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WQ0004298_2008 Residuals Annual Report_20090212
AININUAL LA1V1) AYrl-.IUA11Vlr U K1111IUAl1Vlr VUK1V1 t#: WQ0004298 '`County: Madison Year: 2008 Facility Name (as shown on permit): Town of Mars Hill Land Application Program Land Application Operator: Robert M. Sams Phone: (828)206-2386 Land application of residual solids as allowed by the permit occurred during the past calendar year? FRI Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A: Total number of application fields in permit: 2 Total number of fields land application occurred during the year: - 2 Total amount of dry tons applied during the year for all application sites: 18.0166518 Total number of acres land application occurred during the year: 18.3 Part B: Facility was compliant during calendar year 2008 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Quality. 2 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dategEi%l l0m-NR / DWQ corrective action taken. I Aquifer Protection Section 1. Only residuals approved for this permit were applied to the permitted sites. .FEB 1 2 .2009 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503:13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing 'violations." Darhyl Boone- Town Manager zz� 2 91 Permittee Name and Title (type or print) Signature of Permittee Date Signature of Preparer* ate Signature of Land Applies Date DENR FORM ACF (5/2003) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0004298 Facility Name: Town of Mars Hill Land Application NPDES # or NCO057151 WQ#: WWTP Name: Town of Mars Hill WWTP Residual Analvsis Data Laboratory: 1) Earth Environmental Services 2) Environmental Testing Solutions, Inc. 3) A&L Eastern Laboratories, Inc. 4) 5) Sample or CompositeDate EMEEMEEMEEME Molybdenum Mill "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are signific penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." .,x- 2 /)x Signature of Preparer / 6ate DENR FORM RSSF (5/2003) Farm mironmentai seNices Michael Ladd 75 Bison Lane Murphy, NC 28906 Robbinsville Lab (828) 479-6428 Madison County Lab (828) 649-9250 Residence (828) 837-9543 Name and Address of Facility: Date: 10/20/2008 Town of Mars Hill WWTP Sample Collector: RS P.O. BOX 368 Date and Time Sample Received: 10/1/2008 11:25 AM Mars Hill, NC 28754 Date and Time Sample Collected: 9/30/2008 Aft:'Robert Sams Date and Time Sample Analyzed: < MHT Land Application Analyses - Note: All results in mg/Kg Dry Basis unless othervvise noted. Test Belt Press Sludge Soil Site #1 Soil Site #2 Report Limit Method Units ACIDITY 1.1 meq/100g 1.0 meq/1009 SCA mg/L TOTAL SUSPENDED RESIDUE 1.0 SM2540D mg/L CATION EXCHANGE CAPACITY 11.1 meq/100g 7.1 meq/100g SCA per 100mi PH 5.9 7.5 7.1 0-14 SCA units AMMONIA NITROGEN 720 0.5 SCA mg/L NO2 + NO3-n < 20 1.0 SCA mg/L TOTAL KJELDAHL NITROGEN 48000 SCA mg/L TOTAL PHOSPHOROUS 1900d SCA mg/L PERCENT TOTAL RESIDUE 12.7% 88.1% 93% SCA mg/L • ORGANIC MATTER 2.9% 3.7% SCA NTU • BASE SATURATION - K 4.6% 6.9% SCA mg/L -H -Mg 34.4% 32.4% -Ca 60.1 % 59.4% -Na 0.9% 1.2% PLANT AVAILABLE (surface) 14,544 PPM/dw NITROGEN- PPM DRY WT (subsurf) 14,904 PPM/dw TEMPERATURE SM255013 deg C MANGANESE 320 260 SCA mg/L MAGNESIUM 4000 5300 1 600 SCA mg/L SODIUM 970 44 19 SCA mg/L CADMIUM < 1.9 < 0.28 < 0.27 SCA mg/L CHROMIUM 26 34 32 SCA mg/L COPPER 300 44 21 SCA mg/L LEAD 25 12 10 SCA mg/L NICKEL 25 15 8 SCA mg/L ZINC 750 62 29 1 SCA mg/L CALCIUM 11000 1900 1200 SCA mg/L POTASSIUM 6100 5100 460 SCA mg/L ALUMINUM 8900 N/A NIA SCA mg/L ARSENIC < 3.8 1.2 1.4 1 SCA mg/L SELENIUM 6.4 < 0.55 < 0.54 SCA mg/L MOLYBDENUM 4.7 < 0.55 < 0.54 SCA mg/L MERCURY 3.1 0.065 0.040 SCA mg/L N.C. Laboratory ID# 352 Analyzed By: S Lab Supervisor: Michael J. Ladd; EES-Robbinsville Certified By: Ip dl: ftut Available (PAN)aaf�IKdonsand Ift"d am mx L4 do WWWA tj =SNOW* 39S 01" "fto 2" lwmr�" 2. "WAY dmtXmgfle dwmddMQYAwj%4FqFwFJ oft AID. W-kw oftdab" fa do . - I 8PPH=d R.Old On me(bod Mond *%!z UbK dw blkwaft&B followbi cdcwadm as a PAN Aw stwom Appumtifo® PAR x C PAR "m Dry Wd&% IPA" for sowuxg*m Appikedon PAN mi�)] + ONO -7 PMW wwxk ROBBINSVILLE LABORATORY (828) 479-6428 MADISON COUNTY LABORATORY (828) 649-9250 FAX: (828) 645-3706 RESIDENCE (828) 837-9543 FAX: (828) 835-8631 Client: I, ��1.,1n/\ Address: r f Phone: � �-� — � 0( EARTH ENVIRONMENTAL SERVICES MICHAEL LADD-OWNER P.O. BOX 1177 MARSHALL, NC 28753 75 BISON LANE CHAIN -OF -CUSTODY RECORD MURPHY, NC 28906 Analytical Request Report To: /`c, J Bill To: 'To ✓� P.O. # / Billing Reference: _ FAX #: —rV, �3 ��— o j Init Lab Temp: '� J Rec Lab Tee U *Re es� Due Dat�p- (�c� .1 e ®� J1 • 0 Tv AMON ILL ITE