WQ0010689_Report_20140731

Annual Report Review Class A Distribution E, P
Reporting Period: 2®I j 6I16 II q
Permit Details: W Q D©11®% 29 t4a,4, CAT W ©od Be); (6-- Ask D-RS
Is 503? too
C1ass(Dor B?
Maximum Dry Tons Per Year:
Number of acres permitted: tJh
Number of fields in permit: NA
Counties that land is permitted for. N
Monitoring Frequency for TCLP: l X %r ,,, •' 4 r-y c.l-e-
Monitoring Frequency for Residuals Analysis: 5,-.sed
Monitoring Frequency for Pathogen & Vector Attraction Reduction: PfA
1. Class A Annual Distribution and Marketing/Surface Disposal Certification Form
Was 'a certification form submitted?y-e-5
Was distribution conducted during the reported period?
How many dry tons were produced and distributed? 9 57(o.12
Were the distributions with the permitted amount? yes"
i s�'' ;:`''e^ d^'e^ te�wN
Were recipients information listed? �(��' geo-�- s�.«`c
Did it indicate compliance?y,es o F 9 rec�P;c -i lob s�e� s hpc� &'Ies o go' a �Q 'RCZ9
Was form complete? V-e,5
3
d� /` -
Was it signed by the appropriate people?�t�s
6�
2. Monitoring Ape - �1-
• Were the analyses conducted at the required frequency? Q�� f1rjy Y e-s w.Was
an analyses taken for each source that was distributed? Its .
-A,{ >fo,.+k
Were the metals analyses reported on the Residual Sampling Summary Form?�-O-
Were the results reported in mg/kg? I-ef D-4 r-tpo,+ N D) should b e
L RL
Were the pH's 6.0 or greater for each residual sample?
Were the heavy metals within ceiling concentration permit limits?IDS
Were the lab analyses attached?' ,a
Were all the required parameters tested? q45
Was TCLP analysis conducted? i -e-5 r-Lll "ru-P cla cn-. Uzi
Were the TLCP contaminants within regulatory limits? y-es
Was a corrosivity, ignitability, and reactivity analysis conducted? col
3. Pathogen and Vector Attraction Reduction t4 k
Was a signed copy of the Pathogen and Vector Attraction Reduction Form submitted?
Did the form indicate the period of coverage, the residual class, and the pathogen reduction
alternative and the vector attraction reduction option used?
Was the appropriate documentation to show pathogen and vector attraction reduction included
in the report?
• Was pathogen and vector attraction reduction demonstrated according to 40 CFR Part 503?
Class A Pathogen Review
To be Class A, residuals shall meet either fecal Coliform density or salmonella density.
ITV �r'� S(�Z i'�Q-Gv D� Q,w� IM• '�4� ��O N i5
Re-5 6mk ��si�i�o`s ��tw�w�aa-y F02N�
wl �orrec.��ot�s

Fecal Coliform density
Was the sampling conducted at the required frequency?
Were multiple sarnples taken?
Was each sample less than 1000 MPN/gram of total solids?
Salmonella density
Was the sampling conducted at the required frequency?
Were multiple samples taken?
Was each sample less than 3 MPN/4 grams of total solids?
To be Class A, residuals shall meet one of the following alternatives:
Alternative 1 — Time/Temperature
Were the residuals maintained for correct time and temperature?
Were logs submitted showing time and temperature?
Were temperatures within range for complete time period?
Alternative 2 — Alkaline Treatment
Were logs submitted showing time and temperature?
Was the pH raised to 12 or greater and maintained for 72 hours or longer?
Was the temperature 52°C (126°F) for 12 hours or longer while the pH was 12 or
greater?
Were logs submitted showing time and pH?
Was the temperature corrected to 25°C (771F)?
Alternative 5 — Process To Further Reduce Pathogens
PFRP Composting
Were the within -vessel method or static aerated pile methods used?
Was the residuals temperature maintained at 55°C (131°F) or higher for three
consecutive days or longer in the within -vessel method or static aerated pile method?
OR
Was the windrow composting method used?
Was the residuals temperature maintained at 55°C or higher for 15 consecutive days or
longer in the windrow method, and the windrow turned a minimum of five times during
this time?
PFRP Heat Drying
• Was the residuals dried by direct or indirect contact with hot gases and the moisture
content of residuals reduced to 10% or lower?
• Did the temperature of the residuals or the of the wet bulb temperature of the gas in
contact with the residuals as the residuals leave the dryer exceed 80°C (176°F)?
Vector Attraction Reduction Review
Was the sampling conducted at the required frequency?
Option 1 — 3 8% Volatile Solids Reduction
Was there 38% reduction?
Were lab sheets/calculations in report?
Was the reduction on volatile solids (not total solids)?

• Were the samples taken at beginning of digestion .process and before application
(Inspection)?
• Were calculations correct?
Option 2 — 40-Day Bench Scale Test
Were residuals from anaerobically digested treatment (Inspection)?
Were residuals anaerobically digested in lab?
Was the test run for 40 days?
Was the test done between 30°C (867) and 370C (990F)?
Was the reduction of on volatile solids (not total solids)?
Was the reduction less than 17%?
Were lab sheets/calculations in report?
Were calculations correct?
Option 3 — 30-Day Bench Scale Test
Were residuals from aerobically digested treatment (Inspection)?
Were residuals aerobically digested in lab?
Were residuals 2% or less total solids?
If not 2% total solids, was the test ran on a sample diluted to 2% with unchlorinated
effluent?
Was the test run for 30 days?
Was the test done at 20°C (68°F)?
Was the reduction of on volatile solids (not total solids)?
Was the reduction less than 15%?
Were lab sheets/calculations in report?
Were calculations correct?
Option 4 — Specific Oxygen Uptake Rate(SOUR)
Were residuals form aerobically digested treatment (Inspection)?
Were residuals 2% or less total solids (dry weight basis) (not diluted)?
Was the test done between 10°C (50°F) and 300C (86°F)?
Was the temperature corrected to 200C (68°F)?
Was the SOUR equal to or less than 1.5 mg of oxygen per hour per gram of total
residual solids (dry weight basis)?
Was the sampling holding time two hours?
Was the test started within 15 minutes of sampling or aeration maintained?
k X Option 5 —14-Day Aerobic Process
Were the residuals from aerobically digested treatment (Inspection)?
Were the residuals treated for 14 days?
Was the residuals temperature higher than 40°C (104°F) for a 14-day period?
Was the average residuals temperature higher than 45°C (1137)?
Option 6 — Alkaline Stabilization
Was the pH of the residuals raised to 12 or higher by the addition of alkali?
Did the pH of residuals remain at 12 or higher for two hours without the addition of
more alkali?
• Did the pH of residuals remain at 11.5 or higher for an additional twenty-two hours
without the addition of more alkali?
• Was the pH corrected to 25°C (777)?

Option 7 — Drying of Stabilized Residuals
Does the residuals contain any unstabilized residuals?
Were the residuals mixed with any other materials?
Were the residuals dried up to 75% total solids?
Option 8 — Drying of Unstabilized Residuals
Were the residuals mixed with any other materials?
Were the residuals dried to 90% total solids?
Option 9 — Injection
Was there any significant amount of residuals on land surface one hour after injection
(Inspection)?
Was injection done on pasture or hay field?
Was injection done at time that crop was growing?
If Class A with respect to pathogen, were residuals injected with eight hours after
discharge from pathogen treatment?
4.General
Was the report in the proper format? Ye-s
Was the annual report complete? y-e-J
Was the report submitted on time? N a , 'RcvJ- AA-- -z 54ta-t4y 3191 t LJ

RECEIVED. �n
iomsion of Water Resources
AUG . _ 1 2014
Water fivality Regional Operations
Asheville Regional Office
July 31, 2014
NCDENR Water Quality Regional Operations
Asheville Regional Office
2090 U.S. Highway 70
Swannanoa, NC 28778
Baxter.
RE: Compliance Evaluation Information Resubmittal
Baxter Healthcare, North Cove Steam Generation Plant
Permit No.WQ0010689
Dear Ms. Price,
This is a response regarding your letter to Baxter Healthcare dated June 30, 2014 requesting corrected
information for our 2013 Ash Distribution Program Report.
1. Attached is the 2013 Ash Inventory demonstrating our scrubber pond cleaning schedule.
Samples taken from the North Scrubber Pond were mistakenly referenced on the chain of
custody as being from the South Scrubber Pond (1 WBSP4413). This caused the analytical
results received on April 4, 2013 to be misidentified; these results (1WBSP4413) are in fact for
material taken from the North.Scrubber Pond.
2. Attached are updated Ash Distribution Information Sheets signed by all current ash recipients
dated 2014.
If you have any questions or require additional information, please contact me at 828-756-6017 or
michaelpisarik@,baxter.com.
Sincerely,
G
Michael J. Pisarik
Sr. Environmental Engineer
Enclosures:
Corrected Ash Inventory for 2013
Updated Program Information Sheets
Baxter Healthcare Corporation
PO Box 1390, Marion, NC 28752
T 828.756.4151

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet, Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to
(Recipient). Application of the aforementioned ash is prohibited ex e— pcptt in with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land).
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): Date: 7 : ## 1Y
Ash Recipient's Address: I q Z / &k2rl A 120& c�
IVe �v , ��°c
Intended Use of Ash: S-a -A m ftr- A ocee-1 T -- L; i-e- y.4 lVe PN i •vt,�{ASS
Expected Qty/Yr: 70 6
Page 2 of 3
Acres of Land: yq
Updated: 9-12-13

Ash Inventory
Estimated
Ash Moisture
WET Tons
as Hauled
Dry Ton
Date
Ash Reused
Type Ash
Recipient
(measured)
Conversion
12/31/12
SOUTH SCRUBBER POND
0.00
2/8/13
SOUTH SCRUBBER POND
0.00
2/19/13
Ash Results received
March
20
SOUTH SCRUBBER POND
Phillips
43.00%
11.40
March
480
SOUTH . SCRUBBER POND
English
43.00%
273.60
March
340
SOUTH SCRUBBER POND
Jenkins
43.00%
1,93.80
March
50
SOUTH SCRUBBER POND
Styles
43.00%
28.50
March
North Scrubber Pond.
-0.00
4/4/13
North Scrubber Pond'
0.00
Ash Results Received
June
672
North'Scrubber Pond
Phillips
45.00%
369.60
June
156
North Scrubber Pond
Styles
45.00%
85.80
June
72
North Scrubber Pond
McClure
45.00%.
39.60
June
12
North Scrubber Pond
Paul Boone
45.00%
6.60
June
90
North Scrubber Pond
English
45.00%
49.50
June
40
North Scrubber Pond
Ray Farm
45.00%
22.00
7/9/13
SOUTH SCRUBBER POND
0.00
8/23/13
SOUTH SCRUBBER POND
.0.00
9/12/13
Ash Results Received. .
September
SOUTH SCRUBBER POND
0.00.
September
164
SOUTH SCRUBBER POND
Ricky styles
46.00%
88.56
September
384
SOUTH SCRUBBER POND
Dean McClure
46.00%
207.36
9/27/13
North Scrubber Pond -
October
48
SOUTH SCRUBBER POND
Ray Clark
46.00%
25.92
October
48
SOUTH SCRUBBER POND
Kenneth Hughes
46.00%
25.92
October
274
SOUTH SCRUBBER POND
Terry English
46.00%
147.96
0.00
0.00
0.00
0.00
2850
1576.12
Note: Scrubber ash includes sandbox ash used to dry ponds

Baxter Healthcare, Corp.,
2859 Old Linville Road.
Marion, North Carolina 28751
Ash Distribution Program Information Sheet, Baxter Copy
Baxter Healthcare; Corp., is. the generator of the ash provided to - / eit"
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate .provisions shall be taken to ensure that the transportation of ash doesnot cause
nuisances andhazards to public health and safety or otherwise cause an adverse impact (e.g.; transport
wet ash in leak -proof trucks or cover dry ash)..
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash.
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms; barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e.,. limited to
that needed to meet the. liming -requirements of the crops being grown.on the land).
4 Ash shall not be placed within M feet of any surface water.:
0 Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by 'a liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
The ash shall not be applied .to any site that is flooded, frozen, or snow:covered:
A summary of the ash chemical_ analyses is 'located on page 2 of the information sheet. Detailed
laboratory results are available upon request.' .
Title to the ash will transfer from Baxter.Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third:'
party for any, spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare,, Corp to. Recipient as.an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare,. Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees) -
claim, demand, suit,. action; judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising. from or in connection with Recipient's receipt, trans ortati- 6andlin or other use of
p P P.. g
the ash.
Signed -(Ash Recipient):..
Date:
Ash Recipient's. Address;
/ �•a •✓ . AG 28 7
0 �si .. Intended Use of Ash: /Z Oo 4,0 D �� A?�a�✓
Expected Qty/Yr-: Acres of Land:cS-D
Page 2 of 3 :.
Updated:. 9-12713

