WQ0010689_Report_20100427

April 27, 2010
NCDENR - DWQ
Aquifer Protection Section
Land Application Unit .
2728 Capital Boulevard
Raleigh, NC 27604
RECEIVED / DENR / DWQ
Aquifer Prn+a, g,)r_ cnction
APR 3 0 2010
Barter
MAY 04 2010 Z
Asheville Regional Office
n
RE: 2009 Annual Ash Report
Permit No. WQ0010689
Wood Boiler — North Cove, NC
Enclosed is the annual as distribution report for the calendar year 2008, using the forms provided by NCDENR-
DWQ. During 2009, ash was distributed in two forms:
1. Flyash that settled into the scrubber ponds was mixed with flyash from the multi -cyclone, bottom ash, and
dry wood to reduce the moisture content. The ash was distributed for land application in this form. See the
ash distribution records for a list of recipients.
2. Bottom ash from the boiler grate was also distributed. This ash was hauled in a very dry form and used as a
soil amendment in a commercial operation. A composite sample was collected and Total metals and TCLP
were performed before distribution. Additionally, bottom ash was mixed with pond ash to help reduce the
moisture content.
All samples were analyzed by Pace Analytical Services, Inc., a North Carolina certified laboratory.
If you have any questions or require additional information, please contact Anita Jensen at 828.756.6734 or Ricky
Styles at 828.756.6650.
Sincerely,
rnest Shepard
Plant Manager
Baxter Healthcare
PO Box 1390
65 Pitts Station Rd. & Hwy 221 N
Marion, NC 28752
T 828.756.4151
F 828.756.4821
Enclosures: DWQ Reporting Forms
Ash Distribution Records
Pace Analytical Laboratory Reports
Baxter Healthcare Corporation
PO Box 1390, Marion, NO 28752
T 828.756.4151

Cc: NC Division of Water Quality (3 additional copies with enclosures)
Ricky Styles
Anita Jensen

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0010689 FACILITY NAME: Suez Energy BioPower, Inc. - North Cove (now Baxter Wood Boiler - acquired January 8, 2010)
PHONE: [phone] COUNTY: McDowell OPERATOR: Suez Energy BioPower, Inc. - North Cove
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
E Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 0 No ❑ --► If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) s) ( include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
See attached distribution records
February
March
April
May
June
July
August
September
October
November
December
Total from FORM DMSDF (sup)
Totals: Annual (dry tons):
0
0
I
0
..............................
0
...........•.•.•.•.•.•.•
Amendment(s) used: I
Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit E Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee Date Signatdre of Preparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
RECEIVED ! DENR ! DWQ
Aquifer Protection Section
APR 3 0 2010;
DENR FORM DMSDF (12/2006)

Ash Inventory
Estimated
WET Tons
Ash Moisture as
Date
Ash Reused
Type Ash
Recipient
Hauled (measured)
Comments
10/27/08
SOUTH SCRUBBER POND
OUT OF SERVICE
1/15/09
90
BOTTOM ASH
JEFF BANKS
HAULED BY JEFF BANKS
2/17/09
80
SOUTH SCRUBBER POND
BILL SMITH
52.00%
REMC PROPERTY
2117/09
30
SOUTH SCRUBBER POND
JAMES EDWARDS
52.00%
SPREAD BY JEFF BANKS
2/18/09
110
SOUTH SCRUBBER POND
BILL SMITH
52.00%
SPREAD BY JEFF BANKS
2119/09
90
SOUTH SCRUBBER POND
BILL SMITH
52.00%
SPREAD BY JEFF BANKS
2/20/09
140
SOUTH SCRUBBER POND
BILL SMITH
52.00%.
SPREAD BY JEFF BANKS
2/20/09
10
SOUTH SCRUBBER POND
JEFF BANKS
52.00%
SPREAD BY JEFF BANKS
2/20/09
10
SOUTH SCRUBBER POND
KEITH CLARK
52.000/6
SPREAD BY JEFF BANKS
2/21/09
40
SOUTH SCRUBBER POND
BILL SMITH
-52.00%.
SPREAD BY JEFF BANKS
2/23/09
80
SOUTH SCRUBBER POND
BILL SMITH
52.00%
SPREAD BY JEFF BANKS
2/23/09
20
SOUTH SCRUBBER POND
KEITH CLARK
52.00%
SPREAD BY JEFF BANKS
2/24/09
130
SOUTH SCRUBBER POND
WILLIAM PENLAND
52.00%
SPREAD BY JEFF BANKS
2/24/09
20
SOUTH SCRUBBER POND
BILL PHILLIPS
52.00%
SPREAD BY JEFF BANKS
2125109
100
SOUTH SCRUBBER POND
BILL PHILLIPS
52.00%
SPREAD BY JEFF BANKS
2/25/09
50
SOUTH SCRUBBER POND
JEFF BANKS
52.00%
SPREAD BY JEFF BANKS
2/25/09
20
SOUTH SCRUBBER POND
BILL SMITH
52.00%
SPREAD BY JEFF BANKS
2/26/09
30
SOUTH SCRUBBER POND
DANIEL RAY
52.00%
SPREAD BY JEFF BANKS
2126/09
160
SOUTH SCRUBBER POND
BILL SMITH
52.00%
SPREAD BY JEFF BANKS
2/26109
20
SOUTH SCRUBBER POND
KEITH CLARK
52.00%
SPREAD BY JEFF BANKS
2126/09
SOUTH SCRUBBER POND
RETURNED TO SERVICE
2126/09
NORTH SCRUBBER POND
OUT OF SERVICE
4/16/09
40
BOTTOM ASH
JEFF BANKS
HAULED BY JEFF BANKS
6/1/09
260
NORTH SCRUBBER POND
BOBBY BOONE
47.00%
SPREAD BY JEFF BANKS
6/8/09
90
NORTH SCRUBBER POND
BOBBY BOONE
47.00%
SPREAD BY JEFF BANKS
6/8/09
70
NORTH SCRUBBER POND
DEAN McCLURE
47.00%
SPREAD BY JEFF BANKS
6110/09
90
NORTH SCRUBBER POND
DEAN McCLURE
47.00%
SPREAD BY JEFF BANKS
6/10/09
160
NORTH SCRUBBER POND
DEAN McCLURE
47.00%
SPREAD BY JEFF BANKS
6/11/09
100
NORTH SCRUBBER POND
DEAN MCCLURE
47.00%
SPREAD BY JEFF BANKS
6111/09
40
NORTH SCRUBBER POND
MAX HOLLAND
47.00%
SPREAD BY JEFF BANKS

6111/09
60
NORTH SCRUBBER POND
BOBBY BOONE
47.00%
SPREAD BY JEFF BANKS
6/15/09
20
NORTH SCRUBBER POND
RICKY STYLES
47.00%
RICKY STYLES = SPREAD
6/15/09
10
NORTH SCRUBBER POND
BOBBY BOONE
47.00%
SPREAD BY JEFF BANKS
6/15/09
60
NORTH SCRUBBER POND
MAX HOLLAND
47.00%
SPREAD BY JEFF BANKS
6/16/09
70
NORTH SCRUBBER POND
DEAN McCLURE
47.00%
SPREAD BY JEFF BANKS
6/16/09
40
NORTH SCRUBBER POND
MAX HOLLAND
47.00%
SPREAD BY JEFF BANKS
6/16109
10
NORTH SCRUBBER POND
BOBBY BOONE
47.00%
SPREAD BY JEFF BANKS
6/16/09
40
NORTH SCRUBBER POND
RICKY STYLES
47.00%
RICKY STYLES -.SPREAD
6/17/09
40
NORTH SCRUBBER POND
RICKY STYLES
47.00%
RICKY STYLES - SPREAD
6/22/09
NORTH SCRUBBER POND
RETURNED TO SERVICE
6/22/09
SOUTH SCRUBBER POND
OUT OF SERVICE
TRAVIS
8/26/09
160
SOUTH SCRUBBER POND
GRINDSTAFF
35.00%
SPREAD BY JEFF BANKS
8/28/09
10
SOUTH SCRUBBER POND
MARK COLE
35.00%
SPREAD BY JEFF BANKS
9/1/09
510
SOUTH SCRUBBER POND
TERRY ENGLISH
35.00%
SPREAD BY JEFF BANKS
9/3109
144
SOUTH SCRUBBER POND
DEAN McCLURE
35.00%
SPREAD BY JEFF BANKS
10/1/09
SOUTH SCRUBBER POND
RETURNED TO SERVICE
11/9/09
NORTH SCRUBBER POND
OUT OF SERVICE
12/8/09
70
BOTTOM ASH
JEFF BANKS
20.00% .
HAULED BY JEFF BANKS
3254
Note: Scrubber ash includes sandbox ash used to dry ponds
Ash Pond Activity
Pond Side
Date
Excavated
1/5/09
south
1/6/09
south
1/12/09
south
1/13/09
south
1119/09
south
1 /20/09
south
Tons Wood Added
5
10
5
10
5
10
Wood Moisture
as added
35%
35%
35%
35%
35%
35%

1/26/09
south
5
35%
1/27109
south
10
35%
5/4/09
NORTH
5
35%
5/5/09
NORTH
10
35%
5/11/09
NORTH
10
35%
5/12/09
NORTH
5
35%
5/14/09
NORTH
5
35%
5/15/09
NORTH
5
35%
5/18/09
NORTH
10
35%
5/19/09
NORTH
5
35%
5/25/09
NORTH
5
35%
5/26109
NORTH
5
35%
6/1/09
NORTH
10
35%
6/2/09
NORTH
10
35%
7/6/09
south
5
12%
7/7/09
south
10
12%
7/13/09
south
5
12%
7114/09
south
5
12%
7/20/09
south
10
12%
7/21/09
south
5
12%
8/4/09
south
10
12%
8/11/09
south
10
12%
8/17/09
south
10
12%
8/24109
south
10
12%
8/31/09
south
10
12%
9/1/09
south
5
12%
913/09
south
5
12%
TOTAL WOOD ADDED 245

# OF TESTS
Ash Description
Date
PH - EPA 9045
Arsenic - EPA6010 mg/kg
1
4QTR10709 BOTTOM ASH -GRATE
1/7/2009
11.7
9.1
2
S012809 SOUTH POND ASH
1/28/2009
10
18.4
3
41309 20091ST QTR BOTTOM ASH
4/13/2009
9.8
7.9
4
N5709 NORTH SCRUBBER POND ASH
5/7/2009
9.5
22.7
5
2QTR70609 BOTTOM ASH
7/6/2009
11.6
20
6
SP81309 SOUTH POND ASH
8/13/2009
9.5
20.9
7
3QTR100209 BOTTOM ASH
10/2/2009
12.3
16.7
8
NP11-11-09 NORTH POND ASH
11/11/2009
10.6
27.5
9
NP12-11-09 NORTH POND ASH
11/11/2009
10.6
31.1
AVERAGE
10.62
19.37

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar•year. Use additional forms as needed.
WQ Permit Number: WQ0010689 Laboratory:
Facility Name: Suez Energy BioPower, Inc. - North Cove
Residual Source
NPDES # or WQ#: WQ0010689
WWTP Name:
Residual Analysis Data
1) Pace Analytical Services, Inc.
2)
3)
4)
5)
Parameter
(mg/kg)
Sample or Composite Date
Bottom -
01/07/09
Pond -
01/28/09,
Bottom -
04/13/09
Pond -
05/07/09
Bottom -
07/06/09
Pond -
08/13/09
Bottom -
10/02/09
Pond -
11/11/09
Pond -
11/11/09
pH
11.7
10
9.8
9.5
11.6
9.5
12.3
10.6
10.6
Barium
524
1100
1160
1080
1280
816
1980
1330
1390
Calcium
66500
62900
75600
8400
92700
67500
8400
91100
104000
Iron
14000
12100
17200
12600
18700
9210
21800
10100
10000
Magnesium
18000
17300
13700
13600
12700.
12000
15600
13800
14400
Manganese
1350
1560
1710
1700
2320
2020
2890
3460
3780
Potassium
ND
27000
23800
17200
ND
ND
29300
19200
13300
Silver
0.46
0.85
0.44
1.2
0.79
0.69
0.76
1.4
1.5
Sodium
4350
7800
7960
6900
8280
1690
20200
11600
11900
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significrt V. wdt'ies f fitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature, reparer Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0010689
Facility Name: Suez Energy BioPower, Inc. - North Cove
Residual Source WQ # or WQ0010689
NPDES #:
WWTP Name:
Residual Analvsis Data
Laboratory:
1)
2)
3)
4)
5)
Parameter
(mg/kg)
Cone.
Limit
m /k a
Sample or Composite Date
Bottom -
01/07/09
Pond -
01/28/09
Bottom -
04/13/09
Pond -
05/07/09
Bottom -
07/06/09
Pond -
08/13/09
Bottom -
10/02/09
Pond -.
11/11/09
Pond -
11/11/09
Percent Solids (%)
NA
99.86
63.7
99.67
46.2
99.8
70.4
91.4
35.2
37.4
Arsenic
75
9.1
18.4
7.9
22.7
20
20.9
1.6.7
27.5
31.1
Cadmium
85
0.88
1.7
1.1
1.7
1.7
1.4
1.4
2.3
2.7
Copper
4,300
135
129
290
134
234
112
246
159
168
Chromium
NA
17.3
27.6
22.7
30.6
62.3
32.5
1.79
53.5
56
Lead
840
10
18.6
.4
50.1
831
45.6
38.4
55.1
60.7
Mercury
57
ND
0.021
ND
0.026
ND
0.021
ND
0.012
ND
Molybdenum
75
ND
ND
ND
ND
ND
ND
ND
• ND
ND
Nickel
420
9.8
15.8
10.7
15.7
14.8
15.4
27.9
30.8
33.2
Selenium
100
2.1
2.4
2.2
4.2
3.3
2.6
1.2
ND
2.1
Zinc
7,500
57.8
124
35.2
215
687
199
183
313
369
Total Phosphorus
NA
178
48.4
147
105
35.9
273
166
158
3210
1
TKN
NA
Ammonia -Nitrogen
NA
Nitrate and Nitrite
NA
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

Pace Analytical Servles, Inc.
2225 Riverside Dr.
Asheville, NC'28804
Pace Analytical Services, Inc.
.9800 KinceyAve. Suite 900
Huntersville, NC 28078
/71aceAnalXical'
/ www.pacetabs_com
i
January 15, 2009
Ms. Summer Barber
Suez Energy
302 Duke Street
Forest City, NC 28043
RE: Project: 4QTR10709 BOTTOM ASH
Pace Project No.: 9235521
[phone]
Dear Ms. Barber.
Enclosed are the analytical results for sample(s) received by the laboratory on January 07, 2009.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples,were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
C�Z -I
Kevin Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Without the written consent of Pace Analytical Services, Inc..
[phone]
Page 1 of 11

Pace AnalyticalServices, Inc_ Pace Analytical lincey Services, 100
2225 Riverside Dr. 9800 KinceyAve. Suite 100
wwwpaca hs.com Asheville, NC28804 Huntersville, NC28078
[phone] [phone]
Project: 4QTR10709 BOTTOM ASH
Pace Project No.: 9235521
Charlotte Certification IDs,
West Virginia Certification #: 357
Virginia Certification #: 00213
Tennessee Certification #: 04010
South Carolina Drinking Water Cart #: 990060003
South Carolina Certifleation #: 990060001
Pennsylvania Certification #: 68.00784
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
West Virginia Certification #: 356
Virginia Certification #: 00072
Tennessee Certification #: 2980
South Carolina Certification #: 99030001
South Carolina Bioassay Certification #: 99030002
Pennsylvania Certification 9: 68-03578
North Carolina Wastewmter Certification #: 40
Eden Certification IDs
Virginia Drinking Water Certification #: OD424
North Carolina Wastewater Certification #: 633
CERTIFICATIONS
North Carolina Feld Services Certification #: 5342
North Carolina Drinking Water Certification #: 37706
New Jersey Certification #: NC012
Louisiana/LELAP Certification #: 04034
Kentucky UST Certification #: 84
Florida/NELAP Certification #: E87627
Connecticut Certification #: PH-0164
North Carolina Drinking Water Certification #: 37712
North Carolina Bioassay Certification #: 9
New Jersey Certification #: NC011
Massachusetts Certification #: M-NCO30
Louisiana/LELAP Certification #: 03095
Fiorida/NELAP Certification #: E87648
Connecticut Certification*. PH-0106
North Carolina Drinking Water Certification #: 37738
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
=�-ta�CiLa:
Page 2 of 11

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceA !al �/tical 2225 Riverside Dr. 98
r� ws� QO KinceyAve. Suite 100
ww J `
Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
SAMPLE ANALYTE COUNT
Project: 4QTR10709 BOTTOM ASH
Pace Project No.: 9235521
Lab ID Sample ID Method
Analysts
Analyses
Reported
Laboratory
9235521001 4QTR70709 BOTTOM ASH ASTM D2974-87
KDF
1
PASi-C
EPA365.1
LEP
1
PASI-A
EPA6010
SHB
17
PASI-A
EPA7471
EWS
1
PASI•A
EPA 9045
TEE
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, inc..
Page 3 of 11

d Pace Analytical Services, Inc. Pace Analytical Services, Inc.
�IaceAnalj6cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
wwwpawlabscanr Asheville, NC28804 Huntersville, NC28078
1 [phone] [phone]
ANALYTICAL RESULTS
Project: 4QTR10709 BOTTOM ASH
Pace Project No.: 9235521
-4ampre: 4QTK10709 BOTTOM ASH
LabID: 9235521001
Collected: 01/07/09 09-00 Received: 01/07/09 10:55 Matrix; Solid
Results reported on a "dry-we/ght' basis
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010
Preparation Method: EPA 3050
Arsenic
Barium
8.1 mg/kg
0.31
1
01/0910913.45 01/1210919:39 7440-38-2
524 mg/kg
0.31
1
01/0910913AS 01/12/09 19:39 7440-39-3
Cadmium
0.88 mg/kg
0.061
1
01109/0913:45 01/121091939 7440-43-9
Calcium
Chromium
66600 ffgft
611
100
01/0910913:45 01/12/0919:18 7440-70-2 •
Copper
17.3 mg/kg
0.31
1
01/0910913:45 01/1210919.39 7440-47-3
Iron
135 mg/kg
0.31
1
01/09/09 13:45 01112/0919:39 7440-50-8
Lead
14000 mg/kg
305
100
01/09/0913:45 01/1210919:18 7439-89-6
Magnesium
10.0 mg/kg
0.31
1
01/0910913.45 01112/0919:39 7439-92-1
Manganese
18000 mg/kg
611
100
0110910913.45 01/1210919:18 7439-95-4
Molybdenum
1360 mg/kg
30.5
100
01/0910913:45 01/1210919:18 7439-96-5
Nickel
ND mg/kg
0.31
1
01/0910913:45 01112/0919:39 7439-98-7
Potassium
9.8 mg/kg
0.31
1
0110910913A5 01/1210919:39 7440-02-0
Selenium
ND mg/kg
30500
100
01109/0913:45 01/12/0919:18 7440-09-7
Silver
2.1 mg/kg
0.61
1
01/0910913:45 0111210919.39 778249-2
Sodium
0.46 mg/kg
0.31
1
01/0910913:45 01/121091939 7440-22-4
Zinc
4350 mgflrg
305
1
0110910913:45 01/1210919.39 7440-23-5
67.8 mg/kg
0.61
1
0110910913:4.5 01/12/09 19.39 7440-66-6
7471 Mercury
Analytical Method: EPA7471
Preparation Method: EPA7471
Mercury
ND mg/kg
0.0032
1
01/08/091330 01/09/0911:40 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
0.14 %
0.10
1
01/08/09 15:35
9046 pH Soil
Analytical Method: EPA9046
pH at 25 Degrees C
11.7 Std. Units
0.10
1
01/1310916AO H1
365.1 Phosphorus, Total
Analytical Method: EPA365.1
Phosphorus 978
n'r9/k9 14.0 7 01/1410918;10 7723-14-0
Date: 01 /151 2009 04:55 PM REPORT OF LABORATORY ANALYSIS Page 4 of 11
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
=r

�aceAnalXical
www.pacelabacom
r
Project: 40TR10709 BOTTOM ASH
Pace Project No.: 9235521
QC Batch: PMST/2177
QC Batch Method: ASTM 02974-87
Associated Lab Samples: 9235521001
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Welght/Percent Moisture
SAMPLE DUPLICATE: 220196
9235492001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 14.1 13.6 3
SAMPLE DUPLICATE: 220260
9235586014 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture 23.3 - 24.6 5
Date: 01/15/200904:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 11

__eF'aceAn81Xka10
! �wneµxe&�Dscom
Project: 4QTR10709 BOTTOM ASH
Pace Project No.: 9235521
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7471
QC Batch Method: EPA7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 9235521001
me r ULJ GL KNR ZZU212 Matrix: Solid
Associated Lab Samples. 9235521 D01
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0050 0110910911:28
Pace Analytical Services, Inc,
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 220273
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury mg/kg .067 0.065 98 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 220274
220275
MS
MSD
9235610001
Spike
Spike
MS ' MSD MS MSD % Roc
Parameter Units Result
Conc.
Conc.
Result Result % Rec % Roo Limits RPD Qua[
Mercury mg/kg ND
O59
048
0.062 0.053 105 111 75-125 16
SAMPLt DUPLICATE: 220276
9235521001 Dup
Parameter Units Result Result RPD Qualifiers
Mercury mg/kg ND 0.0051
Date: 01/15/2009 04:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of pace Analytical Services, Inc..
Page 6 of 11

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
I�AeAnalyfical 2225 Riverside Dr. 9800 KinceyAve. Suite 100
V,yPaC&2ps,r10M Asheville, NG28804 Huntersville, NC28078
j [phone] [phone]
QUALITY CONTROL DATA
Project: 4QTR10709 BOTTOM ASH
Pace Project No.; 9235521
QC Batch: MPRP13641
QC Batch Method: EPA3050
Associated Lab Samples: 9235521001
Analysis Method:
Analysis Description:
EPA6010
6010 MET
METHOD BLANK: 221002
Matrix: Solid
Associated Lab Samples: 9235521001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Arsenic
mg/kg
ND
0.50
01/12JO919:36
Barium
mg/kg
ND
0.50
01/1210919:36
Cadmium
mg/kg
ND
0.10
01112/0919:36
Calcium
mg/kg
ND
10.0
01/12/0919:36
Chromium
mg/kg
ND
0.50
01112/0919:36
Copper
mgft
ND
0.50
01/1210919.36
Iron
mg/kg
ND
5.0
01112/0919:36
Lead
mg/kg
ND
0.50
01/1210919:36
Magnesium
mg/kg
ND
10.0
01/1210919:36
Manganese
mg/kg
ND
0.50
01/12/0919:36
Molybdenum
mg/kg
ND
0.50
01/12/091936
Nickel
mg/kg
ND
0.50
0111210919:36
Potassium
mg/kg
ND
500
01/1210919:36
Selenium
mg*9
ND
1.0
0111210919:36
Silver
mg/kg
ND
0.50
01/121091936
Sodium
mg*g
ND
500
01/1210919:36
Zinc
mg/kg
ND
1.0
01/12/0919:36
vit"t(ArUKY CONTROL SAMPLE:
Parameter
221003
Units
Spike
Conc.
LCS
Result
LCS
%Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
49.3
99
80-120
Barium
mg/kg
50
48.4
97
80-120
Cadmium
mg/kg
50
48.5
97
80-120
Calcium
m9/k9
500
492
98
80-120
Chromium
mg/kg
50
50.7
101
80-120
Copper
mg/kg
50
50.2
100
80-120
Iron
mg/kg
500
494
99
80-120
Lead
mg/kg
50
48.8
98
8,0-120
Magnesium
mg/kg
500
485
97
80-120
Manganese
mg/kg
50
50.4
101
80-120
Molybdenum
mg/kg
50
46.8
94
80-120
Nickel
mg/kg
50
50.1
100
80-120
Potassium
mg/kg
500
492J
98
80-120
Selenium
mg/kg
50
48.1
96
80-120
Silver
mg/kg
25
24.5
98
80-120
Sodium
mg/kg
500
561
112
80-120
Zinc
mg/kg
50
48.9
98
80-120
Date: 01/15/2009 04:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 11
r

