WQ0010689_Annual Report_20080211

Z>;0powe"I Inc,
Nov' Cove apo%
pr-tli&(ad'
Annual Report Review Class A Distribution
1. Class A Annual Distribution and Marketing/Surface Disposal Certification Form
• Was a certification form submitted? y,ds
• Was distribution conducted during the reported year? y'P-
• How many dry tons were distributed? 18 � 1 ° 219T
• Were the distributions within the permitted amount? '� �S
• Were recipients information listed? y-e-S I lire re-C Ld
• Did it indicate compliance? y AS � N ° CO ^^ f� �' a'� r d . /isA)
• Was form complete? �J 'J-s �s
• Was it signed by the appropriate people? y ee'
2. Monitoring
• Were the analyses conducted at the required frequency? �S
• Were the metals analyses reported on the Residual. Sampling Summary Form? y� 1
® Were the results reported in mg/kg?yvs
• Were the metals within ceiling concentration permit limits? y,e-3
• Were the metals within monthly average concentration permit limits? N3 N o
• If no, were the lab analyses attached?
• Were all the required parameters tested? No - `fob al PhDs _ P�&tss� n5 U-
• Was TCLP analysis conducted?
re-g"°rid NAvi- CP Sa �[es -� 7
® Were the TCLP contaminants within regulatory limits?
3. Pathogen and Vector Attraction Reduction N A e s ,� �s V
• Was a signed copy of the Pathogen and Vector Attraction Reduction Form submitted?
• Did the form indicate the period of coverage, the residual class, and the pathogen reduction alternative and the
vector attraction reduction option used?
• Was the appropriate documentation to show pathogen and vector attraction reduction included in the report?
• Was pathogen and vector attraction reduction demonstrated according to 40 CFR Part 503 or 2T?
4. General
• Was the report in the proper format?��
• Were any parts of the annual report missing? 0
Was the report submitted on time? �'O3

Energy Generation NA
February 11, 2008
VIA FEDERAL EXPRESS # 790448522402
NCDENR-DWQ
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: 2007 Annual Ash report
Permit No. WQ0010689
SUEZ Energy BioPower, Inc — North Cove, NC
ECE V 10
FEB 25 20u0
Asheville Regional Office
Enclosed is the annual ash distribution report for calendar year 2007, using the forms
provided by NCDENR-DWQ. During 2007, ash was distributed in only one form.
Flyash that was settled in the scrubber ponds was mixed with flyash from the
multicyclone and dry wood to reduce the moisture content. The ash was distributed for
land application in this form.
An average moisture content (52.2%) was obtained from several samples collected and
analyzed periodically throughout the year. A composite sample was collected for
chemical analysis from the final product prior to distribution. All samples were analyzed
by Pace Analytical Services, Inc., a North Carolina -certified laboratory.
The facility received one Notice of Violation from the state for not performing the
required annual ignitability and corrosivity test in 2006. Also, the facility received and
paid one civil penalty in the amount of $832.95 for distributing ash with the average
monthly concentration of arsenic above 41 mg/kg. Refer to page 2 of the report for a
more detailed explanation. Also, copies of the NOV and assessment of the civil penalty
are included in the report.
Under section III.4 of the permit, we are required to test for the total phosphorus with
every ash analysis. On January 31, 2007, the total phosphorus was not included in the
sample analysis. Please note that we tested the ash 7 times and are only required to test
the ash 6 times throughout the year. Refer to page 2 of the report for a more detailed
explanation.
REcRENED
SEC
Cll1Pom PSS 11

If you have questions or require additional information, please contact Frankie Fox or
Summer Barber at 828-287-8834 or Tony Leopard at 828-287-5886.
Sincerely,
V�
Tony eop d
Plant Manager
Enclosures - DWQ Reporting Forms
Ash Distribution Records
1/31/07 Pace Analytical Services, Inc. report
5/11/07 Pace Analytical Services, Inc. report
7/7/07 Pace Analytical Services, Inc. report
11/1/07 Pace Analytical Services, Inc. report
Copy of NOV and civil penalty
cc: NC Division of Water Quality (3 additional copies w/ enclosures)
Ricky Styles
Melinda Allen -file

ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit#: WQ0010689 County: McDowell Year: 2007
Facility Name (as shown on permit): SUEZ Energy BioPower, Inc. - North Cove
Land Application Operator: SUEZ Energy BioPower, Inc. Phone: [phone]
Land application of residual solids as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Total number of application fields in permit: 1 9
Total number of fields land application occurred during the year: 3
Total amount of dry tons applied during the year for all application sites: 1881.3
Total number of acres land application occurred during the year: 150
Part B:
Facility was compliant during calendar year 2007 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Quality. ❑ Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violati
Tony Leopard, Plant Manager
Permittee Name and Title (type or print) Sigaitf& f Pe ittee Date
2-15-o$
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r)
Page 1 DENR FORM ACF (5/2003)

On November 1, 2007, SUEZ Energy BioPower, Inc. received a Notice of Violation for
not conducting the annual ignitability and corrosivity test in 2006 as required in section
III.3 of the permit. Also, on November I", we received a civil penalty in the amount of
$832.95 for distributing ash in May of 2007 with an average arsenic concentration of 51
mg/kg. Section I1.5 of the permit establishes the maximum allowable average
concentration as 41 mg/kg. This non-compliance issue was due to a misinterpretation of
the permit.
Also, we are required under section IIIA of the permit to test for the total phosphorus
with every analysis. On January 31, 2007, the total phosphorus was not included in the
sample analysis. Please note that we tested the ash 7 times and are only required to test
the ash 6 times throughout the year. This was an oversight by the sampler and was
noticed during the preparation of the annual report.
We have a new environmental representative who is supervising all ash analysis requests
and results. She implemented a new procedure requiring an ash distribution approval
form that must be signed by the environmental representative, plant manger, and plant
superintendent before the distribution of ash. We feel that her supervision in these areas
will ensure compliance in the future.
Page 2

ANNUAL DISTRIBUTION AND MARKF;TING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
PERMIT #: WQ0010689 FACILITY NAME: SUEZ Energy BioPower, Inc. - North Cove
PHONE: [phone] COUNTY: McDowell OPERATOR: SUEZ Energy BioPower, Inc.
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? 10 Yes []No No If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
January
February
March
April
Flyash with wood
864
Bobby Boone
451.008
Land Applic.
May
Flyash with wood
900
Max Holland
469.8
Land Applic.
June
July
Flyash with wood
880
Henry Brown
459.36
Land Applic.
August
Flyash with wood
September
October
November
Flyash with wood
960
HenryBrown
501.12
Land Applic.
December
Totals:
Annual (dry tons):
0
0
3604
1881.288
Amendments used:
I NA
Bulking Agent(s) used:
I NA
* If more space than given is required, please attach additional information sheet(s). El Check box if additional sheet(s) are attached
Part C:
Facility was compliant during calendar year 2007 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality. ❑v Yes ❑ No If No, please provide a written description why the facility was not compliant.
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water
Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware
tha7th reare 'g icant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signatur of Pe ittee Date Signature of Preparer* * Date
(if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r)
Page 3 DENR FORM DMSDF (11/2005)