M#, . SAMPLE DESCRIPTION,:, R SID. T TIME, MATRIX'_,, +EES #- :. • • • • _ • REMARKS SMI mm RON IN I IN mm 0 11111 F1 21 1 FAS FA 11 FAS 04 04 110 ■�--■..... mossommosson ■�--■.... sommossommons SHIPMENT OUt/DATE METHOD ITEM RETURNED/DATE # RELINOUISEDBY/AFFILIATION ACCEPTED BY/ DATE TIME ' -■ r /_ RO/ fM�fiWr�� ADDITIONAL COMMENTS:■ __ ■ __ ■ ■ SEE REVERSE SIDE FOR INSTRUCTIONS CP-0771-B ROBBINSVILLE LABORATORY (828) 479-6428 MADISON COUNTY LABORATORY (828) 649-9250 FAX: (828) 645-3706 RESIDENCE (828) 837-9543 FAX: (828) 835-8631 Client: Ow Pj�-J'L Address: mom\ Ni Phone: EARTH ENVIRONMENTAL SERVICES MICHAEL LADD-OWNER P.O. BOX 1177 75 BISON LANE MARSHALL, NC 28753f� 1 c MURPHY, NC 28906 Report To: (`��J�(�� JCS ►�/L Bill To: I tYNl Et P.O. # / Billing Reference: FAX #: (, 0 CkO� cig- 06439, CHAIN -OF -CUSTODY RECORD Analytical Request [nit Lab Temp: Rec Lab Temp: *R,�4eessted 'u? Date: - luE I -ITEM C- Is IN IN is 1111 miles IPMENT.'METHOD ITEM RELINQUISED BY/ AFFILIATION VON ,L'_ SEE REVERSE SIDE FOR INSTRUCTIONS CP-0771-B I Certificate of Analysis Project name: Earth Environmental Services Collection date: 30-Sep-08 Date received: 1-Oct-08 Sample identification: #100827 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 081001.510 VA <: a (-�f p It G�'a n 41 Gk tS Sty-\4 q0, Sample number: 52819 Pa Method Result RL Units Date Analyst Footnotes Analyzed ercent Solids SM 2540 G 12.7 % 6-Oct-08 IvIbatber 1 Mercury EPA 7471 A 3.1 0.16 tng/kg 10-0ct-os Heasler 1 Aluminum EPA 6010 B 8900 19 mg/kg -7-o.t-03 Mcampbell 1 Arsenic EPA 6010 B <3.8 3.8 mg/kg 7-Duos Mcan,pi,ell 1 Cadmium EPA 6010 B <1.9 1.9 mg/kg 7-0c1-os A4eantpbell 1 Calcium EPA 6010 B 11000 38 mg/kg 7-0c1-os Mcampbell 1 Chromium EPA 601013 26 1.9 mg/kg 7-0.t-08 Mcainpbeu 1 Copper EPA 6010 B 300 3.8 nig/kg 7-0ct-08 Mcampbell 1 Lead EPA 6010 B 25 1.9 mg/kg 7-0ct-08 Mcampbell 1 Magnesium EPA 6010 B 4000 19 mg/kg 7-Oct-OS Mcampbell 1 Molybdenum EPA 6010 B 4.7 3-8 mg/kg 7-0ct-08 Mcatpbell ] Nickel EPA 6010 B 25 3.8 mg/kg 7-0ct-08 Mcampbell 1 Potassium EPA 6010 B 6100 19 mg/ clog 7-oct-os Mcampbell 1 Selenium EPA 6010 B 6.4 3.8 mg/kg -i-oct-o8 mcantpbeii ] Sodium EPA 6010 B 970 120 n1g/kg 7-0ct-os Meat» Abell 1 TEPA 6010 B 750 19 mg/kg 7-Cxt-08 Mcampbell 1 to + Nitrite SIv14500 1\103 F <20 20 mg/kg 9-oct-08 Heaslcr 1 T-6al Phosphorus SM 4500 P F 19000 390 mg/kg 9-oa-oe ltlotlin 1 • I Kjeldahl EPA 351.2 48006 20000 mg/kg lo-oct-os Celibki 1 1 Nitrogen Calculation 48000 7.9 mg/Icg 1 onia Nitrogen SM 4500 NH3 D 720 15 mg/kg 3-Oct-08 KEK rcent Solids SM 2540 G 13 0.1 S. U. 2-W-08 KEK SM 9045 C 5.9 % 2-Oct-08. KEK This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the sainples submitted for analysis. Certificate of Analysis Project name: Earth Environmental Services Collection date: 30-Sep-08 Date received: 1-Oct-08 Sample identification: 9100828 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 081001.510 r;S 1 ly Lziti� A -,pp 1\ (3 c1--R o)a V Sample number: 52820 Parameter Method Result RL Units Date Analyst Footnotes Analyzed Percent Solids SM 2540 G 88.1 % 6-oct-08 Mbarber 1 Mercury EPA 7471 A 0.065 0.023 mg/kg 10-oca08 Hasler 1 Arsenic EPA 6010 B 1.2 0.55 mg/kg 7-oct-08 Mcampbell 1 Cadmium EPA 6010 B <0 28 0.28 mg/kg 7-act-o8 Mcampbell 1 Calcium EPA 6010 B 1900 5.5 mg/kg 7-oct-08 Mcampbell 1 Chronuum EPA 6010 B 34 0.28 mg/kg 7-0c1-08 Mcampbell 1 Copper EPA 6010 B 44 0.55 mg/kg 7-oct-o8 mcampbeu 1 Lead EPA 6010 B 12 0.28 mg/kg 7-0ct-oe A4aampbeu 1 Magnesium EPA 6010 B 5300 280 mg/kg 7-oct-08 Mcampbell 1 Manganese EPA 6010 B 320 2.8 mg/kg 7-oct-08 Mcampbell 1 Molybdenum EPA 6010 B <0.55 0.55 mg/kg 7-oct-08 Mcampbell 1 Nickel EPA 6010 B 15 0.55 mg/kg 7-oct-08 Mcampbell 1 Potassium EPA 6010 B 5100 280 mg/kg 7-oct-08 Mcampbelf 1 Selenium EPA 6010 B <0.55 0.55 mg/kg 7-oct-08 Mcampbell 1 Sodium EPA 6010 B 44 17 mg/kg 7-oct-o8 Mcampbell 1 Zinc EPA 6010 B 62 2.8 mg/kg 7-0ct-08 Mcampbell 1 H SM 9045 C 7.3 % 2-Oct-08 KEK Jev 5 Ch oVcCZ LVV- Sample identification: #100829 Sample number: 52821 Parameter Method Result RL Units Date Analyst Footnotes Analyzed Percent Solids SM 2540 G 93.0 % 6-oct-08 Mbarbcr 1 Mercury EPA 7471 A 0.040 . 