WQ0004298_Residuals Annual Report 2014_20150309

N
Town of Mars Hill NC
2014 Land Application Report
WQ0004298
Attached are the required forms for the Town of Mars Hills 2014 land application
program.
The town has land applied 15.805 dry tons of sludge over 14.5 acres in the calendar year
2014. We have also maintained compliance with all terms and conditions except for our
fecal density testing. We had misplaced our test bottles and did not test in the 2014
calendar year. We did remember in January and did the required testing on sludge that
was collected in 2014 and had been in aerobic digestion for 30 days. The results met and
exceeded all requirements but were sampled outside the required monitoring period. A
sampling schedule will be implemented to prevent this from happening again.
Contact Information:
Preparer/ORC
Robert Sams
Public Works Director
Town of Mars Hill
PO Box 368
Mars Hill NC 28754
Phone # [phone]
Permittee
Darhyl Boone
Town Manager
Town of Mars Hill
PO Box 368
Mars Hill NC 28754
Phone # [phone]
E
CEIVED
f Water Resources
— 9 2015
y Regional Operations
le Re ions! Office----
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REUIEIVEDIDENRIDWR
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e _ t ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit#: WQ0004298 County: Madison Year: 2014
Facility Name (as shown on permit): Town of Mars Hill
Land Application Operator: Robert M Sams Phone: [phone]
Land application of residual solids as allowed by the permit occurred during the'past calendar year?
*+ Yes.;' No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Total number of application fields in per 2
Total number of fields land application occurred during the year: 1
Total amount of dry tons applied during the year for all application sites: 15.805
Total number of acres land application occurred during the year: 14.5
Part B:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Resources. J Yes -_** No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
---- 3 Annua sous analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
.....prior. authorization was received from -the Division of -Water -Resources:- - -- .. - -
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for kno g violations."
Darhyl Boone- Town Manager
J
Permi ame prid Title (typ r print) Signature f Permittee Da e
Signature of Preparer* Date
Signature of Land Applier Date
DENR FORM ACF (5/2003)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0004298
Facility Name: Town fo Mars Hill
NPDES # or NC0057151
WQ#:
WWTP Name: Town of Mars Hill WWTP
Residual Analvsis Data
Laboratory: 1) Earth Environmental
2) Environmental Testing Solutions
3) A&L Eastern Laboratories
4)
5)
•D
Sample•.
• 1 - . -
• ,
--------
05 no 0 ! • -
e--_------�
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
sgnifi�t penalties for submitting false,information, including the possibility of fines and imprisonment for knowing violations."
Preparer
2/18/2015
Date
DENR FORM RSSF (5/2003)

Earth oviraoolal Services
Michael Ladd
75 Bison Lane
Murphy, NC 28906
Robbinsville Lab [phone]
Weaverville Lab [phone]
Residence [phone]
Name and Address of Facility: Date: 1/20/2015
Town of Mars Hill WWTP Sample Collector. / RS
P.O. Box 368 Date and Time Sample Received: 5/28/2014 10:55 AM
Mars Hill, NC 28754 Date and Time Sample Collected: 5/28/2014 7:40 - 8:15 AM
Aft: Robert Sams Date and Time Sample Analyzed: < MHT
Land Application Analyses - Note: All results in mg/Kg Dry Basis unless otherwise noted.
Test
Belt Press Sludge
. Soil Site #1
Soil Site #2
Report Limitj
Method
Units
ACIDITY
0.0 meq/100g
0.0 meq/100g
SCA
meq/100g
TOTAL SUSPENDED RESIDUE
1.0
SM2540D
mg/L
CATION EXCHANGE CAPACITY
12.1 meq/100g
9.7 meq/100g
SCA
meq/100g
PH
5.2
7.2
7.2
0-14
SCA
units
AMMONIA NITROGEN
1000 _
0.5
SCA
mg/L
NO2 + NO3-n
< 31.21
1.0
SCA
mg/L
TOTAL KJELDAHL NITROGEN
57200
SCA
mg/L
TOTAL PHOSPHOROUS
18500
972
559
SCA
mg/L
PERCENT TOTAL RESIDUE
13.0%
80.0%,
87.0%
SCA
mg/L
%ORGANIC MATTER
4.3%160.39%.
SCA
NTU
% BASE SATURATION - K
9.5%
SCA
mg/L
- H
0.0%
.Mg
30.6%
-Ca
59.5%
-Na
0.7%
PLANT AVAILABLE (surface)
22980
PPM/dw
NITROGEN- PPM DRY WT (subsurt)
23480
PPM/dw
SAR
1.416501
ESP
7.85124% ` '
7.731959%
MANGANESE
194 /
1.62
SCA
mg/L
MAGNESIUM
2800
3190
1030
SCA
mg/L
SODIUM
542
22.9
14.7
SCA
mg/L
CADMIUM
< 7.48
< 1.20
< 1.15
SCA
mg/L
CHROMIUM
24.4
62.7
43.7
SCA
mg/L
COPPER
203
44.4
20.2
SCA
mg/L
LEAD
19.7
17.7
13.4
SCA
mg/L
NICKEL
17.0-
11.3
9.33
SCA
mg/L
ZINC
590
57.6
27.9
SCA
mg/L
CALCIUM
6480
3320
1450
SCA
mg/L
POTASSIUM
3930
1790
372
SCA
mg/L
ALUMINUM
4770
WA
N/A
SCA
mg/L
ARSENIC
< 18.7
< 2.99
< 2.87
SCA
mg/L
SELENIUM
< 18.7
< 2.99
< 2.87
SCA
mg/L
MOLYBDENUM
< 18.7
< 2.99
< 2.87
SCA
mg/L
MERCURY
1.60
< 0.12
< 0.11
SCA
mg/L
N.C. Laboratory ID# 352 Analyzed By: SC
'Lab Supervisor. Michael J. Ladd; EES-Robbinsville Certified By: ` Qp

