WQ0010689_Report_20120222

4 fV},ai3 �i Yj}� i :�G
12 FEB 2_9 rMl 9: 59
February 22, 2012
NCDENR - DWQ
Aquifer Protection Section
Land Application Unit
2728 Capital Boulevard
Raleigh, NC 27604
RE: 2011 Annual Ash Report
Permit No. WQ0010689
Wood Boiler — North Cove, NC
01 2Ci2
Office
-- A�irtifor P raf otinn
Enclosed is the annual as distribution report for the calendar year 2011, using the forms provided
by NCDENR-DWQ. During 2011, ash was distributed in two forms:
1. Flyash that settled into the scrubber ponds was mixed with flyash from the multi -cyclone,
bottom ash, and dry wood to reduce the moisture content. The ash was distributed for
land application in this form. See the ash distribution records for a list of recipients.
2. Bottom ash from the boiler grate was also distributed.- This ash was hauled in a very dry
form and used as a soil amendment in a commercial operation. A composite sample was
collected and Total metals and TCLP were performed before distribution. Additionally,
bottom ash was mixed with pond ash to help reduce the moisture content.
3: 1348 dry tons were generated during 2011. Monitoring frequency requirements as
established by 40 CFR 503 and 15A NCAC 02T .111 were met (I/quarter — 4 times per
year). Additional samples were collected on 04/18/11, 08/05/11, and 12/15/11, in which
all permit parameters were not requested for analysis on the chain of custody.
4. Permit requirements for the sampling and analysis for Corrosivity, Ignitability,
Reactivity, and Toxicity Characteristics Leaching Procedure (TCLP) were met.
All samples were analyzed by Pace Analytical Services, Inc., a North Carolina certified
laboratory.
If you have any questions or require additional information, please contact Anita Jensen at
828.756.6734 or Ricky Styles at 828.756.6650.
Sincerely,
iq",l a'e
Mike Howell
Plant Manager
Baxter Healthcare Corporation
Po Box 1390, Marion, NC 28752
T 828.756.4151

Enclosures: DWQ Reporting Forms
Ash Distribution Records
Pace Analytical Laboratory Reports
Cc: NC Division of Water Quality (3 additional copies with enclosures)
Ricky Styles
Anita Jensen

2011 Ash Inventory
4 4aa
_H
%rNWR
March
South Pond Ash
Bobby Boone
297.0
April
South Pond Ash
Phillips Farm Mitchell Co.
297.0
August
North Scrubber Pond
Bobby Boone
4.9
August
North Scrubber Pond
Chris Wall
4.9
August
North Scrubber Pond
Matt Cook
14.7
-August
North Scrubber Pond
Mike Hughes
436.1
August
North Scrubber Pond
Phillips Farm Mitchell Co.
29.4
October
South Scrubber Pond
Bobby Boone
86.4
October
South Scrubber Pond
Dean McClure
9.6
October
South Scrubber Pond
Max Holland
158.4
October
South Scrubber Pond
Ricky Styles
9.61
I - - rofar-Dry Fons 1446. U I
5/9/11
South Scrubber Pond
IN SERVICE
5/9/11
North Scrubber Pond
OUT OF SERVICE
9/5/11
North Scrubber Pond
IN SERVICE
9/5/11
South Scrubber Pond
OUT OF SERVICE
10/17/11
South Scrubber Pond
IN SERVICE
12/13/11
South Scrubber Pond-
OUT OF SERVICE
Note: Scrubber ash includes sandbox ash used to dry ponds

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0010689
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analvsis Data
Baxter Healthcare Inc.
WQ0010689
Laboratory:
1) Pace Analytical Services; Inc.
2)
5 3)
4
,1 k
IyVA tiol C� P
Parameter
(mg/kg)
Conc.
Limit
m k a
Scr?-S . Sample o Composite Date
Bottom
02/04/11
SP 1'
03/03/11
SP 2
03/03/12
Bottom
04/18/l1
NP 1
06/28/11
Bo
08 /11
SP
09/O1/11
Ash A,
12/15/11
Ash B
12/15/11
Percent Solids (%)
NA
99.86v
45.1-
46.3
99.22t,
52.8
97.5 �-
42.8 -`'
99.88+-
46.6 e-
Arsenic
75
5
11.3 v
8.9 -,
8.9 r
14.4 v
12.1 V
16.6 v
8 �,
16.1
Cadmium
85
- 2 a
1.9 v
1.8
0.56 v
2.2 -,
1.9
2.5 v
1.8 v
2.7 t.
Copper
4,300
122 a
73.4 v
60.2 t-
91.6
92.4 m
97.210
97.5 v
89.2 v
97.8 ►�
Chromium
NA
18.9 v
22 v
17.1 v
32.5 v
26.1-,
32.8 b
22.1 v
28.8 m
25.5 w
Lead
840
28.9 v
22 v
20.7Y
91.9v
32.41'
C318
23,6 v
93.8 1,
27.
Mercury
57
ND ✓
ND v
0.0091�
ND d
0.0221.
0.015 v
ND w
0.028w
Molybdenum
75
1.3 ✓
ND v
ND V
0.74 4-
5.1 e
1.1 v
ND "
1.3 v
1.3,-
Nickel
420
19.9 v
12.7 v
11.4 -
15.4,-
16.4 -
22.1
13.3'0
14.1
15.2 v
Selenium
100
ND v
ND v
ND
1.2 r
ND v
ND
ND V
1.9 v
ND'
Zinc
7,500
1520 v
499 ./
181 ''
265 -
254 --
90.5+-
225 ,,
loot,
264
Total Phosphorus
NA
564
2950
2640
1510
3340
3080
1680
3310
TKN
NA
Ammonia -Nitrogen
NA
Nitrate and Nitrite
NA
For surface disposal facilities the ceiling concentration limitsAisted in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties f bmittin false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparre Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0010689
]Facility Name: Baxter Healthcare Inc.
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analysis Data
WQ0010689
Laboratory: 1) Pace Analytical Services, Inc.
2)
3)
4)
5)
Parameter
(mg/kg)
Sample or Composite Date
Bottom
02/04/11
SP 1
03/03/11
SP 2
.03/03/12
Bottom
04/18/11
NP 1
06/28/11
Bottom
08/05/11
SP
09/01/11
Ash A
12/15/11
Ash B
12/15/11
pH
11.5
9.3
9.2
9.4
8.7
8.5
Barium
1240
1130
1040
1440
1350
1530
1340
1390
1410
Calcium
49900
64600
57400
46200
64200
55000
75200
56400
86100
Iron
16700
7040
6160
18600
14300
13600
8800
20300
9760
Magnesium
8030
11600
10800
8240
13000
9480
12200
8850
12300
Manganese
1410
2680
2000
1640
2410
2000
2280
1850
3200
Potassium
15500
14200
11600
19800
15800
19000
20400
24500
25100
Silver
0.64
ND
ND
0.51
0.93
0.93
1.2
0.68
1.3
Sodium
13300
9490
8200
14400
12300
11400
15800
10900
18400
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significan�enalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Prepares
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
,2/ C0 /Z
Date

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0010689 FACILITY NAME:
PHONE:[phone] COUNTY:
FACILITY TYPE (please check one):
Baxter Healthcare Inc.
Baxter Healthcare Inc.
❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
a Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 0 No ❑ —► If No skip parts A B C and certif form bel
ivicuowen
OPERATOR:
Part A*:
y ovi
Part B*:
i
Sources() (s nclude NPDES # if
Volume (dry tons)
Recipient Information
Amendment/
Bugg Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
Month
applicable)
January
See Attached DMSDF (Supp)
February
Sheet for Details
March
April
May
June
'
Julycc
7-
August
September
October
November
December
Total from FORM DMSDF (sup)
-0-
': -0
0
0
Totals:.
Annual (dry tons):
F .0. .
_ .. 0
0
.........................
0-
Amendment(s) used-
* If
Bulking Agent(s) used:
517
more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit p Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No -0 If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled.with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
l(0%/z
Signature of Permittee Date Signature of Pr er** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0010689 FACILITY NAME:
PHONE: [phone] COUNTY: McDowell
FACILITY TYPE (please check one):
Baxter Healthcare Inc.
OPERATOR: Baxter Healthcare Inc.
❑ Surface Disposal (complete Part A "Month", "Source(s)" and "Residual In" columns only)
Ef Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
March
WQ0010689
42.5
254.5
297
Bobby Boone
297
Land Application
April
WQ0010689
42.5
254.5
297
Phillips Farm Mitchell Co.
297
Land Application
August
WQ0010689
0.91
3.99
4.9
Bobby Boone
4.9
Land Application
August
WQ0010689
0.91
3.99
4.9
Chris Wall
4.9
Land Application
August
WQ0010689
2.73
11.97
14.7
Matt Cook
14.7
Land Application
August
WQ0010689
80.99
355.11
436.1
Mike Hughes
436.1
Land Application
August
WQ0010689
5.46
23.94
29.4
Phillips Farm Mitchell Co.
29.4
Land Application
October
WIQ0010689
34.04
52.36
86.4
Bobby Boone
86.4
Land Application
October
WQ0010689
3.78
5.82
9.6
Dean McClure
9.6
Land Application
October
WQ0010689
62.4
96
158.4
Max Holland
158.4
Land Application
October
WQ0010689
3.78
5.82
9.6
Ricky Styles
9.6
Land Application
Totals:
Annual (dry tons):
= - ` '- " =280
-1068
1348 ` 13.48
Amendment(s) used: I
Bulking.Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 1 1

Erieirgy Generation NA
Milli f.'aroflao
Ash Distvibudcm. plvgrafn 111form-atio'n sbct:t
SUEV f"cry; BMPOW Nc fBAhmm 2859 (Md 1 hadle Ronk Marioin' i'; the et dZL'f'�11t.iP all
Apphicmon of the
the dsh provi&d :01 1141
'd ast" is prohlbilod Opt in wordanze xxiM the ANnycQu ou this whw
AdCqLG11C jJ.-o, iSivns shall by wkcu to Qnhwv Mai W untwomwAnt 4 ash dow not cam
nuisa.m:t,s innd luvardF"' 11,11-1hc and w6m; or omcm6c cauw an amom ammo (egg vmmq-)f1'
mvi ash In
Hv-;"A-sh sbalf fie '-'ldecpiatwly swrud its pwom knind mwim, ormirfact." ruiloll, fivni
im.0 answrfi-rcl: w'aiers. Kek;pmg the az;h �hghtl� moiz:wnoj v'.01 thii "1hj'.-cHvQ widernorowt
coodiliofh' hnirrik`r,. or %iqis. rll"It
&ircjsion ov rLwor" conlrol he
APPlic'Milifif.. Wlicil k1hing irsh, (fin: "'ollowing, shall 3ppl\-
Ile ash apmicadon macs ShUH be Hmiwd to dum: Ell -at c'111 be limited ti,
thak nui:cfed io meL;i Ac HmWg mqiAmmmi 41c crup ONg gmwn on be Wird).
ti Ash hhall not be pWccd within 30 W cW m, w1w ',k,�acr-
Agh shall no he pb"d %kin oric fcoi ofifte -,!-a�:ooal higli s.tnwr la'(fl,.:.
Ash shall ma hu placud willlitl I00 Ct:.et o-am. or �.Prij)L4 umh�!is unoel'I'do and
OW-flain ba liner wall 'i ilkaxiininn hydmulic wonowt"aw of wo cmdurroem Pa"em? 1 'ill a
linewcom ig pro% W "h Oall nm he P&Wd whirk 25 best or uy wacur huppb weH or if. ing.
Fhe ash W ihq bciipplit,d to any sue that is rhmat immm ;w smww•�ovww
A vimmar� (A' flit' ash chnnihal MOUI)SUS m lcumad on pay 2 of 1hu :sheet Delai)cd
ulhonqlorrusulis are "o;0abit: UPk7D rdtjtic"l
I Aw U) wc ash Will wNwr Sam Fliopomcr w Rucipicril upon deliwv�y 84)flo%�cf
"I! Neu no rmpwQWhq and Wl no be W hahic b) Recipium "w an, Wd pany Or any soil,
lwim)sc' fnivapplicaiiOn or of ter' nlishan=j 'd Me ash Hycipicult and agsrev.i Ilia! Ow 4.1'sh
in hubg dcHtcmd by Bhh.m,cr to Rccipis:m as an
'irldcmllii�-. save. and �Icdd harride"i fi-nin and alg
�igrco.'; lo iii-o'l and -;b Pity.
amm-ne- -An cumv dmwm& hwq avibm jmwmem or mcnor.'?
agaill'st Hbpa"cr by Any Choi !wl. ASUng any gmervint.,irmf "aiato6v., 9,1iolicu- 1'(1r bcxfif\
jinn dcmha ai da"mgc to pnTarly immg Unn tw in onmWon "it Rodp1mrA rewhA
majortw4m hawflint-" 4 11. other tja� of the
I I ,
!�q;iwd
4VI
/ 1z
9. Zee Lam &
0 !,:1 b,'"tall. 1 Ke 1 4 Nh 17 A. ... �ee .
o r Lan d
Y r: 0 0 0 V-5
{Oyu 1 of
POWN 1 of

2859 Odd Linville lloa i
Marion, North Caroiina 28752
Ash Distribution Program linformation Sheet
Baxter Healthcare, Corp., is the generator of the ash provided to f NaLlaft_�
(.Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transporl: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to, public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or Tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
.Applieation: When using ash, the following shall apply:
o The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land).
e Ash shall not be placed within 50 feet of ariy surface water.
R Ash shall not be placed within one foot of the seasonal high water table.
e .Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity o€10-6 centimeters per second. 1f such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
o The ash shall not be applied to any site that is flooded, frozen; or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter ITea.lthcare, Corp to Recipient upon delivery thereof, Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indenuii€y, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter f-Iealtheare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient}: Ji M p4tu ps Date: 1__5 — l7—
Ash Recipient's Address: Qp 60� u9
_94WSOLLL9.0/)L ?OI C z -z )2
Intended Use of Ash: MOA0)L14
Expected QtyNr: 12 alb f `' t t/ �� Acres of Land:.-
Page 1 of 3
Updated: 315110

Baxter Heaftheare, Corp
2859 Old Linville Road
Mariun, North Carolina 28752
Ash }distribution Program information Sheet
Baxter Healthcare, Corp., is the generator of the ash provided to f ANV �
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that .the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
6 The ash application rates shall: be limited to those that can be agrononiicallyyustified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land).
0 Ash shall not be placed within 50 feet of any surface water.
0 Ash shall not be placed within one foot of the seasonal high water table.
a Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of .10-6 centimeters per second. 1.f such a.
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
0 The ash shall not be applied to any site that is flooded, frozen, or snow -coveted.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to recipient upon delivery thereof Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party .for any spill, misuse, misapplication or other mishandling of the ash. ,Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healtheare, Corp by any third
party, including any governmental authority, whether for bodily injury (.including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): t { 11 Date:
Ash Recipient's Address: IR D `1 ,qdt"Lwv!, Uz e /!. t` =04 d
1 lo,5­7
Intended Use of Ash: 6 0 A A-,-. rA wV "M 1
;Expected Qty/Yr: 3 cro
Page I of 3
Updated: 315110
Acres of Land: 4-6

Baxter 'Flea ftheare, Corp.
2859 Old LinvMe Road
Marlon,NNoah Carolina 28752
Asti Distribution )Prograain Information Sheen
Baxter Realthcare, Corp,, is the generator of the ash provided to I 1^ Lt�. 1,J 4 11
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to erasure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under .normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
o The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land).
Ash shall not be placed within 50 feet of any surface water.
Ash shall not be placed within one foot of the seasonal Nigh water table.
o Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a anaxcimum hydraulic conductivity of I e centimeters per second. If such a
liner/cover is, provided, ash shall not be placed within 25 feet of any water supply well or spring.
Q The ash shall not be applied to any site that is flooded, fi°ozen, or snow-covered.
A, summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
.laboratory results are available upon request.
Title to the ash will transfer from .Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter;
Baxter Healtl care, Corp will have no responsibility and shall not be field liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): C I,l" (( _Date: r-3 1
Ash Recipient's Address: t49 t S' US 2-21 No �,
intended Use of Ash:
Expected Qty/Yr: Acres of Land:
Page 2 of 3
Updated: 3/5110

Baxter Henhhealre, Corp.
2859 Old Lanvi fie Road
Marion, North Caroffina 28752
,Ash Distribution Program Information Sheet
Baxter :Healthcare, Corp., is the generator of the ash provided to PI A44 c
(Recipient). .Application of the aforementioned ash is prohibited 'except in accordance with the
instructions on this sheet.
Travisport: Adequate provisions shall be taken to ensure that the transportation of ash does not; cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof ft ucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. beeping the' ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions:or if
erosion or runoff cannot be controlled
Application. When using ash, the following shall apply:
0 The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land).
Q Ash shall not be placed within 50 feet of any surface water.
a Ash shall not be placed within one foot of the seasonal high water table.
a Ash shall not be placed within 1.00 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10 centimeters per second. LC such, a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to .recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by ]recipient or any third
party for any spill, misuse, misapplication or other mishandling ofthe ash. Recipient acknowledges; and
agrees that the ash: is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, .Recipient agrees to indemnify, save and hold Baxter .Tlealthcare,.Corp
harmless from andagainst any and all liability, damage, loss, cost, eXpense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted. against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): iW 0, + � nsp k Date: 19'3 ^ 1 1
Ash Recipient's Address; 1� 6 0 k; c])� ,g L l J
Ne-�O C Z7(01
Intended Use of Ash: L ; m r-
Expected Qty/Yr: 30 Acres of Land: +%
Page I of 3
Updated: 315110

.... ......
Eiriergy Gener"-mlt'(C.Iin fN't��
Nlarion, NoMi Carolina
As.h Dist0buflon Prog.I.am Information Si�eet
SUITY. Energy WoPovver, Ific, (MoPower). 2,959 Old Linvilfc, Road- Marioo. NC 28751"1" is the geftrator of
dv a - �fioko-vided to Al
0 (R coipirnt). Application of t44%
a'sh is prohibited ex"pl in acicordance %ith the instructionson this sheel.
't*hmsftem: Adzquate provistorts shall be taken to ensure that flee tr;uisposunrli-)u of'ash dcos nt-A
nuisaous and kizard§ to pub is health "Uld QmFety or other vise Causo an adverse impa'-A framtkirt.
1vcf: dsh in Icilt-proof truckq or cover dry asli)
The ash- shall ba'adcquately Stovcd to Pro-vinit" v6nd 'OrOS3,013. csr surfiac'e 1, . I "no T j �roxfl ca-Crying 'Ush
into at.;y stiqlavt; wzm"m. K(.'epiag tiro ash slightly frimistoned will accompli*,Ap. ffiis okiectivo midur normal
wadiliow". kowever, be-Ilms, barrieps, or tarps. 'may be nemisary under wind.v or rai-ny condftioivS or if
arosion or runof-fcannot k. contmiled.
AP'PIIC(Taotl> When U";h',g z 0
, ash'. rile fblloivim shall nppv
* The, vuh appticadon taus shod! be limited to those that can lac agronomically- usfified 6.o , knliv.-'d to
iliac aceded to at the liming. reqaaircnxcn(s of the crops being grown on the land),
v Ash shall not bo ptumed:Mfthirt 50 feat of any surface Nvater
0 Ash shall not: be pfacWmithin one foot of kho scasonal Ifigb %vater table,
A--,b slAll. not b(placed. Mthin 1.00 foot of wvy water Supply �8.011 01• spring unjcs5 anded4jil and
ov&xlain by a litter with a mimiminn hydraulic conductivity of 10" ecalimewns pur second. If such a
Unvrkowris provid4, :ab-h shall not bo placed within 25'rect of any water supply iVell or sprii-kgg.
TlIcash shall not be apglii�d to any site t1lat. Is flooded, IrOzcn' or sq.ow-�:ovrcyed.
A summaty of the. ash chcaiic4l mWyscs is Iv..,ated on 12-age 2' of ato inf6miation s1wel. Dul'aded
I��l3atQn"re ants are ,jYaija.bjQ- 11POIi r eqUest.
Thh" to UIC ash will traas&('r from BioPovvLr to Recipient upon delivery thmof. There-aflet. BAPOw"
%ill have no resporLsibility and, sluill not be held hable by Recipient or any third party for any spill,
alisuse; misappliwiJon or t:her mishandiiiig of the ash. Rixipioxa ackno-odd-Alges acid agFees that die .ash
fent as -an aeonimodation to Recipient In iaxchartge thereCorc.
is being defivorcd b% BioPp�ver to R.ccipi
Xecipictil 11grecs to indem lii` v' satire, anti hold BioPowLr hamiless From and agmiruit any and all liability,
dalp".Igu' Wmss' cos"t clatrris (incylodhtg zavuon-,icys' feosj, clais-Li, demand, stjit, action, 'udgmwitor MOV�1'11`
J
wi'krted- oLgalmst - by"my thild party, including 'my whedwr for bodil
iqJv*- (irtcffidi-og d��Ah) orldajbagc; to jm.Tcr()1, arisippi Front or in connection with. Rceirliclit"S roCCIPT,
IMIWIing, or Wier llso of ft
Data
nfcrldt4 k1se, of Ash:
Acro, of Lajvd:
Page I or 2
"tip' lted M;'XW'

Energy Generation NA,
l ariojt, North Carolina
Ash Diisti° bution Program Information mation Sheet
SUEZ Energy BioPowe*r Inc. (BioPovk-r) 2859 Old Linville Road, Marion, NC 28752 is tho. generator a
the ash provided to /LC (Recipientj. Application of the
a:torr mentioned ash is proli iliited except In accordance with the instructions on this sheet.
"1.`ransliort: Adequate provisions shall be taken to ensure that ilic transportation or ash does not cause
nuisances and hazards to publlc health and safety or otherwise cause an adverse impact (e.g., transport
wet'ash in leak -proof trucks or cover dry ash).
Storage The ash shrill be adequately stored to prevent Nvind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly nwistened will accomplish this objective under normal
conditions. However, beans, bkriCrs, or tarps. may be necessary under windy or rainy conditions or It
erosion or runoff cannot be controlled.
Aplrlfcratron. When usin.g ash, the following shall apply:
The ash application rates shall be limited to those that can be agronotnicallyjustified (i.e., limited to
that needed to rmect the liming; requirements of tile crops. being; grown on the land),
• Ash, shall not be placed within 50 .feet of any surface waiter,
• Ash shall not be placed within one foot of the seasonal high "vatcr table.
a Ash shall not be placed within 100 feet of any water supply well or spring; unless underlain and
.overlain by a liner'vifli•a ma imum hydraulic conductivity of 10*' ceot meters per second. If such a
liner/cover.is provided, ash shall not be placed within 25 feet ol'any water supply well or spring.
p The ash shall not be applied to any site that is flooded, frozen, or silow-covered.
A summitry of the ash chemical analyses is located on page 2 or tiie information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from t3ioPower to Recipient upon delivery thereof Therealler,, E�io1'ower
will Have no responsibility acid. shall not be held liable by Recipient or any third party for airy spill,
misuse, misapplication or other mishandling; of the asli. .Recipient ackn.otvledges and agrees that the as'h
is being delivered, by BioPower to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees; to indemnify, save and hold BioPower harmless frown and against any and all liability,
damage, loss, post, expo nse(includ.ing aitarneys' fees), claim, demand, suit, action, judgment or recovery
asserted against B1oPowe''r by any third. party, inchiding any governmental authority, whether for bodily
injury (including death) or daanag e to property, arising from or in connection with Recipient°s receipt,
transportation; handling, t� re. ise of the ash.
Signed (Ash Recipient):` _I ���'""r�•'� Date:
#� d'}
AAshRecspient' s Address: c�' tr,ri.e'�° �/ id
Intended Use of Ash.: ; , 1. e
Expected Qty/Yr: arJ A. res of Land: _1,,P#q t e?d � Idigo
Pate I of 2
updated: 1 t31 /0:7