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalj cal 2225 Riverside Or.9800 l(inceyAve. Suite 100
j wwwgmcefabscom Asheville, NC 28804 HunterWIle, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: 4QTR10709 BOTTOM ASH
Pace Project No.: 9235521
MATRIX SPIKE SAMPLE:
Parameter
221004
Units
9235320001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Roo
Limits Qualifiers
Arsenic
mgMg
4.3
53.2
76.9
136
75-125 MO
Barium
mg/kg
1.6
53.2
51.9
94
75-125
Cadmium
mg/kg
NO
53.2
51.1
96
75-125
Calcium
mg/kg
926
532
1690
143
75-125 MO
Chromium
mg/kg
3.3
53.2
58.0
103
75-125
Copper
mg/kg
3.4
53.2
163
299
75-125 MO
Iron
mg/kg
5220
532
7610
448
75-125 MO
Lead
mg/kg
10.3
53.2
59.2
92
75-125
Magnesium
mg/kg
1210
532
2460
235
75-125 MO
Manganose
mg/kg
67.1
53.2
155
165
75-125 MO
Molybdenum
mglkg
NO
53.2
50.3
94
75-125
Nickel
mg/kg
13.6
53.2
67.7
102
75-125
Potassium
mg/kg
NO
532
657
113
75-125
Selenium
mg/kg
NO
53.2
53.0
99
75-125
Silver
mg/kg
NO
26.6
26.5
99
75-125
Sodium
mg/kg
NO
532
701
127
75-125 MO
Zinc
mg/kg
6.2
53.2
135
243
75-125 MO
SAMPLE DUPLICATE: 221005
9235577001
pup
Parameter
Units
Result
Result
RPD
Qualifiers
Arsenic
mg/kg
88.4
107
19
Barium
mg/kg
42.7
55.7
26 R1
Cadmium
mg/kg
2.1
2.2
3
Calcium
mg/kg
880
43500
192 R1
Chromium
mg/kg
11.5
14.1
20
Copper
mg/kg
37.8
41.2
9
Iron
mg/kg
14100
14000
.5
Lead
mg/kg
61.7
63.1
2
Magnesium
mg/kg
1350
24800
179 R1
Manganese
mg/kg
1660
2060
21 RI
Molybdenum
rng/kg
ND
ND
Nickel
rng/kg
13.6
14.0
2
Potassium
mg/kg
536
S80
49 R1
Selenium
mglkg
1.7
2.7
48 R1
Silver
mg/kg
NO
.42J
Sodium
mg/kg
NO
63J
Zinc
rrp/kg
83.4
78.2
6
Data: 01/15/2009 04:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 11

_ �P'r ceAnalXicaI
www nwiabs.com
Project: 40TR10709 BOTTOM ASH
Pace Project No.: 9235521
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WEfA/4232 Analysis Method: EPA365.1
QC Batch Method: EPA365.1 Analysis Description: 385.1 Phosphorus, Total
Associated Lab Samples: 9235521001
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 222426 Matrix: Solid
Associated Lab Samples: 9235521001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 2.0 0111410916:34
LABORATORY CONTROL SAMPLE: 222427
Spike LCS LCS % Roe
Parameter Units Conc. Result % Roo Limits Qualifiers
Phosphorus mg/kg 20 19.5 98 90110
MATRIX SPIKE SAMPLE: 222428
9235744019 Spike MS MS % Roo
Parameter Units Result Conc. Result % Roe Limits Qualifiers
Phosphorus mg/kg 12300 136 12900 423 90-110 MO
SAMPLE DUPLICATE: 222430
9235466001 Dup
Parameter Units Result Result RPD Qualifiers
Phosphorus mg/kg 204 255 22 R1
Date: 01 /15/2009 04:55 PM
REPORT OF LABORATORY ANALYSIS
Thts report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
t<
Page 9 of 11

,PaceAna1wa1
ww..p acebAb&c=
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 4QTR10709 BOTTOM ASH
Pace Project No.: 9235521
QC Batch: WET/6890 Analysis Method: EPAS045
QC Batch Method: EPA9045 Analysis Description: 9045 pH
Associated Lab Samples: 9235521001
Or+Mt'Lt uurLICAtE: 222628
9235636002 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 12.2 12.1 g
JAMr'Lt UUVLIGA7 E: 222629
9235636003 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 11.3 11.3 0
Date: 01/15/2009 04:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�3
Pace Analytical Services, Inc.
98001dnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 11

e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
I�PalceAnalj&cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
/ www.pacelabscom Asheville, NC 28804 Huntersvilie, NC 28078
[phone] [phone]
QUALIFIERS
Project: 40TR10709 BOTTOM ASH
Pace Project No.: 9235521
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270listed analyte) decomposes to Azobonzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP-Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Paco Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytIas.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PAST -A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
Mo Matrix spike, recovery was outside laboratory control limits.
R1 RPD value was outside control limits.
Date: 01 /1512009 04:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
::11S.�LL41°
Page 11 of 11

I—S ✓ez
Energy Generation NA
Please test the eampk(s) for the parame*m as Isted below.
SOW Invoice and copy of results to:
Ricky am"
SUEZ EmW 13WRowsr, tic.
2 Old Linville Rd.
Marlon, NC 21762
(628) 7m 4m
(fax) 756-7160
Reauested Due nAtn-
Send original results to:
Summer Barber d, Frankie Fox
SUEZ Energy BioPower, Inc.
302 Duke Street
Forest City, NC 28M
summer.barbarMadfsuema eom
frankiedfsaezna.com
dr,&tyggdfsuezna.cam
[phone]
(fax) 286-1229
SWnPk 9
Satnpti
.Deserlition
Sample Data(s)
and Um mnpia
Collected
Omb or
Composite
TWO Weis •
As, Be, Cd, Ca,
Cr, Cu, Fe, Pb,
TCLP Metals -
As, On, Cd,
Cr, Pb, Hg,
lQnit+rblllty,
Rewtivity
pH
Comosivity
TotaNArsank
Ftefi TCLP
Mg, Hg, Mn,
Se, Ag
Mo, Ni, K, Se,
A9, He, Zn,
total
Phosphorus
4QTR110709
BOTTOM ASH
1-749 9AM
COMPOSITE
YES
YES
YES
q 2 3 O2/°d%
Sample sent to: Pace Anaiytica! Servkes, Ir
222$ Rlveretde Drive
Astwift, W. 28804
828-2a4-7176
Chain . stody
Project Manager: Kevin Godwin
9800 Kinay Avenue, Suite 100
Hunt mville, NC 28078
(704) 875 - 9092 md. 233
XGC, IO;SS

Date: /- %- bAnalyst:
Facility: M 110,
Calibration
i CaHbration
Time
vNi �u�Qi
4.0
1-1 lur
1010
Check
Buffer 7.0*
Comments
8.
yor
D. o,
99
2 Z.
x W buffer checks
AM to hA within
t 0 1 H
. p units of the standards true value
pH Analyses
Sample I®
HSaled
H Result
Buffer
Chech-
Comments
Z Z C,
EAnalyzed
ll.
7, DD
Indicates a recommended
drift
shark iic;nn
0-prp.. 7 n -4
.L-_ _
- - --- ­"v W"l GI 1 -v At uia Unu or testing or every 4 hours minimum.
Results should be within t 0.1 pH units of the standard's true value.

I�AceAnalyticalo
f uw'Pacews.com
1
February 12, 2009
Ms. Summer Barber
Suez Energy
302 Duke Street
Forest City, NC 28043
RE: Project: S012809 POND ASH
Pace Project No.: 9236817
Pace Analytical Services, Inc.
2225 Riverside:Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
98001Gncey Ave. Suite 100
Huntersville, NC 28078
Dear Ms. Barber.
Enclosed are the analytical results for sample(s) received by the laboratory on January 28, 2009.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 1 of 14

aceAnalyfical
xmm pxelab&C m
r
Project: S012809 POND ASH
Pace Project No.: 9236817
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDS
West Virginia Certification #: 357
North Carolina Field Services Certification #: 5342
Virginia Certification #: 00213
North Carolina Drinking Water Certification #: 37706
Tennessee Certification 9: 04010
New Jersey Certification #: NCO12
South Carolina Drinking Water Cert. #: 990060003
Louisiana/LELAP Certification #: 04034
South Carolina Certification #: 990060001
Kentucky UST Certification #: 84
Pennsylvania Certification #: 68-00784
Florida/NELAP Certification#: E87627
North Carolina Wastewater Certification #: 12
Connecticut Certification #: PH-0104
Asheville Certification IDS
West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712
Virginia Certification #: 00072
North Carolina Bioassay Certification a : 9
Tennessee Certification #: 2980
Now Jersey Certification M NC011
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
South Carolina Bioassay Certification #: 99030002
Louisiana/LELAP Certification* 03095
Pennsylvania Certification #: 68-03578
Florida/NELAP Certification #: E87648
North Carolina Wastewater Certification #: 40
Connecticut Certification #: PH-0106
Eden Certification IDS
Virginia Drinking Water Certification #: 00424
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
4o�
Page 2 of 14

�aceAnalytical
twwpacalabscom
Project: S012809 POND ASH
Pace Project No.: 9236817
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
9236817001 S012809 ASTM 02974-87
TNM
1
PASI-C
EPA365.1
LEP
1
PAST -A
EPA6010
JMW
7
PASI-A
EPA6010
SHB
17
PASI-A
EPA7470
JDA
1
PASI-A
EPA7471
EWS
1
PASI-A
EPAS045
TEE
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3of14

aceAnalytical
whm.pacelabscrom
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NO 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NO 28078
[phone]
Project: S012809 POND ASH
Pace Project No.: 9236817
Sample: S012809 Lab ID: 9236817001 Collected: 01/28/09 09:30 Received: 01;12810911:02 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 METICP Analytical Method: EPA6010 Preparation Method: EPA3050
Arsenic
18.4 mg/kg
0.61
1
0210310913:50, 0210410918:09 7440-38-2
Barium
1100 mg/kg
0.61
1
02/0310913.50, 02104/0918:09 7440-39-3
Cadmium
1.7 mg/kg
0.12
1
02/03109 1350, 02/04/09 18:09 7440-43-9
Calcium
62900 mglkg
12.3
1
02103/0913:50, 02/03/09 22:07 7440-70-2
Chromium
27.6 mg/kg
0.61
1
02/03/0913:50! 02104/0918:09 7440-47-3
Copper
129 mg/kg
0.61
1
02/03/0913:50i 02104/0918:09 7440-50-8
Iron
12100 mg/kg
6.1
1
02/0310913:56 02/04/0918:09 .7439-89.6
Lead
18,6 mglkg
0.61
1
02103/0913:50' 02/04/0918:09 7439-92-1
Magnesium
17300 mg/kg
123
10
0210310913:50' 0210510915:37 7439-95-4
Manganese
1560 mg/kg
0.61
1
0210310913:50 02/03/09 22:07 7439.96-5
Molybdenum
ND mg/kg
0.61
1
02/0310913:50. 0210410918:09 7439-98-7
Nickel
16.8 mg/kg
0.61
1
02103/0913:50 02/0410918:09 7440-02-0
Potassium
27000 mg/kg
6130
10
02103/0913:50 02/05/0915.37 7440-09-7
Selenium
2.4 mg/kg
1.2
1
02/03/0913:50 0210410918:09 7782-49-2
Silver
0.86 mg/kg
0.61
1
02/0310913:50, 02/04/09 18:09 7440-22-4
Sodium
7800 mg/kg
613
1
0210310913:50 02/0410918:09 7440-23-5
Zinc
124 mg/kg
1.2
1
02103/09 13:50. 02/04/09 18:09 7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
Arsenic
0.029 mg/L
0.025
'1
01 /30109 14:00 01 /30/09 20:59 7440-38-2
Barium
1.7 mg/L
0.025
1
01/30/09 14:00 01/30109 20:59 7440-39-3
Cadmium
0.012 mg/L
0.0050
1
01/30/09 14:00 01/30/09 20:59 7440-43-9
Chromium
0.030 mg/L
0.025
1
01/30/0914:00 0113010920:59 7440-47-3
Lead
ND mg/L
0.025
1
01/3010914.00 01130/0920:59 7439-92-1
Selenium
ND mg/L
0.050
1
01/30/0914:00 01/3010920:59 778249-2
Silver
ND mg/L
0.025
1
01/30/09 14:00 01/30/09 20:59 7440-22-4
T470 Mercury, TCLP .
Analytical Method: EPA7470 Preparation Method: EPA7470
Mercury
ND ug/L
0.20
1
02/02/09 09:30 02/02/09 13:51 7439-97-6
7471 Mercury
Analytical Method: EPA7471 Preparation Method: EPA7471
Mercury
0.021 mg/kg
0.0056
1
01/3010909:10 01/30/0912:35 7439-97-6
Percent Moisture
Analytical Method: ASTM .D2974-87
Percent Moisture
36.3 %
0.10
1
01/29/09 15:58
9045 pH Soil
Analytical Method: EPA9045
pH at 25 Degrees C
10.0 Std. Units
0.10
1
02109/0917:45
366.1 Phosphorus, Total
Analytical Method: EPA365.1
Phosphorus
48.4 mg/kg
3.1 1
Date: 021121200901:55 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
02/10/09 09:41 7723-14-0 R1
Page 4 of 14

aceAnalytical
www.pscebbs.mn
Project: 8012809 POND ASH
Pace Project No.: 9236817
OC Batch: PMST/2240
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 9236817001
SAMPLE DUPLICATE: 229128
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC28804
[phone]
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
9236676231 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 18.7 17.8 5
SAMPLE DUPLICATE: 229129
9236832001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture OA 21.8 22.0 .8
Date: 02/1212009 01:55 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
"` no
Pace Analytical services, Ine.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 14

/5a'ceAnalyticalo
wmpacelabs.com
t
Project: S012809 POND ASH
Pace Project No.: 9236817
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP/1943 Analysis Method: EPA7471
QC Batch Method: EPA7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 9236817001
METHOD BLANK: 229231
Associated Lab Samples: 9236817001
Parameter U nits
mg/kg
Mercury
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
'N D 0.0050 01/30/0912:06
Pace Analytical Services, Inc.
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 229232
Spike
LCS
LCS
% Rec
Parameter Units
Conc.
Result
% Roo
Limits Qualifiers
Mercury mg/kg
.067
0.064
96
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:. 229233
229234
MS
-MSD
9236808001
Spike
Spike MS
MSD
MS MSD % Roo
Parameter Units Result
Conc.
Conc, Result
Result
% Roo % Roo Limits RPD Quai
Mercury mg/kg 0.0047
.062
.038 0.068
0.024
101 52 75-125 95 M0,R1
ug/g
SAMPLE DUPLICATE: 229235
Parameter
Mercury
9236786001 Dup
Units Result Result
mg/kg 12.0 1.8
RPD Qualifiers
10
Date: 02112/2009 01:55 PM REPORT OF LABORATORY ANALYSIS
This report shali not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
L� e
Page 6 of 14

1�2ceAnalyficalo
i
www.paceiabs com
j
Project: S0128 21 POND ASH
Pace Project No.: 9236817
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/3754 Analysis Method: EPA6010
QC Batch Method: EPA3010 Analysis Description: 6010 MET TCLP
Associated Lab Samples: 9236817001
METHOD BLANK: 230254
Associated Lab Samples: 9236817001
Parameter Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
0.025
01 /30/09 20:07
ND
0.025
01/30/09 20:07
ND
0.0050
01 /30/09 20:07
ND
0.025
01 /30/09 20:07 '
ND
0.025
01 /30109 20:07
ND
0.050
01 /30/09 20:07
ND
0.025
01 M/09 20:07
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
230255
Units
Spike
Cone.
LCS
Result
LCS
% Roe
% Rec
Limits Qualifiers
Arsenic
mg/L
2.5
2.8
112
80-120
Barium
mg/L
2.5
2.3
93
80-120
Cadmium
mg/L
2.5
2.5
100
80-120
Chromium
mg/L
2.5.
2.6
105
80-120
Lead
mg/L
2.5
2.3
92
80-120
Selenium
mg/L
2.5
2.8
111
80-120
Silver
mg/L
1.2
1.3
104
80-120
MATRIX SPIKE SAMPLE:
Parameter
230256
Units
9236772001 Spike MS MS % Roe
Result Cone. Result % Roe Limits Qualifiers
Arsenic
mg/L
2.8
Barium
mg/L
2.6
Cadmium
mg/L
2.4
Chromium
mg/L
2.5
Lead
mg/L
2.3
Selenium
mg/L
2.7
Silver
mg/L
1.3
SAMPLE DUPLICATE: 230257
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Date: 02/12/2009 01:55 PM
9236772002 Dup
Units Result Result RPD Qualifiers
mg/L ND ND
mg/L 0.18 0.18 .8
mg/L ND ND
mg/L ND ND
mg/L N❑ ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 14

aceAnalytical0
wwwpacelabs com
i
Project: S012809 POND ASH
Pace Project No.: 9236817
SAMPLE DUPLICATE: 230257
Parameter Units
mg/L
mg/L
Selenium
Silver
Date: 02/12/2009 01:55 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
9236772002 Dup
Result Result
ND ND
ND .0031 J
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
wMout the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078,
[phone]
Page 8 of 14

Pace Analytical Services, Inc.
/�,, + �+ J® 2225 Riverside Dr.
aCeJ`if alyfi ra! Asheville, NC 28804
wwwpa"bs.cam [phone]
QUALITY CONTROL DATA
Project: S012809 POND ASH
Pace Project No.: 9236817
QC Batch: MERP/1947 Analysis Method: EPA7470
QC Batch Method: EPA7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples. 9236817001
METHOD BLANK: 230554 Matrix: Mter
Associated Lab Samples: 9236817001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 02/02/0913:31
LABORATORY CONTROL SAMPLE: 230555
pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rae
Parameter Units Cone. Result % Roe Limits Qualifiers
Mercury ug/L 2.5 2.9 116 80-120
MATRIX SPIKE SAMPLE: 230556
9236772002 Spike MS MS % Roe
Parameter Units Result Cone. Result % Roe Limits Qualifiers
Mercury ug/L ND 2.5 3.2 128 75-125 MO
SAMPLE DUPLICATE: 230557
9236810001 Dup .
Parameter Units Result Result RPD Qualifiers
Mercury ug/L 0.234 ND
Date: 02/12/2009 01:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
,ego,
IJ k
Page 9 of 14

aceAnalyticai0
www.pacelabacom
j
Project: S012809 POND ASH
Pace Project No.: 9236817
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP13765 Analysis Method: EPA6010
QC Batch Method: EPA3050 Analysis Description: 6010 MET
Associated Lab Samples: 9236817001
METHOD BLANK: 231198
Associated Lab Samples: 9236817001
Parameter Units
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Iron
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Manganese
mg/kg
Molybdenum
mg ft
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
(Zinc
mg/kg
LABORATORY CONTROL SAMPLE: 231199
Parameter
Arsenic
Barium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Zinc
Date: 02/12/2009 01:55 PM
Matrix: Solid
Blank
Reporting
Result
Limit
Analyzed
ND
0.50
02/03/09 21:00
NO
0.50
02103/09 21:00
NO
0.10
02/03/09 21:00
ND
10.0
02/03/09 21:00
NO
0.50
02/03/09 21:00
NO
0.50
02/03/09 21:00
NO
5.0
02/03/09 21:00
NO
0.50
02/03/09 21:00
NO
10.0
02/03/09 21:00
NO
0.50
02/03/09 21:00
NO
0.50
02/0310921:00
N D
0.50
02/03/09 21:00
ND
500
02/03/09 21:00
ND
1.0
02/03/09 21:00
N D
0.50
02/03/09 21:00
N D
500
02/03/09 21:00
NO
1.0
02/03/09 21:00
Qualifiers
Units
Spike
Conc.
LCS
Result
LCS
% Roo
% Roe
Limits
mg/kg
50
49.6
99
80-120
mg/kg
50
49.3
99
80-120
mg/kg
50
48.8
98
80-120
mg/kg
500
488
98
80-120
mg/kg
50
50.3
101
80-120
mg/kg
50
48.2
96
80-120
mg/kg
500
509
102
80-120
mg/kg
50
49.6
99
80-120
mg/kg
500
496
99
80-120
mg/kg
50
50.3
101
80-120
mg/kg
50
49.3
99
80-120
mg/kg
50
49.0
98
80-120
mg/kg
500
457J
91
80-120
mg/kg.
50
47.8
96
80-120
mg/kg
25
24.3
97
80-120
mg/kg
500
518
104
80-120
mg/kg
50
49.3
99
80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of,Pace Analytical Services, Inc..
Q�XM
mil-Y�dC1.S.:�
Pace Analytical Services, Inc.
9800 K incey Ave. Suite 100
Huntersville, NC 28078
[phone]
QualHiors
Page 10 of 14

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aceAnalyiical
wvrw.pacelabs.oxn
i
I
Project: S012809 POND ASH
Pace Project No.: 9236817
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/4406 Analysis Method: EPA365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 9236817001
METHOD BLANK: 233639 Matrix: Solid
Associated Lab Samples: 9236817001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mgfkg ND 2.0 02110/0909:38
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 233640
Spike LCS LCS % Roo
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 20 18.0 90 90-110
MATRIX SPIKE SAMPLE: 233641
9236786001 Spike MS MS % Roo
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 7740 50.6 3940 -7480 90-110 MO
SAMPLE DUPLICATE: 233643
9236817001 Dup
Parameter Units Result Result RPD Qualifiers
Phosphorus mg/kg 48.4 61.8 24 R1
Date: 02/12/2009 01:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 14

aceAnalytical
www.pacebbs.com
Project: S012809 POND ASH
Pace Project No.: 9236817
QC Batch: WET17173
QC Batch Method: EPAS045
Associated Lab Samples: 9236817001
SAMPLE DUPLICATE: 233743
Parameter Units
pH at 25 Degrees C Std. Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA9045
Analysis Description: 9045 pH
9236786001 Dup
Result Result RPD Qualifiers
6.9 6.9 0
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Date: 02/12/2009 01:55 PM REPORT OF LABORATORY ANALYSIS Page 13 of 14
This report shall not be reproduced, except In Tull,
without the written consent of Pace Analytical Services, Inc..

�aceAnalyfical o
t WWW.P"bb&WM
J
t
QUALIFIERS
Project: S01 2809 POND ASH
Pace Project No.: 9236817
DEFINITIONS
Pace Analytical Services; Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC28078
[phone]
DF - Dilution Factor, If reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Dipheny1hydrazine (8270 listed analyto) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical Is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
MO Matrix spike recovery was outside laboratory control limits.
R1 RPD value was outside control fimits.
Date: 02/12/2009 01:55 PM REPORT OF LABORATORY ANALYSIS Page 14 of 14
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
,.cgoac

—SNU�e z
Energy Generation NA
Please testthe sample(s) for the parametem as Bsted below.
Send invoice and copy of results to:
Ricky Styles
SUEZ_EneW BloPower, Inc. _
2M Old UrAe Rd.
Marion, NO 28752
[phone]
(fax) 756-7160
RRge uested Due Dane:
Send original results to:
Summer Barber 3 Frankie Fox
SUEZ Energy Biopower, Inc.
302 Duke Street
Forest City, NC 28M
summer.barbe Agdfsuezna com
frankIe.LOAcidfsuezna.com
ricky.stvlea adfsuezna.com
[phone]
(fax) 286-1229
8jimple 6
Sample
Semple Dats(s)
Omab or
Total Metals -
TCLP Metals -
lgnlln AW,
pH
Tofel-,l�rsenic
Full TCLP
Descripow
and time sample
Cornposlte
As, Be, Cd, Co.
As, Ba, Cd,
Raa t tyr
Correshrity
collected
Cr, Cu, Fe, Pb,
Cr, Pb, Hg, -
M9. Hg, Mn,
Se, Ag
Ma NI, K, Sa,
Ag, No,Tn,
total
Phosphorus
$012809
POND ASH
1-2M 9:30AM
COMPOSITE
YES
YES
YES
YES
(o$`
Sample sent to: Pace M&Wcar Services, Ir
2225 R,�eraide Drive
Ache&%, NO 20"
828-254.7176
Chan .rs"
Project Rhinager: Kevin Godwin
8800 Kbm Ave m, Suite 100
Hunlenvik NO 20078
(704) 875 - 9092 e4 233
/IAR/-0117t.
li:o�,

Date:
Facility: M W--. I,, a ti
Analyst:
Calibration
Calibration
Time
Cal Buffer
4.0
Cal Buffer
1.0.0_
Check
Buffer 7.0"
Comments
* pH buffer checks are to be within t 0.1 pH units of the standard's true value.
pH Analyses
Sample ID
Time
Sampled
Time
Analyzed
pH Result
Buffer
Check**
Comments
!go I2fro9
C
Indicates a recommended drift check using Buffer 7.0 at the end of testing or every 4 hours minimum.
Results should be within t 0.1 pH units of the standard's true value.

acemalXical
wwwpacelabs.cam
April 27, 2009
Ms. Summer Barber
Suez Energy
302 Duke Street
Forest City, NC 28043
RE: Project: 2009 1ST QTR BOTTOM ASH
Pace Project No.: 9241973
Dear Ms. Barber:
Pace Analytical services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical services, Inc.
9800 runcey Ave. Suite 100
Huntersville, NC 28078
Enclosed are the analytical results for sample(s) received by the laboratory on April 13, 2009. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 1 of 13

1�;a'cieAnalytical
www.pacefabs.com
I
Project: 2009 1ST QTR BOTTOM ASH
Pace Project No.: 9241973
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Charlotte Certification IlDs
West Virginia Certification #: 357
North Carolina Field Services Certification #k 5342
Virginia Certification #: 00213
North Carolina Drinking Water Certification #: 37706
Tennessee Certification #: 04010
New Jersey Certification #: NC012
South Carolina Drinking Water Cert. #: 990060003
Louisianah-ELAP Certification #: 04034
South Carolina Certification #: 990060001
Kentucky UST Certification #: 84
Pennsylvania Certification #: 68-00784
RoridaINELAP Certification # E87627
Connecticut Certification #: PH-0104
North Carolina Wastewater Certification #: 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Asheville Certification iDs
West Virginia Certification #: 356
Pennsylvania Certification #: 68-03578
Virginia Certification #: 00072
North Carolina Wastewater Certification#: 40
Connecticut Certification #. PH-0106
North Carolina Drinking Water Certification It 37712
Florida/NELAP Certification #: E87648
North Carolina Bioassay Certification M 9
Tennessee Certification t 2980
New Jersey Certification t NC011
South Carolina Certification * 99030001
Massachusetts Certification #: M-NC030
South Carolina Bioassay Certification #: 99030002
LouisianalLELAP Certification M 03095
Eden Certification iDs
North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738
Virginia Drinking Water Certification #: 00424
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
9p
Page 2 of 13