0.022 mg/kg 10-oct-08 Haasler 1 Arsenic EPA 6010 B 1.4 0.54 mg/kg 7-oct-o8 Mcampbell I Cadmium EPA 6010 B <0.27 0.27 mg/kg 7-oct-08 Mcampbell 1 Calcium EPA 6010 B 1200 5.4 mg/kg 7-0c1-08 Mcampbell 1 Chronvunl EPA 6010 B 32 0.27 mg/kg 7-0ct-oe Mcampbell 1 Copper EPA 6010 B 21 0.54 mg/kg 7-0c1-08 Mcampbell 1 Lead EPA 6010 B 10 0.27 mg/kg 7-oct-08 Mcampbell 1 Magnesium EPA 6010 B 600 2.7 mg/kg 7-oct-08 Mcampbell 1 Manganese EPA 6010 B 260 2.7 mg/kg 7-oct-os Mcampbell 1 Molybdenum EPA 6010 B <0.54 0.54 mg/kg 7-oct-08 Mcampbell 1 Nickel EPA 6010 B 8.0 0.54 mg/kg 7-00-09 Mcampbell 1 Potassium EPA 6010 B 460 2.7 mg/kg 7-oct-08 Mcampbell 1 Selenium EPA 6010 B <0.54 0.54 mg/kg 7-0ct-08 Mcautpbeil 1 Sodium EPA 6010 B 19 16 mg/kg 7-oct-08 Mcampbell 1 Zinc EPA 6010 B 29 2.7 mg/kg 7-oct-08 McampbCu 1 PI -I SM 9045 C 7.0 % 2-oct-08 KEK This report should not be reproduced, exept in its entirety, without the written consent ofEnvironmental Testing Solutions, Inc. Tile results in this report reLite only to the samples submitted for analysis. Report Number: dfid�N A&L EASTERN LABORATORIES, INC® R08280-0120 7621 Whitepine Road a Richmond, Virginia 23237-2214raYUQ WEj� Account Number: Phone (804) 743-9401 o Fax (804) 271-6446 46220 Website: www.al-labs-eastern,com • E-mail: office@al-labs-eastern.com R Send To: EARTH ENVIRONMENTAL SVCS Grower: EARTH ENV SVCS Submitted By: EARTH ENVIRONMENTAL SVCS 75 BISON LN MURPHY, NC 28906 Farm I D: Field I D: SOIL ANALYSIS REPORT Analytical Method(s): Page: 1 Date Received: 10/6/2008 Date of Analysis: 10/7/2008 Date of Report: 10/8/2008 Mehlich III Sample Lab Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.C. Number Number % ENR Ibs/A Rate Available ppm Rate Reserve ppm Rate K ppm Rate MG ppm Rate CA ppm Rate NA ppm Rate Soil pH Buffer Index H meq/100g meq/100g 100828 19180 2.9 92 M 109 VH NC=91 201 H NC=103 460 VH 1340 M _ 23 VL 7.5 11.1 100829 19181 3.7 114 M 23 L NC='19 191 H NC=98 275 VH 840 M 20 VL 7.1 7.1 Sample Numbed Percent Base Saturation• Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble as Salts Chloride Aluminum K %° M0, % Ca % Na., ; d�° . H - %o .. NO3-N ppm Rate SO4-S pp m Rate ZN . ppm Rate MN ppm Rate FE ppm Rate Cu ppm Rate B ppm Rate CL ppm Rate AL ppm Rate ms/cm Rate 100828 4.6 34.4 60.1 0.9 6.2 H NC=155 29 H NC=181 4.8 VH NC=240 100829 6.9 32.4 59.4 1.2 3.8 H NC=95 42 H NC=263 4.0 VH NC=200 This report applies to the sample(s) tested. Samples are retained a Values on. this report represent the plant available nutrients in the soil on a dry weight basis. Explanation of symbols: % (percent), ppm (parts per million), Ibs/A (pounds per acre), maximum of thirty days after testing. Soil Analysis prepared by: LTURAL LABORATORIES, INC. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). mslcm (milli -mhos per centimeter), meg1100g (milli -equivalent per 100 grams). � ,A & L EASTERN AGRICIJ ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Conversions: ppm x 2 = IWA, Soluble Salts mslcm x 640 = ppm, by e� — aul Chu, Ph.D. C11\1\VZVL 1V11JLtILIU 71'Aj' LVALLL\V "1L1L\1 1'Vl�l�l Afttach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Town of Mars Hill WWTP Total Dry Tons Applied (Annual): 12.86875 WQ0004298 Cation Exchange Capacity (non 503 only): Robert M. Sams Owner: 14.5 Acres Permitted: 14.5 Site #: Larry Cody Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft .W1. posite Date• © a Q ��: I Total Phos- phorus •��� Annual Heavy Metal Field Loadings (Calculated in lbs/acre): c 1 21 3 4 5 6 7 8 9 10 11 12 4 � y o 0.8875 Arsenic 1 0 0 0 0 0 0 0 0 0 0.0067 0 0 0.0067 Cadmiuml 0 0 0 0 0 0 0 0 0 0.0034 0 0 0.0034 hromiuni 0 0 0 0 0 0 0 0 0 0.0462 0 0 0.0462 Copper 0 0 0 0 0 0 0 0 0 0.5325 0 0 0.5325 Lead 0 0 0 0 0 0 0 0 0 0.0444 0 0 0.0444 Mercury 0 0 0 0 0 0 0 0 0 0.0055 0 0 0.0055 Molyb- 0 0 0 0 0 0 0 0 0' 0.0083 0 0 0.0083 denum Nickel 0 0 0 0 0 0 0 0 0 0.0444 0 0 0.0444 Selenium 0 0 0 0 0 0 1 0 0 0 0.0114 0 0 0.0114 Zinc 0 0 0 0 0 0 0 0 0 1.3313 0 0 1.3313 Total Phos- 0 0 0 0 0 0 0 0 0 33.725 0 0 33.725 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includi the possibility of fi es and imprisonment for knowing violations" a9a q_ L C'4 i1 r 'baAlpl DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Mars Hill Permit #: WQ0004298 Annual Dry Tons Applied: 12.869037 )caner: Larry Cody Operator: 'site #: 01 Field #: 01 Robert M. Sams Cation Exchange Capacity (non 503): 11.1 Acres Utilized: 14.5 Acres Permitted: 14.5 o �, S o S eci Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) 1 e Cond, Dry, Wet, i Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo- ma- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop 2 Gal. Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 0/2/08 8100 558.62 12.7 0.295839931 Belt Press Sludge Dry 0 s 0.5 30% 48000 720 20 8.61723 ####### Fescue 1 0/3/08 6480 446.9 12.7 0.236671945 Belt Press Sludge Dry 0 s 0.5 30% 48000 720 1 20 6.89378 ##44###1 Fescue 2 )/20/08 9720 670.34 12.7 0.355007917 Belt Press Sludge Dry 0 s 0.5 30% 48000 720 20 10.3407 ####### Fescue 3 0 0 0 0 4 0 0 0 0 5 0 0 0 1 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 111 0 0 1 0 0 12 ?OTALS: 1 16761 As Cd Cr - Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied annual lbs/acre 0.006745 0.00337 0.04615 0.5325 0.044381 0.0055 0.00834 0.04438 0.01136 1.33125 33.725 25.851 0 Date lbs/ac ,urrent Cumulative lbs/ac 0.8166158 0.5678 V 1.6092 48.042 5.1252 .10996 .6810 2.2790 1.4490 29.599 -= 10/17/08 5400 'rior Years Cumulative lbs/ac 0.8098708 0.56444 1.56312 47.5099 5.08083 0.10446 2.67272 2.23466 1.43767 28.2684 'ermitted C. P. L. R.