WQ0010689_Report_20180326

Annual Report Review Class A Distribution
Reporting Period: /I I l i� — 1213I / I-T
Permit Details: LU "i bo 10 (olq �� h A , DR S
Is 503? WO
Class 0 or B?
Maximum Dry Tons Per Year: 2-00
Number of acres permitted: NA -
Number of fields in permit: N A
Counties that land is permitted for: NA
Monitoring Frequency for TCLP: 1 )e 1fX
Monitoring Frequency for Residuals Analysis:
Monitoring Frequency for Pathogen & Vector Attraction Reduction: Nq
73 DT=ao/7 30
1. Class A Annual Distribution and Marketing/Surface Disposal Certification Form
Was a certification form submitted? I
Was distribution conducted during the reported period? 1 J
How many dry tons were produced and distributed? IS82. 73 (:2613
Were the distributions with the permitted amount? I� `4(V�dLA,( VO`U-wl- 44 Po'Ot-
Were recipients information listed?
Did it indicate compliance?
Was form complete?ho kadk�,-
Was it signed by the abpropriate people?
2. Monitoring i I
Were the analyses conducted at the required frequency? NP i2I&(o A
Was an analyses taken for each source that was distributed? l
Were the metals analyses reported on the Residual Samplingummary Form?
Were the results reported in mg/kg?y
Were the pH's 6.0 or greater for each residual sample?�
Were the heavy metals within ceiling concentration permit limits?
Were the lab analyses attached?
Were all the required parameters tested?
Was TCLP analysis conducted? �O6cz �
Were the TLCP contaminants within regulatory limifs?
Was a corrosivity, ignitability, and reactivity analysis conducted? �(
N /
3. Pathoge and Vector Attraction Reductio
Was a sign copy of the Pathogen and ector Attraction Reduction Form submitted?
Did the form ' dicate the period of erage, the residual class, and the pathogen reduction
alternative and th ector attractio reduction option used?
Was the appropriate ocumen tion to show pathogen and vector attraction reduction included
in the report?
Was pathogen and vecto a ction reduction demonstrated according to 40 CFR Part 503?
Class A 7ssAresiduals
gen Review\To be Cl shall meet-,
SIi vj WOLALP_ -QOr le_4- -es\
her fecal Coliform density or salmonella density.

Fecal Coliform density
Was the sampling conducted at the required frequency?
Were multiple samples taken?
Was each sample less than 1000 MPN/gram of total solids?
Salmonella density
Was the sampling conducted at the required frequency?
Were multiple samples taken?
Was each sample less than 3 MPN/4 grams of total solids?
To be Class A, residuals shall meet one of the following alternatives:
Alternative 1 — Time/Temperature
Were the residuals maintained for correct time and temperature?
Were logs submitted showing time and temperature?
Were temperatures within range for complete time period?
Alternative 2 — Alkaline Treatment
Were logs submitted showing time and temperature?
Was the pH raised to 12 or greater and maintained for 72 hours or longer?
Was the temperature 52°C (126°F) for 12 hours or longer while the pH was 12 or
greater?
Were logs submitted showing time and pH?
Was the temperature corrected to 250C (77°F)?
Alternative 5 — Process To Further Reduce Pathogens
PFRP Composting
Were the within -vessel method or static aerated pile methods used?
Was the residuals temperature maintained at 55°C (131°F) or higher for three
consecutive days or longer in the within -vessel method or static aerated pile method?
OR
Was the windrow composting method used?
Was the residuals temperature maintained at 55°C or higher for 15 consecutive days or
longer in the windrow method, and the windrow turned a minimum of five times during
this time?
PFRP Heat Drying
• Was the residuals dried by direct or indirect contact with hot gases and the moisture
content of residuals reduced to 10% or lower?
• Did the temperature of the residuals or the of the wet bulb temperature of the gas in
contact with the residuals as the residuals leave the dryer exceed 80°C (176°F)?
Vector Attraction Reduction Review
Was the samkling coil,dected at the required frequency?
Option 1 — 3 o Xolatile Solids Reduction
• Was th e 38% reduction?
efe lab sheets/calculations in report?
as the reduction (�i volatile solids (not total solids)?

• Were the samples taken at beginning of digestion process and before application
(Inspection)?
• Were calculations correct?
Option 2 — 40-Day Bench Scale Test
Were residuals from anaerobically digested treatment (Inspection)?
Were residuals anaerobically digested in lab?
Was the test run for 40 days?
Was the test done between 30°C (86°F) and 37°C (99°F)?
Was the reduction of on volatile solids (not total solids)?
Was the reduction less than 17%?
Were lab sheets/calculations in report?
Were calculations correct?
Option 3 — 30-Day Bench Scale Test
Were residuals from aerobically digested treatment (Inspection)?
Were residuals aerobically digested in lab?
Were residuals 2% or less total solids?
If not 2% total solids, was the test ran on a sample diluted to 2% with unchlorinated
effluent?
Was the test run for 30 days?
Was the test done at 20°C (68°F)?
Was the reduction of on volatile solids (not total solids)?
Was the reduction less than 15%?
Were lab sheets/calculations in report?
Were calculations correct?
Option 4 — Specific Oxygen Uptake Rate(SOUR)
Were residuals form aerobically digested treatment (Inspection)?
Were residuals 2% or less total solids (dry weight basis) (not diluted)?
Was the test done between 10°C (50°F) and 30°C (86°F)?
Was the temperature corrected to 20°C (68°F)?
Was the SOUR equal to or less than 1.5 mg of oxygen per hour per gram of total
residual solids (dry weight basis)?
Was the sampling holding time two hours?
Was the test started within 15 minutes of sampling or aeration maintained?
Option 5 — 14-Day Aerobic Process
Were the residuals from aerobically digested treatment (Inspection)?
Were the residuals treated for 14 days?
Was the residuals temperature higher than 40°C (104°F) for a 14-day period?
Was the average residuals temperature higher than 45°C (113°F)?
Option 6 — Alkaline Stabilization
Was the pH of the residuals raised to 12 or higher by the addition of alkali?
Did the pH of residuals remain at 12 or higher for two hours without the addition of
more alkali?
• Did the pH of residuals remain at 11.5 or higher for an additional twenty-two hours
without the addition of more alkali?
• Was the pH corrected to 25°C (77°F)?

Option 7 — Drying of Stabilized Residuals
Does the residuals contain any unstabilized residuals?
Were the residuals mixed with any other materials?
Were the residuals dried up to 75% total solids?
Option 8 — Drying of Unstabilized Residuals
Were the residuals mixed with any other materials?
Were the residuals dried to 90% total solids?
Option 9 —Injection
• Was there any significant amount of residuals on land surface one hour after injection
(Inspection)?
Was injection done on pasture or hay field?
Was injection done at time that crop was growing?
If Class A with respect to pathogen, were residuals injected with eight hours after
discharge from pathogen treatment?
4. General
Was the report in the proper format?
Was the annual report complete?
Was the report submitted on time?

Bam. tee.
3/26/201
p���nchar9�
Division of Water Resources 9 Chit
Water Quality Permitting Section
Non -Discharge Permitting Unit
1636 Mail Service Center
Raleigh-, NC 27699-1636
RE: 2017 Annual Ash Report
Permit No. WQ001.0689.
Wood Boiler = North Cove, NC
Enclosed is an additional supporting documentation for the 2017 Annual Ash Distribution Report
using the forms provided by NCDEQ-DWQ. This report includes- additional information not
included in our prior submittal (Ash Distribution Utilization Agreements). Included in this report
is the.following information:.
.Ash Distribution Utilization Agreements.
There were no permit deviations noted during the 2017.Reporting Year.
If you have any questions or require additional information, please contact myself at K8_756-
6636.
Sincerely,
Corey Carperitier
Attachments: -Ash Distribution Utilization Agreements (3 -copies)
Cc: Rickey Styles
RECEIVED
Division of Water Resources .
APR - q 2018
Water Quality Regional Operations
Asheville Rpaional 01 ice
Baxter healthcare Corporation
NO Box 1390,.Marion, NC 28752
T 828.756.4151

-r
Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11130 9) axter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to Recipient):
Application of the aforementioned ash is prohibited except in actor ance with th instructions this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
' or cover d ash An spill occurring while ash is in transport or on the application fields is the responsibility of the.
'S dry )• "Any Y P�
transporter. -The transporter must keep spill control provisions on the vehicle.:
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
s Ash shall not_ be stackpiled for more than 60 days prior to land application
• = APpPW ti6n of bulk'residitals shall not occur within 100 feet of a public or private water supply
+;.. A�copy of this Utilization Agreement shall be maintained at the land application site when bulk residuals are
6enn=a lied: .., ... _..:......
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any -site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other pse of the ash. %
Signed (Ash Recipient):y,� e C1_ Date:
Ash Recipient's Address: / 1 S
Intended Use of Ash: 5- o IV Z A,-4 ,4 , er,P g 8' 7 7
Expected Qty/Yr: 6� 5'0 T w S Acres of Land: % o Atyr `,-r
Baxter Representative Signature: —9—# �ge�Of�
Updated:, 11-07-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to d') IQf/e• lly 1e (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Any spill occurring while ash is in transport or on the application fields is the responsibility of the
transporter. The transporter must keep spill control provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
+ Ash shall not be stockpiled for more than 60 days prior to land application
• Application of bulk residuals shall not occur within 100 feet of a public or private water supply
+ A copy of this Utilization Agreement shall be maintained at the land application site when bulk residuals are
being applied.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10' centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash. /
Signed (Ash Recipient): ���,,1 �� J Date: - '7
Ash Recipient's Address: �� Sf f'��s� 1 e,,�� key .p el Alt C ZY 761
Intended Use of Ash: a/ ;,v, C.
Expected Qty/Yr: !7 //—T C rl c of Lan
Baxter Representative Signature:
Page 2 or3
Updated: 10-22-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11130119), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to I A r �Cc, tjli� (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Any spill occurring while ash is in transport or on the application fields is the responsibility of the
transporter. The transporter must keep spill control provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
Ash shall not be stockpiled for more than 60 days prior to land application
Application of bulk residuals shall not occur within 100 feet of a public or private water supply
• A copy of this Utilization Agreement shall be maintained at the land application site when bulk residuals are
being applied.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-' centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient): 7�1� .J Date: d �/
Ash Recipient's Address: Spj 7
Intended Use of Ash: So;1 did P1F��C�,+l¢ 4
Expected Qty/Yr: ),yc Acres o nd: I SL7
Baxter Representative Signature:
Page 2 of
Updated: 10-22-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to l' ���rsiT /y�,,��:d c'y (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Any spill occurring while ash is in transport or on the application fields is the responsibility of the
transporter. The transporter must keep spill control provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
• Ash shall not be stockpiled for more than 60 days prior to land application
• Application of bulk residuals shall not occur within 100 feet of a public or private water supply
• A copy of this Utilization Agreement shall be maintained at the land application site when bulk residuals are
being applied.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10' centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient): u- �En �' f+v Aef Date:
Ash Recipient's Address: �`� `/ % S �,v 2- , I 9-6m
Intended Use of Ash: ;. 1 N 6,1Q M
Expected Qty/Yr: 10C 4�r,•; Acres of Land: }
Baxter Representative Signature:
Page 2 o
Updated: 10-22-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to er-Jy Shy (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Any spill occurring while ash is in transport or on the application fields is the responsibility of the
transporter. The transporter must keep spill control provisions on the vehicle..
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
• Ash shall not be stockpiled for more than 60 days prior to land application
• Application of bulk residuals shall not occur within 100 feet of a public or private water supply
• A. copy of this Utilization Agreement shallbe maintained at the land application site when bulk residuals are
being applied.
lied:
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient):ze< - Date: 1'3 -/%
Ash Recipient's Address: /Zrj B746 /
Intended Use of Ash: L.W&
Expected Qty/Yr: _ f 0 d Acres f Land: y
Baxter Representative Signature:
Page Y o
Updated: 10-22-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to _J ,e f ,q ll S (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Any spill occurring while ash is in transport or on the application fields is the responsibility of the
transporter. The transporter must keep spill control provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
• Ash shall not be stockpiled for more than 60 days prior to land application
• Application of bulk residuals shall not occur within 100 feet of a public or private water supply
• A copy of this Utilization Agreement shall be maintained at the land application site when bulk residuals are
being applied.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient): W-�\J.5 Date:
Ash Recipient's Address: 874 CO,,,:15 ot,4 ..bd- de MAst,'alv ill za'iS,
Intended Use of Ash: `.-:.-t.L
Expected Qty/Yr: �,U [`
Baxter Representative
Acres of Land.
Page 2 of 3
Updated: 10-22-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752 .
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
„ Baxter Healthcare, Corp., is the generator of the ash provided to
Application of the aforementioned ash is prohibited except in accordance with the instructions on this (Recipient).
sheet.
Transport. Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Any spill occurring while ash is in transport or on the application fields is the responsibility of the
UftVWtW- The tntrteporter must keep spill control provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
Ault t11 not_be shrehpiled for more than 60 drays prior to land
' Applicadon of bulk residuals shall not occur within 100 feet of application c oprivate water supply
' A mpy of this Utilization
aPPh Agreement shall be maintained at the land application site when bulk residuals are
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim; demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient): �_LlGK//ili►I _ '
Date: ✓" 3 - / 7
Ash Recipient's Address:
Intended Use of Ash:oe
to i
Expected Qty/Yr:
Acres of Land:
Baxter Representative Signature:
Page 2 of
Updated: 11-07-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to De*& 4 `/tl,[ >C (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Any spill occurring while ash is in transport or on the application fields is the responsibility of the
transporter. The transporter must keep spill control provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
• Ash shall not be stockpiled for more than 60 days prior to land application
• Application of bulk residuals shall not occur within 100 feet of a public or private water supply
• A copy of this Utilization Agreement shall be maintained at the land application site when bulk residuals are
being applied.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-' centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or, in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient): 604/ !",t Date: 1-3-1-7
Ash Recipient's Address: S??A y`O Fo44 sw * V I i .G4- &No* iv t Zt' % s'i
Intended Use of Ash: L - rA L `' 4wL
Expected Qty/Yr: 1 t% 6 p %L% N Acres of Land: LP S G Iwo
Baxter Representative Signature:
Page 2 0 3
Updated: 10-22-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to Ar-A Cou-10S (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Any spill occurring while ash is in transport or on the application fields is the responsibility of the
transporter.. The transporter must keep spill control provisions on the vehicle,
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
• Ash shallnat be stockpiled for more than 60 days prior to land application
• Applicatton of bulk:residuals shall not occur within 100 feet of a public or private water supply
.'A copy of this [Italizktion Agreement shall be maintained at the land application site when bulk residuals are
beingapplied.;
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient): \(,— r -,,� Date: 7 / Vn l t l
Ash Recipient's Address: 1004 ('�,ic „5 '���,� Aj 30, h e, �h101
Intended Use of Ash:
Expected Qty/Yr: 400 raAS Acres of Land: j v 0 INle S
Baxter Representative
Updated: 11-07-14 � P e ryt c o r e

Parameter :
(mg/kg)
'Conc.
Limit .:
m . a
� Sam le a �o .aye
NP 12816A .
NP 12816
SP6217A
t.
SP6217B
NP 10217A
hi
NP 10217
Percent Moisture (%)
NA
40.9 v
40.5 j
55.9
54.6
50.7
49.3 j'
Arsenic
75
6.6 v
6.3 V
5.8 1.,;
4.6 1/
..2.6 toe..
3 ,r
Cadmium
85
1.2
1 V
2.2
2.8
1.2 t/
1:3 s®
Copper .
4,300...
1.10 v
8T8 .
90.4
. 89.3 y ..
48.7.✓
54.5
Chromium
NA
30.2 v .
21.2 :i� .
- 19.9 a,,:.
19.6
11.9
12
Lead ..
840.
23.1.a9
.22.6 v
28.3-
26.1
18.2. ✓
.22.0 t--
Mercury
57 `
-NI5'V.0 6
ND , 4
ND
ND
ND
ND
Molybdenwn
75
'0,99 :v
1.1 ✓ ' :
ND .
ND .✓
1.2
1.2
Nickel
420 '
20 v
19.1: V
22.3 ; ::
22.3 t. . Ile14.1
14.4 V,
Selenium.
100.
"ND v
ND v.
ND V
ND
ND tom..
ND
Zinc.
715.06
189 v
187.v;
274 ✓..
265.
.149
186 0�
Total Phosphorus
NA
1710- ✓-
1640
3130
3100 ,€
2240 V
2420
Barium
NA
1510 v
1540 V
15,70 yr
1550 v
961 d
1020
Calcium
NA
91400 v
83300
96800 V.
82400 v
51500
61000 t®
Iron-
NA
13200 V
MOO v
1030.0.✓.
10000 v
6350 ✓
6470 ✓
a For surface disposal facilities the, ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"1 certify, under penalty of law, that this document was prepared under my direction. or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted..1 am aware that there are significant
penalties for submitting: lse information, including the possibility of fines and imprisonment for knowing violations:"
�z z/l
Signature Prepares *. Date
*Prep'arer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL -RESIDUAL SAMPLING SUMMARY .FORM - B.
Report all sampling analysis results for parameters not listed in FORM RSSF that are part, of the WQ permit or were analyzed for over the past
- calendar year: Use :additional forms as needed.:
-
WQ-.Permit Number:
WQ0010689 Laboratory: 1)
Pace Analyd vices
Facility Name: ..
Baxter Healthcare Corporation North Cove
2)�
Steam Generation Plant Ash'
Residual Source.
�VQ0010689.:.
NPDES # or WQ#:
4)
4P#
WWTP Name:
NA. 5) . .
.Residual Analysis Data
Sample. or .Composite Date.
Parameter
(mg) _
NP 12816A'
NP 12816B
'SP6217A . . , :
SP6217B
NP1:0217A
NP 10217B
.
.Magnesium
16800 ,i
15600 v
15200 ✓
14700 ;;
8640. 61-1
8980.
Manganese
3030 v
3'160 .a
3610 ;y.....
2950.
1870
2180 , -
p H
10:3
10.2 .
9.9
1.0 1 ..:
9:4 ; . ,
.. 9.3 .
Potassium
14000. v
16600 ✓
10800 v • :
9480
11300
11600
Silver
... ND V
ND V. .....
ND if '...
ND td ..
-ND tom' ..
ND.
Sodium
4510 v
4930 V .:
3860
3650 �/
3740 t .:
409.0
41 certify, under penalty of law, that this document was prepared: under my direction. or: supervision m accordance: with a system
designed to assure that qualified 'personnel properly,gathered. and, evaluated the information submitted:.
I •a-m.aware that there are.
significant.penalties for
submitting false information, including the. possibility of fines and imprisonment for knowing violations."
. Z Z l Ij
Signature o reparer *.
Date
*Preparer is defined'in 40, CFR Part 503.9(r) 'and 15A NCAC 2T :1102 (26)
SF - B 12/2006
DENR.FORM RS ( )

