
11/06/15 14:00
7440-02=0. .
Potassium
-.ND mg/kg. 25100 .50 .
11/04/15 21:00
11/06/1515:19
7440-09-7
Selenium.
.'ND rng/kg 1.0 1
11/04/15 21:00
.11/06/15' 14 00
7782-4972
Silver'
2.1 mg/kg 0.50 1
11/04/15 21:00.
11/06/15 14:00
7440-22.4
Sodium.
6340. mg/kg 502 1
11/04/15 21;00
11/0115 14:00
' 7440-23-5
Zinc.
147 mg/kg 1.0 . 1
11/04/15 21:00
11/06/1514:00
7440-66-6
., a010 MET,ICP, TCLP
Analytical Method:.EPA6010 Preparation Method: EPA3010
Leachate.Method/Date: EPA 1311; 11/02/15 00:20
Arsenic
ND mg/L 0:050 1
11/04/15 04:05
11/04/1514:11..7440-38-2
Barium
8. mg/L 0.25 1
11/04/15 04:05
11/04/15 14 11
.7440-39-3
Cadmium
0.0087 mg/L 0.0050. 1
11/04/15 04:05
11/04/15 14:11
7440-43-9
Chromium
ND mg/L 0.025 -1
11/04/15.04:05
11/04/15 14:11
7440-47-3
Lead'
ND mg/L 0.025 1
11/04/15 04:05
11/04/15 14:11
7439-92-1
Selenium
ND mg/L 040 1
11/04/15 04005
11/04/15-14:11
778249-2
Silver
ND -mg/L 0.026. 1
11/04/15 04:05
11/04/15 14:11
7440-22-4
.7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA7470
Leachate Method/Date: EPA 1311; 11102/15 00:20
Mercury. ....
ND mg/L .0.00020.: "T
11/04/1510:15. 11/04/1514:16.7439-9776.
.
7471 Mercury
Analytical Method: EPA'7471 Preparation Method: EPA
7471
Mercury
IND mgNg 0.0070 1
11/10/1516:45.11/1.1/15.13:19 7439.97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent-Moisturd
41.4 "/o 0.10 1
11/0211515:00
1010 Flashpoint;Closed Cup
Analytical Method: EPA :1010
Flashpoint
>200 deg F 70.0 1
11/02/15
14:30
9045,pH Soil,
Analytical Method: EPA 9045
pH at 25 Degrees C
8.9 Std. Units 0.10 1
11/05/15
15:35
.:REPORT OF.LABORATORY ANALYSIS .: .
This report shall not be reproduced, except in full,
Date: 11/11/2015 04:23 PM
without -the written consent of Pace Analytical Services, -Inc:.
Page 4-of,22

Pace Analytical Services, Inc.
®
IaC19AnalXical
• • ,
9800 Kincey Ave. Suite 100
liuntersville, NC 28078
xww.peoelabaoom.
. [phone]
ANALYTICAL. RESULTS.
Project: Ash .10/29
Pace Project No.: .92274113
.Sample: SP1029.16A
Lab ID: 92274113001 " Collected` 10/29/15 09:45 Received:
10/29/1513:38 'Matrix: Solid
-Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF 'Prepared
Analyzed'.
CAS No. Qual . .
366.1 Phosphorus,:Total
Analytical Method: EPA365:1
Phosphorus
7370 - mg/kg 33.5 10
11/10/15 05:16
7723-14-0 M6; R1
7336 S Reactive Cyanide .
Analytical Method: SW 846 7.3.3.2
Cyanide, Reactive-
ND. mg/kg 1:7. - - 1.
11/03/15 18:22
735S Reactive Sulfide.
Analytical Method:. SW 846 7.3.4.2
'Sulfide, Reactive
is
- ND mg/kg 16.9 .1
11/02/15 15:00
. .
'I
i
I
REPORT OF. LABORATORY.ANALYSIS .
This report shall not be reproduced, except in full,
Date: 11/11/2015 04:23 PM
without the written consent of Pace Analytical Services, Inc..
Page 5 of 22