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
,��aneAnalytical 2225 Riverside Dr. 9800 IGnceyAve. Suite 100
WVmPacembs.com Asheville, NO 28804 Huntersville, NO 28078
[phone] [phone]
SAMPLE ANALYTE COUNT
Project: 2009 1 ST QTR BOTTOM ASH
Pace Project No.: 9241973
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
9241973001 41309 COMPOSITE ASTM D2974-87
TNM
1
PASI-C
EPA 365.1
TEE
1
PASI-A
EPA6010
JMW
7
PASI-A
EPA 6010
EWS
17
PASI-A
EPA 7470
SHB
1
PASI-A
EPA 7471
SHB
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc._
Cl`. "L11G�1
Page 3 of 13

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
JacMnalXical! 2225 Riverside Dr. 9000 lgncey Ave. Suite 100
www.pacews.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: 2009 1 ST QTR BOTTOM ASH
Pace Project No.: 9241973 .
Sample: 41309 COMPOSITE Lab Iq: 9241973001
Results reported on a 'dry -weight" basis
Parameters Results Units
Collected: 04/13/09 10:15
Report Limit DF
Received:: 04/13/09 12:00 Matrix: Solid
Prepared Analyzed CAS No.
Qua]
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
7.9 mg/kg
0.43
1
04/23/09 09:11
04/23/09 23:32 7440-38-2
M0,R1
Barium
1160 mg/kg
4.3
10
04/23/09 09:11
04/24/09 08:59 7440-39-3
M0,R1
Cadmium
1.1 mg/kg
0.086
1
04/23109.09:11
0412310923:32 7440-43-9
M0,R1
Calcium
75600 mg/kg
86.5
10
04/23109 0901
04124/09 08:59 7440-70-2
MO
Chromium
22.7 mg/kg
0.43
1
04/23/09 09 11
04/23/09 23:32 7440-47-3
M0,R1
Copper
290 mg/kg
0.43
1
04/23/09 09:11
04/23/09 23.32 7440-50-8
M0,R1
Iron
17200 mg/kg
43.2
10
04/23/09 09:11
04/24/09 08:59 7439-89-6
MO
Lead
4.0 mg/kg
0.43
1
04/23/09 09:11
04/23/09 23:32 7439-92-1
M0,R1
Magnesium
13700 mg/kg
86.5
10
04/23/09 0911
04/24/09 08:59 7439-95-4
MD
Manganese
1710 mg/kg
4.3
10
04/23/09 09:11
04/24/09 08:59 7439-96-5
MO
Molybdenum
ND mg/kg
0.43
1
04/23/09 09:11
04/23/09 23:32 7439-98-7
MO
Nickel
10.7 mg/kg
0.43
1
04/23/09 09:11
04/23/09 23:32 7440-02-0
M0,R1
Potassium
23800 mg/kg
4320
10
04/23/09 09:11
04/24/09 08:59 7440-09-7
M0,R1
Selenium
2.2 mg/kg
0.86
1
04/23/09 09:11
04/23/09 23:32 778249-2
M0,R1
Silver
0.44 mg/kg
0.43
1
04/23/09 09:11
04/23/09 23:32 7440-22-4
MO
Sodium
7960 mg/kg
4320
10
04/23/09 09:11
04124/09 08:59 7440-23-5
MO
Zinc
35.2 mglkg
0.86
1
04/23/09 09:11
04/23/09 23:32 7440-66-6
M0,R1
6010 MET ICP, TCLP
Analytical Method: EPA 6010
Preparation Method: EPA
3010
Arsenic
ND mg/L
0.025
1
04/20/09 15.30 04/21/09 15:17 7440.38-2
Barium
2.7 mg/L
0.025
1
04/20/09 15:30
04/21/09 15:17 7440-39-3
Cadmium
ND mg/L
0.0050
1
04/20/0915:,30
04/21/09 15:17 7440-43-9
Chromium
0.045 mg/L
0.025
1
04/20/0915:30
04/21/09 15:17 7440-47-3
Lead
ND mg1L
0.025
1
04/20/09 15:30
04/21/09 15:17 7439-92-1
Selenium
ND mglL
0.050
1
04/20/09 15:30
04/21109 15:17 7782-49-2
Silver
ND mg/L
0.026
1
0412010915:30
04/21/09 15:17 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
W21109 08:30
04/21/09 15:18 7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
ND mg/kg
0.0044
1
04/15/09 11:45
04/15/09 18:55 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
0.33 %
0.10
1
04/16/09 18:30
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
147 mg/kg
9.1
2
04/17/09 19:17 7723-14-0
Date: 04/27/2009 0331 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 13

�aceAnalytical
WW..pacera 3.com
Project: 2009 1ST QTR BOTTOM ASH
Pace Project No.: 9241973
QC Batch: WETA14864
QC Batch Method: EPA 365.1
Associated Lab Samples: 9241973001
METHOD BLANK: 264586
Associated Lab Samples: 9241973001
Parameter
Units
Phosphorus
mglkg
LABORATORY CONTROL SAMPLE:
264587
Parameter
Units
Phosphorus
mg/kg
MATRIX SPIKE SAMPLE:
264588
Parameter
Units
Phosphorus
mg/kg
SAMPLE DUPLICATE: 264589
Parameter
Units
Phosphorus
mg/kg
Date: 0427/2009 03:31 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Pace Analytical Services, Inc.
98o0 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Matrix. Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 04/17/0919:00
Spike LCS LCS %: Rec
Conc. Result % Rec Limits Qualifiers
20 20.4 102 90-110
9241477001 Spike
Result Conc.
3080 74
9241973001 Dup
Result Result
147 163
MS MS
Result Rec
6050 2020
RPD Qualifiers
10
REPORT OF LABORATORY ANALYSIS
This report sha➢ not be reproduced, except in full,
without the written consent of Pace
Analytical Services, Inc_
% Rec
Limits Qualifiers
90-110 MO
Page 5 of 13

aceAnalytical
wwwpacelab.cnrm
Project: 2009 1 ST QTR BOTTOM ASH
Pace Project No.: 9241973
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP/2075 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 9241973001
METHOD BLANK: 263275 Matrix: Solid
Associated Lab Samples: 9241973001
Blank Reporting
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units
Result
Limit
Analyzed Qualifiers
Mercury mg/kg
ND 0.0050
04/1510916:37
LABORATORY CONTROL SAMPLE: 263276
Spike
LCS
LCS % Rec
Parameter Units
Cone.
Result
% Rec Limits Qualifiers
Mercury mg/kg
.067
0.073
109 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 263277
263278
MS
MSD
9241082001
Spike
Spike MS
MSD MS MSD % Rec
Parameter Units Result
Cone. .
Cone. Result
Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.78
.053
.073 0.66
3.0 -223 3100 75-125 129 M0,R1
SAMPLE DUPLICATE: 263279
Parameter
Mercury
Date: 04/27/2009 03:31 PM
9241961005 Dup
Units Result Result
mg/kg 0.0126 0.013
RPD Qualifiers
4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the mitten consent of Pace Analytical Services, Inc._
Page 6 of 13

lacmnalyticala
www.pacelabs.com
Project: 2009 1 ST QTR BOTTOM ASH
Pace Project No.: 9241973
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MERP/2080
Analysis Method:
EPA 7470
QC Batch Method: EPA 7470
Analysis Description:
7470 Mercury TCLP
Associated Lab Samples: 9241973001
METHOD BLANK: 265771
Matrix. Water
Associated Lab Samples: 9241973001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Mercury
ug/L
NO 0.20 04121/0914:08
LABORATORY CONTROL SAMPLE:
265772
Spike LCS
LCS %, Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Mercury
ug/L
2.5 2.7
109 80-120
MATRIX SPIKE SAMPLE:
265773
9241497001 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Mercury
ug/L
NO 2.5
3.1 123 75-125
SAMPLE DUPLICATE: 265774
9241497002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Mercury
ug/L
NO NO
Date: 04/272009 03:31 PM
REPORT OF LABORATORY ANALYSIS
This report shall trot be reproduced, except In full,
without the written consent of Pace Analytical Services. Inc..
. CA
Page 7 of 13

r
aceAnalXical
www.pace1abawm
Project: 2009 1 ST QTR BOTTOM ASH
Pace Project No.: 9241973
QC Batch: PMST/2386
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 9241973001
SAMPLE DUPLICATE: 264038
Parameter Units
Percent Moisture %
SAMPLE DUPLICATE: 264039
Parameter
Percent Moisture
Date: 04/272009 03:31 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: ' Dry Weight/Percent Moisture
9242192008 Dup
Result Result RPD Qualifiers
13.0 13.7 5
9242204010 Dup
Units Result Result
% 20.4 20.7
RPD Qualifiers
2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
OgOq
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersvflle, NC 28078
[phone]
Page 8 of 13

aceAnalytical
www.pacelab3.com
Project 2009 1ST QTR BOTTOM ASH
Pace Project No.: 9241973
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/4184 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 9241973001
METHOD BLANK: 267363
Associated Lab Samples:
Parameter
9241973001 '
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed Qualifiers
Arsenic
mglkg
ND
0.50
04/23/09 23:25
Barium
mg/kg
ND
0.50
04/23/09 23:25
Cadmium
mg/kg
ND
0.10
04/23/09 23:25
Calcium
mg/kg
ND
10.0
04/23/09 23:25
Chromium
mg/kg
ND
0.50
04/23/09 23:25
Copper
mglkg
ND
0.50
04123/09 23:25
Iron
mg/kg
ND
5.0
04/23/09 23:25
Lead
mg/kg
ND
0.50
04/23/09 23:25
Magnesium
mg/kg
ND
10.0
04/23/09 23:25
Manganese
mg/kg
ND
0.50
04/23/09 23:25
Molybdenum
mglkg
ND
0.50
04/23/09 23:25
Nickel
mg/kg
ND
0.50
04/23109 23:25
Potassium
mg/kg
ND
500
04/23/09 23:25
Selenium
mg/kg
ND
1.0
04/23/09 23:25
Silver
mg/kg
ND
0.50
04/23/09 23:25
Sodium
mg/kg
ND
500
04/23/09 23:25
Zinc
mg/kg
ND
1.0
04/23/09 23:25
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
267364
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
44.7
89
80-120
Barium
mg/kg
50
46.9
94
80-120
Cadmium
mg/kg
50
44.9
90
80-120
Calcium
mg/kg
500
467
93
80-120
Chromium
mg/kg
50
44.6
89
80-120
Copper
mg/kg
50
45.6
91
80-120
Iron
mg/kg
500
471
94
80-120
Lead
mg/kg
50
44.6
89
80-120
Magnesium
mg/kg
500
476
95
80120
Manganese
mg/kg
50
45.4
91
.80-120
Molybdenum
mg/kg
50
46.2
92
80-120
Nickel
mg/kg
50
45.1
90
80-120
Potassium
mg/kg
500
433J
87
80-120
Selenium
mg/kg
50
44.6
89
80-120
Silver
mg/kg
25
23.1
92
80-120
Sodium
mglkg
500
476J
95
80-120
Zinc
mg/kg
50
45.6
91
80-120
Date: 04/27/2009 03:31 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 13

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
�aceAnalytical 2225 Riverside Dr. 98001Gncey Ave. Suite 100
www.pacelabs.com Asheville, NC, 28804 Huntersviile, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: 2009 1 ST QTR BOTTOM ASH
Pace Project No.: 9241973
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 267365 267366
Parameter
9241973001
Units Result
MS
Spike
Cone.
MSD
Spike
Cone.
MS
Result
MSD
Result
MS;
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
7.9
47.4
50.2
51.6
22.2
92
28
75-125
80 MO, R1
Barium
mg/kg
1160
47.4
50.2
941
1300
-462
282
75-125
32 M0,R1
Cadmium
mg/kg
1.1
47.4
50.2
35.3
1.1
72
.1
75-125
18B M0,R1
Calcium
mg/kg
75600
474
502
75400
86600
-43
2200
75-125
14 MO
Chromium
mg/kg
22.7
47.4
50.2
69.5
29.4
99
13
75-125
- 81 MO, R1
Copper
mg/kg
290
47.4
50,2
166
1.12
-262
-355
75-125
39 M0,R1
Iron
mg/kg
17200
474
502
16700
16200
-105
-194
75-125
3 MO
Lead
mg/kg
4.0
47.4
50.2
37.7
12.4
71
17
75-125
101 MO, R1 '
Magnesium
mg/kg
13700
474
502
15200
15600
314
381
75-125
3 MO
Manganese
mg/kg
1710
47.4
50.2
1700
1860
-20
289
75-125
9 MO
Molybdenum
mg/kg
ND
47.4
502
33.6
NO
71
0
75-125
MO
Nickel
mg/kg
10.7
47.4
502
442
12.5
71
4
75-125
112 M0,R1
Potassium
mg/kg
23800
474
502
21400
27400
-517
709
75-125
25 M0,R1
Selenium
mg/kg
2.2
47.4
50.2
42.0
3.1
84
2
75-125
173 M0,R1
Silver
mg/kg
0.44
23.7
25.1
22.6
0.50
94
.2
75-125
MO
Sodium
mg/kg
7960
474
502
7660
8320
-64
72
75-125
8 MO
Zinc
mg/kg
35.2
47.4
50.2
80.1
354
'95
636
75-125
126 M0,R1
SAMPLE DUPLICATE: 267367
9242244001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Arsenic
mg/kg
0.50
0.78
35 R1
Barium
mg/kg
9.6
8.7
18
Cadmium
mg/kg
ND
ND
Calcium
mg/kg
136
92.9
45 R1
Chromium
mg/kg
4.9
5.2
1
Copper
mg/kg
1.4
0.97
44 R1
Iron
mg/kg
2740
2660
11
Lead
mg/kg
2.4
2.5
3
Magnesium
mg/kg
68.6
66.2
11
Manganese
mg/kq
6.0
4.1
44 R1
Molybdenum
mg/kg
0.15J
3.3
Nickel
mglkg
0.65
0.68
2
Potassium
mg/kg
127J
108J
Selenium
mg/kg
ND
.591
Silver
mg/kg
ND
ND
Sodium
mg/kg
6AJ
5AJ
Zinc
mg/kg
2.1
1.6
34 R1
Date: 04127/2009 03:31 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
s
Page 10 of 13

IeAnalyficalo
www.pacetabs.com
Project: 2009 1 ST QTR BOTTOM ASH
Pace Project No.: 9241973
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NQ 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
98o0 KnceyAve_ Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MPRP/4160
Analysis Method: EPA 6010
QC Batch Method: EPA 3010
Analysis Description: 6010 MET TCLP
Associated Lab Samples: 9241973001
METHOD BLANK: 265788
Matrix: Water
Associated Lab Samples: 9241973001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Arsenic
mg/L
ND 0.025
04/21/09 15:46
Barium
mg/L
ND 0,026
04/21/09 15:46 ,
Cadmium
mg/L
ND 0.0050
04121/0915:46.
Chromium
mg/L
ND 0.025
0412110915:46
Lead
mg/L
ND 0.025
04/21/0915:46
Selenium
mg/L
ND 0.050
04121/0915:46
Silver
mg/L
ND 0.025
04/21/0915:46
LABORATORY CONTROL SAMPLE:
265789
Spike LCS
LCS %;
Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Arsenic
mg/L
2.5 2.7
109 80-120
Barium
mg1L
2.5 2.4
96
80-120
Cadmium
mg/L
2.5 2.5
101
80-120
Chromium
mg/L
2.5 2.6
102
80-120
Lead
mg/L
2.5 2.3
94
80-120
Selenium
mg/L
2.5 2.7
109
80-120
Silver
mg/L
1.2 1.3
106
80-120
MATRIX SPIKE SAMPLE:
265790
9241497001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/L
ND 2.5
2.8
110
75-125
Barium
mg/L
0.052 2.5
2.4
96
75-125
Cadmium
mg1L
0.052 2.5
2.6
101
75-125
Chromium
mg/L
0.22 2.5
2.8
101
75-125
Lead
mg/L
ND 2.5
2.4
94
75-125
Selenium
mg/L
ND 2.5
2.8
108
75-125
Silver
mg/L
ND 1.2
1.3
107
75-125
SAMPLE DUPLICATE: 265791
9241497002 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Arsenic
mg/L
ND ND
Barium
mg/L
0.26 0.25
5
Cadmium
mg/L
0.11 0.10
7
Chromium
mg/L
1.0 0.98
4
Lead
mgiL
ND ND
Date: 04/2712009 03:31 PM
REPORT OF LABORATORY ANALYSIS
Page 11 of 13
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc

'aceAnalytical
wwwpacelabs.com
1
I
r
Project: 2009 1ST QTR BOTTOM ASH
Pace Project No.: 9241973
SAMPLE DUPLICATE: 265791
Parameter
Selenium
Silver '
Date: 04/27/2009 03:31 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NG28804
[phone]
QUALITY CONTROL DATA
9241497002 Dup
Units Result Result
mg/L ND ND
mg/L ND .018J
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Ina.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 13

laneAnalytical
www.pacelabs.mm
f
I
QUALIFIERS
Project: 20091 ST QTR BOTTOM ASH
Pace Project No.: 9241973
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-0iphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate °% recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
MO Matrix spike recovery was outside laboratory control limits.
R1 RPD value was outside control limits.
Date: 04/27/2009 03:31 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 13

--s%kMoee z
Energy Generation NA
Please test the sample(s) for the parameters as listed below.
Send invoice and copy of results to:
Ricky Styles
SUEZ Energy BioPower, Inc.
2859 Old Linville Rd,.
Marion, NC 28752
[e-mail]
[phone]
(fax) 756-7160
Renuestad Due Datp-
Send original results to:
Summer Barber & Frankie Fox
SUEZ Energy BioPower, Inc.
302 Duke Street
Forest City, NC 28043
[e-mail]
[e-mail]
[phone]
(fax) 286-1229
Sample
Sample -
Sample Dates)
Grab or
Total Metals'-
TCLP Metals -
Ignitabiilty,
pH
Total Arsenic
Full TCLP
Description
and time sample
Composite
As, Ba, Cd, Ca,
As, Ba, Cd,
Reactivity
Corrosivity
collected
Cr, Cu, Fe, Pb,
Cr, Pb, Hg,
Mg, Hg, Mn,
Se, Ag
Mo, NI, K, Se,
Ag, Na, Zn,
12 117 3
total
Phosphorus
41309
20091st QTR
BOTTOM ASH
4-13-0910:15AM
COMPOSITE
YES
YES
YES
2�d l q ?'0QI
Sample sent to: Pace AnaWcal Services, Ir
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Project Manager: Annette Scott
9800 Kimsey Avenue, Suite 100.
Huntersville, NC 28078
(704) 875 - 9092 ext. 233 �'�' c d
Chain kody

Date: LI-13 — 0 � Analyst: R
Facility: /M .4A d+-'
Calibration
Ca ftra inn
u •.
Time .
C' �. "
— l o
4.0
I Ri ad...
al SuftI
10.0
("heck
("heck
Buffer 7.04
Comments
7: 37
/0. 01
7.00
n14 nl lffer checks
ar t b
h' 0
e o e wit in x- .1 pH units of the standard s true value
pH Analyses
Sample IC
Time
Sam led
`lime
Analyzed
PH Result
Buffer
Check,"
Comments
ZI-136
2: 5W
0: os
'� If1 C�I!'.A4PS n rarnmmonrinA
ri
rifl ns, 11
.. n..rc... ••Y n _
•••^•�•���� .+ ..++.+.nnv. wa.� Wnn vnci,n uailly ouimi r.0 aL tile ena or testing or every 4 hours minimum.
Results should be within ± 0.1 pH units of the standard's true value.

laucceeAn'aly'fical
www.pacelabs.com
May 22, 2009
Ms. Summer Barber
Suez Energy
302 Duke Street
Forest City, NC 28043
RE: Project: N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
Dear Ms. Barber:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kncey Ave. Suite 100
Huntersville, NC 26078
Enclosed are the analytical results for sample(s) received by the laboratory on May 07, 2009. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated `in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was .performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 1 of 14

I
eAnalytical
wmpaWabs com
Project: N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Charlotte Certification IDs
West Virginia Certification #: 357
North Carolina Field Services Certification #: 5342
Virginia Certification #: 00213
North Carolina Drinking Water Certification #: 37706
Tennessee Certification #: 04010
New Jersey Certification #: NC012 '
South Carolina Drinking Water Cert. #: 990060003
Louisiana/LELAP Certification #: 04034
South Carolina Certification A 990060001
Kentucky UST Certification #: 84
Pennsylvania Certification #: 68-00784
Flodda/NELAP Certification #: E87627
Connecticut Certification #: PH-0104
North Carolina Wastewater Certification # 12
Asheville Certification IDs
West M ginia Certification #: 356
Pennsylvania Certification #: 68-03578
Virginia Certification #: 00072
North Carolina Wastewater Certification #: 40
Connecticut Certification #: PH-0106
North Carolina Drinking Water Certification # 37712
Florida/NELAP Certification #: E87W
North Carolina Bioassay Certification #: 9
Tennessee Certification #: 2980
New Jersey Certification P NC011
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
South Carolina Bioassay Certification #: 99030002
Louisiana/LELAP Certification #: 03.095
Eden Certification IDs
North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738
Virginia Drinking Water Certification #: 00424
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
��v�1O�yRp'
� 4aLLlS�RI�f,�a
Pace Analytical Services, Inc.
9800 ItlnceyAve. Suits 100
Huntersville, NC 28078
[phone]
Page 2 of 14

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical 2225 Riverside Dr. 9800 KinceyAve: Suite 100
Asheville, NC 28804 Huntersville, NC 28078
VAmpacelabs.com
[phone] [phone]
SAMPLE ANALYTE COUNT
Project: N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
9243711001 N5709 ASTM D2974-87
TNM
1
PASI-C
EPA 365.1
DMN
1
PASI-A
EPA 6010
EWS
7
PASI A
EPA 6010
EWS
17
PASI-A
EPA7470
SHB
1
PASI-A
EPA 7471
SHB
1
PASI-A
EPA 9045
JMIM1I
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
.`sae CA
Page 3 of 14

© Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acmnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville, NC 28804 Hunterwille, NC 28078
rwrw.pacelabs.com
[phone] [phone]
ANALYTICAL RESULTS
Project: N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
Sample: N5709
Lab ID: 9243711001
Collected: 05/07/09 11:30
Received: 05107109 14:12 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Quaff
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
22.7 mg/kg
1.1
1
05/13/09 13:58 05/14/09 18:44 7440-38-2
Barium
1080 mg/kg
1.1
1
05/13/09 13:58 05/14/09 18:44 7440-39-3
Cadmium
1.7 mg/kg
0.21
1
05/13/09 13:58 05/14109 18:44 7440-43-9
Calcium
80400 mg/kg
212
10
05/13/09 13:58 05115/09 10:24 7440-70-2
Chromium
30.6 mg/kg
1.1
1
05/13/09 13:58 05/14/09 18:44 7440-47-3
Copper
134 mg/kg
1.1
1
05/13/09 13:58 05/14/09 18:44 7440-50-8
Iron
12600 mg/kg
10.6
1
05/1310913:58 0511410918:44 7439-89-6
Lead
50.1 mg/kg
1.1
1
05/13/09 13:58 05114/0918:44 7439-92-1
Magnesium
13600 mg/kg
21.2
1
05/13/09 13:58 05/14/09 18:44 7439-95-4
Manganese
1700 mg/kg
1.1
1
05/13/09 13:58 05/14/09 18:44 7439-96-5
Molybdenum
ND mg/kg
1.1
1
05/13/09 13:58 05/14/09 18:44 7439-98-7
Nickel
15.7 mg/kg
1.1
1
05/13/09 13:58 05/1410918:44 7440-02-0
Potassium
17200 mg/kg
10600
10
05113/0913:58 05115/09 10:24 7440-09-7
Selenium
4.2 mg/kg
2.1
1
0511310913:58 05/14/09 18:44 778249-2
Silver
1.2 mg/kg
1.1
1
0511310913:58 05/14/09 18.44 7440-22-4
Sodium
6900 mg/kg
1060
1
05113/09 13:58 05/14/09 18:44 7440-23-5
Zinc
215 mg/kg
2.1
1
05/13/09 13:58 05114/09 18:44 7440-66-6
3010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
0.052 mg/L.
0,025
1
05/21/09 12:30 05121/0917:12 7440-38-2
Barium
3.1 mg/L
0.025
1
0512110912:30 05121/0917:12 7440.39-3
Cadmium
0.0094 mg/L
0.0050
1
05/2110912:30 05/21/09 17:12 7440-43-9
Chromium
ND mg/L
0.025
1
05/21/09 12:30 05/2110917:12 7440-47-3
Lead
ND mg/L
0.025
1
05/21/09 12:30 05/21/09 17:12 7439-92-1
Selenium
ND mg/L
0.050
1
05121/0912:30 0512110917:12 7782-49-2
Silver
ND mg/L
0.025
1
05/2110912:30 05121/0917:12 7440-22-4
7470 Mercury, TCLP AnalyGca► Method: EPA 7470 Preparation Method: EPA 7470
Mercury
7471 Mercury
Mercury
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
)ate: 05/22/2009 10:33 AM
ND ug/L
0.20
1 05/21/09 12:30
05121/0916:00 7439-97-6
Analytical Method: EPA 7471 Preparation Method: EPA 7471
0.026 mg/kg
0.0093
1 05/15109 11:30
05115/09 18:09 7439-97-6
Analytical Method: ASTM D2974-87
53.8 %
0.10
1
05/14/09 09:08
Analytical Method: EPA 9045
9.5 Std. Units
0.10
1
05/12/09 11:25 H1
Analytical Method: EPA 365.1
105 mg/kg
7.7
1
05/19/09 21:37 7723-14-0 MO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,
Page 4 of 14