Ach InvPntory
Date
Estimated Tons
Ash Reused
Type Ash
Recipient
Approx. Amt. Remaining in
Inventory
Comments
Intended Use
1/29,30/07
SCRUBBER/SANDBOX
DRYING, MIXING WOOD SOUTH POND, PACE
PICKED UP ASH SAMPLES, 1/31/07
Dry Tons
Distributed
4/2,3/07
864
SCRUBBER/SANDBOX
BOBBY BOONE
SOUTH POND CLEANED
70 TONS WAS WOOD
451.0 jSoil
Amendment
5/7/07
900
SCRUBBER/SANDBOX
MAX HOLLAND
NORTH POND CLEANED
80 TONS OF WOOD ADDED
469.8
Soil Amendment
7/23/07
880
SCRUBBER/SANDBOX
HENRY BROWN
SOUTH POND CLEANED
80 TONS OF WOOD ADDED
459.4
Soil Amendment
11/30/07
960
SCRUBBER/SANDBOX
HENRY BROWN
NORTH POND CLEANED
100 TONS OF WOOD ADDED
501.1
Soil Amendment
Total Tons
3604
1881.3
Note: Scrubber ash includes sandbox ash used to dry ponds
Ash Pond Activitv
Date
Pond Side
Excavated
Tons Wood Added
Wood Moisture as
added
Dry Tons (Wood Added)
Ash Moisture as Hauled (measured)
1/29/07
south
10
10%
9.0
52.2%
1/30/07
south
10
10%
9.0
52.2%
2/5107
south
10
10%
9.0
52.2% "
2/6/07
south
10
10%
9.0
52.2%
2/12/07
south
10
10%
9.0
52.2%
2113/07
south
10
10°%
9.0
52.2%
2/20/07
south
10
10%
9.0
52.2%
3/13/07
NORTH
10
10%
9.0
52.2%
3/22/07
NORTH
10
10%
9.0
52.2%
3/29/07
NORTH
10
10%
9.0
52.2%
4/3/07
NORTH
10
10%
9.0
52.2%
4/5/07
NORTH
10
10%
9.0
52.2%
4/9/07
NORTH
10
10%
9.0
52.2%
4/17/07
NORTH
10
10%
9.0
52.2%
4/19/07
NORTH
10
10%
9.0
52.2%
4/30/07
NORTH
10
10%
9.0
52.2%
614/07
south
10,
10%
9.0
52.2%
6/5/07
south
10
10%
9.0
52.2%
6/11/07
south
10
10%
9.0
52.2%
6/14/07
south
10
10%
9.0
52.2%
6/15/07
south
10
10%
9.0
52.2%
6/19/07
south
10
10%
9.0
52.2%
7/12107
south
10
10%
9.0
52.2%
7/13/07
south
10
10%
9.0
52.2%
11/1/07
north
10
10%
9.0
52.2%
11/2/07
north
10
10%
9.0
52.2%
11/5/07
north
10
10%
9.0
52.2%
11/6/07
north
10
10%
9.0
52.2%
11/8/07
north
10
10%
9.0
52.2%
11/9/07
north
10
10%
9.0
52.2%
11/12/07
north
10
10%
9.0
52.2%
11/13/07
north
10
10%
9.0
52.2%
11/15/07
north
10
10%
9.0
52.2%
Total Tons Wood Added
1 330
297.0
-
Page 4

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0010689 Laboratory: 1) Pace Analytical Services, Inc.
Facility Name: SUEZ Energy BioPower, Inc. - North Cove 2)
NPDES # or WQ0010689 3)
WQ#:
4)
WWTP Name: 5)
Residual Analvsis Data
Sample or
Composite Date
Flyash
1/31/07
Flyash
5/11/07
Flyash
5/11/07
Flyash 1
7/07/07
Flyash 2
7/07/07
Flyash 3
07/07/07
Flyash
11/01/07
Flyash
11/01/07
- - -- -- - ------
+ i,
( < S �
( /6\ 0-
( o,\ �t„vnt d
tr4iW eew-ey
- - - --
Percent Solids
62
40.6
48.8
45.2
45.8
45.7
48
44.6
q--
CD
y
Arsenic
16
71
31
29
32
24
11.7
10.1
Cadmium
2.6
4
2.6
2.1
2.1
1.4
0.44
0.54
Chromium
36
63
44
26
29
18
10.5
12.7
Copper
100
140
110
76
79
61
50.1
86.6
Lead
33
71
32
.40
40
33
23
27.9
Mercury
-
<.0078
0.057
0.015
0.021
0.021
<.012
<.010
<.011CD
Molybdenum
<.66
3.1
<.78
1.4
1.6
1.2
<.91
<1.1
Nickel
26
21
23
13
14
8.9
6.5
7.8
Selenium
<1.3
1.6
<1.6
<2.2
<2.2
3.3
3.6
3.8
Zinc
190
430
280
190
210
160
159
99.3
Total Phosphorus
3670
55.4
938
1400
2050
34.6
60.6
TKN
Ammonia-Nitrogen
Nitrate and Nitrite
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer Date
21"-
Page 5 DENR FORM RSSF (5/2003)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number:
WQ0010689
Facility Name: SUEZ Energy BioPower, Inc.' North Cove
NPDES # or WQ0010689
WQ#:
WWTP Name:
Residual Analysis Data
Laboratory: 1) Pace Analytical Services, Inc.
2)
3)
4)
5)
Sample or
Composite Date
Flyash
1/31/07
Flyash
5/11/07
Flyash 1
7/07/07
Flyash 2
7/07/07
Flyash 3
7/07/07
Flyash
11/01/07
Flyash
11/01/07
pH
11.4
10.8
8.8
9.1
9.1
8.2
8.6
Barium
1200
2600
1600
1600
1400
868
1150
Calcium
89000
130000
66000
68000
60000
36500
45800
Iron
28000
31000
13000
13000
8300
9210
10400
,b
Magnesium
12000
23000
9400
9800
8100
5060
5780
Manganese
1900
3400
1800
1900
1600
892
1110
Potassium
33000
37000
22000
23000
19000
13100
14300
Silver
0.92
<.78
<1.1
<1.1
<1.1
<.91
<1.1
rA
Sodium
9100
9900
4900
4900
4300
4190
4470
G6I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer Date
Page 6
DENR FORM RSSF-B (5/2003)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: SUEZ Energy BioPower, Inc. - North Cove Permit Number: WQ 0010689
WWTP Name: NPDES Number:
Monitoring Period: From
To
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost [3-1
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion [3
Anaerobic Digestion[] estion
If applicable to alternative performed (Class A or Class B) complex the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g �
Umber o
Excee-
ences
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
inim
Geo. Mean
aximu
1
Fecal Coliform
2 x 10 to the 6th
power MPN per
gram of total
solids or 2 x 10 to
the 6th power
CFU per gram of
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ❑ Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑
Option 6 ❑ Option 7 0 Option 8 ❑ Option 9 ❑ Option 10 ❑
No vector attraction reduction options were performed p P ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Preparer Name and Title (type or print)
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer
Date Signature of Land Applier (if applicable) Date
Page 7 DENR FORM RF (sonnR)