CLASS A ANNUAL DISTRIBUTION AND.MARKETR4G/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0010689 FACILITY NAME: Baxter Healthcare Corporation North Cove Steam Generation Plant Ash
PHONE:[phone] COUNTY: [_ McDowell OPERATOR: j Baxter Healthcare
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
0 Distribution and. Marketing (complete Parts A. and B)
Part A*:
Part B*:
Month :
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent .
Residual In
'.
Product. Out
Name(s)-
Volume,(dry
tons)
Intended use(s) •
.March
WQ0010689
1.74:69
486:51
661:20
Kenneth Hughes, Max Holland,
Bobby Boone, Herbert Nanney,
Rickey Styles
661.20
Land Application
July
WQ0010689
93.97
261.71
355.68,
Bobby Boone, Jeff Banks, Lee
Moore, Dean McClure
355.68
Land Application
October
WQ0010689
9.04
25.16
34.20 •
Collins Farm
34.20
Land Application
November
WQ0010689
142.31.
396.34
.538.65.
Collins Farm Bobby Boone; Jeff .
Banks
538.65
Land Application
or
O
Totals:
Annual (dry tons):
420
1169.73
1589.73
1589.73
Amendment s used:
I
Bulking Agent(s) used: Dry Wood Chips
DMSDF.(Supp) (12/2006) Total Number of Form DMSDF (Supp) 1
* If more space is required, .attach additional information sheets (FORM DIM:RK

CLASS A ANNUAL.DISTRMUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0010689 . FACILITY NAME: Baxter Healthcare Corporation North Cove Steam Generation -Plant Ash
PHONE: [phone] COUNTY: McDowell OPERATOR:.. Baxter Healthcare
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
0 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the Dast calendar vear? Yes. 0. No ❑ -*'If No.skiD harts A. B. C and certifv form below
'Part A*:
Part B*:
Month
Sources s include NPDES # if
() (.
applicable)
Volume. (dry tons)
Recipient Information .
Amendment/.
Bulking Agent,
Residual In...
Product Out '.
Name(s)
Volume (dry tons).
Intended use(s)
January. . _ -
*See DMSDF sheet
February
supplemental for .
March-'
breakdown*
-
April .
a►
May
az
June
P
July
August
Fti
September
October
t
November.
ce
December
Total from FORM DMSDF (sup)
420
1169.73
1589.73
15891.73
Totals: . '
Annual (dry tonsy:
420
1169.73
1589.73
1589.73
Amendments used: I Bulking Agent(s) used: Dry Wood Chips
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) .1
cart u:
Facility was compliant during the past calendar year with all conditions of the land application.permit p. Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑'' No ► If No, Explain in Narritive
L . All monitoring was done in accordance with the permit and reported for the year as required and three (3)'copies. of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the. Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
z3/�/Zz��fS
SignstuVe ofPermittee Date Signa a of pf6parer.* Date
(if different from Permittee)
**Pre is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) .
DENR FORM DMSDF (12/2006)

Ash Inventory
Estimated
Ash Moisture as
WET Tons Ash
Hauled
Dry Ton
Date
Reused
Type Ash
Recipient
(measured)
Conversion
10/15/16
North Scrubber Pond
0.00
10/15/16
South Scrubber Pond
0.00
12/8/16
NP12816A
0.00
12/8/16
NP12816B
0.00
Mar-17
540
North Scrubber Pond
Kenneth Hughes
42.00%
313.20
Mar-17
204
North Scrubber Pond
Max Holland
42.00%
118.32
Mar-17
132
North Scrubber Pond
Bobby Boone
42.00%
76.56
Mar-17
228
North Scrubber Pond
Herbert Nanney
42.00%
132.24
Mar-17
36
North Scrubber Pond
Rickey Styles
42.00%
20.88
Apr-17
South Scrubber Pond
0.00
Apr-17
North Scrubber Pond
0.00
6/2/17
SP6217A
0.00
6/2/17
S P6217B
0.00
Jul-17
72
South Scrubber Pond
Bobby Boone
48.00%
37.44
Jul-17
36
South Scrubber Pond
Jeff Banks
48.00%
18.72
Jul-17
360
South Scrubber Pond
Lee Moore
48.00%
187.20
Jul-17
216
South Scrubber Pond
Dean McClure
48.00%
112.32
8/14/17
South Scrubber Pond
0.00
8/14/17
North Scrubber Pond
0.00
10/2/17
North Scrubber Pond
0.00
Oct-17
60
North Scrubber Pond
Collins Farm
43.00%
34.20
Nov-17
420
North Scrubber Pond
Collins Farm
43.00%
239.40
Nov-17
465
North Scrubber Pond
Bobby Boone
43.00%
265.05
Nov-17
60
North Scrubber Pond
Jeff Banks
43.00%
34.20
0.00
0.00
0.00
0.00
0.00
0.00
0.00
2829
1589.73
Note: Scrubber
ash includes sandbox ash used to dry ponds

PaceAnalytical Services, LLC.
• ®
aceAnal /��cal
9800 KinceyAve."Suite 100
J `.
Huntersville,-
NC 28078.
www.pudabs.mm'
[phone]
SAMPLE ANALYTE COUNT
Project: Wood Boiler Ash 10/2 :.
Pace Project No.:: "92357432
Analytes
Lab ID : Sample ID.
Method
Analysts
Reported
Laboratory
92357432001. NP70217A
EPA6010:" '
SH1
17
PAST -A:
EPA6010
SH1
7
PASI-A
EPA 7470
KAL
1
PAST -A..
EPA 7471
KAL
1
PASI=A
ASTM D2974-87
KDF
1
PASI-C
EPA-1010-
KMM
1,
PASI-A
EPA"9045
ECH
1 ..
PASI-A
EPA865.1
MDW.
A
PASI-A .
EPA:9014 '
PAS"
1
PASI-PA `
SM450082F-00
PAS
1
PASI-PA
' 02357432002 NP10217B _
EPA'6010 "." . "
SER
17
PASI-A. .
EPA 6010
SH.1
7
PASI-A
_ -
EPA.7470 "
KAL
1
PASI-A' .: .
EPA 7471
KAL
1
PASI-A
_
ASTM D2974-87
KDF _
1 "
: PASI-C
EPA 1010 '•
KMM
1
PASI-A"
:
EPA9045
ECH..
1
PASI-A ,
EPA365.1', .:
MDW
1
PASI-A- -
.. .
EPA 9014
PAS.
1 ...
PASI-PA ' . .
SM4500S2F-00
PAS
1
PASI-PA
r
HECEIVED
- .DmsionofWater"Resources
APR:. = 2 2ot1
D. A
Water Quallty Reglonal Operatlons
Asheville Re tonal Ofllce
REPORT OF LABORATORY ANALYSIS .
This report shall not be reproduced; except in full,
-
t
vnthou the:written consent of Pace Analytical Services; LLC. ..
Page 3'of 25

Pace Analytical Servides, LLC . .
®
�Ce/�LfaI�Ica
; .
9800 Kincey Ave. Suite 100
Huntersville, NC 28071r
wwv✓pecelebs:corn .
[phone] .
ANALYTICAL RESULTS
Project:., Wood Boiler Ash
10/2
Pace Project No.: , 92357.432 .
Sample: NP10217A
Lab ID: 92357432001 Collected: 10/02/17 09,45
Received: 1WOW 7 03:31 Matrix: Solid
Results reported on a "dry.'welght" basis and are adjusted for percent moisture, sample size and any dilutions:
Parameters
Results Units Report Limit DF ..
Prepared Analyzed ..
CAS No. Qual
6010 MET ICP.
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
2.6 :: mg/kg 1-.7 1
10/03/17 21:00 10/05/17 05:56
7440=38-2
Barium
961 mg/kg 0.83 1
10/03/17 21:00 10/05/17 05:56
7440-39-3
Cadmium
11.2 mg/kg 0.17 1
10/03/17 21:00 10/05/17 05:56
7440-43-9
Calcium.
51500 mg/kg 83.2 5
10/03l17 21:00- 10/05/17 11:53
7440-70-2
Chromium '
11.9 mg/kg 0.83 1
10/03/17 21:00 10/05/17 05:56
7440-47-3
Copper
48.7 • mg/kg 0.83 1
10/03/17 21:00 1.0/05/17 05:56
7440-50-8,
Iron
6350 . mg/kg 16.6 1
10/03/17 21:00 10/05/17 05:56
7439-89=6
Lead ..
18.2 mg/kg . 0.83 1
10/03/17 21:00 10/05/17 05,56
7439-92-1 '
Magnesium
8640 mg/kg 16.6 1
10/03/17 21:00 10/05/17 05:56
7439-954
Manganese
1870 mg/kg 4.2 5
10/03/17 21:00 10/05/17 11:63
.7439-96-5
Molybdenum
1.2 - mg/kg 0.83 1
10103/17 21:00 10/05/17 05:56
7439798-7
Nickel '..
14.1 mg/kg . 0.83 1
10/03/17 21:00 10/05/17 05:56
7440-02-0
Potassium
11306 mg/kg 832 1
10/03/17 21:00 ' 10/05/17 05:56
7440-0977.
Selenium
ND mg/kg = 1.7 1
10/03/17 21:00 10/05/17 05:56
7782-49-2 .
Silver .. -
ND, mg/k4 ' 0.83 1
10703/17 21:00 10/05/17 05:56
7440-22=4
Sodium
3740 r-hglkg 832 .1
10/03/17 21:00 10/05/17 05:56.7440-23=5
Zinc
149 :. mg/kg 1.7 1
10/03/17 21:00 10/05/17 05:56
7440-66-6
6010 MET ICP, TCLP.
Analytical Method: EPA 6010. Preparation Method: EPA.3010A
Leachate Method/Date: EPA 1311; 10/04/17 01:00 Initial pH: 9.9; Final pH: 5.5
Arsenic.::
ND V. mg/L 0.050 1
10/04/1122:15 :10/06/17 05:02
7440-38-2
Barium
7:4 v mglL 0.25 1
1.0/04l17 22:15 10/06/17 05:02
7440-39-3
Cadmium - . -
ND. V mg/L 0.0050 1...
10/04/17 22:15 10/06/17 05:02
7440-43-9
Chromium
ND `r '. mg/L... 0.050 1
10/04/1722:15- 10/06/17 05:02
744047-3
Lead
0.064 V mg/L 0.025 1
10/04/17 22%15 10/06/17 05:02
7439-92-1
Selenium
ND mg/L . 0.10 1
10/04/17 22:15 - 16/06/17 05:02
7782-49-2
Silver
ND V mg/L 0.025 1
10/04/17 22 15 .10/06/17 05:02
7440=22-4
7410 Mercury TCLP
Analytical Method: EPA 7470. Preparation Method: EPA 7470 .
Leachate Method/Date: EPA 13.11; 10/04/17 01:00 Initial pH: 9.9; Final pH: 5.5
Mercury
ND mg/L , 0.00020 1
10/04/17 22:30 10./05/17 19:11
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 ' Preparation Method: EPA 7471
Mercury
ND mg/kg 0.0094 1
16/04/17 22:20 10/05/17 21:24
7439-97-6
Percent Moisture
Analytical Method:ASTM D2974-87.
_ - __r ��. �--•_ _--�
Percent Moisture .
50.7 % 0.10 1
10/05/97`08 12
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010 -.
Flashpoint
s200.0 deg F 70.0 .1
a 1 /09/17 19�12,,
9046 pit So' W
Analytical' Method: EPA 9045
PH at 25,Degrees ':C
9.4 Std. Units 0.10 1
16:20u,:)
REPORT OF LABORATORY ANALYSIS.
This report shall not be reproduced,, except.in full,
Date: 10/11 /2017 04A5 PM
without the written consent of Pace Analytical Services, LLC:
Page 4 of2E

Pace Analytical Services,. LLC_
g r� ®
9800KinceyAve. Suite 100
fACQ GAIIaIIV/+� f1I
Huntersville, NC 28078-
www.pmbbs.com
[phone].
ANALYTICAL RESULTS
Project: Wood Boiler Ash 10/2
Pace Project No.: 92357432
Sample: NP10217A :
Lab ID: 92357432001 .Collected: 10/02/17 09:45 Received: 10/03/17 63:31 Matrix: Solid
Results reported on a dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results ;.. Units Report Limit DF Prepared Analyzed
CAS No. Qual .
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
2240, mg/kg 68.8 20 10/05/17 23:23
7723-14-0 M6, R1
733C S_Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Cyanide,. Reactive
-ND mg/kg . 2.0 1 10/10/17 12:57 10/10/17 19:36
-
.734S Reactive Sulfide
Analytical Method: SM4500217-00 Preparation Method: SW-846 T3.4.2
Sulfide; Reactive
Nb mg/kg ... 20.3 1 10/10/17 12:57. 10/10/17 18:06
...
REPORT OF_ LABORATORY ANALYSIS..
This report shall not be reproduced, except in full,
Date: 10/11/2017.04:45-PM
without the. -written consent of Pace Analytical Services, LLC.'
Page 5'of 25

1ac/7
eAnalX cal
uvwapaceWbs.=..
ANALYTICAL RESULTS
Project: Wood Boiler Ash 10/2
Pace Project -No.: -92357432
Pace Analytical Services, LLC
9800 i(inceyAve. Suite 100
Huntersville, NC:28078'
[phone]
Sample: NP102179
Results reported on a 'dry
Results
Lab ID: •92357432002 Collected: 10/02/17 09:45 Received: 10/03/17 03:31 Matrix: Solid
weight' basis and aie adjusted for percent moisture, sample size and any dilutions-
Results Units Report Limit DF . Prepared Analyzed. CAS No.. Qual
6610 MET ICP
Analytical Method:- EPA 6010 Preparation Method: EPA 3050.
Arsenic
3.0
mg/kg
1.6 1 . _
10/05/17 15:55
10/09/17 06:54
7440-38-2
Barium
1020
mg/kg
0.78. 1
10/05/17 15:55
10/09/17 06:54
7440-39-3
Cadmium
1.3
nlg/kg
0:16 1
10/05/17 15:55
10/09/17 06:54
7440-43-9
Calcium
61000
mg/kg
157 10.,
10/05/1.715:55.
10/09/1715:50
7440-70-2
Chromium
.
12.0
mg/kg
0.78 1
10/05/17 15:55
10/09/17 06:54
7440-47-3
Copper
54.5
mg/kg
0.78 1
10/05/17 15:55
10/09/17 06:54
7440-5078
Iron
6470..
mg/kg
15,7 1
10/05/1715:55
10/09/17 06:54
7439-89-6
Lead
22.11
mg/kg .
0.78. 1
10/05/17 15:55
10/09/17 06:54
7439-92-1
Magnesium
8980
mg/kg
15.7 1
10/05/17 15:65
10/09/17 06:54
7439-95-4
Manganese
2186
mg/kg
7.8 10
10/05/17 15:55
10/09/1715:50
7439-96-5
Molybdenum
1.2
mg/kg
0.78 1
10/05/17 15:55
10/09/17 06:54
7439-98-7
Nickel
-14.4
mg/kg
0.78 1
10/05/1.715:55
10/09/17 06:54
7440-02-0
Potassium-
11600
mg/kg
783 1
10/05/17 15:55
10/09/17 06:54
7440-09-7
Selenium
ND
mg/kg
1.6 1.
10/05/1715:55
10/09/17 06:54
7789-49-2
Silver
N.D.
mg/kg
0.78 1
10705/17 15:5510/09/17
06;54
7440-22-4
Sodium
- 4090 -
mg/kg .
783 1
10/05/17 15:55.
10/09/17 06:54
7440-23-5
Zinc
186
mg/kg
1.6 1
10/05/17 15:55
10/69/17 06;54
7440,66-6
6010 M& ICP, TCLP
-Analytical Method;. EPA 6010 Preparation Method: EPA 3010A
Leachate Method/Date: EPA
1311; 10/04/17 01:00 Initial pH: 9.9; Final
pH: 5.5
10/06/17 05 06
7440-313-2
Arsenic :.
ND V
mg/L
0.050
1
10/04/17 22.15
Barium
7.8 ✓
mg/L
0.25
1
10/04/17 2215
10/06/17 05:06
7440-397-3 .
Cadmium
ND ✓
'mg/L
0.0050
1.,
10/04/1122:15,
10/06/17 05:06
7440-43-9
Chromium
ND ✓
mg/L
0.050
1 :.
10/04/17 22:15
.10/06/17 05 06
7440-47-3
Lead
6.664 ✓
mg/L
0.025
1
10/04/17 22.15
10/06/17 05:06
7439-92-1
Selenium
ND ✓
mg/L .
0.10
1'
10/04/17 22:15
10/06/17 05:06
7782-49-2
Silver.
ND ✓
mglL
0.025
1
10/04/17 22i15
10/06/17 05:06
1.440=22.
7470 Mercury, TCLP Analytical Method: EPA 7470. Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 10/04/17 01:00 Initial pH: a.v, rmai pn. as
Mercury :
ND mg/L 0.00020 1 10/04/17 22:30
10/05/17 19:14 7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation.Method: EPA 7471
Mercury.
ND :mg/kg 0.0061 1 10/04/17 22:20
10/05/17 21:27 7439-97-6 -
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture •
49.3 % 0.10 1
10/05/17 08:12
1010 Flashpoirit,Closed Cup -_ ::
Analytical Method: EPA 1010
yt
Flashpoint
>200.0 deg F 70.6 .1
10/03/17 19:12 ,
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C _
9.3 Std. Units 0.16 1
10/05/17 16:20
=
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/11/2017 04:45 PM
without the written consenbof Pace Analytical Services, LLC.
Page 6 of 2.