® Pace Analytical Services, Inc.
aceMalytical 2225 Riverside Dr.
www.pacelabs.com Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
QC Batch: MPRP/4410 Analysis Method: EPA6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET TCLP
Associated Lab Samples: 9243711001
METHOD BLANK: 282567
Associated Lab Samples: 9243711001
Parameter
Units
Arsenic
mg1L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg1L
Selenium
mg/L
Silver
mg/L
LABORATORY CONTROL SAMPLE:.
282568
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg1L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg1L
MATRIX SPIKE SAMPLE:
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
SAMPLE DUPLICATE: 282570
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
)ate: 05/22/2009 10:33 AM
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
0.025
0512110915:55 -
ND
0.025
05/2110915:55
ND
0.0050
05/21/0915:55
ND
0.025
05/2110915:55
ND
0.025
05/21/0915:55
ND
0.050
05/2110915:55
ND
0.025
05/2110915:55
Pace Analytical Services, Inc.
9800 linter Ave. Suite 100
Huntersviile, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Conc.
Result
% Rec
Limits Qualifiers
2.5
2.7
108
80-120
2.5
2.4
94
.80-120
2.5
2.4
97
80-120
2.5
2.4
98
80-120
2.5
2.3
91
80-120
2.5
2.7
109
80-120
1.2
1.3
102
80-120
282569
9243405001
Spike
MS
MS
% Rec
Units
Result
Conc.
Result'
% Rec
Limits Qualifiers
mg/L
0.19
2.5
3.3
124
75-125
mg/L
ND
2.5
2.4
96
75-125
mg/L
0.022
2.5
2.3
92
75-125
mg/L
ND
2.5
2.6
105
75-125
mg/L
0.026
2.5
2.0
81
75-125
mg/L
ND
2.5
3.0
119
75-125
mg/L
ND
1.2
1.6
125
75-125
9243701007 Dup
Units Result Result RPD Qualifiers
mg/L ND ND
mg/L 0.091 0.098 7
mg/L ND ND
mg/L ND ND
mg/L 0.64 0.69 7
REPORT OF LABORATORY ANALYSIS Page 5 of 14
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

faceAnalXical
w mvpacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828)254=7176
QUALITY CONTROL DATA
Project N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
SAMPLE DUPLICATE: 282570
9243701007 Dup
Parameter Units Result Result RPD
Selenium mg/L ND ND
Silver mg/L ND ND
)ate: 05/22/2009 10:33 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
"ii.lfriCJS..] s
Qualifiers
Pace Analytical Services, Inc.
9800 IGncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 14

aceAnalytical
wwwpacala6acom
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
QC Batch: MPRP/4327 Analysis Method: EPA6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 9243711001
METHOD BLANK: 276841
Associated Lab Samples:
Parameter
9243711001
Units
Matrix. Solid
Blank Reporting
Result Limit
Analyzed Qualifiers
Arsenic
mglkg
NO
0.50
05/1410916:51
Barium
mg/kg
ND
0.50
05/14/0916:51
Cadmium
mg/kg
ND
0.10
05/14/0916:61
Calcium
mg/kg
NO
10.0
0511410916:51
Chromium
mg/kg
NO
0.50
05114/0916:51
Copper
mg/kg
NO
0.50
05114/0916:51
Iron
mglkg
ND
5.0
05114/0916:51
Lead
mg/kg
NO
0.50
05/1410916:51
Magnesium
mg/kg
NO
10.0
05114/0916:51
Manganese
mg/kg
NO
0.50
05/14/0916:51
Molybdenum
mg/kg
NO
0.50
05114/0916:61
Nickel
mg/kg
NO
0.50
0511410916:51
Potassium
mg/kg
NO
500
05/14/0916:51
Selenium
mg/kg
ND
1.0
05/14/0916:51
Silver
mg/kg
NO
0.50
0511410916:51
Sodium
mg/kg
NO
500
05/1410916:51
Zinc
mg/kg
NO
1.0
05/1410916:51 '
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
276842
Units
Spike
Conc. '
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mglkg
50
49.2
98
80-120
Barium
mg/kg
50
49.5
99
80-120
Cadmium
mglkg
50
49.2
98
8D-120
Calcium
mg/kg
500
504
101
80-120
Chromium
mg/kg
50
49.1
98
80-120
Copper
mg/kg
50
49.1
98
80-120
Iron
mg/kg
500
508
102
80-120
Lead
mglkg
50
48.6
97
80-120
Magnesium
mg/kg
500
506
101
80-120
Manganese
mg/kg
50
49.5
99
80-120
Molybdenum
mg/kg
50
49.1
98
80-120
Nickel
mg/kg
50
49.4
99
80-120
Potassium
mg/kg
500
454J
91
'80-120
Selenium
mg/kg
50
48.1
96
80-120
Silver
mg/kg
25
24.8
99
80-120
Sodium
mg/kg
500
509
102
80-120
Zinc
mg/kg
50
47.9
96
80-120
)ate: 05/22/2009 10:33 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 14

°aceAnalytical
VMW.Pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
Pace Analytical Services, Inc.
9800 KnceyAve. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
277399
Units
9243806020
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
1.0
48.5
45.7
92
75-125
Barium
mg/kg
92.3
48.5
139
95
75-125
Cadmium
mgikg
0.89
48.5
43.7
88
75-125
Calcium
mg/kg
55.2
485
493
90
75-125
Chromium
mg/kg
1.8
48.5
46.1
91
75-125
Copper
mg/kg
9.2
48.5
57.4
99
75-125
Iron
mg/kg
13000
485
14100
246
75-125 MO
Lead
mgikg
17.3
48.5
53.0
74
75-125 MO
Magnesium
mg/kg
2590
485
3290
144
75-125 MO
Manganese
mg/kg
654
48.5
611
-88
75-125 MO
Molybdenum
mg/kg
ND
48.5
41.9
86
75-125
Nickel
mg/kg
0.52
48.5'
42.3
86
75-125
Potassium
mg/kg
5970
485
7510
319
75-125 MO
Selenium
mg/kg
1.9
48.5
44.8
88
75-125
Silver
mg/kg
ND
24.2
23.4
96
75-125
Sodium
mg/kg
ND
485
751
134
75-125 MO
Zinc
mg/kg
49.7
48.5
98.7
101
75-125
SAMPLE DUPLICATE: 277400
Parameter
Units
9243806021
Result
Dup
Result
RPD Qualifiers
Arsenic
mg/kg
0.95
1.6
52 R1
Barium
mg/kg
50.9
79.5
44 R1
Cadmium
mg/kg
ND
0.14
Calcium
mg/kg
ND
6.7J
Chromium
mg/kg
ND
.27J
Copper
mg/kg
ND
0.90
Iron
mg/kg
4940
7440
40 R1
Lead
mg/kg
19.9
32.8
49 R1
Magnesium
mg/kg
717
1440
67 R1
Manganese
mg/kg
753
1430
62 R1
Molybdenum
mg/kg
ND
ND
Nickel
mg/kg
ND
ND
Potassium
mg/kg
1310
2740 ,
70 R1
Selenium
mg/kg
ND
1.4
Silver
mgikg
ND
.15J
Sodium
mgikg
ND
114J
Zinc .
mg/kg
17.0
32.4
63 R1
)ate: 05/22/2009 10:33 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
"a
Page 8 of 14

�aceAnalytical
www.pacelabs.com
I
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
Pace Analytical Services, Inc.
9800 rincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MERP/2142
Analysis Method: EPA 7471
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 9243711001
METHOD BLANK: 278945
Matrix: Solid
Associated Lab Samples: 9243711001
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Mercury mg/kg
ND 0.0050 05/1510918:04 '
LABORATORY CONTROL SAMPLE: 278946
Spike LCS LCS °% Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Mercury mg/kg
.067 0.075 112 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 278947
278948
MS MSD
9243711001
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result 'Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.026
.13 .15 0.16 0.18 106 109 75-125 13
SAMPLE DUPLICATE: 278949
9243798001 Dup
Parameter Units
Result Result RPD Qualifiers
Mercury mg/kg
0.076 0.074 2
)ate: 05/22/2009 10:33 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc:.
:1 Y f Y.lQ�,.] s
Page 9 of 14

IeAnalytical
www.pacelabs.com
Paco Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
QC Batch: WETA/5106 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 9243711001
METHOD BLANK: 281289
Associated Lab Samples: 9243711001
Parameter
Units
Phosphorus
mg/kg
LABORATORY CONTROL SAMPLE:
281290
Parameter
Units
Phosphorus
mg/kg
MATRIX SPIKE SAMPLE:
281291
Parameter
Units
Phosphorus
mg/kg
SAMPLE DUPLICATE: 281292
Parameter Units
Phosphorus mg/kg
)ate: 05/22/2009 10:33 AM
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 05/19/09 21:37
Spike LCS LCS
Conc. Result % Rec
20 20.8 104
9243711001 Spike MS
Result Conc. Result
105 90.3 216
9244249001 Dup
Result Result
1230 1800
Paco Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
% Rec
Limits Qualifiers
90-110
MS % Rec
% Rec Limits Qualifiers
123 90-110 Mo
RPD Qualifiers
37 R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
e� a
Page 10 of 14

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 8800 tanceyAve. Suite 100
:5a'aeAnalXical Asheville, NC 28804 Huntersville, NC 28078
www.pacelabs,cam
i (828)254,7176 [phone]
I
QUALITY CONTROL DATA
Project: N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
QC Batch: PMST/2456 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9243711001
SAMPLE DUPLICATE: 278370
9243811007 Dup
Parameter Units Result Result RPD 'Qualifiers
Percent Moisture % 85.1 85.5 .5
SAMPLE DUPLICATE: 278371
9244062013 Dup
Parameter Units Result Result
Percent Moisture % 14.4 14.0
)ate: 0522/2009 10:33 AM
RPD Qualifiers
3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,.
Page 11 of 14

® Pace Analytical Services, Inc.
lvneAnalXical 2225 Riverside Dr.
www.pacelabs.com Asheville, NC 28804
(828)25477176
QUALITY CONTROL DATA
Project: N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
QC Batch: MERP/2158 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 9243711001
METHOD BLANK: 282554
Associated Lab Samples: 9243711001
Parameter Units
Mercury ug/L
LABORATORY CONTROL SAMPLE: 282555
Parameter Units
Mercury ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.20 05121/0916:37
Pace Analytical Services, Inc.
9800 lGncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
2.5 2.5 99 80-120
MATRIX SPIKE SAMPLE: 282556
9243606001 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
Mercury ug/L ND 2.5 2.8 112 75-125
SAMPLE DUPLICATE: 282557
Parameter
Mercury
)ate: 05/22/2009 10:33 AM
9243606002 Dup
Units Result Result
ug/L ND ND
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�las..1 Q
Page 12 of 14

aceAnalytical
vmw.pacalabs.ccrm
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: N5709 NORTH SCRUBBER. POND ASH
Pace Project No.: 9243711
QC Batch: WET/8243 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 9243711001
SAMPLE DUPLICATE: 276857
Parameter
pH at 25 Degrees C
)ate: 05/2212009 10:33 AM
9243305004 Dup
Units Result • Result
Std. Units 5.3 5.2
RPD Qualifiers
2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(/04)875-9092
Page 13 of 14

o Pace Analytical Services; Inc. Pace Analytical Services, Inc.
eAnalylical 2225 Riverside Dr. 9800 KnceyAve. Suite 100
_ ac
www.pacalabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALIFIERS
Project: N5709 NORTH SCRUBBER POND ASH
Pace Project No.: 9243711
DEFINITIONS
DF - Dilution Factor, if reported, representsthe factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed anatyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical Is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PAST -A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
MO Matrix spike recovery was outside laboratory control limits.
R1 RPD value was outside control limits.
)ate: 05/22/2009 10:33 AM REPORT OF LABORATORY ANALYSIS Page 14 of 14
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
fC
ILL

Energy Generation NA
Please test the sample(s) for the parameters as listed below.
Send invoice and copy of results to:
Ricky Styles
SUFZ Energy BioPower, Inc.
2859 Old Linville Rd.
Marlon, NC 28762
[phone]
(fax) 756-7160
Renuested Due Date.
Send original results to:
Summer Barber & Frankie Fox
SUEZ Energy BioPower, Inc.
302 Duke Street
Forest City, NC 28043
summer. barberCWgdfsuezna.corn
frankie.foxCa.gdfsuezna.com
ricky.sty les(o)gdfsuezna.com
[phone]
(fax) 286-1229
Sample #
Sample
Sample Date(s)
Grab or
Total Metals -
TCLP. Metals
Ignitability,
pH
Total -Arsenic
Full TCLP
Description
and time sample
Composite
As, Ba, Cd,
As, Ba, Cd,
Reactivity
Corrosivity
collected
Ca, Cr, Cu, Fe,
Cr, Pb, Hg,
Pb, Mg, Hg,
Se, Ag
Mn, Mo, Ni, K,
Se, Ag, Na,
Zn, total
Phosphorus
NORTH
N5709
SCRUBBER
5/7/09 11:30AM
COMPOSITE
YES
YES
YES
YES
POND ASH
Sample sent to: Pace Analytical Services,
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Project Manager: Kevin Godwin
9800 Kincey Avenue, Suite 10C
Huntersville, NC 28078
(704) 875 - 9092 ext. 233
Chain of Custody

Date: 7 - 4 s Analyst: �tC41 J7r/�.3
Facility: _ *4,j ,,l
Calibration
Calibration
-Time
r-gg
vul Buffer
4.0
�a 1 u
Cal Buller
10.0-
na.. �.
LIICck
Suffer 7.01
Comments
/O:no
y.pv
/p.el
(o.�tg
- /
2Z•�G
'w ..LI L...LL---,-----
-
p i-1 uuliei cl iecks are to be within t 0.1 pH units of the standard's true value
pH Analyses
Sample ID
Time
Sampled
Time
Analyzed
pH Result
Buffer
Check**
Comments
N5- D
ln:
0;3D
Z,YG
Indicates a iecdlnniendeu onrt cnecK using buffer 7.0 at the end of testing or every 4 hours minimum.
Results should be within t 0.1 pH units of the standard's true value.

jaceAnalytical
f wwwpacelabs co n
f
July 15, 2009
Ms. Summer Barber
Suez Energy
302 Duke Street
Forest City, NC 28043
RE: Project: 2QTR70609 BOTTOM ASH
Pace Project No.: 9247912
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 t0ncey Ave. Suite 100
Huntersville, NC 28078
Dear Ms. Barber:
Enclosed are the analytical results for sample(s) received by the laboratory on July 06, 2009. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated .in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
C�'z - �"z-1
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This repot shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
1
[phone]
Page 1 of 11

laceAnalytical
wvnvpacelabs.com
Project: 2QTR70609 BOTTOM ASH
Pace Proiect No.: 9247912
Charlotte Certification IDs
West Virginia Certification P. 357
Virginia Certification #: 00213
Tennessee Certification #: 04010
South Carolina Drinking Water Cen. #: 990060003
South Carolina Certification#: 990060001
Pennsylvania Certification #: 68-00784
Connecticut Certification #: PH-0104
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
North Carolina Field Services Certification #: 5342
North Carolina Drinking Water Certification #: 37706
New Jersey Certification #: NC012
Louisiana/LELAP Certification #: 04034
Kentucky UST Certification #: 84
Flodda/NELAP Certification #: E87627
North Carolina Wastewater Certification #: 12
Pace Analytical Sorvlces, Inc.
9800 IGncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Asheville Certification IDs
West Virginia Certification #: 356
Pennsylvania Certification #: 68-03578
Virginia Certification #: 00072
North Carolina Wastewater Certification #: 40
Connecticut Certification #: PH-0106
North Carolina Drinking Water Certification #: 37712
Florida/NELAP Certification #: E87648
North Carolina Bioassay Certification #: 9
Tennessee Certification #: 2980
New Jersey Certification P. NC011
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
South Carolina Bioassay Certification #: 99030002
Louisiana/LELAP Certification # 03095
Eden Certification IDa
North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738
Virginia Drinking Water Certification #: 00424
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
(1 1c1aic:
Page 2 of 11

�aceAnalytical
www.pacelabs.com
Project: 2QTR7D609 BOTTOM ASH
Pace Project No.: 9247912
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 IGncey Ave. Suite 100
Huntersviile, NC 28078
[phone]
Analytts
Lab ID Sample ID Method
Analysts
Reported
Laboratory
9247912001 BOTTOM ASH ASTM D2974-87
TNM
1
PASI-C
EPA365.1
JDA
1
PASI-A
EPA 6010
SHB
17
PASI-A
EPA7471
SAJ
1
PASI-A
EPA 9045
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
AGCOR�'
f/�,yM�y�.��,�(/���\/fin
r Ala -1./��
\a
Page 3 of 11

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
f� gaceHllaly�ical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville, NC 28804 Huntersville, NC 28078
www pacalabs cam
[phone] [phone]
ANALYTICAL RESULTS
Project: 2QTR70609 BOTTOM ASH
Pace Project No.: 9247912
Samplo: BOTTOM ASH Lab ID: 9247912001 Collected: 07/06/09 09:30 Received: 07/06/0912:00 Matrix Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
20.0 mg/kg
0.45
1
07/08/09 15:35 07/10109 16:08 7440-38-2
Barium
1280 mg/kg
4.5
10
07/08/09 15:35 07/1010916:35 7440-39-3
Cadmium
1.7 mg/kg
0.089
1
07/08/09 115:35 07110/0916:08 7440-43-9
Calcium
92700 mg/kg
179
20
07/08/09 15:35 07/10/09 16:40 7440-70-2
MO
Chromium
62.3 mg/1<9
0.45
1
07/08/09 15:35 07/10/09 16:08 744047-3
MO
Copper
234 mg/kg
6.45
1
07/08/09 15:35 07/10/09 16:08 7440-50-8
MO
Iron
18700 mg/kg
44.7
10
0710810915:35 07/1010916:35 7439-89-6
MO
Lead
831 mg/kg
0.45
1
07/0a/0915:35 07/10109 16:08 7439-92-1
MO
Magnesium
12700 mg/kg
89.5
10
07/0810915:35 0711010916:35 7439-95-4
MO
Manganese
2320 mg/kg
4.5
10
07/08/09 15:35 07/10/09 16:35 7439-96-5
MO
Molybdenum
ND mg/kg
0.46
1
0710810915:35 0711010916:08 7439-98-7
Nickel
14.8 mg/kg
0.45
1
07/08/09 15:35 07110/09 16:08 7440-02-0
Potassium
ND mg/kg
447
1
0710810915:35 07/09/09 22:31 7440-09-7
MO
Selenium
3.3 mglkg
0.89
1
07/08/09 15:35 07/10/09 16:08 7782.49-2
Silver
0.79 mg/kg
0.45
1
07/0810915:35 07/10/09 16:08 7440-22-4
Sodium
8280 mg/kg
447
1
07108/09 15:35 07/10/09 16:08 7440-23-5
MO
Zinc
687 mg/kg
0.89
1
07/08/09 15:35 07/10109 16:08 7440-6M
MO
7471 Mercury
Analytical Method: EPA 7471 Prepara►ion Method: EPA 7471
Mercury
ND mg/kg
0.0047
1
07/13/09 10.45 07/14/09 11:16 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
0.20 %
0.10
1
07/08/09 13:57
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
11.6 Std. Units
0.10
1
07/08/09 16:00
366.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
35.9 mg/kg
7.2
2
07/12/09 12:49 7723-14-0
Date: 0711 W009 09:55 AM REPORT OF LABORATORY ANALYSIS Page 4 of 11
This report shell not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
i oo"U,

aceAnalytical
www.pwelabs.c=
Project: 2QTR70809 BOTTOM ASH
Pace Project No.: 9247912
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/4704 Analysis Method: EPA6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 9247912001
METHOD BLANK: 305012
Associated Lab Samples:
Parameter
9247912001
Units
Matri)c Solid
Blank Reporting
Result Limit
Analyzed
Arsenic
mglkg
ND
0,50
07/1010916:16
Barium
mg/kg
ND
0.50
0711010916:16
Cadmium
mg/kg
ND
0.10
0711010916:16
Calcium
mg/kg
ND
10.0
07/1010916:16
Chromium
mglkg
ND
0.50
07110/0916:16
Copper
mg/kg
ND
0.50
0711010916:16
Iron
mg/kg
ND
5.0
07/10/0916:16
Lead
mg/trq
ND
0.50
07/10/0916:16
Magnesium
mglkg
ND
10.0
0711010916:16
Manganese
mg/kg
ND
0.50
0711010916:16
Molybdenum
mg/kg
ND
0.50
07/10/0916:16
Nickel
mg/kg
ND
0.50
07110/0916:16
Potassium
mglkg
ND
500
0711010916:16
Selenium
mg/kg
ND
1.0
0711010916:16
Silver
mg/kg
ND
0.50
0711010916:16
Sodium
mglkg
ND
500
07/1010916:16
Zinc
mg/kg
ND
1.0
07/1010916:16
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
305013
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Arsenic
mg/kg
50
48.6
97
80-120
Barium
mg/kg
50
46.9
94
80-120
Cadmium
mg/krq
50
50.1
100
80-120
Calcium
mg/kg
500
531
106
80-120
Chromium
mg/kg
50
51.2
102
80-120
Copper
mg/kg
50
45.4
91
80-120
Iron
mg/kg
500
506
101
80-120
Lead
mg/kg
50
49.4
99
80-120
Magnesium
mg/kg
500
482
96
80-120
Manganese
mglkg
50
60.3
101
80-120
Molybdenum
mg/kg
50
50.4
101
80-120
Nickel
mg/kg
50
49.5
99
80-120
Potassium
mg/kg
500
429J
86
80-120
Selenium
mglkg
50
48.3
97
.80120
Silver
mglkg
25
24.8
99
80-120
Sodium
mg/kg
500
474J
95
80-120
Zinc
mg/kg
50
51.1
102
80-120
Date: 07/15/2009 09:55 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
midact.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvlle, NC 28078
[phone]
Qualifiers
Page 5 of 11

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
te 100
aceAnalytical ® Asheville, NC Riverside804 Dr 9800Hunter viI e, NC'28078
www.pacelabs.com
(826)254-117e [phone]
1
QUALITY CONTROL DATA
Project: 2QTR70609 BOTTOM ASH
Pace Project No.: 9247912
MATRIX SPIKE SAMPLE:
Parameter
305014
Units
9247912001
Result
Spike
Cone.
MS MS
Result % Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
20.0
43.2
60.0
93
75-125
barium
mg/kg
1280
43.2
1320
100
75-125
Cadmium
mg/kg
1.7
43.2
37.1
82
75-125
Calcium
mg/kg
92700
432
81600
-2570
75-125 MO
Chromium
mg/kg
62.3
43.2
92.5
70
75-125 MO
Copper
mg/kg
234
432
236
4
75-125 MO
Iron
mg/kg
18700
432
19400
157
75-125 MO
Lead
mg/kg
831
43.2
485
-801
76-125 MO
Magnesium
mg/kg
12700.
432
11200
-354
75-125 MO
Manganese
mg/kg
2320
43.2
2470
365
75-125 MO
Molybdenum
mg/kg
ND
43.2
34.7
80
75-125
Nickel
mglkg
14.8
43.2
52.3
87
75-125
Potassium
mg/kg
ND
432
22300
5160
75-125 MO
Selenium
mg/kg
13
43.2
42.0
90
75-125
Silver
mg1kg
0.79
21.6
23.1
103
75-125
Sodium
mg/ity
8280
432
7750
-122
75-125 MO
Zinc
mg/kg
687
43.2
3670
6890
75-125 MO
SAMPLE DUPLICATE: 305015
9247938001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Arsenic
mg/kg
0.77
.511
Barium
mg/kg
67.0
51.0
27 R1
Cadmium
mg/Itq
ND
ND
Calcium
mg/kg
98.1
187
62 RI
Chromium
mg/kg
6.3
6.0
5
Copper
mg'kg
10.6
5.9
56 R1
Iron
mg/kg
6940
6550
6
Lead
mg/kg
10.4
6.4
47 R1
Magnesium
mg/kg
1540
1410
8
Manganese
mg/kg
511
328
43 R1
Molybdenum
mgfkg
0.65
19J
Nickel
mg/kg
4.5
3.8
16
Potassium
mg/kg
ND
1980
Selenium
mg/itq
ND
.91
Silver
mg/kg
0.0891
ND
Sodium
mg/kg
34.5J
26.8J
Zinc
mg/kg
31.4
29.5
6
Date: 07/15/2009 09;55 AM
REPORT OF LABORATORY ANALYSIS.
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 11

aceAnalytical
( avnxpacalabs.=
{
Project: 20TR70609 BOTTOM ASH
Pace Project No.: 9247912
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WET18937 Analysis,Method: EPA9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 9247912001
SAMPLE DUPLICATE: 305065
9247765001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 12.4 12.4 0
Date: 07115=09 09:55 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc -
Pace Analytical Services, Inc.
9800 Kncey Ave. Suite 100
Huntersviile, NC 28078
(704)87&9092
Page 7 of 11