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash. Distribution Program Information Sheet, Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to i1 1" 5gr2.Pns
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken. to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall -be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters: Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application When using ash, the following shall apply:
• The ash application rates shall be limited to, those that can be agronomically justified (i.e., limited to
that needed to meet the liming requirements of the crops being: grown on the land).
e Ash shall not be placed within 50 feet of any surface water,
• Ash shall -not be placed within one foot of the'seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring_.
• The ash shall not be applied to any site that is flooded,_ frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees. that the ash .is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient: In exchange therefore, Recipient agrees to indemnify; save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising, from or in connection with Recipient's receipt, transportation; handling or other use of
the ash. .
Signed (Ash Recipient): �.J�Ir1.i1�1J: ds Date: 71./��./y
Ash Recipient'.s Address:. - 7:9 9 7 . .. 14wy Jg _
-nle W I *.Id . Nc87s
Intended Use of Ash:: A q u e t4 Ault . Sa i j. an.,fly�D Ud M P✓�
Expected Qty/Yr: Acres of Land: l0 2,
Page 2. of . 3
Updated: 9-12-0

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet, Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to �AI C�M,k
(Recipient). Application of the aforementioned ash is prohibited exe t in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored .to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the' land).
• Ash shall not be. placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 1.00 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10 centimeters per second. If such a
liner/cover is provided, ash shall riot be.placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request:
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill,- misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees 'that the ash is being delivered by Baxter. Healthcare, Corp to Recipient: as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including at fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including -any governmental authority, whether for bodily injury (including death) or damage to
property, arising. from or in connection with Recipient's. receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): Date: 7 2/- /1/
Ash Recipient's Address: w J. ; I l e 120..E
m A2Z.N Ne- 2e 7-
Intended Use of Ash:
Expected Qty/Yr: IS-0 . � o
Page 2:0f 3
Updated: 9-12-13
Acres of _Land:. S'17

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet, Baxter Copy
Baxter Healthcare; Corp., is the generator of the ash provided to e,`
(Recipient). Application of the aforementioned ash is pro ibit6d except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does .not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e:; limited to
that needed to meet the liming requirements of the crops being grown on the land).
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10"6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to -
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability; damage, loss, cost, expense (including at fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): Date: 7-21- 041
Ash Recipient's Address: X ,2 .7 �e 2d g cl
22
Intended Use of Ash: t:7 N 1pA, t. e jk.e ✓,r
J
Expected Qty/Yr: l L�� /D•✓ - Acres of Land:
Page 2 of 3
Updated: 9-12-13

Baxter Healthcare, Corp.
2859 Old Linville Road
.Marion, North Carolina 28752
Ash Distribution Program Information Sheet', Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided toj<}� 1Dt� ail
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using -ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to
that needed to meet the liming requirements .of the crops being grown on the land). -
Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one; foot of the seasonal high water table.
•. Ash shall not be placed within 100 feet of any water supply well or spring unless underlain. and
overlain by a liner with .a maximum hydraulic conductivity of 10'6 centimeters per second. If'such a
liner/cover.is provided, ash shall not be placed within 25 feet of -any water supply well orspring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash .chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will.transfer from Baxter. Healthcare, Corp to Recipient upon delivery thereof. Thereafter;
Baxter Healthcare, Corp will have no responsibility andshall not be held liable by Recipient or any thud
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered. by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient.,.In exchange therefore, Recipient agrees to 'indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees);
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or 1.damage to
property, arising. from or in connection with Recipient's receipt; transportation, handling or other use of
the ash.
Signed : (Ash. ARecipient): Date:.. 9. is ly
( r )
Ash Recipient's Address: AL; 't ICar—L • I (<c7 ro d
New NG A_& 7
Intended Use of Ash! _ . S.rk p MJe... -YAS L (L. e L
Expected Qty/Yr: :. 0 D ^]'v Acres of Land: %00 . A C_,
Page 2 o. f 3
Updated: 9-127.13

Baxter Healthcare, Corp®
2859 Old Linville Road
Marion, North Carolina 28752
Ash .Distribution Program Information Sheet, Baxter Copy
Baxter Healthcare, 'Corp., is the generator of the ash provided to Ant. ;a q .
(Recipient). Application of the aforementioned ash is prohibited except in a cordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).,
Storage: The ash shall be adequately stored to prevent winderosion or surface runoff from carrying ash
into any surface waters. Keeping the. ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application:: When using ash,the following shall apply:
The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land):
4 Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a finer with a maximum hydraulic conductivity of 10"6 centimeters per,second. If such a
liner/cover is provided,, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses, is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse; misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and. against any and all liability, damage, loss; cost, expense (including attorneys' fees),
claim; demand; suit, action, judgment or, recovery asserted against Baxter Healthcare, Corp: by any' third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising. from or in Connection with Recipient's receipt, transportation; handling or other use of
the ash.
Date: 7'Signed (Ash Recipient):( 4
Ash Recipient's- Address: .13 //� �S .2Z/. - ,✓-a &4-4
in 1f 2�`y �G .2t 7S Z
Intended Use of Ash:- SD ' }.N 2.'c 4,-,e
Expected Qty/Yr::. Acres of Land:cre S
Page 2 of 3`
Updated: 9-12-13

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet, Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to De.►,� . _ Mb L k� tiZ
(Recipient). Application of the aforementioned ash is 'prohibited except in accordance' with the
instructions on -this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact-(e.g., transport
wet ash in leak=proof trucks or cover dry ash).
Storage: The, ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When, using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited: to ._
that needed to meet the liming requirements of the crops being grown on the land).
• Ash shall not be placed -within 50feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10'6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical: analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request:
Title to the ash will -transfer from Baxter Healthcare, .Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse; misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that "the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange .therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, .Corp
harmless from and against any and all liability, damage; loss, cost, expense (including. attorneys' fees),
claim, demand, suit,action, judgment or recovery asserted against Baxter Healthcare, Corp. by. any, third
party, including any governmental authority, whether for bodily injury (including death) or damage to .
property, arising from or -in connection with Recipient's receipt, transportation, handling or other use of
the ash. .

Baxter Healthcare, Corp
2859 Old Linville Road .
Marion, North Carolina 28752
Ash Distribution Program Information Sheet; Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to ���.✓.��L h/u.y /.-1
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions. shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact. (e.g., transport
wet ash in leak=proof trucks or cover dry ash).
Storage: The 'ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However; berms, barriers, or tarps, may be necessary under windy, or rainy conditions or if
erosion or runoff cannot be controlled. .
Application:. When using ash,. the following shall apply:
• The ash application rates shall be, limited to those that can be agronomically justified (i.e.- limited to
that needed to meet the liming requirements: of the crops being grown on the land):
e Ash shall -not be placedwithin 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high" water table.
• Ash shall not be placed within, 100 feet of any, water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10-6 centimeters per.second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2. of the information sheet... Detailed
laboratory results are available upon ,request-.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter;
Baxter Healthcare, Corp will. have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse; misapplication or other mishandling of the ash. Recipient acknowledges and
Agrees that..the ash is being delivered. by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability; damage, loss, cost, expense.(including attorneys' fees),
claim, demand, suit, Action;:judgnient or recovery assertedI..against Baxter Healthcare, Corp by any third
1.party, including any governmental authority, whether for Bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt,: transportation, handling or other use of
the ash.
Signed Ash Recipient): Date: 7 Z/-/
Ash Recipient's Address: to S C
- ^
Ne- NL2a'.77
Intended Use of Ash aOe- /h c.-, T
Expected Qty/Yr: 3. 5. 2,: f. OA15 Acres of Land:
Page. 2 of 3-
Updated: 9-12-13

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet, Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to K (Recipient). Application of the aforementioned ash is prohibite-d exce in accordance with the
instructions on this sheet.
Transport' Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the -ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled. .
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land).
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not 'be applied to any site that is flooded, frozen, or snow-covered.
A summary of .the ash chemical analyses is located on page 2 of the information; sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to.
Recipient. In exchange therefore, Recipient agrees to indemnify,- save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees);
claim; demand, suit, action, judgment or recovery asserted against Baxter. Healthcare; Corp. by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property; arising from .or -in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient .. Gtl Date:
Ash Recipient''s Address:
D /d %2..t -We n297 2.
Intended Use of Ash-.'
GSS
Expected Qty/Yr: Gr'iO . f dam/ S Acres of Land: d-
CZv-s
Page 2 of 3
Updated: 9-12-13

�41
February 26, 2014
NCDENR - DWQ
Aquifer Protection Section
Land Application Unit
2728 Capital Boulevard
Raleigh, NC 27604
RE: 2013 Annual Ash Report
Permit No. WQ0010689
Wood Boiler — North Cove, NC
Enclosed is the annual ash distribution report for the calendar year 2013, using the forms
provided by NCDENR-DWQ.
If you have any questions or require additional information, please contact me at 828.756.6809.
Sincerely,
Amanda Richcreek
Environmental Engineer
Cc: NC Division of Water Quality (3 additional copies with enclosures)
Ricky Styles
(ED
Resources
MAR 1 8 2014
Water Quality Regional Operations
Asheville Regional Office
Baxter Healthcare Corporation
PO Box 1390, Marion, NC 28752
T 828.756.4151

Section 1 For'DMSDF
Class A Annual
Distribution and
RECEIVED
Qivision of Water Resources
MAR 1 8 2014
Water Ouality Regional Operations
Asheville Regional Office
Marketing Surface
Disposal Certification
and Summary Form and
Supplemental
SQ
Information
�

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0010689 FACILITY NAME: Baxter Healthcare Corporation North Cove Steam Generation Plant Ash
PHONE: [phone] COUNTY: McDowell OPERATOR: Baxter Healthcare
FACILITY TYPE (please check one): ® Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
21 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during. the past calendar year? Yes 0 No ❑ —► If No skip parts A, B, C and certify form below
Part A*: Part B*:
Month
Sources(s) (include NPDES # if Volume (dry tons) Recipient Information
Amendment/
applicable) January See DMSDF sheet
Residual In Product Out Names () Volume (dry tons) Intended use(s)
Bulking Agent
February supplemental for
March breakdown
une
FR
jOctober 1 6 ;® o
Annual
nuliu t� ems uses: D Wood Chips
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF Su 1
Part C: ( Pp)
Facility was compliant during the past calendar year with all conditions of the land application permit p Yes
(including but not limited to items 1-3 below) issued by the Division of WaterQuality:
1. All monitoring was done in accordance with -the permit and reported for the year as required and three (3) copies of certified laboratory results are aNo If No, ittachedain in Narritive
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
-e� Z -t
Signature of PermitiWe Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature -of Preparer**
(if different from Permittee)
z- Z-& y
Date
DENR FORM DMSDF (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0010689 FACILITY NAME4 Baxter Healthcare r;Coxporahon North'Cove Stem Gerieration'Plant Asl
PHONE: [phone]' COUNTY:[.,.,,,-.IVcDowell _ _.OPERATOR• Baxter •
FACILITY TYPE (please check one): ® Surface Disposal (complete Part A -"Month", "Souree(s)" and "Residual In" columns only)
R1 Distribution and Marketing (complete Parts A, and B)
Part A*:
Month
March
March
March
June
June
June
June.
June
June
October
October
October
Sources(s) (include NPDES # if
applicable)
110689
110689
110689
110689
i 10689
110689
110689
110689
110689
10689
10689
10689
10689
10689
10689
Annual
Volume (dry tons) ..
Amendment/
Bulking Agent
1.12
26.97
19.10
2.81
38.69
8.98
4.15
0.69
5.18
2.30
14.96
35.04
2.59
2.59
14.81
Residual In I Product Out
Part B*:
Recipient Information
Name(s) Volume (dry
tons)
Intended use(s)
10.28
246.63
174.70
25.69
330.91
76.82
35.45
11.40
273.60
193.80
28.50
369.60
85.80
39.60
Jim Philips
English Dairy Farm
11.40
Land
273.60
Land
Doug Jenkins
Ricky Styles
193.80
Land
28.50
Land
Jim Philips
369.60
Land
Ricky Styles
85.80
Land
Dean McClure
39.60
Land
5.91
6.60
Paul Boone
6.60
Land
44.32
19.70
73.60
172.32
23.33
23.33
133.15
49.50
22.00
88.56
207.36
25.92
25.92
147.96
English Dairy Farm
49.50
Land
Daniel Ray
Ricky Styles
22.00
88.56
Land
Land
Dean McClure
207.36
Land
Keith Ray Clark
25.92
Land
Kenneth Hughes
25.92
Land
English Dairy Farm
147.96
Land
1t more space is required, attach additional information sheets (FORM DMSDF (supp)):
used. Dry Wood Chips
Total Number of Form DMSDF (Supp)l 1
.icati
.icati
.icati
icati
icati
icati,
icatii
icati,
DENR FORM DMSDF (Supp) (12/2006)