Pace Analytical Services, LLC
Q /��
® 9800IGnceyAve. "Suite 100
acemalxical - Huntersville,NC 28078
www.paWabsxom
[phone].
ANALYTICAL RESULTS
Project:- Wood Boiler Ash 10/2
Pace Project No.: 92357432
Sample: NP10217B : tab 1D: 92357432002 Collected: 10102/17 09:45 Received: 10/03/17 03:31 Matrix: Solid
Results reported on a 'dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
365.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus 2420 mg/kg 79.0 20 10/05/17 23:25, 7723-14-0
733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3:2
Cyanide, Reactive ND mg/kg 2.0 1 10/10/17 12:57 10/10/17 19:36
734S Reactive Sulfide Analytical Method: SM4500S2F-00 Preparation Method: SW-846 7.3.4.2
Sulfide, Reactive ND mg/kg 19.7 1. 10/1011712:57. 10/10/17 18:06
Date: 10/1112017 04:45 PM -
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Wood Boiler Ash 10/2
Pace Project No.: 92357432
QC Batch: 380928 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92357432001, 92357432002
METHOD BLANK: 2110932 Matrix: Water
Associated Lab Samples: 92357432001, 92357432002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/L ND 0.00020 10105/1717:03
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078'
[phone]
LABORATORY CONTROL SAMPLE: 2110933
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury mg/L .0025 0.0030 118 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2110934 2110935 -
MS IUSD
92357274001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND .0025 .0025 0.0029 0.0029 116 114 75-125 2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/11 /2017 04:45 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 2;

Pace Analytical Services, LLC
�^Q A �alwa�
VGf�, V
9800 Kinsey Ave: Suite 100
Huntersville, NC 28078
wwwpecelabs.com
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Ash 10/2
Pace Project No,: 92357432
QC Batch: 380.919 Analysis Method:. EPA 7471
QC Batch Method: EPA7471 Analysis Description:- 7411 Mercury
Associated Lab Samples: 92357432001, 923.57432002
METHOD BLANK: 2110902 Matrix: Solid
Associated Lab Samples: 92357432001, 92357432002
Blank . `.. Reporting
Parameter Units Result Limit - - - Analyzed Qualifiers
Mercury... mg/kgND 0.0060 - 10/05/17 20:50
LABORATORY CONTROL SAMPLE: 2110903
Spike. LCS . LCS % Rec.
Parameter Units Conc:. Result %Red. Limits Qualifiers
Mercurymg/kg . .083 ' .. 0.084 101. -80-120
MATRIX SPIKE & MATRIX SPIKE. DUPLICATE: - 2110904 : - -. - 2110905 ' .:.. :. ...
.
MS MSD
- - 35761900t Spike Spike - .. MS.:. .MSD.:. MS
92
• MSD .
%.Res -
Parameter. Units' Result Conc. Conc.. Result Result. - %Rec % Rec
Limits RPD . Qual
.. ry.. - mg/kg . ., ND .053 :033 0:0042 .0018J 8 - 5
Mercu
75-125 M1
Results presented on this page are in the units Indicated bythe "Units" column except where analternate unit Is presented to the right of.the-result:
REPORT OF LABORATORY -ANALYSIS .
This report shall not be reproduced, except in full,
Date:10/11/2017 04:45 PM , without -the written consent of Pace Analytical Services; LLC.
Page 9 of 95

Pace Analytical Services, LLC.
®
aceAnalytical
9800 KtnceyAve. Suite 100
Huntersville,.NC 28078
www.pace/abs.coa+
... . (704)875-9 092
QUALITY CONTROL DATA
Project: Wood Boiler Ash 10/2
Pace Project No.: 92357432
QC Batch: 380583
Analysis Method:
EPA 6010
QC Batch. Method: EPA 3050
Analysis Description:
6010
MET
Associated Lab Samples: 92357432001
METHOD BLANK: 2108944
Matrix: Solid
.Associated Lab Samples: 92357432001
Blank
Reporting
Parameter-
Units.
Result
Limit
Analyzed
Qualifiers
Arsenic.
mg/kg ::
ND
1.0
10/05/17 04:30
Barium.
mg/kg
ND
0.50
10/05/17 04:30
Cadmium
mg/kg
ND
0:10
10/05/17 04:30
.
Calcium. _ .
mg/kg .
ND
10.0
10/05/17 06:06
Chromium .:
mg/kg
Nb-"
.0.50
10/05/17 04:30
Copper
mg/kg
ND
0:50
10/05/17 04:30
Iron
mg/kg.
ND
10.0
10/05/17 04:30
Lead ..
mg/kg
ND.
0.50
10/05/17 04:30
Magnesium
mg/kg
ND
10.0
10/05/17 04:30
Manganese
mg/kg
ND
0.50
10/05/17 04:3.0
Molybdenum
mg/leg
ND
0.50
10/05/17 04:30
Nickel
mg/kg_
ND
0.50
10/05/17 04:30
Potassium :
mg/kg
ND
560
10/05/17 04:30
Selenium
mg/kg
ND
1.0
10/05/17 04:30
Silver ..
mg/kg
ND
.0.50
.10/05117 04:30
Sodium
mg/kg
ND
600
10/05/17 04:30
Zinc
mg/kg
ND
1.0
10/05/17 06:06
LABORATORY CONTROL SAMPLE:. 2108945 -
Spike
.
LCS
LCS • %
Rec
Parameter
Units
Conc..
Result
% Rec Limits
Qualifiers
Arsenic
rhg/kg :
50
49.2
".
98
80-120
Barium-. ,
mg/kg .
50
49.1:
98
80=120
Cadmium
mg/kg
50
50.0
100
80-120
Calcium
mg/kg
600
528
106
80-120
Chromium
mg/kg
.50
50.0
100
806120
Copper
mg/kg
50
50,7
101
80-120
Iron
mg/kg..
500
516
103
80-120
Lead ..
mg/kg
50
50.2
100
80-120
Magnesium
mg/kg
500
609
102
80-120
Manganese
mg/kg
50
50.6
101
80-120
Molybdenum
mg/kg
50
54.2
108
80-120
Nickel
mg/kg
_ 50
49.3
99
80-120 •
Potassium
mglkg
500
506
101
80-120
.Selenium
mg/kg
50
51.3
103
.80-120
Silver
fng/kg..
.25
26.3
105
80-120.
Sodium
mg/kg
500:
513
103
80-120;
Zinc
mg/kg : "
50
52.0
104
80-120
Results presented on this page am In the units Indicated:by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF. LABORATORY ANALYSIS
This reportshall not be reproduced, except in full,
Date: 10/11/2017 04:45 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 25

PaceAnalytic
acemalytiol
980
in
KceyAve.. Suite 100
www.pacelabs mn..
Huntersville; NC 28078
.
.
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Ash.10/2
Pace Project No.: 92357432
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2108946
2108947
MS
MSD, .
92356587008
Spike
Spike
MS.
MSD
MS
MSD
% Rec
Parameter .
Units
Result
Conc.. -
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Quat
Arsenic.
mg/kg
0.79J
57.8
62.3:
45.3
48.4
77
76.
75-125
7
Barium
mg/kg
63.7
57.8
:'62.3.
193
116
223.
84'
75-125
50 M1,R1
Cadmium
mg/kg
ND
57.8.
62.3
50.6
.58.4
87
94
.:75-125
14
Calcium
mg/kg
1540
578
623
4600.
.2090
530.
89
75-.125
75 M1-,R1' '
Chromium
mg/kg
60.1
57.8
62.3
103
128
75::
109
75-125:
21 R1
Copper
mg/kg
U.2
57.8
62.3
124
115..
123
102
75.125
7
Iron
mg/kg
45800
578:
-623.
32700 .
54900
-2260
-1460
75-125'.
" 51 E,M1,R1.
Lead ..
mg/kg
14.8
57.8
62.3
64.2..
65.7
85
82
75-125
2:
Magnesium
mg/kg
148.0
578
623
7880
: • 2060
1110
. • 93 -:
75-125:
117 M1,R1
Manganese
mg/kg
328
.57.8
62.3:.
839
399.,
-885
115.
75=125.
7:1 M1,R1
Molybdenum
mg/kg
2.3
57.8 .
-.62.3
46.3
53:2:
-76
82
75-125.
14
Nickel.
mg/kg
8.9
57.8
•62.3
68.2
64:4
103
- 89
75-125:
6.
Potassium .
mg/kg
619 ...
578.
623
2440
1070
314.,
72
75-125.
78 M1;R1
Selenium
mg/kg
3.5
• 51.8
62.3
42.2..
45.3.
67
67
75-125
7.M1 -
Silver ..
mg/kg
ND
28.9
31.1-
27.3
- 31.6
93
101.
75-125
15
Sodium:
mg/kg :
ND
576
'623.
'696
705
104
98
75-125
::.1
Zinc
mg/kg
27.0
57,8
62.3" :
105
832
136
90 ".
75-125
24 M.1, R1
Results presented an
this page are In the units Indicated by the "Units" column except where an alternate uoit.is presented to the right of the.result..
REPORT
OF LABORATORY ANALYSIS
•
This.
report shall
not be rdomduced,-except in full,
Dater 10/11/2017 04:45 PM
without the written consent of Pace Analytical Services, LLG
.
page. 11. of 25

IaceAnalytical®
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytleal Seivlces, LLC
9800 Kinceykve. Suite 100,
Huntersville, NC 28078
.. 7oa.�a75-so
Project: Wood Boiler Ash 10/2
Pace Project No.: 92857432
QC Batch: 381038
Analysis Method: EPA6010
QC Batch Method: EPA 3050
Analysis
Description: 6010
MET
Associated Lab Samples: 92357432002,
METHOD BLANK: 2111521
Matrix: Solid
Associated Lab Samples: 923574.32002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Arsenic
mg/kg
ND
1.0
•16/09/17 05:43
Barium
mg/kg
ND
0.50
10/09/17 05:43
Cadmium
mg/kg_
ND
0.10
10/09/17 05:43
Calcium
mg/kg
ND
10.6
10/09/17 05:43
Chromium
mg/kg
ND
0.50
10/09/17 05:43
Copper
mg/kg
ND
_ 0.50
10/09/17 05:43
Iron
mg/kg
ND
10.0
10/09/17 05:43
Lead
mg/kg.
ND
0.50
10/09/17 05:43
Magnesium
mg/kg
ND
10.0
10/09/17 05:43
Manganese
mg/kg .:
-.ND
0.50
10/69/17 05:43
Molybdenum
mg/kg
ND-
0.50
10/09/17 05:43
Nickel
mg/kg
ND
0.511
10/09/17 05:43
Potassium
mg/kg
ND
.
500
10/09/17 05:43
Selenium
mg/kg
-
ND
1.0
10/09/17 05:43
Silver
mg/kg
ND
0.50
10/09/17 05:43
Sodium
mg/kg
ND
500
.10/09/17 05:43
Zinc
mg/kg
ND
1.0
10/09/17 05:43
LA90RATORY CONTROL' SAMPLE: 2111522
Spike.
LCS
-LCS %
Rec
Parameter
Units
Cone.
Result
% Rec Limits Qualifiers
Arsenic
mg/kg
.50
47.9.
96
80-120
Barium
mg/kg
50
48.9
98
80-120
Cadmium
mg/kg
50
48.2
96
80-120
Calcium
mg/kg ;.
500
504
101
80-120
Chromium
mg/kg
50
46.5
97
80-120
Copper
mg/kg
50
49.1
98
80-126'_
Iron
mg/kg
500
408
160
80-120
Lead
mg/kg
50
47.8
96
80-12.0
Magnesium
mg/kg
500
492
98
80-120.
Manganese
mg/kg'
50
48:9.
.98
80-120
Molybdenum
mg/kg
50
51.T
103
80-120.
Nickel
Ing/kg
50
47.3
.95
80-120
Potassium
mg/kg
500
ND
99
80.120
Selenium
mg/kg
50
48.6
97.
80-120
Silver
mg/kg
25
25.3
101
80-120
Sodium
mg/kg
500
498J
.100
80-120
Zinc
mg/kg
50
49.6
99
80-120
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/11/2017 04:45 PM . without the written consent of Pace Analytical Services, LLC.. Page 12 of 25

QUALITY CONTROL DATA
Project: Wood Boiler Ash 10/2
Pace Project No.: . 92357432
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:.
2111523 -
2111524
-
MS
MSD,
92357319008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result .
Conc..
Cones
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic ,
mg/kg
0.89
42.2
42.2
33.6
36.4 _
77.
: = 84
. 75-125
8
Barium
mg/kg
14.6
42.2
:.42.2.
54:0 ,'
56.3
93.
99
75-125
4
Cadmium
mg/kg
ND
42.2
42.2
'. 37.9
37.8
90
90
-.75-125
0
Calcium
mg/kg
ND,
422
422
399
405;
94.
95
75-125
1
Chromium
mg/kg
12.0
42.2
42.2
52.5
46.9
96
83.
.75-125
11
Copper
mg/kg
10.9
42.2
42.2
52.7
47.4.
99
87
75-125
11 .
Iron
mg/kg
18000
422.
422.
22100
9770
:758
-2160
75-125
77 E,M1,R1.
Lead
mg/kg
5.6
42.2
42.2
43.0 ' ..
42.1:
88
86
75-125
2 - _
Magnesium
mg/kg
2560
.422
422
3080
2620
124
15
75-125
16 M1.:
Manganese
mg/kg
41.0
42.2..
42.2
81.1
72;4
95.
75
7$-125
11
Molybdenum
mg/kg
0:95 -
42:2.
42.2-
39.2
39:3 :
91 ..
91
75-125
0
Nickel
m /k
g 9
10.6
42.2'
.42.2
47.7.
45:0 1
.88:.
82
75-125
6.
.,Potassium
mg/kg
ND ..
- 422.
422
745
639
112
87
-.75-125
A5
Selenium ..
mg%kg
1.3
42.2
42.2
32.2.
37;1.
73
85
75-125
14 M1
Silver "..
mg/kg
ND
21.1
21.1
20.3
20:3
96
96:
75-125
0
Sodium ' '
mg/kg
ND
422
422.
470, .
478
95
97
75-125
2
Zinc
mg/kg
30.3
42.2
.42.2
: `70.7
.64:5 -
96.
81
75-125
9
Results presented on this page are in the units indicated by the "units" column except where an alternate, unit Is presented to the right of the. result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced; except in full,.
Data:10/11 /2017 04:45 PM
without the written consent of Pace Analytical Services, LLC.
' Page 13 of 25

Pace Analytical Services, LLC
o
rf J �►g
ceAnalyfica
9800 Kincey Ave. Suite 100.
Huntersville, NC 2807.8
wwwpscelebs com
-
[phone]"
QUALITY CONTROL DATA
Project:.. Wood Boiler Ash
10/2
Pace Project No.: 92357432
QC Batch: 380927
Analysis Method: EPA 6010
QC Batch Method: EPA 3010A
Analysis Description: 6010 METTCLP
Associated Lab.Samples• 92357432001, 92357432002
METHOD BLANK: 2110928
Matrix: Water
Associated Lab Samples: 92357432001, 92357432002
Blank Reporting -
Parameter
Units
Result Limit Analyzed
Qualifiers
Arsenic
mg/L
NO 0;050 10/06/17-04:13.
_
Barium
mg/L
ND 025 10/06/17.16:53
Cadmium
mg/L
ND 0.0056 10/06/17 04:13
Chromium
mg/L
ND 0.050 10/06/17 04:13
Lead
mg/L
ND 0.025 10/06/17 04:13
Selenium
mg/L
ND 0.10. 10/06/17 04:13
Silver
mg/L
ND 0.025 10/06/17 04:13
LABORATORY CONTROL SAMPLE:
2110929
Spike.. LCS LCS %
Ree
Parameter
Units
Conc. Result % Rec Limits Qualifiers..
Arsenic
mg/L
2.5 2.3 94
80-120
Barium
mg/L
2.5 2.4 97
80-120
Cadmium
mg/L
2.5 -2.4 . 95
80-120.
Chromium
mglL
2.5 2.3 .93
80-120
Lead, -
mglL
2.5 2.1. 82
80-120
Selenium
mg/L
2.5 2.4 97
80-126
Silver
mg/L ...
- 1.2 . -... 1.2.. 97
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2110930 2110931
MS MSD.
92357274001
Spike Spike : MS : MSD. MS
. MSD.
% Rob
Parameter
Units Result
Conc. Conc. .:Result Result % Rec : . %. Rec
. Limits.. RPD, Qual
Arsenic
mg/L ND
2;5 2.5 2.3 2.3
91'91
75-125 0
Barium
mg/L ND
2.5 2.5 2.5 2.4
99 97
75-125 2
Cadmium.
mg/L ND
2.5 2.5 2.3 2.3
93 92
75-125 1
Chromium
mg/L ND
2.5 2.5 2.3 2.3
92 91
75-125 1
Lead
mg/L . ND
2.5 2.5 2.0 2.0
81 81
75-125 -0
Selenium
mg/L ND
2.5 2.5 2.4 2.4
97 97
.75-125 0
Silver
mg/L ND
1.2 1.2 1.2 _ 1.2
98 97
75-125 0
Results presented on this palls are In the units indicated by the "Units" column except where an alternate unit Is
presented to thosight of the'msult.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full; .
Date: .10/11/2017 04:45 PM .
without the written consent of Pace Analytical Services, LLC.
Page.14 of 25