Pace Analytical Services,; Inc. Pace Analytical Services, Inc.
,,
® 2225 Riverside Dr. 98M IGnceyAve. Suite 100
acemaIxical Asheville, NC 28804 Huntersvflle, NC 28078
www.pacelabs.com
[phone] [phone]
QUALITY CONTROL DATA
Project 2QTR70609 BOTTOM ASH
Pace Project No.: 9247912
QC Batch: MERP12259.
Analysis Method: EPA7471
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 9247912001
METHOD BLANK: 305962
Matrix: Solid
Associated Lab Samples: 9247912001
Blank Reporting
Parameter
Units
Result Limit Analyzed
Quaffers
Mercury
mg/kg
ND 0.0050 07/14/0910:27
LABORATORY CONTROL SAMPLE:
305963
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Mercury
mg/kg
.067 0.058 86
80-120
MATRIX SPIKE SAMPLE:
305964
9247963005 Spike MS
MS % Rec
Parameter
Units
Result Conc. Result
% Rec Limits Qualifiers
Mercury
mg/kg
0.0069 .067 0.064
85 75-125
SAMPLE DUPLICATE: 305965
9247963006 Dup
Parameter
Units
Result Result RPD
Qualifiers
Mercury
mg/kg
0.011 0.015 29 R1
Date: 07/15/2009 09:55 AM REPORT OF LABORATORY ANALYSIS Page 8 of 11
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services. Inc. Pace Analyticat Services, Inc.
aceAnalyiical ca 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville, NC 28804 Huntersville, NC 28078
www.pacelabs.wm 875-9092
[phone] (704 )
QUALITY CONTROL DATA
Project 2QTR70609 BOTTOM ASH
Pace Project No.: 9247912
QC Batch: WETA/5444
Analysis Method:
EPA 365.1
QC Batch Method: EPA365.1
Analysis Description:
365.1 Phosphorus, Total
Associated Lab Samples: 9247912001
METHOD BLANK: 306176
Matrix: Solid
Associated Lab Samples: 9247912001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Phosphorus
mg/kg
ND
2.0 07112/0912:34
LABORATORY CONTROL SAMPLE:
306177
Spike LCS
LCS % Pec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Phosphorus
mg/kg
20 18.4
92 90-110
MATRIX SPIKE SAMPLE:
306178
9247906004 Spike
MS MS % Rec
Parameter
Units
Result Cone.
Result % Rec Limits Qualifiers
Phosphorus
mg/kg
1980 31.2 1910 -211 90-110 MO
SAMPLE DUPLICATE: 306179
9247757001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Phosphorus
mg/kg
161
129 22 R1
Date: 07/1512009 09:55 AM REPORT OF LABORATORY ANALYSIS Page 9 of 11
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�o�a�

aceAnalyfical
www.pacatsbs.com
Project: 20TR70609 BOTTOM ASH
Pace Project No.: 9247912
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(628)254,7178
QUALITY CONTROL DATA
QC Batch: PMST/2575 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9247912001
SAMPLE DUPLICATE: 304742
9247665010 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 5.7 5.5 2
SAMPLE DUPLICATE: 304743
9248034001 pup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 18.3 18.9 4
Date: 07/15/2009 09:55 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 11

aceAnalytical
www.pacelabsxam
QUALIFIERS
Project: 2QTR70609 BOTTOM ASH
Pace Project No.: 9247912
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M0 Matrix spike recovery was outside laboratory control limits.
R1 RPD value was outside control limits.
Date: 07/15/2009 09:55 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 11 of 11

Energy Generation NA
Please test the sample(s) for the parameters as listed below.
Send invoice and copy of results to
Ricky Styles
SUEZ Energy BioPower, Inc.
2869 Old Linville Rd.
Marion, NC 28752
[e-mail]
[phone]
(fax) 756-7160
Reauested Due Date:
Send original results to:
Summer Barber
SUEZ Energy BioPower, Inc.
1990 PostOak Blvd. Suite 1900
Houston _, TX 77056
summer. barber(c-)gdfsuezna.com
713-636-1639
Sample #
Sample
Sample Date(s)
Grab or
Total Metals -
TCLP Metals
Ignitability,
pH
Total -Arsenic
Full TCLP
Description
and time sample
Composite
As, Ba, Cd,
As, Ba, Cd,
Reactivity
Corrosivity
collected
Ca, Cr, Cu, Fe,
Cr, Pb, Hg,
Pb, Mg, Hg,
Se, Ag
Mn, Mo, Ni, K,
Se, Ag, Na,
Zn, total
Phosphorus
2QTR70609
BOTTOM ASH
7-6-09 9:30AM
COMPOSITE
YES
YES
YES
Sample sent to:
Pace Analytical Services,
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Project Manager. Kevin Godwin
9800 Kincey Avenue, Suite 10C
Huntersville, NC 28078
(704) 875 - 9092 ext. 233
Chain of Custodv

Date: -7P (p- 0
Facility: `K �}rt-•�J�✓
Analyst:
Calibration
Calibration
Time
Cal Buffer
4.0
Cal Ba;ffer
10.0
Ch eck
Buffer 7.04
Comments
:30
`.
10.01
7.01
D
Z 2.
* pH buffer checks are to be within t 0.1 pH units of the standard's true value
pH Analyses
Sam le ID
Time
Sampled
Time
Anal zed
Result
Buffer
Check"
Comments
-7. 01
Z 2 . G
Indicates a recommended drift check using Buffer 7.0 at the end of testing or every 4 hours minimum.
Results should be within t 0.1 pH units of the standard's true value.

acmnalydical
www.pacslabs.com
August 21, 2009
Ms. Summer Barber
Suez Energy
302 Duke Street
Forest City, NC 28043
RE: Project: SP81309 SOUTH' POND ASH
Pace Project No.: 9250804
Dear Ms. Barber:
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
Enclosed are the analytical results for sample(s) received by the laboratory on August 13, 2009. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NEIAC standards, where applicable, unless otherwise narratedin the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Erin Waters for
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 1 of 17

acmnalytical
wwvw.pacelabs.com
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
Pennsylvania Certification IDs
Alabama Certification M 41590
Arizona Certification #: AZ0734
Arkansas Certification
Califomia/NELAC Certification #: 04222CA
Colorado Certification
Connecticut Certfication #: PH 0694
Delaware Certification
Florida/NELAC Certification #: E87683
Georgia Certification #. 968
Guam/PADEP Certification
Hawaii/PADEP Certification
Idaho Cerfification
Illinois/PADEP Certification
Indiana/PADEP Certification
Iowa Certification #: 391
Kansas/NELAC Certification #: E-10358
Kentucky Certification #: 90133
Louisiana/NELAC Certification #: 4086
Louisiana/NELAC Certification #: LA080002
Maine Certification M PA0091
Maryland Certification #: 308
Massachusetts Certification #: M-PA1457
Michigan/PADEP Certification
Charlotte Certification IDs
Connecticut Certification #: PH-0104
Florida/NELAP Certification #: E87627
West Virginia Certification #: 357
Virginia Certification #: 00213
Tennessee Certification #: 04010
South Carolina Drinking Water Cert. #: 990060003
South Carolina Certification #: 990060001
Asheville Certification IDs
Connecticut Certification #: PH-0106
Virginia Certification #: 00072
Tennessee Certification #: 2980
South Carolina Certification #, 99030001
South Carolina Bioassay Certification #: 99030002
Pennsylvania Certification #: 68-03578
West Virginia Certification #: 356
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Minnesota Certification #: 042-999,425
Missouri Certification M 235
Montana Certification #: Cert 0082
Nevada Certification
New Hampshire/NELAC Certification #: 2976
New Jersey/NELAC Certification #i PA 051
New Mexico Certification
New York/NELAC Certification * 10888
North Carolina Certification #: 42706
Oregon/NELAC Certification #: PA200002
Pennsylvania/NELAC Certification #: 65-282
Puerto Rico Certification #: PA01457
South Dakota Certification
Tennessee Certification #: TN2867
Texas/NELAC Certification #: T104704188-09 TX
Utah/NELAC Certification #: ANTE
Virgin Island/PADEP Certification
Virginia Certification #: 00112
Washington Certification #: C1941
West Virginia Certification #: 143
Wisconsin/PADEP Certification
Wyoming Certification #: 8TMS-Q
Pennsylvania Certification #: 68-00784
North Carolina Wastewater Certification #: 12
North Carolina Field Services Certification #: 5342
North Carolina Drinking Water Certification M 37706
New Jersey Certification #: NC012 '
Louisiana/LEIAP Certification #: 04034
Kentucky UST Certification #: 84
North Carolina Drinking Water Certification #: 37712
North Carolina Bioassay Certification #: 9
New Jersey Certification #: NC011
Massachusetts Certification #: M-NC030
Louisiana/LELAP Certification #: 03b95
Flodda/NELAP Certification #: E87648
North Carolina Wastewater Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Riney Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 17
'--ne��C

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
/�acmnalXical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
SAMPLE ANALYTE COUNT
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804 '
[phone] [phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
9250804001 SOUTH POND ASH ASTM D2974-87
TNM
1
PASI-C
EPA365.1
JDA
1
PASI A
EPA 6010
SHB
7
PASI-A
EPA6010
SHB
17
PASI-A
EPA7470
SAJ
1
PASI-A
EPA7471
SAJ
1
PASI-A
EPA 9045
TEE
1
PASI A
SW-846 7.3.3.2
DLD
1
PASI-PA
SW-846 7.3.4.2
DLD
1
PASI-PA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
T12ia,C
Page 3 of 17

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalylcal 2225 Riverside Dr. 9800 IGnceyAve. Suite 100
wwwpacelabs.com Asheville, NC28804 Huntersville, NC 28078
[phone] C/04)875-9092
- ANALYTICAL RESULTS
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
Sample: SOUTH POND ASH Lab ID: 9250804001 Collected: 08/13/09 10:10
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF
Received: 08/13/09 11:52 Matrix: Solid
Prepared Analyzed CAS No.
Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
20.9 mg/kg
0.48
1
08/18/09 12:45
08/19/09 15:01
7440-38-2
Barium
816 mpg
0.48
1
08/18/09 12:45
08/19/09 15:01
7440-39-3
MO
Cadmium
1.4 mg/kg
0.096
1
08/18/09 12:45
08/19/09 15:01
7440- 43-9
Calcium
67500 mg/kg
96.0
10
08/18/09 12:45
08/20/09 18:48
7440-70-2
Chromium
32.5 mg/kg
0.48
1
08/18/09 12:45
08/19/09 15:01
7440-47-3
Copper
112 mg/kg
0.48
1
08/18/09 12:45
08/19/09 15:01
7440-50-8
MO
Iron
9210 mg/kg
4.8
1
0811810912:45
08/19/09 15:01
7439-89-6
MO
Lead
45.6 mg/kg
0.48
1
08/18/09 12:45
08/19/09 15:01
7439-92-1
MO
Magnesium
12000 mg/kg
96.0
10
08/18/09 12:45
08120/09 18:48
7439-95-4
Manganese
2020 mg/kg
4.8
10
0811810912:45
08/2010918:48
7439-96-5
Molybdenum
ND mg/kg
0.48
1
08/18/09 12:45
08/19/09 15:01
7439-98-7
Nickel
15.4 mg/kg
0.48
1
08/18/09 12:45
08/19/09 15:01
7440-02-0
Potassium
ND mg/kg
4800
10
08/18/09 12:45
08/20/09 18:48
7440-09-7
Selenium
2.6 mg/kg
0.96
1
08/18/09 12:45
08/19/09 15:01
778249-2
Silver
0.69 mg/kg
0.48
1
08/18/09 12:45
08/19/09 15:01
7440-22- 4
Sodium
6090 mg/kg
480
1
08/18/09 12:45
08/19/09 15:01
7440-23-5
Zinc '
199 mg/kg
0.96
1
08/18/09 12:45
08/19/09 15:01
7440-66-6
MO
3010 MET ICP, TCLP
Analytical Method: EPA 6010
Preparation Method:
EPA 3010
Leachate Method/Date: EPA 1311; 08/19/09 10:26
Arsenic
0.10 mg/L
0.025
1
08/20/09 09:05
08/20/09 16:54
7440-38-2
Barium
2.5 mg/L
0.025
1
08/20/09 09:05
08/20/09 16:54
7440-39-3
Cadmium
0.015 mg/L
0-0050
1
08/20/09 09:05
08/20/09 16:54
7440-43-9
Chromium
ND mg/L
0.025
1
08/20/09 09:05
08/20/09 16:54
7440-47-3
Lead
0.094 mg/L
0.025
1
08/20/09 09:05
08/20/09 16:54
7439-92-1
Selenium
ND mg/L
0.050
1
08/20/09 09:05
08/20/09 16:54
7782-49-2
Silver
ND mg/L
0.025
1
08/20109 09:05
08/20/09 16:54
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470
Preparation Method: EPA
7470
Leachate Method/Date: EPA 1311; 08/19/09 10:26
Mercury
ND ug/L
0.20
1
08/20/09 09:22
08/20/09 12:46
7439-97-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA
7471
Mercury
0.021 mg/kg
0.0061
1
08/20/09 09:23
08/20/09 13:38
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
29.6 %
0.10
1
08/14/09 14:36
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
9.5 Std. Units
0.10
1
08/19/09 16:55
H1
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus 273 mg/kg 14.2 2 08/18/09 13:19 7723-14-0 MO
)ate: 08/21/2009 10:23 AM REPORT OF LABORATORY ANALYSIS Page 4 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
nGIQ,C �:

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
��IaneAnalPacelabXical2225 Riverside Dr. 9800 IGnceyAve. Suite 100
xavK!cnmAsheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
Sample: SOUTH POND ASH Lab ID: 9260804001 Collected: 08/13/09 10:10 Received: ': 08/13/09 11:52 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters. Results Units Report Limit DF Prepared; Analyzed CAS No. Qual
733C S Reactive Cyanide Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive ND mg/kg 0.99 1 08/18/09 19:02
735S Reactive Sulfide Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive ND mg/kg 9.9 1 08/18/09 16:31
-)ate: 08/21/2009 10:23 AM REPORT OF LABORATORY ANALYSIS Page 5 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

acmnalytical
wvmpacelabs.com
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
QC Batch: WET/9418
QC Batch Method: EPA 9045
Associated Lab Samples: 9250804001
SAMPLE DUPLICATE: 323779
Parameter Units
pH at 25 Degrees C Std. Units
)ate: 08/21/2009 10:23 AM
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC28604
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 9045
Analysis Description: 9045 pH
9250713009 Dup
Result Result RPD
3.3 3.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
neh
Qualifiers
0
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 17

,��IaceAnalj&cal ®
WW.pacetabs.c=
i
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/2549 Analysis Method: SW-846 7.3.3.2
QC Batch Method: SW-846 7.3.3.2 Analysis Description: 733C Reactive Cyanide
Associated Lab Samples: 9250804001
Me I HOD BLANK: 85343 Matrix: Solid
Associated Lab Samples: 9250804001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide, Reactive mglkg ND 1.0 08/18/09 19:02
SHMrLL UUPLICATE: 85344
3014181005 Dup
Parameter Units Result Result RPD ' Qualifiers
Cyanide, Reactive mg/kg ND ND
)ate: 08/21/2009 10:23 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
r
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 17

(�5a'neAnalyfical'4
wrnvpawlabs.com
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave_ Suite 100
Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
QC Batch: MPRP/4932
Analysis Method: EPA 6010
QC Batch Method: EPA 3010
Analysis Description: 6010 MET TCLP
Associated Lab Samples: 9250804001
METHOD BLANK: 324716
Matrix: Water
Associated Lab Samples: 9250804001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Arsenic
mg/L
ND 0.025
08/2010916:47
Barium
mg/L
ND 0.025
08/20/0916:47
Cadmium
mg/L
ND 0.0050
08/20/0916:47
Chromium
mg/L
ND 0.025
08/2010916:47
Lead
mg/L
ND 0.025
08/2010916:47
Selenium
mg/L
ND 0.050
08/20/0916:47
Silver
mg/L
ND 0.025
08120/0916:47
LABORATORY CONTROL SAMPLE:
324717
Spike LCS
LCS %
Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Arsenic
mg/L
2.5 2.7
108
80-120
Barium
mg/L
2.5 2.2
86
80-120
Cadmium
mg/L
2.5 2.6
105
80-120
Chromium
mg/L
2.5 2.6
104
80-120
Lead
mg/L
2.5 . 2.4
97
80-120
Selenium
mg/L
2.5 2.7
109
80-120
Silver
mg/L
1.2 1.2
96
80-120
MATRIX SPIKE SAMPLE:
324718
9250804001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/L
0.10 2.5
2.8
107
75-125
Barium
mg/L
2.5 2.5
4.7
88
75-125
Cadmium
mg/L
0.015 2.5
2.6
103
75-125
Chromium
mg/L
ND 2.5
2.6
103
75-125
Lead
mg/L
0.094 2.5
2.5
96
75-125
Selenium
mg/L
ND 2.5
2.8
110
75-125
Silver
mg/L
ND 1.2
1.2
98
75-125
SAMPLE DUPLICATE: 324719
9250558002 Dup
Parameter
Units
Result Result
RPD
;Qualifiers
Arsenic
mg/L
ND .017J
Barium
mg/L
0.58 0.56
3
Cadmium
mg/L
0.26 0.25
1
Chromium
mg/L
ND .0024J
Lead
mg/L
6.0 5.9
1
)ate: 08/21/2009 10:23 AM
REPORT OF LABORATORY ANALYSIS
Page 8 of 17
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

�aceAnalytical
www.pacelabs.com
Project. SP81309 SOUTH PONDASH
Pace Project No.: 9250804
SAMPLE DUPLICATE: 324719
Parameter
Selenium
Silver
)ate: 08/21/2009 10:23 AM
Pace Analytical Services, Inc.
2226 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
9250558002 Dup
Units Result Result
mg/L ND ND
mg/L ND .0012J
RPD � Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
•uo.,
mill&
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 17

laceAnalyfical
www.pacclabs.cam
Project: SP81309 SOUTH POND ASH
Pace Project No.: . 9250804
QC Batch: MERP/2326
QC Batch Method: EPA 7471
Associated Lab Samples: 9250804001
METHOD BLANK: 323535
Associated Lab Samples: 9250804001
Parameter Units
mg/kg
Mercury
LABORATORY CONTROL SAMPLE:
323536
Parameter
Units
Mercury
mg/kg
MATRIX SPIKE SAMPLE:
323537
Parameter
Units
Mercury
mg/kg
SAMPLE DUPLICATE: 323538
Parameter
Units
Mercury
mg/kg
fate: 08/21/2009 10:23 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7471
Analysis Description: 7471 Mercury
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0050 08/20/0913:09
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
.067 0.065 98 80-120
9250504001 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
0.38 .076 0.38 5 75-125 MO
9250504002 Dup
Result Result RPD Qualifiers
0.0058 0.0060 4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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aceAnalXical C,
vimpacelabs.com
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/5686 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 9250804001
METHOD BLANK: 323460
Associated Lab Samples: 9250804001
Parameter Units
Phosphorus mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 08/18/0913:07
LABORATORY CONTROL SAMPLE:
323461
Spike
LCS
Parameter
Units
Conc.
Result
Phosphorus
mg/kg
20
18.0
MATRIX SPIKE SAMPLE:
323462
9250804001
Spike
Parameter
Units
Result
Conc.
Phosphorus
mg/kg
273 74.7
SAMPLE DUPLICATE: 323463
9250486001
Dup
Parameter
Units
Result
Result
Phosphorus
mg/kg
5040
5110
)ate: 08/21/2009 10:23 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
90 90-110
MS : MS
Result % Rec
396 164
RPD Qualifiers
38 R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
.ccs.
% Rec
Limits Qualifiers
90-110 MO
Page 11 of 17

Z!;a'neAna1j4ica1
wwwpacelabs.cam
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
QC Batch: MERP/2327
QC Batch Method: EPA 7470
Associated Lab Samples: 9250804001
METHOD BLANK: 324108
Associated Lab Samples: 9250804001
Parameter Units
Mercury ug/L
LABORATORY CONTROL SAMPLE: 324109
Parameter Units
Mercury ug/L
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7470
Analysis Description: 7470 Mercury TCLP
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.20 08/20/09 12:41
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.6 106 80-120
MATRIX SPIKE SAMPLE: 324110
9250804001 Spike . MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Mercury ug/L ND 2.5 2.9 115 75-125
SAMPLE DUPLICATE: 324111
9250558002 Dup
Parameter Units Result Result RPD
Mercury ug/L ND ND
)ate: 08/21/2009 10:23 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
°nel2Ic ,
Qualifiers
Page 12 of 17

aceAnalXical
www.p=1415s.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
QC Batch: MPRP/4925 Analysis Method: EPA6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 9250804001
METHOD BLANK: 323540
Associated Lab Samples:
Parameter
9250804001
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed
Arsenic
mg/kg
ND
0.50
08/1910914:54
Barium
mg/kg
ND
0.50
08/19/0914:54
Cadmium
mg/kg
ND
0.10
0811910914:54
Calcium
mg/kg
ND
10.0
08/19/0914:54
Chromium
mg/kg
ND
0.50
08/19/0914:54
Copper
mg/kg
ND
0.50
08/19/0914:54
Iron
mg/kg
ND
.5.0
08/19/0914:54
Lead
mg/kg
ND
0.50
08/19/0914:54
Magnesium
mg/kg
ND
10.0
08/1910914:54
Manganese
mg/kg
ND
0.50
0811910914:54
Molybdenum
mg/kg
ND
0.50
08/19/0914:54
Nickel
mg/kg
ND
0.50
08/19/0914:54
Potassium
mg/kg
ND
500
08/19/0914:54
Selenium
mg/kg
ND
1.0
08/1910914:54
Silver
mg/kg
ND
- 0.50
08/19/0914:54
_- Sodium
mg/kg
ND
500
08/19/0914.54
Zinc
mg/kg
1.5
1.0
08119/0914:54
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
323541
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Arsenic
mg/kg
50
49.7
99
80-120
Barium
mg/kg
50
49.8
100
' 80-120
Cadmium
mg/kg
50
50.2
100
80-120
Calcium
mg/kg
500
577
115
80-120
Chromium
mg/kg
50
50.7
101
80-120
Copper
mg/kg
50
49.2
98
80-120
Iron
mg/kg
500
532
106
80-120
Lead
mg/kg
50
49.9
100
:80-120
Magnesium
mg/kg
500
517
103
'80-120
Manganese
mg/kg
50
51.1
102
80-120
Molybdenum
mg/kg
50
50.1
100
80-120
Nickel
mg/kg
50
51.0
102
80-120
Potassium
mg/kg
500
488J
98
80-120
Selenium
mg/kg
50
49.8
100
80-120
Silver
mg/kg
25
25.5
102
:80-120
Sodium
mg/kg
500
537
107
;80-120
Zinc
mg/kg
50
49.8
100
80-120
-)ate: 08/21/2009 10:23 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�i1GiC
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 13 of 17

acmnalytical
WMpacetabs.cum
I
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
2225 Riverside Dr.
9800 IGncey Ave. Suite 100
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
QUALITY CONTROL DATA
MATRIX SPIKE SAMPLE:
323542
9250804001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/kg
20.9
52.3
70.0
94
75-125
Barium
mg/kg
816
52.3
744
-138
75-125 MO
Cadmium
mg/kg
1.4
52.3
45.9
85
75-125
Calcium
mg/kg
67500
523
51200
-3117
75-125
Chromium
mg/kg
32.5
52.3
73.6
79
75-125
Copper
mg/kg
112
52.3
142
56
75-125 MO
Iron
mg/kg
9210
523
8640
-109
75-125 MO
Lead
mg/kg
45.6
52.3
72.8
52
75-125 MO
Magnesium
mg/kg
12000
523
9790
-419
75-125
Manganese
mg/kg
2020
52.3
1410
-1159
75-125
Molybdenum
mg/kg
ND
52.3
44.2
85
75-125
Nickel
mg/kg
15.4
52.3
56.8
79
75-125
Potassium
mglkg
ND
523
16000
3064
75-125
Selenium
mg/kg
2.6
52.3
53.6
98
75-125
Silver
mg/kg
0.69
26.1
25.8
96
75-125
Sodium
mg/kg
6090
523
6480
76
75-125
Zinc
mg/kg
199
52.3
230
59
75-125 MO
SAMPLE DUPLICATE: 323543
Parameter
Units
9250921009
Result
Dup
Result
RPD Qualifiers
Arsenic
mg/kg
0.83
1.3
41 R1'
Barium
mg/kg
260
265
2
Cadmium
mg/kg
3.1
2.3
30 R1
Calcium
mg/kg
8900
8830
1
Chromium
mg/kg
182
379
70 R1
Copper
mg/kg
101
99.7
1
Iron
mg/kg
21900
21800
1
Lead
mg/kg
715
1770
85
Magnesium
mg/kg
20900
19800
5
Manganese
mg/kg
542
494
9
Molybdenum
mg/kg
42.5
90.6
72 R1
Nickel
mg/kg
27.9
23.9
16
Potassium
mg/kg
16100
14600
9
Selenium
mg/kg
2.5
1.7
38 R1
Silver
mg/kg
0.15J
.15J
Sodium
mg/kg
178J
173J
Zinc
mg/kg
106
99.4
6
.)ate: 08/21/2009 10:23 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
nela&
Page 14 of 17