Pace Analytical Services, Inc. .
®
�•
aceAnal i+Cai
9800'Kincey Ave. Suite 100
Huntersville; NC 28078
www.PWkb&c"
[phone]
ANALYTICAL'RESULTS
.
Project: Ash 10/29
Pace Project No.: 92214113
Sarinple: SP102915B _
Lab ID: 92274113002 Collected:. 10/29N509:45 Received: 10/29/1513:38
Matrix: Solid._'
Results reported on a dry welght" basis and are adjusted for percent moisture,, sample.size and any. dilutions.
Parameters
Results Units. Report,Limit DF
Prepared
Analyzed
CAS'N6. Qual
6010 MET ICP
Analytical Method: EPA 6010. Preparationi, Method:; EPA 3050
Arsenic'
� 3.0 mg/kg, , 0.86 . -1
1.1/04/15 21:00.
11/06/15 14:13
'7440-38-2
Barium
765 mg/kg 211.5. '50
11/04/15 21:00
.11/06/15 15 22
.7440 39-3
Cadmium
0.70 mg/kg 0.086 1
11/04/1521:00
llift 14:13
15
7440-43-9 .
Calcium .
37400 - .' mg/kg.. 430 50
11/04/15 21':dd
MOMS 15:22
1440-70-2 -
Chromium
21.1 mg/kg. 0.43 1
.11/04/15 21:06
11/06/15 14:13
7440-47-3
Copper
'68.4 mg/kg 0.43 1
11/04/15-21:00.11/06/15.1'4:13
7440=50-8
Iron
8730 mg/kg 430 .50
11/04/15 21:00
11/06/15 15:22
•7439=89-6
Lead •
_
16.1 mg/kg 0.43 1
11/04/15 21:00
. 11/06/15 14:13
7439-92-1
Magnesium...
6990 mg/kg 430 50
11/04/15'21:00
11/06/15 15:22
:7439-95-4
Manganese
1390 mg/kg -. 21.5 50
11/04/15 21:00
11/06/15 15:22
. 7439-96-5 ,
Molybdenum
0.45 mg/kg 0.43 1
11/04/15 21:00.
11/06115.14:13
7439-98-7 -
Nickel'
1.7:5 mg/kg 0.43 1
11/04/15 21:00
11/06/1514:13
7440-&0
Potassium
ND - mg/kg- 21500 50
11/04/15 21:00
11/06/15 15:22.
7440-09-7
Selenium
1.3 rng/kg 0.86 1
11/04/15 21:00
11/66/15 14:13
7782.49-2.
Silver:.
2.1 mg/kg: 0.43 1
.11104/15 21 W
11/06/15 14:13
7440-22-4
Sodium
6420 mg/kg 430- 1 ,
11/04/15 21:00
11/06/15 14:13
7446-23-5
Zinc
129 mg/kg. 0.86 1 ..11104/15
21:00 -
11/06/15 14:13.
7440-66-6
c 6010 MET ICP, TCLP
Analytical Method:.EPA6010 Preparation Method: EPA3010
Leachate Method/Date:.EPA 1311; 11/02/15 00:20'
Arsenic .
ND mg/L 0.050 1.
11/04/15 04:05'.
11/04/1514:14 .7440-38-2
.
Barium
7.8 mg/L 0:25 1
11/04/1.504:05
11/04115 14:14-
7440-39-3
Cadmium
-0.010 mg/L 0.0050. 1
11104/15'04:05.11/04/15-14:14
7440-43-9.
Chromium
ND mg/L 0.025 . 1
'11/04/15 04,05.
11/04/15.14:14
7440-47-3.. .
:..
Lead
' . .
• 0.625 : 1
ND mg/L
'11/04/15 04:05
11/04/15 14:14 "7439-92-1
Selenium
ND: mg/L 0.10 1.
11/04/15 04:05
11/04/15 14:14.
7782=49-2
:Silver-
ND mg/L 0:025 1
11/04/1504:05
11/04/1514:14
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 11/02/15 00:20
Mercury.
ND mg/L 0:00020. 1
11/04/15'1.0:15
1:1/04/1514:19
7439-97-6, -
7471 Mercury.
Analytical Methotl:-EPA 7471; Preparation Method: EPA 7471
Mercury.
ND. mglkg. 0.'0052 1
11/10/1516:45."11/11/1.513:21
7439-97-6
Percent, Moisture
Analytical Method:ASTM D2974-87 -
- Percent Moisture
-39.4 . % 0.10 1
11/02/15 15:00
1.010 Flashpoint,Closed Cup
Analytical Method: EPA 1010.
Flashpoint
>200 deg F 70:0 1
11/02/15 14:30
9045.pH Soil'
Analytical Method: EPA9045
OH at25 Degrees C
9.0 Std.:Unit,s 0:16 1
11/05/1.5 15:35
REPORT OF LABORATORY -ANALYSIS
{
This report shall not be reproduced, except in full,
Date: 11/11/2015 04:23 PM
without the written consent of Pace Analytical Services; Inc..
Page 6 of 22

Pace Analytical Services,
®
/+�
�C�AI r1 alyt c II
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pao"scom
(704)875-9.692
ANALYTICAL RESULTS
Project: Ash 10/29 .
Pace Project No.: 92274113
Sample: 'SP102915B
Lab ID: 922741.13002: Collected:. 10/29/15-09:45 ° Received:
10/29/1513:38.
Matrix: Solid
Results reported on: a dryweight"
basis and are adjustedforpercent moisture, sample size and any.dilutions..
Parameters
Results Units. Report Limit. DF . Prepared
Analyzed
CAS No. Qua[
313M Phosphorus, Total
Analytical Method: EPA '366.1
Phosphorus
1430 mg/kg 32.3.. 10
11/10/15 05:18.
772344-0
733C S:Reactive Cyanide
Analytical Method: SVN 846.7.3.3:2
Cyanide, Reactive
ND mg/kg.: - 1.6 1
11/03/15 18:23
735S Reactive Sulfide
Analytical -Method` SW 846 7.3.4.2
Sulfide, Reactive
ND mg/kg- 16.5 1
11/02/1515:00
.
yips
REPORT OF. LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/11/2015 04:23 PM
without the written consent of Pace Analytical Sery a, Inc..
Page 7 of 22