Pace Analytical Services, LLC
®
aceAnalytical
9800 KinceyAye. Suite 100
' w�rw.pacelebs.com
Huntersyilla, NC 28078
.
[phone].
QUALITY CONTROL DATA
Project: Wood Boiler Ash 10/2
Pace Project No.: 92357432
QC Batch: '380883
Analysis Method: ASTM D2974-137
QC Batch Method: ASTM D2974-8.7
Analysis De_ sceiption: '. Dry Weight/Percent Moisture
Associated Lab Samples: 92357432001, 92357432002
SAMPLE DUPLICATE: 2110658
923 001
56700 Dup.
Parameter.
Units, Result Result RPD Qualifiers
Percent. Moisture
63.6. , 38.5. 49: R1.
'SAMPLE DUPLICATE: 2110659
92357739004 Dup .
Parameter
Units i2esult. Result RPD, Qualifiers
Percent Moisture
% 21.3. .20.8 2
Results presented orrthis page are In the units.indicated by the "Units".column except where an alternate unit is presented to the right of the result.
..REPORT OF.LABORATORYANALYSIS..
This report shall not, be reproduced, except in full,
Date: 10/11 /2017 04:45 PM
without the written consent of Pace AnalyticatServices, CLG.
Page 15 of 25

Pace Analytical Services, LLC
® 9800
eAnalytical Hun ersv Ile, NC 2807�
a - .
www.pacelabs.com .. .
[phone]
(QUALITY CONTROL DATA
Project: Wood Boiler Ash 10/2
Pace Project N. o.: 02357432
OC Batch: 380716 Analysis Method: EPA 1010
QC Batch Method: EPA 1010 Analysis Description: 1010 Flash Point, Closed Cup
Associated Lab Samples: 92357432001, 92357432002
SAMPLE DUPLICATE: 2109783
92357432001, Dup
Parameter Units Result Result RPD Qualifiers
Flashpoint deg F >200.01 >200.0
cResults presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall riot be reproduced, except in full,
Date: 10/11/2017 04:45 PM without the written consent of Pace Analytical Services, LLC. Page16-of 25

Ric to; Analjftal
wwvw.pawlebs.com
QUALITY CONTROL DATA
Project: Wood Boiler Ash 10/2
Pace Project No.: 92357432
Wt; batch: 380987 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92357432001, 92357432002
SAMPLE DUPLICATE: 2111154
Parameter
pH at 25 Degrees C
92357067006
Units Result
Std. Units 7.3
Dup
Result RPD Qualifiers
7.4 1
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1Oil 1/2017 04:45 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 25

�'..apeAnqlyfical
www.pacelabs.= i
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
'Project: Wood Boiler Ash 10/2
Pace Project No.: 92357432
QC Batch: 380926
Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92357432001, 62357432002
METHOD BLANK: 2110924
Matrix: Solid
Associated Lab Samples: 92367432001, 92351432002
Blank Reporting
Parameter Units
Result Limit
Analyzed. Qualifiers
Phosphorus mg/kg.
ND 2.0
10/05/17 22:43 .
LABORATORY CONTROL SAMPLE: 2110925
Spike LCS _ ..
LCS % Rec
Parameter Units
Conc... Result
% Re& Limits 06alifiers
Phosphorus mg/kg
50 50.5
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2110926 2110927
MSMSD
- 92357432001
Spike Spike MS
MSD MS, MSD % Rec
Parameter Units Result:
Conc.... Conc. Result
Result "/o Rec /6 Rec Limits RPD Qual, .
Phosphorus mg/kg 2240
83.2 99.5 2010
2300 -267 68 90-110 13 M6, R1
Results present®d on this page are In the units indicated by the "Units" column except where an alternate unit is. presented to th® right of the result.
REPORTOFLAEORATORYANALYSIS:
This report shall not be repioduced,, except in full,:
Date: 10/11 /2017 04:45 PM. without the written consent of Pace.Analytical Services, LLC. Page 18 of 2

acemaIxical
www.pacLIabs.com
Project: Wood Boiler Ash 10/2
Pace Project No.: 92357432
QC Batch: 274847
QC Batch Method: SW-846 7.3.3.2
Associated Lab Samples: 92357432001, 92357432002
METHOD BLANK: 1351735
Associated Lab Samples: 92357432001, 92357432002
Parameter Units
Cyanide, Reactive mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 9014
Analysis Description: 733C Reactive Cyanide
Matrix: Solid'
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.99 10/10/1719:31
Pace Analytical Services, LLc
9800 KinceyAve. Suite 10a
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1351736
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Cyanide, Reactive mg/kg 99.5 .68J 1
0-8
SAMPLE DUPLICATE: 1351737
Parameter
Cyanide, Reactive
30232417001 Dup
Units Result Result RPD Qualifiers
mg/kg ND ND
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/11/2017 04:45 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 25

Pace Analytical Services, LLC: .
9800 Kincey Ave. Suite 100
B /jam ! gr®
aCG /`U l�f 1 ICQI
Huntersville, NC 26078
www.pacelabs.com :..
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Ash 10/2
'Pace Project"No.: 92357432
QC Batch: 274846
Analysis Method:' SM4500S2F-00
QC Batch Method: SW-846 7.3.4.2
Analysis Description: 734S Reactive Sulfide
Associated Lab Samples:. 92357432001, 92357432002
METHOD BLANK: 1351732
Matrix: Solid
Associated. Lab Samples: 92357432001, 92357432002
Blank Reporting
Parameter Units
Result -Limit Analyzed Qualifiers
Sulfide, Reactive mg/kg
ND 9.9 10/10/17 18:06
LABORATORY CONTROL SAMPLE: 1351733
Spike LCS LCS % Rob
Parameter Units
Conc. Result %'Rec :.. Limits Qualifiers
Sulfide, Reactive mg/kg
199 43.7 22 0-52
SAMPLE DUPLICATE: 1351734
30232417001' Dup
Parameter Units
Result . Result RPD Qualifiers .
Sulfide, Reactive mg/kg
ND D
.N
Results presented on this page are In the units Indicated by the ".Units" column except where an alternate unit is presented to the right of the r®sult.
REPORT OF LABORATORY ANALYSIS.
.:
This report shall not be reproduced, except in full,
Date: 10/11 /2017 04:45 PM
without the written consent of Pace Analytical Servic®s, LLC. Page .20. of 2

aceAnalytical
www.pawlabs.com
QUALIFIERS
Project: Wood Boiler Ash 10/2
Pace Project No.: 92357432
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC -'Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for.
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A
Pace Analytical Services -Asheville
PASI-C
Pace Analytical Services - Charlotte
PASI-PA
Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
Date: 10/11/2017 04:45 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 25

Pace Analytical Services, LLC
®
9800 Kincey Me. Suite 100;
a
Hun tesvilleNC 28078
(704)875-909ceAoaly2
wiMpMISO com;
.
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Wood Boiler Ash 10/2
Pace Project No.:
62357432
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Meth'od
. Batch
92357432001
NP10217A
EPA3050.
380583
EPA6010
380776
92357432002
- NP10217B
EPA 3050
381038
EPA 6010
381116
02357432001
NP10211A
EPA 3010A
380927
EPA 6010
380947
92357432002
NP10217B
EPA 3010A
380927
EPA 6010
380947
957432001 '
23
NP10217A
EPA 7470
380928 -
EPA 7470' .
380949
380949
92357432002,
NP70217B
EPA 7470
380928
EPA 7470
.
92357432001
N010217A
EPA 7471
380919
EPA 7471
380952
380952
92357432002
NP.10217B
EPA 7471
3i30919
EPA 7471
92357432001
NP1021.7A
ASTM D2974-87
380883
92357432002
NP10217B
ASTM-D2974-87.
380883
92357432001
NP10217A
EPA1010:
380716
9236741002
NP10217B
1010 EPA
3807.16
92357432001
NP10217A
EPA 9045
380987 .'
92357432002
NP102170
EPA 9046
380987
92357432001
N010217A
EPA 365;1 _
380926
92357432002
NP16217B
EPA 365.1- -
380926
923572001
43
NP70217A
SW-8467.3.3.2
274847
EPA9014
274912
274912
92357432002
NP10217B
SW-846 7.3.3.2
274847
EPA 9014
92357432001
'NP10217A
SW-846 7.3.4.2
274846
SM450062F-00
2.74911
_ _
92357432002
NP10217B
SW-846 7.3.4.2
274846
SM4500S2F-00
274911
REPORT :OF LABORATORY ANALYSIS
This.report shall not be reproduced, except in full,
Date: 10111 /2017
04:45 PM
without the written consent of Pace Analytical Sen4ces, LLC.
Page 22 of 2

Document Name:.
Document Revised; July'25; 2017
a
SarripleConditionUponReceipt (SCUR) ;
Page,l'Of 2.
D:ocument'No.:
lsuing'Authority:
8Ct'4i7alyflCd�
F-CARrCS•033-Rei►.03
Pace quality Office
Laboratory. receiving: sa es:
Asheylle Eden Greenwood Huntersville. _ gh[] Mechanicsville
❑ ❑ ❑ Ralel ❑
SampleClient Name:
.. Pro' it WO# 9237432
I. I
Courier: ❑Fed Ex ❑UPS (]USPS e client
Commercial OPace QOther.
Custody Seal Present? QYeseals Intact? QYes ❑No.. 57
923 432:
\" Date/Initials Person Examining Contents 1�.
J.V r
1V
Packing Material.•' ❑Bubble Wra ;p :: [f Bubble Bags None. ❑ Other BioidgicaLTfssue fr n?
Thermometer - []Yes ' E]No N/A
et QBlue . None
IR bun ID: Type. of is : .
Correction Parlor: Cooler Temp Corrected (°C): - Teritp should be above freezing to fi°C'
QSamples:out of tempt Samples on ice, cooling process
��. has begun
USDA Regulated Soil ((] N/A, water Sample)
Did,samples originate in'a quarantine zone withih°the United States: CA; NY, or SC, (check maps)? Did samples originate.from a foreign source (intematlon ,
Yes ❑No incloding:Hawaii and Puerto Rico)? dYes ❑N'
Comments/Discrepancy:.
Chain of CustodyPresent? es ❑No
Samples Arrived within Hold Time? . ❑No . ❑N/A 2
Short Hold'Tirrie.Analysis (i72 hr:)? []Yes. ❑N/A 3...
Rash Tern Around Time Requested? QYes o - ❑N/A �4:
Sufficient Volume? ::.. []No es:
Correct Containers Used? j]No QN%A '6
=Pace Containers Used? -❑No . QN/A
Containers Intact?, . es ❑No ❑N/ - .7,
y p a]Ye : QNo /A 8. .
D.issolved::anaf sis: Sam' les'Field Filtered?"
Sample Labels Match COE?' :. es : ❑No []N%R' 9. .
Includes:Date/Tire/ID/A.nalysis Matrix:
Headspace inVOA Vials (>5-6tnm)? Oyes: ❑No N 10. .
Trip Blank Present? Des ❑No / 11.
TripfllankCustodySeais:Present?_ ❑Yes ❑No N/A'..
CL E T NOTO CATIONJRESOLtIT16N Field -Data Required? [3Yes ❑No
Person Contacted:" .. Date/Tme:
Comments/Sample piscrepancY
Project Manager SCURF Review;
�JDate: io , ,.
Project Manager SRF Review: Date; /11/5Z ;z
%
Note: Whenever there is adiscrepancyaffecfing North Carolina compliance, samples, a copy ofthis form will be sent to the North Car`oiinaDEHNRCeitification Office (i.e.
Out of hold, incorrect p'redervatiye.out of temp; incorrect contelners)
3
. Page 2 of 25

0
N
N
C
.to
cc
V,
.01
in
.p
W
ri
Item#
ZZZZZ—XZZZZZ
BP4U=125 mL Plastic Unpreserved (N/A) (Cl-)
MU250 ml. Plastic Unpreserved (N/A)
BPZU-500 mL Plastic Unpreserved (N/A)
SP1U-1 liter Plastic Unpreserved (N/A)
zz
BP4S-125•mL Plastic H2SO4 (pH '<2) (Cl-)
zX
BP3N-250 mL plastic HNO3 (pH'< 2)
BP3Z-250 mLPlastic`ZN:Acetate & WOH (>9) .
BP30250 m'L.Plastic NaOH. (pH> 12) (Cl-)
WGFU-Wide-mouthed Glass.)ar Unpreserved
AG1U-1 liter Amber Unpreserved (N/A) (CI-)
zzlzzz—z
zzzzzz
AGiH-1 liter Amber HCl (pH < 2)
AG3U2SO mL-Amber Unpreserved (N/A).(CI-)
AGSS-Saiter Amber H2SO4 (pH < 2)'
AG3S-250 mL Amber H2904 (pH <2).
AG3A(DG3A)-250 ml.Amb"er NH4Cl (N/A)(Cl=)
DG9H-40 mL VOA HCl (N/A)
VG9T-40 mL:VOANa2S203 IN/A)
VG9V-40 mL VOA'Unp (N/A)
DG9P-40 mL VOA H3PO4 (N/A)
VOAK (6 Vials per kit)-5035 kit (N/A)
V/GK (3 vlais per kit)-VPH/Gas kit (N/A)
SP5T-125 mL Sterile Plastic (N/A —lab)
SP2T-250 mI.Sterile Plastic (N/A -lab)
BP3A450 mL Plastic(NH2)2SO4 (9.3-9.7)
Cubita)ner
VSGU 20 mlScintillation vials (N/A)
GN
W N fCD
O M
N CO.
O I
X v�i
N • S
C) �
m
N A
rt M
V
Cr
� rD
-w
Cr m
O
rD �
VA

LO
a er �omass -Wood
B:oiler.A,sh:-Ricky Styles
LO
a
Please .t . .. :.
test the sam le s for the :parameters as
P � .)
listed below:
Send original results to: email: ricky_styles@baiter' com
-Send invoice -and .copy of results -to:
email: ricky_styles.@baxter:corn
Ricky Styles
Baxter Biomass.
Purchase Order # 155314
2859:OId.Linville Rd:
Marion, NC 28752
[phone] ..
3 73a
Requested:®ue: Da tec 10/16120.1
m'7 SaIe ALL.LISTED'
Sample.
Sample_
Sample Date(s) .
: Grab: or:,Total
°Metals -
TCLP. Metals.
Ignitability
pH .
Total -Arsenic
Full TCLP .
Description
and time sample
Composite
As,'Ba, Cd,
As, Ba;.Cd,'
Reactivity
Corrosivity
collected .
Ca; Cr; Cu, Fe,
Cr,:Qb, H9,:
P.b; Mg, :H9,- .
.Se; Ag..
Mn
Se, .Ag, Na; Zn;
total.
Phos horus
NP1021,7A.
ASH.
10/2/17 9:45AM
COMPOSITE-
YES`
YES
YES
YES
YES
00�. .
NP1:0217.13
ASH
1.0/2/17 9`45AM
COMPOSITE
YES"...
YES.::
YES
YES"
YES
.002
Sample. sent to,• Pace Analytical Services, Inc.
Project Manager: Torn -Williams
2225 Riverside Drive
98 y Avenue,
Suite<t00.Asheville,
Ki nc_e.
NC 28804:
•
n3
Hur§ille, NC,80738282
.
...
4)54=71:76 (70875_9092e3
Chain of -Custody
f
.• .
r'�

Pace Analytical Services, LLC
acen
GCV Analytical.
9800 KinceyAve. Suite 100
.
www.pacelabs.coni
Huntersville, NC 28078
[phone]-
SAMPLE ANALYTE COUNT
Project: Wood Boiler Ash 12/8
Pace Project No.: 92322611
Analytts .
Lab ID' .: Sample:ID
Method
Analysts
Reported
Laboratory .
92322611001 NP12816A
EPA6010
JMW,SH1
17
PASI-A
EPA6010
SH1
7":.
PASI-A
EPA 7470
-WAB
1
PASI-A
EPA 7471 `.
WAB
1
PASI-.
-ASTM D2974-87
CLW
1 ..
PASI-C
EPA 1010
ALC
1
PASI-A
EPA 9045
KDF1
1
PASI-A
fPA365.1,
MDW
1
PASI-A
EPA.9014
PAS
1
PASI=PA
SM4500S2F-00
PAS :
1.
PASI-PA -
92322611002 NP12816B
EPA 6010
JMW, SH1
17
PASI-A
•
EPA6010
SH1
7
: PASI-A
EPA-7470
WAB
1
PASI-A ..:
EPA7471
WAB.
1 ."
. PASI-A .
:ASTM D2974-87
CLW
1
PASI-C
EPA 1010
ALC
1
PASI-A'
EPA 9045
KDF1
1
PASI-A
EPA365.1.
MDW
1
PASI-A
EPA 9614 '
PAS
1
PASI-PA .
- SM4500S2F-00
� PAS
1
.PASI-PA-
�ECEIVE®
D�irision
of Water Resources
APR" -.2- 2011
...
�pe►atbrls
R�
Asheviffe
REPORT OF.LABORATORYANALYSIS. " .
. This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
page 3 of 23

aceAnalytical
www.pewlabs.coin.
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28018
[phone]
Project: Wood Boiler Ash 12/8
Pace Project No.: 92322611
Sample: NP12816A
Lab ID: 92322611001 Collected:
'12108/16'09:45,
Received: -12/08/16 12:56 Matrix: Solid
Results reported on a "dry weight' bails and are adjusted for percent moisture, sample size and any dilutions.
Parameters.
Results Units: Report Limit _ DF
Prepared
Analyzed
CAS No. Qua!
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
6.6 mg/kg
0.99 1
12/11/16 12:30
12/12/16 23:26
7440-38-2
Barium
1510 mg/kg
5.0: 10
12/11/16 12:30
12/13/16 14:45
7440-39-3
Cadmium
1.2 mg/kg
0.099 1
12/11/16 12:30
12/12/16 23:26
7440-43-9
Calcium
91400 mg/kg
99.5 10
12/11/16 12:30
12/13/1614:45
7440-70-2
Chromium
30.2 mg/kg
0.60 1
12/11/16 12:30
12/12/16 23:26
7440-47-3
Copper
119 mg/kg
0.50 1
12/11/16 12:30
12/12/16 23:26
7440-50-8
Iron
13206 mg/kg
99:5 10 •
12/11/16 12:30
12/13/16 14:45
7439-89-6
Lead
23:1 mg/kg.
0.50- 1
12/11H612:30
12/12/16 23:26
7439-92-1
Magnesium .
16800 mg/kg
99.6 10
' 12/11/16 12:30
12/13/16 14:45
7439-95-4 -
Manganese
3030 . mg/kg
5.0 10
12111/1612:30
12/13/1614A5.7439-96-5
Molybdenum
0.99 mg/kg ..
0.50 1
12/11/16 12:30
12/12/16 23:26-
7439-98-7
Nickel
20.0 .. mg/kg
0.50 . -1
12/11/16 12:30
12/12/16 23:26
7440-02-0
Potassium ..-
14000 mg/kg ., ,'
4970 10
12/11/1612:30
12/1311614:46
7440-09-7
Selenium .
ND ' . , mg/kg
0.09 1
12/11/16 12:30
12112116 23:26
7782-49-2 .
Silver
ND mg/kg ..
0.50 1
12/11/16:12:30
12/12/16 23:26
7440-22-4
Sodium'.
4510 mg/kg
49.7 1
12/11116 12:30
12/12/16 23:26
7440-23-5
Zinc
189 mg/kg
0:99 1
12/11/16 12:30 _
12/12/16 23:26
7440-66-6
6016 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 30104
Leachate Method/Date: EPA 13.11; 12/09/1615:00_ Initial- PH` 10:3; Final
pH: 4.8
Arsenic
ND mg/L . -
0.650. 1.
12/12/16 15:47
12/13/16 11:47
7440-38-2
Barium
12.1 V. mg/L
0.25 1 ,
12/12116 15:47
12/13/16 11:47
7440739-3
Cadmium
0.019 mg/L
0.0050, 1.
12/12116 15;4Z
12113/.16 11.:47
7440 43=9 .
Chromium
ND mg/L
0.050 1
:12/12/1.6 15:47
12/13/16 11:47
7440-.
Lead
0.16 m9/L
0.025. 1
12)1211615:47
12113/16 11:47
7439-92-1
Selenium
ND V. mg/L •
0.10.. 1
12/12/16 15:47.
12/13/16 11:4.7
7782-49-2
Silver
ND V mglL ..
0.025 1
12/12/16.15:47
12/13/16.11:47
7440-22-4
7470 Mercury, TCLP
Analytical Method: _EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/09/16 15:00 Initial pH: 10.3; Final pH: 4.8
Mercury
ND mg/L
0.00020 1
12/13/16 07:35
12/13/16 13:54
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method- EPA 7471
Mercury
0.019 mg/kg
0.0095 1
12/13/16 03:50
12/13/16 16:45
7439-91-6 L2
Percent Moisture
Analytical Method: ASTM,D2974-87
Percent Moisture
40.9 %
0.10 1
112/12f*07:,36,5 r t
a
1070 Flashpoint,Clo'sed Cup --
:Analytical Method: EPA 1010
l
Flashpoint .
>200 deg f
70.0 1
i 12, 3/16' 09:45,, rf
9646. pH Soil
Analytical ,Method: EPA 9045
R
pH at 25.Degrees C
. 16.3 Std. Units
0.10 1
L9Nii'i� 6�il t+fi, i'-)T �r,'A�f1i: :.Rtli[+=P.*vam+`I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2016,07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 4 of 2:

Pace Analytical Services, LLC
®
acemalytical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pm1ab&com
[phone].
ANALYTICAL RESULTS
Project:Wood Boiler Ash 12/8
Pace Project No.: 92322611
Sample: NP12816A
Lab ID: 92322611001 Collected: 12/08/16 09:45 Received: 12/08/16 12:56 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed
CAS No. Qual
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
1710 mg/kg 84.6 25 12/17/16 00:21
7723-14-0
733C S:Reactive Cyanide
Analytical Method: EPA 9014. Preparation Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg 1.7 1. 12/13/16 15:18 12/14/16 00:16
734S Reactive Sulfide
Analytical Method: 8M4500S2F-00 Preparation Method: SW-846 7.3.4.2
Sulfide, Reactive,
ND mg/kg 16.9 1 12/13/16 15:18 12/13/16 22:14.
REPORT OF LABORATORY ANALYSIS
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Date: 12/1,7/2016 07:33 AM
without the written consent of Pace Analytical Services, LLC.
Page 5 of 23

aceAnalytical
ww .pece/ebs.com...
Pace Analytical $erVlces, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Wood Boiler Ash 1218
Pace Project..No.: 92322611 .
Sample: NP128166
Lab ID; 92322611002 Collected:
12/08/16 09:45
"Received: 12/08/16 12:56 Matrix: Solid
Results reported on a "dry weight® basis and are adjusted for percent moisture, sample size and any dilutions:
Parameters "
Results _ Units ReportLimit DF.
Prepared
Analyzed.. "
CAS No. Qual "
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
6.3 : mg/kg
1.4 1-
12111116 12:30
12/12/16 23:30
7440-38-2 .
Barium
1540 .. 'mg/kg
6.8: 10
12/11/16 12:30
12/13/16 14.48
7440-39-3'
Cadmium
1.0 mg/kg
0.14 1
12/11/1612:30
12/12./162130
7440-43-9
Calcium,
83300 :. mg/kg
136 10
12111/1612:30
12113/1614:48.
7440-70-2
Chromium
21.2 mg/kg
0.68 1
12111/16 12:30
12/12/16 23:30
7440-47-3
Copper,
87.8 mg/kg
0.68 1
12/11/16 12:30
12/12/16 23:30
7440-50-8
Iron
15200 . mg/kg
136 10
12/11/16 12:30
12/13/1614:48
7439-89-6
Lead
22.6 mg/kg :
0.68 1
12/11/16 12:30
12/12/16 23:30
7439-92-1
Magnesium
16000 mg/kg
136 10
12/11/16 12:30 ,12/13/16
14:48
7439-95-4
Manganese
3160 .. mg/kg
6.8 10.
12/11/16 12:30
12/13/16 14:48
743979675
iVlolybdenum
1.1 mg/kg -
0.68 1-
12/11/16 12:30
12/12/16 23:30
7439-98-7
Nickel
19.1 " = mg/kg
0.68 _ 1
12/11/16 12:30
12/.12/16 23:30
7440-02-0
Potassium.
16600 mg/kg
6780 -10
12/11/16 12:30
12/13/16 14:48
7440-09-7.
Selenium :
ND mg/k'
1.4 1:
12/11/16 12:30
12/12/16 23`.30
7782-49-2'
_
Silver
.
ND mg/kg
0.68 1
12/11/16 12:30
12/12/16 23:30
7440-22-4
Sodium
4930 mg/kg.
678 1
12/11/16 12:30
12/12/16 23:30
7440-23-5
Zinc
187 mg/kg
1.4. 1
1V11/1612:30-_12/12/1623:30
7440-66-6
6010 MET ICP; TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010A .
Leachate Method/Date: EPA 1311; 12/09/16 15:00 Initial pH; 10.3.; Final
pH: 4A.
Arsenic .:
ND. 'V mg/L
0.060 1
12/12/16 15:47
.12/13/16 12:00
7440-38-2
Barium
11.7 v mg/L
0.25 • 1
12/12/.16 15:47
12/13/16 12:00
7440739-3
Cadmium .
0.019 -V mg/L
0.0056 1
12/12/1615:47.12/1311612:00
7440-43-9
Chromium
ND V mg1L_ -
0.050 1
12/12/16 15:47
.12/13/16 12:00
7440-47-3
Lead
0.034 ✓ :mg/L
.0.025 1. 1.
12/12/16
12113/1.612:00
7439-92-1
Selenium
ND. v mg/L
0.10 1
1211211615:47
12/13/.1612:00
7782-49-2
Silver :
ND :V .mg/L _
0.025 1
12/12/16 15.47
12/13/16 12:00
7440-22-4
7470 Mercury; TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311- 12/09/16 15:00 Initial pH: 10.3; Final pH: 4.8
Mercury-
ND mg/L
0.00020 1
12/13/16 07:35
12/13/16 13:57.
7439-97-6
7471 Mercury
Analytical Method: EPA7471 Preparation Method: EPA7471
.Mercury
NDmg/kg
0.0056 1
12/13/16 03:50
12/13/16 16:47
7439=97-6 L2
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
40.5 %
0.10 1
12/12/16 07:36
1610 Fiashpoint,Closed Cup
'Analytical Method: EPA 1010
Flashpbint
>200 deg F
70:0 1
12/18/16 09:45
0045 pH Soil
Analytical Method: EPA 9045- ,
pH. at 25 Degrees G
16.2 Std. Units
0.10 1
12/14/16 10:39
H1
• REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2016 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 6 of 21'

Pace. Analytical Services, LLC
®
acemalxical
9800 KinceyAve. Suite 100
Huntersville . NC 28078
www.pawlabsxam(704)875-9.092
ANALYTICAL RESULTS.
Project. Wood Boiler Ash 12/8
Pace Project No.: 92322611
Sample:- N012816B
Lab ID: 92322611002 Collected: 12/08/16 09:45 Received: 12/08/16 12:56 Matrix: Solid .
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results :. Units Report Limit DF Prepared Analyzed .
CAS No. Qual .
365.1 Phosphorus, Total
Analytical. Method: EPA365.1
Phosphorus
1640 mg/kg 84.0 25 • - 12/17/16 00;22
7723-14-0
733C S Reactive Cyanide
Analytical Method:.EPA 9014 Preparation Method: SW-846 7.3.3.2
Cyanide, Reactive
ND : mg/kg 1.7 1 12/13/16 15:18 12114/16 00:17
734S Reactive Sulfide
Analytical Method: SM4500S2F-00 Preparation Method: SW-846 7.3.4.2
Sulfide, Reactive
ND .. mg/kg 16.8 1. 12/13/16 15:18 12/13/16 22:14
i
REPORT OF LABORATORY ANALYSIS .
This report shall not be reproduced, except in full,
Date:.12117/2016 07:33 AM _ . '
without the written consent of Pace Analytical Services, LLC.
Page 7 of 23

aceAnalytical
www.pacelabs.com. .
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/8
Pace Project No.: 92322611
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 340527
Analysis Method: EPA 7470
QC Batch Method: EPA 7470
Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92322611001, 92322611002
METHOD BLANK: 1888636
Matrix: Water
Associated Lab Samples: 92322611001, 92322611002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mg/L
ND 0.00020
12/13/1616:37
LABORATORY CONTROL SAMPLE: 1888637
Spike. LCS
LCS % Rec
Parameter. Units
Conc. Result
% Rec Limits Qualifiers
Mercury mg/L
.0025 0.0021
84 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1888638 1888639
MS MSD
92321829001
Spike Spike MS
MSD. MS MSD % Rec
Parameter _ . Units . Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND
.0025 .0025 0.0020
0.0.020 72 72 75-125 1 M1
Results presented on this page are In the units Indicated by the "Units" column oxcept whom an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2016 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 2;

Pace Analytical Services, LLC
®
aceAnalytica!
9800,KinceyAve. Suite100
Hunter;ville, NC28078
wwwpecelabs:com
[phone] .
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/8
Pace Project No.: 92322611
QC Batch: 340265
Analysis Method: EPA 7471
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 92322611001, 92322611002
METHOD BLANK: 1887476
Matrix: Solid
Associated Lab Samples: 92322611001, 92322611002
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Mercury mg/kg
ND 0.0060 12/13/1615:14
LABORATORY CONTROL SAMPLE: 1887477
Spike LCS LCS % Rec.
Parameter Units
Conc. Result . % Rec Limits -Qualifiers .
Mercury mg/kg
.083 .004J 5- 80-120 LO
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: ..1887478 1887479
MS MSD
92322580005
Spike Spike MS MSD MS MSD
% Rec
Parameter. Units Result
Conc. Conc. Result Result : % Rec % Rec
Limits. RPD Qual
Mercury, mg/kg 0.020
.056 .056 0.061 0.066 73 81
75-125 7 M0.
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 12/17/2016 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 23

(�'MeAnalytcalo
w ww.pamlabs.com
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/8
Pace Project No.: 92322611
QC Batch: 340116 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 92322611001, 92322611002
METHOD BLANK: 1886477 Matrix: Solid
Associated Lab Samples: 92322611001, 92322611002
Pace Analytical SerWces, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone],
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Arsenic
mg/kg
ND
1.0
12/12/16 22:25
Barium
mg/kg
ND
0.50
12/12/16 22:25
Cadmium
mg/kg
ND
0.10
12/12/16 22:25
Calcium
mg/kg
ND
10.0
12/13/1614:21
Chromium
mg/kg
ND
0.50
12/12/16 22:25
Copper
mg/kg
ND
0.50
12/12/16 22,25
Iron
mg/kg
ND
10.0
12/12/16 22:25
Lead
mg/kg
ND
0.50
12/12/16 22:25
Magnesium
mg/kg
ND
10.0
12/12/16 22:25
Manganese
mg/kg
ND
0.50
12/12/16 22:25
Molybdenum
mg/kg
ND
0.50
12/12/16 22:25
Nickel
mg/kg
ND
0.50
12/12/16 22:25
Potassium
mg/kg
ND
500
12/12/16 22:25
Selenium
mg/kg
ND
1.0
12/12/16 22:25
Silver
mg/kg
ND
0.50
12/12/16 22:25
Sodium
mg/kg
ND
500
12/12/16 22:25
Zinc
mg/kg
ND
1.0
12/13/1614:21
LABORATORY CONTROL SAMPLE:
1886478
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Arsenic
mg/kg
50
49.3
99
80-120
Barium
mg/kg
50
50.7
101
80-120
Cadmium
mg/kg
50
50.8
102
80-120
Calcium
mg/kg
500
555
111
80-120
Chromium
mg/kg
50
53.9
108.
80-120
Copper
mg/kg
50
50.3
101
80-120
Iron
mg/kg
500
520
104
80-120
Lead
mg/kg
50
51.4
103
80-120
Magnesium
mg/kg
500
522
104
80-120
Manganese
mg/kg
50
63.7
107
80-120
Molybdenum
mg/kg
50
53.5
107
80-120
Nickel
mg/kg
50
50.9
102
80-120
Potassium
mg/kg
500
506
101
80-120
Selenium
mg/kg
50
50.8
102
80-120
Silver
mg/kg
25
25.9
104
80-120
Sodium
mg/kg
500
507
101
80-120
Zinc
mg/kg
50
56.0
112
80-120
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2016 07:33 AM without the written consent of Pace Analytical Services, LLC_
Page 10 of 23

Pace Analytical Services, LLC
aceAng1j cal
9800 KlnceyAve. Suite 100
Huntersville,
NC 28078
WWW-PacelabS.cwn
. •
875 9092-
QUALITY CONTROL DATA
Project: Wood Boiler
Ash 1218
Pace Project No.: 92322611
`
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1886479
1886480
MS
MSD
92321770002
Spike
:Spike
MS
MSD'..
MS
MSD
% Rec
Parameter
Units
Result
Conc..
Conc..
Result .
Result
% Rec
% Rec -
Limits RPD Clual :.
Arsenic
mg/kg
49.8
33.8
32.9.
60.2
72.6
31
69
75-125
19 -Ml
Barium
mg/kg
114
33.8
32.9
101
83.0
-40
-95
75-125
19 -Ml
Cadmium
mg/kg
0.68
33.8
32.9
32.2
32.7
93
97
75-125
2
Calcium
mg/kg
10800
338
329
7060
7700
-1100
-931
75-125
.9 M1
Chromium
mg/kg
1.3
33.8
32.9
35.9
36.1
103
106
75-125
1-
Copper
mg/kg
0.85
33.8
_ 32.9
33.5
34.0
97
101
75-125
2
Iron
mg/kg
1110 -
338
329
1310
1300
59
57
_
75-125
1 M1
Lead
mg/kg
5.8
33.8
32.9
36.4
37.2
91
95
75-125
2
Magnesium
mg/kg
612
338
329
752
789
41
54
75-125
5 M1
Manganese a
mg/kg
37:9..
33.8.
32:9
66.5
67.4
85
90
75-125
1
Molybdenum
mg/kg
ND
33.8
32.9.
32.9
33.4
97
161
75-125
2
Nickel r
mg/kg
0.81
33.8
32.9
30.8
31.4
89
93
75-125
2
Potassium
mg/kg
793
338
329.
896
780
30
-4
'75-125
14 M1
Selenium
mg/kg
1.3
33.8
32.9
31.7
31..9
90
93
75-125
1 .
Silver
mg)kg
ND
16.9
-16.4
16.7
16.8
- 98
101
75-125
1
Sodium
mg/kg
21800
- 338
329
13000
8560
-2610
-4020
75-125
41.M1,111
Zinc
mg/kg
5.7
33.8-
32.9
39.6
41.7
- 100
110
75-125
5 '
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS.
This report shall
not be reproduced, except in full,
Date: 12/17/2016 07:33 AM
without the written consent of Pace Analytical Services, LLC.
Page 11 of 23

aceAnalytical
www.pacelabs.com... .
QUALITY CONTROL DATA
Project: Wood Boiler Ash 1218
Pace Project No.: 92322611
QC Batch: 340468 Analysis Method: EPA 6010
QC Batch Method: EPA 3010A Analysis Description: 6010 MET TCLP
Associated Lab Samples: 02322611001, 92322611002
METHOD BLANK: 1888347 Matrix: Water
Associated Lab Samples: 92322611001, 92322611002
Parameter Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
LABORATORY CONTROL SAMPLE: 1888348
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
0.050
12/13/1611:25
ND
0.25
12/1311611:25
ND
0.0050
12/13/1611:25
ND
0.050
12/13/1611:25
ND
0.025
12/13/1611:25
ND
0.10
12/13/16 11: 25
ND
0.025
12/13/1611:25
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter
-
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/L
2.5
2.5
99
80-120
Barium
mg/L
2.5
2.4
96
80-120
Cadmium
mg/L-
2.5
2.5
98
80-120
Chromium
mg/L
2.5
2.4
98
80-120 .
Lead
mg/L
2.5
2.3
93
80-120
Selenium
mg/L
2.5
2.5
100
80-120
.Silver
mg/L
1.2
1.2
99
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1888349
1888350
MS
MSD
92321829001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD _ Qual
Arsenic
mg/L
ND
2.5
2.5
2.7
2.6
107
104
75-125
3
Barium
mg/L
0.37
2.5
2.5
3.0
2.9
106
102
75-125
4
Cadmium
mg/L
ND
2.5
2.5
2.6
2.6
105
104
75-125
1
Chromium
mg/L
ND
2.5
2.5
2.6
2.6
105
102
75-125
3
Lead
mg/L
ND
2.5
2.5
2.5
2.5
99
97
75-125
2
Selenium
mg/L
ND
2.5
2.5
2.7
2.7
107
107
75-125
1
Silver
mg/L
ND
1.2
1.2
1.3
1.3
106
103
75-125
2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2016 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 22

