WQ0010689_Annual Report_20150126

. col y
Annual Report Review Class A Distribution
1. Class A Annual Distribution and Marketing/Surface Disposal Certification Form
• Was a certification form submitted? Y-e-S
• Was distribution conducted during the reported year? e.S
• How many dry tons were- distributed? 1715 7 !� 7
e Were the distributions within the permitted arnount9 oS
s Were recipients information listed? 7 rec ��i s w/104corle4
• Did it indicate compliance?yd,s' a f d �� 3
® Was form complete?yam s /Q / j 11A
• Was it signed by the appropriate people? y _s A
2. -Monitoring -
• Were the analyses conducted. -at the required frequency? ps
• Were the metals analyses reported on the Residual. Sampling Summary Form? e_ s
Were the results reported in mg/kg? �-o
• Were the metals within ceiling concentration permit limits?
• Were the metals within monthly average concentration permit limits?
• If no, were the lab analyses. attached?
• Were all the required parameters tested?.
s Was. TCLP analysis conducted? Re?a;. lx �p y cl e
• Were the TCLp conta'inants-within regulatory limits? N Nj-
d'k,
3. Pathogen and Vector Attraction Re R.
® Was a signed copy of the Pa gen and Vector Attraction Reduction Form submitted?
• Did the form indicate th eriod of coverage, the residual class, and the pathogen reduction alternative and the
vector attraction redu ion option used?
• Was the appropria documentation to show pathogen and vector attraction reduction included in the report?
• Was pathogen d vector attraction reduction demonstrated according to 40 CFR Part 503 or 2T?
4. General
• . Was the report in the proper format?
Were any parts of the annual report missing?
• Was the report submitted on time?
recF"`+ u,,
Ce: I • i�v- n" AO D
ON R��s
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M S D�"i;
-Sect* n 1 Form.

CLASS A ANNUAL i)ISTRIBUTION AND .MARKETING/ SURFACE DISPOSAL CERTIFICATION ANDSUMMARY FORM.
WQ PERMIT #: WQ0010689 ]FACILITY NAME: : Baxter Healthcare Corporation. North Cove, Steam Generation Plant Ash
PHONE: [phone] COUNTY: - McDowell OPERATOR: . Baxter Healthcare
FACILITY TYPE (please eheckone): ® Surface Disposal.(complefe.Part A (Source(s).and "Residual In11 Volume only) and Part C)
Distribution and Marketing .(complete Parts A, B; and C)
Xas the facility,in operation during the past calendar year? Yes: 2 ' No ®. --► If No skip parts A, B, C and certify form below
Part,A*:
. _ Part-B*:
Sources(s)' (include NPDES # if Volume.(dry tons} . Recipient Information
Month Amendment/
applicable) Residual In Product .Out Natrie(s) Volume (dry .to
Bulking,Agent ) Intended use(s)
ranuary See DMSDF sheet
?ebruary sunnlemental fnr A.
March .
breakdown
kpril
day
rune
ruly
kngust
ieptember:
)ctober
Joveniber
)ecember
Total from FORMDMSDF. (sup)
totals: Annual (dry, tons):
1'S0
150
1565:7
1565:7
;
1715.7
:1715.7
171'5:7
: >:•:
.............
en ent s) used. Bulking Agent(s):used: Dry Wood -Chips-
If more space is required„attach additional. information sheets (FORM DMSDF- (sup
p)): Total Number of Form DMSDF (Supp) ,1
"aft C:
acility was compliant during the, past:calendar. year with all :conditions of the landapplication permit. . 'Yes -
including but not limited: to items.]-3 below) issued
-by the Division of Water
-Quality: _ ® 1Vo:-lo If No, Explain.M.Narritive
All monitoring was done.in accordance .with the permit and reported for the: year as required and three (3) copies of certified laboratory: results are attached:.
;. All operation and maintenance requirements: were compiled with -or,. in the case of a deviation, prior authorization was.received from the Division of Water. Quality:
No contravention of Ground Water Quality Standards occurred at a monitoring well.
'I certify; under penalty of.law, that the=above information is, to the best --of 7ny knowledge and belief, true ,-accurate.'and complete. Lam aware that there are significant
ienalties: for submitting:false information, including the possibility of fines and imprisonment for :knowing ;violations.'
ignature Petmittee Date; Signature of Preparer** Date
(if different from Permiftee).'
"Prepares is defined in 40 &R Part 503:9(r) and 15A NCAC 2T J 102 (26) . .
DENR FORM DMSDF (12/2006)

CLASS A A'NNUAILDISTRIDUTIGN AND MARKETING/.SURFACE DISPOSAL CERT'IFICATION.AND
SUMIVIAItY
FOIt1VI7"
Supplemental Information
WQ PERMIT #: WQ0010689 FACILITY NAME: Baxter Health-care---' Corporation North Cove Stearn Generation Plant Ash
PHONE: [phone] COUNTY: �� McDowell
>1ACILITY TYPE (please check one)::Surface Disposal (complete Part A:='!Month!!,
OPERATOR: Baxter
"S6urce(s)" and "Residual In'! columns only)
Healthcare f
. Distribution andMarketing'(coimplete. Parts:A; and' B)
Part A*:
-Part. B*::
Volume (dry tons)
Recipient Information
Month
.Sources(s)' (include.NPDES # if
.
applicable)''
Amendment/
Residual In
Product Out.
Names
Volume.(dry
Intended use(s)
Bulking. Agent.
tons)
March
March,
WQ0010689.
WQ0010689
19.79
200.71
220.50
Bobby Boone : , _ ?
220:50
Land Application
April : ,
�;�
i. I - WQ0010689:
-30.21
30.00
366.39...
.336,60 ...
-
Brian. McKinney.
-336.60,
Land Application'.
.
June.,
,�.� WQ0010689 .,
19.14
205.80
'385A1
235.8.0
404.25.
Chris .Clark- .:
235.80
Land Application
June -a
a i, -W 0010689 . .
Q
5 86
117.89
123.75
Henry:Brown . .
Terry English
.404.25
Land Application_
123,.75
Land Application
October
'ice W OO.1068.9
Q .
45.00.
349.80
3.94.80
Ray -Wits on,
394;80 .
Land, Application
:. :.:
Cotals:
Annual (dry tons):
_150
1565.7
1715,7
..::......::.....
171'S.7
Amendm6nt(s) used:
Bulking Agent(s) used
gD
Wood Chi s
If more space, is required,: attach additional information sheets (FORM DMSDF (supp)):.
.Total .Number of Form DMSDF (Supp) 1
DENR FORM. DMSDF:(8Upp) (12/2006)

ANNUAL RESIDUAL 'SAMPLING SUM
MARY FORM
Please note that -your. permit:may: containaddiiti6nal;paraneters to: be analyzed. The parameters:can be.reported,in FORM RSSF - B
WQ.Permit Number WQ0010689 :Laboratory; 1) Pace Analytical. Services .
Baxter -Healthcare :Corporation NorEh Cove
Facility Name 2)
Steam Generation Plant'Ash
ResidualSource WQ # or
NPDES
WQ0010689 ' 3)
4)
WWTP Name: NA 5) .
Residual Anahcis Dntn
Parameter
(mg/kg)
Conc.
Limit
m a-.
Sample or:Composite.Date
W'BN.PL14A4A ::'-WBNP1.14J4.A
.
WBSP411 ::
WBSP41142)
NPSEP14A1
NPSEP14B2
'Percent Moisture (%)
NA
51..3 ✓
27.9 rj.
47.6 V
54.4 6/
44 ✓
44.8
4.8
Arsenic
Cadmium
Copper
75
85
4,300
5.9 .,�
1:7.;v
78.3
.4.2
1.2
52.4 . ✓
6:1. ✓
1.2 ✓
78,2
5.5
1?4 .
80:4 tX
6.2: ..
0.99.`/
117 ✓
0.9
93.9
18:9
Chromium
Lead
NA
840
23.4.
38.8 ✓
15.4 . ►
14.5
:26.6 ,� .
20.5
25:8
2L5 ..
25.7 . ✓
95:5
11'5 r/
ND�g.®
Mercury
Molybdenum:
57
75 .
ND�.e�p ..
0:92
0.004
ND I &
ND�.0095
'1.8 .
IVDt,�pq
..2.5 '/ .:
NDi W4i
- 0.09
1:2 i/
23.8
Nickel
420
20.9
14:3 ,r
22A ✓ .
.23
28:5
Selenium
100
ND. yI,
ND �!.
NDL 7
ND y, g.
8:4
7.2 ¢/ .
293
Zinc
Total Phosphorus
Barium
7,500:
NA
NA
194:
2510 �-
1330 - ,i .
:1 24' ✓ ....
894 ✓ ..
962 ie
1,67 :::; .:
3300 ✓
1'580 '
175
3000'w-
1590.✓
348 ,/
1510
1960
915
1560
Calcium
Iron
NA
NA
79400 ✓
12900 ✓
54900
8540 : _
90200 �.:
. 15000 ✓
90200 �/
15200
1:140.00,/
10800 r/
91200 �.
8630
- - ---r- - - -------- -••- ��-• Eu -AAA AI"" .VU IIIILILb lbW«U iu.Luus corm are not appucaule: Reterence.the individual permit for metals "limits.
4':certify; under: penalty of law; that -this ,document :Was prepared: under aiiy.direction :or. supervision I accordance W th.a system designed
.to assure that qualafied.personnel.properly 'gati eyed- and. evaluated the: information:submitted : J.am aware that there -are significant
penalties for submitting false information, includingihe-possibilityof fines'and imprisonment for knowing violations:"
..
Zt� i S
Signatur \j
f Prepares.* ' Date.
*Preparer is -defined in.40 CFR Part 503.9(r): and 15A NCAC 2T :1102' '(26)'
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL, SAMPLING SUM.'
MAR FORM.- B _
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit -or were analyzed for over the past
calendar year. Use additionaf forms as needed. _
WQ Permit Number: W 0010689 .: Laboratory:. 1) Pace Analytical Services
Q Laborato '.
Baxter. Healthcare, Corporation North Cove
Facility Name: 2),
Steam Generation Plant Ask
Residual Source
WQ00.10689
3).
NPDES # or WQ#:
4)
WWTP Name: NA.,5) .
Residual Anal sis, Data. _
Sample -or Composite,
Date
Parameter
(mpg) WBNP1.14.14A . WBNPI 14.14B WBSP41141 WBSP41142 .. NESEP14Ai NPSEP14B2
Magnesium 14700 ,� 10100. ,r 16500 ,/ 161:00 23,600: a/ 19500
Manganese 2390 ,i° 16.90.4i 2900 j,,- .2960 ,., 3690 ✓ 3000
pH Not -Reported Not.Reported9 S 10:9. ,� 11:1 9.4 9:1 .
440
Potassium 19200 �,,- 13300 262QOs 27000 25360 21300 �
Silver ND .�: ;ND _/ ND � , ND. �.; e :0:86 ® 0.68 �
Sodium 4990 319.0 4010 4280 ,/ .8860 t�- 7510.
"I.certify, under penally, of law, that thisdocument was prepared under my direction or`supervision in accordance. with a. system
designed to assure that qualified personnel'pr®perly gathered and evaluated the information submitted. I am'aware that there are
significant penalties for -submitting false information, including-thepossibility of fines and.imprisonment for. know violations."
Signature of i parer* Date
*Preparer is.defined in 40 CFR Part 5019(r) and 15ANCAC 2T .1102 (26).,
DENR FORM RSSF - B.(12/2006)