*** 36 34 nl 1338 267 IS nl 374 89 2498 'ermit PAN Limit 1st/2nd Crop „, ._. .:;:. ,..� ,,•;� 'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system lesigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are ignifica enalti s for submitting false information, including the possibility of fines and imprisonment for knowing violations." ��E ��V a2 C) *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of fadd App ier ate **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate *** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) AINIIIUAL 1viL' lAL3 riL' Lll LV1iUllrlT aulvllriniml r Vi(lvl" Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Town of Mars Hill WWTP Total Dry Tons Applied (Annual): WQ0004298 Cation Exchange Capacity (non 503 only): Robert M. Sams 3.8 Acres Permitted: 5.147614801 11.1 —Owner: Larry Cody 3.8 Site #: 1 Field #: 2 Residual Analysis Data(Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft • IN Total • •• •l�l Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 3 4 5 6 7 8 9 10 11 12 o d CD .. o 1.3546 Arsenic 0 0 0 1 0 0 0 0 0 0 0 0.0103 0 0.0103 Cadmium 0 0 0 0 0 0 0 0 0 0 0.0051 0 0.0051 hromiuir 0 0 0 0 0 0 0 0 0 0 0.0704 0 0.0704 Copper 0 0 0 0 0 0 0 0 0 0 0.8128 0 0.8128 Lead 0 0 0 0 0 0 0 0 0 0 0.0677 0 0.0677 Mercury 0 0 0 0 0 0 0 0 0 0 0:0084 0 0.0084 Molyb- 0 0 0 0 0 0 0 0 0 0 0.0127 0 0.0127 denum Nickel 0 0 0 0 0 0 1 0 0 0 0 0.0677 0 1 0.0677 Selenium 0 0 0 0 1 0 0 0 0 0 0 0.0173 0 0.0173 Zinc 0 0 0 0 0 0 0 0 0 0 2.032 0 2.032 Total Phos- 0 0 0 0 0 0 0 0 0 0 51.476 0 51.476 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, inclu the ssibility of fines and imprisonment for knowing violations" A' � `e r DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Mars Hill Permit #: WQ0004298 Annual Dry Tons Applied: 5.1476148 Owner: Larry Cody site #: 01 Field #: Operator: 02 Robert M. Sams Cation Exchange Capacity (non 503): 11.1 Acres Utilized: 3.8 Acres Permitted: 3.8 �. N o 2 Svecify Totals Per Acre % Solid s I Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Dry, Wet, Moist Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo- ma- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop 2 * Gal. Cu.Yd. Report in Gal. Crop 1 Crop 2 i 1/5/08 9720 2557.91 12.7 1.354.635474 Belt Press Sludge Dry 0 s 0.5 30% 48000 720 20 39.4578 ####### Fescue 1 0 0 0 0 2 0 0 0 0 3 0 0 0 0 4 0 0 0 0 5 0 0 0 0 16 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 12 COTALS: 25581 As Cd Cr - Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied knnuallbs/acre 0.010295264 0.00515 0.07044 10.81278 0.06773 1 0.0084 0.01273 0.06773 10.01734 2.03196 514763 39.457 0 Date lbs/ac �urrent Cumulative lbs/ac 0.268443864 0.3024 1.2324 28.94 3.3406 .0963 1.5597 1.24497 .6719 17.754��� 0.2581486 10.29728 1.16205 28.1302 3.27289 0.08791 1 1.54702 1.17724 0.6546 15.722 36 34 nl 1338 267 15 nl 374 89 2498 , 10/17/08 5400 N. 11rior Years Cumulative lbs/ac 'ermitted C. P. L. R.*** ?ermit PAN Limit l st/2nd Crop `I. certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system iesigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are ;ignifica enalties for submi 'ng false information, including the possibility of fines and imprisonment for knowing violations." Ql?lr�20 v *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature o Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loadine Rate k*** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL PATHOGEN AND VEUTOR A'1'TRAUT1ON REDUCTION NORM ' Facility Name: Town of Mars Hill Land Application Permit Number: WQ004298 WWTP Name: Town of Mars Hill WWTP NPDES Number: NCO057151 Monitoring Period: From January 12008 To December 312008 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4® Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 Alternative 2 ❑ Alternative 3 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ® Air Drying ❑ Composting ❑ jAerobic Digestion 2 Anaerobic Digestion❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number of Excee- dences Frequency of Anal sis y Sample Type Analytical Tech-ni u q Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to the 6th power CFU per gram of 3400 4300 6300 col./gram 0 1/year Grab 9222d 1000 mpn per gram of