Mars Hill Land Application Belt Press Sludge 5/28/14
PAN
•
,o
j2ngijear
_;a
Applied on
% Solids
0.13
PAN Surface
MR(TKN-NH3)+ + .5(NH3)+NO3+NO2
=mg/kg
22980 rn /k
46.96 Ibs/dry ton
40.07.1q-x ,,/ 1,2
-3
O
Ibs total! PAN
mg/kg x .002
=Ibs/dry ton
#DIV/01
Ibs PAN/acre
PAN Injection
MR(TKN-NH3) + 1(NH3)+NO3+NO2
=mg/kg
23480 mg/kg
46.96 Ibs/dry ton
0
Ibs total PAN
mg/kg x .002
=Ibs/dry ton--
#DIV/OI
Ibs PAN/acre
Dry Tons/1000 gal.
0.6421
1 st year PAN
Surface Ibs.
0
1st year PAN
Injected Ibs.
0
Ibs./acre
Surface
#DIWOI
Ibs./acre
Injected
#DIV/0!
1000 X 8.34 X %solids X sp. gravity
2000
"=dry tons/1000gal."
r

SAR & ESP Mars Hill Land Application
Belt Press Sludge5/28/14
Sodium Absorption Ratio
Na M /L1 Ca(Mq/L1
`6480
Mg(M /L
Na: Sodium (Mg/L) Equivalent weight: 23
542
2800
Ca: Calcium (Mg/L) Equivalent weight: 20
Mg : Magnesium (Mg/L) Equivalent weight: 12
Na ME
23.56522
Ca (ME)
Na ME
Ca (ME)
324
Mg (ME)
23.565217
233.3333
V//
The amount of exchangeable sodium ions
amount of exchangeable calcium & magne
material.
Permitting guidance is if greater than 10 re

AR & ESP Mars Hill Land Application Soil Site #1 5/28114
,xchangeable Sodium Percentage
SP = Na (Milli Equivalents) / CEC X 100
ESP 7.85124 %
a on NC soil test is expressed as meq.
The percentage of sodium ions occupying the cation exchange complex of soils
Na ME GEC
0.95000000000 12.1
Should be less than 15% (15-20%)

AR & ESP Mars Hill Land Application Soil Site #2 5/28/14
,xchangeable Sodium Percentage
BP = Na (Milli Equivalents) / CEC X 100. The percentage of sodium ions occupying the cation exchange complex of soils
Na (ME) F CEC
0.75000000000 9.7
ESP 17.731959 % Should be less than 15% (15-20%)
a on NC soil test is expressed as meq.

PO Box 7565
-
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
.i?A
4_.
Environmental Testing Solutions, Inc.
Certificate of Analysis
Project name: Earth Environmental Services
Project number: 140528.510
Collection date: 28-May-14/��
Date received: 28-May-14
n
r�
nre-�
IY
S l l
Sample identification: #051425
Sample number:
116482
Parameter
Method
Result
RL
Units
Date
Analyst Footnotes
Analyzed
Percent Solids
SM 2540 G
13.0
0.100
%
30-May-14
ASB
I
Mercury
7471B
1.60
0.74
mg/kg
9-Jun-14
DER
I
Aluminum
6010C
4770
935
mg/kg
3-Jun-14
NEC
1
Arsenic
6010C
<18.7
18.7
mg/kg
3.Jun-14
MEC
I
Cadmium
6010C
<7.48
7.48
mg/kg
3-Jun-14
NEC
1
Calcium
6010C
6480
935
mg/kg
3-Jun-14
MEC
I
Chromium
6010C
24.4
18.7
mg/kg
3-Juna4
MEC
1
Copper
6010C
203
7.48
mg/kg
3 Jun-14
NEC
1
Lead
6010C
19.7
18.7
mg/kg
3-Jun-14
NEC
1
Magnesium
6010C
2800
935
mg/kg
3 Jun-14
MEC
1
Molybdenum
6010C
<18.7
18.7
mg/kg
3 Jun-14
MEC
1
Nickel .
6010C
17.0
7.48
mg/kg
3-Jun-14
MEC
1
Potassium
6010C
3930
37.4
mg/kg
3-Jun-14
MEC
1
Selenium
6010C
<18.7
18.7
mg/kg
3Jun-14
MEC
1
Sodium
6010C
542
37.4
mg/kg
3-Jun-14
MEC
1
Zinc
6010C
590
18.7
mg/kg
3-Jun-14
MEC
1
Nitrate + Nitrite
<31.21
31.21
mg/kg
1,2
Total Phosphorus
6010C
18500
748
mg/kg
3-Jun-14
MEC
1
Total Kjeldahl Nitrogen
351.2
57200
935
mg/kg
10-wn-14
LDP
1 -
Total Nitrogen
Calculation
57200
935
mg/kg
10-Jun-14
LDP
1
Ammonia Nitrogen
SM 4500 NM D
1000
18
mg/kg
29-May-14
KEK
Percent Solids
SM 2540 G
22
%
28-May-14
KW
pH in Soil
SW 846 9045D
5.2
S.U.
28-May44
KW
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Methods EPA 9210A and SM 450ONO2 B by LDP and REH on 06-04-14 and 06-05-14.
Date reviewed: NC Certification Number. 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
Signature:
Iti NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis. '

r ANNUAL METALS FIELD LOADING SUMMARY FORM[*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Mars Hill Land Application Total Dry Tons Applied (Annual): 15.805
Permit #: WQ0004298 Cation Exchange Capacity (non 503 only): 12.1
Operator: Robert M Sams Owner: Larry Cody
Acres Used: 14.5 Acres Permitted: 14.5 Site #: 1 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #l:
Sample
or Com-
posite
Date
11
5/28/14
2
5/28/14
3',`
4!
5
6
7
8
9;
10;
11;
12;
% Solids
13
13
Arsenic
18.7
18.7
Cadmium
7.48
7.48
Chromium
24.4
24.4
Copper
203
203
Lead
19.7
19.7
Mercury
1.6
1.6
Molyb-
denum
18.7
18.7
Nickel
17
17
Selenium
18.7
18.7 t.
Zinc
590
590
Total
Phos-
horus
18500
18500
Annual -aeavv ivletai view Loaames (ualculated in 1bs/acre):
0
1!
2
3t
41
5
6i
7j
8
9F
10
11;
12
�3 a
H
CD e
o "
0.545
1 0.545
Arsenic
0.0204
0.0204
0
0
0
0
0
0
0
0
0
0
10.0408
Cadmium
0.0082
0.0082
0
0
0
0
0
0
0
0
0
0
0.0163
Chromiuni
0.0266
0.0266
0
0
0
0
0
0
0
0
0
0
0.0532
Copper
0.2213
0.2213
0
0
0
0
0
0
0
0
0
0
0.4425
Lead
0.0215
0.0215
0
0
0
0
0
0
0
0
0
0
0.0429
Mercury
0.0017
0.0017
0
0
0
0
0
0
0
0
0
0
0.0035
Molyb-
0.0204
0.0204
0
0
0
0
0
0
0
0
0
0
0.0408
denum
Nickel
0.0185
0.0185
0
0
0
0
0
0
0
0
0
0
0.0371
Selenium
0.0204
0.0204.
0
0
0
0
0
0
0
0
0
0
0.0408 i
Zinc
0.6431
0.6431
0
0
0
0
0
0
0
0
0
0
1.2862
Total
Phos-
20.165
20.165
0
0
0
0
0
0
0
0
0
0
40.33
horus
"I cermy, under penalty oY law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includi e. oss' 'ty of fines imprisonment for knowing violations"
�2%
DENR FORM MFLSF (5/2003)
n