205 East Meadow Road - Suite A
Eden, NC V.288
[phone]
Project WOOD BOILER POND ASH
Pace ProjectNo., 92186896
2225 Riverside 0L
Asheville, NO 2880.1
[phone]
.9830 K[3ric-2yAve; guk.el 100
RuntervAle, N.C. 28078
(.764)6.ail
Sample: WBNP1.14.1.4A Lab ID: 92186806001 Collected: 01114/1415:60 Received: 0111-7i'14114.15 Matrix: Solid
Results reported on a "dry-walght' basis
Parameters Results Units Report. Limit DF Prepared Analyzed OAS No. Qual
6010. MET -1CP Analytical Method:, EPA 601.0 Preparation Method: EPA.3050
Arsenic
6.9 mglkg
1..8
1
01j,21114 13-45
0112311415:62
744038-2
Barium
1330 mglkg
0.89
1
011/21114 13:45
01128114 15-02
-7440-39-3
Cadmium
1.7 mglkg
018
1
01J21114 113:45
01/29ii 4,11-5-02
7440-43-9
Calcium,
79400 Mgft
177
10
011211-14 la-45
01/2411412-01
7440-70-2
Chromium,
23.4 . M glkg
D�89
1.
0112V14 .13*45
01=114 1502�
744 0-4.7-3
Copper
78.8, m9/k9
0.80
1
01/21114 1145
01123/14 1 662
744o.50-8
Iron
ligod Mg/kg
17.7
1
01/21/14 1145
01123j14 15*02
7439-83-6
Lead.
38.8 Mg/kg
0.89
1
0 11211/14 13 45
6 1 /22 3114 15 :0 2
7439-92A
Magnesium
14760 mg/kg,
17.7
1
O1J21/14 13,45
61123114115-02
7439r95-4
Pfartgarlese
2.390 M Ikg,
8.9
10
011MV14 13:45
01124/14 12:01
7439-96.5
Molybdenum
.0.92 m_qlkg ,
0.89
1
01121/14 13*45
011,2 1415,02
743979 -1
Nickel
.20.9 Mq1kq
0,89
1
OU-21/14 '13-A5
011M 4 1 5i0Z
744002t0
Potassium
19200 mglkg
8850
10
OIJ21114 13.45
01/2411412:61
7440-09-7
Selenium
Na rn'Jkq
1.8
1
01/21/14 13:45
01,123/14 1&02'
77,82-49-2
Silver
IVY -mglkg
0.89
1
Olt2lj-14 13,45
�
01123,114 15.02
7440-22-4
Sodium
4990 rn/kq
885
1
01/2.1/14 13A5
01/23il 4 15:02 -
7440-23Z
Zinc
184 m gikg
1.8
1
011'/21/14 13:45
0112311415,02
7440-65 6,
5010 MET 1CP, TCLP
Analytical Method., EPA6010
Preparation Method: EPASOO
Leachate Method,'Date: EPA
131.1- 01/211114 22:30
Arsenic'
ND mg/L
0.650
1
01/23/1417,00
01/24114 161$
7440-36-2
Barium
7.0 mg/L
0�25
1
' 01123/1417,00
01124/1416:13
744 0-39-.3
Cadmium
0.020 mg/L
0-0050
1
01/23f1417=
01j24.114 16:1.3
7446-43=9
Chromium
0.040 mg/L
0.025
1
01/2311417-00
01/24j14 1'6;13
7440-47-3
Lead
0.034 mg/L
0.025
1
01123114 17:00
01/24,141613
7439-92-11
Selenium
ND mqll�
0-10
1
01/23/14 17-00
01/241141613
7782-49R2
Silver
ND mg/L
0.025
1
01/23l14 17'00
01/241141613
7440-22-4
7470 Ms rcur
-.y, TCLP
Analytical Method. EPA 7470
Preparation Mel od: EPA 7470
th
Leachate lvlethod;'Dats: EPA 1311; 01/21/14 22:30
Mercury.
ND Uq,,L-
0.26
1
01/2Z/1418.15
01/23!1418:32
7439-97-6
7471 Mercury
Analytical Method: EPA 7471
Preparation, Method: EPA 7471
Mercury.
ND m9ft
0.0073
1
01/21/1421=
OV2211415:53
7439-97v-6
Percent M oisture
Analytical Method: ASTIVI D974-87.
Percent Moisture
0.10
1
01i2111414:07
9045 OH Soil
Analytical Method: EPA 9045.
pH at 25 Degrees C
16 Std. Units
0.10
1
ISSA Phosphorus, Total
AnaVioal Method- EPA 365.1
Phosphorus
2510 mgJkg
64,2
.20
01120416:13
772 .0
T RIM. 13
101 ZR a P -3

205.5a5t f4eadow Road - Suite A 2225 Riverside Dr 980OKimeyAve. SiAG100
',AceAha1jd1ca( Eden, NC 27288 AsheAjlf, NC 28804 N"C' 28"07'6
[phone] (828)254-7,76
Project: WOOO BOILER POND ASH
Pace ProjeotNo.: 92186896
SampJe: WSNPI.14.1413 Labl[V: 92186896002
Results reported on a Wly-weight, basis
Parameters Results Units
Collected: 01/14,11415:00 ReoeWed: 01117114 14:15 Matrix: Solid
Report Limit OF Prepared Analyzed CAS No. Qual
601101MET ACP
Analyfflcaf Method: EPA6010 Preparaiion Method: EPA 3050
Arsenic
4-2 mg/kg
1.1 1.
0112111413:45
01123/14 15:08
7440-38-2
barium
962 mg/Rg
0.56 1
01/21114 13:45
01123/1415:08
7440-39-3
,Cadmium
.1.2. mgprcg
0,11 1
01121/1413:45
01011415:08
744043-9
calcium,
54900 Tng/kg
112 10
01121/1413:45
51a4/1412,,04
7440;70!-2
Chromium
15.4 mgfjKg
0-56 1
01/211141$:45
01123/141wa
7440,473
Copper
52.4 m9jkg
0.56 1
01/21/14 13:45
01123/14 15:0.8
7440-5078
fron
8640 mg/kg!
11.2 1
0 1,121/14 is I- 4s
Q1123/14 15:08
7439-89-6
Lead
14Z rng'tkg'
0.56 1
01121/14 13:45
01123/14 15.,08
709-92-1
Magnesium
10100 mgjkg
11.2 1
01/2.1/14 13:45
0119-3114 15:087489-945-4
Manganese
1690 ing/kg,-
5.6 10
01121.114 13:45
01124/14 12:04
74397!a,6-..5-
M ' 04,bdenum.
ND mg/kg
0.56 1
01/21/14l3:45
01/23/14 15 08
7439-918-7
Ticket
1+ 3 mgPKg
0.56 1
61121/14 13-45
01/23/14 15:08
7440-0Z0
13300 rng'ft
5590 10
01/21114 413:45
01124114 12-04
744,6-09-7
Selenium
ND mg/kg
I'l i
oion4 i3:45
011,23/1416:08
7782-49,2.
ND mg4kg
0,56 1
01/21,1413.,45
01123114 i5:08
744022-4
Sodium
3190 mg/kg
559 1
01/21/14 13:45
01/23/14 15:08
7440-23-5
Zinc
124 mg1kq
1.1 1
01/21114 13:45
01123114-16M
1440a&6
6010. MET JCP, TC.LP
Analytical Method: EPA 6010 Preparation Methodi EPA SGIO
L6achate,Method/Date: EPA
1311;.04122/14 21
Arsenic
ND mg!L
0.050 1
01/23/14 17:25
01124114 114,40
7440-38r2
Barium
11.1 mg,/L
025 1
01123114 4.7.25
01/24114 14A0
7440-39-3
Cadmju'm
0.023 mg/L
0.0050. 1
.0.1/23114 17;25
01/2.4/.14 14:40
744043-9
Chromium
NO, r6g/L
0.025 1
011R3,114 17:25
01/24/14 14,40
744047-3
Lead
NDm0_jL
0.025 1
0*1123114 17:25
01124114 1440
7439t92-1
Selenium
NO MgjL
0.10 1
GIJ23114 17,25
01/24j14 14:40
7782-49-2
Silver
NO mg/L
0.025 1
01123114 17-25
011204 14:40
7440-22-4
7470 Mekoury, TCLP
Analytical Method.: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA
'1 311; 01122114 21.06
Mercury
ND uglL, .
0.20 1
0112311418:30
01/24114 16:26
7439-97-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
mercury
0.0040 Mg/kg -
1.
01121114 21:30
01/22114 15:55
7439-97-6
Percent Moisture
Analytical Method: ASTM'02974-87
Percent Moisture
27.9 %
0.10 1
01/21/1414:07
9045 pH Soff
.p H at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Analytical Method EPA 9045
9.8 Std. Units�
Analytical Method: EPA 365.1
894 mglkg
0A 0 1 '
16.3 10
01/30114 15:90
01/24114 16:06 7723-14-0
I T 76;
I51! 111 11111111 1 111 1
I.-Watift li, Ji" -0 w

Pace Analytical Services, Inc. Pace Analytical Services, Inc.. Pace Analytical Services, Inc.
a ® 205 East Meadow Road- Suite A 2225 Riverside Dr. 980.0 Kincey Ave. Suite 100
Orin Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28079
www..pacelabs.com [phone] [phone] [phone]
QUALITY CONTROL DATA
Project: WOOD BOILER POND ASH
Pace Project No.: 92186896
QC Batch: MERP/6083 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis (.ascription: 7470 Mercury TCLP
Associated Lab Samples: 92186896001
METHOD BLANK: 1125986 Matrix: Water
Associated Lab Samples: 92186896001
Blank Reporting
Parameter Units. Result Limit Analvzed Qualifiers
Mercury ug/L
ND 0.20
01/2311417:50
LABORATORY CONTROL SAMPLE: 1125987
Spike
LCS
LCS
%Rec
Parameter Units
Conc.
Result
% Rec
Limits Qualifiers
Mercury ug/L
2.5
2.6
102
80-120
MATRIX SPIKE &'MATRI.X SPIKE DUPLICATE: 1126988
1125989
MS
MSD
92186822001
Spike
Spike MS
MSD
MS MSD % Rec
Parameter - Units Result
Conc.
Conc. Result
Result
% Rec % Rec Limits RPD Qual
Mercury ug/L ND
2.5
2.5 2.6
2.5
102 100 75-125 2
Date: 01/27/2014 02:11 PM
REPORT OF LABORATORY ANALYSIS.
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 18