'acelAnalytical
wrnvp�celabs.com
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
QC Batch: WETA/2553
QC Batch Method: SW-846 7.3.4.2
Associated Lab Samples: 9250804001
METHOD BLANK: 85366
Associated Lab Samples: 9250804001
Parameter Units
Sulfide, Reactive mg/kg
SAMPLE DUPLICATE: 85367
Parameter Units
Sulfide, Reactive mg/kg
-)ate: 08/21/2009 10:23 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SW-846 7.3.4.2
Analysis Description: 734S Reactive Sulfide
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10 08118/0916:31
3014181005 Dup
Result Result
ND ND
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 17

raceAnalytical
www.paWabs.=m
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: PMST/2644 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9250804001
SAMPLE DUPLICATE: 322300
9250643008 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 8.0 7.2 11
SAMPLE DUPLICATE: 322301
9250790004 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 16.3 15.6 5
)ate: 08/21/2009 10:23 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.:
melee
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 17

n �7 r (© Pace Analytical Services, Inc. Pace Analytical Services, Inc.
ac AllalXical 2225 Riverside Dr. 9800 KinceyAve. Suite too
www.pacelabsxam Asheville, NC 28804 Huntersville, NC 28078
(82B)254-7176 [phone]
QUALIFIERS
Project: SP81309 SOUTH POND ASH
Pace Project No.: 9250804
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting! limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values_
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited.. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
PASI-PA Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
MO Matrix spike recovery was outside laboratory control limits.
R1 RPD value was outside control limits.
-)ate: 08/21/2009 10:23 AM REPORT OF LABORATORY ANALYSIS Page 17 of 17
This report shall not be reproduced, except iri full,
without the written consent of Pace Analytical Services, Inc..
.:nelad',

SGS North America, Inc.
Mr. Kevin Godwin
PACE Incorporated
9800 Kincey Ave.
Huntersville NC 28078
Report Number: G150-523
Client Project: SPS 1309 SOUTH POND ASH 9250804
Dear Mr. Godwin:
Enclosed are the results of the analytical services performed under the 'referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our files for a period of five years in the event
they are required for future reference. Any samples submitted to our laboratory will
will be retained for a maximum of thirty (30) days from the'date of this report unless
other arrangements are requested.
If there are any questions about the report or the services performed during this project,
please call SGS at [phone]. We will be happy to answer any questions or
concerns which you may have.
Thank you for using SGS Environmental Services for your analytical services. We look
forward to working with you again on any additional analytical needs which you may have.
Sincerely,.
SGS Environmental Services, Inc.
Environmental Division 5500 Business Dr., Wilmington, NC 28405 t i910) 350.1903 f )910) 350.1557 www,us.sgsxorn
N.C. Certification #481 Page 1 got 4e SGS Group

SGS North America, Inc.
List of Reporting Abbreviations
And Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Quantification Limit (RL or MDL)
DF = Dilution Factor
Dup = Duplicate
D = Detected, but RPD is > 40% between results in dual column method.
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL/CL = Reporting Limit / Control Limit
RPD = Relative Percent Difference
UJ = Target analytes with recoveries that are 10% < %R < LCL; # of MEs are allowable
and compounds are not detected in the sample.
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block; see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
M134.021808.4
N.C. Certification #481 Page 2 of 4

SGS North America, Inc.
Results for Ignitabillty
by EPA 1030
Client Sample ID: SOUTH POND ASH Analyzed By: BAO
Client Project ID: SP81309 SOUTH POND ASH 9250804 Date Collected: 8/13/2009 10:10
Lab Sample ID: G150-523-1A Date Received: 8/18/2009
Lab Project ID: G150-523 Matrix: Solid
Parameter
lgnitablillty
Comments:
Result Units
< 0.8 mm/sec
N.C. Certification #481
Date
Analyzed
8/19/2009
Reviewed By:
Page 3 of 4

Z.
Chain of Custody
CeAn*Wcal
Workorder. 9250804 WorkGrder Name- SDAVAnn Cell ITO DllAir-I Ace .. _
Friday, August 14, 2M9 9:37:01 AM FMT-ALL-C-.O(Mev.p9 24March2M
Page 1 of i

-S11%./e
Energy Generation NA
Please test the sample(s) for the parameters as listed below
Send Invoice and copy of results to: Send original results to:
R" Styles Summer Barber
SUEZ Energy BloPower, Inc. SUEZ Energy BloPower, Inc.
2859 Old-Linvllie Rd: 1990 Post Oak Bivd-Sulfe 1900
Marlon,, NC 28752 Houston, TX 77056
[e-mail] summer. barber r0odfsuezna.com
(828) 7564M 713-636-1639
(fax) 756-7160
RUSH RUSH RUSH z.5,o10Y
Requested Due Date:
Sample
Sample
Description
Sample Date(s)
and time sample
collected
Grab or
Composite
Total Metals -
As, Ba, Cd,
Ca, Cr, Cu, Fe,
TCLP Metals
_As, Ba,, Cd,
Cr, Pb,, Hag,
Ignitablilly,
Reactivity
pH
Corrosivity
Total -Arsenic
Full TCLP
Pb, Mg, Hg,
_` , • `g
Mn, Mo, Ni, K,
Se, Ag, No, Zn,
total
Phosphorus
SP81309
SOUTH POND
ASH
8"13-Q910:10AM
COMPOSITE
YES
YES
YES
YES
YES
Zsa�o vp
�7 Y
Sample sent to: Pace Analytical SerAces, 1
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Chain stody
Project Manager. Kevin Godwin
9800 Klncey Avenue, Suite 100
Huntersviile, NC 28078
(704) 875 - 9092 ext. 233

/55'ceAnalAcat"
Sample Condition Upon Receipt
Client Name: 5;,, z Project # qz5'0aoY
'Courier: ❑ Fed Fit ❑ UPS ❑ USPS ❑ Client ❑ Commercial Pace Other
Custody Seal on Cooler/Sox Present: ❑ yes 2-. no Seals intact: ❑ yes E7­no
Packing Material: ❑ Bubble Wrap []Bubble Bags [Kone ❑Other
Thermometer Used, 1239i/ 72490786 Type of Iced'' Blue None ❑ Samples on ice, cooling process has begun
Temp Correction Factor: Add b_` try D_� C
Corrected Cooler Temp.: S-6 C
Biological Tissue is Frozen: Yes
g
Date and Initials of arson amining
contents:
Temp should be above freezing to VC
Comments:
Chain of Custody Present.
s
ONO
❑N/A
1.
Chain of Custody Filled Out:
es
ONO
❑N/A
2.
Chain of Custody Relinquished:
Yes
ONO
❑N/A
3.
Sampler Name & Signature on COC:
as
ONO
❑N/A
4.
Samples Arrived within Hold Time:
Yes
ON.
❑WA
5_
Short Hold Time Analysis (<72hr):
Oyes
f o ❑N/A
6.
Rush Turn Around Time Requested:
Yes
❑No
❑N/A
7.
Sufficient Volume:
es
ONO
❑N/A
8.
Correct Containers Used:
es
ONO
❑N/A
9.
-Pace Containers Used:
/� <
ONO
❑N/A
Mainers Intact:
es
❑No
❑N/A
10.
Filtered volume received for Dissolved tests
❑Yes
ONO
/A
11.
Sample Labels match COC:
Yes
ONO
❑N/A
12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
❑Yes
ONO
I�i/A
13.
All containers needing preservation are found to be in
compliance with EPA recommendation.
❑yes
ONO
A
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
Oyes
o
Initial when completed
Samples checked for dechlorination:
❑Yes
ONO
ETNIA
14.
Heads ace in VOA Vials ( >6mm):
❑Yes
ONO
N/A
15.
Trip Blank Present:
❑Yes
ONO
N/A
•16.
Trip Blank Custody Seals Present
Dices
ONO
A
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: C //,'o tf cw,'TL Sc� Z Date/Time: /y vpyp2 �i-
Comments/ Resolution: 7=— t h_s, —r,a/ 9
Project Manager Review:
Date:
Note: Whenever there is a discrep6taraffecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( Le out of hold, incorrect preservative, out of temp, incorrect containers)

Date: Sl -13 ' D 5 Analyst:
Facility: M—+9kZ, )Al
Calibration
Calibration
Time
Cal Buffer
7.0
Cal Buffer
10.0
Check
Buffer 12.0*
Comments
Temp C
-7.o
10.0
* pH buffer checks are to be within ± 0.1 pH units of the standard's true value
pH Analyses
Sample ID
Time
Sampled
Time
Analyzed
pH Result
Buffer
Check**
Comments
Temp C .
5CP 91309
C1: sv Aa
/0.-10it,
10 , S
IZ. 0
02(P.5"
** Indicates a recommended drift check using Buffer 12.0 at the end of testing or every 4 hours minimum.
Results should be within ± 0.1 pH units of the standard's true value.
Results and Buffers are in standard units
Updated 7-29-09

aceAnalyticat
wmpawlabs.com
October 09, 2009
Ms. Summer Barber
Suez Energy
302 Duke Street
Forest City, NC 28043
RE: Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 2BB04
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Ms. Barber:
Enclosed are the analytical results for sample(s) received by the laboratory on October 02, 2009.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�L.LL�SIGL6�; s
Page 1 of 13

aceAnalytical
www.pacelabs.com
Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
Pennsylvania Certification IDs
Louisiana[NEIAC Certification #: 4086
Kentucky Certification * 90133
Kansas/NELAC Certification #: E-10358
Iowa Certification #: 391
Indiana/PADEP Certification
Illinois/PADEP Certification
Idaho Certification
Hawaii/PADEP Certification
Guam/PADEP Certification
Georgia Certification #: 968
Florida/NELAC Certification #: E87683
Delaware Certification
Connecticut Certification #: PH 0694
Colorado Certification
Califomia/NELAC Certification #: 04222CA
Arkansas Certification
Arizona Certification #. AZ0734
Alabama Certification #: 41590
Wyoming Certification #: 8TMS-Q
Wisconsin/PADEP Certification
West Virginia Certification #: 143
Washington Certification #: C1941
Virginia Certification #: 00112
Charlotte Certification IDs
West Virginia Certification #: 357
Virginia Certification M 00213
Connecticut Certification #: PH-0104
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisianall-ELAP Certification #: 04034
New Jersey Certification* NC012
Pace Analytical Services; Inc.
Pace Analytical Services, Inc.
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
Asheville, NC 28864
Huntersville, NC 28078
[phone]
[phone]
CERTIFICATIONS
Virgin Island/PADEP Certification
Utah/NELAC Certification * ANTE
Texas/NELAC Certification #: T104704188-09 TX
Tennessee Certification #: TN2867
South Dakota Certification
Puerto Rico Certification #. PAO1457
Pennsylvania/NELAC Certification #: 65-282
Oregon/NELAC Certification M PA200002
North Carolina Certification #: 42706
New York/NELAC Certification #: 10888
New Mexico Certification
New Jersey/NELAC Certification M tPA 051
New Hampshire/NELAC Certification #: 2976
Nevada Certification .
Montana Certification M Cert. 0082 .
Missouri Certification M 235
Minnesota Certification M 042-999-425
Michigan/PADEP Certification
Massachusetts Certification M M-PA1457
Maryland Certification #: 308
Maine Certification #: PA0091
Louisiana/NELAC Certification #: LA080002
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pennsylvania Certification #: 68-00784
South Carolina Certification #: 990060001
South Carolina Drinking Water Cert. #: 990060003
Tennessee Certification #: 04010 `
Asheville Certification IDs
West Virginia Certification #: 356
North Carolina Wastewater Certification #: 40
Flodda/NELAP Certification #: E87648
Pennsylvania Certification #: 68-03578
Louisiana/LELAP Certification #: 03095
South Carolina Bioassay Certification #: 99030002
Massachusetts Certification #: M-NC030
South Carolina Certification #: 99030001
New Jersey Certification #: NC011
Tennessee Certification * 2980
North Carolina Bioassay Certification #: 9
Virginia Certification #: 00072
Connecticut Certification #: PH-0106
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2of13

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aG/ I ce 11nalj4ica ( 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.paceelaabs.coml Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
SAMPLE ANALYTE COUNT
Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
9254358001 3QTR100209 BOTTOM ASH ASTM D2974-87
KDF
1
PASI-C
EPA365.1
LEP
1
PASI-A
EPA6010
JMW
17
PASI-A
EPA 7471
SHB
1
PASI A
EPA9045
JDA
1
PASI-A
SW-846 7.3.3.2
DLD
1
PASI-PA
SW-946 7.3.4.2
DLD
1
PASI-PA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
eae
Page 3 of 13

aceAnalytical
www.pacclabs.com
1
Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 3QTR100209 BOTTOM ASH
Lab ID: 9254358001 Collected:
10/02/09 09:30
Received: ,10/02/09 10:39 Matrix: Solid
Results reported on a "dry-weight"basis
Parameters
Results Units Report Limit
DF
Prepared!
Analyzed
GAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
16.7 mglkg
0.40
1
10/05/09 13:45
10/06/09 13:17
7440-38-2
Barium
1980 mglkg
4.0
10
10/05/0913:,45
10/06109.16:50
7440-39-3
Cadmium
1.4 mg/kg
0.080
1
10/05/0913.45
10106/0913:17
7440-43-9
Calcium
80400 mg/kg
80.4
10
10/05/09 13:45
10/06/09 16:50
7440-70-2
Chromium
179 mg/kg
0.40
1
10/05/09 13:45
10/06/09 13:17
7440-47-3
Copper
246 mglkg
0.40
1
10/05/09 13:45
10106/09 13:17
7440-50-8
Iron
21800 mglkg
40.2
10
10/05/09 13:45
10/06/09 16:50
7439-89-6
Lead
38.4 mg/kg
0.40
1
10/05/09 13:45
10106/09 13:17
7439-92-1
Magnesium
15600 mg/kg
80.4
10
10/05/09 13:45
10/0610916:50
7439-954
Manganese
2890 mg/kg
4.0
10
10/05/09 13:45
10/06/09 16:50
7439-96-5
Molybdenum
ND mg/kg
0.40
1
10/05/09 13:45
10/06/09 13:17
7439-98-7
Nickel
27.9 mg/kg
0.40
1
10/05/09 13:45
10/06/09 13:17
7440-02-0
Potassium
29300 mg/kg
4020
10
10/05/09 13:45
10/06/09 16:50
7440-09-7
Selenium
1.2 mg/kg
0.80
1
10/05/09 13:45
10/06/09 13:17
7782-49-2
Silver
0.76 mg/kg
0.40
1
10/05/09 13:45
10/06/09 13:17
7440-22-4
Sodium
20200 mg/kg
4020
10
10/05/09 13:45
10/06109 16:50
7440-23-5
Zinc
183 mg/kg
0.80
1
10/05/09 115
10/06/09 13:17
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
ND mg/kg
0.0043
1
10/0710916:50
10/0810912:20
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
8.6 %
0.10
1
10/06/09 10:45
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
733C S Reactive Cyanide
Cyanide, Reactive
735S Reactive Sulfide
Sulfide, Reactive
Date: 10/09/2009 06:32 PM
12.3 Std. Units
Analytical Method: EPA 365.1
166 mglkg
Analytical Method: SW-846 7.3.3.2
ND mglkg
Analytical Method: SW-846 7.3.4.2
ND mg/kg
0.10 1
2.2 1
1.0 1
10.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
10/09/0911:26 H1
10/09/0913:56 7723-14-0 MO
10/05/09 17:53
10/01/09 17:07
Page 4 of 13

laneAnalytical"
www.pacelabs.com
Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828)254; 7176
QUALITY CONTROL DATA
QC Batch: WET110036 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 9254358001
SAMPLE DUPLICATE: 348240
Parameter
pH at 25 Degrees C
Date: 10/09/2009 06:32 PM
9253931001 Dup
Units Result Result
Std. Units 6.5 6.5
RPD Qualifiers
0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 13

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aceAnalytical. Asheville, NC 28804 Huntersville, NC 28078-
www.pacelabs.com
[phone] [phone]
Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
QC Batch: WETA/5988
QC Batch Method: EPA 365.1
Associated Lab Samples: 9254358001
METHOD BLANK: 347974
Associated Lab Samples: 9254358001
Parameter Units
Phosphorus mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 10/09/0913:55
LABORATORY CONTROL SAMPLE:
347975
Spike
LCS
LCS % Rec
Parameter
Units
Cone.
Result
% Rec Limits
Qualifiers
Phosphorus
mg/kg
20
17.9
90 90-110
MATRIX SPIKE SAMPLE:
347976
9254358001
Spike
MS MS
%-Rec
Parameter
Units
Result
Cone.
Result % Rec
Limits Qualifiers
Phosphorus
mg/kg
166 21.9
303 626
90-110 MO
SAMPLE DUPLICATE: 347980
9254024001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Phosphorus
mg/kg
2200
3330
41 R1
0
Date: 10/09/2009 06:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
n •c0'A\C
��1.1.1�f1f4»s
Page 6 of 13

�aceAnalytical
www.pacelabs.com
Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/2824 Analysis Method: SW-846 7.3.4.2
QC Batch Method: SW-846 7.3.4.2 Analysis Description: 734S Reactive Sulfide
Associated Lab Samples: 9254358001
METHOD BLANK: 99953
Associated Lab Samples: 9254358001
Parameter Units
Sulfide, Reactive mg/kg
SAMPLE DUPLICATE: 99954
Parameter
Sulfide, Reactive
Date: 10/09/2009 06:32 PM
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 10/01/0917:07
3016333001 Dup
Units Result Result
mg/kg ND ND
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
S
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 13

aceAnalytical
www.pscelabs.ccm
f
Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/2823 Analysis Method: SW-846 7.3.3.2
QC Batch Method: SW-846 7.3.3.2 Analysis Description: 733C Reactive Cyanide
Associated Lab Samples: 9254358001
METHOD BLANK: 99939
Associated Lab Samples: 9254358001
Parameter Units
Cyanide, Reactive mg/kg
SAMPLE DUPLICATE: 99940
Parameter
Cyanide, Reactive
Date: 10/09/2009 06:32 PM
Units
mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 10/0510917:53
3016333001 Dup
Result Result RPD Qualifiers
ND .64J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
ono„
ie
Pace Analytical Services, Inc.
9800 Kncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 13

/5a'ceAna1jdica1-
Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/5162
QC Batch Method: EPA 3050
Associated Lab Samples: 9254358001
Analysis Method:
Analysis Description:
EPA6010
6010 MET
METHOD BLANK: 345696
Matrix: Solid
Associated Lab Samples: 9254358001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Arsenic
mglkg
ND
0.50
10/06/0912:07
Barium
mg/kg
ND
0.50
10/06/0912:07
Cadmium
mg/kg
ND
0.10
10/0610912:07
Calcium
mg/kg
ND
10.0
10106/0912:07
Chromium
mg/kg
ND
0.50
10106/0912:07
Copper
mg/kg
ND
0.50
10/06/0912:07
Iron
mg/kg
ND
5.0
10/0610912:07
Lead
mg/kg
ND
0.50
1010610912:07
Magnesium
mg/kg
ND
10.0
1010610912:07
Manganese
mg/kg
ND
0.50
10/0610912:07
Molybdenum
mg/kg
ND
0.50
10/06/0912:07
Nickel
mg/kg
ND
0.50
1010610912:07
Potassium
mg/kg
ND
500
10/0610912:07
Selenium
mg/kg
ND
1.0
1010610912:07
Silver
mgtkg
ND
0.50
10/0610912:07
-- Sodium
mg/kg
ND
500
10/06/0912:07
Zinc
mg/kg
ND
1.0
10/0610912:07
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
345697
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Arsenic
mg/kg
50
48.2
96
80-120
Barium
mg/kg
50
48.5
97
80-120
Cadmium
mglkg
50
48.2
96
80-120
Calcium
mg/kg
500
487
97
80-120
Chromium
mg/kg
50
48.4
97
- 80-120
Copper
mg/kg
50
47.5
95
80-120
Iron
mg/kg
500
500
100
80-120
Lead
mg/kg
50
48.7
97
80-120
Magnesium
mg/kg
500
484
97
80-120
Manganese
mg/kg
50
48.8
98
80-120
Molybdenum
mg/kg
50
49.4
99
.80-120
Nickel
mg/kg
50
48.8
98
80-120
Potassium
mg/kg
500
460J
92
80-120
Selenium
mg/kg
50
47.2
94
80-120
Silver
mg/kg
25
24.5
98
80-120
Sodium
mg/kg
500
497J
99
80-120
Zinc
mg/kg
50
49.2
98
80-120
Date: 10/09/2009 06:32 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 9 of 13

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
1aaeAnalyfical"
www.pacelabs.com Asheville, NO 28804 Huntersville, NO 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
345698
345699
MS
MSD
9254262001
Spike
Spike
MS
MSD
MS I
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
0.57
54.8
53
50.1
48.5
90
91
75-125
3
Barium
mg/kg
4.0
54.8
53
58.3
55.5
99
97
75-125
5
Cadmium
mg/kg
ND
54.8
53
51.8
51.0
95
96
75-125
2
Calcium
mg/kg
55.4
548
530
613
551
102
94
75-125
11
Chromium
mg/kg
1.8
54.8
53
55.1
54.1
97
99
75-125
2
Copper
mg/kg
0.77
54.8
53
54.1
52.9
97
98
75-125
2
Iron
mg/kg
530
548
530
1340
970
147
83
75-125
32 MO,R1
Lead
mg/kg
2.5
54.8
53
55.4
53.6
97
96
75-125
3
Magnesium
mg/kg
29.0
548
530
607
576
106
103
75-125
5
Manganese
mg/kg
1.2
54.8
53
55.0
53.4
98
99
75-125
3
Molybdenum
mg/kg
ND
54.8
53
51.8
50.9
95
96
75-125
2
Nickel
mglkg
0.57
54.8
53
54.2
52.6
98
98
75-125
3
Potassium
mg/kg
ND
548
530
626
582
1,11
106
75-125
7
Selenium
mg/kg
ND
54.8
53
48.6
47.7
89
90
75-125
2
Silver
mg/kg
ND
27.3
26.6
26.4
26.0
96
98
75-125
2
Sodium
mg/kg
ND
548
530
623
596
112
110
75-125
4
Zinc
mg/kg
3.4
54.8
53
59.1
56.1
102
99
75-125
5
SAMPLE DUPLICATE: 345700
9254414001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Arsenic
mg/kg
1.7
1.7
1
Barium
mg/kg
9.6
11.7
20
Cadmium
mg/kg
ND
.059J
Calcium
mg/kg
12900
6940
60 R1
Chromium
mg/kg
3.5
4.5
25 R1
Copper
mg/kg
1.7
17.1
164 R1
Iron
mg/kg
1880
2520
29 R1
Lead
mg/kg
7.5
14.5
63 R1
Magnesium
mg/kg
276
230
19
Manganese
mg/kg
7.2
8.6
18
Molybdenum
mg/kg
ND
ND
Nickel
mg/kg
0.79
1.1
30 R1
Potassium
mg/kg
ND
1901
Selenium
mg/kg
ND
ND
Silver
mg/kg
ND
.072J
Sodium
mg/kg
ND
31.6J
Zinc
mg/kg
21.3
64.0
100 R1
Date: 10/09/2009 06:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
. o
vci�la�=
Page 10 of 13

aceAnalytical
mm.pecolabs.com
Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: PMST/2771 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9254358001
SAMPLE DUPLICATE: 345651
9254399001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 10.6 10.8 1
SAMPLE DUPLICATE: 345668
9254405006 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 21.0 20.1 4
Date: 10/09/2009 06:32 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace
..Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 13

aceAnalytical
www.pacelabs.com
Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
QC Batch: MERP/2422
QC Batch Method: EPA 7471
Associated Lab Samples: 9254358001
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7471
Analysis Description: 7471 Mercury
METHOD BLANK: 346778
Matrix: Solid
Associated Lab Samples: 9254358001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Mercury
mg/kg
ND
0,0050
10/0810911:33
LABORATORY CONTROL SAMPLE:
346779
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Mercury
mg/kg
.067
0.066
99
80-120
MATRIX SPIKE SAMPLE:
346780
9254306001
Spike
MS
MS % Rec
Parameter
Units
Result
Cone.
Result
% Rec Limits Qualifiers
Mercury
mglkg
0.0087 .067
0.069
91 75-125
SAMPLE DUPLICATE: 346781
9254306002
'Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Mercury
mg/kg
0.021
0.021
0
Date: 10/09/2009 06:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 13

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
pace 11na11 ical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Asheville, NO 28804 Huntersville, NO 28078
[phone] [phone]
QUALIFIERS
Project: 3 QTR 100209 BOTTOM ASH
Pace Project No.: 9254358
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited_ Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-PA Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
MO Matrix spike recovery and/or matrix spike duplicate recovery wat outside laboratory control limits.
R1 RPD value was outside control limits.
Date: 10/09/2009 06:32 PM REPORT OF LABORATORY ANALYSIS Page 13 of 13
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