Section 2 Form RSSF
Annual Residual
Sampling Summary
Form and Form B

Y�✓t Oi w �c�..� v
ANNUAL RESIDUAL SAMPLING SUMMARY FORM i✓
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
WQ0010689
Baxter Healthcare Corporation North Cove
Facility Name: Steam Generation Plant Ash
Laboratory: 1) Pace Analytical Services
Residual Source WQ # or WQ0010689
NPDES #:
WWTP Name: NA
�Vd
Residual Analvsic Data
2)
3)
4)
5)
Conc.
F Sample or Composite Date
Parameter
(mg g)
Limit
a
1WBS04�13
2WBS 4813
IWBS�
2WBS 441
SP82313 ASH
m
�I
'
Percent Solids (%)
NA
Arsenic,
75
6.3 ✓
8.0 ,/
7.7 ✓
9.4 ✓
9.1
Cadmium,
85
1.3
1.4 v
0.79 v
0.82 ✓
1.9
Copper.
4,300
53.7 ,/
68.7,i
50.7 v
45.8 ✓
Chromium
NA
18.7 ,/
20.7 ✓
13.0 ,i
13.2 ,/
26.4 ,/
Lead
840
18.7 ,/
20.4 ,/
6.6
7.0 ✓
22.6 /
Mercury
57
ND
ND !/
ND ✓
ND �/
ND,✓
Molybdenum
75
ND i/
1.1,/
0.3 8 ,/
ND,/
1.6 ,/
Nickel
420
15
16.4 ,/
7.3
7.4 ✓
20.6 V
Selenium.
100
ND ,o
ND,/
ND V
ND V
,
ND,.-
Zinc
7,500
143
1.57 ,�
84.5 ✓
95.8 ✓
197 ,/
Total Phosphorus
NA
2210 ',/
3010 ,/
1380 ✓
1400 ,/
'3070 ✓
Barium.
NA
1240 1
1530 v
661 ✓
604 ,/
1300 ✓ .
Calcium
NA
74700 ,/
82300 ✓
44700,/
42600V
84200 !/
Iron -
NA
1 10000 %/
11900 ✓
5350 ✓
4780!/.
10700 !/
]Ell
- �- ...... - F-- -__- - ...,,_lur, t'vllkvll-L-11 uuuw ttswu in tms corm are not applicable. Keterence the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
z- z& -I y
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0010689
Baxter Healthcare Corporation North Cove
Facility Name: Steam Generation Plant Ash
Residual Source WQ0010689
NPDES # or WQ#:
WWTP Name: NA
Residual Analvsis Data
Laboratory: 1) Pace'Analytical Services
2)
3)
4)
5)
Parameter
(mg/kg)
Sample or Composite Date
1WBSP4813
2WBSP4813
1WBSP4413
2WBSP4413
SP82313 ASH
Magnesium
Manganese'
10600 ,/
2270 v,
12200 ,/
2470 ,/
5510 ✓
1140 ✓
5450 4/
1200 ,/
12900 ,-
2670 ✓
pH
Potassium,
Silver
8.6 , ,�
14000 ,/
ND V
8.6 ,/
18900,/
ND ,/
8.4 ,/
14500 v
0.52 ,/
8.6 ✓
11600,/
0.43 ,f
9.7
21600V
0.93 ✓
,
Sodium
2180
2610 ✓
. 3380✓
2730,/
6040✓
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
2- z�
Date T
DENR FORM RSSF - B (12/2006)

Section 4 Ash Receiver
Signature Sheets
Signed Ash Distribution
Information' Sheets

Baxter Healthcare, Corp.
285:9 Old Linville.Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet
Baxter Healthcare, Corp., is the generator of the ash provided to -NW(-5 f ` 5
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not'cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in -leak-proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on. the land).
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within. 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability,- damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling- other use of
the ash. (�
Signed (Ash Recipient): �i11`Il`tj te: �" 0 — I Z--
Ash Recipient's Address: 7gJ?7 /Av V
&)L*06, AJC 20752-
Intended Use of Ash: A63 L Ti. C SOIL I eU7'
Expected Qty/YYr:
Page 1 of 3
Updated: 3/5/10
Acres of Land., 6,7?

'Baxter Healthcare., Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet
Baxter Healthcare, Corp., is the generator of the ash provided to P- r4Ze K Aft,!�'k-A
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g.,, transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be -adequately stored to prevgnt �vind erosion or surface runoff from carryx asli
into any surface waters. Keeping the ash ,slightly moistened will accomplish this objective utndor tsrmal.­
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply: ,_ G
• The ash application rates shall be limited to those that can be agronomically,lustified (i:e�,rlaitei '
that needed to meet the liming requirements of the crops being grown on the land),
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10'6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from. Baxter .Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter 1.1taltheare, Corp
harmless from and against any and all liability, damage, loss, cost; expense (including#;attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): Date: , 2. z S ._13
.Ash Recipient's Address: �r' `1 ' %'S Z 2 +" .
Intended Use of Ash: rr� ��'�%> �` °"-
Expected Qty/Yr:
Page l of 3
Updated: 3/5/10
Acres of Land: -7 .S 6)

113 to x I r I - ,.Its at I , "i". i', Z� ri�: � ( , � "i i -,ip ,
1 , N59 f Q; 101 is 15wid
W—W, N,q 0; An Ohna 28-S,*,
Ash Distribution Prograni Inforanation Sheet
B aster Healthcwx(,.orp., is lbe generator of the ash pnowded, to DOIA.5 .... . ....�'ev/�_,uS
. .. ......
kt;cipient)Applicabon of Te in accxn-htnc&; Tht,
on this sheet:
Jrreitt5porl, Adequate provisions ,;.halt be lakon 'ir, znsur (hal the to;m porlation of ash does nol cause
nuisances and hazards w publie health, and sat otherwise cause an afriversw WMaw (ag, hwaparl
wci. ash in leak-prcR)f umcks or cavu (hy nmk
iow any surfaowawrs. Ke-eping the ash slightly rn-,,-istened I= accmnoNh dos ONanhe ' Under 'zormal
QIV,J),fitiow, However her -Ins, bw-riers� 01, larps''way 1w Ste ,,Ssat� wl(fi?r wiody or
ero�.,kmi or ruii(Afcannot be
Jp,pikwtion. When using ash, the
A Ile ash appfication Yates shall be hm.ited zo tf osc dip -I Carl At. to
dur nveded to ineet the Haing requiemews thie rop,; fbeifl,(g �hc W I , grown or, -"c
as ASh WU mn be placed within 50 ficet of*arry sturf�iec vater,
* Ash ON! ma he placed)vifthin one foot ofthe, it}?te water suble.
,vdr) slhail be piac,,;'d w'ithin- 100 feet of al-,,,waier sappl� well or sprilg an'
f
vwrWia by is kner a miaximuni hrimukic :,owjuc-,Oviay oJ* 0)" fi)'e i..i3zax 0
hver/.,(""Ver is providedt ash shalf not be �`5 feel ior any Hie r Q.o,v vkdl; k.0
T he ash shal 1 not be appUed Q 0-iiii frozen, VIC,, 'y-* -Ock- �;f Cd.
is locatC6 on page of1ho infonnatiotl shoe'-
resuh" arc upon. requesi,
T'ide to, lilt, asfra ill transwr Orn Elmer liesitheare, Qwp to Wcipieal upon dehveny ther,2-01,
f3axipr i-Jealthwirc, Carp M have no wSpArMAY and Shall pt tDe held fiahkI by Recipient of wlv- third
panvy- l'or any, spil Muse, INSOPPIWAM iv vahw, MiAMNg V!, t"w e, ai'd
,Agrees thai tilt a.sh N bAng defivt%rrd b�, 13am.,cr 14yuhhown, Cwp io ReeWmin ab an awornatodmion
'Recipient. In excliallge therefclre. Rocipiew, iigree, Io indemnify, save, and hold Baxter- 1, lleakhcare,.Corp
hannies.,-, from an(j against any and all fiabda loan agc. ioss, Qxpeftse (inclading, attorney", 1,Eesj,
-laiin, d or recovery anewed. ��,gairjst. Fiax,14��,r I lealthcare, Coqp� hy chird,
lemand, �uit,
par, including any goverilnii�ntafl autfionty. wh0her Q Noddy jiijwry ioo��hoding dwath'! or dwit agk�.�
L, h-1 I I ,
prope.-l'y' 1rising "'roo, in with I other w.,�e �-to
Dam.
Si gne d A �3111-j Rec ip i e Yf ty,
......... ..
Address, -/I- ,:,I /one SKY
. ..... .... ... ..... . .. - -I'll 1 1-1... - f ... . . .......... . .....
Wended Use of A'W�:�'- Asia
Ac%S I K eyc.

Baxter Healthcare, Corp.
2859 old Linville Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet — Return this sheet to Ricky Styles
Baxter Healthcare, Corp., is the generator of the ash provided to i�er_4 / 6�4IS
(Recipient), Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage.: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or. tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land).
• Ash shall not be placed within 50 feet of any surface water,
• Ash shal l not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 106 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10"6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from :Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter .Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to'
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),.
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): Date: '�S ^ 1310,
Ash Recipient's Address: /1/2 F l54�•� � ��� jigS1
Intended Use of Ash: /c e IV. -I A -e
LIQ
Expected Qty/Yr:f 1i Acres of Land: 71
Page 1 of 3
Updated: 3/ 5/12

B.a ter f ". e" Corp.
nad
Marion, North Caro ire 2 7-52
Ash Distribution Program Information Sheet
Baxter Healthcare, Corp., is the generator of the ash provided to )(6 &4� L-aon
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
,Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
.Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically. justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land).
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10"6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on. page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Balmer Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental -authority, whether for bodily injury (including- death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): ��"1/ Date:
Ash Recipient's Address: j u j a_ I -oil �\_) aLna _ &-C�...,"
r.,
Intended Use of Ash:'
Expected Qty/Yr: ' 00 /0f -1 . (, 1 Acres of Land:
Page I of 3
Updated: 315110

4
Ash Distrilmdon Pro.gram Inforn-tation Slheel
Barter Healthf-are. Corp., i.s thegemerator ol' dw� as provided to
'
pzIl 3Recpient), Application o(fie al"Oreen6(n-tash is"prohil)Ited ecuo'danc., xOtlj ;he
oti this shoo.
Dlanspory Adequate provislows shall be taken to �!nsure, that the transponation of ash does cause
nuisances and hazards, to public health and safety or otherwise cause an alverse impact fe.g,, transpoll
or
Storage.- The ash shall be adequately sts:ired to pre,,f-ra tind erf.A'1011) OV MAOIff i"Offi ash
jilto anv sur'k:& waters. Keeping The asb slight)--, nloistk.ned will accurri.1.111-3h LhIS OhieCtive under norma"
J
S, 01- tart 0
com(litiolis. Hcnvever' bermst bam.er s" 111�� wil)& i-r n-,'rv, �.on
ert,:)Sicifl or 1 1 - cannot he Controlled
API)Ik'ation. When using ash, the
I'lle ash application mte,>, shali be Imuted Iko 1hose. thal (:an be Ju,tkfiteu 1, 1
tha! riceded it n;ect the limim-, requiveniewt-s of gilt c"rops heifl� iRWQI Q)31 I hc toildn.
Ash shal 1 not he placed vvid) ill 50 fieet of w�,� �varer-
0 Ash shall Tiol. be T..)Iaced withill one of tile sleasomal high Water tabit'.
s Ash shall not be ptaced within 100 fleet, arty Waler Supply wef! or spring uniess underlain arid
OvIe-dain bv- F.I. lintr With is maximum hvdravlic o*," celltiffielvl`s wL If 'a per Secor
linero"cover is prov.ded,. ash shall not be placcd t1. iflilin it ',4elf or �;Plifig.
a 11he asb shall not be, applit�d to -that is Rc,(xk,,d. frozen, or snow-Covu—ed,
A surninary of the ash cherolcal ana`vse. is ove zh-� t rmali(m
labormory restdts are available upon req-IWISI
116-- to the &sh w-11.1 transfer from Bixfer Healnkare, Corp tc, Rut�ipiem Upon del"Ve'), mereof. Thor+3a-ftev
Baxter Healam-tre, Cori.) will have ",m) and ;hail ool b,held I air f)", t"),
41 mc.� DY Kt:CPu- r�
W)Rv fiol xm, ent 'pifl. mlsuse� Inksappil 4-ath Ill or 1-iish c 6ze ash'. R ecirpl, utd',
th ash Is fvIng defivere-1-1 by Ba-,,;,t�,r as un m to
.Agrucs Ojai
Recipient- In exchall K -ge th refore., kek,)pient agrees ;mAevind'N' save and 17 ; id. Eitvxuev Healuhcart�, ("orl,
I±arvnless from and agamst. aj 3 and all habilit�-, darmilgC%. f()ss, Qost, exptmse iilridudinyl llees
N, '-�v any
1,Liii, iCI60� .0(4',Tiiezu Or 1'.,Ixw�t K, 011ird
. J
parr�, inehiding any uUvcrnjne.nvaJ whether fi-,; bodilv I'll urf,, �ricluidin�o, death', or dan-vage tc
properTy, arising from, or ill vomfwztion vith transpomation., ja t ts~ x It Other use of
S4)med (A-sh Recipient)� Date:
s 6 . ..... ..
Aih Recipient's Addm,,;s-
.... ....... . .. . .....
lutended c,&.Ash.
Ai,'f ('S 0;
. ... .....
.... .. .. li� . . .... ....... ..... ..... I