;8C
Pace Analytical Services, LLC
Q n ®
al
9800101ceyMe. Suite 100
uAI j6cal
Huntersville, NC 28078
wwtvpa I.abs.com
(704)$75-9092
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/8
Pace Project No.: 92322611
QC Batch: 340158
Analysis, Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture .
Associated Lab Samples: 92322611001, 9232261.1002
SAMPLE DUPLICATE: 1686637
35280739001_ Dup
Parameter
Units Result' Result RPD Qualifiers
Percent Moisture
% 28.0 34.6 21
SAMPLE DUPLICATE: 1886638
92322663002 Dup
Parameter..
Units Result Result RPD Qualifiers
Percent Moisture
% 91.0 91.01 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF. -LABORATORY ANALYSIS = .
This report shall not be reproduced, except in full,
Date::12/17/2016 07:33.AM
without the written consent of Pace Analytical Services, LLC.
Page 13 of 23

Pace Analytical Services, LLC
/�.,
® 9800 KinceyAve. Suite 100
acemaIx l Huntersviile, NC 280T8
wwwpacelebs.com .. [phone] , .
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/8
Pace Project No.: 92322611
QC Batch: 340576 Analysis. Method: EPA 1010
QC Batch Method: EPA 1010 Analysis Description: 1.010 Flash Point, Closed Cup
Associated Lab Samples: 92322611001, 92322611002
SAMPLE DUPLICATE: 1888791 "
92322848001 Dup
Parameter Units Result Result RPD Qualifiers
Flashpoint deg F >200 >200
Results presented on this page are in the units Indicated by the "Units" column except whirs an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS .
This report shall not be reproduced, except in full,
Data: 12/17/2016 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 14 of 2f

acemal Cal
www.pacelsbs,com
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/8
Pace Project No.: 92322611
QC Batch: 340621 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92322611001, 92322611002
SAMPLE DUPLICATE: 1889166
92322440001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 8.1 8.1 0 H1
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2016 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 23

Pace Analytical Services; LLC
®
aceAnaJyt 0
9800 Kincey Ave. Suite 100
Huntersville, NC 280T8
wwwpacelabs.com ..
[phone]
QUALITY CONTROL DATA
Projecti Wood Boiler Ash 12/8
Pace Project No.: . 92322611
QC Batch: - 341108, Analysis Method: EPA 365.1 "
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus,: Total
Associated Lab Samples: 92322611001; 92322611002
METHOD BLANK: 1892404 Matrix: Solid
Associated Lab Samples: 92322611001, 92322611002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND . 2.0 ':12/17/16 00:16
LABORATORY CONTROL SAMPLE: 1802405
Spike LCS LCS % Rec
Parameter Units Cone. Result "/o Rec Limits Qualifiers
Phosphorus mg/kg 50 53.6 107 90-110
MATRIX SPIKE'& MATRIX SPIKE DUPLICATE: 1892406 1892407
MS MSD.
92322119001 Spike Spike MS MSD, MS . MSD
% Rec
Parameter Units_ - Result Cone. Cone. _ Result". Result "/o Rec % Rec
Limits RPD Qual.:
Phosphorus mg/kg 5820. 69.4 69.4 9460. . 8920 2000 " 1220-
90-110 6 M6:
Results presented on this page are In the units Indicated by the "Units" column excopf whete.an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS .
This report shall not be reproduced, except in full,
bate:,12/17/2016 07:33 AM without the written consent of Pace Analytical Services, LLC:
Page 16 of Z

aceftlj cal
tmwpacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/8
Pace Project No.: 92322611
QC Batch: 243209 Analysis Method: EPA 9014
QC Batch Method: SW-846 7.3.3.2 'Analysis Description: 733C Reactive Cyanide
Associated Lab Samples: 92322611001, 92322611002
METHOD BLANK: 1196356 Matrix: Solid
Associated Lab Samples: 92322611001, 92322611002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide, Reactive mg/kg ND 1.0 12/14/16 00:13
SAMPLE DUPLICATE: 1196357
30205148001 Dup
Parameter Units Result Result RPD Qualifiers
Cyanide, Reactive mg/kg ND ND
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2016 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 17 of 23

aceAnalytical
www.paeelebs.com .
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28018
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/8
Pace Project No.: 92322611
QC Batch: 243211 Analysis Method: SM4500S2F-00
QC Batch Method: SW-846 7.3.4.2 Analysis Description: 734S Reactive Sulfide
Associated Lab Samples: 92322611001, 92322611002
METHOD BLANK: 1196360 Matrix: Solid
Associated Lab Samples: 92322611001, 92322611002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfide, Reactive mg/kg ND 10.0 12/13/16 22:14
SAMPLE DUPLICATE: 1196361
Parameter
Sulfide, Reactive
30205148001
Units Result
mg/kg ND
Dup
Result RPD Qualifiers
ND
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2016 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 2:

Pace Analytical Services, LLC
acekdytkal a 9800 KlnceyAve. Suite 100
Huntersville, NC 28078
mvwpacelabs.com [phone]
QUALIFIERS
Project: Wood Boiler Ash 12/8
Pace Project No.: 92322611
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A
Pace Analytical Services -Asheville
PASI-C
Pace Analytical Services - Charlotte
PAST -PA
Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M 1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 12/17/2016 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
980014nceyAve. Suite 100
Huntersvilie, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Wood Boiler Ash 12/8
Pace Project No.: 92322611
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92322611001
NP12816A
EPA 3050
340116
EPA 6010
340359
92322611002
NP12816B
EPA 3050
340116
EPA 6010
340359
92322611001
NP12816A
EPA 3010A
340468
EPA 6010
340487
92322611002'
NP12816B.
EPA 301 OA
340468
EPA 6010
340487
92322611001
NP12816A
EPA 7470
340527
EPA 7470.
340561
92322611002
NP12816B
EPA 7470
340527
EPA 7470.
340561
92322611001
NP12816A
EPA 7471
340265
EPA 7471
340536
92322611002
NP12816B
EPA 7471
340265
EPA 7471
340536
92322611001
NP12816A
ASTM D2974-87
340158
92312611002
NP12816B
ASTM D2974-87
340158
92329611001
N012816A
EPA 1010
340576
92322611002
NP12816B
EPA 1010
340576
92322611001
NP12816A
EPA 9045
340621
92322611002
NP12816B
EPA9045
340621,
92322611001
NP12816A.
EPA 365.1
34.1108 .
92322611002
NP12816B
EPA 365.1
341108
92322611001
NP12816A
SW-846 7.3.3.2
243209
EPA 9014
243293
92322611002
NP12816B
SW-846 7.3.3.2
243206
EPA 9014
243293
92322611001
NP12816A
SW-846 7.3.4.2
243211
SM4500S2F-00
243289
92322611002
NP12816B
SW=846 7.3.4.2
243211
SM4500S2F-00
243289
Date: 12/17/2016 07:33 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
withbut the written consent of Pace Analytical Services, LLC.
Page 20 of 2c

Document Name:
Sample Condition upon Receipt(scuk)
Document No.:
F=CAR-CS-0921-kev.01
Document Revised'.
Page 1 c
Issuing A4—tl
211 2'016
Laboratory, recejving,said OIL is:
AshevIllep EdenEl
Greenwood [] Huntersville 1:1
RaliiighEl
MinhanksVillel
Sample Condition Upbn
RecgipName:
Client Name:
Project WO# :
9232261 1
--ourier:
C
Ded Ex —10PS EIUSOs
E
Client
❑ commercial
Op� ace 0Other:
02322611
Custody Sea! Present?
E]Yes Seals Intact? []YO
JIN
Packirig-Matetial:
[]Bubble. Wrap []Bubble gags IBNone
Datb/lnitlals
[]Other:
Person Exeimining Contents
Thermometer:
12*346 16:
[1wet 13[ilue J�Bilrone
r-- S
amplin on Ice, coolin g process has beg
Type of Idei
Correction factor:
Cooler. Temp Corrected (,C)
Biological Tissue Frozen? FiYe.s E]No 2NIA
Temp should be above freezing to 6 C.
om Regulated'Soll N/A, Water simple)
Did s ' apriples 0 igiriate in a quarantine zone within the United States: CA, NY, or k (check maps)? Did samples orli I in ate from a to 0 '8 foreign (internationally,
Myes samples
A ... 41.� U--... '.J IN.MS Mv— CUT;:
C I d m-ments/Discrepancy:
Chain of ustody present?
-134s"
ONO,
EIN/A
-I.
Samoles-ArtIved within Hold Time?
Ls
[:]No
[]N/A
-2.
Short Hold Time Analysis,. Olhir.)?
[]Yes
Jallo
[]N/A
1
Rush Turn Around Time Requested?
ElVes
'ONG
[IN/A
4,
Sufficient volurrie?
. Yes
[314o,
EIN%A
S..
Corrkt.Containers Used?
-Pace'Containers Used?
IDYet
OYes
Oft
E39.
[]NIA
ON/A
-6.
Containers Intact?
-21' res.
EINo.
EINIA
7.,
Samples Field Filtered?
Mes
ONo
bWg-
'& Note if sediment is Visible in the dissolved container
Sample Labels Match tot?
-Includes Date/Time/ID/Analysis
6.e,
Matrix:
❑N'o'
-EINIA
'9.'
HeqdsOce In VOA ViaN.(>5;-6Mm)?
. E]Yes
EIN,,
8-N/A
10.
Trip Blank Present?
Trip, Blank. Custody Seals. Oresent1
ElYes
I byes
EiNo
ONo
�N
M/'A
11:
CLIENT NOTIFICATION RESOLUTION
Person Cohtd.ded:
.p6rdrilibfits/Sample
Discrepancy;
Project Manager SCURF Review.
pirOjOct w Manager SRF Revie
Date/Time;
bate:
Date:
Field Data. Required? []Yes []No
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DENO Certification Qffice (Le
Out of hold, incorrect preservative, out of temp, incorrect containers.)
Page 21 of 23

Docurrieht Name:
Document No.:
nt Revised:'5ept. 21, 2016
Page 2 of 2
Issuing Authority:
*Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range for
preservation.samples,
**Bottom half of box is to list number of bottles
Project $ Wa# ■ 92322611
PM: CDl Due Date: 12/22/16
CLIENT: 82-Baxter
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pH Adjustment
Log for Preservea sampies
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot#
Sample ID
Page 22 of 2:

Baxter Biomass Wood Boiler Ash - Ricky Styles
Please test the sample(s) for the parameters as
listed below.
Send original results to: email: [e-mail]
Send invoice and copy of results to: email: [e-mail]
Ricky Styles
Baxter Biomass Purchase Order # 125535
2859 Old Linville Rd.
Marion, NC 28752
[phone]
Ranntiaetarl n1la nthta.
Ramnla Al 1 1 IRTi=n
q;L. 3.26.1 (
Sample #
Sample_
Sample Date(s)
Grab or
Total Metals -
TCLP Metals
Ignitability,
pH
Total -Arsenic
Full TCLP
Description
and time sample
Composite
As, Ba, Cd,
As, Ba,. Cd,
Reactivity
Corrosivity
collected
Ca, Cr, Cu, Fe,
Cr, Pb, Hg,
,Pb, Mg, Hg,
S.e,.Ag
Mn; Mo, Ni, K,
Se, Ag,Na,
Zn, total
Phos horus
NP12816A
.ASH
12-8-16 9:45AM
COMPOSITE
YES
YES
YES
YES
NP128168
ASH
12-8-16 9:45AM
COMPOSITE
YES
YES
YES
YES
Sample sent to: Pace Analytical Services,
2225 Riverside Drive
Asheville., NC 28804
828-254-7176
Chain of Custody
Project Manager: Tom Williams
9800 Kincey Avenue, Suite 10C
Huntersville, NC 28078.
(70.4) 875. - 9092 ext. 233'
M
N
0
O
M
N
m
a
a a ;

Pace -Analytical Servlces,'LLC
` aceAnalytical ®
9800 KinceyAve.. Suite 100
Huntersville,
NC 28078
.
www.pawlabs.coln:.[phone]
SAMPLE.ANALYTE COUNT
Project: ASH 6/5.
Pace Project No.: 92342918 .
Analytes
Lab ID Sample ID
Method
Analysts
Reported
:Laboratory
92342918001 SP6217A-
EPA6010 :- -
: SH1
17
PAS[ -A'
EPA6010
SH1.
7
PASI-A
EPA 7470
KAL
1
PASI-A
EPA 7471
WAB
1
PASI-A
ASTM D2074-87
CLW
1
PASI-C .
EPA 1010
MJS1.
1
PASI-A
EPA 9045
MJS7.
1
PASI-A
EPA365.1 .
AES2 _
1
PASI-A
• EPA 9014 ..
PAS
1
PASI-PA' •
•
SM4500S2F-00•
PAS
1-
PASI-PA . .
92342918062 SP6217B:.
EPA6010.
SH1.
17 .
PASI-A.
EPA6010
7
PA$I-A
_
EPA 7470
KAL -
1.
.. . PASI-A
EPA 7471
WAB
1
PASI-A
_
ASTM 02974-87
CLW
1.
PASI-C
EPA 101.0
MJS1
1
- • PASI=A
EPA 9045 ..
MJS1 .
1
PAS[ -A..
EPA365.1
AES2.
1
PASI=A
EPA 9014
PAS
1
PAS[ -PA .
SM4500S2F-00 _
PAS
1
PASI-PA
Division
of Water Resources
APR _ 2
Water 011211 y Regbnw Opetallwa
Asheville R Iona) Offi..
-REPORT-OF LABORATORY ANALYSIS
This report shall not be reproduced; except.In full, -
without the written consent of Pace. AnalyticalServices, LLC:
_Page 3 of 23

aceAnalytcal
wiompaoetabs.cotn
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite.100
Huntersville, NC 2807.8
.(704)875-9o92'
Project: ASH 6/5 .
PaceProject No.: '62342018
Sample: SP6217A Lab ID;:' 92342918001 Collected: 06/65/17 10:45 Received: 061/05/17 13:69- Matrix: Solid
Results reported on. a ."dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters. Results Units. Report Limit . DF Prepared Analyzed CAS No. Qual
6010 .MET ICP. Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 5.8 mg/kg 2.0.. 1 06/06/17.19:55 06/08/1719:16 7440-38-2
Barium 1570' mg/kg 0.98 • . 1 . 06/06/17 19:55 06/08/17 19:16 7440-39-3
Cadmium 2.2 mg/kg 0.20. 1 06/06/17 19:55 06/08/17 19:16 7440-43-9
Calcium, 96800 mg/kg 195 10 06/06/17 19:55 016/09/17 12:03 7440-70-2
Chromium; 19.9 mg/kg 0.98 1 06/06/17 19:55 06/08/17 19:16 7440-47-3
Copper 90.4 mg/kg 0.98 1 06/06/1719:55 06/68/1719:16 7440=50-8
Iron 10300 mg/kg 19.5 1 06/06/17.19:55 06/08/17 19:16 7439-89-6
Lead 28.3. mg/kg' 0:98 1 06/06/1719:55. 06/08/1719.16 7439-92-1
Magnesium 15200 mg/kg 19:5 1 06/06/17 19:55 '06/08/17 19:16 7439-954
Manganese 3610 .: mg/kg 9.8 10' 06106/1719:55 06/0911712:03 7439-96-5
Molybdenum ND mg/kg 0.98. ; 1 06/06/17-19:55 06/08/17 19:16 7439-98-7
Nickel 22.3 mg/kg 0.98 :1 O6/O6/1719:65 06/08/1719:16 7440-02'-0
Potassium 10000 mg/kg .. 977 1- 06/06/17 - 19:55.06108/171916 7440-09-7
Selenium ND mg/kg 2.0 1 06/06/1719:55 06/0811719,16 7782-49-2
Silver.. ND mg/kg 0.98: 1 06/06/17 19:55 06/08/17 19:16 7440-224
Sodium 3860 mg/kg 971, A 06/0611119`55 06/08/17 19:16 7440-23-5
Zinc .' 274 mg/kg 2.0.. 1 06/06/1710:55 06/0811719:16 7440-66-6
6010 MET ICP, TCLP_ . _ Analytical Method:. EPA 6010 'Preparation Method: EPA 3010A .
Leachate Method/Date: EPA 1311; 06/06/17 21:30. Initial pH: 10.22; Final pH: 5.36
Arsenic ND ✓ ` mg/L 0.050' . ; 1 06/07/1716:40 06l08117 19:38 7440-38-2
Barium ... 7.6 % mg/L 0.25 1 06/07/17 16:40 06/08/17 19:38 7440-39-3
Cadmium 0.015 V mg/L 0.0050 1 06/07/1716:46 06/08/1719:38 7440-43-9
Chromium ND V .mg/L 0,050 1 06/07/17 16:40 06/06/17 19:38. 7440-47-3
Lead ND mg/L 0.025 1 06/07/1716:40. 06/08/1719:38 7439=92-1
Selenium ND-/ mg/L 0:10 1.:: 06/07/1716:40: 06/0811719:38 778249-2 .
Silver =:. ND ✓ mglL 0.025:: 1 06/07/1716AQ 06/08/1719:3.8 7440-22-4
7470 Mercury, TCCP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 06/06/17 21:30 Initial pH: 10 22; Final. pH: 5.36 -
Mercury ND -mg/L 0.00020 1 06/07/17 17:55 06/09/17 00:40. 7439-97-6
7471 Mercury . Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury ND mg/kg 0.013 1 06/07/1714:08 0.610811713:30 7439-97-6
P rcent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 55.9 % 0.10 1 06/08/17 08:08 .._- ._
1010 Flashpoint,Closed Cup Analytical Method: EPA 1010
_.�.y: �- :_,gib ��, �•. �'k�
Flashpoi s200 deg F 70.0 1 06/14/1.7.18:30 i
9045 pH Soil/ nalytical Method: EPA9045 Oil
�: 1� • 7
pH at 25 Degrees C 9:9 Std. Units 0.10 1 06/14/17 18:40
e
Date: 06/15/2017 08:35
REPORT OF LABORATORY ANALYSIS .
fThis report shall not be reproduced, except in full,
AM without the written consent of Pace.Analytical Services, LLC. Page 4 of 23