jr&A rwir­
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mars Hill Permit #: WQ0004298 Annual Dry Tons Applied: 15.8054676
Owner: Larry Cody Operator: Robert M Sams Cation Exchange Capacity (non 503): 7.2
Site #: 1 Field #: 1 Acres Utilized: 14.5 Acres Permitted: 14.5
o
a o
A �
Specify
Totals
Per
Acre
%
Solid
s
Dry. Tons Per
Acre
Residual
Sources
(Summarize)
site
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
nation
Rate
TKN
Ammo-
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p p
2
*
*
*
Gal.
�:
�.yd.
I&I
Report
Totals
in T Gal.
Crop 1
Crop 2
5/20/14
14578
1005.4
13
0.545016124
Belt Press Sludge
Dry
0
s
0.5
30%
57200
1000
31.21
18.957
#######
silage
1
5/21/14
14578
1005.4
13
0.545016124
Belt Press Sludge
Dry
0
s
0.5
30%
57200
1000
31.21
18.957
00#0
silage
2
0
0
0
0
3
0
0
0
0
4
0
0
0
0
15
0
0
0
0
6
0
0
0
0
j
0
0
0
0��L
0
0
0
0
iok
0
0
0
0
r
0
0
0
0
k< 5�
P;
0
0
0
0
TOTALS:
2011
1
As
Cd
Cr
Cu 11
Pb
Hg
Mo
6.04047
Ni
Se I
Zn
P
PAN 1
PAN 2
Lim: r
Annual lbs/acre
0.040766 4
0.016314
0.05319
0.4425410.0429
0.00349
0.03706
0.04077
12862
40.33
37,914 0
Di
Current Cumulative lbs/ac
0.961154
0.63325
.07257
52.4997
5.4939
.1354
.84821
.64244
.6247&
7.8624
6.5762
2498n
, ` �?i
--
Prior Years Cumulative lbs/ac
0.920388
0.61694
2.01938
52.0572
5.45104
0.132
2.80744
2.60538
1.58401
Permitted C. P. L. R.***
36
34
NL
1338
267
15
NL
374
89
Permit PAN Limit lst/2nd Crop
:.. Wes. .: a
?c=.:. ,
r
ti�
_F sue'
s ....---.TI --"aA NcaaauJ' UA &ATV, LAAAL Wl1A UUUU1 MIL W43 prepureu unuer my
designed to assure that qualified personnel properly gathered and evaluated
significa en 'es or submittinwfalse information, including the possibilil
Si ature of Applie Date
s
rro
in accoraance wit a s em
ted. I am aware that there are alp
nent for knowing violations."
iod: S - Surface, IN - Injection, INC - Incorporation
gate: Surface - 0.5. Iniection/Incorvoration -1.0
w �ulative Pollutant Loading Rate
CLA**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. TC Oi
thematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered 111(5,010 byte the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

I
s
OE'
t Environmental Testing Solutions, Inc.
Certificate of Analysis
Project name: Earth Environmental Services
Collection date: 28-May-14 S to
Date received: 28-May-14
Sample identification: #051426
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 140528.511
ArAP
Sample number: 116483
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed
Percent Solids
SM 2540 G
80.0
0.10
%
30-May-14
ASB
1
Mercury
7471B
<0.12
0.12
mg/kg
9-Jun-14
DER
1
Arsenic
6010C
<2.99
2.99
mg/kg
3-Jun-14
MER
1
Cadmium
6010C
<1.20
1.20
mg/kg
3-Jun-14
MER
1
Calcium
6010C
3320
149
mg/kg
3-Jun-14
MER
1
Chromium
6010C
62.7
2.99
mg/kg
3-Jun-14
MER
1
Copper
6010C
44.4
1.20
mg/kg
3-Jun-14
MER
1
Lead
6010C
17.7
2.99
mg/kg
3-Jun-14
MER
1
Magnesium
6010C
3190
149
mg/kg
3-Jun-14
MER
.1
Mangenese
6010C
194
1.20
mg/kg
3-Jun-14
MER
1
Molybdenum
6010C
<2.99
2.99
mg/kg
3-Jun-14
MER
l
Nickel
6010C
11.3
1.20
mg/kg
3-Jun-14
MER
1
Potassium
6010C
1790
5.98
mg/kg
3-Jun-14
MER
1
Selenium
6010C
<2.99
2.99
mg/kg
3-Jun-14
MER
1
Silver
6010C
<1.20
1.20
mg/kg
3-Jun-14
MER
1
Sodium
6010C
22.9
5.98
mg/kg
3-Jun-14
MER
1
Zinc
6010C
57.6
2.99
mg/kg
3-Jun-14
MER
I
Total Phosphorus
6010C
972
120
mg/kg
3-Jun-14
MER
1
pH in Soil
SW 846 9045D
7.2
S.U.
28-May-14
KW
Acidity
See Attached Sheets
A&L
2
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