001001CITZ
rgy Generation �_A
Vharkm, N'ortb Carolina
As ffisirTution Prop -am Infoe-mation Sheet
SLEZ EnCTY BUY"V". inc. (13jopcmVer), 2851) CAd 1 in We R(ad, Whin, \C 28., ik ehc pencrat,,n oi�,
the ash pro�-ided to Ro" ipitnni Applic;titiov
a N wen wn I On ed asti iss p ro I i i k ile(i e:",' Fil I stllt w t i o > ci !1 " Cet
lAvvynwr. Adequate prc'lvisions' 4,,aH. tn: wks; a, or"s, Wai IN .
nuisances and hazards '�o public lhicnjlth and Wa-v x othy"4c catwe an a-dfncr! .Q inapacr rrampon
xA el ash in Wah,proij trucks or con ar Q M �
Snnwgc I he ash SIM11 "het ­-'n,td to, p-re�L'n-, wind crosimi or surtl'tce nnnofffrom; carrying ash
So an; surkice mrs. Keeping the Aqh SAPQ moly0wo "M a=-'nlplish Tht'-is objecli":v u;'Klt:r norrlai
flol:iever' bernns, bait iery — In P� nmy cc Pecessarl under or rainy conStAms or if
­rr"Sio!j or '-unoff bv
VVhcrI uAng W. ,,it wAYwhy ihad yvh:
* The ash applWon raw shMi heAnnhed :o dw"e Kai omi he a;m(2mnNQ0uRMed Om. Hohod w
dwi neededl w meet the kniing requirumens of nw c"Vs hdhp py"n on ow iwd').
* Ash shaH uot b(. placed wifl-in 50 c'f aw" wilier
* Ash shaH m be piaced VQ in ice K 4w of di'm ne4qmn I high -water tab!"
0 Ao onn nobe phiced 'xi.Khin' li0i.,'= ti tif?}c7 suppl' or �t' iii Jt ti tunderlain aml
=Wby m: 1W per V'suck-
is laf idleda:. h Shall m he 25 6_-C! +-! wa"er �.'t"Ppin § ef.
W a3h shaH m be applid vi anx the rho tz):'s. t:_:.iCred,
A Aunfitary of the ash Chnnical analyses, llocmed on pa":'.e 2 of the inf-unna.-Con, :sheet. Det',ailed
�zuhorntor� rcsulv� are ivaifahle upoil
Wic U, Ae onh wd! imnsbr Rom �o f*%;<.6"ri"-n.i zipon dclk"n-'% ih"reof' filhcrvaller' BioPo­er
have w) �;nd hW !i.a ! to,, it.:o thble hl ReApian or any thin, pan, thr any ipdl,
ion or other inishmiling 4 im N,. an"i, Agret:-+ '' al One '­iji
1, icing OCK ewd ny llollv'Cver '(',' '10 sm Rocy.� ;,. li,.
jACCq1tela agrees, "", inlernlli'_�, sc and hAd Wlnwr hmmins hom and aphist wjAWd aH NOW,
darnage. #>e hs. cosr, eywn, Qchiding aqorne�j�C-� aonn. denl'lld� 'xgner'-L'llncvverN
erl.ed agaiins! [36power by my thir'd incio".3 'goveinlnlental a'ulhorilyv'.1helher 1�or hodily
narl fonaluding deqM or P'ropen: "'OfIl V it) ith Rll!e"-'Wl*C"w lvceipl.
lk.'
.. ................. _Z. . ......
tft
AnvN of L an& a
. .. ..... . .. ... . ..
Kim i 01

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, forth Carolina 28752
Ash Distribution Program Information Sheet
Baxter Healthcare, Corp., is the generator of the ash provided to
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e:g., transport
wet ash in leak -,proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to
that needed to meet the .liming requirements of the crops being grown on the land).
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
l
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): Date:,
Ash Recipient's Address: S"2(��.� XR
Intended Use of Ash: �y
Expected Qty/Yr: Acres of Land: 45TV
Page 1 of 3
Updated: 9-12-1.3

Baxter Healthcare, Corp,
2859 Old Linville Road
Marion, forth, Carolina 28752
Ash Distribution Program Information Sheet
Baxter Healthcare, Corp., is the generator of the ash provided to
(Recipient). Application of the aforementioned ash is prohibi a except in 'acc&&n6l wic the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion. or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., Limited to
that needed. to meet the liming requirements of the crops being grown on the land).
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10"6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded; frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon. request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof.. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation an or atheir.use of
the ash.
Signed (Ash Recipient):
Ash Recipient's Address:
7- 3 o ---/ 9,.
Intended Use of Ash: `7r3 l r� - c t ,�.r, -t je-r ,P.t 71"
Ex ected /Yr: 5
p � ;�: 2
Page 1 of 3
Acres of Land: l %)
Updated: 3/5/10

Section 3 Lab Sheets
Sample 1-
1WBSP4813
February 8, 2013

ac"Anaoical
www.pacawbs.com
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 1WBSP4813 Lab ID: 92147495001 Collected: 02/08/13 11:45 Received: 02/08/13 13:00 Matrix: Solid
Results reported on a dry -weigh!" basis
Parameters Results Units Report Limit DF Prepared . Analyzed CAS No. Qua[
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
Barium
6.3 mg/kg
1.7 1
02/09/13 16:35 02/11/13 22:34
7440-38-2
Cadmium
1240 mg/kg
0.83 1
02/09/13 16:35 02/11/13 22:34
7440-39-3 `
Calcium
1.3 mg/kg
0.17 1
02/09/13 16:35 02/11/13 22:34
7440-43-9
Chromium
74700 mg/kg
166 10
02/09/13 16:35 02/12/1315:47
7440-70-2
Copper
18.7 mg/kg
0.83 1
02/09/13 16:35 02/11/13 22:34
7440-47-3
Iron
53.7 mg/kg
0.83 1
02/09/13 16:35 02/11/13 22:34
7440-50-8
Lead
10000 mg/kg
16.6 1
02/09/13 16:35 02/11/13 22:34
7439-89-6
Magnesium
18.7 mg/kg
0.83 1
02/09/13 16:35 02/11/13 22:34
7439-92-1
Manganese
10600 mg/kg
16.6 1
02/09/13 16:35 02/11/13 22:34
7439-95-4
2270 mg/kg
8.3 10
02/09/13 16:35 02/12/1315:47
7439-96-5
Molybdenum
ND mg/kg
0.83 1
02/09/13 16:35 02/11/13 22:34
7439-98-7
Nickel
Potassium
15.0 mg/kg
0.83 1
02109/1316:35 02/11/13 22:34
7440-02-0
14000 mg/kg
829 1
02/09/13 16:35 02/11/13 22:34
7440-09-7
Selenium
ND mg/kg
1.7 1
02/09/1316:35 02/11/13 22:34
7782-49-2
Silver
ND mg/kg
0.83 1
02/09/13 16:35 02/11/13 22:34
7440-22-4
Sodium
2180 mg/kg
829 1
02/09/13 16:35 02/11113 22:34
7440-23-5
Zinc
143 mg/kg
1.7 1
02/09/13 16:35 02/11/13 22:34
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 02/11/13 22:30
Arsenic
ND mg/L
0.050 1
02/12/1317:50 02/14/13 15:21
7440-38-2
Barium
9.4 mg/L
0.25 1
02/1211317:50 02/14/13 15:21
7440-39-3
Cadmium
0.022 mg/L
0.0050 1
02/12/13 17:50 02/14/13 15:21
7440-43-9
Chromium
ND mg/L
0.025 1
02/1211317:50 02/14/13 15:21
7440-47-3
Lead
0.033 mg/L
0.025 1
02/12/1317:50 02/14/13 15:21
7439-92-1
Selenium
ND mg/L
0.10 1
02/1211317:50 02/14/13 15:21
7782-49-2
Silver
ND mg/L
0.025 1
02/12/13 17:50 02/14/13 15:21
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 02/11/13 22:30
Mercury
'ND ug/L
0.20 1
02/13/13 19:45 02/15/1316:11 7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
ND mg/kg
0.0075 1
02/18/13 11:35 02/18/13 14:55 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
40.9 %
0.10 1
02/12/13 08:17
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
8.6 Std. Units
0.10- 1
02/14/1316:10
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus 2210 mg/kg 146 25 02/16/1313:01 7723-14-0
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 4 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc

Section 3 Lab Sheets
Sample 2 —
2WBSP4813
February 8, 2013

aceAnalytical
vnvw.pacetabs.aom
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
Sample: 2WBSP4813 Lab ID: 92147495002 Collected: 02/0811311:45 Received: 02/08/1313:00 atrix:
Results reported on a dry -weight" basis MSolid
Parameters Results Units Report Limit DF Prepared P Analyzed CAS No. Qual
6010 MET ICP Analytical M t
e hod. EPA 6010 Preparation Method: EPA 3050
Arsenic
Barium
8.0 mg/kg
1530 mg/kg
1.5 1
02/09/13 16:35 02/11/13 22:37 7440-38-2
Cadmium
1.mg/kg
0.77 1
02/09/13 16:35 02/11/13 22:37 7440-39-3
Calcium
82300 mg/kg
0.15 1
02/09/13 16:35 02/11/13 22:37 7440-43-9
Chromium
20.7 mg/kg
155 10
02/09/13 16:35 02/12/13 15:50 7440-70-2
Copper
7 68.mg/kg
0.77 1
02/09/1316:35 02/11/13 22:37 7440-47-3
Iron
11900m /k
g g
0.77 1
02/09/13 16:35 02/11/13 22:37 7440-50-8
Lead
20.4 mg/kg
15.5 1
02/09/13 16:35 02/11/13 22:37 7439-89-6
Magnesium
12200 mg/kg
0.77 1
02/09/13 16:35 02/11/13 22:37 7439-92-1
Manganese
2470 mg/kg
15.5 1
02/0911316:35 02/11/13 22:37 7439-95-4
Molybdenum
1.1 mg/kg
7.7 10
02/09/13 16:35 02/12/13 15:50 7439-96-5
Nickel
16.4 mg/kg
9 g
0.77 1
02/09/13 16:35 02/11/13 22:37 7439-98-7
Potassium
18900 mg/kg
0.77 1
02/09/13 16:35 02/11/13 22:37 7440-02-0
Selenium
ND m /k
9 g
7740 10
02/09/13 16:35 02/12/13 15:50 7440-09-7
Silver
ND mg/kg
1.5 1
02/09/13 16:35 02/11/13 22:37 7782-49-2
Sodium
2610 mg/kg
0.77 1
02/09/13 16:35 02/11/13 22:37 7440-22-4
Zinc
157 mg/kg
774 1
02/09/13 16:35 02/11/13 22:37 7440-23-5
6010 MET ICP, TCLP
1.5 1
02/09/1316:35 02/11/13 22:37 7440-66-6
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311;
02/13/13 23:50
Arsenic
Barium
ND m /L
g
9.2 mg/L
0.050 1
02/15/13 18:45 02/17/1319:11 7440-38-2
Cadmium
0.023 mg/L
0.25 1
02/15/13 18:45 02/17/13 19:11 7440-39-3
Chromium
ND mg/L
0.0050 1
02/15/13 18:45 02/17/1319:11 7440-43-9
Lead
ND mg/L
0.025 1
02/15/13 18:45 02/17/1319:11 7440-47-3
Selenium
ND mg/L
0.025 1
02/15/13 18:45 02/17/1319:11 7439-92-1
Silver
ND mg/L
0.10 1
02/15/13 18:45 02/17/1319:11 7782-49-2
7470 Mercury, TCLP
0.025 1
02/15/13 18:45 02/17/1319:11 7440-22-4
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 02/13/13 23:50
Mercury
7471 Mercury
ND ug/L
0.20 1
02/18/13 12:50 02/18/13 15:54 7439-97-6
Analytical Method: EPA 7471 Preparation Method: EPA
7471
Mercury
Percent Moisture
ND mg/kg
0.0044 1
02/18/13 11:35 02/18/13 14:58 7439-97-6
Analytical Method: ASTM D2974-87
Percent Moisture
48 7 %
9045 pH Soil
0.10 1
02/12/13 08:26
Analytical Method: EPA 9045
PH at 25 Degrees C
8.6 Sid. Units
0.10 1
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
02114/1316:10
Phosphorus
3010 mg/kg
60.9 10
02/16/13 13:05 7723-14-0
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS
Page 5 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Section 3 Lab Sheets
Quality Control Data for
IWBSP4813
2WBSP4813
February 8, 2013

aceAnalytical
www.pacelabacom
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
QC Batch: MERP/4915 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92147495001
METHOD BLANK: 921016 Matrix: Water
Associated Lab Samples: 9214749500,
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 02/15/1315:10
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 10o
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 921017
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.4 97 80-120
MATRIX SPIKE SAMPLE: 921018
92147344004 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Mercury ug/L ND 2.5 1.8 73 75-125 M1
SAMPLE DUPLICATE: 921019
92147404016 Dup
Parameter Units Result Result RPD Qualifiers
Mercury ug/L ND ND
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 6 of 20
This report shall not be reproduced, except in full,
Without the written consent of Pace Analytical Services, Inc..