Pace Analytical Services,. Inc. Pace Analytical Services, Inc.
aceAn4 /+� 0 205 East Meadow Road- Suite A 2225 Riverside Dr.
na�ytrca� Eden, NC 27288 Asheville, NC 28804
www.pscAbscom [phone] [phone]
QUALITY CONTROL DATA
Pace Analytical Services; Inc.
9806 KinceyAve. Suite 100 .
Huntersville; NC,28078
[phone]
Project: WOOD BOILER POND ASH
Pace Project No.: 92186896.
QGBatch: MERP/6091 Analysis Method, EPA7470.
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92186896002
METHOD BLANK: 1126927 Matrix: Water'
Associated Lab Samples: 92186896002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L NO 0.20 01/24/1415:54
LABORATORY CONTROL SAMPLE: 1126928
Spike LCS LCS :. : % Rea
Parameter Units Conc. Result % Rec Limits Qualifiers.
Mercury ug/L . 2.5 2.2 88 - 80-120
MATRIX SPIKE &-MATRIX SPIKE DUPLICATE: 1126929 1126930
MS MSD
92185790001 Spike Spike AS: MSD MS. MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Red . Limits RPD Qual
Mercury ug/L NO 2.5 2.5 2.2 . "2.2 90 :. 88 75-125 : 3
Date:'01/27/2014 62:11 PM

Pace Analytical Services, Inc. Pace Analytical Services; Inc.
Pace Analytical Services, Inc.
ee /�j,�..,,,^,J ® 205 East Meadow Road - SuiteA 2225 Riverside Dr.
�ceA lL1IXIlal
98.00 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
wwwpecele6stvm [phone] [phone]
[phone]
.QUALITY CONTROL DATA
Project: _ WOOD BOILER POND ASH
Pace Project -No.:'. 92.186896
QC Batch: ' : MERP/6080 -Analysis Method' . EPA 7471.
QC Batch Method: EPA7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92-186896001; 92186896002
METHOD BLANK: 1125341 Matrix: Solid, .
Associated Lab Sarriples: 92186896001; 92186896002
•
Blank Reporting
Parameter Units Result. " Limit" " :. Analyzed Qualifiers .
Mercury . - mg/kg ND-0.0050 01/22/14.15-13
LABORATORY CONTROL SAMPLE: • 1125.342
Spike LCS LCS . - %Rec
Parameter : Units Conc: Result % Rec. Limits Qualifiers .
Mercury mg/kg .067 O.Oti3• 95 :: .' 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: '" 1125343 A125344
MS MSD .
92-186843002. Spike : -Spike MS MSD . - MS. MSD...
°
/o Rec.. .. ,
.
Parameter Units _ Result Conc.... Conc. Result. Result %q Rec.. % Rec
Limits - RPD Qual -
Mercury. mg/kg .. ..6.055 .. .066 .073 0:10 0:11 75 . 70
75-125 : 3 M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2014 02:11 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 18,

Pace Analytical Services, Inc.
Pace Analytical Services, Inc..
Pace Analytical Services,16c.
+� a
6lCPi/`UIaIr�I
205 East Meadow Road - Suite A
2225 W r$lde Dr.
9800 KinceyAve: Suite 100
Eden, NC27288
Asheville, NC
28804
Huntersville, NC"28078
wwwpecelebacom
[phone]
[phone]
[phone] "
QUALITY CONTROL• DATA -
Project: WOOD BOILER
POND ASH
r
Pace Project No.: 9218689fi
QC Batch: MPRP/15085
' .
Analysis Method:
EPA 6010.
QC Batch Method: EPA 3050
Analysis Description:
6010 MET
Associated Lab Samples: 92186896001., 921.86896062
METHOD'BLANK: 1124474
Matrix: Solid
• Associated Lab Samplesi 92186896001; 92186896002
Blarik Reporting
• Parameter
Units ..
Result Limit
Analyzed
Qualifiers .
Arsenic
mg/kg
ND
1.0 01/23/141412
Barium
mg/kg
ND
0.50 01/23/14.14:12
"
Cadmium
mg/kg
ND
.
6.1,0 .01%23/.14.14:12
Calcium
mg/kg
= ND
10.0 01723/1414:12
Chromium
mg/kg
ND
0.50- 0.10/1414:12
.
Copper
mg/kg .
ND
0:50 .01/23/14 14:12
. -
Iro.n
mg/kg
ND
10.0- 01/23/1414:12
"
Lead
mg%kg
ND
0.56 0.1/23/1414:12
Magnesium
mg/kg
ND " .
10.0 01/23/14 14:1"2
Manganese
mg/kg
ND
0.50. 01/23/14`14:12
_.
Molybdenum
mg/kg
ND
6.50. 01/23/1414.12.
Nickel ` ..
mg/kg
ND
0.50 01/23/14 14:12
-Potassium
mg/kg
ND
50.0 01/23/14.14:12
-
Selenium
ing)kg
ND
1.0 01/23/1414:12
Silver
mg/kg
ND '."
0.50: 0.1/23/1414:12
Sodium
mg/kg .
ND
500 .01%23/14 14`.12
Zinc -
mg/kg.
ND ,
.1,0 0.1/23/14 14:12 ."
'LABORATORY CONTROL SAMPLE:
..1124475 .."
.
Spike LCS "
LCS . %.Rec..
Parameter
Units
Conc. Result
% Rec - . Limits
Qualifiers
Arsenic
mg/kg
50. 50.7
101
80-120
. .
' Barium
mg/kg.
50 51.8
-104 :-
'80-120.
Cadmium
mg/kg
50 51.3
- 103
80-120
Calcium.. _
mg/kg
500 " 509
102
80-120
.
Chromium
mg/kg
50 50:8 .
• 102 -
80-120
"
Copper
trig/kg
50 51..6
103
80-120.
.
Iron
mg/kg -
500 518
104
80-120
Lead
mg/kg
50.. 51.0
102 -
80-120_"
Magnesium
mg/kg
500 533
107
80A20
Manganese
mg/kg' .
50 _ 51.4
103
80-120
Molybdenum .
rrrg/kg
50 .53.4
107
80=120
Nickel.
mg/kg -
50 51.7
103
80-120
Potassium-
mg/kg
500 522
104
80-120 .
Selenium
mg/kg
50 51.2
10.2
807120
Silver
mg/kg
25 25.4
102
80-120
Sodium -
mg/kg
500 540
108
80-120:
Zinc
mg/kg
50 50.3'
101
80-120
REPORT OF LABORATORY ANALYSIS
This
report shail'not be reproduced, except in full,
Date: 01/27/2014 02:11 PM
without the written consent of Pace Analytical Services, Inc..
Page 9 of "19

Pace Analytical Services, Inc.
Pace Analytical
Services, Inc..
Pace Analytical Services, Inc..
t�C�A17�J I ®
r raljft al
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 I(inceyAye..Suite 100
Eden, NC 27288
Asheville;
NC 28804
Huntersville; NC, 28078
widw.pswgbscom
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILER
POND -ASH
Pace Project No.: .92186896.
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: ` 1124476
1124477'
MS MSD.
92186851015
Spike Spike,
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.. Conc. .
Result
Result.
'/o Rec
%.Rec
Limits
RPD Qual .
Arsenic
mg/kg
ND'
58 :.. 43.9
55.6
42.1
95
95
75-126
28 R1
• Barium
mg/kg
26.4
58 43.9
• .79.5
61.9
102
95
75-125
25. R1
Cadmium
mg/kg
ND
58 43:9
56.0
- 42.4
97
'97
75-125
28 R1
Calcium
mg/kg
629
580 439
1190
1010,
' 97
86.
75-125
17
Chromium
mg/kg ..
3.5
58 43.9'
60.5
46:7
98
99
75-125
26'R1 "
Copper
mg/kg
1.9
.58 43.9
.61.2.
47.2
102
103
75-126
26 R1
Iron
mg/kg
2450
580 439.
- 3340
2980
153
121
75-125
11.M1.
Lead
mg/kg
.8.5
.58 " 43.9-
64.0•
.49.0
- 96 .'
92
" 75-125
26 R1
Magnesium
mg/kg
123
580- 439
738
'589
106
106
75-125
. 22 R1
Manganese
rrtg/kg.
12.4
58 43.9
67:4'
54.0
95
95
. 75-125
22 R7
Molybdenum
mg/kg
ND.
58 43.9
56.2
- 42.6
97
97
. 75-125
27 R1 -
Nickel
mg/kg.
0.8.3
58 43.9.
-57.8
44.0
; 98.
99
75,-125'
27 R1.
Potassium,
mg/kg
ND
580, 439
893
739
- 120
123
75-125'
19
Selenium
mg/kg
ND
58 43.9
55.2 .
40A
95
92'
75-125
31 R1 .
Silver
mg/kg
ND'
29 22
28.3'
21.5
97
98
75-125
27 R1
Sodium.-
mg/kg
ND
580 439
685
533
117
1.19
75-125
:.25 R1
Zinc :.
mg/kg
9.2
58 43:9
65.5
51.9
97
97
75-125
.23 R1
REPORT
OF LABORATORY ANALYSIS
This
report shall not be reproduced, except in full,
Data: 01 /27/2014 92:11 PM
without the
written consent of Pace
Analytical, Services, Inc..
Page 10 of 18

Pace Analytical Services, Inc. Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
aceAnalyiica� a
205 East Meadow Road = Suite. A 2225 Riverside Dr.
9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, -NC 28804
Huntersville, NC 28078*
w ww.pecelabs com
[phone] [phone]
[phone]
QUALITY CONTROL DATA.
Project: - WOOD BOILER POND ASH
Pace. Project'No.: 92186896
QC.Batch:. MPRP/15117
Analysis Method:" EPA6010. '
QC Batch Method: EPA 3010
Analysis Description: 6010 MET TCLP.
Associated Lab'Samples: 92186896062.
METHOD BLANK: 1126920 :
Matrix: Water -
Associated Lab Samples: 92186896002
Blank.. Reporting.
Parameter .
Units., Result. Limit Analyzed Qualifiers
Arsenic
mg/L
- ND ' . 0:050 - 01/24/1414:11
Barium
mg/.L
: ND 0.25 01/24/1414i11
Cadmium ...
mg/L
ND ..
0.0050 01/24/1414:11
Chromium
m /L
'ND - - 0.025 01/24/14 14:11
Lead
mg/L
ND .. .0.025 01/24/1414:11
Selenium
mg/L
. ND 010 . 01%24hN 14:11:
Silver
mg/L
ND 0.025- 01/24/1414:11
LABORATORY CONTROL SAMPLE: 1126921 .
Spike LCS LCS % Rec
Parameter
Units Conc. Result. :.. %Rec Limits Qualifiers
Arsenic
mg/L
2.5 2.6 104- '80A20
Barium ,
mgfL
2.5 24 95 80-120
Cadmium
mg/L
2.5 " 2.3 94 80-120 .
Chromium
mg/L.
2.5 2:4 94 80-120 -
Lead
mg/L
2.5 • 2.2 89 80=120
Selenium
rig/L
2.5. 2.7 :107 80A20
-
Silver.
mg/L
1.2:. 1.2 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1126922 1126923
MS MSD
92185760001'
Spike _ . Spike: MS' MSD MS -MSD
% Rec'
-Parameter
Units '
Result :.' Conc. Conc. Result Result % Rec % Rec .
Limits RPD Qua[
Arsenic
mg/L
ND - - " 2.5 : .2.5 2.7. 2.7. 106 110
75-125 , _3
Barium
mg/L
0.49: 2.5 2.5 2.9 .3.0 ... 98 , • 101.
75-125 3
.. Cadmium
rig/L
ND 2.5 '. 2:5 2.4 '2.5 98 160
75-125 3
Chromium
mg/L
ND _ 2.5 . 2.5 2.4 2.5 98 100
75-125. 3 .
Lead'.
mg/L
ND 2.5 ifi. 2.3 2.4, 94' 96
75-125 3
Selenium
mg/L .
ND. _ 2'.5 2.5..." 2.8 2.9 112 115
75-125 3
Silver
mg/L
ND -1.2 1.2 1.3. 1.3 :102 104 "
75-125 2
REPORT OF LABORATORY ANALYSIS
This report shall'not be reproduced, except in full,
Date:01 /27/2014 02:11 PM
without the written consent of Pace Analytical Services, Inc..
Page.11 of 18