:
Pace.Analytical Services; LLC
/+ p,, /+ ®
�lre/`11 !�lxica'
9800:KinceyAve. Suite 100
NC
wwwpacelabs.com. .
.
Huntersville 28078
. (70 4)875-9092 .
ANALYTICAL RESULTS
Project: ASH 6/5.
Pace Project No.: .' :92342918
Sample: SP6217A .
Lab ID: 92342918001, Collected: 06105/1.7 10,45 Received: 06/05/.1713:09 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted forpercent moisture, sample size.and any dilutions.
Parameters
Results. Units Report Limit ' OF Prepared Analyzed .
CAS No. • ' Qual .
365.1. Phosphorus, Total.
Analytical Method:. EPA 365.1
:. Ph' phorus .
3130 mg/kg 231 5U° 06/13/1713:01
7723-14-0
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
\
Cyanide, Reactive
ND mg/kg - 2.3 1. 06/12/17 14:26. 06/12/17 2302
4S Reactive Sulfide
Analytical Method::SM4500S2F-00 .Preparation Method: SW-846 7.3.4.2
Sulfide, Reactive °'
NO mg/kg 22.7 1: .06/12/1714:26 06/12/1721:32
-
-REPORT OF LABORATORY ANALYSIS:.
This report shall not be reproduced, exdept in full,
Date06/15/2017 08:35 AM.
without the. written consent of Pace Analytical Services, LLC.
23
Page 5 of..

aceAnalytical
ivww.pacelabs.com ::
Pace AnaljRical Services, LLC
96001(inceyM6. Suite.100
Huritersville, NC 28078
.. .- [phone]
ANALYTICAL RESULTS
Project: ASH 6/5
Pace Project No.: : 92342918
Sample:: S06217B
Lab ID: 92342918002 Collected:
06/05/17*10:45
Received: 06/05N7 13:09 Matrix: Solid
Results reporied on: 4 ."dry weight"
bas/s and are adJusto for percent moisture, sample size and any dliutlons. -
:. Parameters ..
Results
Units Report Limit
DF
Prepared
Analyzed
CAS .No. Qual.
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic-
4.6
mg/kg
2.0.
1
06/06/1719:55
06108/1719:19
7440-38-2
Barium
A650
mg/kg
6.98
1 .
06/06/17 19:55,
06/08/17 19,19
7440-39-3
Cadmium
2.8...
mg/kg
0.20
1
06/06/17 19:55
06/08/1719:19
7440-43-9
Calcium
82400
mg/kg
98.3 '
5
06/06/17 19:55
0.6/08/17 19:22
7440-70-2
-Chromium
19.6
mg/kg ..
0.98
1
06/06/17 19:55
06/08/17 19:1.9
7440-47-3
Copper.
89.3
mg/kg
0.98
1
06/06/17 19:55
06/68/17 19:19
7440-50-8
Iron
10000
mg/kg
19.7
1
06/0611719:55
06/08/171919
7439-89-6
Lead
26.1
mg/kg
0.98
1
06/06/17 19:55
06/08/1719.19
7439-92-1
Magnesium
14100
mg/kg
19.7
1
06/06/17 19:55
06108/1719:19
7439-954
Manganese
2950:
mg/kg
4.9
5
06/06/17 19:55
06/08117.19,22
7439-96-5
Molybdenum
ND
rrig/kg .
0.98::
1
06/06/17 19.55
06/08/17 19:19
7439-9877
Nickel
22.3
mg/kg.
0.98 r
1
06/06/17 19:55
06/08/17 19:19
7440702-0
Potassium
9480
mg/kg
983.
-1-
66/06/17.19:55.
06/08M7 1909.
7440-09-7
Selenium
ND
mg/kg .
2.0
1
06/06/17 19:55
06/08/17.19:19
778249-2
Silver
ND
mg/kg
0..98 -
1
06/06/17 19:55
06/0811.7 19:19
7440-22-4
Sodium
3650.
mg/kg
983
1
06/66/1719:55
06/0811719:19
7440-215
Zinc
265
mg/kg
2.0
1
06/0611719:55
06/081171919.
744.0-6676
.6010 MET ICP, TCLP
Analytical Method: EPA.6010 Preparation Method: EPA 30.10A .
Leachate Method/Date: EPA 1311; 06/06/17 21:30
Initial pH`. 10.25; Final pH: 5.25
Arsenic ::
ND-V
mg/L
0.050
1
06/07/17 16:40
06/08/17 19:41
7440-38-2
Barium
6:8 V
mg/L
0.25
1
06/07/17 16:40
06/08/17 19:41 -
7440-39-3
--
Cadmium
0.014
mg
0.0050
1
.06/07/1716AID
66/08117.16:41
7440-43-9
Chromium
ND
mg/L
0.050
1
06/07/17 16:40
06/08/17 19:41
7440-47-3
Lead
ND f
mg/L
0.025
1
06/07/17 16:40
06/08/17 19:41
7439-92-1
Selenium
ND V
mg/L
0.10
1-
06/07/17 16:40
06/08/17 19:41
7782-40-2
Silver
ND
riig/L, : :
0.025
1
06/07/17 16:40
06108/17-19:4.1
744042-4
7470 Mercury, 4CLP .
Analytical Method:
-EPA 7470-Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 06/06/17 21:30
Initial pH: 10:25; Final pH: 5.25
Mercury
ND
mg/L
0.00020
1
06/07/17 1755
06/09/17 00:42
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
ND
mg/kg_
0.010
•1
06/07/1714:08,
06/08/1713:33
7439-97-6
Percent Moisture -
Analytical Method: ASTM D2974-87
Percent Moisture
54.6
%.
0.10
-1
06/08/17 08:08
1010 Flasahpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200
deg.F
70 0-
1
06/14/17 18:30
9045 pH Soil
Analytical Method: EPA 9045
pH at 25-Degrees C•
104
Stdr Units
0.10
1-
06/14/17 18:40
Dater 06/15/2017 08:35 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 23

Pace Analytical Services, LLC .
®
aceAnalyt N
9800 Kinsey Ave. Suite 100
HuntersAlle, NC 28078
www.pscelabs.cow. . .-9092.
ANALYTICAL RESULTS
Project:::. ASH 6/5
Pace ,Project No.: 92342918.
Sample:. SP6217B
Lab ID: 92342918002 - Collected: ,06/05/17 10:45 Received: 06/05/17 13:09 . Matrix: Solid.
Results reported on_ a -"dry weight" basis and are. adjusted for percent moisture,. sample size.and any. dilutions... .
Parameters
Results' . Units Report Limit DF Prepared Analyzed
CAS No: Qual
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 .
Phosphorus :
3100 mg/kg . 234 50 06/13/17 13:02
7723-14-0
733C S Reactive Cyanide
Analytical Method: EPA -9014 Preparation Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg . 2.2 1 06/1211714:26 06/12/17 23:04
.
734S-Reactive Sulfide
Analytical Method: SM450052F-00 ;Preparation Method: SW-846 7.3.4.2
Sulfide, Reactive
ND.: mg/kg . 21.9 1 06/12/17 14:26 06/12/17 21.:32
REPORT OF LABORATORY ANALYSIS :
This report shall not be reproduced, except In full,
Date: O6/15/2017 0&96 AM
without the written consentof, Pace Analytical Services, LLC..
Page 7 of 23

Pace Analytical Services, LLC
V.�NI�' �irAl
Kincey Ave. te IGO
OOHun ersvlle, NC128078
www.paml bs.com ..
.
704 8.7
( ) 5-9092
QUALITY CONTROL DATA
Project: ASH 6/5
Pace Project No.: 92342918
-QC Batch: 363845
Analysis Method: EPA 7470
QC Batch Method: EPA 7470
Analysis Description: 7470 Mercury TCLP
Associated Lab.Samples: 92342918001,
92342918002
METHOD BLANK: 2017073
Matrix: Water
Associated Lab Samples: 92342918001,
92342918002
Blank Reporting
Parameter
Units Result Limit Analyzed Qualifiers
Mercury
mg/L. ND 0.00020 O6/09/17 00:25
LABORATORY CONTROL SAMPLE:
2017074 -
Spike LCS LCS % Rec
Parameter
Units Conc. Result % Rec Limits Qualifiers
Mercury
mg/L . .0025 0.0022 87 80-120 .-
MATRIX SPIKE: & MATRIX.SPIKE DUPLICATE:. 201-1075... - 2017076
MS MSD
92341996001 Spike Spike MS MSD MSMSD
% Rec
Parameter
Units Result Conc. Conc. Result_ Result %Rec .. % Rec
Limits RPD Qual
Mercury
mg/L - ND ,0025 .0025 0.0022 0.0022 87 87
75-125 0
Results presented on this page are in the units Indleated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS .
This:reportshall not be reproduced, except in full,
Date: 06/15/2017 08:35 AM
withouFthe written consent of Pace Analytical Services, LLC.
Page 8 of 23

Pace Analytical Services, LLC
aWnalxical
-9800 [dnceyAve. Suite 100
Huntersville, NC 28078
—.p—gabs,com..
(704)t175 9092
QUALITY CONTROL DATA
Project:: ASH 6/5
Pace Project No.: 92342918
QC Batch: - 363761
Analysis Method: EPA 7474
QC Batch Method: EPA 7471
Anal sis Description: 7471 Mercury
y
: Associated Lab Samples: : 92342918001, 92342918002
METHOD BLANK: 2016714
Matrix: Solid
Associated Lab Samples: ` 92342918061,.92342918002 '
Blank . ' Reporting
Parameter
units _ Result . Limit Analyzed. Qualifiers
.
Mercury
:.mg/kg ND 0.0060 06/08/1712:45
LABORATORY -CONTROL SAMPLE:
2016715
Spike LCS LCS ; % Rec
Parameter ..
Units Conc. Result . %.Rec • :.. Limits Qualifiers
Mercury. ..
mg/kg .083, . 0.078 93. 80A20
-MATRIX SPIKE & MATRIX SPIKE DUPLICATE: .2016716 2016717 ' .
-MS - MSD
-
:. 92 342814005 Spike Spike MS MSD MS MSD
% Rec•
Parameter
Units . Result Conc.. Conc. Result Result %. Rec . % Rec - ;;
. Limits RPD ' Qual .
:.Mercury..:.
mg/kg . 0.067 : .054., .05 • -0.10 0.12. 63 111
.75-125 19. M1 . .
Results presented on this page are in the units Indicated by the "Units" -column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced; except in full,. -
Date: 06/15/2017 08:35;AM -
without the written consent of Pace Analytical Services, LLC:.
Page 9 of 23 .

Pace Analytical Services, LLC
Q /�,,r� ®
aCG/`U-lGI�IC�I
9800KinceyAve. Suite'100
Huntersville, NC 28078
wivwpecelabs.com.' .:
[phone]
QUALITY CONTROL DATA
Project:.: ASH 6/5'
Pace Project. No,: 92342918
QC Batch: '. 363585
Analysis Method: EPA 6010
QC Batch Method`. EPA3050
Analysis Description: 6010 MET
Associated Lab. Samples: 92342918001,
92342918002
.METHOD BLANK: 2015716
Matrix: Solid
Associated Lab. Samples: 92342918001, 92342918002
Blank Reporting
Parameter
Units
Result Limit Analyzed
Qualifiers
Arsenic
mg/kg
ND 1.0 0610811717:17
Barium
mg/kg
ND 0.50 ' 06/08/17 17:17
Cadmium
mg/kg
ND 0.10 06/08/17 17:17
Calcium
mg/kg
ND 10.6 06/08/1717:20.
Chromium
mg/kg
ND 0.50 06/0811717:17
Copper
mg/kg
ND 0.50 06/08/17 21:07
:.
Iron
mg/kg
ND 10.0. 06/08/17 21:07
Lead
mg/kg
ND 0.50.06/08/1117::17
Magnesium
mg/kg
ND 10.0 06/08/1717:17
Manganese ":::
mg/kg
ND 0.50 '06/08/17 1717
Molybdenum .
mg/kg
ND 0.50 06/08/17 17:17
Nickel
mg/kg
ND 0.50 06/08/1717:17
Potassium
mg/kg
ND 500 06/08/17 17:17.
Selenium
mg/kg
ND 1.0 06/08/17 17:17
Silver
mg/kg
ND 0.50 06/08/17 17:17
Sodium
mg/kg
ND 500 06/08/17 21:07
Zinc
mg/kg
ND 1.0- 06/08/1717:20
LABORATORY CONTROL SAMPLE:
2015717
Spike LCS LCS.. %.Rec
Parameter
Units
Conc. Result % Rec " " Limits Qualifiers
Arsenic
mg/kg
' 50 46.6 . 93
807-120
Barium
mg/kg .
50 50.6 101
80-120,
Cadmium _
mg/kg .
50 51.0 102
80-120
Calcium
mg/kg
500 526 105
80-120
Chromium
mg/kg _
50 46A 97
80-120
Copper
mg/kg
50 48.4 97
80-120
Iron
mg/kg
500 478 96
80-120
Lead
mg/kg
50 48.9 98
80-120.
Magnesium
mg/kg
Soo 470 94
80-120
Manganese.
mg/kg
50 _ 47.0 94
80-120
Molybdenum.
mg/kg
50 52.0.. 104
86-120
Nickel
mg/kg
50 50.3 101
80-120
Potassium
mg/kg
500 ND- 95
80-120
Selenium
mg/kg
50 49.2- 98
80-120
Silver
mg/kg
25 23.7 95
80-120.
Sodium
mg/kg
500 542 .108
80-120 .
Zinc
mg/kg
50 49.5. 99
807120
Results presented an this page are in the units Indicated by the "Units" column, except where an alternate unit Is presentad to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date:.06/15/2017 08:35 AM
without
the written consent of Pace Analytical Services, LLC.
Page 16 of 23

Pace Analytical Services.; LLC
aceMaocal
s:3 00 MnceyAve. Suite 100
Huntersinlle, NC 28078
. .
www.pacela6s.com.-90
QUALITY CONTROL DATA
Project: ASH 6/5
Pace Project No.: 92342918
MATRIX SPIKE & MATRIX SPIKE DUPLICATE::
2015718
2015119 .
1NS .
MSD .:.
92342494001 Spike .
Spike
MS
MSD
MS
MSD
% Rec
Parameter .
Units
Result Conc.:::
Ccric..
Result
Result
% Rec
% Rec
Limits
RPD :Qual
Arsenic
mg/kg
ND 34.5 ,
32 .'
. 32.7 :
' 30.1-
94
94
75-125
8•
Barium.
mg/kg _
. 3.0 34.5
32
- 37.8
35.4
101
102.
75-125
6
-Cadmium.
mg%kg
ND. - 34.6
32.
35.5
33.1 -
103
103
75-125
7
Calcium
mg/kg
345
320
380
356
106
' 107
75-125
7
Chromium.
mg/kg
0.82 34.5
32 .
35.3-
,.
- 32.9
A0.0.:
100
75-125
. 7
Copper
mg/kg
34.5
32 '.
34.0
31:6
- 98
98
75-126
7
.Iron
mg/kg
345
.320
1290
1490
115
185
75-125
. • 14 M1' .
Lead
mg/kg
0.66 84.5
32
34.5
32.1
98
9a
75-125
- 7
Magnesium
. 9
rb /k
9 9
345
320
370
- 352-1
98
100
- 75-125
5 ... ,
Manganese.
mg/kg ..
34.5.
32
40'.8 .
40.6
92
99.
75-125
1
Molybdenum
mg/kg
34.5
32
36.1 "
33.7
105
105
75-125
•
Nickel ..
mg/kg
34.5
32
35.3
33.0.
102
102
..75-126.
7
Potassium
mg./kg. ° .
345.'
.. 320
:. : 371
356.
97 ..
'100-
75-125
. 4 . = ::
Selenium .
mg/kg
ND . 34.5.
32'
34.2
31.5.
99,
98
75-125
. 8.:
Silver.
mgNg
ND 17.2
. 16
16.6
15.4
96
96
'75A25.
8.. '
..Sodium,
mg/kg.
345...
320
321J'
298J
93
93
75-125
Zinc
mg/kg
. 34.5
32--
35.6
33.5
161
102
75-125
6" - .
Results presented on this page are In the units Indicated by the "units" column except where an alternate unitis presented to the, right of the result.
REPORT OF LABORATORY ANALYSIS
.:.
This report shall
not be reproduced, except In full,
Date: 06/15/2017 08:35 AM
without the written co.nient of Pace Analytical Services, LLC,
Page 11 of 23