aceAnalytfcal
www.pawabs.com
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP/4930 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92147495002
METHOD BLANK: 924026
Associated Lab Samples: 92147495002
Matrix: Water
Blank Reporting
Parameter Units Result Limit Analyzed yz Qualifiers
Mercury ug/L ND 0.20 02/18/1315:34
LABORATORY CONTROL SAMPLE: 924027
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury uglL 2.5 2.4 96 80.120
MATRIX SPIKE SAMPLE: 924029
92147495002 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits
Qualifiers
Mercury ug/L ND 2.5 3.1 123 75125
SAMPLE DUPLICATE: 924028
92147420022 Dup
Parameter Units Result Result RPD Qualifiers
Mercury ug/L ND ND
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS
Page 7 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

UWAINVical
www.pecolabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
QC Batch: MERP/4928 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92147495001, 92147495002
METHOD BLANK: 923347 Matrix: Solid
Associated Lab Samples: 92147495001. 92147495002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0050 02/18/1314:07
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 923348
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg .067 0.061 91 80-120
MATRIX SPIKE SAMPLE: 924068
92147290001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.11 .066 0.16 61 75-125 M1
SAMPLE DUPLICATE: 923350
92147275001 Dup
Parameter Units Result Result RPD Qualifiers
Mercury mg/kg 0.021 0.017 18
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 8 of 20
This report shall not be reproduced, except in full,
without the written consent of PaceAnalytical Services, Inc..

aceAnapical
j »tivxtP wwbS.tom
I
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Wood BoileAsh 2/8/13
Pace Project No.: 92147495
QC Batch: MPRP/12579
Analysis Method:
EPA 6010
QC Batch Method: EPA 3050
Analysis Description:
6010 MET
Associated Lab Samples: 92147495001, 92147495002
METHOD BLANK: 919629
Matrix: Solid
Associated Lab Samples: 92147495001, 92147495002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Arsenic
Barium
mg/kg
ND
1.0
02/11/13 21:44
Cadmium
mg/kg
mg/kg
ND
0.50
02/11/13 21:44
Calcium
mg/kg
ND
0.10
02/11/13 21:44
Chromium
mg/kg
ND
10.0
02/11/13 21:44
Copper
mg/kg
ND
0.50
02/11/13 21:44
Iron
ND
0.50
02/11/13 21:44
Lead
mg/kg
ND
10.0
02/11/13 21:44
Magnesium
mg/kg
mg/kg
ND
0.50
02/11/13 21:44
Manganese
mg/kg
ND
10.0
02/11/13 21:44
Molybdenum
mg/kg
ND
0.50
02/11/13 21:44 B
Nickel
mg/kg
ND
0.50
02/11/13 21:44
Potassium
mg/kg
ND
0.50
02/11/13 21:44
Selenium
mg/kg
ND
500
02/11/13 21:44 B
Silver
mg/kg
ND
1.0
02/11/13 21:44
Sodium
mg/kg
ND
0.50
02/11/13 21.44
Zinc
ND
500
02/11/13 21:44 B
mg/kg
ND
1.0
02/11/13 21:44
Pace Analytical Services, Inc.
98110 KinceyAve. Suite lo0
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
919630
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
47.0
94
80-120
Barium
Cadmium
mg/kg
50
47.3
95
80-120
Calcium
mg/kg
mg/kg
50
500
46.8
94
80-120
Chromium
mg/kg
50
485
48.2
97
96
80-120
Copper
mg/kg
50
46.4
93
80-120
80-120
Iron
Lead
mg/kg
500
474
95
80-120
Magnesium
mg/kg
mg/kg
50
500
47.3
95
80-120
Manganese
mg/kg
50
487
48.2
97
96
80-120
Molybdenum
mg/kg
50
48.3
97
80-120
80-120
Nickel
Potassium
mg/kg
50
48.0
96
80-120
Selenium
mg/kg
mg/kg
500
474J
95
80-120
Silver
mg/kg
50
25
47.5
23.7
95
80-120
Sodium
mg/kg
500
494J
95
99
80-120
80-120
Zinc
mglkg
50
49.2
98
80-120
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS
Page 9 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalyticai
www..pacolabs.com
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersvlle, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
919631
Units
92147541003
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
1.3
52.4
45.7
85
75-125
Barium
mg/kg
27.5
52.4
83.6
107
75-125
Cadmium
mg/kg
0.17
52.4
48.1
92
75-125
Calcium
mg/kg
948
524
1400
86
75-125
Chromium
mg/kg
7.4
52.4
60.9
102
75-125
Copper
m9fk9
5.9
52.4
54.8
93
75-125
Iron
mg/kg
6900
524
6920
5
75-125 M1
Lead
mg/kg
22.5
52.4
70.2
91
75-125
Magnesium
mg/kg
135
524
672
103
75-125
Manganese
mg/kg
26.7
52.4
74.9
92
75-128
Molybdenum
mg/kg
0.47J
52.4
47.0
89
75-125
Nickel
mg/kg
1.4
52.4
51.2
95
75-125
Potassium
mg/kg
166J
524
685
99
75-125
Selenium
mg/kg
ND
52.4
42.4
80
75-125
Silver
mg/kg
0.28J
26.2
24.5
92
75-125
Sodium
mg/kg
35.3J
524
552
99
75-125
Zinc
mg/kg
21.5
52A
79.6
111
75-125
SAMPLE DUPLICATE: 919632
92147541004
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Arsenic
mg/kg
2.7
3.6
28 D6
Barium
mg/kg
16.9
16.9
0
Cadmium
mg/kg
0.11
0.17
39 D6
Calcium
mg/kg
922
887
4
Chromium
mg/kg
18.6
18.5
1
Copper
mg/kg
3.7
4.2
13
Iron
mg/kg
11500
15600
30 D6
Lead
mg/kg
4.6
4.9
6
Magnesium
mg/kg
125
119
4
Manganese
mg/kg
0.62
,48J
Molybdenum
mg/kg
0.63
0.68
7
Nickel
mg/kg
0.90
0.85
6
Potassium
mg/kg
197J
1901
Selenium
mg/kg
0.64J
.76J
Silver
mg/kg
0.14J
.18J
Sodium
mg/kg
23.2J
25.6J
Zinc
mg/kg
1.7
1.7
1
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 10 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAinalytical
www.Pacobs.com
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
QC Batch: MPRP/12591
QC Batch Method: EPA 3010
Associated Lab Samples: 92147495001
METHOD BLANK: 920842
Associated Lab Samples: 92147495001
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
Matrix: Water
Blank
Parameter
Units
Result
Arsenic
mg/L
ND
Barium
mg/L
ND
Cadmium
mg/L
ND
Chromium
mg/L
ND
Lead
mg/L
ND
Selenium
mg/L
ND
Silver
mg/L
ND
LABORATORY CONTROL SAMPLE: 920843
Reporting
EPA 6010
6010 MET TCLP
Limit Analyzed Qualifiers
0.050
02/14/13 14:17
0.25
02/14/13 14:17
0.0050
02/14/13 14:17
0.025
02/14/13 14:17
0.025
02114/1314:17
0.10
02114/1314:17
0.025
02/14/13 14:17
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 1o0
Huntersville, NC 28078
[phone]
Parameter
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
Barium
mg/L
2.5
2.6
104
80-120
Cadmium
mg/L
mg/L
2.5
2.5
2.6
102
80A20
Chromium
mg/L
2.5
2.5
2.4
98
97
80-120
80-120
Lead
Selenium
mg/L
2.5
2.3
93
80-120
Silver
mg/L
2.5
2.5
100
80-120
mg/L
1.2
1.2
97
80-120
MATRIX SPIKE SAMPLE:
920846
Parameter
Units
92147344004
Result
Spike
Conc.
MS
MS
% Rec
Result
% Rec
Limits Qualifiers
Arsenic
Barium
mg/L
ND
2.5
2.8
110
75-125
Cadmium
mg/L
mg/L
ND
ND
2.5
2.7
106
75-125
Chromium
mg/L
ND
2.5
2.5
2.6
2.6
105
75-125
Lead
mg/L
ND
2.5
2.5
106
100
75-125
75-125
Selenium
Silver
mg/L
ND
2.5
2.7
107
75-125
mg/L
ND
1.2
1.3
105
75-125
SAMPLE DUPLICATE: 920847
92146632001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Arsenic
mg/L
ND
ND
Barium
mg/L
0.86
0.87 1
Cadmium
mg/L
ND
ND
Chromium
mg/L
ND
ND
Lead
mg/L
ND
ND
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 11 of 20
This report shall,not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnaIXical
wwwpecelabacom
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
SAMPLE DUPLICATE: 920847
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite 2226 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Parameter Units
Selenium mg/L
Silver mg/L
92146632001 Dup
Result Result
ND .024J
ND ND
RPD Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 12 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytiMl
www.pacafabs.com
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
QC Batch: MPRP/12623 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92147495002
METHOD BLANK: 923672
Associated Lab Samples: 92147495002
Matrix: Water
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
Barium
mg/L
ND
0.050
02117/1318:56
Cadmium
mg/L
mg/L
ND
0.25
02/17/1318:56
Chromium
mg/L
ND
0.0050
02/17/1318:56
Lead
ND
0.025
02/11/1318:56
Selenium
mg/L
mg/L
ND
0.025
02/17/1318:56
Silver
ND
0.10
02/17/1318:56
mg/L
ND
0.025
02/17/1318:56
LABORATORY CONTROL SAMPLE: 923673
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits. Qualifiers
Arsenic
mg/L
2.5
2.6
105
80-120
Barium
mg/L
2.5
2.3
94
80-120
Cadmium
mg/L
2.5
2.4
97
80-120
Chromium
mg/L
2.5
2.6
103
80-120
Lead
mg/L
2.5
2.3
92
80-120
Selenium
mg/L
2.5
2.6
104
80-120
Silver
mg/L
1.2
1.2
100
80-120
MATRIX SPIKE SAMPLE: 923690
[phone]
92147495002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc:
Result
% Rec
Limits Qualifiers
Arsenic
Barium
mg/L
ND
2.5
2.8
111
75-125
Cadmium
mg/L
mg/L
9.2
0.023
2.5
11.7
101
75-125
Chromium
mg/L
ND
2.5
2.5
2.6
101
75-125
Lead
mg/L
ND
2.5
2.7
2.5
107
75-125
Selenium
mg/L
ND
2.5
2.8
99
111
75-125
75-125
Silver
mg/L
ND
1.2
1.3
106
75-125
SAMPLE DUPLICATE: 923674
92147420022
Parameter
Units
Result
Arsenic
mg/L
ND
Barium
mg/L
0.083J
Cadmium
mg/L
0.0056
Chromium
mg/L
ND
Lead
mg/L
ND
Dup
Result RPD Qualifiers
.016J
.078J
.0048J
ND
ND
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 13 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
www.Pacabbs.com
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
SAMPLE DUPLICATE: 923674
Pace Analytical Services, Inc. Pace Analytical services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
92147420022 Dup
Parameter Units Result Result RPD Qualifiers
Selenium mg/L ND
ND
Silver mg/L 0.00181 .0012J
Pace Analytical Services, Inc.
9800 Kinceyme. Suite 1o0
Huntersville, NC 28078
[phone]
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 14 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

I
aceAnalytical
www.pecelabs.00m
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
QC Batch: PMST/5302
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92147495001
SAMPLE DUPLICATE: 919407
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry WeightlPercent Moisture
92147555001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 22.2 17.2 26 R1
0MJVIrLC UU1'LII:AI t: UI U43U
92147546001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 11.6 11.6 0
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PaceAnaiytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 20

aceAna�ytical e
www.pegelatrs.com
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
ctc: i3atcn: PMST/5303
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92147495002
SAMPLE DUPLICATE: 919412
Parameter
Percent Moisture
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight(Percent Moisture
92147557001 Dup
Units Result Result RPD Qualifiers
28.1 28.0 0
SAMPLE DUPLICATE: 919795
92147570002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 12.0 13.0 8
Pace Analytical Services, Inc.
9800 I(incey Ave. Suite 100
Huntersville, NC 28078
[phone]
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 16 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnaljftal
www.pacslabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
QC Batch: WET/24187 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92147495001, 92147495002
�riNirLt uurLIGATE: 922257
92146274005 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Sid. Units 5.8 5.8 1
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 20078
[phone]
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 17 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnal icai 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite =
www.pacatabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
1 [phone] [phone] [phone]
QUALITY CONTROL DATA
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
QC Batch: WETA/14517
Analysis Method:
EPA 365.1
QC Batch Method: EPA 365.1
Analysis Description:
365.1 Phosphorus, Total
Associated Lab Samples: 92147495001, 92147495002
METHOD BLANK: 922177
Matrix: Solid
Associated Lab Samples: 92147495001, 92147495002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Phosphorus
mg/kg
ND 2.0 02/16/1311:34
LABORATORY CONTROL SAMPLE:
922178
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Phosphorus
mg/kg
50 52.6
105
90-110
MATRIX SPIKE SAMPLE:
922180
92147051001 Spike
MS
MS % Rec
Parameter
Units
Result Conc.
Result
% Rec Limits Qualifiers
Phosphorus
mg/kg
8640 1650
10900
135 90-110 M1
SAMPLE DUPLICATE: 922179
92147051001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Phosphorus
mg/kg
8640 8040 7
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 18 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

ace Analjftal
j www.pawbbs.com
i
Project: Wood Boile Ash 2/8/13
Pace Project No.: 92147495
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
$G - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
[phone]
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 19 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