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
aceAnaly ical ®
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 KinceyAve. ,Suite 100
Eden, NC 27288
Asheville, NC 28804
'Huntersville, NC28078
www.pacelgbs.com
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
'.Project: WOOD BOILER
POND
ASH .
Pace Project No.:. 92186896
-
QC.Satch: MPRP/1511.8
Analysis Method: EPA 6010
QC Batch Method: EPA 3010
Analysis Description: .6010 MET TCLP.
Associated Lab Samples: 92186896001
METHOD BLANK; 1126932
Matrix:.Water
Associated Lab Samples: 92186896001
Blank Reporting
Parameter
Units . -
Result Limit. -Analyzed
Qualifiers
Arsenic
mg/L.ND
0.050.
01/24/1415:12
. Barium
mg/L
ND 0.25
01/24/.1415:12
Cadmium -
mg/L,
ND 0.0050
01124/14.15:12
Chromium
irtg/L
ND 0.025
01/24/1415:12
Lead
mg/L
ND .....0.025.
01/24/1415:12 ..
_Selenium,
mg/L
ND 0.10
01%24/1415`.12 -
Silver
mg/L
.
ND 0.025
01/24l14 15:12
LABORATORY CONTROL SAMPLE:.
-1126933 :
Spike LCS
LCS % Rec
Parameter
Units
Conc. Resuit % Rec Limits
Qualifiers
Arsenic
mg/L
2.5 2:6
404 80=120
Barium;.
mglL
2.5 2:4
97 80-120
Cadmiuni
mg/L
2.5 2.4 -
95 80-120
Chromium
mg/L
2.5 2.4
95 80-120
Lead
mg/L,
2.6 2-.3
91 ... 80=120
Selenium
mg1L,
2.5' - 2.7
107 - 80=120
Silver ..
mg%L
1..2. 1.2
99 80-120'
.
MATRIX SPIKE-& MATRIX SPIKE DUPLICATE`.. 1126934 • 1126935
MS MSD
92186822001:
Spike' Spike MS
MSD MS MSD % Rec
Parameter Units
Result
Conc. Conc. Result
Result % Rec' % Rec Limits RPD Qual
Arsenic mg/L.
ND
2.5. 2:5 2.9
2.9 115
116 75-125 1
Barium mg/L
-97.OJ:
2.5 2.5 2.8
28 108
107 75-125 1
ug/L
Cadmium mg/L
12.9
2.5 2.5 2.6
2.6 '106
105 75-125 1
ug/L .
Chromium . mg/L
.-
96.5-
-2.5- 2.5, 2.7.
2.7 .106
105 75-125 1
ug/L
Lead mglL
65.0
2.5 2.5 2.6
2,6 102'
101 75-125 1
ug/L .
Selenium mg/L
3U.8L
2.5-. 2:5, ' 3.0
3,0. 121
119 75-.125 1
g
Silver- mg/L
ND
1.2 . 1.2 .1.2
1.2. 93.
92 75-125 0.
,REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced; except in full,
Date: 01l27/2014 02:11 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of-18

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
aceAnalytical ® 205 East Meadow Road - Suite A 2225 Riverside Dr.
9800 KinceyAve. Suite 100
Eden, NC. 27288 Asheville, NC 28804
Huntersville, NC 28078
www.pscelas.00m
[phone] [phone]
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILER POND ASH
Pace Project No.: 92186896
QC Batch: PMST/6171
Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92186896001, 92186896002
SAMPLE DUPLICATE: 1124088 .
92186929001 -Dup
Parameter Units
Result Result - RPD Qualifiers
Percent Moisture %
22.9 22.4 2
SAMPLE DUPLICATE: 1124089
92186896002 -Dup
Parameter Units
Result Result . RPD Qualifiers
Percent Moisture %
27.9 46:2 49 R1
Date: 01/27/2014 02:11 PM
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 18

Pace Analytical'Services; Inc. Pace AnalyticalServices, Inc.
Pace Analytical Services; Inc. .
® 205 East Meadow Road - Suite A 2225 Riverside Dr.
aeeAnalytrcal
9800 Kiricey Ave..Suite 100
"28078
Eden, NC 27288 Asheville; NC 28804
Huntersville, NC
www.pacdaftcom [phone] [phone]
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILER POND ASH
Pace Project No.: 92186896
QC Batch: WETA/17841 Analysis Methods EPA 365:1
QC Batch Method: EPA 365.1 Analysis Description:. 365.1 Phosphorus; Total
Associated Lab Samples: 92186896001, 92186896002
METHOD BLANK: 1126549 Matrix: Solid
Associated Lab Samples: `92186896001; 92186896002.
Blank" Reporting
Parameter units. Result Limit. Analyied , Qualifiers
Phosphorus mg/kg - _ _ ND 2.0 01/24/14 15:44
LABORATORY CONTROL SAMPLE: 1:126550
Spike . LCS LCS %Rec
Parameter Units Conc: Result `. % Red Limits Qualifiers
Phosphorus rng/kg 50 50.6. 101 90-110
MATRIX SPIKE &'MATRIX SPIKE`DUPLICATE:. 1126551 1126552
MS. MSD..
92185770001 . Spike Spike MS MS MS MSD " •
% Rec
Parameter Units Result Cone. Cone. Result Result %-Rec % Rec..
Limits RP - . Qual
Phosphorus- m /k 123. 10.8 "- 11.6 1'46.. 90.2 219 -280
P 9 .9 .
90-110 47 M1,R1-
-
REPORT OF.LABORAT•ORYANALYSIS
-
This report shall not be reproduced, except in full,
Date: 01/27/2014 02:19 PM withodt the written consent of,Pace Analytical.Services, Inc..
Page 14 of 18

Pace Analytical Services, Inc.
acUAnaiyiical ®
9800 Kincey Ave. Suite 100
amrw.psaefebxcarn
HuntersJille, NC 28078
[phone]
ANALYTICAL.RESU,LTS
Project: Wood Boiler.Pond Ash 411 .
Pace Project No.:..92195461
Sample;. WBSP41141
Lab*ID. 92195461001
Collected: 04/01/14..10::10 :Received: 04/01/1:414:50 Matrix: Solid
Results reported on a 'dry weight"basis
Parameters
Results Units
Report Limit DIF
Prepared
Analyzed CA3 No. Qua[ ,
6010 MET ICIP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
6.1 mg/kg
U . 1
04/02/14 11:40
04/03/14 21:55 7440-38-2
Barium
1580 mg/kg
0.87 ..
1
...
04/02I1411:40
04/03/14 21:55 7440-39;3 .
.Cadmium ..
1.2 mg/kg
0.1.7 •1.
04/02/1411:40
04/03/14 21:55 7440. 43-9 .
Calcium ..
90200 rng/kg
173 10
04/021-1411`40
04/04/14 13:16 7440-70-2
Chromium
26.6 mglkg
0.87 1
04/02114,11:40
04/03/14 21:55 7440-47-3
Copper
78.2. mg/kg
0:87 1
04/02/14 U:40.
04/03/14 21:55. 7440-50r8
Iron
15000 rng/kg;
17.3 1
04/02/1411:40
04/0311421'55 7439-89-6,
Lead
: 20.5 . rig/kg .
6.87 ` . 1
04/02/14.11.:40
04/03/14 21:55.. 7439-92-1
Magnesium ...
16500 mg/kg .
.1 TV 1
04/02/14.1.1:40
04/03/14 21:55 7439-95-4'
Manganese
2900 mg/kg
8.7 10
04/02/1.411:40
04/04/14 13.16 7439-96-5
Molybdenum
1.8 mg/kg
0.87 1.
04/02/.14 11:40
04/03/14 21:55 `7439-W7
Nickel
22.4 rig/kg
. 0.8.7 _ - 1.
04/02/14:11:40
04/03/14 21:55 7440 02-0 .
Potassium
26200- mg/kg
8670 10
04/02/14 11:40.
04/64/1413:.16 , 7440-09-7 .
Selenium
ND mg/kg
1:7 +. 1
04/02/14 11.40
04/03/14 21:55 7782=49-2
Silver
ND mg/kg
0:87- :. 1
04/02/14 11:40
04/03/14 21:55 7440-22-4
Sodium
401.0 mg/kg
867:. 1 -
04/02/14 11:40
04/03114 21:55 7440-23-5 -
. Zinc .
167 .mg/kg
1.7, 1
04/&14 11:40
04/03/14 21:55 7440=66-6
6610-MET .ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: ,EPA 3010
Leachate Method/Date: EPA.1311;
04/01/14-19:10
Arsenic
ND mg/L
0.050.-.. 'I..
04/02/14-17:20
04/03/14.16:13..7440-38-2
Barium
3.0 mg[L
0.25. .9-
04/02/1417:20
04./03/14.16:13' 7440-39-3
Cadmium'
ND mg/L
0.0050' '1
04/02/1417:20
04/03/1416:13 7.440-43-9
Chromium
ND mg/L
'0:025 1
04/02/1417:20
04/03/14 16:13 7440-47=3
Lead
ND mg/L
0.025 1
04/02/1417:20
04/03/1416:13. 7439-92-1 •'
Selenium .' .
ND mg/L
0.10 1
04/0211417:20-
04/03/14 16:13 .7782-49-2
Silver
ND mg/L
-0.025 1
04/02/1417:20
04/03/1416:1,3 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470
. Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 04/01/14 19:10
Mercury
ND ug/L
0.20 ..1 '
04/02/1418:00
04/03/1415:50 7439-97-6.
7471 Mercury.
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Mercury
ND mg/kg- ;
0.0095 1
04/01/1'418:30
04/01/14 21:33 7.439-9T6 .
Percent Moisture
Analytical Method: ASTM D2974-87 . .
Percent Moisture
. 47.6 "%
0:10 1
04/08/14 15:43
9045. pH Soil -
Analytical Method: EPA'9045
pH at 25, Degrees C
1.0.9. Std. Units
0.10 1
04/03/14.15:24
365.1 Phosphorus, Total,
Analytical Method: EPA 365.1
Phosphorus
3300 mg/kg _ ;. _
112 20
04/15/14 16:01 7723-14-0
=
REPORT OF LABORATORY ANALYSIS.
This report shall not be reproduced, except in full,
Date.:.04116/2014 01:00 PM
without the written consent of Pace Analytical Services, Inc.. _
Page 4 of 17

