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HomeMy WebLinkAboutWQ0013419_Sludge Landfill Monitoring Report November 2021_20211109leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 November 19, 2021 Mr. Mike Cody Glatfelter Corp. 228 South Main Street Spring Grove, PA 17362 RE: Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Dear Mr. Cody: Enclosed are the analytical results for sample(s) received by the laboratory between November 01, 2021 and November 03, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Lord Patton lorri.patton@pacelabs.com 1(828)254-7176 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 VirginiaNELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Project: Pace Project No.: Glatfelter Sludge Landfill 92569918 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92569918001 WQ0013419-SWP1 EPA 6010D CBV 18 PASI-A EPA 1631E RDT 1 PASI-A EPA 8270E PKS 74 PASI-C EPA 8260D SAS 63 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 5310B-2014 MDW 1 PASI-A 92569918002 WQ0013419-SWP2 EPA 6010D CBV 18 PASI-A EPA 1631E RDT 1 PASI-A EPA 8270E PKS 74 PASI-C EPA 8260D SAS 63 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 5310B-2014 MDW 1 PASI-A 92569918003 FIELD BLANK EPA 1631E RDT 1 PASI-A 92569918004 WQ0013419-Q06V09 EPA 6010D CBV 18 PASI-A EPA 1631E RDT 1 PASI-A EPA 8270E PKS 74 PASI-C EPA 8260D CL 63 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 5310B-2014 MDW 1 PASI-A 92569918005 WQ0013419-Q06V10 EPA 6010D DS 18 PASI-A EPA 1631E RDT 1 PASI-A EPA 8270E PKS 74 PASI-C EPA 8260D CL 63 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 2540C-2015 MJP 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 5310B-2014 MDW 1 PASI-A 92569918006 WQ0013419-Q06V11 EPA 6010D CBV 18 PASI-A EPA 1631E RDT 1 PASI-A EPA 8270E PKS 74 PASI-C EPA 8260D CL 63 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 5310B-2014 MDW 1 PASI-A 92569918007 TRIP BLANK EPA 8260D NSCQ 63 PASI-C EPA 8260D Mod. LMB 3 PASI-C PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SUMMARY OF DETECTION Project: Pace Project No.: Glatfelter Sludge Landfill 92569918 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92569918001 WQ0013419-SWP1 Performed by Pace 11/18/21 14:29 Collected By J.Zambanin i 11/18/21 14:29 Collected Date 11/1/21 11/18/21 14:29 Collected Time 10:55 11/18/21 14:29 pH 7.9 Std. Units 11/18/21 14:29 Temperature 14.5 deg C 11/18/21 14:29 Specific Conductance 914 umhos/cm 11/18/21 14:29 Oxygen, Dissolved 8.2 mg/L 11/18/21 14:29 REDOX 57.2 mV 11/18/21 14:29 Turbidity 85.0 NTU 11/18/21 14:29 Odor Foul 11/18/21 14:29 Appearance Dirty 11/18/21 14:29 EPA 601OD Barium 184 ug/L 5.0 11/12/2103:19 EPA 601OD Calcium 95200 ug/L 100 11/12/2103:19 EPA 601OD Cobalt 12.9 ug/L 5.0 11/12/2103:19 EPA 601OD Magnesium 45300 ug/L 100 11/12/2103:19 EPA 601OD Potassium 9810 ug/L 5000 11/12/2103:19 EPA 601OD Sodium 26300 ug/L 5000 11/12/2103:19 EPA 601OD Vanadium 22.8 ug/L 5.0 11/12/2103:19 SM 2320B-2011 Alkalinity, Total as CaCO3 543 mg/L 5.0 11/08/21 18:03 SM 2540C-2015 Total Dissolved Solids 494 mg/L 25.0 11/03/21 10:33 EPA 300.0 Rev 2.1 1993 Sulfate 0.65J mg/L 1.0 11/03/21 04:04 SM 4500-CI-E-2011 Chloride 27.9 mg/L 1.0 11/10/21 21:47 SM 531OB-2014 Total Organic Carbon 7.3 mg/L 1.0 11/16/21 06:06 92569918002 WQ0013419-SWP2 Performed by Pace 11/18/21 14:31 Collected By J.Zambanin i 11/18/21 14:31 Collected Date 11/1/21 11/18/21 14:31 Collected Time 10:20 11/18/21 14:31 pH 6.9 Std. Units 11/18/21 14:31 Temperature 13.1 deg C 11/18/21 14:31 Specific Conductance 242.1 umhos/cm 11/18/21 14:31 Oxygen, Dissolved 7.1 mg/L 11/18/21 14:31 REDOX 58.0 mV 11/18/21 14:31 Turbidity 27.4 NTU 11/18/21 14:31 Odor None 11/18/21 14:31 Appearance Clear 11/18/21 14:31 EPA 601OD Barium 107 ug/L 5.0 11/12/2103:22 EPA 601OD Calcium 28500 ug/L 100 11/12/2103:22 EPA 601OD Cobalt 11.4 ug/L 5.0 11/12/2103:22 EPA 601OD Magnesium 5950 ug/L 100 11/12/2103:22 EPA 601OD Sodium 11400 ug/L 5000 11/12/2103:22 EPA 601OD Vanadium 26.7 ug/L 5.0 11/12/2103:22 SM 2320B-2011 Alkalinity, Total as CaCO3 110 mg/L 5.0 11/08/21 18:21 SM 2540C-2015 Total Dissolved Solids 132 mg/L 25.0 11/03/21 10:34 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Lab Sample ID Method 92569918002 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92569918004 EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 SM 5310B-2014 92569918005 Client Sample ID Parameters WO0013419-SWP2 Sulfate Chloride WO0013419-QO6V09 Performed by Collected By Collected Date Collected Time pH Temperature Static Water Level Specific Conductance Oxygen, Dissolved Total Well Depth REDOX Turbidity Odor Appearance Antimony Arsenic Barium Calcium Cobalt Magnesium Nickel Potassium Sodium Vanadium Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride Total Organic Carbon WQ0013419-Q06V10 Performed by Collected By Collected Date Collected Time pH Temperature Static Water Level Specific Conductance Oxygen, Dissolved Total Well Depth REDOX SUMMARY OF DETECTION Result Units 3.4 mg/L 3.2 mg/L Pace J.Zambanin 11/2/21 11:30 6.5 14.6 29.68 1331 1.1 70.44 73.8 22.1 None Slightly cloudy 3.OJ 5.3J 304 161000 11.9 82900 16.9 4880J 33900 43.1 745 780 2.5 48.4 4.6 Pace J.Zambanin 11/2/21 09:55 5.4 13.9 27.84 33.3 2.5 32.40 43.1 Std. Units deg C feet umhos/cm mg/L feet mV NTU ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L mg/L mg/L mg/L mg/L mg/L Std. Units deg C feet umhos/cm mg/L feet mV REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Report Limit Analyzed Qualifiers 1.0 11 /03/21 04:18 1.0 11/10/21 21:48 11/18/21 14:33 11/18/21 14:33 11/18/21 14:33 11/18/21 14:33 11/18/21 14:33 11/18/21 14:33 11/18/21 14:33 11/18/21 14:33 11/18/21 14:33 11/18/21 14:33 11/18/21 14:33 11/18/21 14:33 11/18/21 14:33 11/18/21 14:33 5.0 11 /12/21 03:26 10.0 11/12/2115:18 B,BC 5.0 11 /12/21 03:26 500 11 /12/21 15:15 5.0 11 /12/21 03:26 100 11 /12/21 03:26 5.0 11 /12/21 03:26 5000 11 /12/21 03:26 5000 11 /12/21 03:26 5.0 11 /12/21 03:26 5.0 11 /08/21 20:48 50.0 11/04/21 11:00 1.0 11/05/21 01:18 2.0 11/10/21 21:49 1.0 11/16/21 07:21 11/18/21 14:34 11/18/21 14:34 11/18/21 14:34 11/18/21 14:34 11/18/21 14:34 11/18/21 14:34 11/18/21 14:34 11/18/21 14:34 11/18/21 14:34 11/18/21 14:34 11/18/21 14:34 Page 6 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Lab Sample ID Method 92569918005 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 1631 E SM 2320B-2011 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92569918006 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 1631 E SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 Client Sample ID Parameters W00013419-Q06V10 Turbidity Odor Appearance Barium Calcium Magnesium Sodium Mercury Alkalinity, Total as CaCO3 Sulfate Chloride WQ0013419-Q06V11 Performed by Collected By Collected Date Collected Time pH Temperature Static Water Level Specific Conductance Oxygen, Dissolved Total Well Depth REDOX Turbidity Odor Appearance Barium Calcium Magnesium Sodium Zinc Mercury Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride SUMMARY OF DETECTION Result 6.0 None Clear 5.7 2220 826 2280J 2.83 12.1 0.85J 2.5 Pace J.Zambanin 11/2/21 10:30 5.5 12.9 40.01 62.5 3.2 57.82 49.1 7.0 None Clear 6.9 4460 2150 5110 12.7 1.16 22.4 43.0 3.0 1.9 Units Report Limit Analyzed NTU 11/18/21 14:34 11/18/21 14:34 11/18/21 14:34 ug/L 5.0 11 /05/21 19:55 ug/L 100 11 /05/21 19:55 ug/L 100 11 /05/21 19:55 ug/L 5000 11 /05/21 19:55 ng/L 0.50 11/18/21 14:37 mg/L 5.0 11 /08/21 20:15 mg/L 1.0 11 /05/21 02:03 mg/L 1.0 11/10/21 21:50 Std. Units deg C feet umhos/cm mg/L feet my NTU ug/L ug/L ug/L ug/L ug/L ng/L mg/L mg/L mg/L mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11/18/21 14:36 11/18/21 14:36 11/18/21 14:36 11/18/21 14:36 11/18/21 14:36 11/18/21 14:36 11/18/21 14:36 11/18/21 14:36 11/18/21 14:36 11/18/21 14:36 11/18/21 14:36 11/18/21 14:36 11/18/21 14:36 11/18/21 14:36 5.0 11 /12/21 03:29 100 11 /12/21 03:29 100 11 /12/21 03:29 5000 11 /12/21 03:29 10.0 11/12/2103:29 BC 0.50 11/18/21 14:45 5.0 11 /08/21 20:21 25.0 11/04/21 11:00 1.0 11 /05/21 02:18 1.0 11/10/21 21:50 Page 7 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-SWP1 Lab ID: 92569918001 Collected: 11/01/21 10:55 Received: 11/01/21 17:15 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by Pace 1 11/18/21 14:29 Collected By J.Zambani 1 11/18/21 14:29 ni Collected Date 11/1121 1 11/18/21 14:29 Collected Time 10:55 1 11/18/21 14:29 pH 7.9 Std. Units 1 11/18/21 14:29 Temperature 14.5 deg C 1 11/18/21 14:29 Specific Conductance 914 umhos/cm 1 11/18/21 14:29 Oxygen, Dissolved 8.2 mg/L 1 11/18/21 14:29 7782-44-7 REDOX 57.2 mV 1 11/18/21 14:29 Turbidity 85.0 NTU 1 11/18/21 14:29 Odor Foul 1 11/18/21 14:29 Appearance Dirty 1 11/18/21 14:29 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 1 11/11/2110:54 11/12/2103:19 7440-36-0 Arsenic ND ug/L 10.0 1 11/11/2110:54 11/12/2103:19 7440-38-2 BC Barium 184 ug/L 5.0 1 11/11/2110:54 11/12/2103:19 7440-39-3 Cadmium ND ug/L 1.0 1 11/11/2110:54 11/12/2103:19 7440-43-9 Calcium 95200 ug/L 100 1 11/11/2110:54 