Raxte a Ilea Rthen e, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
.Ash Distribution Program Nformation Sheet
Baxter Healthcare, Corp., is the generator of the ash provided to
(Recipient). Application of the aforementioned ash is prohibited exce t in a cordance with the
instructions on this sheet.
Tianspvrl: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storgge: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this, objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
© The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to
that needed to meet the Hibbing requirements of the crops being grown on the land).
o Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
a Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of .10-6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the aslh chemical analyses is located on page 2 of the 'information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter .fleal.thcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless fi•orn and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp, by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): Dater
Ash Recipient's Address: ZK�
loylla/o
Intended Use of Ash: 4'M a 4P4 /Y e f1WmP1%,11
ZIA
Expected Qty/Yr: 10 0 Acres of Land: 7
Page 1. of 3
Updated: 315110

SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
Client
Pace Analytical services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Order Number
1113186
Project Number
9297122
Issued
Monday, July 11, 2011.
Total Number of Pages
4 (excluding C.O.C. and cooler receipt form)
Approved By: Y
QA Manager
NELAC Accreditation #E87688
"Analytical Integrity" - EPA Certified • NELAP Certified
3310 Alin Street - Cuyahoga Falls, Ohio 44223 0 Phone: [phone] - Fax: 330-253-44€ 9
Web Site: www.settek-com

v3
SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
Sample Summary
Client: Pace Analytical Services, Inc.
Order Number: 1113186
Laboratory ID Client ID Matrix Sampling Date
1113186-01 9297122001 Solid 6/28/2011
"Analytical Integrity„ • EPA Certified • NELAP Certified
MO Win Street • Cuyahoga Fails, Ohio 44223 Phony:: 330-253-8211 • Fax: [phone]
Web Site: wwwsettek.com

SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
. rr Analytical Laboratories
Report Narrative
Client: Pace Analytical Services, Inc.
Order Number: 1113186
3
Solid sample results are reported on a wet weight basis except as noted.
No problems were encountered during analysis of this order number, except as noted.
Data Qualifiers:
B = Analyte found in the method blank
J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ)
C = Analyte has been confirmed by another instrument or method
E = Analyte exceeds the upper limit of the calibration curve.
D = Sample or extract was analyzed at a higher dilution
X = User defined data qualifier.
S = Surrogate out of control limits
U = Undetected
a = Not Accredited by NELAC
ND = Non Detected at LOQ
DF = Dilution Factor
Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor)
Limit Of'Detection (LOD) = Laboratory Detection Limit
Estimated uncertainty values are available upon request.
A = Air
C = Cream
DW = Drinking Water
L = Liquid
O = Oil
St. = Sludge
SO = Soil
S = Solid
T = Tablet
TC = TCLP Extract
WW = Waste Water
W =Wipe
The test results meet the requirements of the NELAC standard, except where noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot
be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this
report was issued. The results contained in this report are only representative of the samples received. Conditions
can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc, is not
responsible for use or interpretation of the data included herein.
"Analytical Integrity" • EPA Certified • NELAP Certified
3310 Wiry Street - Cuyahoga Falls, Ohio 44223 o Phone: [phone] - Fax: [phone]
Web Site: www.settek.com

SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
July 11, 2011
Client: Pace Analytical Services, Inc.
Address: 2225 Riverside Drive
Asheville, NC 28804
Received: 7/1/2011
Project #: 9297122
Client ID#
Lab M#
Collected Analyze
Result
Units
Matrix Method
DF
LOQ
Run Anal st
9297122001
1113186-01
28-Jun-11 Flash Point's
>140
OF
S 1010
1
06-Jul-11 DVW
Client ID#
Lab ID#
Collected Mal to
Result
Units
Matrix Method
DF
LOQ
Run. Analyst
9297122001
1113186-01
28-Jun-11 Reactive Cyanide ✓
ND
mg/kg
S 7.3.3.2
1
0.5
06-Jul-11 1111
Client ID#
Lab ID#
Collected Anale
Result
Units
Matrix Method
DF
LOQ
Run Analyst
9297122001
1113186-01
28 Jun-11 Reactive SuCfide
ND
mg/kg
S 7.3.4.2
1
25
06-Jul-11 TIR
Page 4
"Analytical Integrity" - EPA Certified - NELAP Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 a Phone: [phone] • Fax: [phone]
Web Site; www.settek.com

Baxter Healthcare - Wood Boiler
Please test the sample(s) for the parameters as listed below.
Send original results to: email: [e-mail]
Send invoice and copy of results to:
Ricky Styles email: [e-mail]
Baxter Healthcare Purchase Order # 25819
2859 Old Linville Rd.
Marlon, NC 28762
[phone]
email: [e-mail]
uested Due Date:
Sample # Sample Sample Dates) Grab or Total Metals -
Description and time sample Composite
TCLP Metals
As, Ba, Cd,
collected Ca, Cr, Cu, Fe,
As, Ba, Cd,
Cr, Pb, Hg,
Pb, Mg, Hg,
Se, Ag
Mn, Mo, Ni, K,
Se, Ag, Na,
Zn, total
Phosphorus
Ignitability, I pH c Full TCLP
Total-Arseni
Reactivity Corrosivity
WB1 QTR2011 BOTTOM ASH 2-4-11 8:30AM COMPOSITE YES
YES YES YES
WBPAPER PAPER
SLUDGE 2-4-118:30AM COMPOSITE YES YES
Sample sent to: Pace Analytical Services,
Project Manager: Tom Williams
2225 Riverside Drive - 9800 Kincey Avenue, Suite 10f
Asheville, NC 28804 Huntersville, NC 28078
828-254-7176 (704) 875 - 9092 ext. 233
e S n) p0 2 ®SS.1 b 0 C ; N P'L4 fi d lei eAA wa a c/T
Chain of Custody P
kOVO4? N4 i2eee:Ugd o2 IA-vd Aepf,&� — Te6 e5J-4s 0,,)y

aceAnalytical o
www.Aveh,bS.COM
February 25, 2011
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NO 28752
lililll'111'
w1
��
205 East Meadow Road - Suite A
Eden, NC 27288:
[phone]
RE: Project: WOOD BOILER 02/04
Pace Project No.: 9287180
�I
2225 Riverside Dr.
Asheville, NC 28804
[phone]
i
9800KinceyAve. Suite100
Huntersville. NC 28078
[phone]
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on February 04, 2011.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tom Williams
[e-mail]
Project Manager
Enclosures

REPORT OF LABORATORY AMALYSIS Page 1 of 15
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Analytical
wwr:Paoekbs com
Project: WOOD BOILER 02/04
Pace Project No.: 9287180
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Charlott® Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NCO12
North Carolina Drinking Water Certification * 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #. 12
Pennsylvania Certification M 68-00784
South Carolina Certification P 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Connecticut Certfication * PH-0106
Florida/NELAP Certification 0. E87648
Massachusetts. Certification #: M-NC030
New Jersey Certification #: NC011
North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
South Carolina Drinking Water Cert. #: 99006003
Virginia Certification #: 00213
Connecticut Certification #: PH-0104
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DHH Drinking Water# LA 100031
West Virginia Certification #. 357
North Carolina Wastewater Certification #. 40
Pennsylvania Certification #: 68-03578
South Carolina Bioassay Certification #: 99030002
South Carolina Certification M 99030001
Virginia Certification #. 00072
West Vrginia Certification #: 356
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
i ,N ♦CCCgC
c
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 15

aceAnal ical
www'Pa-labs.com
Project: WOOD BOILER 02/04
Pace Project No.: 9287180
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE AMALYTE COUNT
Pace Analytical Services, Inc,
9800 ftceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab 10 Sample ID
_�
Analytes
9287180001 W81QTR2001 BOTTOM ASH
Method
Analysts
Reported
Laboratory
EPA6010
JMW
17
PASI-A
EPA6010
JMW
7
PASI-A
EPA 7470
EWS
1
PASI-A
EPA 7471
EWS
1
PASI-A
ASTM 02974-87
TNM
1
PASI-C
EPA 9045
JKS
1
PASI-A
9287180002 WBPAPER PAPER SLUDGE
EPA 365.1
LEP
1
PASI-A
EPA 6010
JMW
17
PASI-A
EPA6010
JMW
7
PASI-A
EPA 7470
EWS
1
PASI-A
EPA 7471
EWS
1
PASI-A
ASTM D2974-87
TNM
1
PASI-C
EPA 365.1
LEP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 15

aceAnalytical
wwwpacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
PaceAnalytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: WOOD BOILER 02/04
Pace Project No.: 9287180
Sample: WBIQTR2001 BOTT )M Lab ID: 9287180001 Collected: 02/04/11 08:30 Received: 02/04/11 10:30 Matrix: Solid
ASH
ResufBs reportemf on a dry-wefgrht" basis
Parameters Results Units Report Limit DI= Prepared P Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
Barium
5.0 mg/kg
1240 mg/kg
0.42 1
02/15/11 15:05 02/23/11 11:33 7440-38-2
Cadmium
2.0 mg/kg
4.2 10
02115/1115:05 02/23/1118:48 7440-39-3
Calcium
49900 m k g
0.083 1
02/15/11 15:05 02/23/11 11:33 7440-43-9
Chromium
18. mg/
g
83.4 10
02/15/11 15:05 02/23/11 18:48 7440-70-2
Copper
2 mg/kg
0.42 1
0.42
02/15/11 15:05 02/23/11 11:33 7440-47-3
Iron
16700 mg/kg
1
02/15/11 15:05 02/23/11 11:33 7440-50-8
Lead
28.9 mg/kg
41.7 10
02/15/11 15:05 02/23/11 18:48 7439-89-6
Magnesium
8030 m g
0.42 1
02/15/11 15:05 02/23/11 11:33 7439-92-1
Manganese
1410 �g
8.3 1
02/15/1115:05 0212311111:33 7439-95-4
Molybdenum
1.mg/kg
4.2 10
0211511115:05 02/23/1118:48 7439-96-5
Nickel
19.9
mg/kg 9/kg
0.42 1
02/15/11 15:05 02/23/11 11:33 7439-98-7
15500 mg/kg
0.42 1
02/15/11 15:05 02/23/1111:33 7440-02-0
Selenium
ND mg/kg
4170 10
02/15/11 15:05 02/23/11 18:48 7440-09-7
Silver
0.mg/kg
0.83 1
02/15/11 15:05 02/23/11 11:33 7782-49-2
Sodium
13300 mg/kg
9 g
0.42 1
02/15/11 15:05 02/23/11 11:33 7440-22-4
Zinc
1520 mg/kg
4170 10
02115/1115:05 02/23/1118:48 7440-23-5
6010 MET ICP, TCLP
8.3 10
02/15/11 15:05 02/23/11 18:48 7440-66-6
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 02/16/11 16:00
Arsenic
Barium
0.050 mg/L
3.4 mg/L
0.025 1
02/17/11 12:15 02/22/1123:34 7440-38-2
Cadmium
ND mg/L
0.50 1
02/17/11 12:15 02/22/11 23:34 7440-39-3
Chromium
ND mg/L
0.0050 1
02117/1112:15 02/22/1123:34 7440-43-9
Lead
ND mg/L
0.025 1
02/17/11 12:15 02/22/1123:34 7440-47-3
Selenium
ND mg/L
9/
0.025 1
02/17/11 12:15 02/22/1123:34 7439-92-1
Silver
ND mg/L
0.16 1
02/17/11 12:15 02/22/1123:34 7782-49-2
7470 Mercury, TCLP
0.025 1
02/17/11 12:15 02/22/11 23:34 7440-22-4
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 02/16/11 16:00
Mercury
ND
ND u /L
9
0.20 1
02121/1116.40 02/2211111:05 7439-97-6
7471 Mercury
Method: EPA 7471 Preparation Method: EPA
7471
Mercury
ND mg/kg 9 9
0.0038 1
02118/1115:00 02/22/11 12:29 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
0.14 %
0.10 1
02/08/11 15:14
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
11.5 Std. Units V
0.10 1
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
02/15/11 15:10
Phosphorus
564 mg/kg
14.0 7
02/08/1115:57 7723-14-0
Date: 02/25/2011 04:49 PM REPORT OF LABORATORY ANALYSIS
Page 4 of 15
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytkal
Ww.pacelabs.com
Project: WOOD BOILER 02/04
Pace Project No.: 9287180
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: WBPAPER PAPER Lab ID: 9287180002 Collected: 02/04/11 08:30 Received: 02/04/11 10:30 Matrix: Solid
SLUDGE
Results reported on a "dry- wreight"basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
1.3 mg/kg
0.80
1
02/15/11 15:05
02/23/11 11:39
7440-38-2
Barium
32.5 mg/kg
0.80
1
02/15/11 15:05
02/23/11 11:39
7440-39-3
Cadmium
ND mg/kg
0.16
1
02/15/11 15:05
02/23/11 11:39'
7440-43-9
Calcium
156000 mg/kg
796
50
02/15/11 15:05
02/23/11 18:51
7440-70-2
Chromium
10.3 mg/kg
0.80
1
02/15/11 15:05
02/23/11 11:39
7440-47-3
Copper
28.4 mg/kg
0.80
1
02/15/11 15:05
02/23/11 11:39
7440-50-8
Iron
1080 mg/kg
8.0
1
02/15/11 15:05
02/23/11 11:39
7439-89-6
Lead
1.2 mg/kg
0.80
1
02/15/11 15:05
02/23/11 11:39
7439-92-1
Magnesium
2150 mg/kg
15.9
1
02/15/11 15:05
02/23/11 11:39
7439-95- 4
Manganese
43.5 mg/kg
0.80
1
02/15/11 15:05
02/23/11 11:39
7439-96-5
Molybdenum
ND mg/kg
0.80
1
02/15/11 15:05
02/23/11 11:39
7439-98-7
Nickel
ND mg/kg
0.80
1
02/15/11 15:05
02/23/11 11:39
7440-02-0
Potassium
ND mg/kg
796
1
02/15/11 15:05
02/23/11 11:39
7440-09-7
Selenium
ND mg/kg
1.6
1
02/15/11 15:05
02/23/11 11:39
7782-49-2
Silver
2.5 mg/kg
0.80
1
02/15/11 15:05
02/23/11 11:39
7440-22-4
Sodium
1230 mg/kg
796
1
02/15/11 15:05
02/23/11 11:39
7440-23-5
Zinc
120 mg/kg
1.6
1
02/15/11 15:05
02/23/11 11:39
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010
Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311;
02/16/11 16:00
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, TCLP
Mercury
7471 Mercury
Mercury
Percent Moisture
Percent Moisture
365.1 Phosphorus, Total
Phosphorus
ND mg/L
0.025
1
02/17/11 12:15
02/22/11 23:38
7440-38-2
ND mg/L
0.50
1
02/17/11 12:15
02/22/11 23:38
7440-39-3
ND mg/L
0.0050
1
02/17/11 12:15
02/22/11 23:38
7440- 43-9
ND mg/L
0.025
1
02/17/11 12:15
02/22/11 23:38
7440-47-3
ND mg/L
0.025
1
02/17/11 12:15
02/22/11 23:38
7439-92-1
ND mg/L
0.10
1
02/17/11 12:15
02/22/11 23:38
7782-49-2
ND mg/L
0.025
1
02/17/11 12:15
02/22/11 23:38
7440-22-4
Analytical Method: EPA7470 Preparation Method: EPA7470
Leachate Method/Date: EPA 1311; 02/16/11 16:00
ND ug/L 0.20 1 02/21/11 16:40 02/22/11 11:07 7439-97-6
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
Analytical Method: ASTM D2974-87
53.2 %
Analytical Method: EPA 365.1
350 mg/kg
0.0094 1 02/18/1115:00 02/22/1112:40 7439-97-6
0.10 1 02/08/11 15:14
21.3 5 02108/1114:50 7723-14-0
Date: 02/25/2011 04:49 PM REPORT OF LABORATORY ANALYSIS Page 5 of 15
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

��aucmnalj&cal
www.pacelabscom
Project: WOOD BOILER 02/04
Pace Project No.: 9287180
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QC Batch: MPRP/7868
QC Batch Method: EPA 3050
Associated Lab Samples: 9287180001, 9287180002
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 6010
Analysis Description: 6010 MET
METHOD BLANK: 562901
Associated Lab Samples:
Parameter
9287180001, 9287180002
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed
Arsenic
mg/kg
ND
0.50
02/23/1109:14
Barium
mg/kg
ND
0.50
02/23/1109:14
Cadmium
mg/kg
ND
0.10
02/2311109:14
Calcium
mg/kg
ND
10.0
02/23/1109:14
Chromium
mg/kg
ND
0.50
02/23/1109:14
Copper
mg/kg
ND
0.50
02/2311109:14
Iron
mg/kg
ND
5.0
02/23/1109:14
Lead
mg/kg
ND
0.50
02/2311109:14
Magnesium
mg/kg
ND
10.0
0212311109:14
Manganese
mg/kg
ND
0.50
02/23/1109:14
Molybdenum
mg/kg
ND
0.50
02123/1109:14
Nickel
mg/kg
ND
0.50
02/23/1109:14
Potassium
mg/kg
ND'
500
02/23/1109:14
Selenium
mg/kg
ND
1.0
02/23/1109:14
Silver
mg/kg
ND
0.50
02123/1109:14
Sodium
mg/kg
ND
500
02/23/1109:14
Zinc
mg/kg
ND
1.0
02123/1109:14
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
562902
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Arsenic
mg/kg
50
47.6
95
80-120
Barium
mg/kg
50
49.9
100
80-120
Cadmium
mg/kg
50
47.1
94
80-120
Calcium
mg/kg
500
467
93
80-120
Chromium
mg/kg
50
46.0
92
80-120
Copper
mg/kg
50
49.7
99
80-120
Iron
mg/kg
500
495
99
80-120
Lead
mg/kg
50
48.7
97
80-120
Magnesium
mg/kg
500
507
101
80-120
Manganese
mg/kg
50
47.3
95
80-120
Molybdenum
mg/kg
50
48.1
96
80-120
Nickel
mg/kg
50
47.9
96
80-120
Potassium
mg/kg
500
492J
98
80-120
Selenium
mg/kg
50
48.6
97
80-120
Silver
mg/kg
25
23.9
96
80-120
Sodium
mg/kg
500
502
100
80-120
Zinc
mg/kg
50
46.3
93
80-120
Date: 02/25/2011 04:49 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 6 of 15

aceAnalytical
www.pacelabs.com
Project: WOOD BOILER 02/04
Pace Project No.: 9287180
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
(.QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800IQnceyAve. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
567884
Units
9287165002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
ND
61.2
52.4
86
75-125
Barium
mg/kg
14.0
61.2
72.8
96
75-125
Cadmium
mg/kg
2.7
61.2
58.5
91
75-125
Calcium
mg/kg
729
612
1280
89
75-125
Chromium
mg/kg
35.9
61.2
104
111
75-125
Copper
mg/kg
24.6
61.2
96.3
117
75-125
Iron
mg/kg
27800
612
33100
861
75-125 MO
Lead
mg/kg
5.1
61.2
57.8
86
75-125
Magnesium
mg/kg
111
612
719
99
75-125
Manganese
mg/kg
87.4
61.2
151
104
75-125
Molybdenum
mg/kg
ND
61.2
52.3
85
75-125
Nickel
mg/kg
2.0
61.2
59.4
94
75-125
Potassium
mg/kg
271J
612
1060
129
75-125 MO
Selenium
mg/kg
0.67J
61.2
49.0
79
75-125
Silver
mg/kg
0.064J
30.6
31.6
103
75-125
Sodium
mg/kg
47AJ
612
791
121
75-125
Zinc
mg/kg
12.2
61.2
73.6
100
75-125
SAMPLE DUPLICATE: 562904
9287165001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Arsenic
mg/kg
0.67
ND
Barium
mg/kg
17.5
16.4
6
Cadmium
mg/kg
1.5
3.3
75 R1
Calcium
mg/kg
923
842
9
Chromium
mg/kg
39.6
50.9
25 R1
Copper
mg/kg
25.5
29.0
13
Iron
mg/kg
31900
35300
10
Lead
mg/kg
4.9
6.0
21 R1
Magnesium
mg/kg
165
161
2
Manganese
mg/kg
25.4
29.8
16
Molybdenum
mg/kg
0.64
.2J
Nickel
mg/kg
2.2
2.0
12
Potassium
mg/kg
423J
413J
Selenium
mg/kg
1.6
.46J
Silver
mg/kg
0.0511
.063J
Sodium
mg/kg
1051
95.11
Zinc
mg/kg
10.6
27.6
89 R1
Date: 02/25/2011 04:49 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 15

aceArralydical
%ww.pacelabscom
Project: WOOD -BOILER 02/04
Pace Project No. 9287180
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services; Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MPRP/7896
Analysis Method: EPA 6010
QC Batch Method: EPA 3010
Analysis Description: 6010 MET TCLP
Associated Lab Samples: 9287180001, 9287180002
METHOD BLANK: 565756
Matrix: Water
Associated Lab Samples: 9287180001, 9287180002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Arsenic
mg/L
ND 0.025
02122/1122:52
-Barium
mg/L
ND 0.50
02/22/1122:62
Cadmium
mg/L
ND 0.0050
02/2211122:52,
Chromium
mg/L
ND 0.025
02/22/1122:52
Lead
mg/L
ND 0.025
02/22/1122:52
Selenium
mg/L
ND 0.10
02122/1122:52
Silver
mg/L
ND 0.025
02JWll22:52
LABORATORY CONTROL SAMPLE:
565757
Spike LCS
LCS %
Rec
Parameter
Units
Conc. Result
% Rec Limits
Qualifiers
Arsenic
mg/L
2.5 2.8
110
80-120
Barium
mg/L
2.5 2.5
100
80-120
Cadmium
mg/L
2.5 2.4
96
80-120
Chromium
mg/L
2.5 2.3
92
80-120
Lead
mg/L
2.5 2.3
93
80-120
Selenium
mg/L
2.5 3.0
119
80-120
Silver
mg/L
1.2 1.3
107
80-120
MATRIX SPIKE SAMPLE:
565759
9287266003 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/L
ND 2.5
2.3
93
75-125
Barium
mg/L
0.84 2.5
2.7
74
75-125 MO
Cadmium
mg/L
0.028 2.5
2.0
80
75-125
Chromium
mg/L
ND 2.5
1.9
78
75-125
Lead
mg/L
ND 2.5
2.0
79
75-125
Selenium
mg/L
ND 2.5
2.5
98
75-125
Silver
mg/L
ND 1.2
1.1
90
75-125
SAMPLE DUPLICATE: 565758
9286984001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Arsenic
mg/L
ND ND
Barium
mg/L
ND .082J
Cadmium
mg/L
ND_ ND
Chromium
mg/L
0.090 ND
Lead
mg/L
ND ND
Date: 02/25/2011 04:49 PM
REPORT OF LABORATORY ANALYSIS
Page 8 of 15
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
io i