aceAna1jdica1
rrnvuspacedabscom
ANALYTICAL.RESULTS .
Pace Analytical Services, Inc.
98.00 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9.092
Project: Wood Boiler.Pond Ash 4/1
Pace Project No.: 92195461 .'
Sample: WBSP41142
Lab ID` 92195461002
Collected: 64/01/14.16:15-Received: 04/01/14 11:56 Matrix: Solid_
Results reported on a 'dry-weight"basis
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No: Qua[ ,
6010 MET ICP
Analytical Method: EPA 6010
Preparation Method: EPA 3050 .
Arsenic
5.5 mg/kg
1.8 1
04/02/14 11:40 04/03/14 21:68 7440-38-2
Barium
1590 mg/kg
0.9.1 1
04/02/14 11:40 04/03/14 21:58 74,40-39=3
Cadmium .
-1:4 mg/kg
0.18 1.
04/02/14 11:40 04/63/14 21:58 7440. 43-9
Calcium
90200 mg/kg
183 10
04/021.1411:40 04/04/14 13:19 7440-70-2
Chromium
25.8 mWkg
0:91 1
04/02/14 11:40 04/03i14 21:58 7440-47-3
Copper
80.4, mg/kg
0.91 1
04/02/14 11:40 04/03/14 21t58 7440-50-8
Iron
15200 mg/kg
18.3 J.
04/02/1411 40 04/03/14 21:58 7439-89-6 .
Lead
'
21.5.mg/kg
0.91 1
04/02/1411,:40 .04/03/14 21:58 7439-92-1 , ..
Magnesium ..
16100 mg/kg
18.3 1
04/02/14.11:40 04/03/14 21:58 7439-954
Manganese
29.60 mg/kg
9.1 10
04/02/1.4 11:40 04/04/1413:19 7439-96-5
Molybdenum
2.6 mg/kg'
0.91 .1
04/02/14 11:40. 04/03/14.21:58 7439-98-7
Nickel
23.0 mg/kg
.0.9.1 1.
04/02/14',11:40 04/03/14 21:58 7440-02-0 .
Potassium
27900 mg/kg
9130 10
04/0271411:40 04/04/1413:19 7440-09-7
Selenium
ND mg/kg
18 . 1
.04/02/14 11:40 04/03/14 21:58 778249-2
Silver
ND .mg/kg
0.91-- 1
04/02/14 11:40 04/03/14 21.58 7440-22-4
Sodium T
4280 mg/kg.
9.13 1
04/02/14 11:40 04/03/14 21:58 7440-23-5
Zinc
175 rnq/kg
1..8 1`
04/02/14' 11.40 04/03M4 21:58 7440-66-6
6010 MET ICP, TCLP
Analytical ,Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA
1311; 04/01/14 19:10
Arsenic
ND mg/L
0.050 1 ...
04/02/14,17:20 04/63114.16:19 7440-38-2
Barium
2.8 m9 /L
0.25,. 1
04/02/14.17:20 04/08/1416:19 7440-39-3
Cadmium
ND mg/L
0.0050 1
04/02/1417:20 04/03/1416:19 7440-43-9
Chromium
ND mg/L
-0.025 1 .
04/02/14.17:20 04/03/14 16:19 7440477.3
Lead
ND mg/L
0.025 1
04/02/1417:20 04/03/14 16:1.9 7439-92-1
Selenium
ND. mg/L
0A0 1
04/02/1417:20 04/03/14 16:19 7782-49-2
Silver
ND 'mg/L
0.025 1
04/02/1417:20 04/03/1416:19 7440-224
7470 Mercury; TCLP
Analytical Method: EPA 7470
Preparation Method: EPA 7470
Leachate Method/Date: EPA
1311; 04/0.1/14 19:10
Mercury .
ND uglL
0.20 1
04/02/1418:0.0 04/03/14 15:53. 7439-977.6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Mercury
ND mg/kg • .
0.6097. 1' ..
04/01%14 -18:30 04/01%14 21:36 7439-97-6
Percent Moisture .
Analytical Method- ASTM D2974-87
Percent Moisture
54.4 %-
0.10 1 ..
04/08/14 15:43
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
11.1'Std. Units'
0.90 1
04/03/14 15:24
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
3000 mg/kg
91.3 10
04/15/14 16:62 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/16/2014 01:00 PM without the written consent of Pace Analytical Services,' Inc.. Page 5 of 17

Pace AnalyticalServices, Inc. -
aceAnalytilrial ®
9800 Kincey Ave. Suite 10.0
Huntersville, NC 28078
pacetabs torri
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461.
QC Batch: MERP/6415
Analysis Method; EPA7470
QC Batch Method: EPA 7470
Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92195461001, 92195461002
METHOD BLANK: 1170110
Matrix: Water
Associated. Lab Samples: 92195461001, 92195461002
Blank' Reporting
Parameter Units
-Result Limit Analyied Qualifiers
.
Mercury ug/L
ND 0.20 04/03/14.15i37
LABORATORY CONTROL SAMPLE: 1170111
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Mercury .. ug/L..
2,5 2.7 107 SO 120 . .
MATRIX SPIKE &" MATRIX SPIKE DUPLICATE: ' .1170.112_ 1170113 .
MS MSD
92193601001 .
Spike Spike MS: MSD MS MSD
%Rec
Parameter Units Result
Conc.. Conc. Result Result % Rec . % Rec
Limits ROD Qua[
. Mercury uglL ND
2.5 .. 2.5 3:1-, ;2.6 12.1 ' , 109
. 75-125 . • 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/1:6/2014 01:00 PM without the
written consent of Pace Analytical Services, Inc..
Page 6 of 17

Pace Analytical Services, Inc.
aceAnal�tieal
9800 Kincey-Ave. Suite 100
Huntersville, NC 2807&
www.pW8bhs com
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461
QC Batch: MERP/6410
Analysis Method: EPA 7471.
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated_ Lab Samples- 92195461001, 92195461002
METHOD BLANK: 1169339
Matrix: Solid
Associated.Lab Samples: 92195461001; 92195461002
Blank Reporting
Parameter Units -
Result Limit Analyzed Qualifiers
Mercury mg/kg
ND 0.0050-04/01/14 21:01
LABORATORY CONTROL SAMPLE: 116934.0
Spike ' LCS LCS . %• Red
Parameter Units
Conc: Result % Red Limits Qualifiers
Mercury .. mg/kg
.067 . 0.067 100 80-120
MATRIX SPIKE &-MATRIX SPIKE DUPLICATE: 1169341 1169342
MS MSD
92195408001
Spike Spike MS- MSD MS MSD
% Red
Parameter Units Result
Conc. Conc. Result Result % Rec % Red
Limits RPD oual
MercUry mg/kg ND',-
.056 .05.6 '0.043.. 0,:042 77 76
75-125- : -2
REPORT OF LABORATORY ANALYSIS
This
report shall not be reproduced, except in full,
Date: 04/16/2014 01:00 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 17

aoAnalyticai®
www.paWabs.com
QUALITY CONTROL DATA
Project: Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461
QC Batch: MPRP/15581 Analysis Method: EPA 6010.
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 92195461001, 92195461002
METHOD BLANK: 1169500
Associated Lab Samples: 92195461001, 92195461002
Parameter Units .
Matrix: Solid
Blank Reporting
Result Limit
Analyzed Qualifiers
Arsenic
mg/kg
ND
1.0
04/03/14 21:08
Barium
mg/kg
ND
0.50
04/03/14 21:08
Cadmium
mg/kg
ND
0.10
04/03/14 21:08
Calcium
mg/kg
ND
10.0
04/03/14 21:08
Chromium
mg/kg
ND
0.50
04/03/14 21:08
Copper
mg/kg
ND
0.50
04/03/14 21:08
Iron
mg/kg
ND'
10.0-
04/03/14 21:08
Lead
mg/kg
ND
0.50
04/03/14 21:08
Magnesium
mg/kg
ND
10.0
04/03/14 21:08
Manganese
mglkg
ND
0.50
04/03/14 21:08
Molybdenum
mg/kg
ND
0.50
04/03/14 21:08
Nickel
mg/kg
ND
0.50
04/03/14 21:08
Potassium
mg/kg
ND
500
04/03/14 21:08
Selenium
mg/kg
ND
1.0
04/03/14 21:08
Silver
mg/kg
._ND
0.50.
04/03/14 21:08
Sodium
mg/kg
ND
500
04/03/14 21:08
Zinc
mg/kg
ND .
1.0
04/03/14 21:08
Pace Analytical Services, Inc.
9800 Kincey Aye. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1169501
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec .Limits Qualifiers
Arsenic
Barium
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Zinc .
Date: 04/16/2014 01:00 PM
mg/kg
50
47.5
95
80-120
mglkg
50
47.7
.96
80-120
mg/kg
50
48.8
98
80-120
mg/kg
500
471
94
80-120
mg/kg
50
47.3
95
80120
mg/kg
50
49.0
98
80-120
mg/kg
500
486
97
80-120
mg/kg
50
47.3
95
80-120
mg/kg
500
485
97
80-120
mg/kg
50
.47.8
96
80-120
mg/kg
50
48.7
97
80-120
mg/kg
50
48.6
97
80-120
mg/kg
500
501
100
80-120
mg/kg
50
48.0
96
807120
mg/kg
25
24.2
97
80120
mg/kg
500
508
102
80120
mg/kg
50
47.2
94
80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 17

Pace Analytical Services, Inc. .
aceAnal lipal ®
9.800 Kincey Ave. Suite 100
", -
Huntersville; NC 28078
www.pacefeaeom
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1169502
1169503
MS
MSD
92195233001
Spike
Spike
MS .
MSD
MS
MSD
?/o Rec.
Parameter
Units
Result
Conc:
Conc.
Result
Result
% Rec
%.Rec
Limits
RPD Qual .
Arsenic
mg%kg
ND.
43.1
49
.40.3
45.4
93.
.92
.75A25
12.
Barium
mg/kg.
ND .
-43:1.
49
40.4
45.1 .
93.
91
75-125
11
Cadmium
mg/kg
ND
43.1
49
39.1
_ 45.6
91
93
75-125
15.
Calcium .
mg/kg
280 .
-431
490
650
737
86
93
75-125
12
Chromium
mg/kg
10.7
43A
49
50.8
56.2
93
93
75A25
10
Copper
mg%kg
.1.4
43.1
49
43.0
48.5
97
:. 96
.75-125
12 .
Iron
mg/kg
78.8
431
490
378
492.
70.
84
75 125
26 M1,R1
Lead.
mg/kg
ND
43.1 `
49.
39.4-
...44.3
91
90
75=125
. 12..
Magnesium
m /k
9 9
46.7.
431..
-.-490
448
504
93
93'
-75-125
12
Manganese
rng/kg
2.8..
43A
.49
42.5`
47.8
-
92
92
- 75-125
12
Molybdenum
mg/kg
ND,
43.1.
49.
35.8
43.5
82
.88
.75-125
19..
Nickel.
rng/kg:
4.8
43.1.
49.
45:7
51.1
95-..
95
75-125..
11
Potassium
mg/kg
ND.
431
490
_ 423J.
478J
93
93
75-125
_ Selenium
rn.
ND
.43.1
49
40.9;
45.9
95
94.
75-125
12
Silver
mg/kg
ND,'
21.6
24.5
19.1`
22:0
,
88
89 _
75-125
14
Sodium
mg/kg
550 ..
431
490
.948
1020
92
96
75-125
7
Zinc .
mg/kg
1.7
43.1
49
39.8
45.6
88.
90.
75-125
14
REPORT OF .LABORATORY ANALYSIS
This
report shall not
be reproduced, except
in full,
Date: 04/1.6/2014 01:00 PM
without the written consent of Pace
Analytical Services, Inc..
Page 9 of 17