- Section 3:La-b Sheets
Data Quality..Control for
SP102915A
SP102915B
�.
October, 2015

Z.
eAnal ical
wwivpacMb mn
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve..Suite 100
Huntersville, NC 28078
[phone]
Project:. Ash 10/29
Pace Project No.: 92274113
QC Batch: MERP/8609
Analysis Method: EPA 7470.
QC Batch Method: EPA 7470
Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 922741130011 92274113002
METHOD BLANK: 1598202
Matrix: Water .
Associated Lab Samples: 92274113001, 92274113002
Blank Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
mg/L
ND 0.00020.
11/04/15.13:27
LABORATORY CONTROL SAMPLE:
1598203
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
mg/L
.0025
0.0026
102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1598204
1598205
MS
MSD
92274030001
Spike
Spike MS
MSD' MS MSD % Rec
Parameter
Units Result.
Conc..
Conc. Result
Result % Rec % Rec Limits RPD Qual
Mercury,
mg/L ND
.0025
.0025 .0.0031
0.0032 12.3. 127 75-125 3 M1.
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. I
REPORT OF LABORATORY. ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/11/2015 04:23 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 22

Pace Analytical Services, -Inc.
®'
aeeAnal. cal
9800 Kincey Ave: Suite 100.
Huntersville, NC 28078
xma peCea96s can .
[phone]
QUALITY CONTROLDATA
Project: Ash 10/29
Pace Project No.: 92274113
QC Batch:. MERP/8634
Analysis Method: EPA 7471
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 92274113001, 92274.113002'
METHOD BLANK: 1602842
Matrix: Solid
Associated.Lab Samples: 92274113001, 9227411.3002
Blank Reporting
Parameter,
Units
Result Limit Analyzed Qualifiers
Mercury
mg/kg.
ND 0.0062 11/1111513:67
LABORATORY CONTROL SAMPLE:
1602843-
-Spike LCS LCS. % Rec
" . Parameter
Units
Conc. Result % Rec Limits Qualifiers
. Mercury
mg/kg
.083 0.084 100, 80-120.

Pace'Analytical Servicesi Inc. .
®
+'
aceAnallXieal
9800 Kincey Ave. Suite 100
Huntersville, NO 28078
xlvx pe0818t1aCOm
[phone]
i.
QUALITY CONTROL DATA
Project: Ash.10/29
Pace Project No.! 9227411.3
QC Batch: MPRP/19963..
Analysis Method: EPA6010
QC Batch Method:. EPA 3050
Analysis Description:. 6010 MET• '
Associated Lab.Samples:. 92274113001',
92274113002
METHOD BLANK: 1599273
Matrix:. Solid
Associated Lab Samples: 92274113001,
92274113002
Blank . Reporting
Parameter
Units
Result Limit, Analyzed
Qualifiers
Arsenic.
mg/kg
ND. 1'.0 11/06/15 13:20
Barium- _
mg/kg,
ND. 0.50 11/06/15 13.20
Cadmium
mg/kg -
ND 0:10- 11106/1513:20
Calcium
mg/kg,
ND 10.0 11/06/1513:20.
Chromium ...
mg/kg.
ND : -0.50 11106/1513.20
Copper
mg/kg::
" ND' 0.50 '11/06/1513:20
Iron
mg/kg
ND 10.0 11/06/1513:20
Lead
mglkg
ND 0.50 11/06/1513:20
Magnesium:
mg/kg
ND 10.0. 11/06/1513:20
Manganese
mg/kg
ND 0.50 11/06/1513:20
Molybdenum
mg/kg
ND 0,.50 .11/06/1513:20.
Nickel.
mg/kg
ND 0.50 11/06/1513:20
Potassium
mg/kg.
ND 500 11/06/1513:20
Selenium
mg/kg.
ND 1.0 11/06/1513:20..
3ilvei ..
rng/kg
ND 0.50 11/06/1513:20
Sodium
mg/kg;
ND 500 .11/OEi/1513:20-
Zinc:
mg/kg
ND 1.0; • 11/06/1513:20
LABORATORY CONTROL SAMPLE:
:1599274
SpikeLCS LCS %"Rec
.
Parameter
Units
Conc. Result %.Rec Limits Qualifiers ..
.
Arsenic
mg/kg
50 50.6 101
86-120
Barium-.
mg/kg
50 52.4 105
80-120.
Cadmium
mg/kg
50 53.0 106
80-120
Calcium
500 524 105
80-120
Chromium
mg/kg..
50 51.9 104
80-120.
Copper
mg/kg
50 52.9. 106
80-120
Iron
mg/kg .
500 533_ 167 . .807120
.
Lead
mg/kg
50 51.5 .103.
80A20
Magnesium
mg/kg
500 520- = .104
80-120
Manganese
mg/kg
50 : 51.6' 103
80-120
Molybdenum
mg/kg .
50 54.0 .. .108
•
80-120.
.Nickel.
mg/kg.
50 52.2 104.
80-120.:. .
Potassium
mg/kg
500 526 105
80=120
Selenium
mg/kg
50 52.8 106
80-120
Silver
mg/kg
25 26.0 104
80-120
Sodium
mg/kg
500 534 .. 107
807120
Zinc_ .
mg/kg
50 50.7. 101
80-120
Results presented on this
page are In the units Indicated by the"Units" column except where an alternate unit Is presented,to the right of the result.,
"r
REPORT OF LABORATORY ANALYSIS
This report shall not be.reprod'u xcepfin cede 'full
Date: 11/11l2015 04:23. PM :.
without the
written consent of Pace Analytical Services, Inc..
Page 10 of 22