aceAnalytical`"
www.p,icolabs.com
Lab Sample No: 927963553
Client Sample ID: MARION ASH 2O1-2
Pace Analytical Services, Inc.
9800 Kmcey Avenue, Suite 100
Hunteisvllle, NC28078
Phone [phone]
.Fix 704 875 9097
Pace Analytical Services, inc.
2225 Riverside Drive
Asheville. NC 29804
Phone. [phone]
Fax: 828, 252.467 S
Lab Project Number: 92137232
Client Project 10. ASH SAMPLE
Project Sample Nt,mber: 92137232-002 Date Collected: 01/31/07 10:00
Matrix: Soil Date Received: 01/31/07 12:00
Parameters _
Results
_Units
_ Report. Limit
OF _
Analyzed
�BL_
_CAS -No ual RULmt
Metal
Metals, Trace ICP
Prep/Method:
EPA 3050 !
EPA 6010
Arsenic
16.
mg/kg
0.66
1 3
02107107
19:09
SHB
7440-38.2
Barium
1200
mg/kg
0
66
1.3
02101107
19:09
SHB
7440-39.3
Cadmium
2.6
mglkg
0,13
1.3
02/07/07
19:09
SHB
7440.43.9
Calcium
89000
mg/kg
130
13.2
02/07/07
19:09
SHB
7440.70-2
Chromium
36.
mg/kg
0.66
1.3
02/07/07
19:09
SHB
7440-47 3
Copper
100
mglkg
0.66
1.3
02/07/07
19:09
SHB
7440-50.8
Iron
28000
mglkg
66-
13.2
02/07/07
19:09
SHB
7439-89-6
Lead
33.
mglkg
0.66
1.3
02/07/07
19:09
SH8
7439-92-1
Magnesium
12000
mg/kg
13.
1.3
02/07/07
19:09
SHB
7439.95.4
Manganese
1900
mg/kg
0.66
1.3
02/07/07
19:09
SHB
7439-96.5
Molybdenum
NO
mg/kg
0.66
1.3
02107/07
19:09
SH8
7439-98.7
Nickel
26.
mglkg
0.66
1.3
02/07/07
19-09
S1H8
7440.02-0
Potassium
33000
mg/kg
1300
13.2
02/07/07
19:09
SHB
7440-09 7
Selenium
NO
mg/kg
1.3
1 3
021D7/D7
19:09
SHB
7782.49-2
Silver
0.92
mg/kg
0.66
1.3
02/07/07
19.09
SHB
7440.22-4
sodium
9100
mg/kg
130
1.3
02/07/07
1.9:09
SHB
7440.23.5
Zinc
190
mg/kg
1-3
1 3
02/07/07
19:09
SHB
7440-66.6
-late Digested
02/07/07 14:15
02/07/07
14:15
Mercury. CVAAS, in Soil
Mercury
Wet Chemistry
Percent Moisture
Percent Moisture
PH
PH
Date, 02121t07
4 0 , r�l� w( lPS
VG ...,slewater 40
VC Drinking Water 37712
;C 99030
1 NELAP E8'648
Method: EPA 7471
NO mglkg
Method: X Moisture
38.0 X
Method: EPA 9045
11.4 units
0.0018 1 6 07;06/07 11-43 ALV 7439-97.6
1.0 02/05/07 09:42 TNM
02/13/07 14:10 MDK
REPORT OF LABORATORY ANALYSIS
This report shall nol ba reproducea, except w 10.
,,othoul the wrn;len con3ew oofrPPace Ana._;tir,3i Services inn.
'n lar .
Page 3 of 4
4t. r!QIte.LffW!awn 1L1_5
NC wastewater 12
NC DwAing Wale' 377-06
SC 99006
FL NELAP E87627

1143ZI J1 CUU / 11: UUrII'I JUtG I-IrIMLUII tlCtf- (Z)b- /1bU P. b
I
I
Results W Ignitability
by EPA 1030
I
Client Sample 1D: 92798354WMarion ASH201.1 Analy4ed By- BAO
Client Project ID: 92137232 Date affected: 1/31/2007 08:40
Lab Sample ID: G150-392-1A Date eceived: 2/5/2007
Lab Project ID: G150-392 Matrix Soil
Parameter Result Units Date
Analyzed
i
Ignitablility < 0.8 mmisec - 2/8/2007
Commente:
e
Revlewed By: ud _
2 ofa

Mai 31 2007 11:00HM SUEZ MHKIUN
�i
�Y.
ti Ibb- /1bU P.:i
, PaccAnalytical
into: flacelibra enru
Ms. Annette Scott
Pace Anaiyticai Servioea, Inc
Charlotte Laboratory
9800 Kincey Avenue, Suite 100
HuntemAile, NC 28079
Client Site: Asheville Laboratory
Client Ref.: 92137232(Smm Energy
Test
Cyanlde (Rew&e) 7,
twMde(Fiea0tivet ..
Test
Msthod
Result
,3.T19014t>>
<l.01
QMO)
<10'
Method
Reawt
% SoMds
gal
Pac® AWydoa/ Sa wom, Inc.
i 5203 Trlenple Larne
Export, PA 15632
Phone: [phone]
i Far 724.327.7793
Lab P ID:
07-0977
Lab Sam le ID:
0702-0853
Client Sa a ID;
927963545
Sample Matrix:
Solid
Date Sanpied:
02/02=7
Date R ved:
02/02/2007
9 Units
Ase
Art>alYelsI hWhod
Blenk
Date I Blank 10
Result
1.0+ rrtg/kg BKH i 0WIW007 005-raW110,
<1.0
n►B/kg 9KH ; ' 02115/2007 0057QA8-1
<1t)
Units ' Asstye( l Anatywe Method BlaA
II Debi Bbnklo I Result
% JPZ 02NCIZ007 WA WA
(') U.S. &wkonmerrtai Pr0600on Agency, 1 we, Test Methods f0r Evefuating Solid S
Waste. VY-818, 3rd ed., Oifice of SOW Waste and
EMNOWcy Response, Washington. DC.
SamPIG Comments:. Resits reported In dry weight equivalence.
REPORT OF LABORATORY ANALYSIS
This report shall rtot be reproduced, except -in full, :
without the written consent of Pace Analytical Services, Inc.
Page 2 of 2

May 31 2007 10:54AM SUEZ MARION
?Analytical®
www.pavelsbs.com
Solid results are reported on a dry weight basis
028-756-7160 p.'2
Pace Analytical Services, Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
HuntersvIlle, NC 28078 Asheville, NC 28804
Phone: [phone] Phone: 828.254J176
Fax [phone] Fax.• 828.252.4618
Lab Project Nwober: 92144455
Client Project ID: Marion Fly Ash
Lab Sample No: 928377050
Project Sample Number: 92144455-001 Date Collected: 05/11/07 00:00
Client Sample ID: J MARION FLY ASH
Natrix:'Sot1
Date Received: 05/11/07 16:00
Parameters
Results Units
Report Limit DF Analyzed
By CAS No, Qual ReaLmt
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
56.8 %
1.0 05/15/07
18:21 OF
Phosphorus, Total. Soil
Method: EPA 366.2
Phosphorus
55.4 mg/kq
3.45 1.7 05/22/07
09:35 DMN 7723.14.0
PH
Method: EPA 9045
PH
10.8 units
05119/07
13:00 MJRI
Date: DS/22/07
Asheville Certification
IDs
REPORT OF LABORATORY ANALYSIS
NO Wastewater
40
This report shall not be reproduced, except in full,
NC Drinking Water
37712
without the written consent of Pace Analytical Services, Inc.
Sc
99030
FL NELAP
E87648
° `'r' "°'•
Page: 1 of 4
Chgdotle Cenifleallon IDS
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