1�l5aceAnapicale
wmpmwbs.com
1
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2226 Riverside Dr.
Asheville, NC'28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Wood Boile Ash 218/13
Pace Project No.: 92147495
Pace Analytical Services, Inc.
9800KinceyAve. Suite100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92147495001
1WBSP4813
EPA3050
MPRP/12579
EPA 6010
ICP/11472
92147495002
2WBSP4813
EPA 3050
MPRP/12579
EPA 6010
ICP/11472
92147495001
1WBSP4813
EPA 3010
MPRP/12591
EPA 6010
ICP/11497
92147495002
2WBSP4813
EPA 3010
MPRP/12623
EPA 6010
ICP/11517
92147495001
1WBSP4813
EPA 7470
MERP/4915
EPA 7470
MERC/4791
92147495002
2WBSP4813
EPA 7470
MERP/4930
EPA 7470
MERC/4803
92147495001
1WBSP4813
EPA 7471
MERP/4928
EPA 7471
MERC/4802
92147495002
2WBSP4813,
EPA 7471
MERP/4928
EPA 7471
MERC/4802
92147495001
1WBSP4813
ASTM D2974-87
PMST/5302
92147495002
2WBSP4813
ASTM D2974-87
PMST/5303
92147495001
1 WBSP4813
EPA 9045
WET/24187
92147495002
2WBSP4813
EPA 9045
WET/24187
92147495001
1WBSP4813
EPA 365.1
WETA/14517
92147495002
2WBSP4813
EPA 365.1 l
WETA114517
Date: 02/19/2013 02:44 PM REPORT OF LABORATORY ANALYSIS Page 20 of 20
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Section 3 Lab Sheets
Sample 3 —
IWBSP4413
April 4, 2013

acaAMIJI cal
www.pacalabacom
Project: Wastewater Sampling
Pace Project No.: 92153516
Pace Analytical Services, Inc.
206 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 10o
Huntersville, NC 28078
[phone]
Sample: 1WSSP4413 Lab ID: 92163516001 Collected: 04/04/13 12:45 Received; 04/04/13 13:49 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
7.7 mg/kg
0.76
1
04/05/13 13:50 04/06/13 20:36 7440-38-2
Barium
661 mg/kg
0.38
1
04/05/13 13:50 04/06/13 20:36 7440-39-3
Cadmium,
0.79 mg/kg
0.076
1
04/05/13 13:50 04/06/13 20:36 7440-43-9
Calcium
44700 mg/kg
75.8
10
04/05/13 13:50 05/03/13 12:58 7440-70-2
Chromium
Copper
13.0 mg/kg
0.38
1
04/06/13 13:50 04/06/13 20:36 7440-47-3
50.7 mg/kg
0.38
1
04/05/13 13:50 04/06/13 20:36 7440-50-8
Iron
5350 mg/kg
7.6
1
04/05/13 13:50 04/06/13 20:36 7439-89-6
Lead
6.6 mg/kg
0.38
1
04/05/13 13:50 04/06/13 20:36 7439-92-1
Magnesium
5610 mg/kg
7.6
1
04/05/13 13:50 04/06/13 20:36 7439-95-4
Manganese
1140 mg/kg
1.9
5
04/05/13 13:50 04/07/13 13:45 7439-96-5
Molybdenum
0.38 mg/kg
0.38
1
04/05/13 13:50 04/06/13 20`:36 7439-98-7
Nickel
7.3 mg/kg
0.38
1
04/05/13 13:50 04/06/13 20:36 7440-02-0
Potassium
14500 mg/kg
1890
5
04/05/13 13:50 04/07/13 13:45 7440-09-7
Selenium
ND mg/kg
0.76
1
04/05/13 13:50 04/06/13 20:36 7782-49-2
Silver
0.52 mg/kg
0.38
1
04/05/13 13:50 04/06/13 20:36 7440-22-4
Sodium
3380 mg/kg
379
1
04/05/13 13:50 04/06/13 20:36 7440-237.5
Zinc
84.5 mg/kg
0.76
1
04/05/13 13:50 04/06/13 20:36 7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010
Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 04/08/13 23`:50
Arsenic
0.081 mg/L
0.050
1
04/09/13 22:30 04/10/13 18:11 7440-38-2
Barium
2.5 mg/L
0.25
1
04/09/13 22:30 04/10/13 18:11 7440-39-3
Cadmium
0.023 mg/L
0.0050
1
04/09/13 22:30 04/10/13 18:11 7440-43-9
Chromium
0.13 mg/L
0.025
1
04/09/13 22:30 04/10/13 18:11 7440-47-3
Lead
0.063 mg/L
0.025
1
04/09/13 22:30 04/10/13 18:11 7439-92-1
Selenium
ND mg/L
0.10
1
04/09/13 22:30 04/10/13 18:11 7782-49-2
Silver
ND mg/L
0.025
1
04/09/13 22:30 04/10/13 18:11 7440-22-4
7470 Mercury, TCLP
Mercury
7471 Mercury
Mercury
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
Date: 09/12/2013 03:44 PM
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 04/08/13 23:50
ND ug/L 0.20 1 04110/1311:05 04/11/1311:19 7439-97-6
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg 0.0037 1 04/05/1316:00 04/11/1312:44 7439-97-6
Analytical Method: EPA 9045
8.4 Std. Units 0.10 1 04/11/13 14:00
Analytical Method: EPA 365.1
1380 mg/kg 69.4 25 04/12/13 10:16 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PaceAnalytical Services, Inc..
Page 4 of 19

Section 3 Lab Sheets
Sample 4 —
2WBSP44-13
April 4, 2-013

acuMnalytical
www.paca/abs.00m
Project: Wastewater Sampling
Pace Project No.: 92153516
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
sample: 2WBSP4413 Lab ID: 92153516002
Results reported on a "wet -weight" basis
Parameters Results Units
Collected: 04/04/13 12:45
ReportLimit : DF
Received: 04/04/13 13:49 Matrix: Solid
Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010
Preparation Method: EPA 3050
Arsenic
9.4 mg/kg
0.78
1
04/10/13 17:35 04/11/13 18:38
7440-38-2
Barium
604 mg/kg
0.39
1
04/10/13 17:35 04/11/13 18:38
7440-39-3
Cadmium
0.82 mg/kg
0.078
1
04/10/13 17:35 04/11/13 18:38
7440-43-9
Calcium
42600 mg/kg
78.1
10
04/10/13 17:35 04/12/13 12:04
7440-70-2
Chromium
13.2 mg/kg
0.39
1
04/10/13 17:35 04/11/13 18:38
7440-47-3
Copper
45.8 mg/kg
0.39
1
04/10/13 17:35 04/11/13 18:38
7440-50-8
Iron
4780 mg/kg
7.8
1
04/10/13 17:35 04/11/13 18:38
7439-89-6
Lead
7.0 mg/kg
0.39
1
04/10/13 17:35 04/11/13 18:38
7439-92-1
Magnesium
5450 mg/kg
7.8
1
04/10/13 17:35 04/11/13 18:38
7439-95-4
Manganese
1200 mg/kg
3.9
10
04/10/13 17:35 04/12/13 12:04
7439-96-5
Molybdenum
ND mg/kg
0.39
1
04/10/13 17:35 04/11/13 18:38
7439-98-7
Nickel
7.4 mg/kg
0.39
1
04/10/13 17:35 04/11/13 18:38
7440-02-0
Potassium
11600 mg/kg
3910
10
04/10/13 17:35 04/12/13 12:04
7440-09-7
Selenium
ND mg/kg
0.78
' 1
04/10/13 17:35 04/11/13 18:38
7782-49-2
Silver
0.43 mg/kg
0.39
1
04/10/13 17:35 04/11/13 18:38
7440-22-4
Sodium
2730 mg/kg
391
1
04/10/13 17:35 04/11/13 18:38
7440-23-5
Zinc
95.8 mg/kg
0.78
1
04/10/13 17:35 04/11/13 18:38
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 04/08/13 23:50
Arsenic
0.069 mg/L 0.050 1
04/09/13 22:30
04/10/13 18:14
7440-38-2
Barium
2.6 mg/L 0.25 1
04/09/13 22:30
04/10/13 18:14
7440-39-3
Cadmium
0.024 mg/L 0.0050 1
04/09/13 22:30
04/10/13 18:14
7440-43-9
Chromium
0.13 mg/L 0.025 1
04/09/13 22:30
04/10/13 18:14
7440-47-3
Lead
0.070 mg/L 0.025 1
04/09/13 22:30
04/10/13 18:14
7439-92-1
Selenium
ND mg/L 0.10 1
04/09/13 22:30
04/10/13 18:14
7782-49-2
Silver
ND mg/L 0.025 1
04/09/13 22:30
04/10/13 18:14
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 04/08/13 23:50
Mercury
ND ug/L 0.20 1
04/10/13 11:05
04/11/1311:22
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
ND mg/kg 0.0034 1
04/05/1316:00
04/11/1312:49
7439-97-6
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
8.6 Std. Units 0.10 1
04/11/13 14:00
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
1400 mg/kg 64.1 25
04/12/13 10:20
7723-14-0
Date: 09/12/2013 03:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 19

Section 3 Lab Sheets
Quality Control Data for
IWBSP4413
2WBSP44-13
April 4, 2013

aceAnalytical
wew.Pecelebs.00m
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kinoey Ave. Suite 10o
Huntersville, NC 28078
[phone]
Project: Wastewater Sampling
Pace Project No.: 92153516
QC Batch: MERP/5075
Analysis Method:
EPA 7470
QC Batch Method: EPA 7470
Analysis Description:
7470 Mercury TCLP
Associated Lab Samples: 92153516001, 92153516002
METHOD BLANK: 953479
Matrix: Water
Associated Lab Samples: 92153516001, 92153516002
Blank Reporting
Parameter Units
Result Limit.
Analyzed Qualifiers
Mercury ug/L
ND 0.20 04/10/1315:49
LABORATORY CONTROL SAMPLE: 953480
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury ug/L
2.5 2.5
100 80-120
MATRIX SPIKE SAMPLE: 953481
92153075001 Spike
MS MS % Rec
Parameter Units
Result Conc.
Result % Rec Limits Qualifiers
Mercury ug/L
ND 2.5
2.5 99 75-125
SAMPLE DUPLICATE: 953618
92153677001 Dup
Parameter Units
Result Result
RPD Qualifiers
Mercury ug/L
ND ND
Date: 09/12/2013 03:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 19

iaceAnaiytical
www.pacalabs.com
Project: Wastewater Sampling
Pace Project No.: 92153516
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP/5073 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92153516001, 92153516002
METHOD BLANK: 951524 Matrix: Solid
Associated Lab Samples: 92153516001, 92153516002
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0:0050 04/11/1311:41
LABORATORY CONTROL SAMPLE: 951525
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg .067 0:063 94 80-120
MATRIX SPIKE SAMPLE: 951526
92153065001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.0052 .086 0.064 68 75-125 J(MI)
SAMPLE DUPLICATE: 951527
92153516001 Dup
Parameter Units Result Result RPD Qualifiers
Mercury mg/kg ND _00321
Date: 09/12/2013 03:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 19