total solid (dry weight) Sahnonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 ❑ Option 2 ❑ Option 3 ❑ Option 4 2 Option 5 ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ No vector attraction reduction options were performed ❑ ;w CERTIFICATION STATEMENT (please check the appropriate statement) . ® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Robert M. Sams/Public Works Director Prepare Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) EARTH ENVIRONMENTAL SERVICES 75 Bison Lane Murphy, NC 28906 Residence — (828) 837-9543 Robbinsville Lab — (828) 479-6428 Marshall Lab — (828) 649-9250 Shelby Lab — (704) 482-5227' E-Mail — earthenvser@,,webworkz.com\ October 21, 2008 NC ID#474, 052 Mr. Robert Sams Town of Mars Hill P.O. Box 368 Mars Hill, NC 28754 Dear Mr. Sams: Following is a report of laboratory analyses for digester sludge samples received 10/15/2008. Colony Counts dt ,mm�le Pate Cnlifhr rlencitiec (enlnnirc/arum) o Tntnl Cnlvlc 1 0 ml 0 1 ml 001 rnl 1 1017/08 3,900 Colonies/Gram 0.88% 34 7 1 2 10/8108 4,200 Colonies/Gram 0.88% 37 10 1 3 10/9/08 3,500 Colonies/Gram 0.88% 31- 8 1 4 10/10/08 4,800 Colonies/Gram 0.89% 43 9 0 5 10/13/08 3,400 Colonies/Gram 0.88% 30 3 0 6 10/14/08 4,800 Colonies/Gram 0.88% 42 6 1 7 10/15/08 6,300 Colonies/Gram 0.89% 56 11 4 Geometric mean for all seven samples: 4,300 colonies/gram. Thank you for your business. If you have any question or need additional sample analyses performed, please call. Respectfully submitted, rn J�X7'A ! 'C Michael J. Ladd Laboratory Director ROBBINSVILLE LABORATORY (828) 479-6428 MADISON COUNTY LABORATORY (828) 649-9250 FAX: (828) 645-3706 RESIDENCE (828) 837-9543 FAX: (828) 835--86311� Client: Address: ),�t 14 P\j-C_ ac�'%��� Phone: 81 '— L!? T (2'T-s> EARTH ENVIRONMENTAL SERVICES MICHAEL LADD-OWNER P.O. BOX 1177 MARSHALL, INC 28753 75 BISON LANE CHAIN -OF -CUSTODY RECORD MURPHY, NC 28906 Analytical Request Report To: & 6e�, Bill'To: ]nit Lab Temp: P.O. # / Billing Reference: FAX #: Rec Lab Temp: *Requested Due Date: Sampled By (pri t)- ole,4, M, WA REMARKS 'p SAMPLE- RIPTI MME0111111 son loss 1jjj jolool ME E =monsoon 11010100000 SHIPMENT METHOD ITEM ACCEPTED BY/ AFFILIATION 'DATE-,, ADDITIONAL COMMENTS: SEE REVERSE SIDE FOR INSTRUCTIONS cP-0771-s Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Digester Temperature:' Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: a 146F 0.1 5.0 1.0 Ililiters Dry Solids grees Celsius qrees Celsius Oxygen Uptake Rate: 5.81 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.54 mg Oxygen/glhr Average Temperature: 16 degrees Celsius Temperature Correction Factor. 1.31079601 Temperature Corrected Specific Oxygen Uptake Rate: 0.70 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. (salnupw) owpl 9 :paaC) ale.N aMLqdn u96Rx® Z90V9 + X9960'0- = A ■ A N N O fD O. ice: 3 t 1 t Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Mars Hill Biosolids Permit Number:FMQ6042 Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 3: 5/20/2098 13:30 Michael Ladd 1000 0.88 16 15.7 Slope: Intercept: Correlation Coefficient. 0.1 5.4 1.0 Dry Solids grees Celsius arees Celsius Oxygen Uptake Rate: 5.71 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.65 mg Oxygen/g/hr Average Temperature: 16 degrees Celsius Temperature Correction Factor: 1.31079601 Temperature Corrected Specific Oxygen Uptake Rate: 0.86 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 6 5 �. 4 a� E 1 f y =-0.0951 x + 5.5107 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1b it Time (minutes) r--- Y � 7 Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name:i Biosolids Permit Number:, Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning End Dissolved Oxygen Level 16. 13/2008 9:4 0 6/13/2008 9:450 liliters Dry Solids grees Celsius ❑rees Celsius Slope: 0.1 Intercept: 4.3 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 4.73 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.50 mg Oxygen/g/hr Average Temperature: 17 degrees Celsius Temperature Correction Factor: 1.225043 Temperature Corrected Specific Oxygen Uptake Rate: 0,62 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. y =-0.0789x + 4.352 Oxygen Uptake Rate Chart 4.5 4 � 3,5 c 3 I 2.5 O 2- o N I N ' 0 1.5 1 I 0.5 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Time (minutes) t) Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Digester Temperature:' Sampling Daterfime: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning T End T Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: VA Ladd liliters Dry Solids grees Celsius arees Celsius 0.1 4.0 1.0 5.08 mg Oxygen/hr 0.47 mg Oxygen/g/hr 18 degrees Celsius 1.1449 Temperature Corrected Specific Oxygen Uptake Rate: 0.54 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. r- 4.5 4 3.5 3 8 aci 2.5 O d 2 0 N N cl fib y =-0.0847x + 4.0648 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 10 Il lG lJ i`r Time (minutes) ♦' ( 1 7 Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name-, Biosolids Permit Number.' Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: illiliters Dry Solids agrees Celsius mrees Celsius 0.1 4.5 1.0 5.10 mg Oxygen/hr 0.56 mg Oxygen/g/hr 19 degrees Celsius 1.07 Temperature Corrected Specific Oxygen Uptake Rate: 0.60 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 4.5 4 3.5 E 3 m a� 2.5 m 0 2 N 1.5 A 0.: y =-0.0851 x + 4.5793 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 10 II IL Time (minutes) Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Mars Hill Biosolids Permit Number: WQ004298 Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Ladd 1 0.83 % Dry Solids 18.3 degrees Celsius 18.5 dearees Celsius Slope: 0.1 Intercept: 6.2 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 5.95 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.72 mg Oxygen/g/hr Average Temperature: 18 degrees Celsius Temperature Correction Factor. 1.1449 Temperature Corrected Specific Oxygen Uptake Rate: 0.82 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 7 6 0 2 1 c y =-0.0992x + 6.2873 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E Time (minutes) Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Biosolids Permit N Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time:' Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor. 1 /2008 17. Dry Solids grees Celsius arees Celsius 0.1 5.5 1.0 6.06 mg Oxygen/hr 0.59 mg Oxygen/g/hr 18 degrees Celsius 1.1449 Temperature Corrected Specific Oxygen Uptake Rater 0.68 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 6 5 4 0) E c w M 0 3 1 y =-0.1009x + 5.6023 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1t Time (minutes) Town of Mars Hill WQ0004298 Request for additional information: 2008 Exchangeable Sodium Robert M.Sams Town of Mars Hill IECEW D AUG 12 2CU9 Asheville regional Office =tagea-jifer Protection icuC-WED 1 DENR 1 DWQ Aquif— P mtertion Section AUG 10 2009 Town of Mars Hill WQ0004298 2008 Exchangeable Sodium Percentage Field #1- 1.9%ESPY C1LS \> I Field #2- 2.5% ESP See attached calculation sheet for. details. QA 04 09 01:38p Earth Environmental Ser. 8288358631 ` (828}b'ts�sss� ,inn 04,09 12:49p MmW Boone aca-c�rnoys t I -Lee r�o�rnoc r-sae _ ass -as= IU: w rnA+-rU1=1" o ors - 14"+ y1 Apo yt c am` 4I120.1" sod"m= pro OMP) is an evalmdos that cm 1 posswe access 3OwOM won ia*c, Soil itsdf m o Fsw is soils eatioa exshst wit!► (Cq .that r °Od h9 *e s detaasiaatioa cm 6t Mack lion s tYPical sp0 fa 7 �nduata rOWTIs: Ift s 190 EWw CED EsP=Rw*MjPwbft sodains Pareec"w NK-Soawmc+WA01080M CEO $ coon Ent rw WSORIPID 1: tip') 0 MW CDC of a soil is 5.4 aAW100 cm; aad the Na % 0.7 WbalisamewboomblauxUMPOCOGROW Pbx 100 ESP= COC a7:100 5.4 Wa100 S /[dog op q aged a dde mine pie of the and CawUbwa as p.2 1, p 7a Ese r0� r7S ��G e Na�yQ?.3b Cwc-�,� eSez +2-7-4737 °% a 6.30 0 W a r17 � C7 � � �jt l� ! f •�`J -oto/l of Mars ffi rl ���9�°0? Annual Report Review SOP Class B Land Application Annual Land Application Certification Form • Was a certification form submitted? YZT • Was land application conducted during the reported year?ye- • How many dry tons and dry tons per acre were applied? /$ D% 1ko • Were the applications within the permitted amount? y,,-,-S • Verify PAN if more than 10 tons/acre . • Did it indicate compliance?YRS • . Was it signed by the appropriate people? Yes 2. Monitoring • Were the analyses conducted at the required frequency? Y eS • Were the metals analyses reported on the Residual Sampling Summary Form?ye' • Were the results reported in mg/kg?yes • Were the metals within ceiling concentration permit limits?jPlls • If no, were the lab analyses attached? • Were all the required parameters tested?y,,s . • Was TCLP analysis conducted? NA. _. On �� re-70.�vace �Pe,��if Cr��% • Were the TCLP contaminants within regulatory limits? 