11/12/2103:19 7440-70-2 Chromium ND ug/L 5.0 1 11/11/2110:54 11/12/2103:19 7440-47-3 Cobalt 12.9 ug/L 5.0 1 11/11/2110:54 11/12/2103:19 7440-48-4 Copper ND ug/L 5.0 1 11/11/2110:54 11/12/2103:19 7440-50-8 Lead ND ug/L 5.0 1 11/11/2110:54 11/12/2103:19 7439-92-1 Magnesium 45300 ug/L 100 1 11/11/2110:54 11/12/2103:19 7439-95-4 Nickel ND ug/L 5.0 1 11/11/2110:54 11/12/2103:19 7440-02-0 Potassium 9810 ug/L 5000 1 11/11/2110:54 11/12/2103:19 7440-09-7 Selenium ND ug/L 10.0 1 11/11/2110:54 11/12/2103:19 7782-49-2 Silver ND ug/L 5.0 1 11/11/2110:54 11/12/2103:19 7440-22-4 Sodium 26300 ug/L 5000 1 1111112110:54 11/12/2103:19 7440-23-5 Thallium ND ug/L 10.0 1 1111112110:54 11/12/2103:19 7440-28-0 Vanadium 22.8 ug/L 5.0 1 1111112110:54 11/12/2103:19 7440-62-2 Zinc ND ug/L 10.0 1 1111112110:54 11/12/2103:19 7440-66-6 BC 1631E Mercury,Low Level Analytical Method: EPA 1631 E Preparation Method: EPA 1631 E Pace Analytical Services -Asheville Mercury ND ng/L 0.50 1 11/17/2115:35 11/18/2113:58 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Acenaphthene ND ug/L 9.1 1 11/03/2105:50 11/03/2122:08 83-32-9 Acenaphthylene ND ug/L 9.1 1 11/03/2105:50 11/03/2122:08 208-96-8 Aniline ND ug/L 9.1 1 11/03/2105:50 11/03/2122:08 62-53-3 v1 Anthracene ND ug/L 9.1 1 11/03/2105:50 11/03/2122:08 120-12-7 Benzo(a)anthracene ND ug/L 9.1 1 11/03/2105:50 11/03/2122:08 56-55-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-SWP1 Lab ID: 92569918001 Collected: 11/01/21 10:55 Received: 11/01/21 17:15 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)pyrene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 50-32-8 Benzo(b)fluoranthene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 205-99-2 Benzo(g,h,i)perylene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 191-24-2 Benzo(k)fluoranthene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 207-08-9 Benzoic Acid ND ug/L 45.5 1 11/03/21 05:50 11/03/21 22:08 65-85-0 Benzyl alcohol ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:08 100-51-6 4-Bromophenylphenyl ether ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 101-55-3 Butylbenzylphthalate ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 85-68-7 4-Chloro-3-methyl phenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 59-50-7 4-Chloroaniline ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:08 106-47-8 bis(2-Chloroethoxy)methane ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 111-91-1 bis(2-Chloroethyl) ether ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 111-44-4 2-Chloronaphthalene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 91-58-7 2-Chlorophenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 95-57-8 4-Chlorophenylphenyl ether ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 7005-72-3 Chrysene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 218-01-9 Dibenz(a,h)anthracene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 53-70-3 Dibenzofuran ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 132-64-9 1,2-Dichlorobenzene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 95-50-1 1,3-Dichlorobenzene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 541-73-1 1,4-Dichlorobenzene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 106-46-7 3,3'-Dichlorobenzidine ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:08 91-94-1 2,4-Dichlorophenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 120-83-2 Diethylphthalate ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 84-66-2 2,4-Dimethylphenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 105-67-9 Dimethylphthalate ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 131-11-3 Di-n-butylphthalate ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:08 534-52-1 2,4-Dinitrophenol ND ug/L 45.5 1 11/03/21 05:50 11/03/21 22:08 51-28-5 2,4-Dinitrotoluene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 121-14-2 2,6-Dinitrotoluene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 606-20-2 Di-n-octylphthalate ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/L 5.5 1 11/03/21 05:50 11/03/21 22:08 117-81-7 Fluoranthene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 206-44-0 Fluorene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 86-73-7 Hexachloro-1,3-butadiene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 87-68-3 Hexachlorobenzene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 118-74-1 Hexachlorocyclopentadiene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 77-47-4 Hexachloroethane ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 193-39-5 Isophorone ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 78-59-1 1-Methylnaphthalene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 90-12-0 2-Methylnaphthalene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 91-57-6 2-Methylphenol(o-Cresol) ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 15831-10-4 Naphthalene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 91-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-SWP1 Lab ID: 92569918001 Collected: 11/01/21 10:55 Received: 11/01/21 17:15 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 2-Nitroaniline ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:08 88-74-4 3-Nitroaniline ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:08 99-09-2 4-Nitroaniline ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:08 100-01-6 Nitrobenzene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 98-95-3 2-Nitrophenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 88-75-5 4-Nitrophenol ND ug/L 45.5 1 11/03/21 05:50 11/03/21 22:08 100-02-7 N-Nitrosodimethylamine ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 621-64-7 N-Nitrosodiphenylamine ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 108-60-1 Pentachlorophenol ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:08 87-86-5 Phenanthrene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 85-01-8 Phenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 108-95-2 Pyrene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 129-00-0 1,2,4-Trichlorobenzene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 120-82-1 2,4,5-Trichlorophenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 95-95-4 2,4,6-Trichlorophenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:08 88-06-2 Surrogates Nitrobenzene-d5 (S) 81 % 10-144 1 11/03/21 05:50 11/03/21 22:08 4165-60-0 2-Fluorobiphenyl (S) 68 % 10-130 1 11/03/21 05:50 11/03/21 22:08 321-60-8 Terphenyl-d14 (S) 116 % 34-163 1 11/03/21 05:50 11/03/21 22:08 1718-51-0 Phenol-d6 (S) 40 % 10-130 1 11/03/21 05:50 11/03/21 22:08 13127-88-3 2-Fluorophenol (S) 39 % 10-130 1 11/03/21 05:50 11/03/21 22:08 367-12-4 2,4,6-Tribromophenol (S) 47 % 10-144 1 11/03/21 05:50 11/03/21 22:08 118-79-6 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 1 11/04/21 08:42 67-64-1 Benzene ND ug/L 1.0 1 11/04/21 08:42 71-43-2 Bromobenzene ND ug/L 1.0 1 11/04/21 08:42 108-86-1 Bromochloromethane ND ug/L 1.0 1 11/04/21 08:42 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/04/21 08:42 75-27-4 Bromoform ND ug/L 1.0 1 11/04/21 08:42 75-25-2 Bromomethane ND ug/L 2.0 1 11/04/21 08:42 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/04/21 08:42 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 11/04/21 08:42 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/04/21 08:42 108-90-7 Chloroethane ND ug/L 1.0 1 11/04/21 08:42 75-00-3 Chloroform ND ug/L 1.0 1 11/04/21 08:42 67-66-3 Chloromethane ND ug/L 1.0 1 11/04/21 08:42 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 11/04/21 08:42 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 11/04/21 08:42 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/04/21 08:42 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/04/21 08:42 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/04/21 08:42 106-93-4 Dibromomethane ND ug/L 1.0 1 11/04/21 08:42 74-95-3 REPORT OF LABORATORY ANALYSIS v2 This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-SWP1 Parameters 8260D MSV Low Level Landfill 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) ANALYTICAL RESULTS Lab ID: 92569918001 Collected: 11/01/21 10:55 Received: 11/01/21 17:15 Matrix: Water Results Units Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 94 % 92 % 108 % PQL DF Prepared Analyzed CAS No 1.0 1 11/04/21 08:42 95-50-1 1.0 1 11/04/21 08:42 541-73-1 1.0 1 11/04/21 08:42 106-46-7 1.0 1 11/04/21 08:42 75-71-8 1.0 1 11/04/21 08:42 75-34-3 1.0 1 11/04/21 08:42 107-06-2 1.0 1 11/04/21 08:42 75-35-4 1.0 1 11/04/21 08:42 156-59-2 1.0 1 11/04/21 08:42 156-60-5 1.0 1 11/04/21 08:42 78-87-5 1.0 1 11/04/21 08:42 142-28-9 1.0 1 11/04/21 08:42 594-20-7 1.0 1 11/04/21 08:42 563-58-6 1.0 1 11/04/21 08:42 10061-01-5 1.0 1 11/04/21 08:42 10061-02-6 1.0 1 11/04/21 08:42 108-20-3 1.0 1 11/04/21 08:42 100-41-4 2.0 1 11/04/21 08:42 87-68-3 5.0 1 11/04/21 08:42 591-78-6 1.0 1 11/04/21 08:42 99-87-6 5.0 1 11/04/21 08:42 75-09-2 5.0 1 11/04/21 08:42 108-10-1 1.0 1 11/04/21 08:42 1634-04-4 1.0 1 11/04/21 08:42 91-20-3 1.0 