aceAffl y kal
www.podabs.com
QUALITY CONTROL DATA.
Pace Analytical Services, Inc.
980.0 KinceyAve..Suite 100
Huntersville, NC 28078
[phone]
Project: Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461`
QC Batch: MPRP/15583
Analysis Method: EPA 6010
QC Batch Method: EPA 3010
Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92195461001, 92195461002
METHOD BLANK: 1170118
Matrix: Water
Associated Lab Samples: 921954.61001; 92195461002
Blank
Reporting
Parameter - _ Units
Result Limit
Analy2ed Qualifiers
.
Arsenic mg/L
ND 0.050
-04/03/14 15:54
Barium mg/L
ND '6.25
64/03/1415:54
Cadmium. mg/L
ND' 0.0050
_04/03/14.15:54 : -
Chromium. mg/L
ND 0.025'
04/03/14 15:54 '
Lead mg/L
ND 0.025.
04/03/1415:54
Selenium mg/L
ND 0.10
04/03/1415:54
Silver mg/L
ND 0:025
.04/03/1415:54
LABORATORY CONTROL SAMPLE: • ,11,70119 .,
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result % Rec Limits
Qualifiers
Arsenic mg/L .
2.5
2:6'
104 80-120
Barium mg/L
2.5
12 -
90 80-120
Cadmium mg/L
2.5
2.4
96 80-120
Chromium mg/L
2.5
2:4
96 80-120
Lead mg/L.
2.5
2.4
94 80A20
Selenium mglL. -
2.5
2.7
108 - 80=126
-Silver mg/L
-1.2.
1.3 :
102 .. 00-120
MATRIX SPIKE &.MATRIX SPIKE DUPLICATE:.. .1170120
1170121
MS
MSD `
92193601001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec`. - % Rec
Limits
ROD Qual
Arsenic mg/L ND
2.5
2.5... 2.81.
2.9 112
114
757125
�2
Barium mg/L ND.
2.5
2.5 2:7
2.7... 100
101
75-125
1
Cadmium mg/L - ND
2.5'
2.5 2.6
2.6 103
103
75A25
1
Chromium mg/L ND
2.5 -
2.5 2.6,
2.6 104
104
75-126
0
Lead mg/L ND
2.5
2:5 2.6
2.6 102
102
75-125.
0
Selenium mg/L ND
2.6
2.5 2.9
3.0 116
117
75-125
1
Silver mg/L -ND
1.2
1.2 1.4--
1.4 112
112
75-125
'0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date:-04/1 6/2014 01;00 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 17: .

aceAr►afytical
wwwpacelabscom
QUALITY CONTROL. DATA
Project: Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461
QC Batch: WET/30336 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92195461001, 92195461002
SAMPLE DUPLICATE: 1170868
92195093001 'Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 7.8 7.7 0
Date: 04/16/2014 01:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 17

Pace Analytical Services; Inc.
'
aceAnal ical a
9800 KinceyAve. Suite 100
Huntersville, NC 28078
www.pecelaftcam '
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Pond Ash 4/.1-
Pace Project No.:.. 92195461
OC Batch: 1NETA/18684
Aralysis Method: EPA 365.1
OC Batch Method: EPA 365:1 .
Analysis Description: .365:1. Phosphorus, Total .
Associated Lab Samples: 92195461001, 92195461002
METHOD BLANK: 1177434
Matrix: Solid
Associated Lab Samples: 92195461001; 92195461002
Blank Reporting
Parameter Units.
Result Limit Analjiied Qualifiers
Phosphorus mg/kg
ND 2.0 .04/15/1415:30-
LABORATORY CONTROL SAMPLE: 1177435
Spike. LCS LCS % Rec
. Parameter Units
Cone. Result '/o Rec . Limits Qualifers -
Phosphorus mg/kg
50 47.2 - 94 907110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: `.1177436 1177437,
MS- MSD -
- 92195456001 ..
Spike-: Spike MS: MSD MS. MSD -
%Rec
Parameter Units Result
Cone. Cone. Result -Result % Rec % Rec
Limits RPD Qual
Phosphorus rng/kg . 198
284 : 284 427. 323 81 :. 44
90-110 28 M1,R1
REPORT OF LABORATORY ANALYSIS
This
report shall not be reproduced, except in full,
.Date: 04/16/2014 01:00 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of.17 .

aceAnaljftal
witw .pndab&com
ANALYTICAL. RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville; NC 28078
[phone]
Project: Wood Boiler Ash 9/12 ".
Pace Project No.: .9221726.2
Sample: NPSEP14A1
'Lab ID: 9221,7262001
Collected: 09/12/14,12:45 ' , Received:.69/12/14 13:50 Matrix: Solid
Results reported on a 'dry -weight" basis
Parameters
Results Units
Report Limit DF
Prepared - An CAS No. Qual
8010 MET ICP
Analytical Method: EPA 6010
yt
aration Method: EPA 3050 .
Pre p .
Arsenic
6.2 ing/kg
1.5 1-
09/16/14 15:30 09/17/14 03:42 7440-38-2
Barium
1960 mg/kg
15.4 20'
09/16/14 15:30. 09/17/14 14:40 7440-39-3
Cadmium
0.99 mg/kg
05 1
09116/1415:30 09/17/.14 03:42 74.4043.9
Calcium
114000 mg/kg
308 20
09/16/14 15:30 14;40. 7440=7072
Chromium
25.7 :mg/kg
0.77' . 1
.09117/14
09/16/14 15:30 09/17/14 03:42. 7440-47-3
Copper,
117. mg/k.g
0.77 1
09/16/14'15.30 09/17/14 03:42 7440=50-8
Iron
10800 mg/kg
15.4 1
09%16114 15:30 .09/17/14 03:42 7439-89-6 •-
Lead
95.5 .mg/kg
_ 0.77 1
09/16/14'.15:30 .09/17/14 03.42 7439-92-.1.
Magnesium
2360.0.mg/kg.
.308 20
09/1611415:30- 09117/1.4.14:40 7439-95-4
Manganese.
3690 mg/kg.
15.4 20
09/16/14 15:30 09/17/14 14:40 7439-96-5
Molybdenum
0.99 mg/kg
0.77 .1
09/16/14 15:30 09/17/14 03:42 7439-98-7
Nickel
28.5 mg/kg
0.77 1,
09/16/14 15:30 09/17/14 03:42 7440-02-0
Potassium.
25300 mg1kg .
15400 20
09/16114.15:30 09/17/14 14:40 7440-094.
Selenium
8A mg/kg
1.5 1
09/16/14 15:30 09/17/14 03:42 778249-2
Silver
0.86 mg/kg
0.77 1
09/16/1415:3.0 09/17/14 03:42 7440-224
Sodium
8860 mg/kg
770. 1
09/16/1.4 15:30 09/17/14 03t42 7440-23-5
Zinc
348 mg/kg.
1.5 1
09/16/14 1530 .09/17/14 ,03:42 7440-66-6 . .
601.6 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA
1311; 09/17/14 19:00
Arsenic
ND mg/L
0.050 1
09/18/14 15:50 09/19/14 02:32 7440-38-2
Barium
4.5 mg/L
0.25 1
06/18/1415:50 09/19/14 0232 7440-39-3
Cadmium
ND mg/L
.'0.0050 : 1.
09/.18/14.15:50 .09/19/14 02:32 .7440.4379.
Chromium_
ND mg/L.
0.025 1
09/18114.15:50 09/19/14 02:32. 744047-3
Lead
`ND mg/L,
o.625 1
09/18/14 15:50 09/19/14 02:32 7439-92-1
Selenium
ND mg/L
0.10 1
09/18714 15:50 09/19/14 02:32 778249-2
:Silver
ND mg/L
0.025 1
09/18/14 15:50. 09/19/14 02:32 7440-224 .
7470 Mercury, TCLP
Analytical Method: EPA•7470'
PreparatiomMethod: EPA 7470
Leachate Method/Date: EPA
1311; 09/17/14 19:00
Mercury
ND ug/L
0.20 1 -
09/18/14 16:50 09/19/14 13:44 7439-97-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471,
Mercury
ND mg/kg
0:0061 ' 1
09/16/14 14:30 09/18/14 13:19 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
44.0.%
0.10 1
69/15/1413:17
9045 pH Soil
Analytical Method:. EPA 9045
pH at 25 Degrees C
9.1 Std.- Units .
0.10 1
09/15/14 14:10 H1
365.1 Phosphorus, Total.
Analytical Method: EPA 365.1
-
t
Phosphorus
1510 mg/kg
42.6 10
09/21/14 11:44 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 11:09 AM- without the written consent of Pace Analytical Services, Inc.. Page 4 of 17

Pace Analytical Services, Inc.
98.0.0 KinceyAve. Suite 100
ace Analyicall
wM1vwperslabs.com Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: ,' .. Wood Boiler Ash 9/12 . .
Pace Project.No.: 62217262
$ample:.: NPSEP14B2
Lab ID 922.1,7262002
Collected: 09/12/14.12:45 Received: 09/12/1413:50 Matrix: Solid
Results reported on a 'dry-weight"basis
Parameters
Results Units..
Report Limit DF
Prepared Analyzed CAS No.' Qual . .
6010 MET ICP.
Analytical Method: EPA 6010
Preparation Method: EPA 3050
Arsenic
4.8 mg/kg
1.3 1•
09/16/14 15:30 09/17/14 03:48 7440-38-2
Barium
1560'mg/kg
. 13.1 20
. '09/16/14 15:30. 09/17/14 14:44 7446-39-3
Cadmium -..
0.90 mg/kg
0:13, 1..
09/16/14 15:30 09/17/14 03:48.7440-43-9
Calcium
91200 mg/kg-
263 20
09/16/14 15:30 09/17/14 14:44 7440-70-2
Chromium
18.9 -mg/kg
0.66 _ 1
09/16/1, 4"15:30 09/17/14 03:487440-47-3
Copper '
93.9 mg/kg
0.66 : 1
09/16/14 15:30 09/17/14 03:48 7440-50-8
Iron
8630 mglkg
13.1 1
09/16/1415:30 09/17/14 03:48 7439-89-6
Lead
'.31.5 .mg/kg..
0.66 .. 1..
09/16/14 15:30 09/17/14 03:48 .7439-92-1
Magnesium
19500 mg/kg
263 - :20
09/16/14:15:30 09/17/94.14:44 7439,95 4
Manganese -
3000 mg/kg
13.1 20
. .
09/16/14 15:30 09/17/14 14:44 7439-96-5
Molybdenum
1.2 mg/kg -
0.66 .1
09/1611415:30 09/17/14 03:48. 7439-987.7
Nickei
23.8 'mg/kg .
0:66 '1
09/16/14 15:30 09/17/14 03:48 7440-02-0
Potassium ..
21300 mg/kg
1.9100 20
09/16/14 15:30 09/17/14 14:44 7440-06-7 .
Selenium
7.2 mg/kg
1.3 ' 1 -
09/16/14 100 09/17/14 03:48 7782-49-2
Silver
0.68 mg/kg
0.66 1
09/16/1415:30 09/17/14 03:48 7440-224
Sodium _
: 7516 mg/kg
657 :. 1
09/16/1415:30 09/17/14 03:48 7440 23-5
Zinc
293 mg/kg
. 1.3 1
09/16/14 15.30 09/17/14 03:48 7440-66=6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA
1311; 69/17/14 19:00
Arsenic
ND mg/L
0:050 -1
69/18/1415:50 09/19/14 02:36 7440-3$-2
Barium
4.4 mg/L
0.25. 1
09/18/14-15:50 09/19/14 02:36 7440-39-3 .
Cadmium
ND mg/L
0.0050 1
09/18/14 15:50 09/19/14 02:36 .7440,43-9
Chromium
ND. mg/L
0:025 1.
09/18/1415i56 09/19/14 02:36 7440-47-3
Lead
ND mglL
0.025 _ .1
09/18/1415:50 09/19/14 02:36 7439-92-1.
Selenium _
ND mg/L
0.10 1-
09/18/1415:50 09/19/14 02:36 7782-49-2
Silver.
ND mg!L
0.025 1
09/18/14 15-50 .09/19/14 02:36 7440224
7476 Mercury; TCLP
Analytical Method: EPA7470
.Preparation Method: EPA 7470
Leachate-Method/Date: EPA 1311; 09/17/1410:00
Mercury,
ND ug/L
0.20 1
09/18/14 16:50 09/19/14 13:47 7439-97-6
`7471 Mercury
Analyticai Method: EPA 7471
Preparation Method: EPA 7471
:. Mercury
ND mg/kg
0.0060 ' 1
09/16/14 14:30 09/18/14 13:22 7439-97-.6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
44.8. %
0.10 1
69/15/14 13:17
9045.'PH Soil
Analytical Method: EPA9045
pH at:25 Degrees C
9.1 Std. Units
0.10 1
09/16/14 14:10 H.1
365.1. Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
915 mg/kg
19.3 5
09/21/14 11'41 7723-1470
Date: 09/22/2014 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall. not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 17