Selenium
Silver
aceAnalyiical
wwwpacelabs.com
Project: WOOD BOILER 02/04
Pace Project No.: 9287180
SAMPLE DUPLICATE: 565758
Parameter Units
mg/L
mg/L
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Date: 02/25/2011 04:49 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
9286984001 Dup
Result Result RPD Qualifiers
ND .021J
ND .0017J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc__
A
V i
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersvilfe, NC 28078
[phone]
Page 9 of 15

aceAnalidical
wmpacew corrr
Project: WOOD BOILER 02104
Pace Project No.: 9287180
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP13305 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 9287180001, 9287180002
METHOD BLANK: 567384 Matrix: Water
Associated Lab Samples: 9287180001, 9287180002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 0212211110:28
Pace Analytical Services, Inc.
9800lonceyAve. Suite100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
567385
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Mercury
ug/L
2.5 2.6
103
80-120
MATRIX SPIKE SAMPLE:
567498
9287256003 Spike
MS
MS
%Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Mercury
ug/L
ND 2.5
1.9
75 75-125
SAMPLE DUPLICATE: 567387
9286933001 Dup
Parameter Units Result Result RPD Qualifiers
Mercury ug/L ND ND
Date: 02/25/2011 04:49 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Coy
Page 10 of 15

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Eden. NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: WOOD BOILER 02104
Pace. Project No.: 9287180
QC Batch: MERP/3302 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 . Analysis Description: 7471 Mercury
Associated Lab Samples: 9287180001, 9287180002
METHOD BLANK: 563997 Matrix: Solid
Associated Lab Samples: 9287180001, 9287180002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0050 02/22/1111:34
LABORATORY CONTROL SAMPLE: 563998
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg .067 0.060 90 80-120
MATRIX SPIKE SAMPLE: 563999
9287165001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.035 .078 0.090 71 75-125 MO
MATRIX SPIKE SAMPLE:
564001
9287165003
Spike
MS
MS % Rec
Parameter
Units
Result
Conc.
Result
'/o Rec Limits Qualifiers
Mercury
mg/kg
0.080
.054
0.17
168 75-125 MO
SAMPLE DUPLICATE: 564000
9287165002
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Mercury
mg/kg
0.033
0.034
3
SAMPLE DUPLICATE: 564002
9287165008
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Mercury
mg/kg
0.022
0.019
12
Date: 02/25/2011 04:49 PM
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
4
Page 11 of 15

acaAnalykal
wwwpacelabs.=
Project: WOOD BOILER 02104
Pace Project No.: 9287180
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road -Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
QC Batch: PMST/3725 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9287180001, 9287180002
SAMPLE DUPLICATE: 560882
Parameter
Percent Moisture
SAMPLE DUPLICATE: 560883
Parameter
Percent Moisture
Date: 02/25/2011 04:49 PM
9287228001 Dup
Units Result Result
% 20.1 22.4
9287198011 Dup
Units Result Result
% 14.7 15.2
RPD Qualifiers
11
RPD Qualifiers
4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
���p\��
7�_.�3TlF.L.;r
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 15

aceAnaly ical
v1 w.paceWs.c=
Project: WOOD BOILER 02/04
Pace Project No.: 9287180
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WET/15376 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 9287180001
SAMPLE DUPLICATE: 564400
Parameter
pH at 25 Degrees C
9287180001 Dup
Units Result Result RPD Qualifiers
Std. Units 11.5 11.6 1
Date: 02/25/2011 04:49 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 15

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
,�acemalxical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 IGncey Ave. Suite 100
wmpacela6scom Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: WOOD BOILER 02/04
Pace Project No.: 9287180
QC Batch: WETAI9075
Analysis Method:
EPA 365.1
QC Batch Method: EPA 365.1
Analysis Description:
365.1 Phosphorus, Total
Associated Lab Samples: 9287180001, 9287180002
METHOD BLANK: 560945
Matrix: Solid
Associated Lab Samples: 9287180001, 9287180002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Phosphorus
mg/kg
ND 2.0
02/0811114:11
LABORATORY CONTROL SAMPLE:
560946
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Phosphorus
mg/kg
50 51.9
104
90-110
MATRIX SPIKE SAMPLE:
560947
9287133001 Spike
MS
MS % Rec
Parameter
Units
Result Cone.
Result
% Rec Limits Qualifiers
Phosphorus
mg/kg
22.0 77.8
98.3
98 90-110
SAMPLE DUPLICATE: 560949
9286999001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Phosphorus
mg/kg
142 171 18
Date: 02/25/2011 04:49 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services; Inc..
Page 14 of 15

acaArralytical
ww-pacelabscnm
Project: WOOD BOILER 02/04
Pace Project No.: 9287180
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden. NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 MnceyAve. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean* -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
R1 RPD value was outside control limits.
[phone]
Date: 02/25/2011 04:49 PM REPORT OF LABORATORY ANALYSIS Page 15 of 15
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Date: — a - q .-!
Analyst: k— C,
Facility: LYI,+A, Ow
Calibration
Calibration Cal Buffer Cal Buffer Check
Time 4.0 10.0 Buffer 7.0"
Comments
* pH buffer checks are to be within t 0.1 pH units I the standard's true value
PH Analyses
I-- - -LCIIJ CIRU b true value.

Baxter Healthcare - Wood Boiler
Please test the sample(s) for the parameters as listed below.
Send original results to: email: [e-mail]
Send invoice and copy of results to: email: [e-mail]
Ricky Styles
Baxter Healthcare
2859 Old Linville Rd.
Marion, NC 28752
[phone]
email: [e-mail]
Requested Due Date:
Purchase Order # 26560
Sample #
Sample
Description
Sample Date(s)
and time sample
collected
Grab or
Composite
Total Metals -
As, Ba, Cd,
Ca, Cr, Cu, Fe,
TCLP Metals
As, Ba, Cd,
Cr, Pb, Hg,
Ignitability,
Reactivity
pH
Corrosivity
Total -Arsenic
Full TCLP
Pb, Mg, Hg,
Se, Ag
Mn, Mo, NI, K,
Se, Ag, Na,
Zn, total
Phosphorus
WBSPS1-22511
SOUTH POND
3-3-11 11:30AM
COMPOSITE
YES
YES
YES
WBSPS2-22511
SOUTH POND
3-3-11 11:30AM
COMPOSITE
YES
YES
YES
Sample sent to: Pace Analytical. Services,
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Chain of Custody
Project Manager: Tom Williams
9800 Kincey Avenue, Suite 10(
Huntersville, NC 28078
(704) 875 - 9092 ext. 233

aceAialyfical
www.pacelabs.com
March 23, 2011
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
Pace Analytical Services, Inc.
205 Fast Meadow Road - Suite A
Eden, NC 27288
[phone]
RE: Project: WOOD BOILER 03/03
Pace Project No.: 9289100
Dear Mr. Styles:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC28804
[phone]
Pace Analytical Service;;, Inc.
98M Nncey Ave. Suite 100
Huntersville, NC 28078
Enclosed are the analytical results for sample(s) received by the laboratory on March 03, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise na
report. rrated in the body of the
'
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
/"2Z�
Tom Wiliams
[e-mail]
Project Manager
Enclosures
REPORT OF LAEORATORYANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analyfical Services, Inc..
. 4E� g",c s
[phone]
Page 1 of 15

aceMalximl
wwwpacelabs.com
Project WOOD BOILER 03103
Pace Project No.: 9289100
PaceAralytical Services, Inc.
205 East Meadow Road - SuiteA
Eden, NC 27288
[phone]
Charlotte Certification IDs
98W KinceyAve. Ste 100, Huntersville, NC28078
Louisiana/LELAP Certification #: 04034
New Jersey Certification P NCO12
North Carolina Drinking Water Certification P 37706
North Carolina Feld Services Certification * 5342
North Carolina Wastewater Certification * 12
Pennsylvania Certification #: 68-00784
South Carolina Certification * 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Connecticut Certification # PH-0106
Florida/NELAP Certification #. E87648
Massachusetts Certification #. M-NCO30
New Jersey Certification * NC011
North Carolina Bioassay Certification * 9
North Carolina Drinking Water Certification 1k 37712
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
South Carolina Drinking Water Cert. #. 99006003
Virginia Certification #. 00213
Connecticut Certification It PH-0104
Florida/NELAP Certification 1P E87627
Kentucky LIST Certification * 84
Louisiana DHH Drinking Water # LA 100031
West Virginia Certification * 357
North Carolina Wastewater Certification * 40
Pennsylvania Certification #. 684W78
South Carolina Bioassay Certification * 9SD30002
South Carolina Certification * 99030001
Virginia Certification 1P 00072
West Virginia Certification * 356
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
.«o"
:C�Elf�.=
Pace Analytical Services, Inc.
98M KnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 15

1
aceArralytical
wuvw.pacelabscam
I
Project: { WOOD BOILER 03/03
Pace Project No.: 9289100
PaceAreDlytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COURT
Pace Analytical Services, Inc.
9800 MnceyAve: Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sarr & ID
Method
Analysft
AnaWas
Repotted
Laboratory
928910MI
MSPS1-22511 SOUTH POND
EPA6010
MIN
17
PASI-A
EPA6010
SHB
7
PASI-A
EPA 7470
EWS
1
PASI,A
EPA7471
EWS
1
PASI-A
ASTIVID2974-87
TNM
1
PASI-C
EPA 9045
SDH
1
PASI-A
928910=2 to MPS2-22S11 SOUTH POND
EPA365.1
EPA6010
LEP
JmW
1
17
PASI-A
PASI-A
EPA6010
SHB
7
PASI-4
EPA7470
EV S
1
PASI-A
EPA7471
EVUS
1
PASI-A
ASTM D2974-87
TNM
1
PASI-C
EPA9045
SDH
1
PASI-A
EPA 365.1
LEP
1
PASI-A
REPORT OF LABORATORYANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
4 N
Page 3 of 15

i
aceAnayical
wins pacelabs com
i
Project:
Pace Pn
Sample:
WOOD BOILER 03/03
NO.: 9289100
Q^r
Pace Analytical services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
• • • r.au ,v. a60ylUUuuJ
Results *Orfed on a 3r-"ght-basis
Parameters
6010 MET ICP
Arsenic
Barium {
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Zinc
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mer+cu
ry, TCLP
Mercury
7471 Mercury
I,
Mercury
Pericent Moisture
Percent Moisture'!
I
9045 PH Soil
PH at 25 DegreesiC
365.1 Phosphorus, Total
i
Phosphorus !
Date: 03f23)2011 OT49 AM
i
I
1
Pace. Analytical Services, Inc.
9800 KnoeyAve. Suite too
Huntersville, NC 28078
[phone]
Collected: 03/03/11 11:30 Received: 03/03/11 13:34 Matrix. Solid
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 6010 Preparation Method: EPA3050
11.3 mg/kg
1130 mg/kg
1.0 1
03/13/11 12:54 03/14/11 17.47 7440-38-2
1.9 mg/k9
1.0 1
0.21 1
03/13/11 12:54 03114/11 17:47 7440.39-3
6466000
1050 50
03/13/11 12:54 03/14/11 17:47 7440-43-9
�9
1.0 1
03/13/11 12:54 03/15/11 16:36 7440-70-2
73.4 mg/kg
1.0
03/13/1112:54 03/14/1117:47 7440-47-3
7040 mgk9
1
03/13/11 12:54 03/14/11 1 T47 7440-50.8
22 0 kg
10.5 1
03/13/11 12:54 03/14/11 17.47 7439-89-6
11600 mg/kg
1.0 1
03/13/11 12:54 03/14/11 17,47 7439-92-1
26N800
20.9 1
03/13111 12:54 03/14/11 17.47 7439-95-4
�
52.3 50
03/13/11 12:54 03(15/11 1636 7439-96-5
12.7
1.0 1
0311311112:54 03/14/1117:47 7439-98-7
,mg/kg
14200 mg/kg
1.0 1
1050
03M3/11 12:54 03/14/11 17:47 7440-02-0
ND mgtkg
1
03/13/11 12:54 03/14/11 17.47 7440-09-7
ND mg/kg
2.1 1,
1.0
03113(1112.54 03/14/1, 17.47 7782•49-2
9490 mg/kg
1
1050
03/13/11 12:54 03/14/11 17:47 7440-22-4
499 mg/kg
1
03/13/11 12:54 03/14/11 17,47 7440-23-5
2.1 1
03/13/11 12:54. 03/14/11 17.47 7440-66-6
Analytical Method: EPA 6010
Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 03/07/11 16:45
0.052 mg/L
4,mg/L
0.025 1
03/08111.15:50 03/09/11 13:03 7440 38 2
0.016 mg/L
0.50 1
0.0050
03/08/11 15:50 03/09/11 13:03 7440-39-3
ND mg/L
1
0.025 1
03"111 15.50 03/09/11 13:03 7440-43-9
ND mg/L
0.025 1
03/08/11 15:50 03/09/11 13:03 7440-47--3
ND mg/L
0.10 1
03(08/11 15:50 03/09/11 13:03 7439-92-1
ND mg/L
0.025 1
03/08/11 15:50 03109111 13:03 7782-49-2
03✓08/11 15.50 03/09/11 13:03 7440-22-4
Analytical Method: EPA 7470 Preparation
Method: EPA
7470
Leachate Method/Date: EPA1311; 03107/11 16.45
ND ug/L
0.20 1
03/08/11 15:30 03/09/11 12:22 7439-97-6
Analytical Method: EPA7471 Preparation
Method: EPA7471
ND mg/kg 0.0095 1 03/11/11 09:45 03/15/11 14:24 7439-97-0
Analytical Method: ASTM 02974-87
54,9 % 0.10 1 03/07/11 13:22
Analytical Method: EPA 9045
9.3 Std. Units 0.10 1 03(18/11 16:07
Analytical Method: EPA 365.1
2950 nxj/k9 88.7 20 03109/1123:42 7723-14-0
REPORT OF LASORATORYANALYSIS Page 4 of 15
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
11; 1 C
�¢�JI-J�z

i
aceAnaljdical
-1 www.pacela6scom
Project:
Pace Pn
Sample:
WOOD BOILER 03/03
NO.: 9289100
eft I+E6,rfed on a " jghg° bwl.,
6010 IWET
Arsenic
Barium
Cadmium 1 Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
I
Silver
Sodium
Zinc
6010 MET ICP, TCLp
I
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, *LP
Mercury
7471 Mercury
Mercury
Percent Moisture
I
Percent Moisture
9045 pH Soil
pH at 25 DegreesC
365.1 Phosphorus, Tofai
Phosphorus
Date. 03/23/2011 &.49AM
Pace Analytical Services, Inc.
205 East Meadow Road - SuiteA
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 IGnoeyAve. Suite 100
Huntersville, NC 28078
[phone]
[:ollected: 03/03/11 11:30 Received: 03/03/11 13:34 Matrix: Solid
Results Units Report Limit DF Prepared Analyzed yz CAS No. Qual
Analytical Method: EPA 6010 Preparation Method: EPA3050
8.9 mg/kg
1040 ff Kykg
1.1 1
03/13/11 12:54 03/14/11 18:02 7440-38-2
1.8 mg/kg
1.1 1
03/13/11 12.54 03/14/11 18.02 7440-39-3
57400 mg/kg
0.22 1
03/13/11 12:54 03/14/11 18:02 7440-43-9
17.1 mg/kg
441 20
03/13/11 12:54 03/15/11 16.43 7440-70-2 ---
60.2 mgtk9
1.1 1
1.1
03113/11 12:54 03/14/11 18:02 7440-47-3
6160 mg/kg.
1
03/13/11 12:54 03114/11 18:02 7440-50-8
20.7 mg/kg
11.0 1
03/13/11 12:54 03/14/11 18:02 7439-89-6
10800 mg/kg
1.1 1
03/13/11 12:54 03/14/11 18:02 7439-92-1
2000 mg/kg
22.0 1
03/13/11 12:54 03114/11 18:02 7439-95-4
ND mg/kg
1.1 1
03113/11 12:54 03/14/11 18:02 7439-965
11A mg/kg
1.1 1
03/13/11 12:54 03/14/11 18:02 7439-98-7
11600 mg/kg
1.1 1
03/13111 12:54 03J14/11 18:02 7440-02-0
ND mg/kg
1100 1
03/13/11 12:54 03/14/11 18:02 7440-09-7
ND mg/kg
2.2 1
03/13/11 12:54 03/14/1118:02 7782-49-2.
8200 mg/kg
1.1 1
03/13/11 12:54 03/14/11 18:02 7440-22-4
181 mg/kg
1100 1
03/13/11 12:54 03/14/11 18:02 7440-23-5
2.2 1
03(13/11 12:54 03114/11 18:02 7440-66-6
Analytical Method: EPA6010 Preparation Method: EPA3010
Leachate Method/Date: EPA 1311; 03/07/11 16*45
0.035 mg/L
3.3 mg/L
0.025 1
03/08/11 15:50 03/09/11 13:08 7440-3&2
ND mg/L
0.50 1
03/08/11 15:50 03109/11 13:08 7440-39-3
ND mg/L
0.0050 1
03108✓11 15.50 03/09/11 13:08 7440-43-9
ND mg/L
0.025 1
03/08/11 15:50 03/09/11 13:08 7440-47-3
ND mg/L
0.025 1
03/08/11 15:50 03✓09/11 13:08 7439-92-1
ND mg/L
0.10 1
03/08/11 15.50 03/09/11 13:08 7782-49-2
0.025 1
03/08/11 15:50 03/09/11 13:08 7440-22-4
Analytical Method: EPA7470 Preparation Method: EPA7470
Leachate Method/Date: EPA 1311; 03/07/11 16.45
ND ug/L
0.20 1
03(08/11 15:30 03/09/11 12:25 7439-97-6
Analytical Method: 'EPA 7471 Preparation Method: EPA7471
0.0091 mg/kg
0.0060 1
03/11/11 09:45 03/15/11 14:27 7439-97-6
Analytical Method: ASTM D2974-87
53.7 %
0.10 1
03/07/11 13:22
Analytical Method: EPA 9045
9.2 Sid. Units
0.10 1
03/18✓11 16:07
Analytical Method: EPA 365.1
2640 mg/kg
86.4 20
03/09/11 23:47 7723-14-0
REPORT OF LABORATORYANALYSIS Page 5 of 15
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
9p7

I
i
aceAnalical
jwwwpacelabs com
a
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dc
Eden, NC 27288 Asheville, NC 28804
Project. it WOOD BOILER 03/03
Pace Project No.: 9289100
QC Batch: ' MPRP/8003
QC Batch Method: EPA3050
Associated Lab Samples: 9289100001, 9289,00002
I
METHOD BLANK, 576904
Associated Lib Samples:
i
Arsenic
Barium
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Zinc
LABORATORY
92891001Z01,9289100002
[phone] [phone]
QUALITY CONTROL DATA
Analysis Method: EPA6010
Analysis Description: 6010 MET
Solid
Blank
Reporting
Units
Result
Limit
Analyzed Qualifiers
m94C9
ND
0.50
03/14/111T29
mg/kg
ND
0.50
03/1411117.29
mg/kg
ND
0.10
03/14/1117:29
mg/kg
ND
10.0
0311411117.29
mg/kg
ND
0.50
03/1411117:29
mg/kg
ND
0.50
03114/1117:29
mg/kg
ND
5.0
03(14/11.1T29
mg/kg
ND
0.50
03✓1411117.29
mg/kg
ND
10.0
03114/111729
mg/kg
ND
0.50
03(14(1117:29
mg/kg
ND
0.50
03114(1117:29
mg/kg
ND
0.50
03/14/1117.29
mg/kg
ND
500
03/1411117:29
mg/kg
ND
1.0
03(14/11IT29
mg/kg
ND
0.50
03/14/1117:29
m9fg
ND
500
03/14/1117.29
mg/kg
ND
1.0
03114/111729
PaceAra"cal Services, Inc.
9800 WnceyAve. Suite 100
Huntersville, NC 28078
Parameter
Spike LCS LCS
% Rec
Units Conc. Result % Rec
Limits Qualifiers
Arsenic
Barium
mg/kg
50 49.3 99
80-120
Cadmium
mg/kg
mg/kg
50 49.1 98
80-120
Calcium
mg/kg
50 50.7 101
500
80-120
Chromium
mg/kg
533 107
80-120
Per
m9/k9
50 50.1Cop100
80120
Iron
mglkg
50 51.6 103
Boo
80-120
Lead
nvftg
501 100
50
80-120
Magnesium
mg/kg
50•5 101
500
80-120
Manganese
mg/kg
512 102
50
80-120
Molybdenum
mg/kg
49.4 99
50
80-120
Nickel
mg/kg
51.4 103
50 50.6
80-120
Potassium
mg/kg
101
500 481J 96
80-120
Selenium
Silver
mg/kg
50 49.9 100
80120I
80-120
Sodium
mg/kg
25 25.1 100
80120
Zinc
mg/kg
500 489J 98
80-120
mg/kg
50 51.1 102
80-120
Date: 03/23/2011 07:49AM
REPORT OF LMORATORYANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PaceAnalytical Services, Inc..
/1?1ti .'♦C2,&
�LJI-J��x
[phone]
Page 6 of 15

I
® PaceAnalyticel Services, Inca Pace Analytical Services, Inc. PaceAna
acomal, yfieal 205 East Meadow Road - Suite A h ey Services, Inc.
2225 Riverside Dr. 9800 IGrtceygve Suite 100
www.paaelabs.com Eden, NC 27288 Asheville, NC 28804
(936)62$ 8921 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project I
WOOD BOILER 03103
Pace Project
No.: 9289100
MATRIX SPIKE
SAMPLE:
576906
Parameter
Units
9289161004
Spike
MS
MS
% Rec
Arsenic
I
Result
Cons:
Result
Rec
Li_
Limits Qualifiers
Barium
mgtkg
mg/kg
1780
348
168
2010
132
75-125j1
Cadmium
mg/kg kg
9.0
168
513
98
75-125
Calcium
kg
195000
180
144.7
153
85
75-125
Chromium
m
�k
168
168
187000
-551 .
75-125 MO
mg/kg
58.6
168
191
87
75-125
Iron
Lead
23300
1680
217
25700
94
144
75-125
Magnesium
m9�9
m9nC9
5.2
168
143
82
75-125 M0
75-125
Manganese
Molybdenum
mg ft
8730
102
1680
168
10500
246
107
75-125
Nickel
�
mg/kg�
1
168
188
85
91
75-125
Potassium
mgtkg
mg/kg
16.8.
168
157
83
75-125
75-125
Selenium
I
mg/kg
ND
19.6
1680
3460
177
75-125
Silver
mg/kg
ND
168
191
102
75-125
Sodium
m9k9
19700
84.1
1680
83.6
98
75-125
Zinc
m9k9
51.9
168
20600
54
75-125 MO
216
98
75-125
SAMPLE DUPLICATE: 576974
Arsenic
Barium
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Zinc
Date: 0=3=11 07.49AM
i
9289100001
Dup
- Units
Result
Result
RPD Qualifiers
mg/kg
11.3
14.7
26 R1
m9tk9
1130
1210
7
mg/kg
1.9
2.1
7
m9*9
64600
73200
12
mg/kg
22.0
20.5
7
mg/kg
73.4
75.6
3
mg/kg
7040
8500
19
mgtk9
22.0
22.5
3
mg/kg
11600
12100
5
mg&9
2680
2950
10
mg/kg
ND
ND
mg/kg
12.7
13.1
4
m9&9
14200
16800
17
mg/kg
ND
1.3J
mg1k9
ND
.61J
mg/kg
9490
10900
13
mg/kg
499
208
82 RI
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical, services, Inc..
Page 7 of 15