1 11/04/21 08:42 100-42-5 1.0 1 11/04/21 08:42 630-20-6 1.0 1 11/04/21 08:42 79-34-5 1.0 1 11/04/21 08:42 127-18-4 1.0 1 11/04/21 08:42 108-88-3 1.0 1 11/04/21 08:42 87-61-6 1.0 1 11/04/21 08:42 120-82-1 1.0 1 11/04/21 08:42 71-55-6 1.0 1 11/04/21 08:42 79-00-5 1.0 1 11/04/21 08:42 79-01-6 1.0 1 11/04/21 08:42 75-69-4 1.0 1 11/04/21 08:42 96-18-4 2.0 1 11/04/21 08:42 108-05-4 1.0 1 11/04/21 08:42 75-01-4 1.0 1 11/04/21 08:42 1330-20-7 2.0 1 11/04/21 08:42 179601-23-1 1.0 1 11/04/21 08:42 95-47-6 70-130 1 70-130 1 70-130 1 REPORT OF LABORATORY ANALYSIS 11/04/21 08:42 460-00-4 11/04/21 08:42 17060-07-0 11/04/21 08:42 2037-26-5 Qual This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-SWP1 Lab ID: 92569918001 Collected: 11/01/21 10:55 Received: 11/01/21 17:15 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 11/03/21 16:41 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 88 % 70-130 1 11/03/21 16:41 17060-07-0 Toluene-d8 (S) 90 % 66-133 1 11/03/21 16:41 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 543 mg/L 5.0 1 11/08/21 18:03 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 494 mg/L 25.0 1 11/03/21 10:33 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 0.65J mg/L 1.0 1 11/03/2104:04 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 27.9 mg/L 1.0 1 11/10/2121:47 16887-00-6 5310B TOC Analytical Method: SM 531OB-2014 Pace Analytical Services -Asheville Total Organic Carbon 7.3 mg/L 1.0 1 11/16/21 06:06 7440-44-0 Date: 11/19/2021 04:40 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-SWP2 Lab ID: 92569918002 Collected: 11/01/21 10:20 Received: 11/01/21 17:15 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by Pace 1 11/18/21 14:31 Collected By J.Zambani 1 11/18/21 14:31 ni Collected Date 11/1/21 1 11/18/21 14:31 Collected Time 10:20 1 11/18/21 14:31 pH 6.9 Std. Units 1 11/18/21 14:31 Temperature 13.1 deg C 1 11/18/21 14:31 Specific Conductance 242.1 umhos/cm 1 11/18/21 14:31 Oxygen, Dissolved 7.1 mg/L 1 11/18/21 14:31 7782-44-7 REDOX 58.0 mV 1 11/18/21 14:31 Turbidity 27.4 NTU 1 11/18/21 14:31 Odor None 1 11/18/21 14:31 Appearance Clear 1 11/18/21 14:31 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 1 11/11/2110:54 11/12/2103:22 7440-36-0 Arsenic ND ug/L 10.0 1 11/11/2110:54 11/12/2103:22 7440-38-2 BC Barium 107 ug/L 5.0 1 11/11/2110:54 11/12/2103:22 7440-39-3 Cadmium ND ug/L 1.0 1 11/11/2110:54 11/12/2103:22 7440-43-9 Calcium 28500 ug/L 100 1 11/11/2110:54 11/12/2103:22 7440-70-2 Chromium ND ug/L 5.0 1 11/11/2110:54 11/12/2103:22 7440-47-3 Cobalt 11.4 ug/L 5.0 1 11/11/2110:54 11/12/2103:22 7440-48-4 Copper ND ug/L 5.0 1 11/11/2110:54 11/12/2103:22 7440-50-8 Lead ND ug/L 5.0 1 11/11/2110:54 11/12/2103:22 7439-92-1 Magnesium 5950 ug/L 100 1 11/11/2110:54 11/12/2103:22 7439-95-4 Nickel ND ug/L 5.0 1 11/11/2110:54 11/12/2103:22 7440-02-0 Potassium ND ug/L 5000 1 11/11/2110:54 11/12/2103:22 7440-09-7 Selenium ND ug/L 10.0 1 11/11/2110:54 11/12/2103:22 7782-49-2 Silver ND ug/L 5.0 1 11/11/2110:54 11/12/2103:22 7440-22-4 Sodium 11400 ug/L 5000 1 1111112110:54 11/12/2103:22 7440-23-5 Thallium ND ug/L 10.0 1 1111112110:54 11/12/2103:22 7440-28-0 Vanadium 26.7 ug/L 5.0 1 1111112110:54 11/12/2103:22 7440-62-2 Zinc ND ug/L 10.0 1 1111112110:54 11/12/2103:22 7440-66-6 BC 1631E Mercury,Low Level Analytical Method: EPA 1631 E Preparation Method: EPA 1631 E Pace Analytical Services -Asheville Mercury ND ng/L 0.50 1 11/17/2115:35 11/18/2114:22 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Acenaphthene ND ug/L 9.1 1 11/03/2105:50 11/03/2122:33 83-32-9 Acenaphthylene ND ug/L 9.1 1 11/03/2105:50 11/03/2122:33 208-96-8 Aniline ND ug/L 9.1 1 11/03/2105:50 11/03/2122:33 62-53-3 v1 Anthracene ND ug/L 9.1 1 11/03/2105:50 11/03/2122:33 120-12-7 Benzo(a)anthracene ND ug/L 9.1 1 11/03/2105:50 11/03/2122:33 56-55-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-SWP2 Lab ID: 92569918002 Collected: 11/01/21 10:20 Received: 11/01/21 17:15 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)pyrene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 50-32-8 Benzo(b)fluoranthene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 205-99-2 Benzo(g,h,i)perylene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 191-24-2 Benzo(k)fluoranthene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 207-08-9 Benzoic Acid ND ug/L 45.5 1 11/03/21 05:50 11/03/21 22:33 65-85-0 Benzyl alcohol ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:33 100-51-6 4-Bromophenylphenyl ether ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 101-55-3 Butylbenzylphthalate ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 85-68-7 4-Chloro-3-methyl phenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 59-50-7 4-Chloroaniline ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:33 106-47-8 bis(2-Chloroethoxy)methane ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 111-91-1 bis(2-Chloroethyl) ether ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 111-44-4 2-Chloronaphthalene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 91-58-7 2-Chlorophenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 95-57-8 4-Chlorophenylphenyl ether ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 7005-72-3 Chrysene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 218-01-9 Dibenz(a,h)anthracene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 53-70-3 Dibenzofuran ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 132-64-9 1,2-Dichlorobenzene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 95-50-1 1,3-Dichlorobenzene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 541-73-1 1,4-Dichlorobenzene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 106-46-7 3,3'-Dichlorobenzidine ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:33 91-94-1 2,4-Dichlorophenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 120-83-2 Diethylphthalate ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 84-66-2 2,4-Dimethylphenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 105-67-9 Dimethylphthalate ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 131-11-3 Di-n-butylphthalate ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:33 534-52-1 2,4-Dinitrophenol ND ug/L 45.5 1 11/03/21 05:50 11/03/21 22:33 51-28-5 2,4-Dinitrotoluene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 121-14-2 2,6-Dinitrotoluene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 606-20-2 Di-n-octylphthalate ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/L 5.5 1 11/03/21 05:50 11/03/21 22:33 117-81-7 Fluoranthene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 206-44-0 Fluorene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 86-73-7 Hexachloro-1,3-butadiene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 87-68-3 Hexachlorobenzene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 118-74-1 Hexachlorocyclopentadiene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 77-47-4 Hexachloroethane ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 193-39-5 Isophorone ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 78-59-1 1-Methylnaphthalene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 90-12-0 2-Methylnaphthalene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 91-57-6 2-Methylphenol(o-Cresol) ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 15831-10-4 Naphthalene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 91-20-3 REPORT OF LABORATORY ANALYSIS Qual This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-SWP2 Lab ID: 92569918002 Collected: 11/01/21 10:20 Received: 11/01/21 17:15 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 2-Nitroaniline ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:33 88-74-4 3-Nitroaniline ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:33 99-09-2 4-Nitroaniline ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:33 100-01-6 Nitrobenzene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 98-95-3 2-Nitrophenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 88-75-5 4-Nitrophenol ND ug/L 45.5 1 11/03/21 05:50 11/03/21 22:33 100-02-7 N-Nitrosodimethylamine ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 621-64-7 N-Nitrosodiphenylamine ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 108-60-1 Pentachlorophenol ND ug/L 18.2 1 11/03/21 05:50 11/03/21 22:33 87-86-5 Phenanthrene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 85-01-8 Phenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 108-95-2 Pyrene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 129-00-0 1,2,4-Trichlorobenzene ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 120-82-1 2,4,5-Trichlorophenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 95-95-4 2,4,6-Trichlorophenol ND ug/L 9.1 1 11/03/21 05:50 11/03/21 22:33 88-06-2 Surrogates Nitrobenzene-d5 (S) 81 % 10-144 1 11/03/21 05:50 11/03/21 22:33 4165-60-0 2-Fluorobiphenyl (S) 66 % 10-130 1 11/03/21 05:50 11/03/21 22:33 321-60-8 Terphenyl-d14 (S) 104 % 34-163 1 11/03/21 05:50 11/03/21 22:33 1718-51-0 Phenol-d6 (S) 39 % 10-130 1 11/03/21 05:50 11/03/21 22:33 13127-88-3 2-Fluorophenol (S) 38 % 10-130 1 11/03/21 05:50 11/03/21 22:33 367-12-4 2,4,6-Tribromophenol (S) 36 % 10-144 1 11/03/21 05:50 11/03/21 22:33 118-79-6 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 1 11/04/21 09:01 67-64-1 Benzene ND ug/L 1.0 1 11/04/21 09:01 71-43-2 Bromobenzene ND ug/L 1.0 1 11/04/21 09:01 108-86-1 Bromochloromethane ND ug/L 1.0 1 11/04/21 09:01 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/04/21 09:01 75-27-4 Bromoform ND ug/L 1.0 1 11/04/21 09:01 75-25-2 Bromomethane ND ug/L 2.0 1 11/04/21 09:01 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/04/21 09:01 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 11/04/21 09:01 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/04/21 09:01 108-90-7 Chloroethane ND ug/L 1.0 1 11/04/21 09:01 75-00-3 Chloroform ND ug/L 1.0 1 11/04/21 09:01 67-66-3 Chloromethane ND ug/L 1.0 1 11/04/21 09:01 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 11/04/21 09:01 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 11/04/21 09:01 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/04/21 09:01 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/04/21 09:01 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/04/21 09:01 106-93-4 Dibromomethane ND ug/L 1.0 1 11/04/21 09:01 74-95-3 REPORT OF LABORATORY ANALYSIS v2 This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-SWP2 Parameters 8260D MSV Low Level Landfill 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) ANALYTICAL RESULTS Lab ID: 92569918002 Collected: 11/01/21 10:20 Received: 11/01/21 17:15 Matrix: Water Results Units Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 95 % 93 % 103 % PQL DF Prepared Analyzed CAS No 1.0 1 11/04/21 09:01 95-50-1 1.0 1 11/04/21 09:01 541-73-1 1.0 1 11/04/21 09:01 106-46-7 1.0 1 11/04/21 09:01 75-71-8 1.0 1 11/04/21 09:01 75-34-3 1.0 1 11/04/21 09:01 107-06-2 1.0 1 11/04/21 09:01 75-35-4 1.0 1 11/04/21 09:01 156-59-2 1.0 1 11/04/21 09:01 156-60-5 1.0 1 11/04/21 09:01 78-87-5 1.0 1 11/04/21 09:01 142-28-9 1.0 1 11/04/21 09:01 594-20-7 1.0 1 11/04/21 09:01 563-58-6 1.0 1 11/04/21 09:01 10061-01-5 1.0 1 11/04/21 09:01 10061-02-6 1.0 1 11/04/21 09:01 108-20-3 1.0 1 11/04/21 09:01 100-41-4 2.0 1 11/04/21 09:01 87-68-3 5.0 1 11/04/21 09:01 591-78-6 1.0 1 11/04/21 09:01 99-87-6 5.0 1 11/04/21 09:01 75-09-2 5.0 1 11/04/21 09:01 108-10-1 1.0 1 11/04/21 09:01 1634-04-4 1.0 1 11/04/21 09:01 91-20-3 1.0 1 11/04/21 09:01 100-42-5 1.0 1 11/04/21 09:01 630-20-6 1.0 1 11/04/21 09:01 79-34-5 1.0 1 11/04/21 09:01 127-18-4 1.0 1 11/04/21 09:01 108-88-3 1.0 1 11/04/21 09:01 87-61-6 1.0 1 11/04/21 09:01 120-82-1 1.0 1 11/04/21 09:01 71-55-6 1.0 1 11/04/21 09:01 79-00-5 1.0 1 11/04/21 09:01 79-01-6 1.0 1 11/04/21 09:01 75-69-4 1.0 1 11/04/21 09:01 96-18-4 2.0 1 11/04/21 09:01 108-05-4 1.0 1 11/04/21 09:01 75-01-4 1.0 1 11/04/21 09:01 1330-20-7 2.0 1 11/04/21 09:01 179601-23-1 1.0 1 11/04/21 09:01 95-47-6 70-130 1 70-130 1 70-130 1 REPORT OF LABORATORY ANALYSIS 11/04/21 09:01 460-00-4 11/04/21 09:01 17060-07-0 11/04/21 09:01 2037-26-5 Qual This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-SWP2 Lab ID: 92569918002 Collected: 11/01/21 10:20 Received: 11/01/21 17:15 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 11/03/21 17:00 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/03/21 17:00 17060-07-0 Toluene-d8 (S) 91 % 66-133 1 11/03/21 17:00 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 110 mg/L 5.0 1 11/08/21 18:21 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 132 mg/L 25.0 1 11/03/21 10:34 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 3.4 mg/L 1.0 1 11/03/2104:18 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 3.2 mg/L 1.0 1 11/10/2121:48 16887-00-6 5310B TOC Analytical Method: SM 531OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 11/16/21 06:26 7440-44-0 Date: 11/19/2021 04:40 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: FIELD BLANK Lab ID: 92569918003 Collected: 11/01/21 16:05 Received: 11/01/21 17:15 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 1631E Mercury,Low Level Analytical Method: EPA 1631 E Preparation Method: EPA 1631 E Pace Analytical Services -Asheville Mercury ND ng/L 0.50 1 11/17/2115:35 11/18/2113:27 7439-97-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V09 Lab ID: 92569918004 Collected: 11/02/21 11:30 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by Pace 1 11/18/21 14:33 Collected By J.Zambani 1 11/18/21 14:33 ni Collected Date 11/2121 1 11/18/21 14:33 Collected Time 11:30 1 11/18/21 14:33 pH 6.5 Std. Units 1 11/18/21 14:33 Temperature 14.6 deg C 1 11/18/21 14:33 Static Water Level 29.68 feet 1 11/18/21 14:33 Specific Conductance 1331 umhos/cm 1 11/18/21 14:33 Oxygen, Dissolved 1.1 mg/L 1 11/18/21 14:33 7782-44-7 Total Well Depth 70.44 feet 1 11/18/21 14:33 REDOX 73.8 mV 1 11/18/21 14:33 Turbidity 22.1 NTU 1 11/18/21 14:33 Odor None 1 11/18/21 14:33 Appearance Slightly 1 11/18/21 14:33 cloudy 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony 3.OJ ug/L 5.0 1 11/11/2110:54 11/12/2103:26 7440-36-0 Arsenic 5.3J ug/L 10.0 1 11/11/2110:54 11/12/2115:18 7440-38-2 B,BC Barium 304 ug/L 5.0 1 11/11/2110:54 11/12/2103:26 7440-39-3 Cadmium ND ug/L 1.0 1 11/11/2110:54 11/12/2103:26 7440-43-9 Calcium 161000 ug/L 500 5 11/11/2110:54 11/12/2115:15 7440-70-2 Chromium ND ug/L 5.0 1 11/11/2110:54 11/12/2103:26 7440-47-3 Cobalt 11.9 ug/L 5.0 1 11/11/2110:54 11/12/2103:26 7440-48-4 Copper ND ug/L 5.0 1 11/11/2110:54 11/12/2103:26 7440-50-8 Lead ND ug/L 5.0 1 11/11/2110:54 11/12/2103:26 7439-92-1 Magnesium 82900 ug/L 100 1 11/11/2110:54 11/12/2103:26 7439-95-4 Nickel 16.9 ug/L 5.0 1 11/11/2110:54 11/12/2103:26 7440-02-0 Potassium 4880J ug/L 5000 1 11/11/2110:54 11/12/2103:26 7440-09-7 Selenium ND ug/L 10.0 1 11/11/2110:54 11/12/2103:26 7782-49-2 Silver ND ug/L 5.0 1 11/11/2110:54 11/12/2103:26 7440-22-4 Sodium 33900 ug/L 5000 1 11/11/2110:54 11/12/2103:26 7440-23-5 Thallium ND ug/L 10.0 1 11/11/2110:54 11/12/2103:26 7440-28-0 Vanadium 43.1 ug/L 5.0 1 11/11/2110:54 11/12/2103:26 7440-62-2 Zinc ND ug/L 10.0 1 11/11/2110:54 11/12/2115:18 7440-66-6 BC 1631E Mercury,Low Level Analytical Method: EPA 1631 E Preparation Method: EPA 1631 E Pace Analytical Services -Asheville Mercury ND ng/L 0.50 1 11/17/2115:35 11/18/2114:29 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Acenaphthene ND ug/L 9.1 1 11/05/2115:43 11/07/2112:56 83-32-9 Acenaphthylene ND ug/L 9.1 1 11/05/2115:43 11/07/2112:56 208-96-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V09 Lab ID: 92569918004 Collected: 11/02/21 11:30 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aniline ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 62-53-3 Anthracene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 120-12-7 Benzo(a)anthracene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 56-55-3 Benzo(a)pyrene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 50-32-8 Benzo(b)fluoranthene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 205-99-2 Benzo(g,h,i)perylene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 191-24-2 Benzo(k)fluoranthene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 207-08-9 Benzoic Acid ND ug/L 45.5 1 11/05/21 15:43 11/07/21 12:56 65-85-0 Benzyl alcohol ND ug/L 18.2 1 11/05/21 15:43 11/07/21 12:56 100-51-6 4-Bromophenylphenyl ether ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 101-55-3 Butylbenzylphthalate ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 59-50-7 4-Chloroaniline ND ug/L 18.2 1 11/05/21 15:43 11/07/21 12:56 106-47-8 bis(2-Chloroethoxy)methane ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 111-91-1 bis(2-Chloroethyl) ether ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 111-44-4 2-Chloronaphthalene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 91-58-7 2-Chlorophenol ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 95-57-8 4-Chlorophenylphenyl ether ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 7005-72-3 Chrysene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 218-01-9 Dibenz(a,h)anthracene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 53-70-3 Dibenzofuran ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 132-64-9 1,2-Dichlorobenzene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 95-50-1 1,3-Dichlorobenzene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 541-73-1 1,4-Dichlorobenzene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 106-46-7 3,3'-Dichlorobenzidine ND ug/L 18.2 1 11/05/21 15:43 11/07/21 12:56 91-94-1 2,4-Dichlorophenol ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 120-83-2 Diethylphthalate ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 84-66-2 2,4-Dimethylphenol ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 105-67-9 Dimethylphthalate ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 131-11-3 Di-n-butylphthalate ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 18.2 1 11/05/21 15:43 11/07/21 12:56 534-52-1 