May 31 2007 10:54RM SUEZ MARION
_ aceAnalytical
aVww.Pac618b8.c0m
Lab Sample No: 928377068
Client Sample ED: K MARION FLY ASH
828-756-7160 p.3
Pace AaWyNcal Serricer, - - Pace Analytical Sonless, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NO2BO78 Asheville, NC28804
Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
Lab Project Number: 92144455
Client Project ID: Marion Fly Ash
Project Sample Number: 921444557002 Date Collected: 05/11/07 00:00
Matrix; Soil Date Received: 05/11/07 16:00
Parameters
Results
units
Report Limit
DF
Analyzed
By
CAS No. Qual ReaLmt
Metals
Metals, Trace 1CP
Prep/Method: EPA 3050 /
EPA 6020
Arsenic
31,
mg/kg
0.78
1,6
05118/07
00:39 EWS
7440-3B-2
Barium
2600
mg/kg
78.
156
05/18/07
00:39 EWS
7440.39-3
Cadmium
2.6
aglkg
0.16
1.6
05/18/07
00:39 EWS
7440-43-9
Calcium
130000
mg/kg
1600
156
05/18/07
00:39 EWS
7440.70.2
Chromium
44.
mg/kg
0.78
1.6
05/18/07
00:39 EWS
7440.47.3
Copper
110
mg/kit
0.78
1,6
05/18/07
OD:39 EWS
7440.5D-8
Iron
31000
mg/kg
78D
156
05/18/07
00:39 EWS
7439-89-5
Lead
32.
mg/kg
038
1.6
05/18/07
00:39 EWS
7439-92-1
Magnesium
23000
mg/kg
160D
156
05/18/07
00:39'EWS
7439-95-4
Manganese
3400
mg/kg
78.
156
05/18/07
00:39 EWS
7439.96.5
Molybdenum
NO
mg/kg
0,78
1.6
05118/07
00:39 EWS
7439-98-7
Nickel
23,
mg/kg
0.78
1.6
05/18/07
00:39 EWS
7440-02-0
Potassium
37000
mg/kg
1600D
156
05/18/07
00:39 EWS
7440-09-7
Selenium
ND
mg/kg
1.6
1.6
05/18/07
00:39 EWS
7782-49-2
Silver
ND
mg/kg
0.78
1.6
05/18/07
00:39 EWS
7440-22.4
Sodium
9900
mg/kg
160
1.6
05/18/07
00:39 EWS
7440-23.5
Zinc
280
mg/kg
1.6
1.6
05/18/07
00:39 EWS
7440-66-6
Date Digested
05/16/07 13:15
05/16/07
13:15
Mercury, CVAAS, in Soil
Mercury
Wet Chemistry
Percent Moisture
Percent Moisture
Date: 05/22/07
Method: EPA 747.1
0.015 mg/kg.
Method: % Moisture
50.2 X
0.0079 f 1.6 05/15/07 10:55 ALV 7439-97-6
1.0 06/16/07 09:13 TNM
Asheville Certification IDs REPORT Of LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
SC 903
NC Drinking Water 2 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 •
3 C
t
Page: 2 of 4
Charlotte Certification IDs
NC Wastewater i2
NC Drinking Water 37706
SC 99006
FL NELAP E87627

May 31 2007 10:54AM SUEZ MARION
ace Analytical
wwW.Pac®l*br.com
Lab Sample No: 928377076
Client Sample I0: L.MAR30N FLY ASH
828-756-7160 p.4
Pace Analytical Services, pace Analytical Sarvices, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside, (hive
Huntersville, NC 28078 Asheville, NC 28804
Phone: [phone] Phone: [phone]
Fax: [phone] Fax [phone]
Lab Project Number: 92144455
Client Project ID: Marion Fly Ash
Project Sample Number: 92144455-003 Date Collected: 05/11/07 00:00
Matrix: soil Date Received: 05/11/07 16:00
Parameters
Results
Units
Reoort Limit
OF " Analyzed
BY
. CAS No. Qgal RegLmt
Metals
Metals, Trace ICP
Prep/Method:
EPA 3050 / EPA 6010
Arsenic
71.
mg/kg
0.79
1,6 05/17/07
23:49 EWS
7440.38.2
Barium
1500
mg/kg
0.79
1.6 05/17/07
23:49 EWS
7440.39.3
Cadmium
4.0
mg/kg
0.16
1.6 05/17/07
23:49 EWS
7440-43-9 .
Calcium
14D000
mg/kg
1600
157 D5/17/07
23:49 EWS
7440-70-2
Chromium
63.
mg/kg
0.79
.1.6 05/17/07
23:49 EWS
7440-47-3
Copper
140
mg/kg
0.79
1.6'05/17/07
23:49 EWS
7440.50.8
Iron
13000
mg/kg
7.9
1.6 D5/17/07
23:49 EWS
7439.89.6'
Lead
71.
mg/kg
0.79
1..6 05/17/07
23:49 EWS
7439-92-1
Magnesium
12000
mg/kg
16.
1.6 05/17/07
23:49 EWS
7439-95.4
Manganese
3800
mg/kg
.79.
157 05/17/07
23:49 EWS
7439-96-5
Molybdenum
3.1
mg/kg
0.79
1.6 D5/17/07
23:49 EWS
7439-98-7
Nickel
21.
mg/kg
0.79
1.6 05/17/07
23.49 EWS
7440-02.0
Potassium
A4000
mg/kg
16000
157 05/17/07
23:49 EWS
7440-09-7
Selenium
1.6
mg/kg
1.6
1.6 05/17/07
23:49 EWS
7782.49-2
Silver
NO
mg/kg
0.79
1.6'05/17/D7
23:49 EWS
7440-22.4
Sodium
12000 -
mg/kg,
160
1.605/17/07
23:49 EWS
7440.23-5
Zinc
430
mg/kg
1.6
1.6 D5/17/07
23:49 EWS
7440-66-6
Date Digested
05/16/07 13:15
05/16/07
13:15
Mercury, CVAAS, in Soil
Method: EPA
7471
Mercury
0.057
mg/kg
0.011
2.2 05/15/07
10:53 ALV
7439 97.6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
59.4
%
1.0 05/15/07
18:21 KOF
Phosphorus. Total. Soil
Method: EPA
365.2
Phosphorus
3670 •
Ong/kg
242.
121 05/22/07
11;16 DMN
7723-14.0
Date: 05/22/07
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except In full,
NC'Drinking Water 37712 without the written consent of Pace Analytical Services, Inc.
SC 99030
FL NELAP, E87648
Page: 3 of 4
p,harlotte Certification
IDS
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

1A;a'neAnaVica11--
wwwpacelahs.cafn
Pace Analytical Services, ln..
9800 Klncev A%enue. Sucre 700'
V 28078
�nt�l7u -04 875 90_72
-3s, 7i8-�-9,91
Pace Analytical Services, Inc,
225 Riverside Onve
Asnov:flo W 28804
Phone 828 25,1 :1 6
Lab Project Number- 92148883
Client Pro,lect ID: Marion fly Ash
_..._..._-... - -- _------ .......
Lab Sample No: 928719814
..............._.................__....__..-....-
----....--------.
Protect Sample
...._......
Number: 92148883 003
_... ------
Date Collected: 07/07107 00:00
Client Sample 1D: MARION FLY
ASH #1
Matrix:
Soil
Date Received: 07/17/07 13:30
Paraaleters _
_- _ Results
Units
Ref%of.l- 1.1mtt
DF
_.Analyzed
By
_CAS No. tual • Reglmt
Metals
Metals. Trace 1CP
Prep/Method:
EPA 3050 !
EPA 6010
Arsenic
29.
mg/kg
1.7
2.2
08/05/07
1832-0
JOAi
1440-38-2
Barium
1600
mg/kg
1.1
2.2
08/05/07
18:20
JDAI
744C-39.3
Cadmium
2.1
mglkg
0 22
2.2
08!05/07
18:20
JDA1
744C-43.9
Calcium
66000
mg/kg
22.
2.2
08/05/07
18:20
JDAI
7440.70 2
Chromium
26.
mg/kg
1.1
2.2
08/05/07
18:20
JDAI
7440-47-3
Copper
76.
mg/kg
1.1
2.2
08/05/07
18:20
JDAI
7440-50-8
Iron
13000
mg/kg
ll.
2.2
08/05/07
18:20
JDAI
7439-89.6
Lead
40.
mg/kg
1.1
2.2
08/05/07
18:20
JDAI
7439.92-1
Magnesium
9400
mg/kg
22.
2.2
08/05i07
18:20
JDAI
7439.95.4
Manganese
1800
mg/kg
1.1
2.2
08!05l01
18:20
JDAI
7439-96.5
Molybdenum
1.4
mg!kg
1.1
2.2
08l05/07
18:20
JDAI
7439.98.7
Nickel
13.
mg/kg
1.1
2.2
08/05/07
18:20
JDAI
7440.02.0
Potassium
22000
mg, !kg
220
2.2
08/05/07
18:20
JDAI
7440-09 7
Selenium
NO
mg/kg
2.2
2.2
08/05/07
18:20
JOA1
7782-49.2
Silver
NO
jnglkg
1.1
2.2
08105/07
18:20
JDAI
7440.22-4
Sodium
4900
mg/kg
220
2.2
08/05/07
18:20
JDAI
7440-23.5
Zinc
190
mg/kg
2.2
2.2
08105/01
18:20
JDAI
7440-66-6
Date Digested
08/04/07 13:20
08/04/07
13:20
Mercury. CVAAS. in Soil
Method: EPA
7471
Mercury
0.021
mg/kq
0.0098
1.9
081107/07
13.24
JMW
7439.97 6
Wet Chemistry
Percent Moisture
Percent Moisture
Phosphorus, Total, Soil
Phosphorus
pH
DH
OaW Ohi10%0%
Asheville CPr#1f1calinn 0.5
NC in1351ow3lei 41J
INC 05i'l"kill(i -Afaif'[ 3i i 1
a9D31
ttE1.At E°76AA
Method: � Moisture
54.8
Method: SM 4500•P F
938. mg/kg
Method: EPA 9045
8.80 units
1.0 081'09/01 11:41 ALV
ill. 55.3 08107/01 09:226 SHB 7723-14-0
08/06/07 21:17 SER
REPORT OF LABORATORY ANALYSIS
This fap .-I ,hall nol fie. fepiodiiCed.ltai
U1 it11; .i;1tF`!'I l;i)nsem of Pac%;Qna°r'L al 'li:
Page 3 ai -'
Charlotte Certlticalion ills