SGS North America, Inc.
Ukool- WANZ I'S
GRIM
Mr. Kevin Godwin
PACE Incorporated
9800 Kincey Ave.
Huntersville NC 28078
ReportNumber: G150-528
Client Project: 3 QTR 100209 BOTTOM ASH
Dear Mr. Godwin:
Enclosed are the results of the analytical services performed under the; referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our files for a period of five years in the event
they are required for future reference. Any samples submitted to our laboratory will
will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or the services performed during this project,
please call SGS at [phone]. We will be happy to answer any questions or
concerns which you may have.
Thank you for using SGS Environmental Services for your analytical services. We look
forward to working with you again on any additional analytical needs which you may have.
Sincerely,
SGS Environmental Services, Inc.
SGS North America Inc. I Environmental Division 5500 Business Dr., Wilmington, NC 28405 t [phone] 1(910(350-1557
N.C. Certification #481 pAUnITYto SGS Group

SGS North America, Inc.
List of Reporting Abbreviations
And Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Quantification Limit (RL or MDL)
DF = Dilution Factor
Dup = Duplicate
D = Detected, but RPD is > 40% between results in dual column method.
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL/CL = Reporting Limit / Control Limit
RPD = Relative Percent Difference
UJ = Target analytes with recoveries that are 10% < %R < LCL; # ofMEs are allowable
and compounds are not detected in the sample.
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block; ,see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
MI34.021808.4
N.C. Certification #481 Page 2 of 4

SGS North America, Inc.
Results for Ignitability
by EPA 9030
Client Sample ID:
3QTR 100209 BOTTOM ASH
Client Project ID:
3 QTR 100209 BOTTOM ASH
Lab Sample ID:
G150-528-1A
Lab Project ID:
G150-528
Parameter
Ignitablility
Comments:
Result Units
< 0.8 mmisec
Analyzed By: BAO
Date Collected: 10/2/2009 09:30
Date Received: 1013/2009
Matrix: Solid
Date
Analyzed
10/9/2009
Reviewed By:
N.C. Certification #481 Page 3 of 4

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Results Requested 10/9/2009
lnvbice To ` �>> -.-`-a, _:.;:-" Subcontract'To': ' �a •e':':z ^ r-' rc ?`;:'•ig� :;=tom : of a:.
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Kevin Godwin
Pace Analytical Charlotte P.O. r
9800 Kincey Ave. Suite 100 S (? S
Huntersville, NC 28078
Phone[phone] S50 U B�S•nps5 ��<<�
Email: [e-mail]
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Friday. October 02. 2009 3:44:46 PM
FMT-ALL-C-002rev.00 24March2009
Page -I, f 1

.svez
Energy Generation NA
Please test the sample(s) for the parameters as listed below.
Send invoice and copy of results to: Send original results to:
Ricky Styles Summer Barber.
SUEZ Energy BloPower, Inc. SUEZ Energy BioPower, Inc.
2M Old Linville Rd: 1990 Post Oak Blvd Suite-1900
Marlon, NC 28752 Houston, TX 77056
[e-mail] summer barber(aD_adfsuezna.com
[phone] 713-636-1639
(fax) 756-7160
5 DAY RESULTS PLEASE
Due Date:
Sample Sample Date(s) I Grab or
Description and time sample Composite
collected
30TR100209 IBOTTOM ASH I 10-02-09 9:30AM I COMPOSITE
Sample sent to: Pace Analytical Services,1
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Total Metals -
Tctp Mesta
As, Ba. Cd,
As, Ba, Cd,
Ca, Cr, Cu, Fe,
Cr. Pb, Hg,
Pb, Mg, Hg,
Se, Ag
Mn, Mo, NI, K,
Se. Ag, Na, Zn,
total
Phosphom
YES
gnitability, PH
Reactivity I Corrosivity
YES
Project Manager. Kevin Godwin
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
(704) 876 - 9092 ext. 233
1
YES
13-125,1/351
Total -Am_ nlc I Full TCLP
YES 1 1001
le A��_46

Date: 1� -� -Ocj Analyst:
FacMy: M /4 4,10 IV
Calibration
Calibration
Time
Cal Buffer
7.0
Cal Buffer
10.0
Check
Buffer 12.0*
Comments
Temp C
3o�M1010
121
* pH buffer checks are to be vAthin ± 0.1 pH units of the standard's true value
pH Analyses
Sample ID
Time
Sampled
Time
Analyzed
pFI Result.
Buffer
Check**
Comments
Temp C
3QTRIa©z0g
i 30
0
1 Z, l
/Z, 0
** Indicates a recommended drift check using Buffer 12.0 at the end of testing or every 4 hours minimum.
Results should be within t 0.1 pH units of the standard's true value.
Results and Buffers are in standard units
Updated 7-29-09

faceAnalX cal
www.pacelabs.cam
t
I
December 08, 2009
Ms. Summer Barber
Suez Energy
302 Duke Street
Forest City, NC 28043
RE: Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Ms. Barber:
Enclosed are the analytical results for sample(s) received by the laboratory on November 11, 2009.
The results relate only to the samples included in this report. Results reported herein conform to the
ill NELAC standards, where applicable, unless otherwise narrated in the body of the
r Inorganic Wet Chemistry and Metals analyses were performed t o-ur Pace €lie laborttig-: -,
f
Organic; iesiing was performed ai our Pace
ii you nave any questions concerning t is report. viease ieei Tree io Eton aci me.
Slncerel�,
c:; o I
Kevin Godwin
Project Manager
Enclosures
RFFInRT fie= i ARnF?ATf)R'Y' AMA! VS!i;
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Rana 1 of 27

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.,
ace Analytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacalabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
CERTIFICATIONS
Project: POND ASH
Pace Project No.: 9257321
Ormond Beach Certificatton IDs
8 East Tower Circle Ormond Beach, FL 32174
Alabama Certification #k 41320
Virginia Certification #: 00432
Texas Certification: FL NELAC Reciprocity
Tennessee Certification #: TNO2974
.Puerto Rico Certification #: FLO1264
Pennsylvania Certification #: 68-547
North Carolina Certification #: 12710
New York Certification #: 11608
New Jersey Certification It: FL765
New Hampshire Certification ##. 2958
Nevada Certification: FL NELAC Reciprocitv
ryu ii'YI'AxSa Cc.iiiC!/•aitpPi=_ i Prt On74
tt�r�..t33iL�i}; enific at!on. F=L NELP:C i'iecto€ocay
Chadotte Certification IDs
9800 Kincey Ave. - Ste 100 Huntersville, NC 28078
Connecticut Certification #: PH-0104
Flodda/NELAP Certification #: E87627
Kentucky UST Certification #: 84
t ' n2/LE1 nP (efbficatiOn #: €)4034
Nihri JC-faeV i:cfilflCnkiOn #. NC012
Asheville Certification IDs
Flodda/NELAP Certification #: E87648
Connecticut Certification #: PH-0106
Massachusetts Certification #: M-NC030
New Jersey Certification #: NC011
North Carolina Bioassay Certification ##. 9
North Carolina Drinking Water Certificaiion #. 's ;; i 2
Ai...l r. ('a.nl.r.-, ln;.�a•!®,.,-a44r: .�.i�l:r-oll,,.n it AA
Out
Michigan Certification #: 9911
Massachusetts Certification #: M-FL1264
Maine Certification ##: FL1264
Louisiana Certification #: LA090012
Kentucky Certification #. 90050
Kansas Certification #: E-10383
Hawaii Certification: Ft. NELAC Reciprocity
Guam Certification: FL NELAC Reciprocity
Georgia Certification #: 955
Florida Certification#: E83079
Connecticut Certification 9: PH'r??16
Colorado Certification: FL NELAC Reworouiv
,A.ylrr:�ia rsliif :alrn�) A7n-/%
vVlh3nilfilt Cditificatioi'l. FL NELAC siBC!l55oiit4*
North Carolina Wastewater Certification #: 12
Pennsylvania Certification ##: 68-00784
South Carolina Certification #- 990nF *M1)1
South Carolina Drinking Water Cert. #: 99006d003
Tennessee Certification #: 04010
Vifginia Cc& tiflcation #: 00213
South Carolina Bioassay Certification 4: 99030002
South Carolina Certification #: 99030001
Tennessee Certification #: 2980
Virginia Certification #: 00072
r1Vns,'t %"ircima
LLL:i iitVei Slt7C i.il. a-s�i!>=vatic, iv� s•�ov�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 27
stela

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr.
te 100
-� / �aceAnalXical ® Asheville, NC'28804 9800Hunter ville, NC'28078
www.pacolabs.cam
[phone] [phone]
SAMPLE ANALYTE COUNT
Project: POND ASH
Pace Project No.: 9257321
Analytts
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
9257321001
NP11-11-09 POND ASH
EPA8081
CAH
8
PASI-C
EPA 8151
LJM
3
PASI-0
EPA 6010
JMW
17
PASI-A
EPA6010
JMW
7
PASI-A
EPA 7470
SHB
1
PASI-A
EPA 7471
SHB
1
PASI-A
EPA 8270
EAO
18
PASI-O
ERA8260
DLK
15
PASI-C
ASTM D2974-87
TNM
1
PASI-C
EPA 9045
JDA
1
PASI-A
ASTM D2974-87
GMD
1
PASI-O
EPA 365.1
LEP
1
PASI-A
9257321002
NP12-11-09 POND ASH
EPA 6010
JMW
17
PA$1-A
EPA 7471
SHB
1
PASI-A
ASTM D2974-87
TNM
1
PASI-C
EPA 9045
JDA
1
PASI-A
EPA 365.1
LEP
1
PASI-A
9257321003
STORM WATER
SM 2540D
JDA
1
PASI-A
EPA 9040
JDA
1
PASI-A
SM 5220D
JDA
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 27

-.0001
aceAnalytical
i www.pacalabs.com
f
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: POND ASH .
Pace Project No.: 9257321
Sample: NP11-11-09 PONDASH Lab ID: 9257321001 Collected: 11/11/09,14:15 Received: 11/11/09 15:50 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters
Results Units
Report Limit DF
Prepared
Analyzed
CAS No. Quat
8081 GCS Pesticides, TCLP SPE
Analytical Method. EPA 8081 Preparation Method: EPA 3535
Leachate Method/Date: EPA 1311; 11/25/09 15:00
gamma-BHC (Lindane)
ND ug/L
0.50 1
11/30/09 15:08
12/03/09 12:02
58-09-9
Chlordane (Technical)
ND ug/L
3.0 1
11/30/09 15:08
12/03/09 12:02
57-74-9
Endrin
ND ug/L
0.50 1
11/30/09 15:08
12/03/09 12:02
72-20-8
Heptachlor epoxide
ND ug/L
0.50 1
11/30/09 15:08
12/03/09 12:02
1024-57-3
Methoxychlor
ND ug/L
1000 1
11/30/09 15:08
12/03/09 12:02
72-43-5
Toxaphene
ND ug/L
3.0 1
11/30/09 15:08
12/03/09 12:02
8001-35-2
Decachlorobiphenyl (S)
63 %
10-138 1
11/30/09 15:08
12JO3109 12:02
2051-24-3
Tetrachloro-m-xylene (S)
79 %
10-110 1
11130/0915:08
12/03/09 12:02
877-09-8
815.1 Chlorinate Herbicide TCLP
Analytical Method: EPA 8151
2,4-D
ND mg/L
0.026 1
11117/09 13;30
11/20/09 11:37
94-75-7
2,4,5-TP (Silvex)
ND mg/L
0.028 1
'11/17109 13;30
•11120/09 11:37
93-72-1
2,4-VLPA 1S/
Ili %
70-130 1
11/17/09 13:30
11/20/09 11:37
19719-28-9
6010 MET ICP
Analytical Method: EPA 6010 Preparation l0ethod: EPA 3050
PUuCIb(,
Barium
27.5 ll19lky
i. I 1
iii 12;09 1 I.VV
i U 1GlGa 14. 1,;
74,40-36-2
1330 mglkg
1.1 1
11/12/09 11;00
11/12/09 14:19
7440-39-3
cadr7fival
2.3 lilgPay
0.22 t
i ii i2;Ga i i.00
111t2;09 i419
7440-43-99
Calcium
91100 mglkg
218 10
11/1210911:00
11/12/0916:35
7440-70-2
C1 i101111ul11
Copper
53.5 111 ;1+,
.y �
1. 1 t
{ ll IG/Vy 1 Y.VU
(
lif IGlVJ 14, 19
f't-tVrtl -3
159 mg/kg
1.1 1
11/1210911:00
11/12/09 14:19
7440-50-8
it Uil
Lead
ivivu f6w,"mg
iii.a t
1iii2/09 1I.CG
ii; WOIG i4.17
743a-oa-o
55.1 mg/kg
1.i 1
1111210911:00
11/1210914:19
7439-92-1
ividyuobluli;
14uuu liiyiny
2i.o i
ii;i G;Ga ii.GG
ii; i`;0a ,4.ia
I743;-ai-4
Manganese
3460 mg/kg
10.9 10
11/12/09 11:00
11/12/09 16:35
7439-96-5
iviGiyixicllulil
Nickel
ItlV 171}f/I}j
1.1 1
,
11! {G/V7 II,VV
I I/ IGf V.7 1`F. 15
ITJY:lV-f
30.8 mgiltg
1.1 1
11/12/0911:00
1111210914:19
7440-02-0
rJiaa�wnl
Selenium
1a2vv !ii !n
yy
iviiG i
""'
i v lava i Iglu
iii iuva i=r.ia
T-i-s`v-Ga-!
7
ND mg/kg
2.2 1
111009 11:00
11/12/09 14:19
7782-49-2
JIIVVI
Sodium
uuti
I.4 I11 If\
tj ,y
.11600 mg/kg
7.1 1
1090 1
` `
I111G/VA I I.VV
11/1210911:00
•
11! ILIVS I't. IJ
11112/0914:19
•• 2
f`I-TV-GG-4
7440-23-5
Jij iiiy; ny
2.a i
iit", �rva ii.vG
iii iiiGa i$.ia
6010 MET ICP, TCLP
Analytical Method. EPA 6010 Preparation Method: EPA 3010
Lt-6 ,at= IVl iilVd;Daic. EPA IJ 11,
t Ii IGlVy 15 VV
Arsenic
0.16 mg/L
0.025 1
1/116109 11:05
1111610914:45
7440-38-2
Gil-J111
3.3 IIf JlL
"' t
V.VLJ
. ni. `pr
IIf IVf V� I1.'J:!
. ...,•. • ". _
IIf IVl V,71-r YJ
-+.•..v .,
!-!•-; V-•JJ-J
Cadmium
Diu
0.014 mg/L
0.0050 1
1111=911:05
11/16/09 14:45
7440-43-9
v1711u1i"
'."D 111 ii_ -
�f
" 32
V.VL✓
• Y _ •
iVIVfL'y 11-'J�J
.. ,•
ilf l•JJVJ lT.YJ
7 _ -. 7 ..
r't'+V�tl-J
Lead
ND rng/L
0.025 1
11/16/09 1 i:0115
11116/09 14:45
7439-92-1
JilCtltu111
itlV II;I�IL
V.VJV r
i!) IVJ V.7 11.•JJ
i tf IVIV� fY.Y.J
i7 VL��-L
JiiVC-.'1
ItlV 1ll�fL
V.VLJ !
tl;1V7VJ II.VJ
ISl IIJf VJ IY.TJ
!Y'!V-GG�•f
)ate: 12/08, 2009 09:18 Ali REPORT OF LASORA T ORY ANALYSIS Page 4 of 27
ibis report shaii not be reproduced. except in iuii
without the written consent of Pace Analytical Services, Inc..
fi���a6.

WeAnalXical
mm.pace/abs.com
i
Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NG 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NP11-11-09 POND ASH Lab ID: 9257321001 Collected: 11/11/09 14:15 Received:, 11/11/09 15:50 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311;
11/12/09 15:00
Mercury
ND ug/L
0.20
1
11/13/0915:45
11/1610913:00
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation
Method: EPA 7471
'
Mercury
0.012 mg/kg
0.011
1
11/1210914:10
11/13/0913:22
7439-97-6
8270 MSSV TCLP Sep Funnel
Analytical Method: EPA 8270
1,4-Dichlorobenzene
NO mg/L
0.050
1
1112010909.57
11/21/0919:35
106-46-7
2,4-Dinitrotoluene
NO mg/L
0.13
1
11/20/09 09;57
11121/0919:35
121-14-2
Hexachloro-1,3-butadiene
ND mg/L
0.050
1
1MO109 09:57
11/21/09 19:35
87-68-3
Hexachlorobenzene
NO mg1L
0.050
1
11/20/09 09;57
IM1109 19:35
118-74-1
Hexachloroethane
ND mg/L
0.060
1
11/20/09 09:57
11121/0919:35
67-72-1
2-Methylphenol(o-Cresol)
ND mg/L
0.050
1
11/20/09 09;57
11/21/09 19:35
95-48-7
3&4-Methylphenol(m&p Cresol)
NO mg/L
0.10
1
11/20109 09:57
11/21109 19:35
L1,M0
Nitrobenzene
ND mg/L
0.050
1
11/20109 09:57
11121/09 19:35
98-95-3
Pentachloropheno)
NO mg/L
0.20
1
11/20/09 09.57
11/21/09 19:35
87-86-5
Pyridine
NO mg/L
0.20
1
11/20/09 09:57
11/21/09 19:35
110-86-1
2,4,5-Tri6hlorophenol
NO mg/L
0.050
1
11120/09 09:57
11/21/09 19:35
95-95-4
2,4,6-Trichtorophenol
NO mg/L
0,050
1
11/20/09 09:57
11/21/09 19:35
88-06-2
2-Fluorobiphenyl (S)
69 %
53.5-97.2
1
11/20/09 09:57
11/21109 19:35
321-60-8
Nitrobenzene-d5(S)
93 61.
49.6-97.6
1
11120/0909:57
_11/2110919:35
4165-00-0
Terphenyl-d14 (S)
91 %
62.1-109
1
11/20109 09:57
11121/0919:35
1718-51-0
Phenol-d6 (S)
35 %
10-57.3
1
11/20/09 09:57
11I21/09 19.35
13127-88-3
2-Fluorophenol (S)
45 %
13.2-66.5
1
11120/09 09:57
11/21/09 19:35
367-12-4
2,4,6-Tribromophenoi (S)
83 %
40.5-122
1
11/20/09 09:57
11/21/09 19:35
,18-a79-6
8260 MSV TCLP
Analytical Method: EPA 8260
Benzene
NO ug/L
125,
25
11/17r'09 14:09
71-43-2
2-Butanone (MEK)
ND ug/L
250
25
11/17/09 14:09
78-93-3
Carbon tatrachlonde
NO uglL
125
25
11117/09 14:09
55-23-5
Chlorobenzene
ND ug/L
125
25
11/17/0914.09
108-90-7
Chloroform
ND ug/L
125
25
11/17/09 14:09
67-66-3
1,4-Dichlorobenzene
ND ug/L
125
25
11/17/09 14:09
106-46-7
1,2-Dichioroathane
ND u9&.
125
25
11/17/0914:09
107-06-2
1,1-Dichloroethene
ND ug/L
125
25
11117/09 14:09
75-354
Tatrachloroethane
NO ug/L
125
25
11/17/09 14:09
127-18-4
Trichloroethene
ND ug/L
125
25
11/17/09 14:09
79-01-6
.Vinyl chloride •
ND uglL
125
25
11/17/09 14:09
75-014
1,2-0ichloroethane-d4 (S)
109 %
79-120
25
11/17/09 14:09
17060-07-0
Toluene -dB (S)
98 %
70-120
25
14,117/09 14:09
2037-2G-5
4-Bromofiuorobenzens (S)
92 %
87-109
25
11/17/09 14:09
460-00-4
Dibromofiuoraniethane (S)
100 %
85-115
25
11117109 14:09
1868-53-7
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
60.5 %
0.10
1
11/16/09 09:07
Date: 12/08/2009 09:18 AM REPORT OF LABORATORY ANALYSIS Page 5 of 27
This report shall not oe reproduced, except in full.
without the written consent of Pace Analytical Services, Inc..
melacl.

e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
;-aneAnalyfical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
vimpacolahs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: PONDASH
Pace Project No.: 9257321
Sample: NP11-11-09 PONDASH Lab ID: 9257321001 Collected: 11/11/09 14:15 Received: 11/11/09 15:50 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
9045 pH Soil Analytical Method: EPA 9045
pH at 25 Degrees C 10.6 Std. Units 0.10 1 11/17/09 14:45 H1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 64.8 % 0.10 1 11/13/09 00:00
365.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus 158 mg/kg 15.2 3 11/18/09 12:37 7723-14-0 R1
-)ate: 12/08/2009 09:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
_ elac,
Page 6 of 27

aceAnalXical
www.pacalabs.com
i
Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services. Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NP12-11-09 POND ASH Lab ID: 9257321002 Collected: 11/11/09 14:15 Received: 11/11/09 15:50 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Arsenic
Barium
Cadmium
Calcium
Chromium
Copper
Iron .
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Zinc
7471 Mercury
Mercury
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Phosphorus
.)ate: 12/08/2009 09:18 AM
Analytical Method: EPA 6010 Preparation Method: EPA 3050
31.1 mg/kg
0.98
1
11/12/09 11:00
11/1210914:27
7440-38-2
1390 mg/kg
0.98
1
11/12/09 11:00
11/1210914:27
7440-39-3
2.7 mg/kg
0.20
1
1111210911:00
11112/0914:27
744043-9
104000 mg/kg
197
10
11112/0911:00
11/12/09 16:39
7440-70-2
56.0 mg/kg
0.98
1
11/12/09 11:00
11112/0914:27
7440-47-3
168 mg/kg
0.98
1
11/12/09 11:00
11/12/09 14:27
7440-50-8
10600 mg/kg
9.8
1
11/12/09 11:00
11/1210914:27
7439-89-6
60.7 mg/kg
0.98
1
11/12/09 11:00
11/12/09 14:27
7439-92-1
14400 mg/kg
19.7
1
11/12/09 11:00
11/12/09 14:27
7439-95-4
3780 mg/kg
9.8
10
11/12/0911:00
11/12/0916:39
7439-96-5
ND mg/kg
0.98
1
11/12109 11:00
11/12/09 14:27
7439-98-7
33.2 mg/kg
0.98
1
11/12/09 11:00
11/12/09 14:27
7440-02-0
13300 mg/kg
9830
10
11/12/09 11:00
11/12/09 16:39
7440-09-7
2.1 mglkg
2.0
1
11/12/09 11:00
11/12/09 14:27
7782-49-2
1.5 mg/kg
0.98
1
11/12/09 11:00
11/12/09 14:27
7440-22-4
11900 mglkg
983
1
11/12/09 11:00
11/12109 14:27
7440-23-5
369 mg/kg
2.0
1
/1/12109 11:00
11/12/09 14:27
7440-66-6
Analytical Method: EPA 7471 Preparation Method:
EPA 7471
ND mg/kg
0.011
1
11/12/09 14:10
11/13/09 13:25
7439-97-6
Analytical Method: ASTM D2974-87
62.6 %
0.10
1
11/16/09 09:08
Analytical Method: EPA 9045
10.6 Std. Units
0.10
1
11/17/09 14:45
H1
Analytical Method: EPA 365.1
3210 mg/kg 160 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
11118/0914:32 7723-14-0 MO
Page 7 of 27

a Pace Analytical Services, Inc. Pace Analytical Services, Inc.
/7PalceAnalXical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
mm.pacelabsxam Asheville, NC 28804 Huntersville, NC 28078
ANALYTICAL RESULTS
Project: POND ASH
Pace Project No.: 9257321
[phone] [phone]
Sample: STORM WATER
Lab ID: 9257321003 Collected: 11/11109 14:00
Received: 11/11/09 15:50 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
67.0 mg1L
12.5 1
11/17/09 08:46
9040 pH
Analytical Method: EPA 9040
pH
6.8 Std. Units
0.10 1
11/23/09 10:00 H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
165 mg/L
25.0 1
11/23/09 09:50
)ate: 12/08/2009 09:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pare Analytical Services, Inc..
a`
Page 8 of 27

�aceAnalytical
www.pacclabs.com
r
Project: POND ASH
Pace Project No.: 9257321
QC Batch: OEXT/8678
QC Batch Method: EPA 3535
Associated Lab Samples: 9257321001
METHOD BLANK: 372240
Associated Lab Samples: 9257321001
Parameter
Units
Chlordane (Technical)
ug/L
Endrin
ug/L
gamma-BHC (Lindane)
ug/L
Heptachlor epoxide
ug/L
Methoxychlor
ug/L
Toxaphene
ug/L
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 8081
Analysis Description: 8081 GCS TCLP Pesticides
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed Qualifiers
ND
3.0
12/03/09 05:24
ND
0.50
12/03/09 05:24
ND
0.50
12/03/09 05:24
ND
0.50
12/03/09 05:24
ND
1000
12/03/09 05:24
ND
3.0
• 12/03/09 05:24
66
10-138
12/03/09 05:24
45
10-110
12/03/09 05:24
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 372241
372242
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Cone.
Result
Result
% Rec
% Rec
Limits RPD
RPD Qualifiers
Endrin
ug/L
.4
ND
ND
53
37
20-134
30
gamma-BHC (Lindane)
ug/L
.4
ND
ND
69
44
20-118
30
Heptachlor epoxide
ug/L
.4
ND
ND
58
41
22-133
30
Methoxychlor
ug/L
1.4
ND
ND
64
43
44-150
30 L2
Decachlorobiphenyl (S)
%
65 •
37
10-138
Tetrachloro-m-xylene (S)
%
155
68
10-110
SO
)ate: 12/08/2009 09:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
,n.'pC pip,
p 'elk,
Page 9 of 27