2,4-Dinitrophenol ND ug/L 45.5 1 11/05/21 15:43 11/07/21 12:56 51-28-5 2,4-Dinitrotoluene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 121-14-2 2,6-Dinitrotoluene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 606-20-2 Di-n-octylphthalate ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/L 5.5 1 11/05/21 15:43 11/07/21 12:56 117-81-7 Fluoranthene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 206-44-0 Fluorene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 86-73-7 Hexachloro-1,3-butadiene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 87-68-3 Hexachlorobenzene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 118-74-1 Hexachlorocyclopentadiene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 77-47-4 Hexachloroethane ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 193-39-5 Isophorone ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 78-59-1 1-Methylnaphthalene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 90-12-0 2-Methylnaphthalene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 91-57-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V09 Lab ID: 92569918004 Collected: 11/02/21 11:30 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 2-Methylphenol(o-Cresol) ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 15831-10-4 Naphthalene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 91-20-3 2-Nitroaniline ND ug/L 18.2 1 11/05/21 15:43 11/07/21 12:56 88-74-4 3-Nitroaniline ND ug/L 18.2 1 11/05/21 15:43 11/07/21 12:56 99-09-2 4-Nitroaniline ND ug/L 18.2 1 11/05/21 15:43 11/07/21 12:56 100-01-6 Nitrobenzene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 98-95-3 2-Nitrophenol ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 88-75-5 4-Nitrophenol ND ug/L 45.5 1 11/05/21 15:43 11/07/21 12:56 100-02-7 N-Nitrosodimethylamine ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 621-64-7 N-Nitrosodiphenylamine ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 108-60-1 Pentachlorophenol ND ug/L 18.2 1 11/05/21 15:43 11/07/21 12:56 87-86-5 Phenanthrene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 85-01-8 Phenol ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 108-95-2 Pyrene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 129-00-0 1,2,4-Trichlorobenzene ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 120-82-1 2,4,5-Trichlorophenol ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 95-95-4 2,4,6-Trichlorophenol ND ug/L 9.1 1 11/05/21 15:43 11/07/21 12:56 88-06-2 Surrogates Nitrobenzene-d5 (S) 67 % 10-144 1 11/05/21 15:43 11/07/21 12:56 4165-60-0 2-Fluorobiphenyl (S) 37 % 10-130 1 11/05/21 15:43 11/07/21 12:56 321-60-8 Terphenyl-d14 (S) 117 % 34-163 1 11/05/21 15:43 11/07/21 12:56 1718-51-0 Phenol-d6 (S) 34 % 10-130 1 11/05/21 15:43 11/07/21 12:56 13127-88-3 2-Fluorophenol (S) 18 % 10-130 1 11/05/21 15:43 11/07/21 12:56 367-12-4 2,4,6-Tribromophenol (S) 17 % 10-144 1 11/05/21 15:43 11/07/21 12:56 118-79-6 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 1 11/08/21 18:14 67-64-1 Benzene ND ug/L 1.0 1 11/08/21 18:14 71-43-2 Bromobenzene ND ug/L 1.0 1 11/08/21 18:14 108-86-1 Bromochloromethane ND ug/L 1.0 1 11/08/21 18:14 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/08/21 18:14 75-27-4 Bromoform ND ug/L 1.0 1 11/08/21 18:14 75-25-2 Bromomethane ND ug/L 2.0 1 11/08/21 18:14 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/08/21 18:14 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 11/08/21 18:14 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/08/21 18:14 108-90-7 Chloroethane ND ug/L 1.0 1 11/08/21 18:14 75-00-3 Chloroform ND ug/L 1.0 1 11/08/21 18:14 67-66-3 Chloromethane ND ug/L 1.0 1 11/08/21 18:14 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 11/08/21 18:14 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 11/08/21 18:14 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/08/21 18:14 96-12-8 REPORT OF LABORATORY ANALYSIS IH v2 This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V09 Lab ID: 92569918004 Collected: 11/02/21 11:30 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Dibromochloromethane ND ug/L 1.0 1 11/08/21 18:14 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/08/21 18:14 106-93-4 Dibromomethane ND ug/L 1.0 1 11/08/21 18:14 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/08/21 18:14 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 11/08/21 18:14 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/08/21 18:14 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 11/08/21 18:14 75-71-8 v2 1,1-Dichloroethane ND ug/L 1.0 1 11/08/21 18:14 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/08/21 18:14 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/08/21 18:14 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 11/08/21 18:14 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/08/21 18:14 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/08/21 18:14 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 11/08/21 18:14 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 11/08/21 18:14 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 11/08/21 18:14 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/08/21 18:14 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/08/21 18:14 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 11/08/21 18:14 108-20-3 Ethylbenzene ND ug/L 1.0 1 11/08/21 18:14 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 11/08/21 18:14 87-68-3 2-Hexanone ND ug/L 5.0 1 11/08/21 18:14 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 11/08/21 18:14 99-87-6 Methylene Chloride ND ug/L 5.0 1 11/08/21 18:14 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/08/21 18:14 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 11/08/21 18:14 1634-04-4 Naphthalene ND ug/L 1.0 1 11/08/21 18:14 91-20-3 Styrene ND ug/L 1.0 1 11/08/21 18:14 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/08/21 18:14 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/08/21 18:14 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/08/21 18:14 127-18-4 Toluene ND ug/L 1.0 1 11/08/21 18:14 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 11/08/21 18:14 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 11/08/21 18:14 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 11/08/21 18:14 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/08/21 18:14 79-00-5 Trichloroethene ND ug/L 1.0 1 11/08/21 18:14 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 11/08/21 18:14 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 11/08/21 18:14 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/08/21 18:14 108-05-4 Vinyl chloride ND ug/L 1.0 1 11/08/21 18:14 75-01-4 Xylene (Total) ND ug/L 1.0 1 11/08/21 18:14 1330-20-7 m&p-Xylene ND ug/L 2.0 1 11/08/21 18:14 179601-23-1 o-Xylene ND ug/L 1.0 1 11/08/21 18:14 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 11/08/21 18:14 460-00-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V09 Parameters Lab ID: 92569918004 Collected: 11/02/21 11:30 Results Units PQL DF Received: 11/03/21 11:22 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Surrogates 1,2-Dichloroethane-d4 (S) 109 % 70-130 1 11/08/21 18:14 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 11/08/21 18:14 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 11/04/21 18:03 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 11/04/21 18:03 17060-07-0 Toluene-d8 (S) 98 % 66-133 1 11/04/21 18:03 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 745 mg/L 5.0 1 11/08/21 20:48 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 780 mg/L 50.0 1 11/04/21 11:00 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 2.5 mg/L 1.0 1 11/05/2101:18 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 48.4 mg/L 2.0 2 11/10/2121:49 16887-00-6 531013 TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon 4.6 mg/L 1.0 1 11/16/21 07:21 7440-44-0 Date: 11/19/2021 04:40 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 23 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V10 Lab ID: 92569918005 Collected: 11/02/21 09:55 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by Pace 1 11/18/21 14:34 Collected By J.Zambani 1 11/18/21 14:34 ni Collected Date 11/2121 1 11/18/21 14:34 Collected Time 09:55 1 11/18/21 14:34 pH 5.4 Std. Units 1 11/18/21 14:34 Temperature 13.9 deg C 1 11/18/21 14:34 Static Water Level 27.84 feet 1 11/18/21 14:34 Specific Conductance 33.3 umhos/cm 1 11/18/21 14:34 Oxygen, Dissolved 2.5 mg/L 1 11/18/21 14:34 7782-44-7 Total Well Depth 32.40 feet 1 11/18/21 14:34 REDOX 43.1 mV 1 11/18/21 14:34 Turbidity 6.0 NTU 1 11/18/21 14:34 Odor None 1 11/18/21 14:34 Appearance Clear 1 11/18/21 14:34 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 1 11/04/2116:09 11/05/2119:55 7440-36-0 Arsenic ND ug/L 10.0 1 11/04/2116:09 11/05/2119:55 7440-38-2 Barium 5.7 ug/L 5.0 1 11/04/2116:09 11/05/2119:55 7440-39-3 Cadmium ND ug/L 1.0 1 11/04/2116:09 11/05/2119:55 7440-43-9 Calcium 2220 ug/L 100 1 11/04/2116:09 11/05/2119:55 7440-70-2 