x �
Environmental Testing Solutions, Inc.
Certificate of Analysis
Project name: Earth Environmental Services
Collection date: 28-May-14 tC
Date received: 28-May-14
Sample identification: #051427
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number:
140528.511
Sample number: 116484
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed
Percent Solids
SM 2540 G
87.0
- 0.10
%
30-May-14
ASB
1
Mercury
7471B
<0.11
0.11
mg/kg
9-Jun-14
DER
I
Arsenic
6010C
<2.87
2.87
mg/kg
3-Jun-14
MER
1
Cadmium
6010C
<1.15
1.15
mg/kg
3Jun-14
MER
1
Calcium
6010C
1450
143
mg/kg
3-Jun-14
MER
I
Chromium
6010C
43.7
2.87
mg/kg
3-Jun-14
MER
I
Copper
6010C
20.2
1.15
mg/kg
3-Jun-14
MER
1
Lead
6010C
13.4
2.87
mg/kg
3-Jun-14
MER
1
Magnesium
6010C
1030
143
mg/kg
3-In-14
MER
1
Mangenese
6010C
162
1.15
mg/kg
3-Jun-14
MER
1
Molybdenum
6010C
<2.87
2.87
mg/kg
3-Jun-14
MER
1
Nickel
6010C
9.33
1.15
mg/kg
3-Juna4
MER
1
Potassium
6010C
372
5.74
mg/kg
3-Jun-14
MER
1
Selenium
6010C
<2.87
2.87
mg/kg
3-Jun-14
MER
1
Silver
6010C
<1.15
1.15
mg/kg
3-Jun-14
MER
1
Sodium
6010C
14.7
5.74
mg/kg
3-Jun-14
MER
1
Zinc
6010C
27.9
2.87
mg/kg
3-Jun-14
MER
1
Total Phosphorus
SM 4500 P F
559
115
mg/kg
3-Jun-14
MER
1
pH in Soil
SW 846 9045D
7.2
S.U.
28-May-14
KW
Acidity
See Attached Sheets
16-Apr-13
A&L
2
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Sample analyzed by A&L Eastern Laboratories, Inc.
Date reviewed: 60 • j I.-H
Data reviewed by: Kelley E. Keenan
Signature:
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

Page 1 of I
Report Number: 14-149-0626
Account Number: 46933 Af�:
Send To: ENVIRONMENTAL TESTING
SOLUTIONS INC
POB 7565
ASHEVILLE NC 28802
E ... astem Labor torino.
F-lGil 61, 19X(§04)2T.1440-
PNIiQI W11117- (904)'.,14a�44
Grower: Submitted By: KELLEY EKEENAN
ENVIRONMENTAL TESTING Farm ID:
SOIL ANALYSIS REPORT Analytical Method(s):
Date Received: 05/29/2014 Date Of Analysis: 05/30/2014 Date Of Report: 05/30/2014 Mehlich 3
b"
z
.051426 139 VH 203 VH 506 16579 4.7 M 124 VH 1792 M
NC=116 NC 104 7.3 0.0 13.77
51427
L 107* M 1 336 VH 1255 M 7.3 0 0 9
!C 13 NC55 .3
051426 3.8 1 30.8 65.4 0.0 M
51427
T 3.0 30.1 67.5 0.0
Values an this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VI_ (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR _ Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = lbs/A,- Soluble by: 60wr
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: A&L Eastern Laboratories, Inc.
Pauric McGroary
Td

RA&L Eastem Laboratories
LA
7621 Whltqjn.
f
Submitted By: MICHAEL LADD
Client: -Y. rLJLJ 6/3/2014 SOIL ANALYSIS
T Grower :
FEARTHENVIRONIVIENTAL SVCS SOIL S Report No: 14-153-0592
SOIL SITES I & 2 Cu 0
S Cust No: 46220
75 BISON LN
M MU P Y C 9 Date Printed:
URPHY NC 28906 06/03/2014
Date
ci
Report
eoReceived 06102/2014
Date Analysis 06/03/2014
Dn- Page: I of
Lab Number: 17390 Field Id:05/28114 Sample Id: #051426
Crop: Lawn
(TINS). .-J
0
Crop :
Comment
'11- 1 L;-Fx 1 11-11 1 "UIUMILINIzU
3.5 0 0
1- 0 —T-0.46 0
Rec Units:
Cu Mr
Rec Units:
LB/1 000 SF
0 i4OE
Pod.
Analysis prepared by. A&L Eastern Laboratories; Inc.
Pauric McGroary

A & Eastern Laboratofies
7621 WhRepine Road Richmond; Virginia 23237 [phone] Fax [phone]
W W�.V.d1a�7SQ0rfl,GolY1
Submitted By: MICHAEL LADD 6/3/2014 SOIL ANALYSIS
Client: Grower: Report No: 14-153-0592
EARTH ENVIRONMENTAL SVCS SOIL SITES 1 & 2 Cust No: 46220
75 BISON LN Date Printed: 06/03/2014
MURPHY NC 28906 Date Received: 06/02/2014
Date Analysis : 06/03/2014
PO: Page : 2 of 4
Lap Number: -i fovu Field Id :05/28/14 Sample Id : #051426
�s
TILI►I® T,
1
Forst Applecatloh Second�Applicatton � ' ' F ''� _ ��� Th��d"Application�_f�� -� �,lfir�-F�ourtCt3Appolcation3 �,
sa; 7 �
#19000 S,q Ft < < FiertiUzer? #/7000,Sq Ft , Fertilizer #/100Q Sq sFt„. F@itllizer #/10®0 Sq` t
,-a FB h fFerUUzer
6
21-0-0
6
21-0-0
6
21-0-0
Comments.
Lawn
• The amount of fertilizer recommended on the first page is the total amount needed for the entire growing season. Split into 3-4
applications to keep the lawn green and prevent fertilizer loss. You should not apply more than 0.7 Ibs of soluble nitrogen per 1000
square feet in a 30 day period. Or more than 0.9 Ibs of nitrogen per 1000 square feet if you are using a slow or controlled release
product in a 30 day period.Custom blend is best to meet exactly the requirement, if this is impossible, the above specific fertilizer
application is a general guideline, if the specified grades can not be found, replace with fertilizer having similar N:P:K ratio. The best
time to apply fertilizer for cool season grass (bluegrass, fescue, ryegrass) is in the Fall when the grass is growing. For Mid -Atlantic
region the time is from late August to November. For Northeast region the time is from mid August to October. Fall application should
start as soon as the day time high temperature is below 80-85F, apply with the interval of one month. If you start application late in the
Fall and do not finish all three applications, repeat the same applications in the Fall of next year. Spring application is recommended
when exceptional fertilizer loss due to heavy spring rain leaching and the grasses look pale green. Spring application can start as soon
as the grass starts to grow in April. In the case of exceptional warm spring, the application can be made earlier.
• To reduce soil pH apply 2.6 pounds of elemental sulfur per 1000 square feet for every 0.1 of pH unit above 7.2• For example, a soil
pH of 7.4 requires 5 pounds of elemental sulfur (0.2 * 2.5). Do not apply more than 5 Ibs per 1000 square feet per application or more
than 10 Ibs of elemental sulfur per 1000 square feet per year. Timing between applications should be minimum of 31months. Warm
temperature and moist soil are needed for sulfur to reduce soil pH. If sulfur is applied in winter or under drought conditions, it will take
longer for the the soil pH to be lowered.
Use ammonium sulfate as all or portion of the N requirement to reduce pH.
For a more in depth explanation of the soil test and recommendations, go to our website www.aleastern.com and select the "Lawn
and Garden" tab at the top of home page. Under the "How to Understand a Soil Test Report" header you will find the link to the article
"Soil Test Report & Fertilizer Recommendation Explained".
Analysis prepared by: AFL Eastern Laboratories, Inc. - -
Pauric IVIcGioary