aceAnaljelcal
WMpace/aba com
QUALITY CONTROL DATA
Project: Wood Boiler Ash 9/12
Pace Project No.: 92217262 .
Pace Analytical Services, Inc. _
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MERP/7094 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab.Samples: 02217262001, 92217262002
METHOD BLANK: 1288318 Matrix: Water
Associated Lab Samples: 92217262001, 92217262002
Blank Reporting
Parameter Units Result Limit Analyied Qualifiers
Mercury ug/L ND 6.20 09/19/1413:02
LABORATORY CONTROL SAMPLE: 1288319
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 .2.4 94: 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1288320 1288321 -
MS MSD
922-16155001 Spike Spike MS MSD MS- MSD %.Rec
Parameter Units Result Conc.: Conc. Result - Result % Rec %Rec Limits RPD Quaf
Mercury ug/L ND 2.5 2.5 -2.5. 2.4 95 92 75-125 3
Results presented -on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical services, Inc.. Page 6 of 17

Pace Analytical Services; Inc.
�ce J��,,,/ r^ca,�'
/`U/QI
9800.KinceyAve. Suite 100
Huntersville, NC 28078
www.pwdabs.com
[phone]'
-QUALITY CONTROL DATA
.Project: Wood Boiler Ash 9112
Pace Project No.: 92217262
QC; Batch: MERP/7090 Analysis Method: EPA7471,
QC Batch Method: EPA 7471 Analysis Description:, 7471 Mercury
Associated Lali.Samples: 92217262001, 92217262002
METHOD BLANK: 1285889 Matrix: Solid'
Associated Lab Samples: 92217262601, 92217262002
-
Blank Reporting
Parameter Units, Result Limit Analyzed Qualifiers
Mercury mg/kg ND . ' .:0.0050 •09/18d14 12:58
LABORATORY CONTROL SAMPLE: 1285890
Spike LCS LCS %Rec
"
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg .067 0.056 84. 807120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1285.891 .1285892
MS MSD .. .
92216652001 Spike Spike Ms. MSD MS MSD
% Rec
Parameter Units - Result Conc. Conc. Result. Result': % Rec % Rec
Limits RPD Qual
Mercury mg/kg ND .65 .049 0.034. 0.031 62 58
.7&125' : 8 M1
Results presented on ttiis page are in the. units indicated by the "Units" column except where an alternate unit is presented to the right of the -.result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical Services, Inc..
Page 7 of 17

Pace Analytical Services, Inc.
aceAnah/��cal ®
9800 KinceyAve. Suite 100
J -
Huntersville, NC 28078
.. w�vw.pecefabscom
ab
.
[phone]
QUALITY CONTROL DATA
Project: • Wood Boiler Ash
9/12
Pace Project No.: .92217262
QC Batch: MPRP/18906
Analysis Method:
EPA 6010
QC Batch Method: EPA 3056
Analysis Description:
6010 MET .
Associated Lab Samples: 92217262001' 92217262002
METHOD BLANK: 1286250
Matrix: Solid
Associated Lab Samples' 92217262001; 92217262002
Blank Reporting
Parameter
Units.
Result Limit
Analyzed
Qualifiers
Arsenic
mg/kg
ND
1.0 .09/17/14 02:35
Barium
mg(kg
ND
0.50 09/17/14.02:35.
Cadmium. _
mg/kg
ND,
0.10 09/17/14-02:35
Calcium
mg/kg
ND
10.0 09/1.7/1.4 02:35
Chromium
mg/kg
ND
0.50 09/17/14 02:35
Copper
mg/kg:
ND
0.50 09/17/14 02:35
Iron
mg/kg.
ND'
10:0 09/17/14 02:35.
Lead
mg/kg "
ND'
0.50 09/1.7/14 02:35
Magnesium
mg/kg
-ND
10.0: 09/17/14 02:35
Manganese
mg/kg
ND
0.50 09/17/14 02:35
Molybdenum
mg/kg
ND
0.50. 09/17/1414:00
Nickel
mg%kg
ND
0.50 .09/17/94 02:35,
Potassium
rrig/kg
ND
500 09/17/14.02:35
Selenium
mg/kg-
ND
1:0 - 09/11/14 02:35
"
Silver
mg/kg
ND
0:50. 09/17/14 02:35
mg/kg -
ND
560 09/17/14 02:35
_Sodium
Zinc
mg/kg.
ND
1.0 09/17/14 02:35 ...
.
-LABORATORY CONTROL SAMPLE:
1286251
Spike LCS
LC8 %
Rec
Parameter
Units,
Conc. Result
% Rec ..Limits Qualifiers
Arsenic -
rng%kg
50 48.7
97
80-120
Barium
mg/kg
50 50;5
101
80-120. '
Cadmium .
mg/kg
50 . ,' 48.8
98.
80-120
Calcium
mg/kg ` :
500 485
97
80-120
Chromium
ing%kg
.50 48.8
98
80-120
Copper .
mglkg
50 50:6
101
80=120.
Iron
mg/kg .
500 500
100
80-120
Lead
mg/kg'
50 49.5
99
80-120
Magnesium
mg/kg ...
500 512
102.
80-120
Manganese
mg/kg .
50 49.1
98
80-120.
Molybdenum
mg/kg v
50 . 52.9
106
80-120
Nickel
mg/,kg -
50 49.7
99
80-120
Potassium
mg/kg
500 496J
99
80-120
Selenium
mg/kg
50 49.8
100
80-120
Silver
mg/kg
25 24.4
98
80-120
Sodium ,
mg/kg
500, 486J
97
80-A20
Zinc
mg/kg
50 47.8"
96
86-120
Results presented on this
page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result:
REPORT OF LABORATORY ANALYSIS.
This report shall not be reproduced,
except in full,
Date: 09/22/2014 11:09-AM
without the
written consent of Pace Analytical Services, Inc..
Page 8 of 11 .

auuAnalytical
www.pacefebscom
QUALITY CONTROL DATA
Project: Wood Boiler Ash 9/12
Pace Project No.: 92217262 "
Pace Analytical Services; Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1286252
1286253r
MS
MSD
92217197001
Spike
Spike
MS'
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
ND
239
239
.237
239
99
100
75-125
1
Barium
mg/kg.
284
239
239
.540
512
107
95
75-125
5
Cadmium
mg/kg
ND
239
239
222
222
93
93
75-125
0
Calcium
mg/kg
21600
23.90
2390
25200
22900,
151
55
75-125
.10 M1
Chromium
mg/kg
11.6
239
239
241
237
96
95
75-125
2
copper
mg/kg
378
239
239
653
615
115
99
75-125
6
Iron
mg/kg
3470
2390
2390
5820
5510
98
86
75-125
5
Lead
mg/kg
5.9
239
239.
228
228
.93
93-
75-125
0
Magnesium
mg/kg
2730
2390
2390
5280
5610
107
96
75-125
5
Manganese
mg/kg
140
239
239
374
361
98
92
75-125
4
Molybdenum
mg/kg
9.9
239
.239
237
240
95
96
75-125
1
Nickel
mg/kg,
8.4
239
239
236
236 -
95 .
95
757125
0
Potassium
mg/kg
ND
2390.
2390
4880
4620
139
128
75-125
5 M1
Selenium
mg/kg
4.8
239
239
252
247
103
101
75-125
2
Silver
mg/kg
2.6
119
119
119
119
98
98
75-128
0
Sodium
mg/kg-
ND
2390
2390
3800
3590
123
1.14
75-125
6
Zinc
mg/kg _
629
239
239
906
844
116
90
75-125
7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 17

Pace
Analytical Services, Inc.
ac,i� n�Io �¢� '
l
9800 Kincey Ave. Suite 100
V /"11!
Huntersville; NC 28078
w wpacelab corn
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Ash 9/12
Pace Project No.: 92217262
QC Batch: MPRP/16923
Analysis Method: EPA 6010
QC Batch Method: EPA 3010
Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92217262001, 92217262002
METHOD BLANK: 1288252
Matrix: Water
Associated Lab Samples: 92217262001,
92217262002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Arsenic
mg/L
ND 0.050
09/19/14 01:04
Barium
mg/L
ND 0.25
09/19/14 01:04
Cadmium
mg/L
NJ) 0.0050
09/19/14 01:04
Chromium
mg/L
ND 0.025
09/19/14 01:04
Lead
mg/L
ND 0.625
09/19/14 01:04
Selenium
mg/L
ND 0.10
09/19/14 01:04
Silver
mg/L
ND 0.025
09/19/14 01:04
LABORATORY CONTROL SAMPLE: 1288253
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result %Rec Limits
Qualifiers
Arsenic
mg/L
2.5 2.6
106 80-120
Barium
mg/L
2.5 2.5
100 80-120
Cadmium
mg/L
2.5 2.6
104 80-120
Chromium
mg/L
2.5 2.5
100 80A20
Lead
mg/L
2.5 2.4
97 80-120
Selenium
mg/L
2.5 2:7
107 $0120
Silver.
mg/L
1.2 1.3
102 WAN
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 1288254 1288255
MS MSD
92216155001
Spike Spike. MS
MSD MS MSD
% Rec
Parameter
Units Result.
Conc. Conc. Result
Result % Rec - % Rec
Limits
ROD Qual
Arsenic
mg/L ND
2.5 2.5 2.7
2.7 107
107
.75-125
0
Barium
mg/L 3.8
2.5 2.5 6.3
6.5 101
110
75-125
3
Cadmium
mg/L 0.21
2.5 2.5 2.8
2.9 105
106
75-125
1
Chromium
mg/L ND
2.5 2.5 2.5
2.5 99
100
75-125
1
Lead
mg/L 3.9
2.5 2.5 6.2
6.4 92
99
75-125
3
Selenium
mg/L ND
2.5 2.5 2.7
2.7 108
108
75=125
0
Silver
mg/L ND
1.2 1:.2 1.3
1.3 103
104
75-126
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is: presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical Services, Inc..
Page 10 of 17

aceAnalytical
wwrwpacelabs.cam
QUALITY CONTROL DATA
Project: Wood Boiler Ash 9/12
Pace Project No.: 92217262
QC Batch: PMST/7035 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 " Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92217262001, 92217262002
SAMPLE DUPLICATE: 1285024
92215495001 Dup
Parameter Units Result Result ROD Qualifiers
Percent Moisture % 39.6 29.4 29 R7
SAMPLE DUPLICATE: 1285025
92217262002 Dup
Parameter Units Result Result RPD. Qualifiers
Percent Moisture % 44.8 45.6 2
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical Services, Inc..
Page 11 of 17