Pace Analytical Services, Inc.
®
aceAnalXical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
wwwpaoelsbaeom
[phone]
QUALITY CONTROL DATA
Project: _ Ash 16/29
Pace Project No:: 92274113 -
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1599275
1599276
MS
MSD
"
92273934001
Spike.
Spike
MS
MSD
MS
MSD
%-Rec .
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rea
Limits
RPD Qual
Arsenio
mg/kg
NO
43.7
61.5
45.4
63:9
103
103
75-125
. 34 R1
Barium .
mg/kg
56.1
4.3.7
61:5 .
98.3
112
97
91
75-125.
13
Cadmium
mg/kg
ND
. 43.7
61.5
46.0
65.2
105 .
106
75-125
35 R1
Calcium
mg/kg
4550
437
615
'6550
4720
: 458
27'
75-125
, 33 M1;R1
Chromium
mg/kg
'0.69
43.7
61.5
44.8
62.7
101
101
75-125
33 R1
Copper
mg/kg
2:7
43:7
61.5
49.5
103
107
163
75-125
70 M1;R1
Iron
mg/kg
383
437
'615
866
1040
111'
108
75-125:
19
Lead
mg/kg
0.80
45.7
61.5
43.7.
62.0
98
100
75-125.
35 R1 .
Magnesium
mg/kg
579 .
' 437
615
1030
1180
103
98
75A25
1.4
Manganese
mg/kg.
173
.43,7
61.5 .
221
229
110
90
75-125
3
Molybdenum
mg/kg
ND
43.7'
61.5
44.4..
64.0.
101.
104
75-125
36 R1
Nickel
mg/kg
0.87
.43.761.5
44.9
63:5
101
102
75-125
34 RI
Potassium
mg/kg
1670
437
615.
2210
2260
123
.97
75-125
:3
.Selenium..
mg/kg
ND .
.: 43.7
'.61..5'
52.5
72.9
118
117 "
75-125.
32 R1
Silver .. -
mg/kg.
ND
: 21.9 :..
30.7 ..
22.2:
31.3.
102
102
75.125
34 R1
Sodium
ing/kg
ND
437
615
497
673
106
104
75-125
_ 30 R1
Zinc
mg/kg
12:6
43.7
61.5
54.9
72.5
97
98
75.125
28 R1 .
I`
Results presented on this page are In the
units Indicated by the "Units" column except where an attemate unit Is presented
to the tight olt. f the resu'
:REPORT
OF LABORATORY.ANALYSIS .:.
.
This report -shall not be reproduced, except
in full;
Date: 11/11/20.15 04:23 PM'
without the written consent'of Pace Analytical Services; Inc....
Page:11 of 22