aceAnalj cal
W m:Pacabbs com
Project: Wastewater Sampling
Pace Project No.: 92153516
QC Batch: MPRP/12996
QC Batch Method: EPA 3050
Associated Lab Samples: 92153516001
Pace Analytical Services, Inca
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 6010
Analysis Description: 6010 MET
METHOD BLANK: 951575
Associated Lab Samples:
Parameter
92153516001
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed
Arsenic
mg/kg
ND
1.0
' 04/0611318:42
Barium
mg/kg
ND
0.50
04/06/1318:42
Cadmium
mg/kg
ND
0.10
04/0611318:42
Calcium
mg/kg
ND
10.0
04/06/1318:42
Chromium
mg/kg
ND
0.50
04/06/1318:42
Copper
mg/kg
ND
0.50
04/06/1318:42
Lead'
mg/kg
ND
0.50
04/06/1318:42
Magnesium
mg/kg
ND
10.0
04/06/1318:42
Molybdenum
mg/kg
ND
0.50
04/06/1318:42
Nickel
mg/kg
ND
0.50
04/06/1318:42
Potassium
mg/kg
ND
500
04/06/1318:42
Selenium
mg/kg
ND
1.0
04/06/1318:42
Silver
mg/kg
ND
0.50
04/06/1318:42
Sodium
mg/kg
ND
500
04/06/1318:42
Zinc
mg/kg
ND
1.0
04106/1318:42
LABORATORY CONTROL SAMPLE: 951576
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
15
14.5
97
80-120
Barium
mg/kg
15
15.4
103
80-120
Cadmium
mg/kg
15
14.9
99
80-120
Calcium
mg/kg
150
153
102
80-120
Chromium
mg/kg
15
15.1
101
80-120
Copper
mg/kg
15
14.6
97
80-120
Lead
mg/kg
15
15.1
101
80-120
Magnesium
mg/kg
150
154
103
80-120
Molybdenum
mg/kg
15
15:3
102
80-120
Nickel
mg/kg
15
15.2
101
80-120
Potassium
mg/kg
150
1381
92
80-120
Selenium
mg/kg
15
14.5
97
80-120
Silver
mg/kg
7.5
7.4
99
80-120
Sodium
mg/kg
150
1481
98
80-120
Zinc
mg/kg
15
15.0
100
80-120
MATRIX SPIKE SAMPLE: 951577
Parameter
Arsenic
Barium
Date: 09/12/2013 03:44 PM
92153065001 Spike MS
Units Result Conc. Result
mg/kg 2.1 16.1 16.0
mg/kg 72.3 16.1 78.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
MS % Rec
% Rec Limits Qualifiers
86 75-125
40 75-125 J(M1)
Page 8 of 19

aceAnalytical
www-peso com
Project: Wastewater Sampling
Pace Project No.: 92153616
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinoeyAve. Suite 100
Huntersville, NC 28078
[phone]
MAIKIA srltct SAMVLE:
Parameter
951577
Units
92153065001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Cadmium
mg/kg
ND
16.1
15.1
93
75-125
Calcium
mg/kg
2380
161
2280
-62
75-125 J(M1)
Chromium
mg/kg
7.5
16.1
22.4
93
75-125
Copper
mg/kg
34.6
16.1
45.4
68
75-125 J(M1)
Lead
mg/kg
11.7
16.1
25.9
88
75-125
Magnesium
mg/kg
682
161
821
86
75-125
Molybdenum
mg/kg
2.0
16.1
16.4
89
75-125
Nickel
mg/kg
8.3.
16.1
21:3
81
75-125
Potassium
mg/kg
ND
161
691
148
75-125 J(M1)
Selenium
mg/kg
ND
16.1
15.0
90
75-125
Silver
mg/kg
ND
8
7.7
96
75-125
Sodium
mg/kg
ND
161
2641
114
75-125
Zinc
mg/kg
168
16.1
197
175
75-125 J(M1)
aHMrLt uut'LIGAI t: 951578
Parameter
Units
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Date: 09/12/2013 03:44 PM
92153261001 Dup
Result
Result
RPD Qualifiers
ND
ND
239
292
20
1.8
6.2
110 J(D6)
84.4
103
20
25.0
50.7
68 J(D6)
28.4
71.0
86 J(D6)
7.0
8.5
18
5390
6760
23 J(D6)
0.141
0.72
17.0
18.8
10
10300
13400
27 J(D6)
1.3
1 I
0.141
.231
3051
4911
140
193
32 J(D6)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 19

aceAnalytical
WWWPecelab&com
Project: Wastewater Sampling
Pace Project No.: 92153516
Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
wt., vaicn: MPRP/13030
QC Batch Method: EPA 3050
Associated Lab Samples: 92153516002
Analysis Method:
Analysis Description:
EPA 6010
6010 MET
METHOD BLANK: 954009
Matrix: Solid
Associated Lab Samples:
92153516002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Arsenic
mg/kg
ND
1.0
04/11/1317:29
Barium
mg/kg
ND
0.50
04/11/1317:29
Cadmium
mg/kg
ND
0.10
04/11/1317:29
Chromium
mg/kg
ND
0.50
04/11/1317:29
Copper
mg/kg
ND
0.50
04/11/1317:29
Iron
mg/kg
ND
10.0
04/11/1317:29
Lead
mg/kg
ND
0.50
04/11/1317:29
Magnesium
mg/kg
ND
10.0
04/11/1317:29
Manganese
mg/kg
ND
0.50
04/11/1317:29
Molybdenum
mg/kg
ND
0.50
04/1111317:29
Nickel
mg/kg
ND
0.50
04/11/1317:29
Potassium
mg/kg.
ND
500
04/11/1317:29
Selenium
mg/kg
ND
1.0
04/11/1317:29
Silver
mg/kg
ND
0.50
04/11/1317:29
Sodium
mg/kg
ND
500
04/11/1317:29
Zinc
mg/kg
ND
1.0
04/11/1317:29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LACVKAI UK (;UN I KUL SAMPLE:
Parameter
954010
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
49.0
98
80-120
Barium
mg/kg
50
47.7
95
80-120
Cadmium
mg/kg
50
49.4
99
80-120
Chromium
mg/kg
50
48.9
98
80-120
Copper
mg/kg.
50
47.1
94
80-120
Iron
mg/kg
500
499
100
80-120
Lead
mg/kg
50
49.7
99
80-120
Magnesium
mg/kg
500
507
101
80-120
Manganese
mg/kg
50
49.4
99
80-120
Molybdenum
mg/kg
50
50.4
101
80-120
Nickel
mg/kg
50
50.6
101
80-120
Potassium
mg/kg
500
4661
93
80-120
Selenium
mg/kg .
50
49.1
98
80-120
Silver
mg/kg
25
24.9
100
80-120
Sodium
mg/kg
500
4831
97
80-120
Zinc
mg/kg
50
50.0
100
80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/12/2013 03:44 PM without the written consent of Pace AnalyticalServices, Inc.. Page 10 of 19

_ aceAnalytical
www.pec0ftcom
Project: Wastewater Sampling
Pace Project No.: 92153516
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
954011
Units
92153620003
Result
Spike
Conc.
MS MS
Result % Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
7.9
54.5
66.7
108
75-125
Barium
mg/kg
46.6
54.5
89.9
80
75-125
Cadmium
mg/kg
0.89
54.5
46.6
84
75-125
Chromium
mg/kg
6.9
54.5
55.5
89
75-1.25
Copper
mg/kg
14.9
54.5
74.9
110
75-125
Iron
mg/kg
8530
545
9630
201
75-125 J(M1)
Lead
mg/kg
7.3
54.5
55.3
88
75-125
Magnesium
mg/kg
44000
545
25200 -3459
75-125 J(M1)
Manganese
mg/kg
421
54.5
372
-90
75-125 J(M1)
Molybdenum
mg/kg
2.4
54.5
51.8
91
75-125
Nickel
mg/kg
12.3
54.5
58.3
85
75-125
Potassium
mg/kg
1160
545
2410
230
75-125 J(M1)
Selenium
mg/kg
ND
54.5
51.8
95
75-125
Silver
mg/kg
ND
27.2
30.9
113
75-125
Sodium
mg/kg
ND
545
1230
173
75-125 J(M1)
Zinc
mg/kg
42.2
54.5
102
111
75-125
SAMPLE DUPLICATE: 954012
92153620004
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Arsenic
mg/kg
5.5
8.4
40 J(D6)
Barium
mg/kg
54.0
48.0
12
Cadmium
mg/kg
0.68
0.52
27 J(D6)
Chromium
mg/kg
9.6
9.3
3
Copper
mg/kg
15.0
15.6
4
Iron
mg/kg
9770
10800
10
Lead
mg/kg
12.4
9.5
26 J(D6)
Magnesium
mg/kg
9270
11700
23 J(D6)
Manganese
mg/kg
320
311
3
Molybdenum
mg/kg
1.6
2.5
43 J(D6)
Nickel
mg/kg
12.3
13.2
7
Potassium
mg/kg
752
732
3
Selenium
mg/kg
ND
ND
Silver
mg/kg
ND
ND
Sodium
mg/kg
ND
961
Zinc
mg/kg
50.8
48.6
4
Date: 09/12/2013 03:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 19

aceA1781JI iCal
www.pscfefucom
Project: Wastewater Sampling
Pace Project No.: 92153516
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
wU vaicn: MPRP/13021 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92153516001, 92153516002
ivit i r1Uv CLANK: 953354 Matrix: Water
Associated Lab Samples: 92153516001, 92153516002
Blank
Parameter
Units
Result
Arsenic
mg/L
ND
Barium
mg/L
ND
Cadmium
mg/L
ND
Chromium
mg/L
ND
Lead
mg/L
ND
Selenium
mg/L
ND
Silver
mg/L
ND
LABORATORY CONTROL SAMPLE:
953355
Spike
Parameter
Units
Conc.
Arsenic
mg/L
2.5
Barium
mg/L
2.5
Cadmium
mg/L
2.5
Chromium
mg/L
2.5
Lead
mg/L
2.5
Selenium
mg/L
2.5
Silver
mg/L
1.2
Reporting
Limit Analyzed Qualifiers
0.050
04/10/1317:05
0.26
04/10/1317:05
0.0050
04/10/1317:05
0.025
04/10/1317:05
0.025
04110/1317:05
0.10
04/10/1317:05
0.025
04/10/1317:05
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LCS
LCS
% Rec
Result
% Rec
Limits Qualifiers
2.5
99
80-120
2.5
99
80-120
2.4
96
80-120
2.4
98
80-120
2.3
91
80-120
2.5
99
80-120
1.2
97
80-120
MATRIX SPIKE SAMPLE:
Parameter
953356
Units
92153075001
Result .
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/L
ND
2.5
2.5
101
75-125
Barium
mg/L
0.60
2.5
3.0
96
75-125
Cadmium
mg/L
0.021
2.5
2.5
98
75-125
Chromium
mg/L
ND
2.5
2.5
98
75-125
Lead
mg/L
0.081
2.5
2.4
91
75-125
Selenium
mg/L
ND
2.5
2.5-
99
75-125
Silver
mg/L
ND
1.2
1.2
98
15-125
SAMPLE DUPLICATE: 953357
92153521001
Dup
Parameter
Units.
Result
Result
RPD
Qualifiers
Arsenic
mg/L
ND
ND
Barium
mg/L
ND
.0721
Cadmium
mg/L
ND
ND
Chromium
mg/L
ND
ND
Lead
mg/L
ND
ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/12/2013 03:44 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 19

acmnalytical
WmPacalabs.com
Project: Wastewater Sampling
Pace Project No.: 92153516
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
SAMPLE DUPLICATE: 953357
92153521001 Dup
Parameter Units Result Result RPD Qualifiers
Selenium mg/L ND ND
Silver mg/L ND .00331
Date: 09/12/2013 03:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kinoey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 19

aceAnalytical
ampacelabaoxn
Project: Wastewater Sampling
Pace Project No.: 92153516
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WET/24918 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92153516001, 92153516002
SAMPLE DUPLICATE: 954431
92152947001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 7.3 7.4 0
Date: 09/12/2013 03:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page.14 of 19

aceAnalyiical
www.pecelabscem
I
Project: Wastewater Sampling
Pace Project No.: 92153516
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2226 Riverside Dr.
Asheville, NC 28804
[phone]
(QUALITY CONTROL DATA
ut; batcn: WETA/14966 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92153516001, 92153516002
Pace Analytical Services, Inc.
9800IGnceyAve. Suite too
Huntersville, NC 28078
[phone]
iwt= i rlUU tsLANK: ybZt33Z Matrix: Solid
Associated Lab Samples: 92153516001, 92153516002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 2.0 04/12/13 09:47
LABORATORY CONTROL SAMPLE: 952633
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 50 51.4 103 90-110
MAI KIA SPIKE SAMPLE: 952634
92153547001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 135 208 346 _ 101 90-110
SAMPLE DUPLICATE: 952635
Parameter
Phosphorus
Date: 09/12/2013 03:44 PM
92153516001 Dup
Units Result Result RPD Qualifiers
mg/kg 1380 1370 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 19

_ aceAnalytical
www.peoslaftwM
Project: Wastewater Sampling
Pace Project No.: 92153516
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
ANALYTE QUALIFIERS
I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
J(D6) Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory
control limits.
J(M1) Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS)
recovery.
REPORT OF LABORATORY ANALYSIS
[phone]
This report shall not be reproduced, except in full,
Date: 09/12/2013 03:44 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 19

aceAnalytical
WWW.p=dabs.c=
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Wastewater Sampling
Pace Project No.: 92153516
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92153516001
1WBSP4413
EPA3050
MPRP/12996
EPA 6010
ICP/11838
92163516002
2WBSP4413
EPA 3050
MPRP/13030
EPA 6010
ICP/11869
92163516001
1 WBSP4413
EPA 3010
MPRP/13021
EPA 6010
ICP/11858
92153516002
2WBSP4413
EPA 3010
MPRP/13021
EPA 6010
ICP/11858
92153616001
1 WBSP4413
EPA 7470
MERP/5075
EPA 7470
MERC/4937
92153516002
2WBSP4413
EPA 7470
MERP/5075
EPA 7470
MERC/4937
92153516001
1 WBSP4413
EPA 7471
MERP/5073
EPA 7471
MERC/4935
92153516002
2WBSP4413
EPA 7471
MERP/5073
EPA 7471
MERC/4935
92153516001
1 WBSP4413
EPA 9045
WET/24918
92153516002
2WBSP4413
EPA 9045
WET124918
92153516001
1 WBSP4413
EPA 365.1
WETA114966
92153516002
2WBSP4413
EPA 365.1
WETA114966
Date: 09/12/2013 03:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full;
without the written consent of Pace Analytical Services, Inc..
Page 17 of 19