I
aceAnal ical
ww'wPacelabs am
I
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: WOOD BOILER 03103
Pace Project{ No.: 9289100
QC Batch: MPRP/7982
QC Batch Method: EPA3010
Associated Lib Samples: ' 9289100001, 9289100002
METHOD BEANIE• 57 $744
Associated Lab Samples. 9289100M1. , 9289100002
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
CONTROL SAMPLE.
Pace Analytical Services; Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY COMMOL DATA
Analysis Method: EPA 6010
Analysis Description: 6010 MET TCLP
Matrbc Water
Blank
Reporting
Units
Result
Limit
Analyzed Qualifiers
mg/L
ND
0.025
03/09/1112:17
mgtL
ND
0.50
03/09/1112:17
M91L
ND
0.0050
0309/1112:17
mg/L
ND
0.025
03/09/1112:17
mg/L
ND
0.025
03109/1112:17'
mg/L
ND
0.10
03(09/1112:17
mg/L
ND
0.025
03/09/1112:17
Pace Analytical Services, Inc.
98001CrnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Parameter
I ,
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Arsenic
Limits Qualifiers
Barium
mg/L
mg/L
2.5
2.7
108
80-120
Cadmium
�L
2.5
2.5
99
80-120
Chromium
2.5
2.4
98
80-120
Lead
�L
2.5
2.5
99
80-120
Selenium
2.5
2.3
91
80-120
Silver
i
�L
1.2
2.8
112
80-120
1.3
106
80-120
MATRIX SPIKE
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
SAMPLE
cvw�w�
574746
9288906W2
Spike
MS
MS
% Rec
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
mg/L
mg/L
ND
2.5
2.2
89
75-125
mg/L
0.55
ND
2.5
2.5
79
75-125
mg/L
ND
2.5
2.5
2.0
82
75-125
mg/L
ND
2.5
2.1
83
75-125
mg/L
ND
2.5
1.9
2.3
75
75-125
mg/L
ND
1.2
1.0
90
75-125
84
75-125
Parameter
9289124001
Dup
Units
Result
Result RPD Qualifiers
Arsenic
mg/L
ND
ND
Barium
mg/L
ND
Cadmium
mg/L
ND
.14J
ND
Chromium
mg/L
L
ND
ND
mg/L
ND
ND
Date: 03/23/2011 o7:49AM REPORT OF LABORATORYANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
:Q�lii11�.1
Page 8 of 15

OW
acoAnalftical
wwwPacelabs.com
Project WOOD BOILER 03103
Pace Project No.: 9289100
SAMPLE DUPLICATE: 574747
Pace Analytical Services, Inc.
205 East Meadow Road _ Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUAUTY MMM(X DATA
9289124001 Dup
Parameter Units Result Result RPD QualifiersSelenium mg/L ND
Silver �L ND ND
.00087J
Date: 03J23/2011 07:49 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
ACCSgo'
Pace Analytical Services, Inc.
98001GnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 15

t
,ace Affllj&al
WWW-pacelabsxam
Pace Analytical Services, Inc.
205 East Meadow Road - SuiteA
Eden, NC 27288
[phone]
I —
Project WOOD BOILER 03103
Pace Project INo.: 9289100
QC Batch: I MERP/3333
QC Batch Method: EPA7470
Associated Lab Samples: 92891000()1, 9289100002
METHOD BLANK: 574737 Matrix 1/1/ater
Associated Lab Samples: 9289100001, 928910=2
PBlank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 03/09/1111:50
LABORATORY CONTROL SAMPLE: 574738
1 Spike LCS LCS % Rec
Parameter Units Cona Result % Rec Limits
Qualifiers
Mercury ug/L 2.5 2.9 117 80-120
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 IGnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Q JALITY CONTROL DATA
Analysis Method: EPA7470
Analysis Description: 7470 Mercury TCLP
MATRIX SPIKE SAMPLE: 574739
9288906W2 Spike MS MS % Rec
Parameter Units Result Cona Result % Rec Limits Qualifiers
Mercury ug/L ND 2.5 3.0 118 75-125
SAMPLE DUPLICATE. 574740
9289042001 Dup
Parameter Units Result Result RPD
Qualifiers
Mercury ug/L ND ND
I
1
f
Date. 03/23/2011 07:49 AM REPORT OF LABORATORY ANALYSIS Page 10 of 15
J This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
l _�� N ANC\�CCpgC'
s�Ll�z

ace ® Pace Analytical Services, Inc.
l-U/QI iLial 205 East Meadow Road - Suite A
Pace AnalyUcalservices, Inc.
Pace Analytical Services, Inc.
wpacera6scom
Eden, NC 27288
2225 Piverside Dr.ww98g0
IGnoeyAve. Suite 100
Asheville, NC 28804
Huntersville, NC 28078
I
[phone]
(828)254-76
71
[phone]
QUALM COMOL
DATA
Project: WOOD BOILER 03/03
Pace Project No.: 9289100
QC Batch: MERP/3341
Analysis Method:
EPA 7471
QC Batch Method: EPA 7471
Associated Lab Samples: 9289100001, 9289,00002
Analysis Description:
7471 Mercury
METHOD BLANK 576242
Matrix. Solid
Associated Lai Samples: 9289100001, 9289100002
Parameter Units
Blank Reporting
Result
Mercury
Limit
Analyzed Qualifiers
mg/kg
ND 0.0050 03114/1116:36
I
LABORATORY CONTROL SAMPLE: 576243
1
Parameter Units
Spike LCS
Conc Result
LCS % Rec
°
/o Rec Limits
QualifiersMercury
mg/kg
067 0.059
89 80-120
MATRIX SPIKE {SAMPLE: 576244
P Irameter Units
9289105032 Spike
MS MS
%Rec
Mercury
Result Conc.
Result % Rec
Limits Qualifiers,
1 mg/kg
0.024 .662
0.057 53
75-125 M1
MATRIX SPIKE SAMPLE: 576246
Parameter
9289105034 Spike
MS MS
% Rec
Units
Result Cone.
Result % Rec
Limits Qualifiersmgt
0.023 069
0.077 79
7-1125
SAMPLE DUPLICATE: 576245
Parameter
9289105033 Dup
Units
Mercury9
Result Result
RPD Qualifiers
0.022 0.020
7
SAMPLE DUPLICATE: 576247
1
Parameter
9289105036 Dup
Units
mercury i
Result Result
RPD Qualifiers
I m9�9
0.0049 0.0055
13 --
I
Date: O 2312011 07:49 AM
I
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pam Analyficd Services, Inc..
Page 11 of 15

Percent il
SAMPLE
Percent
Date: 03J23/2011
i
aceAnalytical
www.pacelabs.com
i
Project. I WOOD BOILER 03103
Pace ProjectNo.: 9289100
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
(R)ALITY CONTROL DATA
uu tsarcn: I PMSTJ3784 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9289100001, 9289100002
b;MrLL UUPLIGATE: 574042
9289063001 Dup
Units Result Result
% 27.7 28.0
Parameter
b/4U43
9289198001 Dup
Units Result Result
% 69.4 69.7
RPD Qualifiers
1
RPD Qualifiers
0
OT49 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPaacee Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 MnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 15

i
aeeAnalytical
www-Pwdabs com
Pace Analytical Services, Inc.
205 East Meadow Road - SuiteA
Eden, NC 27288
[phone]
Project WOOD BOILER 03/03
Pace Project No.: 9289100
QC batch' I VVET/15749
QC Batch Method: EPA 9045
Associated Lab Samples: 9289100001, 9289,00002
1
SAMPLE
PaceAralytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA9045
Analysis Description: 9045 pH
9289100001 Dup
Parameter Units Result Result
RPD Qualifiers
.pH at 25 Degrees C Std. Units 9.3 9.3
0
i
Date: 03/23l2011 07..49AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
N ACcpq
Pace Analytical Services, Inc.
9800 Kncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 15

acemalxical
www..pacokbs.com
Project WOOD BOILER 03103
Pace Project No.: 9289100
Pace Analytical Services, Inc.
205 East MeadowRoad - SuffeA
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/9255 Analysis Method: EPA365.1
QC Batch Method: EPA365.1 Analysis Description:, 365.1 Phosphorus, Total
Associated Lab Samples: 9289100001, 9289100002
METHOD BLANK 574924
Associated Lab Samples. 9289100001, 9289100002
Matrix: Solid
Blank Reporting
Parameter Units Result Limit
Analyzed Qualifiers
Phosphorus mg/kg ND 2.0 03/09/1123:08
.LABORATORY CONTROL SAMPLE: 574925
Pace Analytical Services, Inc.
9800 IGnoeyAve. Suite 100.
Huntersville, NC 28078
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 50
50-2 100 30-110
MATRIX SPIKE SAMPLE: 574926
[phone]
9288906001 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec
Phosphorus Limits Qualifiers
mg/kg 9.3 99.7 72.1 63 M1
SAMPLE DUPLICATE: 574928
9289100001 Dup
Parameter Units Result Result RPD
Phosphorus Qualifiersmg/k9 2950 2790
6
Date: 03/23/2011 07:49 AM
REPORT OF LABORATORYANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical services, Inc..
Page 14 of 15

aceAnalyical
www.pacelabaccm
Project: WOOD BOILER 0&03
Pace Project No.: 9289100
DEFINrnOHS
Pace Analytical Services, Inc.
205 East Meadow Road - SuiteA
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
98001QnceyAve, Suite 1o0
Huntersville, NC 28078
DF -Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. ,
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analyticalis NELAP accredited, Contact your Pace PM for the current list of accredited analytes.
LABORA70MES
PAST-4 Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
Mt Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
Date: 03/23/2011 07:49 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�~r
y�x
[phone]
Page 15 of 15

Date: a:• �
Facility:_ HIV
Analyst: _'�,,
Calibration
:alibration Cal Buffer Cal Buffer Check
Time 4.0
10,0 Buffer 7.0"
0 5 110
pH buffer checks are to be within t 0.1 pH units of the standard's true value
PH Analyses
Time Time
' ID Sam led Anal zed
H Result ®offer
Check""
7.0
+++uic:ates a recommended drift check using Buffer 7.0 at the end of testing or every
Results should be within t 0.1 pH units of the standard's true value.
um.

Baxter Healthcare - Wood Boiler
Please test the sample(s) for the parameters as listed below.
Send original results to: email: [e-mail]
Send invoice and copy of results to: email: [e-mail]
Ricky Styles
Baxter Healthcare Purchase order # 25819
2859 Old Linville Rd.
Marion, NC 28752
[phone]
email: [e-mail]
uested Due
Date:
Sample #
Sample Sample Date(s) Grab or Total Metals-- TCLP Metals Ignitability,
Description and time sample Composite As,
Ba, Cd, As, Ba, Cd, Reactivity
collected Ca, Cr, Cu, Fe, Cr, Pb, Hg,
Pb, Mg, Hg, Se, Ag
Mn, Mo, Ni, K,
Se, Ag, Na,
Zn, total
Phosphorus
WB1 QTR2011 I BOTTOM ASH 14-18-11 9:45AM I COMPOSITE I YES
Sample sent to: Pace Analytical Services,
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Chain of Custody a
Project Manager: Tom Williams
9800 Kincey Avenue, Suite 10(
Huntersville, NC 28078
(704) 875 - 9092 ext. 233
pH I Total -Arsenic Full TCLP
Corrosivity
YES

aceAnalytical
www.pwdabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
May 13, 2011
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: WOOD BOILER 04/18
Pace Project No.: 9292205
Dear Mr. Styles:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Enclosed are the analytical results for sample(s) received by the laboratory on April 18, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lord Patton for
Tom Williams
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, [do..
[phone]
Page 1 of 10

�'+Pez�labxcam
Project: WOOD 801LER 04118
Pace Project No.: 9292205
PaceAnalytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Charlotte Certification IDs
9800 KinceyAve. Ste 100, Huntersville, NC 28078
Louisiana/LELAP Certification #: 04034 New Jersey Certification #. NCO12
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification & 5342
North Carolina Wastewater Certification #: 12
Pennsylvania Certification #: 68-00784
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Connecticut Certification P PH-0106
Rodda/NELAP Ce,tification #: E87648
Massachusetts Certification #: M-NC030
New Jersey Certification #. NC011
North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
South Carolina Drinking Water Cent. #: 99006003
Virginia Certification *: 00213
Connecticut Certification #: PH-0104
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DHH Drinking Water # LA 100031
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 40
Pennsylvania Certification & 68-03578
South Carolina Bioassay Certification #: 99030002
South Carolina Certification #: 99030001
Virginia Certification M 00072
West Virginia Certification #: 356
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
ACo
e
u �'
Pace Analytical Services, in,
9800 Kncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 10

accAnalXical
wwwpacetabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project:
WOOD BOILER 04/18
Pace Project No.:
9292205
Lab ID
Sample ID
Method
Analysts
9292205001
VVBIQTIR2011 BOTTOM ASH
EPA6010
JMW
EPA7471
SHB
ASTM D2974-87
TNM
EPA 365.1
JDA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
o,N ACC,*
N
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Reported Laboratory
17
PASI-A
1
PASI-A
1
PASI-C
1
PASI-A
Page 3 of 10

�+•Pace/ebSrom
PaceAnalyticai services. Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-8g21
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: ANALYTICAL RESULTS
Pace Project No.: WOOD BOILER 04/18
9292205
Sample: S QTR2091 BO
ASH TTORN Lab!D: 929220500,
Results Collected: 04/i8/1109:45
��on a parryightw { Received 04/18
Pace Analytical Services, Inc.
9900 lGnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Parameters
W
/11 1050 Matrix: Soir�
6010 IWET ICP
Results Units
��
Repay Limit DP
�� Prepared
Arsenic
Analyzed CAS No. Qual
Analytical Method: EPA 6010 Preparation Method: ��
Barium
8.9 mg/kg
EPA 3050
Cadmium
Calcium
1440 mg/kg
0.56 mg/kg
0.48 1
4.8 10
04/21/1t 1400 04/24/11 19:26 7440 38 2
04/21/11 14:00
Chromium
46200 mglkg
0.095 1
04/25/1, 11:45 7440 9-3.
04/21/11 14:00 04/24/11 19.45
Copper
Iron
32.5 mg/kg
91.6 mg/kg
95.1 10
0.48 1
744 0-43-9
04/21/11 14:00 04/24/11 19:2 7440-70-2
64/21/11 14:00
Lead
18600 mg/kg
0.48 1 475
04/24/1, 19..26 7440-47-3
04/21/11 14:00 04/24/11 19:26
Magnesium
Manganese
91.9 mg/kg
8240' mg/kg
10
0.48 1
7440-50-8
04/21/11 14:00 04/25/11 11:45 7439 g9 0
04/21/11 14:00
Molybdenum
1640 mg/kg
95 1
04/24/11 19:26 7439-92-1
04/21/11 14:00 04/24/11 19:26
Nickel
0.74 mg/kg
4'8 10
1
7439-95-4
04/21/11 1400 04/25/11 11.45 7439-96-5
Potassium
15.4 mg/kg
U48 1
04/21/11 14:00 04/24/11 19:26 7439-98-7
Selenium
19800 mg/kg
.8
4750 10
04/21/11 14:00 04/24/11 19:26 7440-0 2_0
Silver.
1.2 m
mg/kg
0•95 1
04/21/11 14:00 04/25/11 11:45 7440 02_0
9-7
Sodium
0.51 mg/kg
0.48 1
04/21/11 14:00 04/24/11 19:26 7782-49-2
Zinc
14400 mg/kg
4750 10
04/21/1114:00 .04/24/1119:26 7440-22-4
7471 Mercury
265 mg/kg
0.95 1
04/21/11 14:00 04/25/11 11:45 7440-23-5
04/21/11 14:00 04124/11 19:26
Mercury
7440.66-6
Analytical Method: EPA 7471 Preparation Method: EPA 7471
P&fCEDt MOiSQUnB
ND mg/kg
0.0034 1
05/02/11 12:10 05/03/11 14:14 7439-97-6
Analytical Method: ASTM D2974-87
Percent Moisture
285.1 Phosphorus, Total
0.78 %
0.10 1
04/21/11 08:56
Analytical Method: EPA 365.1
Phosphorus
1510 mg/kg
56.0 10
05/0211116:22 7723-14-0 M6
Date: 05/13/2011 01:05 PM REPORT OF LABORATORY ANALYSIS Page 4 of 10
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
R
it

acaAnalidical
www.pacelabs.com
Project: WOOD BOILER 04/18
Pace Project No.: 9292205
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
QC Batch: MPRP/8223
QC Batch Method: EPA3050
Associated Lab Samples: 9292205001
METHOD BLANK: 594254
Associated Lab Samples: 9292205001
Parameter Units
Analysis Method: EPA6010
Analysis Description: 6010 MET
Matrix: Solid
Blank Reporting
Result Limit Analyzed
Qualifiers
Arsenic
mg/kg
ND
0.50
04/2411117:43
Barium
mg/kg
ND
0.50
04/2411117:43
Cadmium
mg/kg
ND
0.10
04/24/1117:43
Calcium
mg/kg
ND
10.0
04/24/1117.43
Chromium
mg/kg
ND
0.50
04/24/1117:43
Copper
mg/kg
ND
0.50
04/24/1117:43
Iron
mg/kg
NO
5.0
04/24/1117:43
Lead
mg/kg
ND
0.50
04/24/1117:43
a
Magnesium
mg/kg
ND
10.0
04/24/1117:43
Manganese
mg/kg
ND
0.50
04124/1117:43
Molybdenum
mg/kg
ND
0.50
04/24/1117:43
Nickel
mg/kg
ND
0.50
04/24/1117:43
Potassium
mg/kg
ND
500
04/24/1117:43
Selenium
mg/kg
ND
1.0
04124/1117:43
Silver
mg/kg
ND
0.50
04/24/1117:43
Sodium
mg/kg
ND
500
04/2411117:43
Zinc
mg/kg
ND
1.0
04/24/1117:43
LABORATORY CONTROL SAMPLE:
594255
Spike
LCS
LCS %Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Arsenic
mg/kg
50
51.0
102
80-120
Barium
mg/kg
50
51.3
103
80-120
Cadmium
mg/kg
50
51.4
103
80-120
Calcium
mg/kg
500
513
103
80-120
Chromium
mglkg
50
51.9
104
80-120
Copper
mg/kg
50
51.4
103
80-120
Iron
mg/kg
500
521
104
80-120
Lead
mg/kg
50
52.4
105
80-120
Magnesium
mg/kg
500
507
101
80-120
Manganese
mg/kg
50
52.1
104
80-120
Molybdenum
mg/kg
50
52.2
104
80-120
Nickel
mg/kg
50
51.4
103
80-120
Potassium
mg/kg
500
476J
95
80-120
Selenium
mg/kg
50
51.7
103
80-120
Silver
mg/kg
25
25.7
103
80-120
Sodium
mglkg
500
507
101
80-120
Zinc
mg/kg
50
52.2
104
80-120
Date: 05/13/2011 01:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
x
[phone]
Page 5 of 10

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnaPytocal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
w-pacelabs com 875-9092
(336)623�921 [phone] n 04 )
QUALITY COMYROL DATA
Project: WOOD BOILER 04118
Pace Project No.: 9292205
MATRIX SPIKE SAMPLE:
Parameter
594563
Units
9292061011
Result
Spike
Conc.
MS
Result
MS
% Rec
%Rec '
Limits Qualifiers
Arsenic
mg/kg
0.53
42.7
42.7
99
75-125
Barium
mg/kg
14.1
42.7
65.4
120
75-125
Cadmium
mg/kg
ND
42.7
42.5
100
75-125
Calcium
mg/kg
136
427
609
111
75-125
Chromium
mg/kg
1.6
42.7
45.8
104
75-125
Copper
mg/kg
1.8
42.7
47.5
107
75-125
Iron
mg/kg
1140
427
2100
223
75-125 MO
Lead
mg/kg
6.3
42.7
52.2
107
75-125
Magnesium
mg/kg
60.5
427
546
114
75-125
Manganese
mg/kg
13.8
42.7
61.5
112
75-125
Molybdenum
mg/kg
ND
42.7
42.4
99
75-125
Nickel
mg/kg
0.59
42.7
44.1
102
75-125
Potassium
mglkg
ND
427
533
109
75-125
Selenium
mg/kg
ND
42.7
43.4
101
75-125
Silver
mg/kg
ND
21.4
21.5
101
75-125
Sodium
mg/kg
ND
427
480
109
75-125
Zinc
mg/kg
31.1
42.7
111
188
75-125 MO
SAMPLE DUPLICATE: 594257
Parameter
Units
9292061010
Result
Dup
Result
RPD Qualifiers
Arsenic
mg/kg
0.79
1.8
75 R1
Barium
mg/kg
16.4
19.8
19 ,
Cadmium
mg/kg
ND
ND
Calcium
mg/kg
25.5
32.2
23 R7
Chromium
mglkg
3.4
4.1
18
Copper
mg/kg
1.7
2.4
35 R1
Iron
mg/kg
1430
4000
95 R1
Lead
mg/kg
8.1
9.1
12
Magnesium
mg/kg
52.6
61.0
15
Manganese
mg/kg
2.1
2.4
11
Molybdenum
mg/kg
ND
.181
Nickel
mg/kg
0.80
0.69
15
Potassium
mg/kg
ND
125J
Selenium
mg/kg
ND
.52J
Silver
mg/kg
ND
ND
Sodium
mg/kg
ND
27AJ
Zinc
mg/kg
1.5
1.8
20
Date: 05/13/2011 01:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 10

i
i Pace Analytical Semiccs, Inc.
® Pace Analytical Services, Inc. Pace Analytical Services, Inc. °
aceAnaly,ica! 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kinsey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Nuntersville, NC 28078
wl w.pacelabs.wm [phone] [phone] [phone]
i
QUALITY CONTROL DATA
Project: WOOD BOILER 04/18
Pace Project No.: 9292205
QC Batch: MERP/3449 Analysis Method: EPA7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 9292205001
METHOD BLANK: 599475 Matrix: Solid
Associated Lab Samples: 9292205001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0050 05/03/1114:03
LABORATORY CONTROL SAMPLE: 599476
Spike LCS ' LCS %Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
80-120
Mercury s
mg/kg _067 0.066 99
MATRIX SPIKE SAMPLE: 599477 MS % Rec
9292205001 Spike MS
Units Result Conc. Result % Rec Limits Qualifiers
Parameter
Mercury mg/kg ND 056 0.057 102 75-125
SAMPLE DUPLICATE: 599478
9292205001 Dup
Parameter Units Result Result RPD Qualifiers
Mercury mg/kg ND ND
Date: 05/13/2011 01:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
uoLJLs
Page 7 of 10

aceAnal dical
www.pamlabs.com
Project: WOOD BOILER 04/18
Pace Project I o.: 9292205
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
(QUALITY CONTROL DATA
QC Batch: PMST/3862 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9292205001
SAMPLE DUPLICATE: 593715
9291724005 Dup
Parameter Units Result Result RPD, Qualifiers
Percent Moisture % 25.8 26.6 3
SAMPLE DUPLICATE: 593716
9292259008 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 15.4 15.9 3
Date: 05/13/2011 01:05 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 10

I
acoAhalytical
www.pacelabs.com
I
Project: WOOD BOILER 04/18
Pace Project No.: 9292205
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/9616 Analysis Method: EPA 365.1
QC Batch Method: EPA365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 9292205001
METHOD BLANK: 599528 Matrix: Solid
Associated Lab Samples: 9292205001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg NO 2.0 0510211116:04
i ARnRATORY CONTROL SAMPLE: 599529
Parameter
Phosphorus
MATRIX SPIKE SAMPLE:
Parameter
Phosphorus
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS
LCS
% Rec
Units
Conc. Result
% Rec
Limits
Qualifiers.
mg/kg
50 51.6
103
90-110
599531
9292205001 Spike
MS
MS
% Rec
Units
Result Conc.
Result
% Rec
Limits Qualifiers
mg/kg
1510 105
1640
118
90-110 M6
SAMPLE DUPLICATE: 599530
9292205001 Dup
Parameter Units Result Result RPD Qualifiers
Phosphorus mg/kg 1510 1260 18
Date: 05/13/2011 01:05 PM REPORT OF LABORATORY ANALYSIS
Page 9 of 10
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�q

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr. 98o0 i<inceyAve. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALIFIERS
Project: 1 WOOD BOILER 04/18
Pace Project N I o.: 9292205
DEFINITIONS!
i
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Sili ica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
PAST -A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE Ql1ALIF1EI2S
Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 I RPD value was outside control limits.
Date: 05/13/2011 01:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
o,H needy
�W s
Page 10 of 10

------Date: �/���~��---------------- � . / --�-- .
- Analyst:
Facility:
Calibration
PH Analyses
• ---- - �•..�.ywu u uUG H61UC.