Analytical
www.paoelabao"
Project: _ Ash 10/29 -
Pace Project No.:. 92274113
Pace Analytical Services,.lnc:
98001(incey Ave. Suite 100
Huntersville, NC 28078
[phone]'
QC Batch: MPRP/19956
Analysis Method:' EPA6010
QC Batch Method: EPA 3010
Analysis Description: 6010' MET TCLP
Associated Lab Samples: 92274113001,
92274113002
METHOD BLANK:. '1598162
Matrix: -Water
Associated Lab Samples: 92274113001, 92274113002
Blank Reporting
Parameter
Units
Result Limit.
Analyzed Qualifiers:
.
-Arsenic
mg/L
-ND 6.050
11/04/15 13:14
Barium
mg/L
ND ', 0.25
11/04/1513:14
Cadmium
mg/L
ND 0.0050
11/04/1513:14
Chromium,
mg/L
ND 0:025
11/04/1513:14 . .
Lead
mglL
ND. 0.025
11/04/1513*14
Selenium
mg/L
ND 0.10
-11/04/1513:14
Silver
mg/L
ND 0.025
11/04/1513:14.
LABORATORY CONTROL SAMPLE: ' 1598163 : .
Spike, . LCS.
LCS %Rec
Parameter
Units
Conc. Result % Rec Limits . Qualifiers
Arsenic
mg/L
2.6 2.5.
160 80-120
Barium
mg/L
2.5. 2.5.
100 ..-80-120 ...
E.: .
Cadmium
mg/L .
2.5 ' 2.5,
100 80 120
Chromium
mg/L
.2.5. 2.6.
.102 80=120
Lead
mg%L -
2.5 2.3
93 80-120
Selenium
:mg/L2:5
2.5:
102 80-120
Silver
mg/L
1.2 1.1,'
91 80-120
MATRIX. SPIKE & MATRIX SPIKE DUPLICATE:, 1568164 . _ 1.596165.
MS .:MSD
9227.4030001 ..
Spike Spike MS
MSD.. MS, MSD
% Rec
Parameter, . Units
Result
Conc. ' Conc., Result
'Result %•Rec . % Rec
Limits RPD Qual .
Arsenic mg/L
ND
2.5 2.5 2.6
.2.7 105: 108
75-125
2
Barium . mg/L
1.5.
2.5: 2.5 3.9
4.0 96 102
757125
4 .
Cadmium' mg/L
ND -
. 2.5 2.5 2.6
2.7 106 108 .
75A25
2
Chromium mg/L
0.035
2.5. 2.5- 2.6
2.6 102 103
75-125
1
Lead. mg/L
0.074
2.5 2.5 2.5
.2.6 99 101
75-125
2.
Selenium mg/L
ND
2.5 2:5 .2.7
1.8 :107 110
75-125
2
Silver mg/L
ND
1.2. 1.2 .1.2
1.2 9.8 96.
75=125
.3
Results presented on this page are
in the units Indicated by the -"Units•' column except where
an alternate unitls presented to'the right o(the result'
REPORT .OF. LABORATORY ANALYSIS
This
report shall not be reproduced, except in full.
Date: 11/11/2015 04:23 PM
without the written consent of Pace Analytical Services, Inc..
Page 12 of:M

Pace Analytical Services, Inc;
® 9800 Kincey Ave. Suite 100
aCel71 %alyfica Huntersviile, NC 28078 . .
www.paombloom [phone]'
it
QUALITY -CONTROL DATA
Project: Ash 10/29
Pace Project No.: 92274113
QC Batch: PMST/8523 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92274113001, 92274113002
SAMPLE DUPLICATE: 1596550
92274222001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture' % 40:0 39.3 2
SAMPLE DUPLICATE: 1596551
92274113002 Dup
Parameter Units Result " Result RPD Qualifiers
Percent Moisture % 39.4.' . 36.6 .7

Pace Analytical Services; Inc:
a rf �+ . ® 9800 Kincey Ave.. Suite 100
aCGAII�IIIKII Huntersville, NC.28078
www'Paw ablcom [phone]
P.
QUALITY CONTROL DATA
Project:,Ash 10/29
Pace Project No.: 92274113
QC Batch: WET/41225 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis_ Description:. 9045 pH
Associated Lab Samples: 92274113001, 92274113002
SAMPLE DUPLICATE: 1599424
30163357001 'Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 7.8 7.8 1
Results presented on this page are in the units Indicatedby the "Units" column except where.an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS -
This report shall not be reproduced, except in full,
Date: 11/11/2615 04:23 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 22

wnw.pscelebicom
Pace Analytical Services; Inc.
9800 Kincey Ave.. Suite 100
Huntersville, NC 28078
[phone]'
QUALITY CONTROL DATA
Project: Ash 10/29
Pace Project No.: 92274113
QC Batch: VVETA125320 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92274113001, 92274113002'
METHOD BLANK: 1602383 Matrix:. Solid
Associated. Lab Samples: 92274113001,'92274113002
Blank Reporting
Parameter Units Result _ Limit Analyzed Qualifiers
Phosphorus mg/kg 'ND " 2.0 11/10/15 04:34
LABORATORY CONTROL SAMPLE: 1602384
Spike LCS . LCS % Rec .
Parameter Units Conc. Result % Rec Limits Qualifiers .
Phosphorus mg/kg 50 50.2 100 90-110
MATRIX, SPIKE & MATRIX. SPIKE DUPLICATE: 1602385 1602386 "
MS. MSD
- 92274:113001 Spike Spike MS -MSD MS MSD ° /o Rec
tt Parameter Units Result- Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
l Phosphorus mg/kg
1370 81.6 79:4 1530 1360 188 -14 90-110 1.1." M6, R1
i
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY -ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11/2015 04:23.PM .. without the written consent of Pace"Analytical Services, Inc.. Page 16 of 22.