Section 3 Lab Sheets
Sample 5 —
SP82313 ASH
August 231 2013

5alclAnalytical
www.pacalabs.cam
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9600 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP82313 ASH Lab ID: 92169897001 Collected: 08/23/13 12:35 Received: 08/23/13 14:07 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
9.1 mg/kg
1.8 1
08/24/13 14:30 08/25/13 17:13 7440-38-2
Barium
1300 mg/kg
0.91 1
08/24/13 14:30 08/25/13 17:13 7440-39-3
Cadmium
1.9 mg/kg
0.18 1
08/2411314:30 08/25/13 17:13 7440-43-9
Calcium
84200 mg/kg
182 10
08/24/13 14:30 08/26/13 14:59 7440-70-2
Chromium
26.4 mg/kg
0.91 1
08/24/13 14:30 08/26/13 17:13 7440-47-3
Copper.
75.0 mg/kg
0.91 1
08/24/13 14:30 08/25/13 17:13 7440-50-8
Iron
10700 mg/kg
18.2 1
08/24/13 14:30 08/25/13 17:13 7439-89-6
Lead
22.6 mg/kg
0.91 1
08/24/13 14:30 08/25/13 17:13 7439-92-1
Magnesium
12900 mg/kg
18.2 1
08/24/13 14:30 08/25/13 17:13 7439-95-4
Manganese
2670 mg/kg
9.1 10
08/24/13 14:30 08/26/13 14:59 7439-96-5
Molybdenum
1.6 mg/kg
0.91 1
08/24/13 14:30 08/25/13 17:13 7439-98-7
Nickel
20.6 mg/kg
0.91 1
08/24/13 14:30 08/25/1317:13 7440-02-0
Potassium
21600 mg/kg
9100 10
08/24/13 14:30 08/26/13 14:59 7440-09-7
Selenium
ND mg/kg
1.8 1
08/24/13 14:30 08/25/13 17:13 7782-49-2
Silver
0.93 mg/kg
0.91 1
08/24/13 14:30 08/25/13 17:13 7440-22-4
Sodium
6040 mg/kg
910 1
08/24/13 14:30 08/26/13 14:41 7440-23-5
Zinc
197 mg/kg
1.8 1
08/24/13 14:30 08/25/13 17:13 7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 08/28/13 16:55
Arsenic
ND mg/L
0.050 1
08/2911314:25 08/30/1313:54 7440-38-2
Barium
3.6 mg/L
0.25 1
08/29/13 14:25 08/30/13 13:54 7440-39-3
Cadmium
ND mg/L
0.0050 1
08/29/13 14:25 08/30/1313:54 7440-43-9
Chromium
ND mg/L
0.025 1
08/29/13 14:25 08/30/1313:54 7440-47-3
Lead
ND mg/L
0.025 1
08/29/13 14:25 08/30/1313:54 7439-92-1
Selenium
ND mg/L
0.10 1
08/29/13 14:25 08/30/1313:54 7782-49-2
Silver -
ND mg/L
0.025 1
08/29/13 14:25 08/30/1313:54 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 08/28/13 16:55
Mercury
ND ug/L
0.20 1
08/29/13 17:15 08/30/13 12:08 7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
ND mg/kg
0.0057 1
08/30/13 17:55 09/04/13 12:07 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
49.2 %
0.10 1
09/03/13 08:48
9045 pH Soil Analytical Method: EPA 9045
pH at 25 Degrees C 9.1 Std. Units 0.10 1 08/27/1311:35
365.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus 3070 mg/kg 151 50 08/30/13 16:49 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/12/2013 12:32 PM without the written consent of Pace Analytical Services; Inc.. Page 4 of 16

Section 3 Lab Sheets
Quality Control Data for
SP82313 ASH
August 23, 2013

1�;'alceftlyficafm
r www.pacelabs.com
1
1
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville. NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP/5536 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92169897001
METHOD BLANK: 1038327 Matrix: Water
Associated Lab Samples: 92169897001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND '0.20 08130/1311:18
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1038328
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.4 94 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1038329 1038330
MS MSD
92168869001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.3 2.2 90 89 75-125 2
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,
Page 5 of 16

aceAnalj*al
www.pacelabs.com
i
/
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP/5541 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92169897001
METHOD BLANK: 1039489 Matrix: Solid
Associated Lab Samples: 92169897001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0050 09/04/1311:41
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1039490
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg .067 0.055 82 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1039491 1039492
MS MSD
92169384001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.52 .05 .05 0.49 0.58 -51 129 75-125 17 M6
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 16

acoAnaljltical
www.pacelabacom
i
Project: WOOD BOILER ASH
Pace Project No.: 92169897.
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC'28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/14056 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 92169897001
METHOD BLANK: 1035357 Matrix: Solid
Associated Lab Samples: 92169897001
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed
Arsenic
mg/kg
ND
1.0
08/25/1316:17
Barium
mg/kg
ND
0.50
08/25/1316:17
Cadmium
mg/kg
ND
0.10
08/25/1316:17
Calcium
mglkg
ND
10.0
08/25/1316:17
Chromium
mg/kg .
ND
0.50
08/25/1316:17
Copper
mg/kg
ND
0.50
08/25/1316:17
Iron
mg/kg
ND
10.0
0812511316:17
Lead
mg/kg
ND
0.50
08125113.16:17
Magnesium
mg/kg
ND
10.0
08/25/1316:17
Manganese
mg/kg
ND
0.50
08/25/1316:17
Molybdenum
mg/kg
ND
0.50
08/25/1316:17
Nickel
mg/kg
ND
0.50
08/2511816:17
Potassium
mg/kg
ND
500
08/25/1316:17
Selenium
mg/kg
ND
1.0
08/2511316:17
Silver
mg/kg
ND
0.50
08/25/1316:17
Sodium
mg/kg
ND
500
08/25/1316:17
Zinc
mg/kg
ND
1.0
08/25/1316:17
LABORATORY CONTROL SAMPLE: 1035358
Parameter Units
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Iron
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Manganese
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Date: 09/12/201312:32 PM
Qualifiers
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
50
46.0
92
80-120
50
46.3
93
80-120
50
47.4
95
80-120 .
500
486
97
80-120
50
47.9
96
80-120
50
44.8
90
80-120
500
471
94
80-120
50
47.2
94
80-120
500
478
96
80-120
50
47.3
95
80-120
50
47.7
95
80-120
50
, 48.0
96
80-120
500
451J
90
80-120
50
46.7
93
80-120
25
23.5
94
80-120
500
444J
89
80-120
50
47.6
95
80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 16

1 /158ceAnalj&cNE'
www.pacelaft com
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services; Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1035359
MS
92168447001 Spike
Parameter Units Result Cone.
MSD
Spike
Cone.
1035360
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
ND
48.1
45.5
43.3
42.1
90
93
75-125
3
Barium
mg/kg
1.1
48A
45.5
44.3
43.1
90
92
75-125
3
Cadmium
mg/kg
ND
48.1
45.5
43.8
42.4
91
93
75-125
3
Calcium
mg/kg
25.3
481
455
470
461
93
96
75-125
2
Chromium
mg/kg
ND
48.1
45.5
44.3
43.2
92
95
75-125
3
Copper
mg/kg
1.7
48.1
45.5
44.1
43.0
88
91
75-125
3
Iron
mg/kg
5330
481
455
5540
5570
42
53
75-125
1 M1
Lead
mg/kg
ND
48.1
45.5
42.8
41.5
88
90
75-125
3
Magnesium
mg/kg
ND
481
455
439
427
90
93
75-125
3
Manganese
mg/kg
15.6
48.1
45.5
59.1
58.4
91
94
75-125
1
Molybdenum
mg/kg
ND
48.1
45.5
43.8
43.0
91
94
75-125
2
Nickel
mg/kg
NO
48.1
45.5
44.6
43.4
92'
95
75-125
3
Potassium
mg/kg
ND
481
455
452J
440J
93
95
75-125
Selenium
mg/kg
ND
48.1
45.5
44.6
43.0
92
94
75-125
4
Silver
mg/kg
NO
24
22.7
22.1
21.5
92
95
75-125
3
Sodium
mg/kg
ND
481
455
445J
434J
85
87
75-125
Zinc
mg/kg
NO
48.1
45.5
45.4
44.4
93
96
75-125
2
Date: 09/121201312:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 16

aceAnalytical
f/ mv.pacelabs.com
t
Project: WOOD BOILER ASH
Pace Project No.: 92169897
QC Batch: MPRP/14085
QC Batch Method: EPA 3010
Associated Lab Samples: 92169897001
METHOD BLANK: 1038184
Associated Lab Samples: 92169897001
Parameter Units
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
LABORATORY CONTROL SAMPLE:
Parameter
1038185
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 6010
Analysis Description: 6010 MET TCLP
Matrix: Water
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Blank
Reporting
Result
Limit
Analyzed
Qualifiers
ND
0.050
08/3011312:43
ND
0.25
08/30/1312:43
ND
0.0050
08/3011312:43
ND
0.025
08/30/1312:43
ND
0.025
08/30/1312:43
ND
0.10
08/30/1312:43
ND
0.025
08130/1312:43
Spike
LCS
LCS % Rec
Conc.
Result % Rec Limits Qualifiers
2.5
2.7
107
80-120
2.5
2.4
96
80-120
2.5
2.3
94
80-120
2.5
2.4
96
80-120
2.5
2.2
90
80-120
2.5
2.8
112
80-120
1.2
1.3
103
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1038186
1038187
MS
MSD
92168869001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
Arsenic
mg/L
ND
2.5
2.5
2.7
2.8
109
111
75-125
2
Barium
mg/L
ND
2.5
2.5
2.5
2.5
98
99
75-125
1
Cadmium
mg/L
ND
2.5
2.5
2.4
2.4
97
96
75-125
0
Chromium
mg/L
0.26
2.5
2.5
2.7
2.7
98
97
75-125
1
Lead
mg/L
NO
2.5
2.5
2.3
2.3
93
93
75-125
0
Selenium
mg/L
ND
2.5
2.5
2.8
2.8
111
112
75-125
1
Silver
mg/L
ND
1.2
1.2
1.3
1.3
106
106
75-125
0
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 16

aceftlytical
www.pacafabs.com
Project: WOOD BOILER ASH
Pace Project No.: 92/69897
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
QC Batch: PMST/5793
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92169897001
SAMPLE DUPLICATE: 1037730
Parameter Units
Percent Moisture %
SAMPLE DUPLICATE: 1037731
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92170134001 Dup
Result Result RPD Qualifiers
22.2 19.6 12
92170066006 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 6.9 6.3 9
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 16

aceAnaljftal
wwwpacelabs.com
i
r
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WET/26852 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92169897001
SAMPLE DUPLICATE: 1035948
Parameter
pH at 25 Degrees C
Date: 09/12/2013 12:32 PM
92169844001 Dup
Units Result Result RPD Qualifiers
Std. Units 10.2 10.6 4 D6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 16

11�;aceftlj cal
wmmpmJabs.com
�r
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QC Batch: WETA/16309
QC Batch Method: EPA 365.1
Associated Lab Samples: 92169897001
METHOD BLANK: 1038955
Associated Lab Samples: 92169897001
Parameter Units
Phosphorus mg/kg
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 08/30/1315:48
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1038956
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 50 49.5 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1038957 1038958
MS MSD
92169068001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 6580 3970 6650 4640 5200 -49 -21 90-110 11 M6
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 16

aceAnaljftal
r www.pacelabs.com
Project: WOOD BOILER ASH
Pace Project No.: 92169897
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside'Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but.not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
[phone]
This report shall not be reproduced, except in full,
Date: 09/12/2013 12:32 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 16

acejn
.pacetabaccm
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92169897001
SP82313 ASH
EPA 3050
MPRP/14056
EPA 6010
ICP/12793
92169897001
SP82313 ASH
EPA 3010
MPRP/14085
EPA 6010
ICP/12823
92169897001
SP82313 ASH
EPA 7470,
MERP/5536
EPA 7470
MERC/5364
92169897001
SP82313 ASH
EPA 7471
MERP/5541
EPA 7471
MERC/5366
92169897001
SP82313 ASH
ASTM D2974-87
PMST/5793
92169897001
SP82313 ASH
EPA 9D45
WET/26852
92169897001
SP82313 ASH
EPA 365.1
WETA/16309
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/12/2013 12:32 PM without the written consent of Pace Analytical Services, Inc..
Page 14 of 16