Baxter Healthcare e Wood Boiler
-Please test the sampie(s) for the parameters as listed below.
Send original results to: email: [e-mail]
Send invoice and copy of results to: email: [e-mail]
Ricky Styles
Baxter Healthcare,
2859 Old Linville Rd.
Marion, NC 28752
[phone]
email: [e-mail]
Purchase order # 31084
uested Due Date:
Sample # Sample Sample Dates) Grab or
Description and time sample Composite
collected
Total Metals -
TCLP Metals
Ignitability,
As, Ba, Cd,
As, Ba, Cd,
Reactivity
Ca, Cr, Cu, Fe,
Cr, Pb, Hg,
Pb, Mg, Hg,
Se, Ag
Mn, Mo, Ni, K,
Se, Ag, Na,
Zn, total
Phosphorus
WBNP628 NORTH POND 6-28-118:30AM COMPOSITE YES YES YES
Sample sent to: Pace Analytical Services, Project Manager: Tom Williams
2225 Riverside Drive 9800 Kincey Avenue, Suite 10(
Asheville, NC 28804 Huntersville, NC 28078
828-254-7176 (704) 875 - 9092 ext. 233
Chain of Custody
pH I Total -Arsenic
Corrosivity
YES
TCLP
YES

aceMglXical
vnn paoebbs.00m
July 15, 2011
I
Mr. Ricky; Styles
Baxter Healthcare
2859 Oldj Linville Road
Marion, NC 28752
I
RE: Project: Wood Boiler
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
Pac.1e Project No.: 9297122
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 IGnceyAve. Suite 100
Huntersville, NC 28078
i
Dear Mr. Styles:
EnclosedI are the analytical results for sample(s) received by the laboratory on June 28, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards, where applicable, unless otherwise narrated in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Mi�
Tom Willi
[e-mail]
Project Manager
i
Enclosures
i
i
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
0
[phone]
Page 1of 21

,�&cce,A'17apical
www.pacews.com
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Arizona Certification #: AZ0735
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH 0216
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Kansas Certification #. E-10383
Kentucky Certification M 90050
Louisiana Certification* LA090012
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL1264
Massachusetts Certification M M-FL1264
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NC012
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #. 12
Pennsylvania Certification #: 68-00784
South Carolina Certification t 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Connecticut Certification #: PH-0106
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
New Jersey Certification #. NC011
North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #. 37712
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Michigan Certification M 9911
Mississippi Certification: FL NELAC Reciprocity
Montana Certification #: Cert 0074
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New Jersey Certification #: FL765
New York Certification #. 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Pennsylvania Certification #: 68-547
Puerto Rico Certification #: FLO1264
Tennessee Certification #: TNO2974
Texas Certification: FL NELAC Reciprocity
Virginia Certification #: 00432
Wyoming Certification: FL NELAC Reciprocity
South Carolina Drinking Water Cert. M 99606003
Virginia Certification #: 00213
Connecticut Certification #: PH-0104
Florida/NELAP Certification M E87627
Kentucky UST Certification #: 84
Louisiana DHH Drinking Water# LA 100031
West Virginia Certification #. 357
North Carolina Wastewater Certification #: 40
Pennsylvania Certification M 68-03578
South Carolina Bioassay Certification #: 99030002
South Carolina Certification * 99030001
Virginia Certification #: 00072
West Virginia Certification M 356
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 21

i
aceAnallcal
w6pawlabsxom
Project:
Wood Boiler
Pace Project No.:
9297122
Lab ID
Sample 10
9297122001
North Pond MNBMP628
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALY E COUMT
Mathod
EPA 8081
EPA 8151
EPA 6010
EPA 6010
EPA 7470
EPA 7471
EPA 8270
EPA 8260
ASTM D2974-87
EPA 9045
EPA 365.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the w6ften consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Analysts Reported Laboratory
BAG
9
PASI-O
LJM
3
PASI-0
SHB
17
PASI-A
SHB
7
PASI-A
JMW
1
PASI-A
JMW
1
PASI-A
PPM
18
PASI-C
DLK
15
PASI-C
KDF
1
PASI-C
SAJ
1
PASI-A
JDA
1
PASI-A
Page 3 of 21

I
I
aceAnalXical®
wIww.pacelabszom
Project: i Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 lGncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: North Pond OWBNP628 Lab ID: 9297122001 Collected: 06/28/11 08:30 Received: 06/28/11 09:25 Matrix: Solid
Results reported on a dry -weight" basis
i
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
Analytical Method: EPA8081
gamma-BHC (Lindane)
ND mg/L
0.0010
1
07/08/11 15:27
07/08/11 17:14
58-89-9
Chlordane (Technical)
ND mg/L
0.0050
1
07/08/11 15:27
07/08/11 17:14
57-74-9
Endrin
ND mg/L
0.0010
1
07/08/11 15:27
07/08/11 17:14
72 20-8
Heptachlor
ND mg/L
0.0010
1
07/08/11 15:27
07/08/11 17:14
76-44-8
Heptachlor epoxide
ND mg/L
0.0010
1
07/08/11 15:27
07/08/11 17:14
1024-57-3
Methoxychlor
ND mg/L
0.0010
1
07/08/11 15:27
07/08/11 17:14
72-43-5
Toxaphene
ND mg/L
0.0050
1
07/08/11 15:27
07/08/11 17:14
8001-35-2
Decachlombiphenyl (S)
66 %
70-130
1
07/08/11 15:27
07/08/11 17:14
2051-24-3 S1
Tetrachloro m-zylene (S)
76 %
70-130
1
07/08/11 15:27
07/08/11 17:14
877-09-8
8151 Chlorinate Herbicide TCLP
Analytical Method: EPA 8151
2,4-D
ND mg/L
0.010
1
07/07/11 14:00
07/12/11 20:17
94-75-7
2,4,5-TP (Silvez)
ND mg/L
0.010
1
07/07/11 14:00
07/12/11 20:17
93-72-1 M1
2,4-DCPA (S)
94 %
70-130
1
07107111 14:00
07/12/11 20:17
19719-28-9
6010 MET ICP i
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
14.4 mg/kg
0.88
1
07/12/11 11:40
07/13/11 14:18
7440-38-2
Barium
1350 mg/kg
0.88
1
07/12/11 11:40
07/13/11 14:18
7440-39-3
Cadmium
2.2 mg/kg
0.18
1
07/12/11 11:40
07/13/11 14:18
7440-43-9
Calcium i
64200 mg/kg
175
10
07/12/11 11:40
07/13/11 16:15
7440-70-2
Chromium 1
26.1 mg/kg
0.88
1
07/12/11 11:40
07/13/11 14:18
7440-47-3
Copper
92.4 mg/kg
0.88
1
07/12/11 11:40
07/13/11 14:18
7440-50-8
Iron
14300 mg/kg
17.5
1
07/12/11 11:40
07/13/11 14:18
7439-89-6
Lead
32.4 mg/kg
0.88
1
07/12/11 11:40
07/13/11 14:18
7439-92-1
Magnesium i
13000 mg/kg
17.5
1
07/12/11 11.,40
07/13/11 14:18
7439-95- 4
Manganese
2410 mg/kg
8.8
10
07/12/11 11:40
07/13/11 16:15
7439-96-5
Molybdenum
5.1 mg/kg
0.88
1
07/12/11 11 A0
07/13/11 14:18
7439-98-7
Nickel
16.4 mg/kg
0.88
1
07/12/11 11:40
07/13/11 14:18
7440-02-0
Potassium
15800 mg/kg
8760
10
07/12/11 11:40
07/13/11 16:15
7440-09-7
Selenium
ND mg/kg
1.8
1
07/12/11 11:40
07/13/11 14:18
7782-49-2
Silver
0.93 mg/kg
0.88
1
07/12/11 11.40
07/13/11 14:18
7440-22-4
Sodium
12300 mg/kg
8760
10
07/12/11 11:40
07/13/11 16:15
7440-23-5
Zinc
254 mg/kg
1.8
1
07/12/11 11:40
07/13/11 14:18
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 07/07/11 18:05
Arsenic !
ND mg/L
0.025
1
07/08/11 15:45
07/11/11 13:43
7440-38-2
Barium
1.1 mg/L
0.50
1
07/08/11 15:45
07/11/11 13:43
7440-39-3
Cadmium
0.037 mg/L
0.0050
1
07/08/11 15:45
07/11/11 13:43
7440-43-9
Chromium
ND mg/L
0.025
1
07/08/11 15:45
07/11/11 13:43
7440-47-3
Lead
ND mg/L
0.025
1
07108/11 15:45
07/11/11 13:43
7439-92-1
Selenium
ND mg/L
0.10
1
07/08/11 15:45
07/11/11 13:43
7782-49-2
Silver
ND mg/L
0.025
1
07/08/11 15:45
07/11/11 13:43
7440-22-4
Date: 07/15/2011,05:47 PM
REPORT OF LABORATORY
ANALYSIS
Page 4 of 21
i
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnaltical
Mw.pawlftcom
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
ANALYTICAL RESULTS
oamium. tnorxn t-ona wilubwnzi; Lab ID: 9297122001
Results reported on a dry -weigh¢" basis
Pace Analytical Services, Inc.
9800 IGnceyAve. Suite 100
Huntersvilie, NC 28078
Collected: 06/28/11 08:30 Received: 06/28/11 09:25 Matrix: Solid
[phone]
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7470,RAercury, TCLP
Mercury
7471 Mercury
Mercury
8270 MSSV TCLI P Sep Funnel
1,4-Dichlorobenz4ene
2,4-Dinkrotoluene
. Hexachioro-1,3-6utadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene j
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl '(S)
Terphenyl-d14 (Sj
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
1
8260 MSV TCLP , .
Benzene
2-Butanone (MEIn
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
11-Dichloroethene
Tetrachloroethene
Tdchloroethene
Vinyl chloride
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-13romofluorobenzene (S)
DibromofluorometF ane (S)
Date: 07/15/2011 0 .47 PM
i
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 07/07/11 18:05
ND ug/L 0.20 1 07/08/11 17:10 07/11/11 13 16 7439-97-6
Analytical Method: EPA 7471 Preparation Method: EPA 7471
0.022 mg/kg 0.0084 1 07/07/11 10:10 07/07/11 16:45 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 06/30/11 16:00
ND ug/L
50.0
1
07/01/11 10:00
07/01/11 21:37
106-46-7
ND ug/L
50.0
1
07/01/11 10:00
07/01/11 21:37
121-14-2
ND ug/L
50.0
1
07/01/11 10:00
07/01/11 21:37
87-68-3
ND ug/L
50.0
1
07/01/11 10:00
07/01/11 21:37
118-74-1
ND ug/L
5010
1
07/01/11 10:00
07/01/11 21:37
67-72-1
ND ug/L
50.0
1
07/01/11 10:00
07/01/11 21:37
95-48-7
ND ug/L
50.0
. 1
07/01/11 10:00
07/01/11 21:37
ND ug/L
50.0
1
07/01/11 10:00
07/01/11 21:37
98-95-3
ND ug/L
100
1
07/01/11 10:00
07/01/11 21:37
874W5
ND ug/L
50.0
1
07/01/11 10:00
07/01/11 21:37
110-86-1
ND ug/L
50.0
1
07/01/11 10:00
07/01/11 21:37
95-95-4
ND ug/L
50.0
1
07/01/11 10:00
07/01/11 21:37
88-06-2
84 %
12-102
1
07/01/11 10:00
07/01/11 21:37
4165-60-0
82 %
13-107
1
07/01/11 10:00
07/01/11 21:37.
321-60-8
82 %
21-132
1
07/01/11. 10:00
07/01/11 21:37
1718-51-0
30 %
107110
1
07/01/11 10:00
07/01/11 21:37
13127-88-3
44 %
10-110
1
07/01/11 10:00
07/01/11 21:37
367-12-4
87 %
27-108
1
07/01/11 10:00
07/01/11 21:37
118-79-6
Analytical Method: EPA 8260
ND ug/L
190
38
07101/11 10:23
71-43-2
ND ug/L
380
38
07/01/11 10:23
78-93-3
ND ug/L
190
38
07/01/11 10:23
56-23-5
ND ug/L
190
38
07/01/11 10:23
108-90-7
ND ug/L
190
38
07/01/11 10:23
67-66-3
ND ug/L
190
38
07/01/11 10:23
106-46-7
ND ug/L
190
38
07/01/11 10:23
107-06-2
ND ug/L
190
38
07/01/11 10:23
75-35-4
ND ug/L
190
38
07/01/11 10:23
127-18-4
ND ug/L
190
38
07/01/11 10:23
79-01-6
ND ug/L
190.
38
07/01/11 10:23
75-01-4
97 %
70-130
38
07/01/11 10:23
17060-07-0
103 %
67-135
38
07/01/11 10:23
2037-26-5
95 %
70-130
38
07/01/11 10:23
460-00-4
91 %
70-130
38
07/01/11 10:23
1868-53-7
REPORT OF LABORATORY
ANALYSIS
(_X
j Page 5 of 21
This report shall not be reproduced, except in full,
i
to
without the written consent of Pace Analytical Services, Inc..
P.
loQ�
t�

ace',�WxiCal
www.pacelabs.com
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800IGnceyAve. Suite 100
Huntersville, NC 28078
[phone]
bampie: worth Pond OWBMP628
Lab ID: 9297122001 Collected:
06/28/11 08:30
Received: 06/28/11 09:25 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
47.2 %
0.10 1
06/30/11 08:43
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
9.4 Sid. Units
0.10 1
- 07/05/11 16:19
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
3340 mg/kg
105 10
07/08/11 16:04 7723-14-0
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�r
Page 6 of 21

aceAnalytical
www.pacews com
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: GCSV/5111 Analysis Method: EPA 8081
QC Batch Method: EPA 8081 Analysis Description: 8081 GCS TCLP Pesticides
Associated Lab Samples: 9297122001
METHOD BLANK: 221091
Matrix: Water
Associated Lab Samples:
9297122001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Chlordane (Technical)
mg/L
ND
0.0050
07/08/11 15:58
Endrin
mg/L
ND
0.0010
07/08/11 15:58
gamma-BHC (Lindane)
mg/L
ND
0.0010
07/08/11 15:58
Heptachlor
mg/L
ND
0.0010
07/08/11 15:58
Heptachlor epoxide
mg/L
ND
0.0010
07/08/11 15:58
Methoxychlor
mg/L
ND
0.0010
07/08/11 15:58
Toxaphene
mg/L
ND
0.0050
07/0811115:58
Decachlorobiphenyl (S)
%
105
70-130
07/08/11 15:58
Tetrachloro-m-xylene (S)
%
78
70-130
07/08/11 15:58
LABORATORY CONTROL SAMPLE:
Parameter
221092
Units
Spike
Conc.
LCS LCS
Result % Rec
Endrin
mg/L
.005
0.0046
gamma-BHC (Lindane)
mg/L
.005
0.0041
Heptachlor
mg/L
.005
0.0041
Heptachlor epoxide
mg/L
.005
0.0047
Methoxychlor
mg/L
.005
0.0046
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
% Rec
Limits
Qualifiers
93 70-130
82 70-130
83 70-130
94 70-130
93 70-130
101 70-130
86 70-130
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
221336
221337
MS
MSD
9297122001
Spike
Spike
M$
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Endrin
mg/L
ND
.005
:005
0.0048
0.0046
96
92
70-130
4
gamma-BHC (Lindane)
mg/L
ND
.005
.005
0.0042
0.0040
84
81
70-130
4
Heptachlor
mg/L
ND
.005
.005
0.0043
0.0041
86
82
70430
5
Heptachlor epoxide
mg/L
ND
.005
.005
0.0049
0.0046
98
93
70-130
6
Methoxychlor
mg/L
ND
.005
.005
0.0050
0.0047
100
95
70-130
5
Decachlorobiphenyl (S)
%
80
77
70-130
Tetrachloro-m xylene (S)
%
87
82
70-130
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
i
Page 7 of 21

1
,aatcl el Analytical
www.pacebbs.com
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: GCSV/5109
Analysis Method: EPA8151
QC Batch Method: EPA 8151
Analysis Description: 8151 GCS Herbicides TCLP
Associated Lab Samples: 9297122001
METHOD BLANK: 220563
Matrix: Water
Associated Lab Samples: 9297122001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
2,4,5-TP (Silvex) mg/L
ND 0.010
07/12/11 19:24
2,4-D mg/L
ND 0.010
07/12/11 19:24
2,4-DCPA (S) %
85 70-130
07/12/11 19:24
LABORATORY CONTROL SAMPLE: 220564
Spike LCS
LCS % Rec
Parameter Units
Cone. Result % Rec Limits Qualifiers
2,4,5-TP (Silvex) mg/L
.012 0.011
88 70-130
2,4-D mg/L
.06 0.049
81 70-130
2,4-DCPA (S) %
92 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 220565
220566
MS MSD
9297122001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
2,4,5-TP (Silvex) mg/L ND
012 .012 0.016
0.011 131 93
70-130 34 M1
2,4-D mg/L ND
.06 .06 0.077
0.056 129 94
70-130 32
2,4-DCPA (S) %
110 92
70-130
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 21

1lan
j wtaw.pawlabs.com
I
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
(QUALITY CONTROL DATA
a
Project: Wood Boiler
Pace Project No.: 9297122
QC Batch: MPRP/8714 Analysis Method: EPA6010
QC Batch Method: EPA3050 Analysis Description: 6010 MET
Associated Lab Samples: 9297122001
METHOD BLANK: 632215
Associated Lab Samples:
Parameter
9297122001
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed Qualifiers
Arsenic
mg/kg
ND
0.60
07/13/1114:06
Barium
mg/kg
ND
0.50
07/13/1114:06
Cadmium
mg/kg
ND
0.10
07113/1114:06
Calcium
mg/kg
ND
10.0
07113/1114:06
Chromium
mg/kg
ND
0.50
07/13/1114:06
Copper
mg/kg
ND
0.50
07/13/1114:06
Iron
mg/kg
ND
10.0
07/13/1114:06
Lead
mg/kg
ND
0.50
07/1311114:06
Magnesium
mg/kg
ND
10.0
07/1311114:06
Manganese
mg/kg
ND
0.50
07/13/1114:06
Molybdenum
mg/kg
ND
0.50
07/13/1114:06
Nickel
mg/kg
ND
0.50
07/13/1114:06
Potassium
mg/kg
ND
500
07/13/1114:06
Selenium
mg/kg
ND
1.0
07/13/1114:06
Silver
mg/kg
ND
0.50
07/13/1114:06
Sodium
mg/kg
ND
500
07113/1114:06
Zinc
mg/kg
ND
1.0
07113/1114:06
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
632216
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
47.4
95
80-120
Barium
mg/kg
50
48.0
96
80-120
Cadmium
mg/kg
50
49.6
99
80-120
Calcium
mg/kg
500
504
101
80-120
Chromium
mg/kg
50
50.2
100
80-120
Copper
mg/kg
50
47.2
94
80-120
Iron
mg/kg
500
516
103
80-120
Lead
mg/kg
50
49.1
98
80-120
Magnesium
mg/kg
500
496
99
80-120
Manganese
mg/kg
50
49.9
100
80-120
Molybdenum
mg/kg
50
49.3
99
80-120
Nickel
mg/kg
50
49.7
99
80-120
Potassium
mg/kg
500
441J
88
80-120
Selenium
mg/kg
50
47.6
95
80-120
Silver
mg/kg
25
24.6
98
80-120
Sodium
mg/kg
500
459J
92
80-120
Zinc
mglkg
50
50.7
101
80-120
Date: 07/15/2011 05:47 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
(a
Page 9 of 21

�aceAnalytical
www.pacelabs.corn
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 WnceyAve. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
632217
Units
9297122001
Result
Spike
Cone.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
14.4
91
108
102
75-125
Barium
mg/kg
1350
91
1540
214
75-125 M1
Cadmium
mg/kg
2.2
91
84.6
91
75-125
Calcium
mg/kg
64200
910
68900
510
75-125 M6
Chromium
mg/kg
26.1
91
117
100
75-125
Copper
mg/kg
92.4
91
190
107
75-125
Iron
mg/kg
14300
910
11800
-266
75-125 M1
Lead
mg/kg
32.4
91
110
85
75-125
Magnesium
mg/kg
13000
910
14700
189
75-125 M1
Manganese
mg/kg
2410
91
2650
262
75-125 M6
Molybdenum
mg/kg
5.1
91
86.5
89
75-125
Nickel
mg/kg
16.4
91
98.5
90
75-125
Potassium
mg/kg
15800
910
17500
190
75-125 M6
Selenium
mg/kg
ND
91
91.0
100
75-125
Silver
mg/kg
0.93
45.4
45.7
98
75-125
Sodium
mg/kg
12300
910
13600
147
75-125 M6
Zinc
mg/kg
254
91
367
124
75-125
SAMPLE DUPLICATE: 632218
9297452002
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Arsenic
mg/kg
ND
ND
Barium
mg/kg
ND
.17J
Cadmium
mg/kg
ND
ND
Calcium
mg/kg
33.5
32.3
4
Chromium
mg/kg
ND
.062J
Copper
mg/kg
ND
.052J
Iron
mg/kg
17.8
15.6
14
Lead
mg/kg
ND
ND
Magnesium
mg/kg
10.2
10.0
2
Manganese
mg/kg
0.55
0.46
17
Molybdenum
mg/kg
ND
.1J
Nickel
mg/kg
ND
ND
Potassium
mg/kg
5700
5860
3
Selenium
mg/kg
1.0
1.0
2
Silver
mg/kg
ND
.0951
Sodium
mg/kg
2390
2470
3
Zinc
mg/kg
1.1
1.2
4
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 21

Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
accAnalical
www.pac labs.com
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/8695 Analysis Method: EPA6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET TCLP
Associated Lab Samples: 9297122001
METHOD BLANK: 631475
Associated Lab Samples: 9297122001
Parameter Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
LABORATORY CONTROL SAMPLE:
631476
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
0.025
07111/1112:41
ND
0.50
07111/1112:41
ND
0.0050
07/11/1112:41
ND
0.025
07111/1112:41
ND
0.025
07111/1112:41
ND
0.10
07/11/1112:41
ND
0.025
07/1111112:41
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Cone.
Result
% Rec
Limits Qualifiers
2.5
2.7
109
80-120
2.5
2.6
103
80-120
2.5
2.5
100
80-120
2.5
2.6
103
80-120
2.5
2.4
94
80-120
2.5
2.7
108
80-120
1.2
1.3
102
80-120
MATRIX SPIKE SAMPLE:
Parameter
631477
Units
9296142001
Result
Spike
Cone.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/L
ND
2.5
2.5
101
75-125
Barium
mg/L
ND
2.5
2.4
88
75-125
Cadmium
mg/L
ND
2.5
2.4
94
75-125
Chromium
mg/L
ND
2.5
2.4
97
75-125
Lead
mg/L
257
2.5
217
-1600
75-125
Selenium
mg/L
ND
2.5
2.5
99
75-125
Silver
mg/L
ND
1.2
1.2
97
75-125
SAMPLE DUPLICATE: 631478
Parameter
9296514001 Dup
Units Result Result RPD Qualifiers
Arsenic
mg/L
ND ND
Barium
mg/L
1.2 1.2 0
Cadmium
mg/L
ND ND
Chromium
mg/L
ND ND
Lead
mg/L
ND 0.057
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 21

11
aceAnalylcal
ww.pacelabs.=
Project: Wood Boiler
Pace Project No.: 9297122 .
SAMPLE DUPLICATE: 631478
Parameter
Selenium
Silver
Date: 07/15/2011 05:47 PM
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY COMTROL DATA
9296514001 Dup
Units Result Result
mg/L ND ND
mg/L ND ND
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 21

aceAnailical o
www.pace4abs.corn
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
QC Batch: MERP13601 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 9297122001
METHOD BLANK: 631610
Associated Lab Samples: 9297122001
Parameter
Units
Mercury
ug/L
LABORATORY CONTROL SAMPLE:
631611
Parameter
Units
Mercury
ug/L
MATRIX SPIKE SAMPLE:
631613
Parameter
Units
Mercury
ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.20 07/11/1112:39
Pace Analytical Services, Inc.
9800 IGnceyAve. Suite 100
Huntersvilie, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.2 86 80-120
9296142001 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 2.5 1.9 75 75-125
SAMPLE DUPLICATE: 631612
9296514001 Dup
Parameter Units Result Result RPD Qualifiers
Mercury ug/L ND ND
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
0
Page 13 of 21

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
�ceAnalXi+cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwrw.pacei� abs corn Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
(336)623- 8921 (828)2547176 [phone]
QUALITY CONTROL DATA
Project: Wood Boiler
Pace Project No.: 9297122
QC Batch: MERP/3594
Analysis Method: EPA 7471
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 9297122001
METHOD BLANK: 630349
Matrix: Solid
Associated Lab Samples: 9297122001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Mercury
mg/kg
ND 0.0050
07/0711115:28
LABORATORY CONTROL SAMPLE:
630350
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Mercury
mg/kg
.067 0.061
91
80-120
MATRIX SPIKE SAMPLE:
630351
9297121005 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Mercury
mg/kg
0.013 .076
0.085
94
75-125
MATRIX SPIKE SAMPLE:
630353
9297031012 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Mercury
mg/kg
0.046 .075
0.11
92
75-125
SAMPLE DUPLICATE: 630352
9297167001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Mercury
mg/kg
ND .00038J
SAMPLE DUPLICATE: 630354
9297031013 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Mercury
mg/kg
0.036 0.032
11
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 21

aceAnalytal
www.pacelabs.com
Project: Wood Boiler
Pace Project No.: 9297122
QC Batch: 0EXT/14105
QC Batch Method: EPA 3510
Associated Lab Samples: 9297122001
METHOD BLANK: 628862
Associated Lab Samples: 9297122001
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA,
Analysis Method: EPA 8270
Analysis Description: 8270 TCLP MSSV
Matrix: Water
Parameter
Units
Blank
Result
1,4-Dichlorobenzene
ug/L
ND
2,4,5-Trichlorophenol
ug/L
ND
2,4,6-Trichlorophenol
ug/L
ND
2,4-Dinitrotoluene
ug/L
ND
2-Methylphenol(o-Cresol)
ug/L
ND
3&4-Methylphenol(m&p Cresol)
ug/L
ND
Hexachloro-1,3-butadiene
ug/L
ND
Hexachlorobenzene
ug/L
ND
Hexachloroethane
ug/L
ND
Nitrobenzene .
ug/L
ND
Pentachlorophenol
ug/L
ND
Pyridine
ug/L
ND
2,4,6-Tdbromophenol (S)
%
84
2-Fluorobiphenyl (S)
%
82
2-Fluorophenol (S)
%
44
Nitrobenzene-d5 (S)
%
85
Phenol-dB(S)
%
31
TerphenyW14(S)
%
74
LABORATORY CONTROL SAMPLE:
Parameter
628863
Units
Spike
Conc.
1,4-Dichlorobenzene
ug/L
500
2,4,5-Trichlorophenol
ug/L
500
2,4,6-Trichlorophenol
ug/L
500
2,4-Dinitrotoluene
ug/L
500
2-Methylphenol(o-Cresol)
ug/L
500
3&4-Methylphenol(m&p Cresol)
ug/L
500
Hexachloro-1,3-butadiene
ug/L
500
Hexachlorobenzene
ug/L
500
Hexachloroethane
ug/L
500
Nitrobenzene
ug/L
500
Pentachlorophenol
ug/L
1000
Pyridine
ug/L
500
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
Reporting
Limit
Analyzed
50.0
07/0111120:15
50.0
07/0111120:15
50.0
07/01/1120:15
50.0
07/01/1120:15
50.0
07101/1120:15
50.0
07/0111120:15
50.0
07/01/1120:15
50.0
07/0111120:15
50.0
07/01/1120:15
50.0
07/01/1120:15
100
07/01/1120:15
50.0
07/01/1120:15
27-108
07/01/1120:15
13-107
07101/1120:15
10-110
07/01/1120:15
12-102
07/01/1120:15
10-110
07/0111120:15
21-132
07101/1120:15
Qualifiers
LCS
Result
LCS
% Rec
% Rec
Limits
312
62
10-110
353
71
39-108
432
86
40-104
384
77
42-109
294
59
31-110
262
52
30-110
276
55
10-110
359
72
39-121
289
58
10-110
449
90
32-101
739
74
18-108
264
53
10-110
88
27-108
89
13-107
49
10-110
92
12-102
31
10-110
88
21-132
Pace Analytical Services, Inc.
9800 WnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Date: 07/15/2011 05:47 PM REPORT OF LABORATORY iAMALYSIS Page 15 of 21
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

i
aceAnalytical
www pacerabs.com
Project: Wood Boiler
Pace Project No: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 628864
9297187001
Parameter Units Result
MS
Spike
Cone.
MSD
Spike
Cone.
628865
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
1,4-Dichlorobenzene
ug/L
ND
500
500
300
290
60
58
30-150
3
2,4,5-Trichlorophenol
ug/L
ND
500
500
352
373
70
75
30-150
6
2,4,6-Trichlorophenol
ug/L
ND
500
500
440
453
88
91
30-150
3
2,4-Diniitrotoluene
ug/L
ND
500
500
375
412
75
82
30-150
10
2-Methylphenol(o-Cresol)
ug/L
ND
500
500
299
281
60
56
30-150
6
3&4-Methylphenol(m&p
ug/L
148
500
500
396
424
50
55
30-150
7
Cresol)
Hexachloro-1,3-butadiene
ug/L
ND
500
500
281
279
56
56
30-150
1
Hexachlorobenzene
ug/L
ND
500
500
359
358
72
72
30-150
0
Hexachloroethane
ug/L
ND
500
500
287
272
57
54
30-150
5
Nitrobenzene
ug/L
ND
500
500
479
463
96
93
30-150
3
Pentachlorophenol
ug/L
ND
1000
1000
764
809
76
81
30-150
6
Pyridine
ug/L
ND
500
500
266
230
53
46
30-150
14
2,4,6-Tdbromophenol (S)
%
85
85
27-108
2-Fluorobiphenyl (S)
%
87
85
13-107
2-Fluorophenol (S)
%
46
44
10-110
Nitrobenzene-d5 (S)
%
87
85
12-102
Phenol-d6 (S)
%
30
28
10-110
Terphenyl-dl4 (S)
%
80
83
21-132
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�`
Qual
Page 16 of 21

acemaIxical
www.pacelabs.com
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
uu batcn: MSV/15868
QC Batch Method: EPA 8260
Associated Lab Samples: 9297122001
Analysis Method: EPA 8260
Analysis Description: 8260 MSV TCLP
METHOD BLANK: 628597
Matrix: Water
Associated Lab Samples: 9297122001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,1-Dichloroethene
ug/L
ND
5.0
07/01/1100:41
1,2-Dichloroethane
ug/L
ND
5.0
07/01/1100:41
1,4-Dichlorobenzene
ug/L
ND
5.0
07/01/1100:41
2-Butanone (MEK)
ug/L
ND
10.0
07/01/1100:41
Benzene
ug/L
ND
5.0
07/01/1100:41
Carbon tetrachloride
ug/L
ND
5.0
07/01/11 00:41
Chlorobenzene
ug/L
ND
5.0
07/01/1100:41
Chloroform
ug/L
ND
5.0
07/01/1100*41
Tetrachloroethene
ug/L
ND
5.0
07/01/1100:41
Trichloroethene
ug/L
ND
5.0
07/0111100:41
Vinyl chloride
ug/L
ND
5.0
07/01/11 00:41
1,2-Dichloroethane-d4 (S)
%
98
70-130
07/01/11 00.41
4-Bromofluorobenzene (S)
%
97
70-130
07/01/1100:41
Dibromofluoromethane (S)
%
104
70-130
07/01/1100:41
Toluene-da (S)
%
103
67-135
07/01/1100:41
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
ulavrwI UKr UUN I KUL SAMPLE:
Parameter
628598
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1-Dichloroethene
ug/L
50
52.1
104
70-141
1,2-Dichloroethane
ug/L
50
54.1
108
70-139
1,4-Dichlorobenzene
ug/L
50
52.4
105
70-141
2-Butanone (MEK)
ug/L
100
98.2
98
63-150
Benzene
ug/L
50
49.2
98
70-132
Carbon tetrachloride
ug/L
50
50.0
100
70-150
Chlorobenzene
ug/L
50
54.4
109
70-134
Chloroform
ug/L
50
54.4
109
70-130
Tetrachloroethene
ug/L
50
54.1
108
70-137
Trichloroethene
ug/L
50
52.1
104
70-131
Vinyl chloride
ug/L
50
47.8
96
56-144
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Dibromofluoromethane (S)
%
102
70-130
Toluene-d8 (S)
%
101
67-135
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
1190
Page 17 of 21

acmnaljical
mW-pacelabs.crom
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QG Batch: PMST/4030 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9297122001
SAMPLE DUPLICATE: 628035
9297061013 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 19.5 19.2 1
SAMI'Ll= DUPLICATE: 628036
9297122001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 47.2 47.9 2
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 21

aceAnaIXical
mm..pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: Wood Boiler
Pace Project No.: 9297122
QC Batch: WET/17032
QC Batch Method: EPA 9045
Associated Lab Samples: 9297122001
SAMPLE DUPLICATE: 629698
Parameter Units
pH at 25 Degrees C Sid. Units
Date: 07/15/2011 05:47 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 9045
Analysis Description: 9045 pH
9297061016 Dup
Result Result RPD Qualifiers
5.4 5.4 0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
98001GnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 21

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalyfical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 K;nceyAve. Suite 100
www.pamlabs.com Eden, NC 27283 Asheville, NC 28W Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL
Project: Wood Boiler
Pace Project No.: 9297122
QC Batch: WETA/10057
Analysis Method:
fPA365.1
QC Batch Method: EPA 365.1
Analysis Description:
365.1 Phosphorus, Total '
Associated Lab Samples: 9297122001
METHOD BLANK: 631125
Matrix: Solid
Associated Lab Samples: 9297122001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Phosphorus
mg/kg
ND 2.0 07/08/1115:55
LABORATORY CONTROL SAMPLE:
631126
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Phosphorus
mg/kg
50 54.8
110
90A10
MATRIX SPIKE SAMPLE:
631127
9296826001 Spike
MS
MS % Rec
Parameter
Units
Result Cone.
Result
% Rec Limits Qualifiers
Phosphorus
mg/kg
11.1 127
134
97 90-110
SAMPLE DUPLICATE: 631128
9296826002 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Phosphorus
mg/kg '
10.8 112 4
Date: 07/15/2011 05:47 PM REPORT OF LABORATORY ANALYSIS Page 20 of 21
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

a ,eAnal `ical
wW..pacehbs som
Project: Wood Boiler
Pace Project No.: 9297122
DEFINITIONS
Pace Analytical Services, Inc.
205,East Meadow Road - Suite A
Eden, NC27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Paoe Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
S1 Surrogate recovery outside laboratory control limits (confirmed by re -analysis).
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 21 of 21

Date: P -
. Analyst:
Facility: _M
Calibration
10.0 Buffer / .0k
F /0, 77_
checks are to be within * 6.1 pH units of the standard's true value
PH Analyses
-- -- — I r- c 41111J vI uie sianaara's true value.

Baxter Healthcare o Wood Boiler
Please test the sample(s) for the parameters as listed below.
Send original results to: email: [e-mail]
Send Invoice and copy of results to: email: [e-mail]
Ricky Styles
SaxW Healthcare Purchase Order * 2 z5 o
2850 Old Linville Rd.
Marion, NC 28732
[phone]
email: [e-mail]
Narivamodk l nim MOM.
, 0 e,
q C--7 '(/
Sample 0
Sample
Description
Sample Date(s)
and time sample
collected
Grab or
Composite
Total Metals -
.As, Be, Cd,
Ca, Cr, Cu, Fe,
TCLP Metals
As, Ba, Cd,
Cr, Pb, Hg,
Ignitability,
Reactivity
pH
Corrosivity
Total -Arsenic
Full TCLP
Pb, Mg, Hg,
Se, Ag
Mn, Mo, NI, K,
Se, Ag, Na,
Zn, total
Phosphorus
WB20TR2011
BOTTOM ASH
8-5-11 8:30AM
COMPOSITE
YES
YES
Sample sent to: Pace Analytical Services,
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Chain of Custody
Project Manager: Tom Williams
9800 Kincey Avenue, Suits 10(
Huntersville, NO 28078
(704) 875 - 9092 ext. 233
10z

aceAnaIX cal
www.pacelabs.0 m
August 30, 2011
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
RE: Project: Bottom Ash 815/11
Pace Project No.: 9299874
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on August 05, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards, where applicable, unless otherwise narrated in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
/'2-' -`
Tom Williams
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 11

aceAnalidical
www.pacelabs.com
Pace Analytical Sarvicez, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Project: Bottom Ash 8/5/11
Pace Project No.: 9299874
Charlotte C®Mcation IDs
9800 Kinsey Ave. Ste 100, Huntersville, NC 28078
Connecticut Certification #: PH-0104
North Carolina Drinking Water Certification #: 37706
Flodda/NELAP Certification #: E87627
North Carolina Field Services Certification ##: 5342
North Carolina Wastewater Certification #: 12
Kentucky UST Certification 0. 84
Louisiana DHH Drinking Water # LA 100031
South Carolina Certification #k. 9NO6001
South Carolina Drinking Water Cert. #: 99006003
West Virginia Certification 8. 357
VrginiafVELAP Certification 0: 460144
Virginia Drinking Water Certification #: 00213
Aahavillo Certiirucation IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification 8: E87648
Massachusetts Certification ##: M-NCO30
North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia Certification #: 00072
West Virginia Certification #: 356
Virgina/VELAP Certification 0: 460147
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
witlmt the written consent of Pace Analytical Services, Inc..
Paco Analytical Semiceu, Inc.
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
(/04)875-9092
Page 2 of 11

cal
2 5 East Meadow Roads -Suite A Pace AnalyticalServices,
RiversideDr.Dr. Pace9800 KKfteyA�Suite,100
auuftlXkalwrrw.pacele6s.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
acl [phone] [phone] [phone]
SAMPLE ANALYTE COUNT
Project: Bottom Ash 815111
Pace Project No.: 9299874
Lab ID Sample ID Wathad
Analysts
Analyt es
Rolgarbd
Laboratory
9299874001 W02QTR2011 EPA 6010
SHB
17
PASI-A
EPA 6010
SHB
7
PASI-A
EPA7470
JMW
1
PASI-A
ASTM D2974-87
TNM
1
PASI-C
REPORT OF LABORATORY ANALYSIS Page 3 of 11
This report shall not ba reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

ace,nali6cal o
www.paWabs com
Project: Bottom Ash 8/5111
Pace Project No.: 9299874
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NQ 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9600 Kinosy Ave. Suits 100
Huntersville, NC 28078
[phone]
Sample: W82QTR2011 Lab ID: SM876001 Collected: 08/05/11 08:30 Received: 08/05/11 17:09 Matrix: S0110
Resuf6a reparbd on a 'airy-vyeggt' bts1,s
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
12.1 mg/kg
0.38
1
08/15/11 12:40
08/16/11 21:07
744038-2
Barium
1530 mg/kg
3.8
10
08/15/11 12:40
08/17/11 21:37
7440-39-3
Cadmium
1.9 mg/kg
0.077
1
08/15/11 12:40
08/16/11 21:07
7440-43-9
Calcium
59M mg/kg
76.6
10
08/15/11 12:40
08/17/11 21:37
7440-70-2
Chromium
32.6 mg/kg
0.38
1
08/15/11 12:40
08116/1121:07
7440-47-3
Copper
97.2 mg/kg
0.38
1
08/15/11 12:40
08/1611121:07
7440-50-8
Iron
136M mg/kg
76.6
10
08/15/11 12:40
08117/1121:37
7439-893
Lead
318 mg/k9
0.38
1
08115/11 12:40
08/16/11 21:07
7439-92-1
Magnesium
9480 mg/kg
76.6
10
08/15/11 12:40
08117/1121:37
7439-95-4
Manganese
2000 mg/kg
3.8
10
08/15/11 12.40
08/17/11 21:37
7439-96-5
Molybdenum
1.1 mg/kg
0.38
1
08/15/11 12:40
08/16/11 21:07
7439-98-7
Nickel
22.1 mg/kg
0.38
1
08/15/11 12.40
08/16/1121:07
7440-02-0
Potassium
19000 mg/kg
3830
10
08/15/11 12,40
08/17/11 21:37
7440-09-7
Selenium
ND mg/kg
0.77
1
08/15/11 12:40
081ISJll 21:07
7782-49-2
Silver
0.93 mg/kg
0.38
1
08/15/11 12:40
08/16/11 21:07
7440-22-4
Sodium
11400 mg/kg
3830
10
08/15/11 12,40
08/17/11 21:37
7440-23-5
Zinc
90.5 mg/kg
0.77
1
08/15/11 12.40
08/16/11 21:07
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 08/18/11 18:50
Arsenic
ND mg/L
0.025
1
08/19/11 19:30
08/22/11 14:32
7440-38-2
Barium
6.4 mg/L
0.50
1
08/19/11 19:30
08/22/11 14:32
7440-39-3
Cadmium
ND mg/L
0:0050
1
08/19/11 19:30
081=11 14:32
7440-43-9
Chromium
ND mg/L
0.025
1
08/19/11 19:30
08/22/11 14:32
7440-47-3
Lead
ND mg/L
0.025
1
08/19/11 19:30
08/22/11 14:32
7439-92-1
Selenium
ND mg/L
0.10
1
08/19/11 19:30
08/22/11 14:32
7782.49-2
Silver
ND mg/L
0.025
1
08/19/11 19:30
08/22/11 14:32
7440-22-4
7470 lillrarcuM TCLP
Analytical Method: EPA7470 Preparation Method: EPA7470
Leachate Method/Date: EPA 1311; 08/18/11 18:50
Mercury
ND ug/L
0.20
1
08/22/11 11:20
08/22/11 15:17
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
2.5 °%
0.10
1
08/09/11 14:23
Date: 08/30/2011 04:03 PM REPORT OF LABORATORY ANALYSIS Page 4 of 11
This report shall not be reproduced, except in full,
without the written consent of Pace Analytcal Services, Inc..

aceAnalytical
www.pac&Mbs.com
Project: Bottom Ash 8/5/11
Pace Project No.: 9299874
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/8902 Analysis Method: EPA6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 9299874001
METHOD BLANK: 647569
Associated Lab Samples:
Parameter •
9299874001
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
Arsenic
mg/kkg
ND
0.60
08/16/1120:26
Barium
mg/kg
ND
0.50
0811611120:26
Cadmium
mg/kg
ND
0.10
08/1611120:26
Calcium
mg/kg
ND
10.0
0811611120:26
Chromium
mg/kg
ND
0.50
0811611120:26
Copper
mg/kg
ND
0.50
08/16/1120:26
Iron
mg/kg
ND
10.0
08/16/1120:26
Lead
mg/kg
ND
0.50
08/16/1120:26
Magnesium
mg/kg
ND
10.0
08116/1120:26
Manganese
mg/kg
ND
0.50
08/16/1120:26
Molybdenum
mg/kg
ND
0.50
08/1611120:26
Nickel
mg/kg
ND
0.50
0811611120:26
Potassium
mg/kg
ND
500
08/1611120:26
Selenium
mg/kg
ND
1.0
08/16/1120:26
Silver
mg/kg
ND
0.50
08116/1120:26
Sodium
mg/kg
ND
500
08116/1120:26
Zinc
mg/kg
ND
1.0
08/16/1120:26
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
647570
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Arsenic
mg/kg
50
50.9
102
80-120
Barium
mg/kg
50
50.0
100
80-120
Cadmium
mg/kg
50
51.3
103
80-120
Calcium
mg/kg
500
517
103
80-120
Chromium
mg/kg
50
52.4
105
80-120
Copper
mg/kg
50
49.2
98
80-120
Iron
mg/kg
500
500
100
80-120
Lead
mg/kg
50
51.9
104
80-120
Magnesium
mg/kg
500
508
102
80-120
Manganese
mg/kg
50
51.1
102
80-120
Molybdenum
mg/kg
50
49.6
99
80-120
Nickel
mg/kg
50
51.7
103
80-120
Potassium
mg/kg
500
460J
92
80-120
Selenium
mg/kg
50
51.4
103
80-120
Silver
mglkg
25
25.4
102
80-120
Sodium
mg/kg
500
509
102
80-120
Zinc
mg/kg
50
52.3
105
80-120
Pace Analytical Services, Inc.
9800 KinoeyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Date: 08/30/2011 04:03 PM REPORT OF LABORATORY ANALYSIS Page 5 of 11
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
wwwpacalabscam
Project: Bottom Ash 815/11
Pace Project No.: 9299874
Pace Analytical Services, Inc.
205 East Meadow Road- Suite A.
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave.. Sub 100
Huntersvilie, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
647571
Units
9299989004
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
500 ug/g
42.4
1680
2797
75-125 M6
Barium
mg/kg
177 ug/g
42.4
68.5
-255
75-125 M1
Cadmium
mglkg
30.3 ugig
42.4
45.0
35
75-125 Ml
Calcium
mg/kg
86000 ug/g
424
37700
-11418
75-125 M6
Chromium
mg/kg
128 ug/g
42.4
47.6
-189
75-125 M1
Copper
mglkg
14.5 ug/g
42.4
54.2
94
75-125
Iron
mg/kg
267 ug/g
424
575
73
75-125 M1
Lead
mg/kg
1660 ug/g
42.4
236
-3361
75-125 ,M1
Magnesium
mg/kg
2500 ug/g
424
812
-398
75-125 M1
Manganese
mg/kg
30.5 ug/g
42.4
52.7
52
75-125 M1
Molybdenum
mg/kg
1.01 ug/g
42.4
44.7
103
75-125
Nickel
mg/kg
5.27 ug/g
42.4
50.3
106
75-125
Potassium
mglkg
ND
424
1040
211
75-125 MI
Selenium
mg/kg
ND
42.4
54.1
127
75-125 M1
Silver
mg/kg
ND
21.2
23.8
111
75-125
Sodium
mg/kg
524 ug/g
424
1590
252
75-125 M1
Zinc
mg/kg
47.2 ug/g
42.4
237
449
75-125 M1
SAMPLE DUPLICATE: 647572
92100024062
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Arsenic
mg/kg
2.6
1.3
68 D8 '
Barium
mglkg
73.4
84.2
14
Cadmium
mg/kg
ND
0.12
Calcium
mg/kg
576
642
11
Chromium
mg/kg
13.5
14.3
5
Copper
mglkg
9.1
10.2
11
Iron
mg/kg
9540
10100
6
Lead
mglkg
10.4
11.3
9
Magnesium
mg/kg
2030
2180
7
Manganese
mg1kg
398
461
15
Molybdenum
mg/kg
ND
.21J
Nickel
mg/kg
5.2
5.9
14
Potassium
mg/kg
1870
2090
11
Selenium
mg/kg
ND
1J
Silver
mg/kg
ND
.082J
Sodium
mglkg
ND
99.4J
Zinc
mglkg
70.0
73.8
5
Date: 08/30/201104:03 PM REPORT OF LABORATORY ANALYSIS Page 6 of 11
This report shall not be reproduced, except in full,
wittwut the written consent of Pace Analytical Services, Inc..