Pace Anaiyticai services, Inc.
® 980o Kincey Ave. Sufte 100.
Mnalyticai Huntersville, NC 28078
wwxcpaceiabloom [phone]
QUALITY CONTROL DATA
Project: Ash 10/29
Pace Project No.: 92274113
QC Batch:; WETA/21707 Analysis Method: SW-846 7.3.3.2
QC Batch Method: SW-846 7.3.3.2 Analysis Description: 733C Reactive Cyanide
Associated) Lab Samples: 92274113001, 92274113002
METHOD BLANK: 976738 Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide, Reactive mg/kg ND 1.0 11/03/15 18:05
SAMPLE DUPLICATE: 976734
Parameter
Cyanide, Reactive
30163640001 Dup
Units Result Result RPD Qualifiers
mg/kg 0.40U ND
y Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT -OF LABORATORY ANALYSIS .
This report shall not be reproduced, except in full, .
Date: 11/11/2015 04:23 PM, without the written consent of Pace Analytical Services, Inc.. Page 17 of 22

Signature Sheets
Signed Ash Distribution
Information Sheets

Baxter :Heiilthcare, :Corp:.
2859 Old :Linville Road
Marion, North Carolina 28752.
Ash Distribution Utilization Agreement (Valid :thru,11/30/19), . Baxter Copy
Baxter Healthcare, Corp.; is -the generator of the ash provided to . me t l N 2C (Recipient).
✓ Application of the aforementioned ash.is prohibited. except -in accordance -with theinstructions on this sheet.
v Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause. nuisances and
hazards to public. health and. safety. or otherwise cause.an-adverse impact (e.g.,:transport wet ash in'leak-proof trucks
or cover -dry ash).
Storage: The ash shall: be adequately stored to prevent ,wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the -ash slightly moistened 'will accomplish this objective under normal conditions.
However,: berms, barriers,. or tarps, may be .necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled:
Application: When using ash, the following, shall apply:
+ . The ash application rates. shallbe limited to those. that can be agronomically justified (i.e., limited to that needed.
to meet.the liming requirements_•of the crops being grown -on the land), .
✓•.. Ash shall not -be placed within one foot of the seasonal high water.table:
,�• Ash shall not be.placed within 100 feet of any water supply well or spring.unless underlain:and.overlain by.a.
liner with a maximum hydraulic conductivity of 10"6 centimeters per second: If such.a liner/cover is provided,
ash shall not be placed, within 25 feet.of any water supply well. or spring.
• The ash shall not be -applied to any site that is flooded/frozen; or snow-covered.
✓A summary of the ash chemical analyses'is located on page 2 of the information -sheet.' :Detailed laboratory, results .
are availableupon request.
Title to the ash will transfer from Baxter Healthcare, Corp to. Recipient upon delivery thereof Thereafter, Baxter:. .
Healthcare, Corp will have no responsibility and shall not be. held liable by Recipient or -any third -panty for any spill, _ ,
misuse, -misapplication or other mishandling of the ash. Recipient acknowledges. and agrees that' the ash -is being .
delivered -by-Baxter Healthcare, _Corp to Recipient as an, accommodation to Recipient: In exchange therefore,
Recipient agrees to indemnify, save .and hold. Baxter- Healthcare, Corp harmless from, -and- against any and all.
liability, damage, loss, cost; expense (including, attorneys' fees); claim, demand,. suit, action, judgment- or recovery
asserted, against.Baxter, Healthcare, Corp by any third party, including any governmental :authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with: Recipient's receipt;
.transportation, handling -or other use of the ash.
Signed (Ash Recipie ..�i�--- -//M � ate:
Ash Recipient's. Address:.
Intended Use of Ash: J .
Expected Qty/Yr: Auetof Land:.
Baxter Representative Signature:
Ppee-2 of 3
Updated: .1 1=07-14-

Baxter Healthcare, :Corp.
2859- Old Linvilleload.
Marion, North:CArolina 28752
Ash Distribution .Utilization Agreement (valid thru . 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the. generator of the ash provided to L /� e. &, Recipient).. .
Application of the aforementioned ash is.prohibited exceptin accordance with the instructions on this sheet.
Transport:. Adequate provisions shall be taken to ensure -that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g.,'transport wet ash in leak -proof trucks;
or cover. -dry. ash):
Storage: The, ash shall be adequately stored- to prevent wind_erosion or surface runoff from carrying ash into any,
surface waters. Keeping the ash slightly moistened will accomplish this objective under. normal conditions.
However, berms, barriers, or tarps; may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled. _
Application: When using ash; the following shall apply:
• The ash application rates shall be limited :to those that -can be agronomically justified (i.e., limited to that needed
to meet the liming.re uirements of the crops being,grown on
Ash shall not be placed within one foot of the seasonal high water table:. .
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10"6 centimeters per second.. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well: or spring.
• The ash shall'not be applied to any site, that is flooded, .frozen, -or snow-covered:
A summary; of the ash chemical analyses is located on pfige 2 of the information sheet. Detailed laboratory results
are available upon.request:
.Title to theash will'transfer'from Baxter Healthcare,.Corp-to Recipient.upon_delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and'shall not be: liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is' being
delivered. by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient. agrees to indemnify, save and hold Baxter Healthcare, Corp . harmless from: and against any and all
liability, .damage, loss, cost,. expense (including attorneys' fees), claim, demand;suit, action, judgment or recovery
asserted against Baxter: Healthcare, Corp by. any third, party, including any governmental authority; whether for . '
bodily injury . (including death) . or damage to property, arising from .or in -connection . with Recipient's receipt,
transportation; handling or other use of the ash.
- 3
Signed (Ash Recipient): -_ 'pia ! .G�� Date: .
Ash Recipient's Address: c7�,Jr �� +��'.��iui91., /v •`
Intended Use of Ash:
Expected Qty/Yr: s. of.Land:
Baxter Representative Signature:
.'Tag4 of 3..
Updated: 11-07-14