Chromium ND ug/L 5.0 1 11/04/2116:09 11/05/2119:55 7440-47-3 Cobalt ND ug/L 5.0 1 11/04/2116:09 11/05/2119:55 7440-48-4 Copper ND ug/L 5.0 1 11/04/2116:09 11/05/2119:55 7440-50-8 Lead ND ug/L 5.0 1 11/04/2116:09 11/05/2119:55 7439-92-1 Magnesium 826 ug/L 100 1 11/04/2116:09 11/05/2119:55 7439-95-4 Nickel ND ug/L 5.0 1 11/04/2116:09 11/05/2119:55 7440-02-0 Potassium ND ug/L 5000 1 11/04/2116:09 11/05/2119:55 7440-09-7 Selenium ND ug/L 10.0 1 11/04/2116:09 11/05/2119:55 7782-49-2 Silver ND ug/L 5.0 1 11/04/2116:09 11/05/2119:55 7440-22-4 Sodium 2280J ug/L 5000 1 11/04/2116:09 11/05/2119:55 7440-23-5 Thallium ND ug/L 10.0 1 11/04/2116:09 11/05/2119:55 7440-28-0 Vanadium ND ug/L 5.0 1 11/04/2116:09 11/05/2119:55 7440-62-2 Zinc ND ug/L 10.0 1 11/04/2116:09 11/05/2119:55 7440-66-6 1631E Mercury,Low Level Analytical Method: EPA 1631 E Preparation Method: EPA 1631 E Pace Analytical Services -Asheville Mercury 2.83 ng/L 0.50 1 11/17/2115:35 11/18/2114:37 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Acenaphthene ND ug/L 10.0 1 11/04/2106:16 11/04/2123:43 83-32-9 Acenaphthylene ND ug/L 10.0 1 11/04/2106:16 11/04/2123:43 208-96-8 Aniline ND ug/L 10.0 1 11/04/2106:16 11/04/2123:43 62-53-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V10 Lab ID: 92569918005 Collected: 11/02/21 09:55 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Anthracene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 120-12-7 Benzo(a)anthracene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 56-55-3 Benzo(a)pyrene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 50-32-8 Benzo(b)fluoranthene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 205-99-2 Benzo(g,h,i)perylene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 191-24-2 Benzo(k)fluoranthene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 207-08-9 Benzoic Acid ND ug/L 50.0 1 11/04/21 06:16 11/04/21 23:43 65-85-0 Benzyl alcohol ND ug/L 20.0 1 11/04/21 06:16 11/04/21 23:43 100-51-6 4-Bromophenylphenyl ether ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 101-55-3 Butylbenzylphthalate ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 85-68-7 4-Chloro-3-methyl phenol ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 59-50-7 4-Chloroaniline ND ug/L 20.0 1 11/04/21 06:16 11/04/21 23:43 106-47-8 bis(2-Chloroethoxy)methane ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 111-91-1 bis(2-Chloroethyl) ether ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 111-44-4 2-Chloronaphthalene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 91-58-7 2-Chlorophenol ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 95-57-8 4-Chlorophenylphenyl ether ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 7005-72-3 Chrysene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 53-70-3 Dibenzofuran ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 132-64-9 1,2-Dichlorobenzene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 95-50-1 1,3-Dichlorobenzene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 541-73-1 1,4-Dichlorobenzene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 106-46-7 3,3'-Dichlorobenzidine ND ug/L 20.0 1 11/04/21 06:16 11/04/21 23:43 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 120-83-2 Diethylphthalate ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 84-66-2 2,4-Dimethylphenol ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 105-67-9 Dimethylphthalate ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 131-11-3 Di-n-butylphthalate ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 20.0 1 11/04/21 06:16 11/04/21 23:43 534-52-1 2,4-Dinitrophenol ND ug/L 50.0 1 11/04/21 06:16 11/04/21 23:43 51-28-5 v1 2,4-Dinitrotoluene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 121-14-2 v1 2,6-Dinitrotoluene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 606-20-2 Di-n-octylphthalate ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 1 11/04/21 06:16 11/04/21 23:43 117-81-7 Fluoranthene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 206-44-0 Fluorene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 86-73-7 Hexachloro-1,3-butadiene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 87-68-3 Hexachlorobenzene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 77-47-4 Hexachloroethane ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 193-39-5 Isophorone ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 78-59-1 1-Methylnaphthalene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 90-12-0 2-Methylnaphthalene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 91-57-6 2-Methylphenol(o-Cresol) ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 95-48-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V10 Lab ID: 92569918005 Collected: 11/02/21 09:55 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 3&4-Methyl phenol (m&p Cresol) ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 15831-10-4 Naphthalene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 91-20-3 2-Nitroaniline ND ug/L 20.0 1 11/04/21 06:16 11/04/21 23:43 88-74-4 3-Nitroaniline ND ug/L 20.0 1 11/04/21 06:16 11/04/21 23:43 99-09-2 4-Nitroaniline ND ug/L 20.0 1 11/04/21 06:16 11/04/21 23:43 100-01-6 Nitrobenzene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 98-95-3 2-Nitrophenol ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 88-75-5 4-Nitrophenol ND ug/L 50.0 1 11/04/21 06:16 11/04/21 23:43 100-02-7 N-Nitrosodimethylamine ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 621-64-7 N-Nitrosodiphenylamine ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 108-60-1 Pentachlorophenol ND ug/L 20.0 1 11/04/21 06:16 11/04/21 23:43 87-86-5 Phenanthrene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 85-01-8 Phenol ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 108-95-2 Pyrene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 129-00-0 1,2,4-Trichlorobenzene ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 120-82-1 2,4,5-Trichlorophenol ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 95-95-4 2,4,6-Trichlorophenol ND ug/L 10.0 1 11/04/21 06:16 11/04/21 23:43 88-06-2 Surrogates Nitrobenzene-d5 (S) 73 % 10-144 1 11/04/21 06:16 11/04/21 23:43 4165-60-0 2-Fluorobiphenyl (S) 72 % 10-130 1 11/04/21 06:16 11/04/21 23:43 321-60-8 Terphenyl-d14 (S) 89 % 34-163 1 11/04/21 06:16 11/04/21 23:43 1718-51-0 Phenol-d6 (S) 38 % 10-130 1 11/04/21 06:16 11/04/21 23:43 13127-88-3 2-Fluorophenol (S) 49 % 10-130 1 11/04/21 06:16 11/04/21 23:43 367-12-4 2,4,6-Tribromophenol (S) 75 % 10-144 1 11/04/21 06:16 11/04/21 23:43 118-79-6 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 1 11/08/21 18:31 67-64-1 Benzene ND ug/L 1.0 1 11/08/21 18:31 71-43-2 Bromobenzene ND ug/L 1.0 1 11/08/21 18:31 108-86-1 Bromochloromethane ND ug/L 1.0 1 11/08/21 18:31 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/08/21 18:31 75-27-4 Bromoform ND ug/L 1.0 1 11/08/21 18:31 75-25-2 Bromomethane ND ug/L 2.0 1 11/08/21 18:31 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/08/21 18:31 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 11/08/21 18:31 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/08/21 18:31 108-90-7 Chloroethane ND ug/L 1.0 1 11/08/21 18:31 75-00-3 Chloroform ND ug/L 1.0 1 11/08/21 18:31 67-66-3 Chloromethane ND ug/L 1.0 1 11/08/21 18:31 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 11/08/21 18:31 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 11/08/21 18:31 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/08/21 18:31 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/08/21 18:31 124-48-1 REPORT OF LABORATORY ANALYSIS IH v2 This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V10 Lab ID: 92569918005 Collected: 11/02/21 09:55 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/08/21 18:31 106-93-4 Dibromomethane ND ug/L 1.0 1 11/08/21 18:31 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/08/21 18:31 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 11/08/21 18:31 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/08/21 18:31 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 11/08/21 18:31 75-71-8 v2 1,1-Dichloroethane ND ug/L 1.0 1 11/08/21 18:31 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/08/21 18:31 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/08/21 18:31 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 11/08/21 18:31 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/08/21 18:31 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/08/21 18:31 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 11/08/21 18:31 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 11/08/21 18:31 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 11/08/21 18:31 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/08/21 18:31 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/08/21 18:31 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 11/08/21 18:31 108-20-3 Ethylbenzene ND ug/L 1.0 1 11/08/21 18:31 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 11/08/21 