aceAnalytrcal'F'
/ wwta'. pacelabs. com
Lab Sample No: 928719798
Client Sample 1D: MARION FLY ASH #2
Pace Analytical Services, in-
9800 Kmcev' AL enue Suite !00
HunteisviPe AIC-960 S
Phttne .704 875 90.4"
,'--as -104 8,75 9091
Pace Analytical Services, Inc.
2225 Rive+srie On e
AStIe1-rUe..NC 2833'
Lab Project Number: 92148883
Client Project ID. Marion Fly Asti
:.7 v 328 :�5? 451.3
Project Sample Number; 9c148883.002 Date Collected: 07107/07 00:00
Matrix: Soil Date Received: 07/17/07 13 30
Parameters Results _ _ Units Report Limit OF Analyzed By CAS No. - Qua1_ Re4Lmt
Metal s
Metals, Trace 1CP
Arsenic
Barium
Cadm i um
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sod i U111
Zinc
Dare niaesLed
Mercury, CVAAS, in Soil
Mercury
Wet Chemistry
Percent Moisture
Percent Moisture
Phosphorus, Total, Soil
Phosphorus
;;ace G8110I1)I
r�shzYllie. Gertillcllt!on IUD
r
SC.' 99030
`i. f*i AP E37648
Prep/Method: EPA 3050 / EPA 6010
32.
mg/kg
I.1
i600
mg/kg
1.1
2.i
ng/kg
0.22
68000
mg/kg
22.
29.
mglkg
1.1
79.
mg/kg
1.1
13000
mg/kg
11.
40.
mg/kg
1.1
9800
mg/kg
22
1900
mg!kg
1-I
1.6
mgikg
1.1
14.
?!Q/ kg
1. 1
23000
mg/kg
220
NO
mglkg
2.2
NO
mg/kg
1.1
4900
mg!kg
220
210
mg /ky
- . 2
08/04/07
13:20
Method: EPA 7471
0.021 mg/kg D.611
Method: Moisture
54.2
Method: SM 4500-P F
1400 mg/kg 99.2
Method: EPA 9045
9,10 unrLS
2 2 08105/07 18:07 JDAI 7440.38 2
2.2 08/05/07 18:07 JDAI 7440-39.3
7.2 08!05/07 18;07 JOAJ 7440.43.9
2.2 08/05/07 18:07 JDAI 7440 70.2
2.2 08/05/07 18:07 JDA1 7440.47.3
2.2 08/05/07 18:07 JDAI 7440.50-8
2.2 08/05/07 18:07 JDAI 7439.89.6
2.2 08/05/07 '18:07 JDAI 7439-92.1
2.2 08i05107 18:07 JDA1 7439 95.4
2 r 08/05/07 18:07 JDAI 7439.96.5
2.2 08105/07 18:07 .JDA1 7439.98.7
2.2 08/05/07 18:07 JDA1 '1440.02-0
2.2 08/05/07 18:07 jDA1 1440.09.7
2.2 08/05/07 18:07 JDAI 7782 49.2
2.2 08/05/07 18:07 JDAI 7440.22.4
2.2 08/05/07 18:07 JDAI 7440.23.5
2.2 08/05/07 18:07 JDAI 7440-66-6
08/04/07 13:20
2.2 08/07/07 13-19 JMW 7439 9.•'-6
1.0 08/09/07 11:40 ALV
49.6 08/07!07 09:26 SHB 7723.14.0
1.0 08/06/07 21.17 SER
REPORT OF LARORr1ka ANALYSIS
Tiis iP.r!or1 Shall not lip ri;pr,iduced I xcapt !« hJ!
:rdi 0ul II?� ,I1tn consent 0 P,-.f A f 1 d 1 v :a: `l!r,: 1:.- 11
nPhr
?age I o+ 4
r:liarlotle, Cerwication I15
::

;a c
ceAnalyfical
/
www. pacelabs. Coll]
Solid results are reported On a dry weight basis
Lau Sample No: 928642172
Client Sample ID: MAR10N FLY ASH ;#3
Pace Analylica/ Services. inc.
+800 tie(.,cey Avenue Sale ?00
F:So-re -04 875 9092
Pace Analylicai Services, Inc.
2225 laver:slide Orr+,'e
Ao0viijo N"' 880-1
yr nRa 82E 2:�a
:a ...S?3 �5.:' -`618
Lat. Pro.t+:ct Number 92148881
Client Project D: Mar -ion Fly Ash
Project Sample Number: 92148883-001 Date Collected: 07/07/07 00:00
Matrix: Soil Date Received: 07/16/07 13:30
Parameters
Results
_ Units
Regprt Limit
DI
Analyzed
��:
CAS No. Quay Re Lmt
Meta 1S
Metals, trace ICP
Prep/Method:
EPA 3050 i
1PA 6010
Arsenic
24.
mg/kg
1 l
2.2
07/26/07
18 39
SHB
/440 38-2
Bar Iwi,
1400
F,g/k9
1.1
2.2
C,7'26!07
18:39
SHB
1440-39 3
Cadmium
1.4
,,g/le. g
0.22
2 2
07/26/07
18 39
SH8
7440.43.9
Calcium
60000
mg/kg
110
10.9
07/26/07
18:39
SH8
7440.70.2
Chromium
is.
mg/kg
1.1
2.2
07/26/07
18:39
SH8
7440.47.3
Copper
61.
mg/k.g
1.1
2.2
07126107
18:39
SH8
7440-50-8
Iron
8300
mg/kg
il.
2.
01/26/07
18:39
SH8
1439.89.6
Lead
33
m9/kg
1.1
2.2
0?126/0?
18:39
SH8
7439.92.1
Matine s)ui±
8100
rg,'kg
22.
2.2
0•1i26!07
18.39
SHB
7439-95.4
Manganese
1600
mg/kg
1.1
2.2
07,126107
18:39
SHB
7439.96.5
'fclyoderium
1.2
g!kg
_.1
? 2
0?/2607
18:3'
SH8
7439.98.7
Nickel
8 9
mg/kg
i
" 2
07 26/07
38:39
SHB
7440.02.0
Potassiuit
19000
mg/kg
2219
2.2
07126/07
118:39
SHB
7440-09-7
Selenium -
3.3
mglkg
2.2
2.2
07126/07
:8;39
SHB
7782-49-2
Silver
ND
mgikg
1.1
2.2
07/26/47
1°:39
SH,B
7440-22.4
Sodium
43110
mg/kg
220
2.;.'
07,26/07
18:39
SHB
7440-23-5
7ii;c
160
lrg/K9
?
27,2
07126r07
18:39
SH8
7440-66-6
Date Digested
07l22/07 19
30
1'"22107
i9:30
Mercury. CdAAS. in Soil
Hercury
Jet Chemistry
Percent Moisture
Percent Moisture
Phosphorus, total. Soil
Phosphorus
Dale 08110!0'
A; he.Q;P t��lit!I lt�fl Ms
NC 'A''a-!e
Ft. ... r
Methoo. EPA. 1471
11D ngIkg
Method: .' Moisture
54.3
Method: SM 4500 P F
2050 mg/k9
0 ti12 2.4 6,7124p)7 1:':40'- JMk 7439-97 6
1 0 67118107 09:56 fNM
109. 54.7 07/31/07 11:15 OMN 7723.14.0
REPORT OF LABORATORY ANALYSIS
?il;oul thU ^iiFrr ,on5er4
14 are f ,
hagprt8 Ctgilisanon ills.
NIC'N"'Sle"valet
A!, r..