Pace Analytical Services, Inc.
�y, /l
aCe CIna f l
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
vimpaMabscom
(704)875=9092
QUALITY CONTROL DATA
Project: Wood Boiler Ash 9/12
Pace Project. No.: 92217.262
QC Batch: WETA/20300 Analysis Method: EPA 365.1 .
QC Batcli Method: EPA 365.1 Analysis Description: 365:1 Phosphorus, Total
Associated Lab Samples: 92217262001, 92217262007
METHOD BLANK: 1289341 Matrix:, Solid
Associated. tab Samples: 92211262001i 92217262002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 2.0 09/21114-11:13
LABORATORY CONTROL -SAMPLE: 1289342
Spike LCS LCS. % Rec'
Parameter Units Conc: Result- % Rec Limits Qualifiers
Phosphorus mg/kg '50 51.9. 1,04 • 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1289343 :1289344
MS MSD
922116551001 Spike Spike MS MSD' Ms MSD.
%-Rec . .
Parameter Units . Result. Conc. , Conc. Result Result % Rec % Rec _
Limits . RPD Qua[
Phosphorus mg/kg 178 -229 215 333. -381 68 95
90-110 . •14 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the .result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical Services, Inc..
Page 13 of 1-

Baxter Healthcare, Corp,
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet Return this sheet to Ricky Styles: .
Baxter. Healthcare, Corp.;, is the generator of the a'sh,provid6d.to fseo 6l0.
Reci lent A lication. of the aforementioned ash is prohibited, e�t in accordance h ie
( p' ) Pp
instructions on this sheet:
Transport: Adequate provisions shall be taken to ensure that the- transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage.. The'ash shall be adequately stored to prevent wind" erosion or surface runoff from carrying, ash:
into any surface waters.. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms; barriers, or. tarps, .may be necessary under windy or rainy conditions or if
erosion. or runoff cannot be.controlled:
Application: When using ash, the following shall apply;
• The ash application.rates shall be'limited to those that can be. agronomically justified (i.e., lirriited.to: .
that needed to meet the liming requirements of the crops being grown on the land).
. Ash shall not be: placed within 50 feet.of any su.0acewater: .
• Ash shall riot be placed within one foot of the seasonal high water table. -
Ash shall not be placed within 100 feet of any water. supply well -or spring unless underlain and.
overlain by a liner with a maximum hydraulic conductivity of 10'6 centimeters per second. If such a.
liner/cover is provided; ash shall not be placed within 25 feet of any watersupply well or spring..
• The ash shall not be applied to any site that'is. flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information. sheet.. Detailed
laboratory'results are available upon request.
Title to the ash 'Will transfer from'Baxter Healthcare, Corp to Recipient upon.delivery thereof. Thereafter,
Baxter Healthcare., Corp will have no responsibility and shall not be held liable by: Recipient or any third
party for any spill, misuse,. misapplication or other.inishandling 'of the .ash.. Recipient acknowledges and
agrees -that -the ash is being delivered by Baxter Healthcare, Corp to.Recipient as an accommodation to
Recipient. In exchange. therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare,. Corp .
harmless from and against any and .all liability, damage, loss, cost, expense (including attorneys'. fees), .
claim, demand, suit, 'action, judgment or. recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental :authority, .whether for bodily injury (including death) or damage to
property, arising from or in connection, with Recipient's receipt, transportation, handling or other use of
the ash. -
Signed (Ash --Recipient): Date:
r t /
Ash Recipient's Address: % G(
'Alt
Intended Use of Ash:
Expected Qty/Yr: ��� ' Acres of Land:
Page 1 of 3.
Updated: 3/5 2

Baxter Headtheare, Con
M, rioag"Nart t.Cnrolina 28`52
Ash Distribution Program Information Sheet
Baxter Healthcare, Corp., is the generator of the ash 'provided to
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions. shall be taken to .ensure that the transportation of ash does not cause
nuisances and hazards to public. health and.safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry. ash).
Storage: The ash shall be, adequately stored .to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash.slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers; . or. tarps; may. be necessary under windy or rainy conditions or if
erosion 'or runoff cannot. be controlled..
Application., When using ash, the following shall apply:
®. The ash application rates shall be ,limited to those that can be agronomically justified (i.e,; imited to
that needed to meet the liming requirements of the crops,being grown on the land).'
Ash shall not be placed within 50 feet of any surface water:
• . Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within .100 feet of any water supply well or spring unless- underlain and
overlain by a 'liner with a maximum hydraulic conductivity of 10 centimeters per second.' If such a
liner/cover is provided; ash shall not be placed within 25 feet of any water supply well or spring:
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash. chemical analyses. is. located on page 2 of the information sheet. Detailed
laboratory results are available upon request..
.Title, to the ash will transfer from Baxter. Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any.third
party or any spill, misuse; misapplication or other mishandling of the. ash. Recipient. acknowledges and
agrees..that the ash is being delivered by Baxter Healthcare, Corp- to Recipient as :an accommodation to
Recipient. In exchange therefore, Recipient -agrees to indemnify; save and hold Baxter Healthcare, Corp
harmless from and a ainst an .. and all liability, damage, _ loss, cost; expense (including attorne s' fees
g Y h'� g Y ).
claim, demand, suit,action;. judgment or recovery ;asserted.against Baxter Healthcare, Corp by. any third
:.party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling'or other use of
the ash. - c
i>
Signed (Ash Recipient): i'` � C.c.�1 d /� p si /Sc Z-I Date: /l ��" l
Ash Recipient's Address: Z : �h ti J"') L''/1:U
Intended Use of Ash: . Air iG L r
Expected Qty/Yr:
Page 1 of 3
Acres of Land:%
Updated: 3/5/10

Baxter Healthcare, Corp®
2559 ®id Linville Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet, Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to g o` & A 4
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be.adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash; the following shall apply:
o The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land).
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): Date: %-Z/-4 i
Ash Recipient's Address: T ,2 7,_ o ld'r Z;N o . Me 12U4 c/
r
Intended Use of Ash: S® `w V 1��L ni e a/1"
/Yr: Expected Qt
p y � ��� ��a/ Acres of Land: l �EJe_
Page 2 of 3
Updated: 9-12-13

Baxter Healthcare, Corp®
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet — Return this sheet to Ricky Styles
Baxter Healthcare, Corp., is the generator of the ash provided to (Recipient). . Application of the. aforementioned ash is prohibited ex%ti accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet .ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters.. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash; the following shall apply:
® The ash. application rates shall be limited to.those that can be agronomically -justified (i.e., limited to
that needed to meet the liming requirements of the crops. being grown on the land).
® Ash shall not be placed within 50 feet of any surface water.
• Ash. shall not be placed within one foot of the seasonal high water table.
• .Ash shall not be placed within l00 feet of any water supply well or spring unless underlain. and
overlain by. a liner with a maximum hydraulic conductivity of 10 centimeters per second. If such a
liner /cover.is provided, ash shall not be placed within 25 feet of any water supply well or.spring.
The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the. information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery.thereof. Thereafter,
Baxter Healthcare, Corp will have no .rey and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or`other mishandling of.theash. Re
mcipient acknowledges arid,
agrees that the ash is being delivered by Baxter Healthcare; Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees -to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all. liability, damage, loss, cost, expense (including attorneys' fees),
claim; demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): n- ^. Date: '
Ash Recipient's Address: k_,4-,,
Intended Use of Ash: b`
Expected Qty/Yr: Acres of Land: Ile
Page 1 of 3
Updated: 3/5/12

}
Baiter Healthcare, Corp.
2559 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Program Inf®rmati®n Sheet
Baxter Healthcare, Corp., is the generator of the ash. provided to N 6 C_ZS A 4,7ig Y
(Recipient). Application of the aforementioned ash is prohibited except in accordance with •the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the . transportation of ash 'does not cause
nuisances and hazards to public health and safety or otherwise cause an'adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry. ash). .
Storage: The ash shall' be adequately. stored, to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective. under iformal.
conditions. However, berms- barriers; or, tarps, may be necessary under windy or rainy conditions or if
erosion. or runoff cannot be .controlled.
;Application: When using ash, 4h e following shall apply:
• The ash application rates shall be limited to: those that can be agronomically justified (i e:- lute ted tp�
that needed to meet the liming requirements of the crops being grown.on the land).,
Ash shall not be placed within 50 feet of any surface.water:
s Ash shall not be placed within one foot of the seasonal high water table.
Ash shall not be placed within: 100. feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of YO"6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed.within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen; or snow-covgrod.
A . summary of the. ash: chemical analyses is located on page 2 _ .of the information sheet:, Detailed
laboratory results are available upon request:,
Title to the. ash will transfer from Baxter' Healthcare; Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any.third
party. for any spill; misuse; misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In :exchange therefore; Recipient agrees to indemnify; save .and hold Baxter Healthcare; Corp
harmless: from and against any and all liability, damage, loss, cost; expense (including=74ttorneys'. fees),
claim; demand, ,suit, action, judgment .or recovery asserted against Baxter Healthcare, Corp by any third
party, .including any governmental authority, whether for bodily injury including• death) or damage to
property, arising from or in connection with Recipient's. receipt; transp rtatio hZa rdlut or other use of
the ash.
Si ed Ash Recipient):. v !/ Date:
Ash Recipient's Address:
!/ 2je)N.
Intended Use of Ash:
Expected Qty/Xr: Acres of Land: - t>
'Page 1 of 3
Updated: 3/5110

a
f^
aiter { +tip `urpE
�r > riou, Nloo t apt o itt« 4is
Ash Distribution Program Information Sheet
Baxter Healthcare, Corp., is the generator of the ash provided to
(Recipient). Application of the aforementioned -ash is prohibited except in accordance with- the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff. from carrying .ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessaryunder windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e.,' limited to
that needed to meet the liming requirements of the crops being grown on! the land).
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10,6.centimeters per second. If such a
Iiner%coves is provided, ash shall not be placed within 25 feet. of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare; Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibi.lity'and shall not be held liable by Recipient or any third
party for any spill,.misitse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),,
claim, demand, suit; .action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transp ation;- andling or other use of
the ash.
Signed (Ash Recipient): 61 % Date:
Ash Recipient's Address:
e
Intended Use of Ash:
Expected Qty/Yr: > _l 06al, et
Page I of 3
Acres of Land:.yG
Updated: 3/5/ 10