Pace Analytical Services, LLC
®
ace.Anapical
.9800 KinceyAve. Suite 100 .
Huntersville, NC 28078
MW..Pi"labacom
•(704)875-,9092
QUALITY CONTROL DATA
Project: ASH 6/5
Pace Project No.: 92342918
QC Batch: 3638"
Analysis Method: EPA 6016
QC Batch Method: EPA 3010A
Analysis Description: 6010. MET TCLP
Associated Lab Samples: .- 9234291800.1, 92342918002
METHOD BLANK: 2017062
Matriu: Water
Associated Lab.Samples: 92342918001, 92342918002
Blank Reporting
Parameter ,
Units
Result Limit Analyzed
Qualifiers
Arsenic
mg/L
ND 0.050 06/08/1716:01
Barium
mgk
ND 0.25 06/08/1716:01
Cadmium
mg/L
ND 0.0050 06/08/1716:01
Chromium
mg/L.
ND: 0.050 • 66/08/17 16:01
Lead
mg/L
ND 0.025 06/08/1716:01
Selenium
mg/L
ND . 0.10 06/08/17 16:01
Silver-
mg1L
ND : 0.025 06/08/17 16:01
LABORATORY CONTROL SAMPLE:
2017063 ,
-
Spike LCS LCS % Rec.
Parameter
Units.,
Conc. Result % Rec Limits Qualifiers
Arsenic. , •
mg/L
2.5 2.3 94.
80-120
- Barium'
mg/L
2.5 2.3 92
80-120
Cadmium
mg/L
2.5 2.3 93
80-120
Chromium_
mg/L • ,
2.5. 2.4 95
80-120
Lead
mg/L
2.5 2.2 88
80-120
Selenium
mg/L
2.5 2A 96
80-120
Silver
mg/L
1.2 1 2 " _ 95
80-120
MATRIX'SPIKE & MATRIX SPIKE'DUPLICATE: 2017064 2017065
MS MSD.
92341996001
Spike Spike MS MSD MS MSD
% Rec
Parameter
Units Result
Conc. Conc: Result Result % Red % Rec
Limits RPD Qual .
Arsehid
mg/L ND
2:5 2.5 2.5 2.4
98 96
`75-125 3
Barium
mg/L 0.81
2.5 2.5 ill 3.2
98 94
75-125 3
Cadmium
mg/L- ND
2.5 2.5. 2.4 2.4
98 96
75-125 2
Chromium
mg/L 0.0036J .
2.5 2.5 - 2.5 2.4
99 97
. 75-125 2
Lead
mg/L ND
2.5 2.5 . _ 2.3 2.3
92 91
75-125 2
Selenium
mg/L ND
2.5 2.5 2.5 2.5
101 98
75-125 2
Silver
mg/L 0.0050J
1.2 1.2 1.3 1.2 -100
97
75-125 2
Rasults presented on this
page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/15/2017 08:35 AM
without the'written consent of Pace Analytical Services, LLC.
Page 12 of 23

`
e
Pace Analytical Services; LLC
aceAnalytical
9800 Kincey Ave.' Suite 100
xwrw.pace/a6s.coai
.
Huntersville, NC 28078
.
[phone]
QUALITY CONTROL: DATA ..
Project: ASH 6/5
Pace Project No.: 92342918
QC Batch: . ' 363766
Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92342918001,
92342918002
SAMPLE DUPLICATE: ' 2016746
92343148001:_. Dup
'Parameter
Units Result Result RPD - Qualifiers
Percent Moisture
% ..24.1 23.9 1:
SAMPLE DUPLICATE: 2016747
92342918002.. Dup
Parameter...
Units '. Result Result RPD Qualifiers .
Percent Moisture
% 54.6 52.5. 4
Results presented on this paga'are In the units Indicated by the "Units" column except wherean alternate unit Is presented to the right of the result.
REPORTOF LABORATORY ANALYSIS"
This report sha!I not be reproduced, except in full,
Date: 06/1.5/2017 08:35 AM
without the written consent of Pace Analytical Services, LLC.
Page 19 of 23

f
aceAnalytical
www.pacelabs.com
Project: ASH 6/5
Pace Project No.: 92342918
QC Batch: 364601
QC Batch Method: EPA 9045
Associated Lab Samples: 9234291.8001, 92342918002
SAMPLE DUPLICATE: 2021328
QUALITY CONTROL DATA
Analysis Method: EPA 9045
Analysis Description: 9045 pH
92342918001 Dup
Parameter Units Result Result. RPD Qualifiers
pH at 25 Degrees C Std. Units 9.9 10 1
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/15/2017 08:35 AM without the written consent of Pace Analytical Services, LLC.
Page 15 of 23

Pace Analytical Services, LLC
®.
98001QriceyAve. Suite.100
/+
�Ce/'7l ►alxical
Hunfersville, NC 28078
-
www.ga a4s.com
{704)875-9092
QUALITY CONTROL DATA
Project: ASH 6/5
Pace Project No.: 92342918
QC Batch: 364226
Analysis Method:' ' EPA 365 1
QC Batch Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples:. 92342918001, 92342918002
METHOD BLANK: 2019525
Matrix: Solid
Associated Lab Samples: 92942918001, 923429,18002
Blank Reporting
Parameter
Units Result Limit Analyzed Qualifiers
Phosphorus .
mg/kg ND' 2:0 06/13/17 12:25
LABORATORY CONTROL SAMPLE:,
2019526
Spike :LCS LCS % Rec.
Parameter
Units Cone. Result %Rec Limits Qualifiers
Phosphorus
mg/kg 50 51.3 103 90-110
MATRIX SPIKE & MATRIX SPIKE.DUPLICATE: '- 2019527 2019528,
MS MSD
92343026001 Spike Spike MS MSD MS MSD
% Rec
Parameter
Units Result Cone. Cone. Result Result'," % Rec - % Rec
Limits RPD Quad
Phosphorus .
104 94.9 89.2 214 205 116 113
90-110 4 M1
Results -presented on
this page are In the units indicated by the "Units" column except where an alternate unit is presented tot he right of the result. '
REPORT OF LABORATORY ANALYSIS '
This report shall not be reproduced, except in full,
Date: 06/15/2017 08:35 AM
without the written co.nsent of Pace Analytical Services, LLC.
Page 16 of 2;

aceAnalj cal
www.P—Iabs.com
QUALITY CONTROL DATA
Project: ASH 6/5
Pace Project No.: 92342918
QC Batch: 261569 Analysis Method: EPA 9014
QC Batch Method: SW-846 7.3.3.2 Analysis Description: 733C Reactive Cyanide
Associated Lab Samples: 92342918001, 92342918002
METHOD BLANK: 1288106 Matrix: Solid
Associated Lab Samples: 92342918001, 92342918002
Blank Reporting
Parameter Units Result Limit Analyzed YZ Qualifiers
Cyanide, Reactive mg/kg ND
1.0 06/12/17 22:48
LABORATORY CONTROL SAMPLE: 1288107
Pace Analytical Services, LLI
9800 KinceyAve. suite 10
Huntersville, NC 2807
(704)875-909:
Spike LCS LCS % Rec
Parameter Units Conc. Result
Rec Limits Qualifiers
Cyanide, Reactive mg/kg 100
ND 0 0-8
SAMPLE DUPLICATE: 1288108
Parameter 30221004001 Dup
Units Result Result RPD Qualifiers
Cyanide, Reactive mg/kg ND
ND
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/15/2017 08:35 AM without the written consent of Pace Analytical Services, LLC.
Page 17 of 23

Pace Analytical Services, LLC
9800 WnceyAve. Suite 160
e
me ' Hu rsville, NC 280713 '
1060
aeAnOc
[phone]
wwwpacelabs.cam
QUALITY CONTROL, DATA
Project: ASH 6/5
Pace Project No.: 92342918
Analysis Method: SM4500S2F-00
QC Batch: 261570
Analysis Description: 734S Reactive Sulfide
QC Batch Method:. SW-846 7.3.4.2
Associated Lab Samples: 92342918001, 9234291800.2
METHOD BLANK: 1288109
Matrix: Solid
Associated Lab Samples: 92342918001, 9234291800.2
Blank Reporting
Units Result Limit . Analyzed Qualifiers
Parameter
mg/kg p 10.0 06112/17 21:32
Sulfide, Reactive,
LABORATORY CONTROL SAMPLE:_
1288110
LCS LCS % Rec
Spike
Units Conc. Result % Rec Limits. Qualifiers
Parameter
mg/kg 202 56.7 28 0-52
Sulfide; Reactive
SAMPLE DUPLICATE: .1288111
30221004001 Dup.
Units Result . Result. RPD. Qualifiers
Parameter
Sulfide, Reactive
.. ND ND
mg/kg ..
on this page are in the units Indicated by the "Units". column except where an alternate unit Is pr®santad to the fight of the result.
Rasuite presented
ROORT.OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,.. page 18 of
without the.wriden consent of Pace Analytical Services, LLC.
Date: 06/15/2017 08:35 AM

x
aceAnalytical
www.pawlabs.com
QUALIFIERS
Project: ASH 6/5
Pace Project No.: 92342918
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J -Estimated concentration above, the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LU
9800 KinceyAve. Suite 10i
Huntersville, NC 28071
(704)875-909,'
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate).
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethyivinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-PA Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
Date: 06/15/201108:35 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services,'LLC.
Page 19 of 23

Pace Analytical Services, LLC
9800
KinceyAve. Suite 100
Huntersville," NC 28078
[phone]
www.paodabscom
QVALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
ASH 6/5
Pace Project No.:
92342918
Analytical
QC•Batch Method
QC Batch.
Analytical.Method.
Batch .
Lab.lD
Sample ID.
EPA 3050
36358
EPA 6010
363790
92342618001
SP6217A
EPA 3050
363585
EPA 6010 "
363790
02342918002
SP6217B
364014
02342918001
SP6217A .:
EPA 3010A
363844
363644
EPA 6010 -
EPA 6010
364014
92342918002
SP6217B
EPA 3010A
EPA 7470
363845
EPA 7470
363962
92342918001
S06217A
EPA 7470
363845
EPA 7470 .
363962
923420180.02
S062176
363761
EPA 7471•
363867
02342918001
SP6217A
EPA 7471
EPA 7471
363761
EPA 7471_
363867
92342918002
SP6217B
92342918001
SP6217A
ASTM D2974-87
363766
92342918002
SP6217B
ASTM D2974-87
363766
92342918001
SP6217A
EPA1010
364735
364735
-92342918002
SP6217B
EPA1010
92342914001
SP6217A
PA 9045
E -
364601
364601
9234291>3e002
SP:62176 :
A . EP 9045
92342918001
SP6217A
EPA 365:1
364226.
364226
923429,18002 -
SP6217B
EPA 366.1
92342918001
SP6217A
SW-846 T3.3.2
261569
261569
EPA9014 •
EPA 9014
261619
261619
92342918002
SP6217B
SW-846 7.3.3.2:
SW-846.7.3.4.2
261570 ,;
SM4500S2F-00
261618
92342918001
SP6217A
SW-846 7.3.4.2
261570
SBA4500S2F-00
269618
92342918002
SP62176
REPORT OF LABORATORY ANALYSIS
This report shall; not be reproduced, except in full, .
Date:.06/15/2017 08:35 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of

Document Name: Document Revised: Sept. 21, 2016
o Sample Condition. Upon Redc ipt(SCUR) Page 1:of 2
` 9ace
AI]r?IytlCal Document"No . Issuing Authority: .
F-CAR-CS-033-Rev.01 - Pace,Quality Office
Laboratory receiving samp
EdpnO..:. Greenwo6d. F ;N mtersyloe.0 Raleigh[(. Mechanicsville(
. .. Client Name: WO# ' 9234.29 1 V .
• Project #: I l
Courier: ❑Fed Ex []UPS QUSPS
❑Pace her: Ifent. II I II' I II LI II I III"� I III
0 Commeec(al ❑Ot
923aze1s
Custody Seal Present? ❑yes Zo7Sea ls Intact?. QYes ❑Ny .
Date/Initials Person Examining Contents.
Packing Material: Bubble Wrap ElBubblq Bags _one ❑Other:
Thermomete• r: -
Gun ID: Type of Ice: 1 et- ❑Blue one ❑Samples on ice, tooling process has be
Cotrection Factor l
Coo 1`Tem Corrected 'C : "
A ( ) BiologfcalTissue Froien? ❑Yes []No /A
Temp should be above 6e? g to 6�C
USDA Regulated Soil (A, water sample)
Did.samples originate in a quarantine zone within the United States:'CA, NV-j or SC (check maps)? Did samples.originate from a foreign source (internationa ly,
Dyes ❑No ..
Including Hawaii and Puerto Rico)? []Yes [2o
Comments/Discrepancy:
Chain of Custody -Present?.
es, :._❑No
. ❑N/A
1
Samples Arrived within Hold Time?.
❑ es
[IN, .
N/A
2.
Short Hold Time Analysis (<72 hr.)?- •
❑Yes-
o.
❑N/A
3.
Rush Turn Around Time,Requested?`
Dyes
o
❑N/A
A.
SufficientVolumeP
Elyes
❑No
❑N/A :.
S.
Correct Containers Used?
Pace'Containert Used?
e- ON-
❑ .[]No
❑NJA
. ❑N/A
6: .
.
Containers Intact? .
❑No
❑N/A
: 7,
Samples Field Filtered?
❑Yes
A96
8.
Note if,sediment is visible in the dissolved container.
Sample Labels Match COC?
r
=lnciudes i)ate/Tinie/iD/Analysis Mmra ix:
Headspace in VOA -Vials (>5-6mm)?
❑Yes
C,
J
Elves
[]No
❑No
❑NJA
N -
9;
_
. 10,
Trip Blank Present?.
Trip Blank Custody Seals Present?
(]Yes
❑yes ..
❑No
❑No
NJ
N/A
�1.
CLIENT NOTIFICATION/RESOLUTION
Person'Contacted:
DateJTfinet
Comments/Sample
Discrepancy:
Project Manager SCURF Review:a Date::"
Project Manager SRF Review: _.. Date: d 7
Note: Whenever there is a discrepancy affecting.North Carolina compliance samples,'a,copy of this form will be sent to the North Carolina DEHNR Certification Office (L
"Out of hoid, incorrect preservative, out -of temp, incorrect containers)
Page 21 of 23

Document Revised: Sept. 21, 2016
Document Name:
ndition Upon Re
Document No.:
*Check mark top half of box if pH and/or dechlorination
is verified and within,the, acceptance range for,
preservation samples.
"Bottom half of box is to list number of bottles
ceipt(SCUR) Page 2 of 2
Issuing Authority:
D1 Pace Quality Office
Project # W®# : 9234291.8
pM: CD1
Due Date: 06/29/17
CLIENT: 92-Baxter
U
1< 0
_ m _
Z z z _ _
v o Z N N m v v v Q ? Ad
a' is 2 v w 2 a z Z ` Y Z Z O m
w 01 2 a 19 'N H = °1 d a� ¢ m Q � u N ">
a� d y d M w x m a, a a v O n \ p v a o a x c
a a a a O Z p a O N Q
> > z
O x u N u O a5 E 2 Z x x C m
N N •N u M y to .O O Q Q Q Q p) W Y ~ a U V
a a a m p ° n a o E Q E < R Q �' O O O m F E n J
J J J 6. J J -J N L �.. E E a E E . 0 NNE 0 W E
Ln tO� O +' O O O O �' ~ %= O t' O l7 O O O O to v .-1 Ln
.N-1 N N .i N {f� 3 .1 .i N
iV N 7 1!v
7 7 > > H 1 f 6 u. N N tin m m os m al (n a a N
E t7 C7 C7 t9 C7 C7 l7 l7 > l7 C \ iA N pap
m m m m m m w m 3 a a a a a a o>> o>>
z i
3
4
5
6
7
9
10
11
1z
pH Adjustment Log for Preserved Samples
d Time tion Amount of
Sample ID Type of Preservative pH upon receipt Date preservation adjusteadjusted added ervative Lot q
Page 22 of

axter Biomas - Wood
-.BdilerahRles
:
:
Please test the sample'(s) for the parameters as .
..
listed below:
.
Send original results to:. -email: ricky_.styles@baxtet`:com
. -Send invoice And .co of results to: -
PY
email: ricky_Styles@baxter:Com
Ricky. Styles
Baxter Biomass:
Purchase,'Order# 13737`1
2859`Old Linville Rd.
Marion, NC 28752
.(628 '756-6650.
Re `uested Due Date:' 6/12/2017.
Sam le ALL LISTED " '
• v- jLl
Sample #
Sample
Description-
Sample Dates)
and,time'sample•
Grab:or
Composite
Total Mr tals -:
As; Ba; Cd,.
.
TCLP Metals
As, Ba.:U,
Ignitability, '
Reactivity
pH:
Corrostvity
Total -Arsenic:
- Full TCLP
collected .:.
,.. ,-
Ga,: Cr Cu Fe
Cr Pb li ,
9
Pb, Mg Hg;
Se; q9
Mnj,M01i,Ni; K;
Se, Ag, Na,::Zn;
total
Phos horns
SP621.7A
ASH:
6/5/17 10:45AM
COMPOSITE
YES. "
YES .
YES,
YES
YES
SP6217B
ASH
8L5/i?:10:45AM
COMPOSITE
YES
YES.
YES
:YE$
YES°
Sample sent to: Pace Analytical Services; Inc.
Project Manager Tom Williams
2225 Riverside Drive
Asheville NC28804 '.
9800 Kincey. Avenue, Suite 100:
.
828-254-7176
Hunters ville, NC 28078;
875 - 9092, ext..233'
Chain of`Custody,'