aceAnalytical
www.pacelabs.com
Pace Analytical Ser s, Inc.
2225 k. de Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Ash Analysis 11/07
Pace Project No.: 926983
Sample: M-11-Al-07 NORTH POND Lab ID: 926983001 Collected: 11/01/07 00:00
Results reported on a "dry -weight" basis
Parameters
Results Units
Report Limit
DF
Arsenic
11.7 mg/kg
0.91
1
Barium
868 mg/kg
0.91
1
Cadmium
0.44 mg/kg
0.18
1
Calcium
36500 mg/kg
91.5
5
Chromium
10.5 mg/kg
0.91
1
Copper
50.1 mg/kg
0.91
1
Iron
9210 mg/kg
9.1
1
Lead
23.0 mg/kg
0.91
1
Magnesium
5060 mg/kg
18.3
1
Manganese,
892 mg/kg
0.91
1
Molybdenum
ND mg/kg
0.91
1
Nickel
6.5 mg/kg
0.91
1
Potassium
13100 mg/kg
915
1
Selenium
3.6 mg/kg
1.8
1
Silver
ND mg/kg
0.91
1
Sodium
4190 mg/kg
915
1
Zinc
159 mg/kg
1.8
1
Arsenic
0.028 mg/L
0.025
1
Barium
2.1 mg/L
0.025
1
Cadmium
ND mg/L
0.0050
1
Chromium
ND mg/L
0.025
1
Lead
ND mg/L
0.025
1
Selenium.
ND mg/L
0.050
1
Silver
ND mg/L
0.025
1
Mercury
ND ug/L
0.20
1
Mercury
ND mg/kg
0.010
1.
Percent Moisture
52.0 %
0.10
1
Phosphorus
34.6 mg/kg
7.2
1
Sample: M-11-A2-07 North Pond Lab ID: 926083002
Results reported on a Vry-weight' basis
Parameters Results Units
Collected: 11/01/07 00:00
Report Limit DF
Arsenic
10.1 mg/kg
1.1
1
Barium
1150 mg/kg
1.1
1
Cadmium
0.54 mg/kg
0.21
1
Calcium
45800 mg/kg
106
5
Chromium
12.7 mg/kg
1.1
1
Copper
86.6 mg/kg
1.1
1
Iron
10400 mg/kg
10.6
1
Lead
27.9 mg/kg
1.1
1
Magnesium
5780 mg/kg
21.2
1
Manganese
1110 mg/kg
1.1
1
Molybdenum
ND mg/kg
1.1
1
Nickel
7.8 mg/kg
1.1
1
Potassium
14300 mg/kg
1060
1
Selenium
3.8 mg/kg
2.1
1
Date: 11/15/2007 12:05 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 6

Pace Analytical Ser : s, Inc. Pace Analytical Services, Inc.
/�,,
® 2225 R. de Dr. 9800 KinceyAve. Suite 100
c?CG A�Ic71j/fICa� Asheville, NC 28804 Huntersville, NC 28078
www.pacefabs.com•
[phone] [phone]
ANALYTICAL RESULTS
Project: Ash Analysis 11/07
Pace Project No.: 926983
Sample: M-11-A2-07 North Pond . Lab ID: 926983002
Collected: 11/01/07 00:00
Results reported on a "dry -weight" basis
TC LP
Parameters
Results Units
Report Limit DF
Silver
ND mg/kg
1.1 1
Sodium
4470 mg/kg
1060 1
Zinc
9mg/kg
2.1 1
Arsenic
ND
ND mg/L
0.025 1
Barium
2.3 mg/L
0.025 1
Cadmium
ND mg/L
0.0050 1 x
Chromium
ND mg/L
0'.025 1
Lead
ND mg/L
0.025 1
Selenium
ND mg/L
0.050 1
Silver
ND mg/L
0.025 1
Mercury
ND ug/L
0.20 1
Mercury
ND mg/kg
0.011 1
Percent Moisture
55.4 %
0.10 1
Phosphorus
60.6 mg/kg
10.7 1
Sample: M-11-A3-07 BOTTOM ASH Lab ID: 926983003
Collected: 11/01/07 00:00
SAND BOX
Results reported on a "dry -weight' basis
Parameters
Results Units
Report Limit
DF
Arsenic
4.9 mg/kg
0.38
1
Barium
1730 mg/kg
7.6
20
Cadmium
1.0 mg/kg
0.076
1
Calcium
85800 mg/kg
153
20
Chromium
27.1 mg/kg
0.38
1
Copper
216 mg/kg
0.38
1
Iron
21800 mg/kg
76.3
20
Lead
89.0 mg/kg
0.38
1
Magnesium
12000 mg/kg
153
20
Manganese
2020 mg/kg
7.6
20
Molybdenum
1.3 mg/kg
0.38
1
Nickel
14.3 mg/kg
0.38
1
Potassium
22300 mg/kg
7630
' 20
Selenium
ND mg/kg
0.76
1
Silver
ND mg/kg
0.38
1
Sodium
9470 mg/kg
7630
20
Zinc
176 mg/kg
0.76
1
Arsenic
ND mg/L
0.025
1
Barium
1.6 mg/L
0.025
1
Cadmium
ND mg/L
0.0050
1
Chromium
0.072 mg/L
0.025
1
Lead
ND mg/L
0.025
1
Selenium
ND mg/L
0.050
1
Silver
ND mg/L
0.025
1
Mercury
ND ug/L
0.20
1
Mercury
ND mg/kg
0.0050
1
Percent Moisture
0.68 %
0.10
1
Date: 11/15/2007 12:05 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
� �yo
Page 5 of 6

Pace Analytical, Sep ' s, Inc. Pace Analytical Services, Inc.
e 2225 F<. :ie Dr. 9800 Kincey Ave. Suite 100
aceAnalytical Asheville, NC 28804 Huntersville, NC 28078
i www.pacelabs.com
J [phone] [phone]
ANALYTICAL RESULTS
Project: Ash Analysis 11/07
Pace Project No.: 926983
Sample: M-11-A3-07 BOTTOM ASH Lab ID: 926983003 Collected: 11/01/07 OO:OC
SAND BOX
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF
Phosphorus 31.7 mg/kg 4.8 1
Date: 11/15/2007 12:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
lo
40
Page 6 of 6