3. Field Summary o Were the land application events recorded on the Field Summary Forms?ya • Was a Field Summary Form submitted for each field applied on?10.5 • Were all the residuals applied to permitted land?y25 • Were all the residuals applied from permitted sources?1,95 • Were the field loading rates for each metal and PAN calculated (year to date)? yIe5 • Were the cumulative pollutant loading rates calculated? fe1 • Were the calculations correct? U45 • Were the. PAN loading rates within permit limits?14-5 . • Were the heavy metal cumulative pollutant loading rates within permit limits?e $ • Were the residuals applied on a suitable crop?10 • Were the applications conducted during the crop's growing season?Ve,s • Were the Field Summary Forms complete?la • Was lime application on Field Summary Form? yes 4: Pathogen and Vector Attraction Reduction • Was a signed copy of the Pathogen and Vector Attraction Reduction Form submitted? a Did the form indicate period of coverage, the residual class, and the pathogen reduction alternative and the vector attraction reduction option used? ✓�' 0 Was the .ap�ropriate documental -ion to show pathogen and vector attraction reduction included in the report? GO• • Was pathogen and vector attraction reduction demonstrated according to 40 CFR Part 503 or 2T? 5. Soil Tests ff-- • Was a Standard Soil Fertility Analysis conducted for each field applied on?y.&S� -%_C&l 6-Sp • Were the soil pH's 6.0 or greater for each application field?yes • Were the copper and zinc indexes in the soil less than 3000 for each application field (state soils lab)?jej 6. General • Was the report in the proper format?1-2S ®N • Were any parts of the annual report missing? Ijo COVP-r PO o Was the report submitted on time?,45 sew - 4dd —1� �. /��/©� Reived 2li2/09 Class B Pathogen Review Alternative 1 - Fecal Coliforin Density • Was the sampling conducted at the required frequency? ItY • Were seven samples takenN. 4-S • Was the geometric mean calculated and done correctly?1,45 • Did the results show compliance (less than either 2,000,000 MPN/gram of total solids or 2,000,000 Colony Forming Units/gram of total solids)19 &S Alternative 2 - Use of Process to Significantly Reduce Pathogens (one of five) • Was the sampling conducted at the required frequency? Aerobic Digestion ® Was it an aerobic process (Inspection)? • Were logs submitted showing time and temperature? • Were temperatures within range for complete time period? • Was the time and temperature between 40 days at 20°C (68T) and 60 days at 15°C (59°F)? _Air Drying • Were residuals on sand beds or pave or unpaved basins for three months? • Was theambienttemperature above 0°C 02°F) for two months? • Were the residuals partially digested? • Were residuals exposed to atmosphere during two months above 0°C (not snow covered)? Anaerobic Di eg stion • Was it an anaerobic process (Inspection)? • Were logs submitted showing time and temperature? • Were temperatures within range for complete time period? .. • Was the time and temperature between 15 days at 350C (95°F) to 55°C (131T) and 60 days at 200C (68°F)? Composting • Was it a. composting procedure (notnatural decay under uncontrolled conditions)? • Were logs submitted showing time and temperature? • Was the temperature raised to 40°C (104T) or higher and remained at 40°C (104T) for five days? o Did the temperature exceed 55°C (13IT) for four hours during the five-day period? Lime Stabilization • Was alkaline material added to residuals a form of lime (hydrated lime, quicklime, lime containing kiln dust or fly ash)? • Were logs submitted showing time and .temperature? • Was the pH raised to 12 after two hours of contact? • Were logs submitted showing time and pH? o Was the temperature corrected to 25°C (77°F)? �j Vector Attraction Reduction Review a • Was the sampling conducted at the required frequency? 38% Volatile Solids Reduction' Was there 38% reduction? • Were lab sheets/calculations in report? • Was the reduction on volatile solids (not total solids)? • Was the samples taken at beginning of digestion process and before application (Inspection)? • Were calculations correct? 40-Day Bench Scale Test • Were residuals from anaerobically digested treatment (Inspection)? ® Were residuals anaerobically digested in lab? • Was the test run for 40 days? ® Was the test done between 300C (86°F) and 370C (990F)? • Was the reduction on volatile solids (not total solids)? o Was the reduction less than 17%? ® Were lab sheets/calculations in report? ® Were calculations correct? 