• ,Ma:•5 ��t j t c�.� �1�
_ xZ
A &L Easto�� Laborato�-ios�-� tj s
7621 Whitepine Road Richmond, Virginia 232N (904) 743401 Fax [phone]S W�
taYrla%aleasteen�eam S[�� j `,�'
• 5
u
m1 a y. MICHAEL LADD
6/3/2014
OIL ANALYSIS
Client:
EARTH ENVIRONMENTAL SVCS
Grower :
SOIL SITES 1 & 2
Report No:
14-153-0592
75 BISON LN
Cust No:
46220
MURPHY NC 28906
Date Printed:
06/03/2014
Date Received :
06/02/2014
Date Analysis :
06/03/2014
PO:
Page:
3 of 4
Lab Number: 17391
Field Id :05/28/14
Sample Id : #051427
SUIL FERTILITY GUIDELINES
Crop: Lawn
Comment:
Rec Units:
LB/1000 SF
Analysis prepared by: A&L Eastern Laboratories, Inc.
Pauric McGroary

o
astern Laboratories
v
M
7621 Whkepine R6ad Riehmond, Vlrglnia 23237 (804) 743,4401 Fax (B04) Z71-W6
w
vv�r�:afeaste�,em�°ra
Submitted By: MICHAEL LADD 6/3/2014 SOIL ANALYS
Client: Grower: Report No: 14-153-0592
EARTH ENVIRONMENTAL SVCS SOIL SITES 1 & 2 Cust No: 46220
75 BISON LN Date Printed: 06/03/2014
MURPHY NC 213906 Date Received: 06/02/2014
Date Analysis : 06/03/2014
PO: Page: 4 of 4
Lab Number: 17391 Field Id :05/28/14 Sample Id : #051427
Lawn
• The amount of fertilizer recommended on the first page is the total amount needed for the entire growing season. Split into 3-4
applications to keep the lawn green and prevent fertilizer loss. You should not apply more than 0.7 Ibs of soluble nitrogen per 1000
square feet in a 30 day period. Or more than 0.9 Ibs of nitrogen per 1000 square feet if you are using a slow or controlled release
product in a 30 day period.Custom blend is best to meet exactly the requirement, if this is impossible, the above specific fertilizer
application is a general guideline, if the specified grades can not be found, replace with fertilizer having similar N:P:K ratio. The best
time to apply fertilizer for cool season grass (bluegrass, fescue, ryegrass) is in the Fall when the grass is growing. For Mid -Atlantic
region the time is from late August to November. For Northeast region the time is from mid August to October. Fall application should
start as soon as the day time high temperature is below 80-85F, apply with the interval of one month. If you start application late in the
Fall and do not finish all three applications, repeat the same applications in the Fall of next year. Spring application is recommended
when exceptional fertilizer loss due to heavy spring rain leaching and the grasses look pale green. Spring application can start as soon
as the grass starts to grow in April. In the case of exceptional warm spring, the application can be made earlier.
Use ammonium sulfate as all or portion of the N requirement to reduce pH.
For a more in depth explanation of the soil test and recommendations, go to our website www.aleastern.com and select the "Lawn
and Garden" tab at the top of home page. Under the "How to Understand a Soil Test Report" header you will find the link to the article
"Soil Test Report & Fertilizer Recommendation Explained".
Analysis prepared by: A&L Eastern Laboratories, Inc: Pauric McGroary

ROBBING ILLE LA28) BORATORY EARTH ENVIRONMENTAL SERVICES
WEAVERVILLE OFFICE MICHAEL LADD-OWNER
[phone] tsw
FAX: [phone] P.O. BOX 2733 75 BISON LANE
RESIDENCE [phone] WEAVERVILLE, NC 28787 MURPHY, NC 28906
FAX: [phone]
Client:lD`3 v� V\( /�' 1 c^i/ l (l� dti� ✓ l I" Report To: O k -�
Address: 11/D&W 3 Bill To: I 6 Y14
1; ' y�/,-� 1`1� �L i (r'� ��Z L'1 P.O. # / Billing Reference:
Phone: 2,9 6 61- alk- ab 0 0\(FAX #: g �� �Ci� Ct
009286
CHAIN -OF -CUSTODY RECORD
Analytical Request _
[nit Lab Temp:
Rec Lab Temp:
Gi^
*Requested Due Dat4.c�
Sampled By- ri t)
REMARKS
CWH
CL
SAMPLE DESCRIPTION RESID. TIME MATRIX EES.
EVE
1
FOR
0061 1 194
1, AT
91
EEE=mmmmmmlmm@mm
@MENEM
EEE=mmmmmmlm
son
son
ME
EEE=mmmmmmmmmmmm
son
Is
Em=mmmmmmlm
monsoon
ME
mmommossonso
mossonsomm
mossonsomm
SHIPMENT METHOD ITEM
OUT/DATE RETURNED/DATE #
RELINQUISED BY/ AFFILIATION
ACCEPTED BY/ AFFILIATION
DATE
ADDITIONAL COMMENTS:
SEE REVERSE SIDE FOR INSTRUCTIONS cP-0771-B