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolir Department of Environment and Natural Resources
Coleen H. Sullins, Director
Division of Water Quality
AQUIFER P
November 1, 2007
I�l NOV 0 G 2007 IUI
CERTIFIED MAIL 7006 2150 0005 2458 8628
RETURN RECEIPT REQUESTED
Tony Leopard
. _�, : _.Re iv_inal Plant Maneger . ,
Suez Energy Biopower, Inc. . -
302 Duke St.
i
Forest City, NC 28043
Subject: NOTICE OF VIOLATION
NOV-20; 7-PC-0734
Coryiplia ice Evaluation Inspection
North Cove Steam Generation Plant
Ash Disc ibution Program
Permit Is' o. WQ0010689
McDow 'il County
Dear Mr. Leopard:
Enclosed please find a copy of the Inspection Report from the] inspection conducted 2007-10-25.
Beverly Price of the Asheville Regional Office conducted the Cor pliance Evaluation Inspection. The
facility was found to be in violation of Permit WQ0010689 for the following:
Review of the 2006 Annual Report. revealed the following violations:
-.
. i
Parameter
Date
Measuring
Violation
Frequency
Ignitability & Corrosivity
2006
Annual
Analyses not conducted
in 2006.
rvorul L;arouna urvision of water Quality — Asheville Regional Office 2090 U.S. Highway 70
Aquifer Protection Section
Customer Service 1-877-623-6748
Internet: h2o.enr.state.nc.us
An Equal Opportunity/Affirmative Action Employer — 50%Recycled/10% Post Consumer Paper
NC 28778
No°` hCarolind
Wura!!y
Phone [phone]
FAX [phone]

Compliance Inspection Re ort
Permit: WQ0010689 Effective: 11/29/06 Expiration: 11/30/10 Owne : Suez Energy Biopower Inc
I
SOC: Effective: Expiration: Facility, North Cove Steam Generation Plant Ash
Distribution Program
County: McDowell 2859 Old Linville Rd
Region: Asheville
Marion NC 28752
Contact Person: Tony Leopard Title: Regional Plant Manager Phone: [phone]
Directions to Facility:
Take NC Hwy. 221 North out of Marion to NCSR 1560 (i.e., located behind Baxter - No
System Classifications:
Primary ORC: Certification:
Secondary ORC(s):
On -Site Representative(s):
24 hour contact name Ricky Styles
On -site representative Summer Barber
On -site representative Tony Leopard
Related Permits:
Inspection Date: 10/25/2007 Entry Time: 10:00 AM
Primary Inspector: Beverly Price
Secondary Inspector(s):
Cove). The facility is located on the left.
Phone:
Phone: [phone]
Phone: [phone]
Phone: [phone]
Exit Time: 121
2 00 PM
Phone: [phone]
Reason for Inspection: Routine Inspection Type: C
Permit Inspection Type: Distribution of Residual Solids (503 exempt)
Facility Status: ❑ Compliant ■ Not Compliant
Question Areas:
V ` Miscellaneous Questions Record Keeping Sampling
(See attachment summary)
Evaluation
Page: 1

Permit: WQ0010689 Owner - Facility: Suez Energy Biopower Inc
Inspection Date: 10/25/2007 Inspection Type: Compliance Evaluation
Type s
Land Application
Distribution and Marketing
Record Keeping
Is GW,monitoring being conducted, if required?
Are GW samples from all MWs sampled for all required parameters?
Are there any GW quality violations?
Is GW-59A certification form completed for facility?
Is a copy of current permit on -site?
Are current metals and nutrient analysis available?
Are nutrient and metal loading calculating most limiting parameters?
a. TCLP analysis?
b. SSFA (Standard Soil Fertility Analysis)?
Are PAN balances being maintained?
Are PAN balances within permit limits?
Has land application equipment been calibrated?
Are there pH records for alkaline stabilization?
Are there pH records for the land application site?
Are nutrient/crop removal practices in place?
Do lab sheets support data reported on Residual Analysis Summary?
Are hauling records available?
Are hauling records maintained and up-to-date?
# Has permittee been free of public complaints in last 12 months?
Has application occurred during Seasonal Restriction .window?
Comment:
Sampling
Describe sampling:
Approximately every five feet of the pile, a grab sample is collected. The grabs are t.
second sample is also collected from the same pile. The samples are collected in a pl
Is sampling adequate?
Is sampling representative?
Reason for Visit: Routine
en composited. A
;tic bucket.
Yes No NA NE
■ ❑ ❑ ❑
■ ❑ ❑ ❑
Page: 3
I

NOV 0 �, 2007 D
AffaMr Protection
November 1, 2007
Mr. Tony Leopard
Regional Plant Manager
SUEZ Energy Biopower, Inc.
302 Duke Street
Forest City, NC 28043
SUBJECT: Assessment of Civil Penalties '
for VIOLATION OF PERMIT CONDITIONS
McDOWELL County
File No. PC-2007-0085
Dear Mr. Leopard:
This letter transmits notice of a civil penalty assessed against SUEZ
$832.95 which includes $82.95 in investigative costs. Attached is a
explaining this penalty.
Michael F. Easley, Governor
William G. Ross Jr., Secretary
Carolina Department of Environment and Natural Resources
Coleen H. Sullins, Director
Division of Water Quality
;y Biopower, Inc. in the amount of
of the assessment document
This action was taken under the authority vested in me by delegation p vided by the Secretary of the
Department of Environment and Natural Resources and the Director of; he Division of Water Quality. Any
continuing violation(s) may be the subject of a new enforcement action' including an additional penalty.
Within thirty days of receipt of this notice, you must do one of the fold wing three items:
,1
1. Submit payment of the penalty:
Payment should be made to the order of the Department of Lnvironment and Natural
Resources. Payment of the penalty will not foreclose furthe, enforcement action for any
continuing or new violation(s). Do not include the attached aiver form if making
payment.
Please send payment to the attention of:
Mr. Ed Hardee
DWQ/Aquifer Protection Section
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
North Carolina Division of Water Quality — Asheville Regional Office 2090 U.S. Highway 70
Aquifer Protection Section
Customer Service 1-877-623-6748
Internet h2o.enr.state.nc.us
NO°` Carolina
iur,g11Y
NC 28778 Phone [phone]
FAX [phone]
An Equal Opportunity/Affirmative Action Employer — 50% Recycled/10% Post Consumer Paper

s
2. Submit a written request for remission or
detailed justification for such request:
A request for remission or mitigation is limited to cc
of the amount of the penalty and is not the proper prc
accuracy of any of the statements contained in the as
remission request forecloses the option of an admini�
must be accompanied by a waiver of your right to an
stipulation that there are no factual or legal issues in
return to this office the attached waiver form and the
Remission Request' which should describe why you
(a) one or more of the civil penalty assessment f
were wrongfully applied to the detriment of 1
(b) the violator promptly abated continuing envi:
the violation;
(c) the violation was inadvertent or a result of ar
(d) the violator had been assessed civil penalties
(e) payment of the civil penalty will prevent pay
remedial actions.
Please submit this information to the attention of:
And to:
Mr. Ed Hardee
DWQ/Aquifer Protection Section
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
Mr. Landon Davidson
DWQ/Aquifer Protection Section
2090 U.S.. Highway 70
Swannanoa, North Carolina 28778
OR
3. Submit a written request for an administrative
including a
isideration of the reasonableness
cedure for contesting the
zssment letter. Because a
trative hearing, such a request
administrative hearing and a
iispute. You must execute and
attached "Justification for
ars in G.S. 143B-282.1(b)
petitioner;
damage resulting from
accident;
.or any previous violations;
lent for the remaining necessary
If you wish to contest any portion of the civil penalt,r assessment, you must request an
administrative hearing. This request must be in the orm of a written petition to the
Office of Administrative Hearings and must conforr 1 to Chapter 150B of the North
Carolina General Statutes. You must file your origi, ial petition with the:
Office of Administrative Hearings
6714 Mail Service Center
Raleigh, North Carolina 27699-6714

AND
Mail or hand -deliver a copy of the petition to:
Mary Penny Thompson.
NCDENR
Office of General Counsel
1601 Mail Service Center
Raleigh, NC 27699-1601
And to:
Mr. Ed Hardee
DWQ/Aquifer Protection Section
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
Failure to exercise one of the options above within thirty days, evidenced by a date stamp (not
a postmark) indicating when we received your response, will re ult in this matter being referred
to the Attorney General's Office with a request to initiate a civil, -action to collect the penalty.
Please be advised that additional assessments may be levied forefuture violations which occur
after the review period of this assessment.
If you have any questions, please contact me at [phone] t r Mr. Ed Hardee at (919) 715-
6189.
Sincerel
G. Landon avidsoft, L.G., Regional Supervisor
Aquifer Protection Section
ATTACHMENTS
cc: Landon Davidson, APS Asheville Regional Office w/
LAPCU Attn: Ed Hardee w/ attachments
APS Central Files w/ attachments
Susan Massengale, PIO w/ attachments