Baxter Healthcare, Corp.
2859 ' Ol& Linville Road'
-Mar on,.North'Carolina 28752
Ash Distribution Utilization: Agreement: (Valid thru.11/30/.19), Baxter -CopyXV
.
Baxter. Healthcare, Corp.; is. the generator of the ash provided toQ y . (Recipient):.
Application of the aforementioned ash. is_ prohibitedexcept in accordance,with theins66ctions on this sheet.
Transport. Adequate provisions shall be taken to ensure that the transportation of ash does -not cause nuisances and.
hazards to public. health and. safety. or otherwise cause.an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover.dry ash):
Storage:. The ash shall. be adequately stored. to.prevent wind. erosion orsurface runoff from carrying ash into any
surface. waters. Keeping the ash slightly moistened will accomplish :.this_ objective wader normal., conditions.
However, berms, barriers, or tarps; maybe -necessary under windy or rainy conditions or:. if erosion.or runoff cannot
be controlled.
Application: When using ash,,the following shall apply:'
• ' The ash application rates shall'.be limited to those that can be agronomically justified (Le.; limited to.that.needed
to -meet .the' liming re uirements of the. crops Hein grown on the .land) .
e
• -Ash shall not be placed within one foot of the seasonal high water table:
• Ash shall not be placed within I00'feet of. any water supply well or spring .unless underlain and overlain by a.
liner With a maximum hydraulic' conductivityof 10-: centimeters per second: - If such a liner/cover: is provided,
ash shall not be placed within 25 feet of any Water -supply wellor spring:
• The ash shall not be applied to any.site: that is flooded, frozeu, ousnow-covered.
A.summary- of -the ash chemical analyses is located on page 2 of the information sheet. Detailed: laboratory. results
are available. upon request:
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon deliverythereof. -Thereafter, Baxter_
Healthcare, Corp will have no responsibility. and shall-not-bbeheld held liable by Recipient or any third party for any spill; .
misuse, misapplication or other mishandling of the ash. Recipient acknowledges.and,agrees. that the ash -is - being .
delivered by Baxter. Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient• agrees to 'indemnify, save and- hold -,Baxter Healthcare, Corp, harmless .from,and. against.any, and -all: .
liability, damage, loss,. cost, expense (including attorneys' fees), claim;, demand, suit; action, judgment or recovery
asserted against Baxter Healthcare.. Corp by any, third party, including any governmental authority;. whether for
bodily injury -(including- death) or damage to property; -arising from or inconnection with Recipient's- receipt,.
transportation; handling or other use of the ash. -
Signed (Ash Recipient): Date: Z��
Ash Recipient's Address:,
p �
'. �
Intended Use' -of -Ash': (fro 414 u e% . j
Expected Qty/Yr. Acres of I;and: j . /0
Baxter Representative Signature: /
ge 2 of 3
-Updated: 10-22-14.:

Baxter. Healthcare,. Co
2859 Old.Linville Road
Marion,North, Carolina 29752
Ash Distribution -Utilization Agreement (Valid thru 11/30/19), .Baxter Copy
Baxter Healthcare,- Corp., is the generator .of the ash provided to: el (Recipient).
Application of the aforementioned ash is: prohibited excepHwaccordance with the instructions on this sheet.
Transport. Adequate provisions shall be taken to ensure that the: transportation of. ash .does not cause nuisances and
hazards to public health :and, safe or otherwise cause an.adverse imp act(e.g;,transport wet ash: in leak- roof trucks
or cover dry ash). t o
Storage: The ash shall be adequately stored to pievent wind erosion or surface runoff from carrying'.ash into any
surface . waters. Keeping the ash slightly moistened will accomplish this. objective under normal . conditions.
However, berms, barriers,.or tarps, may -be .necessary. under windy or rainy conditions or if erosion or-runoffcannot
be. controlled.
Application: When using:ash, the following shall apply:
• The ash application rates. shallbe limited to _those that -can be -agronomically justified (i.e., limited to. that needed .
to meet the liming requirements of the crops being grown'on the.l md).:
Ash; shall not be placed within one foot of the sea
asonif high water table.
• Ash .shall not be placed within 100' feet of any- water supply well or spring unless underlain and -overlain by a
Iiner with a maximum hydraulic .conductivity-of:10' centimeters. per second..If such a.Mer/cover is provided,
- as . shall not be placed within 25 feet of any water supply well or spring. .
• The ash shall not be.applied to.any site that is flooded, frozen, or snow-covered:
A summary of the ash chemical analyses. is located_on.page-2 of the:information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp. to-Recipient.upon delivery.thereof. Thereafter, Baxter.
Healthcare, Corp will have, no. responsibility and.shall,not be heldliable by Recipient or any third party for any spill,
misuse, misapplication or. other mishandling of the ash. Recipient acknowledges - and agrees that the ash is being
delivered_ by Baxter Healthcare,, Corp -to Recipient as an .accommodation. to Recipient. In exchange therefore,
Recipient agrees. to indemnify, save and hold Baxter - Healthcare;- Corp , harmless from and- against - any and all
.liability, damage, loss, cost, expense .(including attorneys' fees); claim,. demand, suit, action, judgment or recovery
asserted a amst Baxter. Healthcare -any- third.: -including -.any. overnmental authority, whether for
g CorprP by P�Y�. g
bodily _injury (ineluding'death) :or damage to ,property,. arising from .or.in connection with Recipient's receipt, .
tmnsportation, .handling or:oth . use -of the ash.
:Signed (Ash. Recipient): _ Date: 7 —=l
Ash Recipient's Address: 3 rij q(p Os Z 2 f Af 04 oi%C
Intended Use of Ash: L . A4 2;
Expected.Qty/Yr:. 2 to
ores o d:
Baxter Representative Signature:
Pa of. 3
Updated: M-22-14

Baxter. Healthcare, Corp.
2859 Old L- inville Road
Marion, North Carolina 28752
Ash Distribution :Utilization Agreement (Valid thlru .1 t/30/1.�9,)l, Baxter Copy
Baxter Healthcare, Corp., is the generator of.the ash provided to l� I U UU� `�� : (Recipient).
Application of the aforementioned ash is prohibited except in accordance th the instructions on.this sheet.
Transport:. Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
1 �fl►��:T.YItI� S ' i"fLu,�B�II.0 �[Q ??#,41. P:n¢ i`n`IS$;9 C" Yl'i4:tU_4.JillJU:MJ?.ii't,kCA$! QJJ lOA I LULVC.#y°-y '&, l—?LL*l iYs,�J tss."^-1 °�!'=v o-a f,:.€J
Storage: The ash shall -be adequately stored: to prevent wind erosion or surface runoff. from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, -berms, barriers, -or tarps; may be necessary under windy or rainy conditions or -if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
• . Ash_ shall not be placed within one toot of the seasonal.mgn water tame.
• Ash shall not be placed within 100 feet of any' water supply well or spring unless underlain .and overlain by a
liner with a maximum hydraulic conductivity of 10 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered:
A summary of the ash chemical analyses is located on page 2 of -the -information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare; Corp -to -.Recipient upon delivery thereof Thereafter, Baxter
Healthcare; Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. 'Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agreesto. indemnify, save and --hold Baxter Healthcare, Corp - harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third. party,. including any governmental authority, whether for.
bodily injury (including death)- or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other yse of the ash.
f A i•
Signed -(Ash Recipient):
I Q 'Id
as s
Date:
-7 1(0 J
�V
Ash Recipient's Address: 20 �
PI 11 1 Vt3
I r G
n b
Intended Use of Ash:
Expected Qty/Yr:
Baxter Represental
-7.
Updated: 11-07-14

Baxter. Healthcare, Corp.
2859 Old Linville .Road
Marion, North'Carolina 28752'
Ash Distribution Utilization Agreement (Valid, thru 11/30/19), Baxter.Copy
Baxter Healthcare, Corp., is the generator of the ash provided to gjaC .. (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the'instructions on this sheet.
Transport: Adequate provisions shall -be taken to ensure -that the transportation of ash does not cause nuisances and
:hazards to public health and safety or otherwise: cause an adverse. impact (e.g-., transportwet ash in. leak=proof trucks
or cover. dry ash). a 1 sus a sb� 't o
Storage: The ash shall -be adequately stored to prevent wind erosionor surface runoff -from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under- normal -conditions.
However, berms; barriers, or tarps, -may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
-Application: When using ash, the following shall apply:
• The -ash application. rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
• Ash shall.not be placed within.one foot of the seasonal -high water table.
•. Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with -a maximum hydraulic conductivity of 10"6 centimeters per second. If such a: liner/cover is provided,
ash shall not be placed within.25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded; frozen, or snow-covered.
A summary. of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, _Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill;
misuse, misapplication or other. mishandling of the ash. Recipient acknowledges and -agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to 'Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp- harmless from' and.against any and, all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient): CL��L� jdTtP. Date: 4 x;r
Ash Recipient's Address:�ja Z7<2
.Intended Use of Ash: G
Expected Qty/Yr: [p /�,,�. �.� Acres of Land: %S
Baxter Representative Signature:
Page 2 of 3
Updated: 11-07-14