VeAnal,�ical
WWW.pacelabs.com
.Project:. Bottom Ash815111
Pace Project No.: 9299874
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace AnalyticalServices, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/8939 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET TCLP
Associated Lab Samples: 9299874001
METHOD BLANK: 650596
Matrix: Water
Associated Lab Samples:
9299874001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.025
08/22/1114:25
Barium
mg/L
ND
0.50
08/22/1114:25
Cadmium
mg/L
ND
0.0050
0812211114:25
Chromium
mg/L
ND
0.025
08/2211114:25
Lead
mg1L
ND
0.025
08/2211114:25
Selenium
mg/L
ND
0.10
08/22J1114:25
Silver
mg/L
ND
0.025
08/2211114:25
Pace Analytical Services, Inca
9800 IGnceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
650597
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/L
2.5
2.6
105
80-120
Barium
mg/L
2.5
2A
97
80-120
Cadmium
mg/L
2.5
2A
95
80-120
Chromium
mg/L
2.5
2.4
95
80-120
Lead
mg/L
2.5
2.2
88
80-120
Selenium
mg/L
2.5
2.8
112
80-120
Silver
mg/L
1.2
1.3
107
80-120
MATRIX SPIKE SAMPLE:
Parameter
650598
Units
9299874001
Result
Spike
Conc.
MS
Result
MS
% Rec
°k Rec
Limits Qualifiers
Arsenic
mg/L
ND
2.5
2.6
103
75-125
Barium
mg/L
6A
2.5
8.2
70
75-125 M1
Cadmium
mg/L
ND
2.5
2.4
95
75-125
Chromium
mg/L
ND
2.5
2.4
94
75-125
Lead
mg/L
ND
2.5
2.3
89
75-125
Selenium
mg/L
ND
2.5
2.7
108
75-125
Silver
mg/L
ND
1.2
1.3
101
75-125
SAMPLE DUPLICATE: 650599
9299929001
Dup
Parameter
Units
Result
Result RPD Qualifiers.
Arsenic
mg/L
ND
ND
Barium
mg/L
0.68
0.68 1
Cadmium
mg/L
ND
ND
Chromium
mg/L
ND
ND
Lead
mg/L
ND
ND
Date: 08/30/2011 04:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
vvi4hout the written consent of Pace Analytical Services, Inc..
Page 7 of 11

aceAinaly6cal
mmn.pacefab&C=
Project: Bottom Ash 815/11
Pace Project No.: 9299874
SAMPLE DUPLICATE: 650599
Parameter
Selenium
Silver
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)62M921
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
9299929001
Units Result
mg/L ND
mg/L ND
Dup
Result RPD Qualifiers
ND
ND
Puce Analytical Services, Inc.
gao0 lQncay Ave. Suite 100
Huntersville, NC 28078
[phone]
Date: 08130/201104:03 PM REPORT OF LABORATORY ANALYSIS Page 8 of 11
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

YaneAnalittical
wmpacdabscom
Project: Bottom Ash 8/5/11
Pace Project No.: 9299874
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP/3700 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 9299874001
METHOD BLANK. 650891 Matrix: Water
Associated Lab Samples: 9299874001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 08/2211115:12
LABORATORY CONTROL SAMPLE: 650892
Parameter Units
Mercury
ug/L
Pace Analytical Services,. Inc.
9800 Kincsy Ave. Suite 100
Huntersville, NC 28078
(704)8754092
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
2.5 2.4 94 80-120
MATRIX SPIKE SAMPLE: 650893
9299874001 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
Mercury ug/L ND 2.5 1.7 69 75-125 M1
SAMPLE DUPLICATE: 650894
Parameter
Mercury
9299029001 Dup
Units Result Result RPD Qualifiers
ug/L ND ND
Date: 08/30/2011 04:03PM REPORT OF LABORATORY ANALYSIS Page 9 of 11
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

a
aceAnalytical0
www.pace4abs.com
Project: Bottom Ash 8/5/11
Pace Project No.: 9299874
QC Batch: PMST/4113
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 9299874001
SAMPLE DUPLICATE: 644830
Pararfieter
Percent Moisture OA
SAMPLE DUPLICATE: 644831
Parameter
Percent Moisture %
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
9299794008 Dup
Units Result Result RPD Qualifiers
12.3 12.7 3
9299932004 Dup
Units Result Result RPD Qualifiers
22.0 21.4 3
Pace Analytical Services, Inc.
9800lCncyAve. Suite 100
Huntersville, NC 28078
[phone]
Date: 08/30/2011 04:03 PM REPORT OF LABORATORY ANALYSIS Page 10 of ll
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

ucueftlXkal
www.pacelabacom
Project: Bottom Ash 8/5111
Pace Project No.: 9299874
DEFINITIOWS
Pace Analytical Services, Inc.
205.East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 MncsyAve. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method. Detection Limit.
S - Surrogate
1,24)iphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica, Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nkrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PAST -A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services Charlotte
ANALVTE QUALIFIERS
D8 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory.control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
MB Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
[phone]
Date: 08/30/201104:03 PM REPORT OF LABORATORY ANALYSIS Page 11 of 11
This report shah not be reproduced, except in full,
- without the written consent of Pace Analytical Services, Inc..

Baader Healthcare - Wood Boiler
Please test the sample(s) for the parameters as listed below.
Send original results to: email: [e-mail]
Send invoice and copy of results to: email: [e-mail]
Ricky Styles
Baxter Healthcare Purchase Order #
2859 Old Linville Rd.
Marion, NC 28752
[phone]
email: [e-mail]
Requested Due Date:
33501
Sample #
Sample
Sample Date(s)
Grab or
Total Metals -
TCLP Metals
Ignitability,
pH
Total -Arsenic
Full TCLP
Description
and time sample
Composite
As, Ba, Cd,
As, Be, Cd,
Reactivity
Corrosivity
collected
Ca, Cr, Cu, Fe,
Cr, Pb, Hg,
Pb, Mg, Hg,
Se, Ag
Mn, Mo, Ni, K,
Se, Ag, Na,
Zn, total
Phosphorus
WBSP92
POND ASH
9-1-11 1:05PM
COMPOSITE
YES
YES
YES
Sample sent to: Pace Analytical Services,
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Chain of Custody
Project Manager: Tom Williams
9800 Kincey Avenue, Suite 10(
Huntersville, NC 28078
(704) 875 - 9092 ext. 233

IeAnalytical
WWW.Pac W&r0m
September 15, 2011
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
Pace Anslptical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
RE: Project: Wood Boiler
Pace Project No.: 92101567
Psce Analytical Services. Inc.
=5 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Serolces, Inc.
980o 1Qnc eyAve. Suite 100
Huntersvil►e, NC 28078
[phone]
Dear Mr. Styles:
Enclosed are the analytical results for included in this eporved t the laboratory on Results reported hereinmconform to the
The results relate only to the samples Incl
plicable, unless otherwise narrated In the body of the report.
most current Ttdl standards, where ap
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
/' , C. '/'� �
Tom Williams
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
wfthout the written consent of Pace Analytical Services,. Inc..
Page 1 of 14

aceAnaifical
wwwpaoelabscom
Project: Wood Boiler
Pace Project No.: 92101567
Pace Analytical ServtCSS, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification V. 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification V. 99006001
South Carolina Drinking Water Cert. V. 99=003
Virginia Drinking Water Certification #: 00213
Asheville Cort ficaUon IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification#: E87648
Massachusetts Certification #s M-NC030
North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
[phone]
Pace Analyticat SOMICes, Inc.
2225 Riverside Dr.
Asheville, NC 28804
CERTIFICATIONS
[phone]
Connecticut Certification V. PH-0104
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DHH Drinking Water# LA 100031
West Virginia Certification #: 357
Vrrginia/VELAP Certification #: 460144
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia Certification #: W072
Vo-st Virginia Certification M 356
Virgina/VELAP Certification #: 460147
Pace AnalOCal 59WWW, Inc.
9800 Kincay Ave: SUim 100
Huntersville, NC 28078
[phone]
REPORT OF LABORATORY ANALYSIS Page 2 of 14
This report shall not be reProduOed- exo* in full,
without the written consent of Paoe Analytical Services, Inc..

aceAnalytical
www.pacelabs com
Proles: Wood Boiler
Pace Project No.: 92101567
PaeeAnsly MI Services, Inc.
205 East meadow Road - Suite A
Eden, NO 27288
[phone]
Pace AnsWcal Services, Inc.
2225 Riverside Dr.
Asheville, NO 26804
[phone]
SAMPLE ANALYTE COUNT
Pace Anatytical Secvlcea, Inc.
9800 lQncW Ave. Suite 100
Huntersville, NO 28078
[phone]
Analytas
6E'l dwd
Analysts
Repofmad
Labofatory
Lab ID Sample 0D
92101967001 bVSSP92 Pond bash EPA 6010
SHB
17
PASI-A
EPA6010
SHB
7
PASI-A
EPA7470
JMW
1
PASI-A
EPA7471
JMW
1
PASI-A
ASTNI D2974-87
JEA
1
PASI-C
EPA 9045
EWS
1
PASI-A
EPA365.1
JDA
1
PASI-A
REPORT OF LABORATORYANALYSIS Page 3 of 14
This repot shall not W reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

acoAnalytical
www.pamlabs.com
pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Ana6btic81 Services. In'
2225 RwraWe Dr.
Asheville, NC 28804
[phone]
ANALYTICAL {RESULTS
Pace Anatylical Services, Inc.
9800 KinceyAve. Suite 100
Huntersvills, NC 28078
[phone]
Project: -Wood Boiler
Pace Project No.: 92101567
Sample: Pr ect No.: 92101ond 6 LabID: 92101567001 Collected: 09/01/11 13:05 Received: 09/01/11 14:22 Matrix: Solid
Resuler reponed orr a 'dry -WOW' balls
Report Limit DF prepared Analyzed GAS No. Qual
Parameters Results Units
Ism MET ICP
Arsenic
Barium
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Zinc
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, TCLP
Mercury
7471 Mercury
Mercury
Percent MMoiature
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
Date: 09/15/2011 11:40 AM
Analytical Method: EPA6010 Preparation Method: EPA3050
09/07/1109:20
09107/1123.25 7440-38-2
09/07/1109:20
09/07/1123:25 7440-39-3
09/07/1109:20
09/0711123:25 7440-43-9
pg/07/1109.20
09/08/1113:13 7440-70-2
09/07/1109:20
09107/1123:25 7440-47-3
09/07/1109:20
09/07/1123:25 7440-50-8
09/07/1109:20
0910711123.25 743"9-6
09/07/1109:20
09/0711123:25 7439-92-1
09/07/1109:20
0910711123:25 7439-95-4
09107/1109:20
09/07/1123:25 7439-98-5
09/07/1109:20
09107/1123:25 7439-98-7
09/07/11 09:20
09107/1123:25 7440-02-0
09/07l1109:20
()910811113:13 7440-09-7
0910711109:20
0910711123:25 7782-49-2
09/0711109:20
09107/1123:25 7440-22-4
09/07/1109:20
0910711123:25 7440-23-5
09/07/1109:20
0910711123:25 7440-06-6
16.6 mg/kg
1.1
1
1340 mglkg
1.1
1
2.5 nt kg
0.23
1
75200 mg/kg
229
10
22.1 mg/kg
1.1
1
97.5 mglkg
1.1
1
8800 mg/kg
22.9
1
23.6 mg/kg
1.1
1
12200 mg/kg
22.9
1
2280 mg/kg
1.1
1
ND mg/kg
1.1
1
13.3 mg/kg
1.1
1
20400 �g
11500
10
ND mg/kq
2.3
1
1.2 mglkg
1.1
1
15800 mg/kg
1150
1
225 mg/kg
2.3
1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 09/09/11 15:40
ND mg/L
0.025 1
0.96 m91L
0.50 1
0.023 mg/L
0.0050 1
ND mg/L
0.025 1
ND mg/L
0.025 1
ND mg/L
0.10 1
ND mg/L
0.025 1
0911211109:10
09/1311113:05
7440-38-2
0911211109:10
09/12/11 18:10
7440-39-3
0911211109:10
0911211118:10
7440-43-9
()911211109:10
09/12111 18:10
7440-47-3
0911211109:10
09/1211118:10
7439-92-1
09,12,1109:10
09112/1118:10
7782-49-2
09/1211109:10
0911211118:10
7440-22.4
Analytical Method: EPA7470 Preparation Method: EPA7470
Leachate Method/Date: EPA 1311; 09/09/11 15:40
ND ug/L 0.20 1 09/12/11 12:00 09/12/11 15:33 7439-97-6
Analytical Method: EPA7471 Preparation Method: EPA7471
0.015 mg/kg 0.011 1 09/08/11 14.65 U9/09/11 12:57 7439-97-6
Analytical Method: ASTM D2974-87
57.2 % 0.10 1 09108/11 14:52
Analytical Method: EPA 9045
0.10 1 09114/11 13:45
8.7 Std. Units
Analytical Method: EPA 365.1
09110111 12:29 7723-14-0
3080 mg/kg 88.3 20
REPORT OF LABORATORY ANALYSIS
This report sMH not be reproduces, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 14

Pace Analytical Services, Inc. Pace Anslytical Services, Inc. Pam Anelydca1 SeevicM, Inc.
®
205 East Meadow Road' Suite 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aceAnalical
Eden, NC 27288 Asheville, NC 28804 Huntemville, NC 28078
we+w.pacOaftcan [phone] [phone] [phone]
QUALITY COMTROL DATA
Project: Wood Boiler
Pace Project No.: 92101567
QC Batch: MPRP19015
Analysis Method:
EPA6010
QC Batch Method: EPA 3050
Analysis Description:
6010
MET
Associated Lab Samples: 92101567001
METHOD BLANK: 656477
Matrix: Solid
Associated Lab Samples: 92101567001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
mg/kg
ND
0.50
09/07/1122:18
Arsenic
mglkg
ND
0.50
0910711122:18
Barium
mglkg
ND
0.10
0910711122:18
Cadmium
,
mglkg
ND
10.0
09/07/11 22:18
Calcium
mglkg
ND
0.50
0910711122:18
Chromium
mglkg
ND
0.50
()910711122:18
Copper
mglkg
ND
10.0
0910711122:18
Iron
mglkg
ND
0.50
09107/1122:18
Lead
mglkg
ND
10.0
09107/1122:18
Magnesium
mg/kg
ND
0.50
0910711122:18
Manganese
mglkg
ND
0.60
09107/1122:18
Molybdenum
mglkg
ND
0.50
0910711122:18
Nickel
mg/kg
ND
500
0910711122:18
Potassium
mglkg
ND
1.0
09/07/1122:i8
Selenium
mg/kg
ND
0.50
09107/1122:18
Silver
mglkg
ND
500
0910711122:18
Sodium
mglkg
ND
1.0
09107/1122:18
Zinc
LABORATORY CONTROL SAMPLE:
656478
Spike
LCS
LCS
% Rec
Units
Conc.
Result
% Rec
Limits Qualifiers
Parameter
mgllkyy
50
50.2
100
80-120
Arsenic
mglkg
50
50.3
101
80-120
Barium
mglkg
50
49.0
98
80-120
Cadmium
mg/kg
00
550
492
98
80-120
Calcium
mg/kg
4
94
80-120
Chromium
mg/l�y
50
101
80-120
Copper
mglkg
500
99
4 99
100
80-120
Iron
mglkg
50
50.7
101
80-120
Lead
mglkg
500
528
106
80-120
Magnesium
mglkg50
48.3
97
80-120
Manganese
�g
50
47.5
95
80-120
Molybderwm
50
49.1
98
80-120
Nickel
mglkg
500
500
100
80-120
Potassium
mglkg
50
49.7
99
80-120
Selenium
mglkg
25
24.2
97
80-120
Silver
mglkg
500
531
106
80-120
Sodium
mglkg
50
49.0
98
80-120
Zinc
mg/kg
Page 5 of 14
Date: 09115/2011 11.40AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

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yoAnalical
wwPaaxlabacom
Project: Wood Boiler
Pace Project No.: 92101567
Pace Analytical Services, Inc.
205 East Meadow Road = Suite A
Eden, NC 27288
[phone]
Pe a Analytical Services, Inc.
2225 Riversids Dr.
Asheville, NC 28804
[phone]
@UALIW CONTROL DATA
QC Batch: MPRP/9034 Analysis Method: EPA6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92101567001
METHOD BLANK: 658363 Matrix Water
Associated Lab Samples: 92101667001
Blank
Reporting
Parameter
Un'Its
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.025
09/1311112:05
Barium
mg/L
ND
0.50
09/12/1116:28
Cadmium
mg&
ND
0.0060
09/12111.16:28
Chromium
mg/L
ND
0.025
0911211116:28
Lead
mg/L
ND
0.025
0911211116:28
Selenium
mg/L
ND
0.10
09/1211116:28
Silver
mg/L
ND
0.025
0911211116:28
LABORATORY CONTROL SAMPLE: 65M
PaceAnalydeal Service:, Inc.
8800 Mncey Ave. Suits 100
Huntersvills, NC 28078
(704)875.M2
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Arsenic
mg/L
2.5
2.7
106
80-120
Barium
mg/L
2.5
2.2
89-
_ 80-120
Cadmium
m91L
2.5
2.4
97
80-120
Chromium
mg/L
2.5
2.4
97
80-120
Lead
mg/L
2.5
2.2
89
80-120
Selenium
mg/L
2.5
2.6
105
80-120
Silver
mg/L
1.2
1.3
104
80-120
MATRIX SPIKE SAMPLE:
Parameter
658365
Units
92101581001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/L
ND
2.5
2.6
106
75-125
Barium
mg/L
1.2
2.5
3.2
81
75-125
Cadmium
mg/L
ND
2.5
2A
95
75-125
Chromium
mg/L
ND
2.6
2A
94
75-125
Lead
mg1L
0.075
2.5
2.3
88
75-125 .
Selenium
mg/L
ND
2.5
2.6
103
75-125
Silver
mg/L
ND
1.2
1.2
100
75-125
SAMPLE DUPLICATE: 658366
92101510MI
Dup
Parameter
Units
Result
Result RPD Qualifiers
Arsenic
mg/L
ND
ND
Barium
mg/L
ND
.26J
Cadmium
mg/L
ND
ND
Chromium
mg/L
ND
.015.1
Lead
mg/L
ND
ND
Date: 09/15/2011 11:40 AM REPORT OF LABORATORY ANALYSIS Page 7 of 14
This report shall not be reproduced, except in full,
without tlta written consent of Pace Analytical Services, Inc..

&qCeAnalytica
wmpacelab&com
Project: Wood Boiler
Pam Project No.: 92101567
SAMPLE DUPLICATE. 65M6
Parameter
Selenium
Silver
Pace Analy MI Smrvicss;, Inc.
205 East Meadow Road • Suite A
Eden, NC 27288
[phone]
Pace Analytdcal Semlcss, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
92101510001
Units Result
mg/L ND
mg1L ND
Dup
Result
.0691
.00191
RPD Qualifiers
Pace AnaWdcal Semices, Inc.
98001GnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Date: 09115I2011 11.40 AM REPORT OF LABORATORY ANALYMS Page 8 of 14
This report shall not be reproduced, except in full,
vftout the written consent of Paw Analytical ServiCea, Inc..

aceAnalytkal
www.pacelabscam
Project: Wood Boiler
Pace Project No.: 92101567
Pare Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)6235921
Pare Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP13731 Analysis Method: EPA 7470
QC Batch Method: EPA7470 Analysis Description: 7470 MercuryTCLP
Associated Lab Samples: 92101567001
METHOD BLANK: 658410 Matrix. Water
Associated Lab Samples: 92101567001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 09/12/1114:59
Pace Analytical Services, Inc.
9800 KJnM Ave. Suite 100
Huntersvilie, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 658411
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.4 96 80-120
MATRIX SPIKE SAMPLE: 658412
92101581001 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
Mercury ug/L ND 2.5 1.9 74 75-125 M1
SAMPLE DUPLICATE: 658413
92101510001 Dup
Parameter Units Result Result RPD Qualifiers
Mercury ug/L ND ND
Date: 09/15/2011 11:40 AM REPORT OF LABORATORY ANALYSIS Page 9 of 14
This report shall not be reproduced, except in foil,
without the written consent of Pace Analytical Services, Inc..