ROBBI (828) E9-6428 LABORATORY GRKI EARTH ENVIRONMENTAL SERVICES
[phone]
WEAVERVILLE OFFICE MICHAEL LADD-OWNER
[phone]
FAX: [phone] P.O. BOX 2733
RESIDENCE [phone] WEAVERVILLE, NC 28787
FAX: [phone]
Client: n M
Address: l 0 3 bg
Phone:.—�
Report To: "\0D L Q"-t
Bill To: �� M
tjL-
RO. # / Billing Reference,
75 BISON LANE CHAIN -OF -CUSTODY RECORD
MURPHY, NC 28906 AnalyticalRequest -
FAX#: 91�- ( 0 V,� 2,33 �p p
Init Lab Temp:
Rec Lab T P.
*RgequvSA-� e Date: g
LL
�3
/r ■ i
7
` ♦�i-� i H a REMARKS
•�
•
.
_/1' All. t
ITEM CL °
# SAMPLE DESCRIPTION RESID. TIME MATRIX. EES.114f .6
monsoons
-M Mo.WNO ININ�
�
IN
■■■�■■■■■■■■
NOON■■■■NNE
■NEB■■■■■■■■
■NOON■■■NNE
■■E�■■■■■■■■
NOON■■■■NNE
■■E�■■■■■■■■■■■■■■■■NNE
■
■■E��■N■■■■■■■■■■■■■NNE
■■E�■■■■■■■■■■■■■■■■NNE
Emmons■■N■��
SHIPMENT METHOD ITEM
OUT/DATE RETURNED/DATE #
" 4
° RELINOUIS,ED BY'/AFFILIATION°'
■ ■■■■�
`
�, ACCEPTED BY
ADDITIONALr
, «
■
i
■
SEE REVERSE SIDE FOR INSTRUCTIONS cP-0771-B

Parker Farm Supply, Inc.,..
1028 US Hlnry. 19 No
Mars Hill, NC 28754 w` .
Phone [phone] • Fax [phone]
Feed, Seed, Fertilizer, Lime
Culvert Pipe, Veterinary Supplies
'Ll 0 ONE Fy f DAT j
NAME LL �i� r
ADDRESS -
SOLD BY
CASH
CHARGE
C.O.D.
QTY.
DESCRIPTION
.:PRICE
AMOUNT
TAX
,F,(;1iIVED BY
TOTAL
Purchaser agrees to pay all.costsofcollecting orsecuring or
n reasonable at coiled or e secure this amount, including a
reasonable asecur d fee, whether the same is to be
collected or secured by suit or otherwise.
pASTDUEACCOUNT$ARESUBlECTTOASERVICE
CHARGE OF 1 IPd% PER MONTH ON THE UNPAID '
PAST DUE BALANCE. 18%ANNUALLY
CURRENT 1-30 DAYS PAST
DUE
3,472.63 0.00
Statement
Amount Due
$3,472.63
Amount
31-60 DAYS PAST . 61-90 DAYS PAST OVER 90 DAYS
DUE DUE PAST DUE
0.00 0.00 0.00
Date
11/24/2014
Amount Enc.
Balance
3,472.63
Amount Due
$3,472.63

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: Town of Mars Hill
WWTP Name: Town of Mars Hill WWTP
Permit Number: WQ0004298
NPDES Number: NCO057151
Monitoring Period: From 1/1/2014 To 12/31/2014
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 10 Alternative 2 0 Alternative 3 0
011§00,aj*,1 19",
Alternative 40 Alternative 5 Alternative 6�'}
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 0 Heat Drying C- 1 Heat Treatment
Thermophilic L � 1M,04 54
Beta -Ray Gamma Ray 0 Pasteurization,6
.... r ,
Class B:
Alternative 121
Alternative 2 v
Alternative 3 10-41
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Air Drying Composting 01 Aerobic Digestion
Anaerobic Digestionsg> wYF
yy f
�r- ,� taf'`�l�?%i k " =kr�� f eta �, vi..a.A +? 3�8� ,.,! .av 4,� � t1.,5•ry .ux�v„ u,.'��iis'
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
Pathogen Density
g tY
Number o
Excee-
Frequency
Sample
Analytical
inim
Geo. Mean
Maximuir
Units
in Sludge
dences
of Analysis
Type
Tech-niqu
2 x 10 to the 6th
power N PN per
29000
13000
5000
col/gram
0
1/year
grab
/9222`
gram of total
solids or 2 x 10 to
Fecal Coliform
the 6th power
,
CFU per juarn of
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
3 NTN per 4
(in lieu of fecal
grams total solid
coliform)
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 Option 2 [7] Option 3 EL Option 4 Option 5 0
Option 6 0 Option 7 ,� Option 8 Option 9 1 O
P tion 10 �
No vector attraction reduction options were performed r ~x
.d,`,a 'a ,.1" xtb.S.t+ •wFii ><,h:{ „t'�+',».3ti4& N.''
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met I
am aware that there are significant penalties for false certification including fine and imprisonment."
Robert M Sams- Public Works Director
Prepa ame and Title ( e or print) Land Applier Name and Title (if applicable)(type or print)
/--

I
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Na
Biosolids Permit Num
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1 4/10/2014 14:154
[d
0.1
4.8
1.0
illiliters
Dry Solids
agrees Celsius
!grees Celsius
6.17 mg Oxygen/hr
0.73 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 11.09 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically:

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Mars Hill V
Biosolids Permit Number: WQ004298
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
9 5/15/201414:059
13.
0.1
4.5
1.0
Ililiters
Dry Solids
grees Celsius
arees Celsius
4.76 mg Oxygen/hr
0.60 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 0.90 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

5
4.5
4
3.5
E 3
pC�
W
.5
O
62
N
N_
0
1.5
1
0.5
0
Oxygen Uptake Rate Chart
y =-0.0793x + 4.578
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Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Na
Biosolids Permit Num
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
1000 milliliters
0.91 % Dry Solids
1 ..5 degrees Celsius
16.2 degrees Celsius
Z'
Slope: 0.1
Intercept: 4.5
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 5.02 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.55 mg Oxygen/g/hr
Average Temperature: 16 degrees Celsius
Temperature Correction Factor: 1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 0.72mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

5
4.5
4
3.5
as
E3
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d
it.5
O
M
m
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1.5
1
0.5
0
Oxygen Uptake Rate Chart
' � v
y = 0.0836x + 4.5695
5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility
Biosolids Permit N
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
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Correlation Coefficient:
4 11:
//1 tSIZU14 11:15
Michael Ladd
0.1
3.4
1.0
Ililiters
Dry Solids
grees Celsius
grees Celsius
Oxygen Uptake Rate: 4.96 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.55 mg Oxygen/g/hr
Average Temperature: 18 degrees Celsius
Temperature Correction Factor: 1.1449
Temperature Corrected Specific O p wmn
P p Oxygen Uptake Rate: 0.63 mg Oxygen/g/hr
:s
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

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Oxygen Uptake Rate Chart y =-0.0826x + 3.4963
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

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3
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7
8
9
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11
12
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Specific Oxygen Uptake Rate
SOUR
Facility
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Digester Temperature:
Sampling Date/Time:
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Analysis Date/Time:
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End Temperature:
Dissolved Oxygen Level
illiliters
Dry Solids
agrees Celsius
.arees Celsius
Slope:
0.1
Intercept:
3.8
Correlation Coefficient:
1.0
Oxygen Uptake Rate:
3.64 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:
0.43 mg Oxygen/g/hr
Average Temperature:
18 degrees Celsius
Temperature Correction Factor:
1.1449
Temperature Corrected Specific Oxygen Uptake Rate: 0.49,mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes.
The Calculation and the Spreadsheet execute automatically.