18:31 87-68-3 2-Hexanone ND ug/L 5.0 1 11/08/21 18:31 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 11/08/21 18:31 99-87-6 Methylene Chloride ND ug/L 5.0 1 11/08/21 18:31 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/08/21 18:31 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 11/08/21 18:31 1634-04-4 Naphthalene ND ug/L 1.0 1 11/08/21 18:31 91-20-3 Styrene ND ug/L 1.0 1 11/08/21 18:31 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/08/21 18:31 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/08/21 18:31 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/08/21 18:31 127-18-4 Toluene ND ug/L 1.0 1 11/08/21 18:31 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 11/08/21 18:31 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 11/08/21 18:31 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 11/08/21 18:31 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/08/21 18:31 79-00-5 Trichloroethene ND ug/L 1.0 1 11/08/21 18:31 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 11/08/21 18:31 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 11/08/21 18:31 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/08/21 18:31 108-05-4 Vinyl chloride ND ug/L 1.0 1 11/08/21 18:31 75-01-4 Xylene (Total) ND ug/L 1.0 1 11/08/21 18:31 1330-20-7 m&p-Xylene ND ug/L 2.0 1 11/08/21 18:31 179601-23-1 o-Xylene ND ug/L 1.0 1 11/08/21 18:31 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 11/08/21 18:31 460-00-4 1,2-Dichloroethane-d4 (S) 108 % 70-130 1 11/08/21 18:31 17060-07-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V10 Lab ID: 92569918005 Collected: 11/02/21 09:55 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Surrogates Toluene-d8 (S) 101 % 70-130 1 11/08/21 18:31 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 11/04/21 18:22 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 89 % 70-130 1 11/04/21 18:22 17060-07-0 Toluene-d8 (S) 95 % 66-133 1 11/04/21 18:22 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 12.1 mg/L 5.0 1 11/08/21 20:15 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids ND mg/L 25.0 1 11/04/21 11:00 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 0.85J mg/L 1.0 1 11/05/2102:03 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 2.5 mg/L 1.0 1 11/10/2121:50 16887-00-6 531013 TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 11/16/21 07:40 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V11 Lab ID: 92569918006 Collected: 11/02/21 10:30 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by Pace 1 11/18/21 14:36 Collected By J.Zambani 1 11/18/21 14:36 ni Collected Date 11/2/21 1 11/18/21 14:36 Collected Time 10:30 1 11/18/21 14:36 pH 5.5 Std. Units 1 11/18/21 14:36 Temperature 12.9 deg C 1 11/18/21 14:36 Static Water Level 40.01 feet 1 11/18/21 14:36 Specific Conductance 62.5 umhos/cm 1 11/18/21 14:36 Oxygen, Dissolved 3.2 mg/L 1 11/18/21 14:36 7782-44-7 Total Well Depth 57.82 feet 1 11/18/21 14:36 REDOX 49.1 mV 1 11/18/21 14:36 Turbidity 7.0 NTU 1 11/18/21 14:36 Odor None 1 11/18/21 14:36 Appearance Clear 1 11/18/21 14:36 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 1 11/11/2110:54 11/12/2103:29 7440-36-0 Arsenic ND ug/L 10.0 1 11/11/2110:54 11/12/2103:29 7440-38-2 BC Barium 6.9 ug/L 5.0 1 11/11/2110:54 11/12/2103:29 7440-39-3 Cadmium ND ug/L 1.0 1 11/11/2110:54 11/12/2103:29 7440-43-9 Calcium 4460 ug/L 100 1 11/11/2110:54 11/12/2103:29 7440-70-2 Chromium ND ug/L 5.0 1 11/11/2110:54 11/12/2103:29 7440-47-3 Cobalt ND ug/L 5.0 1 11/11/2110:54 11/12/2103:29 7440-48-4 Copper ND ug/L 5.0 1 11/11/2110:54 11/12/2103:29 7440-50-8 Lead ND ug/L 5.0 1 11/11/2110:54 11/12/2103:29 7439-92-1 Magnesium 2150 ug/L 100 1 11/11/2110:54 11/12/2103:29 7439-95-4 Nickel ND ug/L 5.0 1 11/11/2110:54 11/12/2103:29 7440-02-0 Potassium ND ug/L 5000 1 11/11/2110:54 11/12/2103:29 7440-09-7 Selenium ND ug/L 10.0 1 1111112110:54 11/12/2103:29 7782-49-2 Silver ND ug/L 5.0 1 1111112110:54 11/12/2103:29 7440-22-4 Sodium 5110 ug/L 5000 1 1111112110:54 11/12/2103:29 7440-23-5 Thallium ND ug/L 10.0 1 11/11/2110:54 11/12/2103:29 7440-28-0 Vanadium ND ug/L 5.0 1 11/11/2110:54 11/12/2103:29 7440-62-2 Zinc 12.7 ug/L 10.0 1 11/11/2110:54 11/12/2103:29 7440-66-6 BC 1631E Mercury,Low Level Analytical Method: EPA 1631 E Preparation Method: EPA 1631 E Pace Analytical Services -Asheville Mercury 1.16 ng/L 0.50 1 11/17/2115:35 11/18/2114:45 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Acenaphthene ND ug/L 8.3 1 11/05/2115:43 11/07/2113:21 83-32-9 Acenaphthylene ND ug/L 8.3 1 11/05/2115:43 11/07/2113:21 208-96-8 Aniline ND ug/L 8.3 1 11/05/2115:43 11/07/2113:21 62-53-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V11 Lab ID: 92569918006 Collected: 11/02/21 10:30 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Anthracene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 120-12-7 Benzo(a)anthracene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 56-55-3 Benzo(a)pyrene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 50-32-8 Benzo(b)fluoranthene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 205-99-2 Benzo(g,h,i)perylene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 191-24-2 Benzo(k)fluoranthene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 207-08-9 Benzoic Acid ND ug/L 41.7 1 11/05/21 15:43 11/07/21 13:21 65-85-0 Benzyl alcohol ND ug/L 16.7 1 11/05/21 15:43 11/07/21 13:21 100-51-6 4-Bromophenylphenyl ether ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 101-55-3 Butylbenzylphthalate ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 59-50-7 4-Chloroaniline ND ug/L 16.7 1 11/05/21 15:43 11/07/21 13:21 106-47-8 bis(2-Chloroethoxy)methane ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 111-91-1 bis(2-Chloroethyl) ether ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 111-44-4 2-Chloronaphthalene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 91-58-7 2-Chlorophenol ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 95-57-8 4-Chlorophenylphenyl ether ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 7005-72-3 Chrysene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 218-01-9 Dibenz(a,h)anthracene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 53-70-3 Dibenzofuran ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 132-64-9 1,2-Dichlorobenzene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 95-50-1 1,3-Dichlorobenzene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 541-73-1 1,4-Dichlorobenzene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 106-46-7 3,3'-Dichlorobenzidine ND ug/L 16.7 1 11/05/21 15:43 11/07/21 13:21 91-94-1 2,4-Dichlorophenol ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 120-83-2 Diethylphthalate ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 84-66-2 2,4-Dimethylphenol ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 105-67-9 Dimethylphthalate ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 131-11-3 Di-n-butylphthalate ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 16.7 1 11/05/21 15:43 11/07/21 13:21 534-52-1 2,4-Dinitrophenol ND ug/L 41.7 1 11/05/21 15:43 11/07/21 13:21 51-28-5 2,4-Dinitrotoluene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 121-14-2 2,6-Dinitrotoluene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 606-20-2 Di-n-octylphthalate ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/L 5.0 1 11/05/21 15:43 11/07/21 13:21 117-81-7 Fluoranthene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 206-44-0 Fluorene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 86-73-7 Hexachloro-1,3-butadiene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 87-68-3 Hexachlorobenzene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 118-74-1 Hexachlorocyclopentadiene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 77-47-4 Hexachloroethane ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 193-39-5 Isophorone ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 78-59-1 1-Methylnaphthalene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 90-12-0 2-Methylnaphthalene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 91-57-6 2-Methylphenol(o-Cresol) ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 95-48-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V11 Lab ID: 92569918006 Collected: 11/02/21 10:30 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 3&4-Methyl phenol (m&p Cresol) ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 15831-10-4 Naphthalene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 91-20-3 2-Nitroaniline ND ug/L 16.7 1 11/05/21 15:43 11/07/21 13:21 88-74-4 3-Nitroaniline ND ug/L 16.7 1 11/05/21 15:43 11/07/21 13:21 99-09-2 4-Nitroaniline ND ug/L 16.7 1 11/05/21 15:43 11/07/21 13:21 100-01-6 Nitrobenzene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 98-95-3 2-Nitrophenol ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 88-75-5 4-Nitrophenol ND ug/L 41.7 1 11/05/21 15:43 11/07/21 13:21 100-02-7 N-Nitrosodimethylamine ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 