IGI(AeAnaly ical
www.paw4absoom
Project Wood Boiler
Pace Project No.: 92101567
Pace Analytica+l Services, Inc. Pace Analytical Services, Inc.
205 Fast Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone]. [phone]
QC Batch: MERP/3727
QC Batch Method: EPA 7471
Associated Lab Samples: 92101567001
METHOD BLANK: 657275
Associated Lab Samples: 92101567001
Parameter Units.
Mercury
mg/kg
QUALITY CONTROL DATA
Analysis Method`. EPA 7471
Analysis Description: 7471 Mercury
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0050 0910911112:39
Pace Analytical SerVION, Inc.
98001GncsyAve. Suiba 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 657276
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury mglkg .067 0.058 87 80-120
MATRIX SPIKE SAMPLE:
657277
92101586011
Spike
MS
MS
% Rec
Parameter
Units
Result
Cone.
Result
% Rec
Limits Qualifiers
Mercury
mg/kg
0.016
.069
0.083
96
75-125
MATRIX SPIKE SAMPLE:
657279
92101764002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Mercury
mgtkg
0.039 ug/g
.067
0.11
103
76-125
SAMPLE DUPLICATE: 657278
92101708001 Dup
Parameter Units Result Result RPD Qualifiers
Mercury mg/kg ND 0.010
SAMPLE DUPLICATE: 657286
92101764003 Dup
Parameter Units Result Result RPD Qualifiers
Memory mg*g 0.017 ug/g 0.014 18
Date: 09/15/2011 11:40 AAA REPORT OF LABORATORY ANALYSIS Page 10 of 14
This report shall not be reproduced, except in full,
without the wxitlen consent of Pace Analytical Services, Inc..

aceAnalytical
tympacelsbswm
Project: Wood Boiler
Pace Projed No.: 92101567
Pace Anaty0cat SWIM, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
pace Analyt6cal Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: PMST/4172 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92101667001
SAMPLE DUPLICATE: 657081
92101528001 Dup
Parameter Units - Result Result RPD Qualifiers
Percent Moisture % 77.1 77.5 1
SAMPLE DUPLICATE: 657082
92101678022 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 18.2 18.1 1
Date: 09/15/2011 11:40 AM REPORT OF LABORATORY ANALYSIS
This report shan not be mprodumd, exoept in fun,
vrilhout the written consent of Pace Analytical Services, Inc..
Pace AnaWWI Swwvl=- Inc -
WO Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of14

acoAnaliltical
wmpacelabscom
Project: Wood Boiler
Pace Project No.: 92101567
Pace Anah llcal Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Se-Im, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WET/17886 Analysis Method: EPA 9048
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92101567001
SAMPLE DUPLICATE: 659306
92101581001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Dagrees C Sid. Units 6.5 6.5 0
Pace Analytical Services, Inc.
9800 l(inceyAve. Suite 100
Huntersvills, NC 28078
[phone]
Date: 09/15/2011 11:40 AM REPORT OF LABORATORY ANALYSIS Page 12 of 14
This report shall not be reprodueed, except in full,
without the written consent of Paoe Analytical Services, Inc..

aceAnalytical
W"..'.RM ftC0M
Project: Wood Boiler
Pace Project No.: 92101567
Pace Analytical Servioea, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytccal SGrvkccs, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/10512 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92101567001
METHOD BLANK: 657744
Associated Lab Samples: 92101567001
Matrix: Solid
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mglk9 ND 2.0 09/1011111:57
LA130RATORY CONTROL. SAMPLE: 657745
Pace AnaVdcol Services. Inc.
9800 [Oncey Ave. Surb 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec limits Qualifiers
Phosphorus mglkg 50 52.2 104 90-110
MATRIX SPIKE SAMPLE: 657746
92101667001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 21.5 64.2 78.7 89 90-110 Mi
SAMPLE DUPLICATE: 667747
92101667002 Dup
Parameter Units Result Result RPD Qualifiers
Phosphorus mg/trq 94.7 93.0 2
Date: 09/15/2011 11:40 AM REPORT OF LABORATORY ANALYSIS Page 13 of 14
This report shag not be reproduced, except in full,
without fhe written consent of Pace Analytical Services. Inc..

Analytical"
Wmpacelabs.cam
Project: Wood Boiler
Pace Project No.: 92101567
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suits
Eden, NC 27288
.[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Rivarside Dr.
Asheville, NC 28804
[phone]
Paca Analytical Services, Inc.
9800IGnoayAve. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to Calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spine (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
WNitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anslytes.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
ANALVTE QUALIFIERS
M7 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
[phone]
Date: 09/15/2011 11.40AM REPORT OF LABORATORYAAIALYSIS Page 14 of 14
This report shall not be reproduced, except in full,.
without the Voitlen consent of Pace Analytical Servioes, Inc..

Date:
Facility:
Time 4.0
*PH buffer checks are to i
Analyst: ��'
Calibration
Buffer 7.0a Comments
* 0.1 pH units of
PH Analyses
true value
-- - w. OLd►Iaafv�s true value.

Baxter Healthcare - Wood Boiler
Please test the sample(s) for the parameters as listed below.
Send original results to: email: [e-mail]
Send invoice and copy of results to: Ricky Styles email: [e-mail]
Baxter Healthcare P
2859-Old Linville Rd. urChase order # 37238
Marion, NC 28752
[phone]
email: [e-mail]
luested Due bate:
Sample # Sample Fand
ple Date(s) Grab or
Descriptionime sample Composite
ollected
W6121 �A I ASH I 12-15-11
10:3 AM I COMPOSITE
W612156 I ASH I 12-15-11
10:35AM I COMPOSITE
Sample sent to: Pace Analytical Services,
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Chain of Custody
Total MetalsFAs,
etals Ignitability, pH As, Ba, Cd,, Cd, Reactivity Corrosivity Total -Arsenic Full TCLPCa, Cr, Cu, F, Hg,Pb, Mg, Hg,AgMn, Mo, Ni, K
Se, Ag, Na,
Zn, total
Phosphorus
YES
YES I I YES I YES
Project Manager: Tom Williams
9800 Kincey Avenue, Suite 10C
Huntersville, NC 28078
(704) 875 - 9092 ext. 233

ceAnalXical
www.pacele &CM
January 19, 2012
Mr. Ricky Styles
Baxter Healthcare
' 2859 Old. Linville Road
Marion, NC 28752
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
RE: Project: WOOD BOILER 12/15
Pace Project No.: 92108538
Dear Mr. Styles:
Pace Analytical Services,'Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 15, 2011.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted.
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tom Williams
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 12

,�awnalyticalo
www.pacelabs.cam
Project: WOOD BOILER 12115
Pace Project No.: 92108538
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Charlotte Certification IDs
9800 KinceyAve. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Virginia Drinking Water Certification #: 00213
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
CERTIFICATIONS
[phone]
Connecticut Certification #: PH-0104
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DHH Drinking Water # LA 100031
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460144
South Carolina Certification #: 99030001
Virginia Certification #: 00072
West Virginia Certification #: 356
Virgina/VELAP Certification #: 460147
REPORT OF LABORATORY ANALYSIS
This report shall not 6e reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 12

.Analj&al4
www.Pacalabs.com
Project: WOOD BOILER 12/15
Pace Project No.: 92108538
Pace Analytical Services, Inc.
206 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COURT
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Repotted
Laboratory
92108538001 WB1215A EPA 6010
JMW
17
PASI-A
EPA 7471
SHB
1
PASI-A
ASTM D2974-87
TNM
1
PASI-C
EPA 365.1
JDA
1
PASI-A
92108538002 WB12158 EPA 6010
JMW
17
PASI-A
EPA7471
SHB
1
PASI-A
ASTM D2974-87
TNM
1
PASI-C
EPA9045
EWS
1
PASI-A
EPA 365.1
JDA
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 12

®
acaAnaly�ical
Pace Analytical Services, Inc.
205 East Meadow Road - SuiteA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
www.pacelaftmn
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
ANALYTICAL RESULTS
Project: WOOD BOILER 12/15
Pace Project No.: 921.08538
Sample: WB1215A Lab ID: 92108538001 Collected: 12/15/11 10:35 Received: 12/15/11 12:11 Matrix: Solid.
Results,reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
8.0 mg/kg
0.45
1
12/16/11 13:55
12/19/11 23:46
7440-38-2
Barium
1390 mg/kg
4.5
10
12/16/11 13:55
12/20/11 14:02
7440-39-3
Cadmium
1.8 mg/kg
0.089
1
12/16/11 13:55
12/19/11 23:46
7440-43-9
Calcium
56400 mg/kg
89.4
10
12/16/11 13:65
12/20/11 14:02
7440-70-2
Chromium
28.8 mg/kg
0.45
1
12/16/11 13:55
12/19/11 23:46
7440-47-3
Copper
89.2 mg/kg
0.45
1
12/16/11 13:55
12/19/11 23:46
7440-50-8
Iron
20300 mg/kg
89.4
10
12/16/11 13:55
12/20/11 14:02
7439-89-6
Lead
93.8 mg/kg
0.45
1
12/16/11 13:55
12/19/11 23:46
7439-92-1
Magnesium
8850 mg/kg
8.9
1
12/16/11 13:55
12/19/11 23:46
7439-95-4
Manganese
1850 mg/kg
4.5
10
12/16/11 13:55
12/20/11 14:02
7439-96-5
Molybdenum
1.3 mg/kg
0.45
1
12/16/11 13:55
12/19/11 23:46
7439-98-7
Nickel
14.1 mg/kg
0.45
1
12/16/11 13:55
12/19/11 23:46
7440-02-0
Potassium
24500 mg/kg
4470
10
12/16/11 13:55
12/20/11 14:02
7440-09-7
Selenium
1.9 mg/kg
0.89
1
12/16/11 13:55
12/19/11 23:46
7782-49-2
Silver
0.68 mg/kg
0.45
1
12/16/11 13:55
12/19/11 23:46
7440-22-4
Sodium
10900 mg/kg
4470
10
12/16/11 13:55
12/20/11 14:02
7440-23-5
Zinc
100 mg/kg
0.89
1
12/16/11 13:55
12/19/11 23:46
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
ND mg/kg
0.0025
1
12/29/11 14:30
12/27/11 15:54
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
0.12 %
0.10
1
12/19/11 09:06
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus 1680 mg/kg 47.7 10 12/19/11 15:53 7723-14-0
Date: 01/19/2012 03:20 PM REPORT OF LABORATORY ANALYSIS Page 4 of 12 .
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

eAffiiical
www.pacelabscom
Project: WOOD BOILER 12/15
Pace Project No.: 92108538
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
sample: W81215B Lab ID: 92108538002 Collected: 12115/11 10:35 Received:12/15/11 12:11 Matrix: Solid
Results reported on a .dry-weighi" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
16.1 mg/kg
0.96
1
12/16/11 13:55
12/19/11 23:52
7440-38-2
Barium
1410 mg/kg
0.96
1
12/16/11 13:55
12/19/11 23:52
7440-39-3
Cadmium
2.7 mg/kg
0.19
1
12/16/11 13:55
12/19/11 23:52
7440-43-9
Calcium
86100 mg/kg
192
10
12/16/11 13:55
12/26/11 14:05
7440-70-2
Chromium
25.5 mg/kg
0.96
1
12/16/11 13:55
12/19/11 23:52
7440-47-3
Copper
97.8 mg/kg
0.96
1
12/16/11 13:55
12/19/11 23:52
7440-50-8,
Iron
9760 mg/kg
19.2
1
12/16/11 13:55
12/19/11 23:52
7439-89-6
Lead
27.0 mg/kg
0.96
1
12/16/11 13:55
12/19/11 23:52
7439-92-1
Magnesium
12300 mg/kg
19.2
1
12/16/11 13:55
12/19/11 23:52
7439-95-4
Manganese
3200 mg/kg
9.6
10
12/16/11 13:55
12/20/11 14:05
7439-96-5
Molybdenum
1.3 mg/kg
0.96
1
12/16/11 13:55
12/19/11 23:52
7439-98-7
Nickel
15.2 mg/kg
0.96
1
12/16/11 13:55
12/19/11 23:52
7440-02-0
Potassium
25100 mg/kg
9580
10
12/16/11 13:55
12/20/11 14:05
7440-09-7
Selenium
ND mg/kg
1.9
1
12/16/11 13:55
12/19/11 23:52
7782-49-2
Silver
1.3 mg/kg
0.96
1
12/16/11 1155
12/19/11 23:52
7440-22-4
Sodium
18400 mg/kg
9580
10
12/16/11 13:55
12/20/11 14:05
7440-23-5
Zinc
264 mg/kg
1.9
1
12/16/11 13:55
12/19/11 23:52
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
0.028 mg/kg
0.0092,
1
12/29/11 14:30
12/27/11 15:59
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
53.4 %u
0.10
1
12/19/11 09:06
9045 pH Soil
Analytical Method: EPA 9045
PH at 25' Degrees C
8.5 Sid. Units
0.10
1
12/20/11 13:30
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
3310 mg/kg
97.6
10
12/19/11 15:55
7723-14-0
Date: 01/19/2012 03:20 PM REPORT OF LABORATORY ANALYSIS Page 5 of 12
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

�0'malxical
www.pacelabscom
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILER 12115
Pace Project No.: 92108538
QC Batch: MERP/3949 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92108538001, 92108538002
METHOD BLANK: 704456 Matrix: Solid
Associated. Lab Samples: 92108538001, 92108538002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0050 12/27/1115:46
LABORATORY CONTROL SAMPLE: 704467
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Parameter Units Conc: Result % Rec Limits Qualifiers
Mercury mg/kg .067 0.058 88 80-120
MATRIX SPIKE SAMPLE: 704458
92108538001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Mercury mg/kg ND .044 0.034 76 75-125
SAMPLE DUPLICATE: 704459
92108538002 Dup
Parameter Units Result Result RPD Qualifiers
Mercury mg/kg 0.028 0.026 7
Date: 01/19/2012 03:20 PM REPORT OF LABORATORY ANALYSIS Page 6 of 12
This report shall not be reproduced, except in full,
- without the written consent of Pace Anayitical Services, Inc..

�aceAnalytical
www.pacelebs.com
Project: WOOD BOILER 12/15
Pace Project No.: 92108538
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NO 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NO 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/9600 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 92108538001, 92108538002
METHOD BLANK: 700831
Associated Lab Samples:
Parameter
92108538001, 92108538002
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed Qualifiers
Arsenic
mg/kg
ND
0.50
12/19/1122:42
Barium
mg/kg
ND
0.50
12/19/1122:42
Cadmium
mg/kg
ND
0.10
12/19/1122:42
Calcium
mg/kg
ND
10.0
12/1911122:42
Chromium
mg/kg
ND
0.50
12119/1122:42
Copper
mg/kg
ND
0.50
12/1911122:42
Iron
mg/kg
ND
10.0
12/20/1113:19
Lead
mg/kg
ND
0.50
12119/1122:42
Magnesium
mg/kg
ND
10.0
12/19/1122:42
Manganese
mg/kg
ND
0.50
12/19/1122:42
Molybdenum
mg/kg
ND
0.50
12/19/1122:42
Nickel
mg/kg
ND
0.50
12/19/1122:42
Potassium
mg/kg
ND
500
12/19/1122:42
Selenium
mg/kg
ND
1.0
12/19/1122:42
Silver
mg/kg
ND
0.50
12/19/1122:42
Sodium
mg/kg
ND
500
12/19/1122:42
Zinc
mg/kg
ND
1.0
12119/1122:42
Pace Analytical Services, Inc.
98001(inceyAve. Suite 100
Nuntersville, NO 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
700832
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
47.5
95
80-120
Barium
mg/kg
50
48.0
96
80-120
Cadmium
mg/kg
50
48.0
96
80-120
Calcium
mg/kg
500
505
101
80-120
Chromium
mg/kg
50
47.9
96
80-120
Copper
mg/kg
50
47.6
95
80-120
Iron
mg/kg
500
492
98
80-120
Lead
mg/kg
50
48.4
97
80-120
Magnesium
mg/kg
500
483
97
80-120
Manganese
mg/kg
50
48.0
96
80-120
Molybdenum
mg/kg
50
49.1
98
80-120
Nickel
mg/kg
50
47.9
96
80-120
Potassium
mg/kg
500
453J
91
80-120
Selenium
mg/kg
50
48.7
97
80-120
Silver
mg/kg
25
24.3
97
80-120
Sodium
mg/kg
500
514
103
80-120
Zinc
mg/kg
50
48.4
97
80-120
Date: 01/19/2012 03:20 PM REPORT OF LABORATORY ANALYSIS Page 7 of 12
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

eAnalXical
www.pacelabs.com
Project: WOOD BOILER 12/15
Pace Project No.: 92108538
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
700833
Units
92108524001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
NO
45.5
46.3
102
75-125
Barium
mg/kg
ND
45.5
43.5
96
75-125
Cadmium
mg/kg
ND
45.5
40.4
89
75-125
Calcium
mg/kg
ND
455
401
88
75-125
Chromium
mg/kg
ND
45.5
42.5
93
75-125
Copper
mg/kg
ND
45.5
42.6
94
75-125
Iron
mg/kg
ND
455
442
97
75-125
Lead
mg/kg
ND
45.5
39.9
88
75-125
Magnesium
mg/kg
ND
455
381
84
75-125
Manganese
mg/kg
ND
45.5
42.4
93
76-125
Molybdenum
mg/kg
ND
45.5
44.5
98
75-125
Nickel
mg/kg
ND
45.5
40.6
89
75-125
Potassium
mg/kg
ND
455
403J
89
75-125
Selenium
mg/kg
1.89 ug/g
45.5
55.5
118
75-125
Silver
mg/kg
ND
.22.7
20.5
90
75-125
Sodium
mg/kg
ND
455
450J
99
75-125
Zinc
mg/kg
ND
45.5
39.5
86
75-125
SAMPLE DUPLICATE: 701005
Parameter
Units
92108351001
Result
Dup
Result
RPD Qualifiers
Arsenic
mg/kg
3.0
3.1
2
Barium
mg/kg
28.6
27.8
3
Cadmium
mg/kg
0.49
0.84
53 D6
Calcium
mg/kg
492
454
8
Chromium
mg/kg
22.7
21.7
4
Copper
mg/kg
7.3
7.8
1
Iron
mg/kg
21200
22800
7
Lead
mg/kg
10.8
11.9
10
Magnesium
mg/kg
512
341
40 D6
Manganese
mg/kg
51.1
45.8
11
Molybdenum
mg/kg
0.89
0.68
26 D6
Nickel
mg/kg
4.7
3.1
42 D6
Potassium
mg/kg
769
637
19
Selenium
mg/kg
2.5
1.0
85 D6
Silver
mg/kg
ND
.038J
Sodium
mg/kg
ND
37J
Zinc
mg/kg
15.7
12.7
21 D6
Date: 01/19/2012 03:20 PM REPORT OF LABORATORY ANALYSIS Page 8 of 12
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

tic
eAnaljical
www.pacelaft=
Project: WOOD BOILER 12/15
Pace Project No.: 92108538
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: PMST/4391 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92108538001, 92108538002
SAMPLE DUPLICATE: 700764
3544998001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 23.7 22.0 7
SAMPLE DUPLICATE: 700765
92108538002 Dup
Parameter Units Result Resuft RPD Qualifiers
Percent Moisture % 53.4 52.3 2
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Date: 01/19/2012 03:20 PM REPORT OF LABORATORY ANALYSIS Page 9 of 12
This report shall not be reproduced, except in full,
without the written, consent of Pace Analytical Services, Inc..

aeeftlytcal
wwwpawlabs.c=
Project: WOOD BOILER 12/15
Pace Project No.: 92108538
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QG Batch: WET/19050
QC Batch Method: EPA 9045
Associated Lab Samples: 92108538002
SAMPLE DUPLICATE: 702043
Parameter Units
pH at 25 Degrees C Std. Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 9045
Analysis Description: 9045 pH
92108599003 Dup
Result Result RPD Qualifiers
5.5 5.5 0
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Date: 01/19/2012 03:20 PM REPORT OF LABORATORY ANALYSIS Page 10 of 12
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

eAnalytical
mmPacelabs.mn
Project: WOOD BOILER 12/15
Pace Project No.: 92108538
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
QC Batch: WETA/11202
Analysis Method:
EPA 365.1
QC Batch Method: EPA 365.1
Analysis Description:
365.1 Phosphorus, Total
Associated Lab Samples: 92108538001, 92108538002
METHOD BLANK: 701634
Matrix: Solid
Associated Lab Samples: 92108538001, 92108538002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Phosphorus
mg/kg
ND 2.0 12/19/1115.18
LABORATORY CONTROL SAMPLE:
701635
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Phosphorus
mg/kg
50 48.5
97
90-110
MATRIX SPIKE SAMPLE:
701636
92107669002 Spike
MS
MS % Rec
Parameter
Units
Result Conc.
Result
% Rec Limits Qualifiers
Phosphorus
mg/kg
4030 150
6410
388 90-110 M6
SAMPLE DUPLICATE: 701637
92107914001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Phosphorus
mg/kg
11300 11000 3
Date: 01/19/2012 03:20 PM REPORT OF LABORATORY ANALYSIS Page 11 of 12
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

�aceAnalytical
www.paca4iftcom
Project: WOOD BOILER 12/15
Pace Project No.: 92108538
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2226 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
Date: 01/19/2012 03:20 PM REPORT OF LABORATORY ANALYSIS Page 12 of 12
This report shall not be reproduced, except In full„
without the written consent of Pace Analytical Services, Inc..

ff]SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
Approved By:
Client
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville., NC 28804
Order Number
1126260
Project Number
92108588
lssved
Tuesday, December 27, 2011
ToUl Number of Wages
4 (excluding C.O.C. and cooler receipt forii�)
QA Manager
L. Accreditation ..
211001
"Analytical Integrity- • EPA Certified • NELAP Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 • Phone: [phone] Fax: [phone]
Web Site: www.settek.com

SUM' IT
ENVIRONMENTAL TECHNOLOGIES, INC.
_ Analytical Laboratories
2
Sample Summary
Client: Pace Analytical Services Inc
Order Number: 1126260
Laboratory 10 Client ID Matrix Saniplhiq Date
1126260-01 92108538002 Solid 1211-5/2011
"Analytical Integrity" • EPA Certified . NELAP Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: [phone] • Fax: [phone]
Web Site: www.settek.corn

ffISUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
Report Narrative
Client: Pace Analytical Services Inc
Order Number: 1126260
3
Solid Sample results are reported on a wet weight basis except as noted.
No problems were encountered during analysis of this order number, except as noted.
Data Qualifiers: .
B Analyte found in the method blank
J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ)
C = Analyte has been confirmed by another instrument or method.
E = Analyte exceeds the Upper limit of the calibration curve.
D = Sample or extract was analyzed at a higher dilution
X = User defined data qualifier.
S = Surrogate -out of control limits
U = Undetected
a' = Not Accredited by NELAC
ND = Non Detected at LOQ
DF = Dilution Factor
Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor)
Limit Of Detection (LOD) = Laboratory Detection Limit
Estimated uncertainty values are available upon request.
Matrices:
A=Air
C = Cream
DW = Drinking Water
L = Liquid
O = Oil
SL = Sludge
So = Soil
S = Solid
T = Tablet
TC:= TCLP Extract
WW= Waste Wbter
W = Wipe
The test results meet the requirements of the NELAC standard, except where noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot
be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this
report was issued. The results contained in this report are only representative of the samples received. Conditions
can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not
responsible for use or interpretation of the data included herein.
"Analytical Integrity" • EPA Certified - NELAP Certified
3310 Win Street • Cuyahoga Falls, Ohio 44223 0 Phone: [phone] • Fax: [phone]
Web Site: www.settek.com

ffISUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
clielit IN
Lab IN
Collected Anal . e
92108538002
1126260-01
15-Dec-11 Flash Point
Client ID#
Lab IN
Col ect d Anal3le
92108538002_
J1126260-01
15-Dec-11 Reactive Cyanide
Client IM
Lab 113#
C011cet d Anal3jg
92108538002 1126260-01 15-Dec-11 Reactive Sulfide
Result
>140
Result
ND
December27, 2011
Client: Pace Analytical Services, Inc.
Address: 2225 Riverside Drive
Asheville, NC 28804
Received: 12/20/2011
Project #: 92108538
Units Matrix, Method DE LQ 'Run Analyst
OF 5 1010 1 20-Dec-11 RMS
Units MaWx Method. Pf- L0,(] Rutt Analyst
mg/kg S 7.3.12 • 1 0.5 20-Dee 11 TIR
Units Matrix Method DF LQQ. Run Analvst
mglkg S 7.3.4.2 1 25 20-Dec-11 TIR
Page 4
"Analytical Integrity" • EPA Certified - NELAP Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 a Phone: [phone] - Fax: [phone]
Web Site: www.settek.com

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