STATE OF NORTH CAROLINA r
DEPARTMI=
NA
COUNTY OF McDOWELL
IN THE MATTER OF
SUEZ ENERGY BIOPOWER, INC. )
FINDI
FOR EXCEEDING THE POLLUTANT )
MONTHLY AVERAGE CONCENTRATION 1
FOR ARSENIC ) .
rH CAROLINA
OF ENVIRONMENT AND
.AL RESOURCES
o. PC-2007-0085
AND DECISIONS
SMENT OF
Acting pursuant to delegation provided by the Secretary of the D:�partment of Environment and
Natural Resources and the Director of the Division of Water Quality, , Landon Davidson, Aquifer
Protection Regional Supervisor for the Asheville Region, of the Division of Water Quality (DWQ),
make the. following:
I. FINDINGS OF FACT:
A. SUEZ Energy Biopower, Inc. operates a Distributioll'i of Residual Solids (503 Exempt)
Ash Distribution program under Permit Number WQ 010689 that was issued November
29, 2006 and expires November 30, 2010.
B. A review of the 2007 monitoring data conduct 1d during the annual compliance
inspection by the Asheville Regional Office revealed a - violation of the Pollutant
Monthly Average Concentration (Dry Weight Basis) tor Arsenic. The May 2007 metals
analyses showed concentrations of 71 mg/kg. and 1 mg/kg: ' The resulting monthly
average was 51 mg/kg.
C. Condition H (5) of permit WQ0010689 states that f(k ash to be distributed through the
approved ash distribution program, the following shay be maintained:
Monthly Average Concentration (Dry Weight, Basis):
Arsenic 41 (mglkg)
D. The cost to the State of the enforcement procedures inthis matter totaled $82.95.
i
Based upon the above Findings of Fact, I make the following:
H. CONCLUSIONS OF LAWN

A. SUEZ Energy Biopower, Inc. is a "person" wit 'in the meaning of G.S. 143-215.6A
pursuant to G.S. 143-212(4).
B. SUEZ Energy Biopower, Inc. violated Condition 11 (5) of permit WQ0010689 by failing
to maintain a Monthly Average Concentration Weight Basis) of 41 mg/kg for
Arsenic. .
C. SUEZ Energy Biopower, Inc. may be assessed civil) enalties pursuant to G.S. 143-
215.6A(a)(2) which provides that a civil penalty of ilot more than twenty-five thousand
dollars ($25,000.00) per violation may be assessed ' gainst a person who violates or fails
to act in accordance with the terms, conditions, or r' quirements of a permit required by
G.S. 143-215.1.
D. The State's enforcement costs in this matter may be ssessed against SUEZ Energy
Biopower, Inc. pursuant to G.S. 143-215.3(a)(9) an � G.S. 143B-282.1(b)(8).
E. The Aquifer Protection Regional Supervisor for the Asheville Regional Office,
Division of Water Quality, pursuant to delegatioli provided by the Secretary of the
Department of Environment and Natural Resources and the Director of the Division of
Water Quality, has the authority to assess civil penalties in this matter.
Based upon the above Findings of Fact and Conclusions of Lw, I make the following:
III. DECISION:
Accordingly, SUEZ Energy Biopower, Inc. is hereby assesse� a civil penalty of:
$ 750.00 For the failure to maintain :a Monthly Average Concentration
(Dry Weight Basis) of 41mg Ig for Arsenic, which is a violation
bfVertriit'`W
$ 750.00 TOTAL CIVIL PENAL'
$ 82.95 Enforcement Costs
$ 832.95
TOTAL AMOUNT DUE
i
As required by G.S. 143-215.6A(c), in determining the amount of the P enalty I have considered the
I
i
I
I

As required by G.S. 143-215.6A(c), in determining the amount of
factors listed in G.S. 14313-282. 1 (b), which are;
(1) The degree and extent of harm to the natural resources
private property resulting from the violation;
(2) The duration and gravity of the violation;
lty I have considered the
the State, to the public health, or to
(3) The effect on ground or surface water quantity or quality`pr on air quality;
(4) The cost of rectifying the damage;
(5) The amount of money saved by noncompliance;
(6) Whether the violation was committed willfully or intenti "nally;
(7) The prior record of the violator in complying or failing tb comply with programs over which
the Environmental Management Commission has regulatory authority;
(8) The cost to the State of the enforcement procedures.
1\ - of-bq
(Date) G. Landon Davidson,
Aquifer Protection Si
Asheville Regional O:
Division of Water Qu
G., Regional Supervisor

TIO
DWQ Case Number: PC-2007-0085 Cou
Assessed Party: SUEZ Energy Biopower, Inc.
Permit No. (if applicable): WQ0010689 Amount Assesses
Please use this form when requesting remission of this civil
Facts" form to request remission of this civil penalty. You
you believe support your request and are necessary for the 1
your request for remission. Please be aware that a reg
consideration of the five factors, listed below as they may rE
- --amount of the civil penalty assessed.'- Requesting remissior.
contesting whether the violation(s) occurred or the accuracy
contained in the civil penalty assessment document. Pursuc-
remission of a civil penalty may be granted only when one or
applies. Please check each factor that you believe applies to
explanation, including copies of supporting documents, as t
additional pages as needed).
(a) one or more of the civil penalty assessmer
were wrongfully applied to the detriment of the petitioner
the civil penalty assessment document);
(b) the violator promptly abated continuing enviro
violation (i.e., explain the steps that you took to correct
occurrences);
: McDowell
$ 832.95
You must also complete the
hould attach any documents that
irector to consider in evaluating
;st for remission is limited to
ate to the reasonableness of the
is -not the proper.-ptaeedure -for
>f any of the factual statements
t to N.C.G.S. § 143B-282.1(c),
tore of the following five factors
,our case and provide a detailed
why the factor applies (attach
tors in N.C.G.S. 14313-282 1(b)
assessment factors are listed in
violation and prevent future
_ (c) the violation was inadvertent or a result of an accident (i.e., explain why the
violation was unavoidable or something you could not prevent ' r prepare for);
(d) the violator
_ (e) payment of the civil penalty will prevent payment for the remaining necessary
remedial actions (i.e., explain how payment of the civil penalty swill prevent you from performing
the activities necessary to achieve compliance).
EXPLANATION (attach additional pages as necessary

STATE OF NORTH CAROLINA
COUNTY OF McDOWELL
IN THE MATTER OF ASSESSMENT )
OF CIVIL, PENALTIES AGAINST )
SUEZ Energy Bionower, Inc
MENTAL MANAGEMENT
COMMISSION
WAIT ER OF RIGHT TO AN
MINI.STRATIVE HEARING AND
STIPULATION OF FACTS
FILE NO.
Having been assessed civil penalties totaling $832.95 for
vlolation(s)-asset forth in -the-assesssment-document,f the Direct' ofthe Division -of Water-Qualit
dated November 1, 2007 , the undersigned, deiring to seek remission of the civil
penalties, does hereby waive the right to an administrative hearing in the above -stated matter and
does stipulate that the facts are as alleged in the assessment docurfient.
The undersigned further understands that all evidence pres' nted in support of remission of
this civil penalty must be submitted to the Director of the Division of Water Quality within thirty (30)
days of receipt of the civil penalty assessment. No new evidence in support of a remission request
will be allowed after thirty (30) days from the receipt of the civil P nalty assessment.
This the
day of
i
SIGN TURF
ADDRESS
i
A
TELEPHONE I
i