4
3.5
3
�.5
0.5
0
1
Oxygen Uptake Rate Chart
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2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

t C
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Na
Biosolids Permit Num
Specific Oxygen Uptake Rate
SOUR
Date: 17-Sep
Digester Temperature: 18
Sampling Date/Time:
Sampled By:
Analysis Date/Time.
Analyzed'By:
Sample Volume:
E
2014 14:20 Ladd
014 14:20 Ladd
1000 milliliters
Total Solids: 0.81 % Dry Solids
Beginning Temperature: 18 degrees Celsius
End Temperature: 17.7 degrees Celsius
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
4.1
1.0
3.54 mg Oxygen/hr
0.44 mg Oxygen/g/hr
18 degrees Celsius
1.1449
Temperature Corrected Specific Oxygen Uptake Rate: �0 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

4.5
4
3.5
'cl
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O
2
1
0.5
Ic
Oxygen Uptake Rate Chart
Y = -0.0589x + 4.1603
0
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. . . . . . . . . .
. . . . . . . .
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
4.07
4
3.91
3.88
3.83
3.79
3.73.
3.68
3.612
3
3
rs
Ladd
1
Ililiters
Dry Solids
grees Celsius
arees Celsius
Slope: 0.1
Intercept: 4.1
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 3.61 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.48 mg Oxygen/g/hr
Average Temperature: 17 degrees Celsius
Temperature Correction Factor: 1.225043
Temperature Corrected Specific Oxygen Uptake Rater 0.69 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

4
3
5?.5
Oxygen Uptake Rate Chart
y=-O.O6O1x+4]S3
MR
an -
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15
2 3 4 5 6 7 8 9 10 11 12 13 14 15 16

EARTH ENVIRONMENTAL SERVICES
75 Bison Lane
Murphy, NC 28906
Residence — [phone]
Robbinsville Lab — [phone]
Weaverville Lab — [phone]
Fax — [phone]
E-Mail — earthenvser@a ebworkz.com\
February 9, 2015
NC ID #352
Mr. Robert Sams
Town of Mars Hill
P.O. Box 368
Mars Hill, NC 28754
Dear Mr. Sams:
Following is a report of laboratory analyses for digester sludge samples received 1/20, 1/21, 1/22, 1/23,
1/27, 1/28, 1/29/15.
Colony Counts
# Smmnle Dnte Cnlifnrm llensities lcnlnniecJornm) %Tntnl Sn1iAQ 1 A m1 n 1 —1 A Al —1
1
1/20115
7,000 Colonies/Gram
1.04
5
2
0
2
1/21/15
10,000 Colonies/Gram
1.04
8
2
1
3
1/22/15
9,000 Colonies/Gram
1.03
8
2
0
4
1/23/15
5,000 Colonies/Gram
1.03
5
0
0
5
1/27/15
20,000 Colonies/Gram
1.06
17
5
1
6
1/28/15
29,000 Colonies/Gram
1.02
30
7
2
7
1/29/15
28,000 Colonies/Gram
1.03
29
8
1
Geometric mean for all seven samples: 13,000 colonies/gram. Thank you for your
business. If you have any question or need additional sample analyses performed, please
call.
Respectfully submitted,
Michael J. Ladd
Laboratory Director

ROBBI (82)1�LABORATORY LABORATORY EARTH ENVIRONMENTA
42
L SERVICES84OWE FFICE
[phone] MICHAEL LADD-OWNER
FAX: [phone] P.O. BOX 2733 75 BISON LANE
FAX: [phone]
RESIDENCE (828) 43 WEAVERVILLE, NC 28787 MURPHY, NC 28906
8631 p j
Gilent: d� ���' S l./ C.C� c�J� Report To:
Address: r' D •&Y
Bill To: l Om
/ ' 1 P.O. # / Billing Reference:
Phone: �o ' %�L U/_!1-4cg -I v 1p - Qt-�T FAX #: -5 <_Z _ (off 2
ocimpmu oy tprim):
Sampler Signature
ADDITIONAL COMMENTS:
009212
CHAIN -OF -CUSTODY RECORD
Analytical Request
Init Lab Temp:
Rec Lab Temp:
*Requested Due Date:
2--
/,#CPS 777B'__2^

0f,. Mars 1-4114
5
t3
-7/a3 /1
_��.rniia; lie- ,r• �, :,Y SOP
1.. Annual Land Application Certification Form
• Was a certification form submitted? : f5
• - Was lard application conducted during the reported year? Y"--S
• Ho;v many dry -tons and dry tons per acre were applied? /5, S6_-�_
• Were the applications within the per—mitted amount? -Yew'
• Verify PAIN if more than 10 tons/acre
• Did it indicate compliance?, Y.QeJ
• Was it signed by the appropriate people? I.C.5
2, itiIonitoring
• Were the analyses conducted at the required frequency?,y-eS
• Were the metals analyses reported -on the Residual Sampling Summary Form? y-e-7
• Were the results reported in mg/lcg?-y4-j
• . Were the heavy metals within ceiling concentration permit limits?* --I
• If no, were the lab analyses attached?
• Were all the required parameters tested? YK-S
• Was TCLP analysis conducted? ak 7u
3. Field Summary
• Were the land application. events recorded on the Field Summary Forms?,�.e-sILI
Aleed
• Was a Field Summary Form submitted for each •field?
• Were all the residuals applied to permitted land?oy eJ
• • Were all the residuals applied from permitted sources?Yes
• Were the field Ioading rates for each metal and PAN calculated (year to date)? I.e.,$
• Were the cumulative pollutant loading rates calculated?.y-rS'
• Were the calculations correct?,Y O
• Were the PAN loading rates. within permit limits? V-0-5
• Were the heavy metal cumulative pollutant loading rates within permit limits?'��'�
• Were the residuals applied on a suitable crop?,y115
• Were the applications conducted during the crop's growing season?•Y•.,eS
• Were the Field Summary Forms complete?
7-
4. Pathogen and Vector Attraction Reduction
• Was a signed copy of the Pathal and Vector Attraction eduction Form submjtted?
• Did the form inatethe period of coverage,"the residuaIclass, and the pathogen reduction aiL--wative and the
vector attraction reduction option used'?
•. Was the appr priate documentatt� to show pathogen and vector attraction reduction included in the report?
• Was pathog n and vector attraction reduction demonstrated according to 40 CFR Part 503'?
�'�-GN'� _tit •
5. Soil Tests'
• Was a Standard Soil Fertility Analysis cotidueted for each application field.y
• Were the soil pH's 6.0 or greater for each application field? N1.v5
Were the copper and zinc indexes in the soil less than 3000 fbr each application field?,
0/11
6. General re�&t,(-(-J', zn
• Was the report in tJX proper format? I U
• Were, any parts of the annual report misbLag? 6
• Was the report submitted on time?
N ov-aot5-- PC- o(9 55 PC-Ace157:- ®�
Any violations of ceiling concentrations should be reported to.'Pret"reafient for- municipalities. only.