'aceAnalXical
wvrw.pacelahs.cam
Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 FQncey Ave. Suite 100
Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
QC Batch: GCSV/1344 Analysis Method: EPA 8151
QC Batch Method: EPA 8151 Analysis Description: 8151 GCS Herbicides TCLP
Associated Lab Samples: 9257321001
METHOD BLANK: 19508
Associated Lab Samples: 9257321001
Parameter Units
2,4,5-TP (Silvex) mg/L
2,4-D mg/L
2,4-DCPA (S) %
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.010 11/20/09 08:05
ND 0.010 11/20/09 08:05
107 70-130 11/20/09 08:05
LABORATORY CONTROL SAMPLE: 19509
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
2,4,5-TP (Silvex) mg/L .012 0.012 98 70-130
2,4-D mg/L .06 0.060 100 70-130
2,4-DCPA (S) % 109 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
19510,
19511
MS
MSD
9257321001
Spike.
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
2,4,5-TP (Silvex)
mg/L
ND
.0341
.0341
0.033
0.035
97
101
70-130 5
2,4-D
mg1L
ND
.17
.17
0.17
0.18
102
104
70-130 2
2,4-DCPA (S)
%
109
116
70-130
Date: 12/08/2009 09:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 27

Y1,, 'aceAnalXical
wvm.pacolebs.com
i
Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
(QUALITY CONTROL DATA
QC Batch: MPRP/5373 Analysis Method: EPA6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 9257321001, 9257321002
METHOD BLANK: 365305 Matrix: Solid
Associated Lab Samples: 9257321001, 9257321002
Parameter
Units
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Iron
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Manganese
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
LABORATORY CONTROL SAMPLE: 365306
Parameter
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Iron
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Manganese
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Date: 12/08/2009 09:18 AM
Blank
Result
Reporting
Limit
Analyzed
ND
0.50
11/1210913:45
ND
0.50
11112/0913:45
ND
0.10
11/12/0913:45
ND
10.0
11/1210913:45
ND
0.50
11/12/09 13:45
ND
0.50
11/1210913:45
ND
5.0
11/12/0913:45
ND
0.60
11112/0913:45
ND
10.0-
11/12/0913:45
ND
0.50
11/1210913:45
ND
0.50
11/12/0913:45
ND
0.50
11/12/09 13:45
ND
500
11/12/0913:45
ND
1.0
11/1210913:45
ND
0.50
11112/0913:45
ND
500
11/12/0913:45
ND
1.0
11112/0913:45
Qualifiers
Spike
Units Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
50
48.5
97
80-120
50
49.7
99
80-120
50
49.0
98
80-120
500
542
108
80-120
50
49.3
99
80-120
50
49.0
98
80-120
500
518
104
80-120
50
48.9
98
80-120
500
517
103
80-120
50
50.5
101
80-120
50
51.2
102
80-120
50
49.4
99
80-120
500
493J
99
80-120
50
48.2
96
80-120
25
26.0
104
80-120
500
546
109
80-120
50
50.1
100
80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
elk.
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 11 of 27

;'aceAn'alyficalo
�nrnvpscelabs,crom
Project: POND ASH
Pace Project No.: 9257321
MATRIX SPIKE SAMPLE:
Parameter
Arsenic
Barium
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Zinc
SAMPLE DUPLICATE: 365308
Parameter
Arsenic
Barium
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Zinc
Date: 12/0812009 09:18 AM
365307
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mglkg
mg/kg
mg/kg
mg/kg
mglkg
mg/kg
mg/kg
mg/kg
mglkg
mg/kg
Units
mg/kg
mglkg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mglkg
mg/kg
mg/kg
mg/kg
mg/kg
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
9257331001
Result
13.5
24.6
5.0
9.51
20.2
41.8
26500
17.1
114
384
4.6
5.2
405J
1.1
0.17J
9.91
34.6
9257237001
Result
ND
ND
ND
9.78 ug/g
ND
ND
4.09 ug/g
ND
ND
1.13 ug/g
ND
0.392 ug/g
ND
ND
ND
ND
ND
Spike
Conc.
50.7
50.7
50.7
507
50.7
50.7
507
50.7
507
50.7
50.7
50.7
507
50.7
25.3
507
50.7
Dup
Result
ND
ND
ND
ND
.13J
.028J
2.5
ND
.39J
1.5
ND
0.36
ND
0.56
ND
.88J
ND
MS
MS
Result
% Rec
58.1
88
71.2
92
48.9
87
493
96
67.0
93
96.2
107
25200
-270
57.8
80
520
80
433
98
50.0
90
48.4
85
966
111
43.8
84
25.1
99
666
130
81.6
93
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent
of Pace Analytical Services, Inc..
28 R1
9
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
75-125
75-125
75-125
75-125
75-125
75-125
75-125 MO
75-125
75-125
75-125
75-125
75-125
75-126
75-125
75-125
75-125 MO
75-125
Page 12 of 27

°ace Analytical
v mvpacalabs.com
i
Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 26804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/5390
QC Batch Method: EPA 3010
Associated Lab Samples: 9257321001
Analysis Method:
Analysis Description:
EPA 6010
6010 MET TCLP
METHOD BLANK: 366926
Matrix: Water
Associated Lab Samples: 9257321001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.025
11116/0914:29
Barium
mg/L
ND
0.025
11/16/0914:29
Cadmium
mg/L
ND
0.0050
1111610914:29
Chromium
mg/L
ND
0.025
11/16/0914:29
Lead
mg/L
ND
0.025
11/16/0914:29
Selenium
mg/L
ND
0.050
11116/0914:29
Silver
mg/L
ND
0,025
11/1610914:29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
366927
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/L
2.5
2.7
109
80-120
Barium
mg/L
2.5
2.3
94
80-120 .
Cadmium
mg/L
2.5
2.5
99
80-120
Chromium
mg/L
2.5
2.5
100
80-120
Lead
mg/L
2.5
2.3
94
80-120
Selenium
mg/L
2.5
2.8
113
80-120
Silver
mg/L
1.2
1.3
105
80-120
MATRIX SPIKE SAMPLE:
366928
9256972001
Spike
MS
MS
% Rec
Parameter
Units
Result
Cone.
Result
% Rec
Limits Qualifiers
Arsenic
mg/L
ND
2.5
2.5
98
75-125
Barium
mg/L
0.18
2.5
2.3
83
75-125
Cadmium
mg/L
0.0073
2.5
2.2
89
75-125
Chromium
mg/L
ND
2.5
2.2
89
75-125
Lead
mg/L
ND
2.5
2.1
84
75-125
Selenium
mg/L
ND
2.5
2.5
100
75-125
Silver
mg/L
ND
1.2
1.2.
- 92
75-125
SAMPLE DUPLICATE: 366929
9257321001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Arsenic
mg/L
0.16
0.15 3
Barium
mg/L
3.8
4.0 4
Cadmium
mg/L
0.014
0.015 8
Chromium
mg/L
ND
.0065J
Lead
mg/L
ND
ND
Date: 12/08/2009 09:18 AM REPORT OF LABORATORY ANALYSIS Page 13 of 27
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
�n'ela-

a'cc eAnalytical
www.pacclabs.com
a
Project: POND ASH
Pace Project No.: 9257321
SAMPLE DUPLICATE: 366929
Parameter
Selenium
Silver
-)ate: 12/08/2009 09:18 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
9257321001 Dup
Units Result Result
mg/L ND ND
mg/L ND .011J
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
---nela
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 27

.11-11
raceAnalytical
wwwpacelabs.com
Project: POND ASH
Pace Project No.: 9257321
QC Batch: MERP/2504
QC Batch Method: EPA 7470
Associated Lab Samples: 9257321001
METHOD BLANK: 366353
Associated Lab Samples: 9257321001
Parameter Units
Mercury ug/L
LABORATORY CONTROL SAMPLE: 366354
Parameter Units
Mercury ug/L
MATRIX SPIKE SAMPLE: 366355
Parameter Units
Mercury ug/L
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7470
Analysis Description: 7470 Mercury TCLP
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.20 11/16/0912:45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.4 97 80-120
9256972001 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 2.5 1.8 72 75-125 MO
SAMPLE DUPLICATE: 366356
9257321001 Dup
Parameter Units Result Result RPD Qualifiers
Mercury ug/L ND ND
Jate: 12/08/2009 09:18 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
AJBIIac
Page 15 of 27

�aceAnalXical
wvnupacalr�bs.com
Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP/2499 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 9257321001, 9257321002
METHOD BLANK: 365346 Matrix: Solid
Associated Lab Samples: 9257321001, 9257321002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0050 11/1310912:14
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 365347
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg .067 0.063 95 80-120
MAI NIX SPIKE SAMPLE:
365348
9257108001
Spike MS MS % Rec
Parameter
Units
Result
Conc. Result % Rec Limits Qualifiers
Mercury
mg/kg
2.0
.081 1.6 -486 75-125 MO
SAMPLE DUPLICATE: 365349
9257108002
Dup
Parameter
Units
Result
Result RPD Qualifiers
Mercury
mg/kg
4.4
6.7 42 R1
Date: 12/08/2009 09:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
.`i�
.`rye{ace;
Page 16 of 27

-aceAnalXical
www.pacelgbs.com
t
Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSSV/1357 Analysis Method: EPA 8270
QC Batch Method: EPA 8270 Analysis Description: 8270 TCLP MSSV
Associated Lab Samples: 9257321001
METHOD BLANK: 19901 Matrix: Water
Associated Lab Samples: 9257321001
Parameter
Units
Blank
Result
1,4-Dichlorobenzene
mg/L
ND
2,4,5-Tdchlorophenol
mg/L
ND
2,4,6-Tdchlorophenol
mg/L
ND
2,4-Dinitrotoluene
mg/L
ND
2-Methylphenol(o-Cresol)
mg/L
ND
3&4-Methylphenol(m&p Cresol)
mg/L
ND
Hexachloro-1,3-butadiene
mg/L
ND
Hexachlorobenzene
mg/L
ND
Hexachloroethane
mg/L
ND
Nitrobenzene
mg/L
ND
Pentachlorophenol
mg/L
ND
Pyridine
mg/L
ND
2,4,6-Tdbromophenol (S)
%
75
2-Fluorobiphenyl (S)
%
63
•2-Fluorophenol (S)
%
40
Nitrobenzene-d5 (S)
%
86
Phenol-d6 (S)
%
31
Terphenyl-d14 (S)
%
78
Reporting
Limit Analyzed Qualifiers
0.050
11 /21109 18:35 IS
0.050
11/21/09 18:35
0.050
11/21/09 18:35
0.13
11/21/09 18:35
0.050
11 /21109 18:35
0.10
11/21/09 18:35
0.050
11/21/09 18:35
0.050
11/21/09 18:35
0.050
11/21/09 18:35
0.050
11/21/09 18:35
0.20
11/21/09 18:35
0.20
11/21/09 18:35
40.5-122
11/21/09 18:35
53.5-97.2
11/21/09 18:35
13.2-66.5
11/21/09 18:35
49.6-97.6
11/21/09 18:35
10-57.3
11/21/09 18:35
62.1-109
11121 /09 18:35
LABORATORY CONTROL SAMPLE:
Parameter
19902
Units
Spike
Conc.
LCS
Result
LCS
% Rec
1,4-Dichlorobenzene
mg/L
.5
0.31
63
2,4,5-Tdchlorophenol
mg/L
.5
0.43
85
2,4,6-Tdchlorophenol
mg/L
.5
0.45
89
2,4-Dinitrotoluene
mg/L
.5
0.42
84
2-Methylphenol(o-Cresol)
mg/L
.5
0.36
71
3&4-Methylphenol(m&p Cresol)
mg/L
.5
0.34
69
Hexachloro-1,3-butadiene
mg/L
.5
0.39
78
Hexachlorobenzene
mg/L
.5
0.42
85
Hexachloroethane
mg/L
.5
0.35
70
Nitrobenzene
mg/L
.5
0.39
78
Pentachlorophenol
mg/L
.5
0.49
98
Pyridine
mg/L
.5
0.22
44
2,4,6-Tribromophenol (S)
%
92
2-Fluorobiphenyl (S)
%
74
2-Fluorophenol (S)
%
42
Nitrobenzene-d5 (S)
%
88
Phenol-d6 (S)
%
34
Terphenyl-d14 (S)
%
73
Date: 12/08/2009 09:18 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
«o,�
i1i ,
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
39.3-83.6
42.7-114
41.2-111
58-111
41.4-83.9
16.1-42.4 L3
20.7-99.2
62.6-106
24.3-91.5
46.4-95
10-207
10-72.9
40.5-122
53.5-97.2
13.2-66.5
49.6-97.6
10-57.3
62.1-109
Page 17 of 27

;-aucceaAnalytical
/ swnupacolabs.com
Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
19903
MS
9257321001
Spike
Parameter
Units
Result
Cone.
1,4-Dichlorobenzene
mg/L
ND
.5
2,4,5-Trichlorophenol
mg/L
ND
.5
2,4,6-Tdchlorophenol
mg/L
ND
.5
2,4-Dinitrotoluene
mg/L
ND
.5
2-Methylphenol(o-Cresol)
mg/L
ND
.5
3&4-Methylphenol(m&p
mg/L
ND
.5
Cresol)
Hexachloro-1,3-butadiene
mg/L
ND
.5
Hexachlorobenzene
mg/L
ND
.5
Hexachloroethane
mg/L
ND
.5
Nitrobenzene
mg/L
ND
.5
Pentachlorophenol
mg/L
ND
.5
Pyridine
mg/L
ND
.5
2,4,6-Tdbromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
Date: 12/08/2009 09:18 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
19904
MSD
Spike
MS
MSD
MS
MSD % Rec
Cone.
Result
Result
% Rec
% Rec Limits
RPD Qual
.5
0.25
0.30
50
59 39.3-83.
18
.5
0.41
0.41
82
82 42.7-114
.8
.5
0.40
0.42
81
85 41.2-111
5
.5
0.39
0.40
79
80 58-111
2
.5
0.29
0.35
58
70 41,4-83.
20
.5
0.29
0.40
57
80 16.1-42.
33 MO
.5
0.32
0.37
63
75 20.7-99.
17
.5
0.41
0.41
82
81 62.6-106
.7
.5
0.27
0.33
53
66 24.3-91.
22
.5
0.35
0.41
71
82 46.4-95
15
.5
0.49
OA9
98
98 10-207
.2
.5
.191
0.21
37
41 10-72.9
88
91 40.5-122
65
69 53.5-97.
36
46 13.2-66.
77
92 49.6-97.
30
52 10-57.3
76
79 62.1-109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
'ieh
Page 18 of 27

ZPAnalyiical
wwv,.pacefabs.com
Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc_
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/9074 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV TCLP
Associated Lab Samples: 9257321001
METHOD BLANK: 367322
Associated Lab Samples:
Parameter
9257321001
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1-Dichloroethene
ug/L
ND
5.0
11/17/09 10:11
1,2-Dichloroethane
ug/L
ND
5.0
11/17/09 10:11
1,4-Dichlorobenzene
ug/L
ND
5.0
11/17/09 10:11
2-Butanone (MEK)
ug/L
ND
10.0
11/17/09 10:11
Benzene
ug/L
ND
5.0
11/1710910:11
Carbon tetrachloride
ug/L
ND
5.0
11/17/09 10:11
Chlorobenzene
ug/L
ND
5.0
11/17/09 10:11
Chloroform
ug/L
ND
5.0
11/17/09 10:11
Tetrachloroethene
ug/L
ND
5.0
11/17/09 10:11
Trichloroethene
ug/L
ND
5.0
11/17/09 10:11
Vinyl chloride
ug/L
ND
5.0
11/17/09 10:11
1,2-Dichloroethene-d4 (S)
%
100
79-120
11/17/09 10:11
4-Bromofluorobenzene (S)
%
101
87-109
11/17/09 10:11
Dibromofluoromethane (S)
%
99
85-115
11/17/09 10:11
Toluene-d8 (S)
%
99
70-120
11/17/09 10:11
LABORATORY CONTROL SAMPLE: 367323
'Parameter
1,1-Dichloroethene
ug/L
1,2-Dichloroethane
ug/L
1,4-Dichlorobenzene
ug/L
2-Butanone (MEK)
ug/L
Benzene
ug/L
Carbon tetrachloride
ug/L
Chlorobenzene
ug/L
Chloroform
ug/L
Tetrachloroethehe
ug/L
Trichloroethene
ug/L
Vinyl chloride
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Dibromofluoromethane (S)
%
Toluene-d8 (S)
%
-)ate: 12/08/2009 09:18 AM
Spike
Units Conc.
LCS
Result
50
58.8
50
61.1
50
57.4
100
129
50
60.1
50
64.6
50
60.1
50
61.6
50
61.5
50
58.8
50
63.4
LCS
% Rec
Qualifiers
% Rec
Limits
118 50-150
122 50-150
115 50-150
129 50-150
120 50-150
129 50-150
120 50-150
123 50-150
123 50-150
118 50-150
127 50-150
101 79-120
98 87-109
100 85-115
96 70-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 19 of 27

/�ParlceAnalyfical
/ www.pacelabs.com
Project: POND ASH
Pace Project No.: 9257321 .
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QG Batch: PMST12881 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9257321001, 9257321002
SAMPLE DUPLICATE: 366334
Parameter
Percent Moisture
SAMPLE DUPLICATE: 366335
Parameter
Percent Moisture
Date: 12/08/2009 09:18 AM
9257321001 Dup
Units Result Result RPD Qualifiers
% 60.5 61.3 1
Units
9257466007 Dup
Result Result RPD Qualifiers
29.3 29.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PaceAnalytical Services, Inc...
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 27

1�;a'ceAnalj4ical'
www.pacetabs.cbm
i
Project: POND ASH
Pace Project No.: 9257321
QC Batch: WET/10499
QC Batch Method: SM 2540D
Associated Lab Samples: 9257321003
METHOD BLANK: 367083
Associated Lab Samples: 9257321003
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE:
367084
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 367085
Parameter
Units
Total Suspended Solids
mg/L
Date: 12/08/2009 09:18 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 11/17/09 08:38
Spike LCS
Conc. Result
250 242
9257578001 Dup
Result Result
239 343
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
97 80-120
RPD Qualifiers
36 R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
lac,,
Page 21 of 27

_ ;'a'ceAnalytica-
www.pacelabs.com
Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville. NC 26804
[phone]
QUALITY CONTROL DATA
QC Batch: WET/10565 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 9257321003
SAMPLE DUPLICATE: 370181
Parameter
pH
Date: 12/08/2009 09:18 AM
9257328001 Dup
Units Result Result
Std. Units 7.7 7.7
RPD Qualifiers
0 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 27

ceAnalytical
www.piicolabs.com
7
Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WET110505 Analysis Method: EPA 9045
QC Batch Method: EPA9045 Analysis Description: 9045 pH
Associated Lab Samples: 9257321001, 9257321002
SAMPLE DUPLICATE: 367430
9257321001 Dup
Parameter Units Result Result
pH at 25 Degrees C Std. Units 10.6 10.6
Date: 12/08/2009 09:18 AM
RPD Qualifiers
0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Me c,.°
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 27

,, aceAnalydical
wwwpacvlabs.com
i
Project: POND ASH
Pace Project No.: 9257321
QC Batch: WET/1703
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 9257321001
SAMPLE DUPLICATE: 19408
Parameter Units
Percent Moisture %
Date: 12/08/2009 09:18 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
353794001 Dup
Result Result RPD Qualifiers
97.0 97.0 .006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 27

�aceAnalytical
mmpacelabs.com
Project: POND ASH
Pace Project No.: 9257321
QC Batch: WETA/6267
QC Batch Method: EPA 365.1
Associated Lab Samples: 9257321001, 9257321002
METHOD BLANK: 367255
Associated Lab Samples: 9257321001, 9257321002
Parameter
Units
Phosphorus
mg/kg
LABORATORY CONTROL SAMPLE:
367256
Parameter
Units
Phosphorus
mg/kg
MATRIX SPIKE SAMPLE:'
368079
Parameter
Units
Phosphorus
mg/kg
SAMPLE DUPLICATE: 368078
Parameter
Units
Phosphorus
mg/kg
Date: 12/08/2009 09:18 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 11118/0912:23
Pace Analytical Services, Inc.
9800 Kncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
20 19.3 97 90-110
9257321002 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
3210 53.5 2550 -1221 90-110 MO
9257321001 Dup
Result .Result
158 991
RPD Qualifiers
145 R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
.c«„u
Page 25 of 27

Ar
_; FaceAnalytical
www.pocalabs.com
Project: POND ASH
Pace Project No.: 9257321
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
QUALITY CONTROL DATA
QC Batch: WETA16304 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 9257321003
METHOD BLANK: 370221
Associated Lab Samples: 9257321003
Parameter Units
Chemical Oxygen Demand mg/L .
LABORATORY CONTROL SAMPLE: 370222
Parameter Units
Chemical Oxygen Demand mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 11/23/09 09:50
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
750 713 95 90-110
MATRIX SPIKE SAMPLE:
370223
9257306001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg/L
33.0
750
776
99
75-125
MATRIX SPIKE SAMPLE:
370225
9257314009
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg/L
81.0
750
842
101
75-125
SAMPLE DUPLICATE: 370224
9257306002 Dup
Parameter Units Result Result RPD Qualifiers
Chemical Oxygen Demand mg/L 38.0 46.0 19
SAMPLE DUPLICATE: 370226
9257334001 Dup
Parameter Units Result Result RPD Qualifiers
Chemical Oxygen Demand mg/L 1290 1310 2
Date: 12/08/2009 09:18 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
'`pie
Page 26 of 27

_� a'OAnalytical
www.pacolabs.com
QUALIFIERS
Project: POND ASH
Pace Project No.: 9257321
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
'Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
H6 Analysis initiated more than 15 minutes after sample collection.
IS The internal standard response is below criteria. Results may be biased high.
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
12 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
R1 RPD value was outside control limits.
So Surrogate recovery outside laboratory control limits.
[phone]
,Date: 12/08/2009 09:18 AM REPORT OF LABORATORY ANALYSES Page 27 of 27
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

z
Energy Generation NA
Please test the sample(s) for the parameters as listed belov.
Send invoice and copy of results to: Send original results to:
Ricky Styles Summer Barber
SUEZ Energy BioPower, Inc. SUEZ Energy BioPower, Inc.
2859 Old Linville Rd. 1990 Post Oak Blvd. Suite 1900
Marion, NC 28752 Houston, TX 77056
ricky.styte-g0-gdfsuezna.com summer.barber(Wgdfsuezna com
(828) 756-4W 713-636-1639
(fax) 756-7160
5 DAY RESULTS PLEASE
Reauested Due Date:
12r5'7 3 z I
Sample #
Sample
Description
Sample Date(s)
and time sample
collected
Grab or
Composite
Total Metals -
As, Ba, Cd,
Ca, Cr, Cu, Fe,
Pb, Mg, Hg,
Mn, Mo, N1, K,
Se, Ag, Na, Zn,
total
Phosphorus
TCLP Metals
As, Ba, Cd,
Cr, Pb, Hg,
Se,.A9
Ignitability,
Reactivity
pH
Corrosivity
Total -Arsenic
Full TCLP
NP11-11-09
POND ASH
11-11-09 2:15PM
Grab
YES
YES
YES
NP12-11-09
POND ASH
11-11-09 2:15PM
Grab
YES
YES
Sample sent to: Pace Analytical Services, 1
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
rti�ir �f"4..
Project Manager. Kevin Godwin
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
(704) 875 - 9092 ext. 233
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Date:
Facility:
Time
PH buffe
Analyst: R •c�- y 54 /Pe -
Calibration
a! Buffer Cal Buffer Check
7.0 10.0 Duffer 1 2.0*
are to be within t 0.1 pH units of the standard's true
Comments
pH Analyses
Time Time Duffer
Sam le ID Sam led Anal zed H Result Check
.Comments
9 11.9y
'- Indicates a recommended drift check using Buffer 12.0 at he endOf testin or
Results should be within t 0.1 pH units of the standard's true value. 9 every 4 hours minimum.
Results and Buffers are in standard units
Updated 7-29-09

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Monitoring Period: From
To
WQ Permit Number:
NPDES Number:
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerformed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment)
Alt. C (Prior Testing)
`' '' ' ' '
A1t.D (No Prior Test)
Process to Further Reduce Pathogengs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying
Heat Treatment
Thermophilic
Beta Ray
Gamma Ray
Pasteurization
.......................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying
Composting
jAerobic Digestion
Anaerobic Digestion
...........................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
Minimum
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
i�®t Required by Permit
laT!'1 ♦ � n..m ....... �. _. _ _
CFU
1000 mpn per gram
of total solid (dry
weight).
Salmonella bacteria
(in lieu of fecal
coliform)
t%nn+a... A 1f..n..4;....
3 MPN per 4 grams
total solid (dry
weight)
D..d....67...- /� c ♦
Alt.1 (VS reduction)
Alt. 2 (40-day bench)
Alt. 3 (30-day bench) Alt. 4 (Spec. 02 uptake)
Alt. 5 (14-Day Aerobic)
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) I Alt. 8 (Drying - Unstable)
Alt. 9 (Injection)
f� DTThi Ird" A rP7/lAT OrT 1 TT.
Alt. 10 (Incorporation)
T --
No vector attraction reduction alternatives were performed
v L+1�111.1-A l iVl\ uitsi EMLEN 1 kpiease cnecx the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Preparer Name and Title (type or print)
Signature of Preparer*
Land Applier Name and Title (if applicable)(type or print)
Date Signature of Land Applier (if applicable) , Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)