30-Day Bench Scale Test • Were residuals from aerobically digested treatment (Inspection)? ® Were residuals aerobically digested in lab? o Were residuals 2% or less total solids? ® Was the test run for 30 days? o Was the test done at 200C (680F)? m Was the reduction on volatile solids (not total solids)? ® Was the reduction less than 15%?. a Were lab'sheets/calculations in report? © Were calculations correct? Specific Oxygen Uptake Rate (SOUR) ® Were residuals from aerobically digested treatment (Inspection)?yt5 m Were residuals 2% or less total solids (dry weight basis) (not diluted)?yam' ® Was the test done between 10°C (50T) and 30°C (86T)?Yes ® Was the temperature corrected to 20°C (68'.F)?)z5 ® Was the SOUR equal to or less than 1.5 mg of oxygen per hour per gram of total residual solids (dry weight basis)?1,0 • Was the sample holding time under two hours?Y111r- 9 Was the test started within15 minutes of sampling or aeration maintained? T&-5 14-DE Aerobic Process ® Were residuals from aerobically digested treatment (Inspection)? ® Were the residuals treated for 14 days? ® Was the residuals temperature higher than 40T (104T) for the 14-day period? ® Was the average residuals temperature higher than 45T (11.3°F)? Alkaline Stabilization ® Was the pH of the residuals raised to 12 or higher by the addition of alkali? ® Did the pH'of residuals remain at 12 or higher for two hours without the addition of more alkali? ® Did the pH of residuals remain at 11.5 or higher for an additional twenty-two hours without the addition of more alkali? • Was the pH corrected to 25T (77T)? Dryingof Stabilized Residuals ® Does the residuals .contain any unstabilized residuals? ® Were the residuals mixed with any other materials? ® Were the residuals dried to 75% total solids? Drying of Unstabilized Residuals © Were the residuals mixed with any other materials? ® Were the residuals dried to. 90% total solids? . Injection ® Was there any significant. amount of residuals on land surface one hour after injection (Inspection)? ® Was injection done on pasture or hay field? ® Was injection done at time that crop was growing? o If Class A with respect to pathogen, were residuals injected within eight hours after discharge from pathogen treatment? Incorporation ® Were the residuals incorporated into the soil within six hours after application? ® Was incorporation done on pasture or hay field? ® Was incorporation done at time that crop was growing? ® If Class A with respect to pathogen, were residuals incorporated within eight __.._.._..__._.hours -after -discharge- from -pathogen- treatment?..__________...__.___._._.._..._..___..._.._._.._______.._.__.__..__:.__..__._._.__._._.............__.. Beverly Eaves Perdue, Governor Dee Freeman, Secretary North Carolina Department of Environment and Natural Resources Coleen H. Sullins, Director Division of Water Quality Aquifer Protection Section FAX TRANSMITTAL To: %, -� sc_�,,S � o �-�" (o - 3333 From: b,, V Comment: -4zO bF-A I -e-V o-� N\(,,-S JA; l k w w'( p �.VL North Carolina Division of Water Quality — Asheville Regional Office 2090 U.S. Highway 70 Swannanoa, NC 28778 Aquifer Protection Section Customer Service 1-877-623-6748 Internet: h2o.enr.state.nc.us Nose Carolina Nturldif Phone (828) 296-4500 FAX (828) 299-7043 An Equal Opportunity/Affirmative Action Employer— 50% Recycled110% Post Consumer Paper Exchangeable Sodium Percentage Exchangeable sodium percentage (ESP) is an evaluation that can be used to determine possible excess sodium concentration in the soil itself. The ESP is the percentage of the soil's cation exchange capacity (CEC) that is occupied by the sodium cations. This determination can be made from a typical soil fertility evaluation and calculated as follows: Nax100 ESP = CEC ESP = Exchangeable Sodium Percentage NA = Sodium Concentration CEC = Cation Exchange Capacity Example 1: (ESP) ❑ The CEC of a soil is 5.4 meq/100 cm3 and the Na is 0.7 meq/100 cm3. What is the exchangeable sodium percentage? Na x 100 ESP = CEC 0.7 x 100 5.4 0.7 x 100 5.4 = F13.0 6-30 Compliance Inspection Report Permit: WQ0004298 Effective: 06/20/06 Expiration: 05/31/11 Owner: Town of Mars Hill SOC: Effective: Expiration: Facility: Residuals Land Application Program County: Madison PO Box 368 Region: Asheville Mars Hill NC 287540368 Contact Person: L Darhyl Boone Title: Town Manager Phone: 828-689-2301 Directions to Facility: From the intersection of NC Hwy. 213 and NCSR 1609, travel south on NCSR 1609 approximately 1.1 miles until the intersection with NCSR 1559. Tr vel southwest on NCSR approximately 0.5 miles until the intersection with NCSR 1560 the site is to north. System Classitications: Primary ORC: Robert M Sams Certification: 14793 Phone: 828-689-2301 Secondary" ORC(s): On -Site Representative(s): 24 hour contact name Related Permits: Inspection Date: 07/22/2009 Primary Inspector: Beverly Price Secondary Inspector(s): Robert M Sams Entry Time: 10:00 AM Exit Time: 11:00 AM Phone: 828-689-9850 Phone: 828-296-4500 Reason for Inspection: Follow-up Inspection Type: Compliance Evaluation Permit Inspectio T pe: Land lication of Residual Solids (503) Facility S s: ■ Compliant Not Compliant Question eas: Miscellaneous ues ions Record Keeping (See attachment summary) -73> ©� �i Page: 1