Vector Attraction Reduction Review]
• Was the sampling conducted at the required frequency?
38% Volatile Solids Reduction
• Was there 38% reduction?
• Were lab sheets/calculations in report?
• Was the reduction on volatile solids (not -total solids)?
• Was the samples taken at beginning of digestion process and before application
(Inspection)?
• Were calculations correct?
40-Dav Bench Scale Test
• Were residuals from anaerobically digested treatment (Inspection)?
• Were residuals anaerobically digested in lab?
• Was the test ran for 40 days?
• Was the test done between 30°C (86°F) and 37C (99°F)?
• Was the reduction on volatile solids (not total solids)?
• Was the reduction less than 17%?
• Were lab sheets/calculations in report?
• Were calculations correct?
30-Dav Bench Scale Test
• Were residuals from aerobically digested treatment (Inspection)?
• Were residuals aerobically digested in lab?
• Were residuals 2% or less total solids?
• Was the test run for 30 days?
• Was the test done at 20°C (680F)?
• Was the reduction on volatile solids (not total solids)?
• Was the reduction less than 15%?.
• Were lab' sheets/calculations. in report?
• Were calculations correct?
Specific Oxygen Uptake Rate (SOURI
• Were residuals from aerobically digested treatment (Inspection)? y-"-,5
• Were residuals 2% or less total solids (dry weight basis) (not diluted)?/ P's
• Was the test done between 10°C (50°F) and 30°C (86°F)? 7 -s
• Was the temperature corrected to 20°C (68°F)? y �S
• Was the'SOUR equal to or less than. 1.5 mg of oxygen per hour per gram of total residual
solids (dry weight basis)? yw�5
• Was the sample holding time under two hours? �(�S
• Was the test started within15 minutes of sampling or aeration maintained?Y'S'

Alternative 5 - Process To Further Reduce Pathogens
PFRP Composting
• Were the within -vessel method or static aerated pile methods used?
0 Was the residuals temperature maintained at 55°C (131°F) or higher for three consecutive days or longer
in the within -vessel method or static aerated pile method?
OR
Was the windrow composting method used?
Was the residuals temperature maintained at 55°C or higher for 15 consecutive days or longer in the
windrow method, and the windrow turned a minimum of five times during this time?
PFRP Heat Drying
• Was the residuals dried by direct or indirect with hot gases and moisture content of residuals reduced to
10% or lower?
• Did. the temperature of the residuals or the of the wet bulb temperature of the gas in contact with the
residuals as they leave the dryer exceed 80°C (176°F)?
PFRP Heat Treatment
• Were the residuals liquid during treatment?
• Were the residuals heated to a temperature of 180°C (356°F) or higher, for 30 minutes?
PFRP Thermophilic Aerobic Digestion_
• Were the residuals liquid *during treatment?
•. Was it anaerobic process with agitation?
• Was the mean cell residence time 10 consecutive days. at 55°C (131°F) to 60°C (140°F)?
PFRP Beta Ray Irradiation
• Were residuals radiated with beta rays at dosages -of at least 1.0 megarad at room temperature
[approximately 20°C (68°F)]?
PFRP Gamma Ray Irradiation
• Were residuals radiated with gamma rays from certain isotopes, such as Cobalt 60 and Cesium 137; at
dosages of at least 1.0 megarad at room'temperature [approximately 20°C (68°F)]?
PFRP Pasteurization
. • Was the temperature of the residuals maintained at 70°C (158°F) for 30 minutes or longer?

Class B Pathogen Review
Alternative 1- Fecal Coliform Density `/ _ / a p �— a•� a 45 f
• Was the sampling conducted at the required frequency?
P q
• Were seven samples taken? ' d
• Was the geometric mean calculated and done correctly? y
• Did the results show compliance (less than either 2,000,000 MPN/gram of total solids or 2,000,000
Colony Forming Units/gram of total solids) �r es
Alternative 2 - Use of Process to Significantly Reduce Patho ens (one of five)
• Was the sampling conducted at the required frequency?
Aerobic Digestion
• Was it an aerobic process (Inspection)?
• Were logs submitted showing time and temperature?
• Were temperatures within range for complete time period?
• Was.the time and temperature between 40 days at 20°C (68T) and 60 days at 150C (590F)?
Air DKyin
• Were residuals on sand beds or pave or unpaved basins for three months?
• Was the.ambient.temperatur6 above 0°C (32T) for two months?
• Were the residuals partially digested?
• Were residuals exposed to atmosphere during two months above 0°C (not snow covered)?
Anaerobic Dijzestion
• Was it an anaerobic process (Inspection)?
• Were logs submitted showing time and temperature?
• Were temperatures within range for complete time period?
• Was the time and temperature between 15 days at 35°C (95T) to 55°C (13IT) and 60 days at 200C
(68-F)?
Composting
• Was it a. composting procedure (not natural decay under uncontrolled conditions)?
• Were logs submitted showing time and temperature?
• Was the temperature raised to 40°C (104T) or higher and remained at 40°C (104T) for five days?
• Did the temperature exceed 55°C (13 PF) for four hours during the five-day period?
Lime Stabilization
• Was alkaline material added to residuals a form of lime (hydrated lime, quicklime, lime containing
kiln dust or fly ash)?
• Were logs submitted showing time and temperature?
• Was the pH raised to 12 after two hours of contact?
• Were logs submitted showing time and pH?
• Was the temperature corrected to 25°C (77°F)?