621-64-7 N-Nitrosodiphenylamine ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 108-60-1 Pentachlorophenol ND ug/L 16.7 1 11/05/21 15:43 11/07/21 13:21 87-86-5 Phenanthrene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 85-01-8 Phenol ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 108-95-2 Pyrene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 129-00-0 1,2,4-Trichlorobenzene ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 120-82-1 2,4,5-Trichlorophenol ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 95-95-4 2,4,6-Trichlorophenol ND ug/L 8.3 1 11/05/21 15:43 11/07/21 13:21 88-06-2 Surrogates Nitrobenzene-d5 (S) 51 % 10-144 1 11/05/21 15:43 11/07/21 13:21 4165-60-0 2-Fluorobiphenyl (S) 32 % 10-130 1 11/05/21 15:43 11/07/21 13:21 321-60-8 Terphenyl-d14 (S) 101 % 34-163 1 11/05/21 15:43 11/07/21 13:21 1718-51-0 Phenol-d6 (S) 32 % 10-130 1 11/05/21 15:43 11/07/21 13:21 13127-88-3 2-Fluorophenol (S) 39 % 10-130 1 11/05/21 15:43 11/07/21 13:21 367-12-4 2,4,6-Tribromophenol (S) 76 % 10-144 1 11/05/21 15:43 11/07/21 13:21 118-79-6 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 1 11/08/21 18:49 67-64-1 Benzene ND ug/L 1.0 1 11/08/21 18:49 71-43-2 Bromobenzene ND ug/L 1.0 1 11/08/21 18:49 108-86-1 Bromochloromethane ND ug/L 1.0 1 11/08/21 18:49 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/08/21 18:49 75-27-4 Bromoform ND ug/L 1.0 1 11/08/21 18:49 75-25-2 Bromomethane ND ug/L 2.0 1 11/08/21 18:49 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/08/21 18:49 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 11/08/21 18:49 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/08/21 18:49 108-90-7 Chloroethane ND ug/L 1.0 1 11/08/21 18:49 75-00-3 Chloroform ND ug/L 1.0 1 11/08/21 18:49 67-66-3 Chloromethane ND ug/L 1.0 1 11/08/21 18:49 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 11/08/21 18:49 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 11/08/21 18:49 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/08/21 18:49 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/08/21 18:49 124-48-1 REPORT OF LABORATORY ANALYSIS IH v2 This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V11 Lab ID: 92569918006 Collected: 11/02/21 10:30 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/08/21 18:49 106-93-4 Dibromomethane ND ug/L 1.0 1 11/08/21 18:49 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/08/21 18:49 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 11/08/21 18:49 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/08/21 18:49 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 11/08/21 18:49 75-71-8 v2 1,1-Dichloroethane ND ug/L 1.0 1 11/08/21 18:49 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/08/21 18:49 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/08/21 18:49 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 11/08/21 18:49 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/08/21 18:49 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/08/21 18:49 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 11/08/21 18:49 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 11/08/21 18:49 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 11/08/21 18:49 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/08/21 18:49 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/08/21 18:49 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 11/08/21 18:49 108-20-3 Ethylbenzene ND ug/L 1.0 1 11/08/21 18:49 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 11/08/21 18:49 87-68-3 2-Hexanone ND ug/L 5.0 1 11/08/21 18:49 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 11/08/21 18:49 99-87-6 Methylene Chloride ND ug/L 5.0 1 11/08/21 18:49 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/08/21 18:49 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 11/08/21 18:49 1634-04-4 Naphthalene ND ug/L 1.0 1 11/08/21 18:49 91-20-3 Styrene ND ug/L 1.0 1 11/08/21 18:49 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/08/21 18:49 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/08/21 18:49 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/08/21 18:49 127-18-4 Toluene ND ug/L 1.0 1 11/08/21 18:49 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 11/08/21 18:49 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 11/08/21 18:49 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 11/08/21 18:49 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/08/21 18:49 79-00-5 Trichloroethene ND ug/L 1.0 1 11/08/21 18:49 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 11/08/21 18:49 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 11/08/21 18:49 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/08/21 18:49 108-05-4 Vinyl chloride ND ug/L 1.0 1 11/08/21 18:49 75-01-4 Xylene (Total) ND ug/L 1.0 1 11/08/21 18:49 1330-20-7 m&p-Xylene ND ug/L 2.0 1 11/08/21 18:49 179601-23-1 o-Xylene ND ug/L 1.0 1 11/08/21 18:49 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 11/08/21 18:49 460-00-4 1,2-Dichloroethane-d4 (S) 107 % 70-130 1 11/08/21 18:49 17060-07-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: WQ0013419-Q06V11 Lab ID: 92569918006 Collected: 11/02/21 10:30 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Surrogates Toluene-d8 (S) 101 % 70-130 1 11/08/21 18:49 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 11/04/21 18:41 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 96 % 70-130 1 11/04/21 18:41 17060-07-0 Toluene-d8 (S) 101 % 66-133 1 11/04/21 18:41 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 22.4 mg/L 5.0 1 11/08/21 20:21 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 43.0 mg/L 25.0 1 11/04/21 11:00 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 3.0 mg/L 1.0 1 11/05/2102:18 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 1.9 mg/L 1.0 1 11/10/2121:50 16887-00-6 531013 TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 11/16/21 07:58 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: TRIP BLANK Parameters 8260D MSV Low Level Landfill Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane ANALYTICAL RESULTS Lab ID: 92569918007 Collected: 11/02/21 00:00 Received: 11/03/21 11:22 Matrix: Water Results Units Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L PQL DF Prepared Analyzed CAS No. Qual 25.0 1 11/09/2118:57 67-64-1 1.0 1 11 /09/21 18:57 71-43-2 1.0 1 11 /09/21 18:57 108-86-1 1.0 1 11 /09/21 18:57 74-97-5 1.0 1 11 /09/21 18:57 75-27-4 1.0 1 11 /09/21 18:57 75-25-2 2.0 1 11 /09/21 18:57 74-83-9 5.0 1 11 /09/21 18:57 78-93-3 1.0 1 11 /09/21 18:57 56-23-5 1.0 1 11 /09/21 18:57 108-90-7 1.0 1 11 /09/21 18:57 75-00-3 1.0 1 11 /09/21 18:57 67-66-3 1.0 1 11 /09/21 18:57 74-87-3 1.0 1 11 /09/21 18:57 95-49-8 1.0 1 11 /09/21 18:57 106-43-4 2.0 1 11/09/2118:57 96-12-8 1.0 1 11 /09/21 18:57 124-48-1 1.0 1 11 /09/21 18:57 106-93-4 1.0 1 11 /09/21 18:57 74-95-3 1.0 1 11/09/2118:57 95-50-1 1.0 1 11 /09/21 18:57 541-73-1 1.0 1 11 /09/21 18:57 106-46-7 1.0 1 11 /09/21 18:57 75-71-8 1.0 1 11 /09/21 18:57 75-34-3 1.0 1 11 /09/21 18:57 107-06-2 1.0 1 11 /09/21 18:57 75-35-4 1.0 1 11 /09/21 18:57 156-59-2 1.0 1 11 /09/21 18:57 156-60-5 1.0 1 11 /09/21 18:57 78-87-5 1.0 1 11 /09/21 18:57 142-28-9 1.0 1 11 /09/21 18:57 594-20-7 1.0 1 11 /09/21 18:57 563-58-6 1.0 1 11 /09/21 18:57 10061-01-5 1.0 1 11 /09/21 18:57 10061-02-6 1.0 1 11 /09/21 18:57 108-20-3 1.0 1 11 /09/21 18:57 100-41-4 2.0 1 11 /09/21 18:57 87-68-3 5.0 1 11 /09/21 18:57 591-78-6 1.0 1 11 /09/21 18:57 99-87-6 5.0 1 11 /09/21 18:57 75-09-2 5.0 1 11 /09/21 18:57 108-10-1 1.0 1 11 /09/21 18:57 1634-04-4 1.0 1 11 /09/21 18:57 91-20-3 1.0 1 11 /09/21 18:57 100-42-5 1.0 1 11 /09/21 18:57 630-20-6 1.0 1 11 /09/21 18:57 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Sample: TRIP BLANK Lab ID: 92569918007 Collected: 11/02/21 00:00 Received: 11/03/21 11:22 Matrix: Water Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 11/19/2021 04:40 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 95 % 92 % 101 % Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 97 % 97 % 1.0 1 11 /09/21 18:57 127-18-4 1.0 1 11 /09/21 18:57 108-88-3 1.0 1 11 /09/21 18:57 87-61-6 1.0 1 11 /09/21 18:57 120-82-1 1.0 1 11 /09/21 18:57 71-55-6 1.0 1 11 /09/21 18:57 79-00-5 1.0 1 11 /09/21 18:57 79-01-6 1.0 1 11 /09/21 18:57 75-69-4 1.0 1 11/09/2118:57 96-18-4 2.0 1 11 /09/21 18:57 108-05-4 1.0 1 11 /09/21 18:57 75-01-4 1.0 1 11 /09/21 18:57 1330-20-7 2.0 1 11 /09/21 18:57 179601-23-1 1.0 1 11 /09/21 18:57 95-47-6 70-130 1 70-130 1 70-130 1 70-130 1 66-133 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11 /09/21 18:57 460-00-4 11 /09/21 18:57 17060-07-0 11 /09/21 18:57 2037-26-5 11 /05/21 15:07 17060-07-0 11 /05/21 15:07 2037-26-5 Page 35 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 660581 Analysis Method: EPA 1631 E QC Batch Method: EPA 1631E Analysis Description: 1631E Mercury,Low Level Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92569918001, 92569918002, 92569918003, 92569918004, 92569918005, 92569918006 METHOD BLANK: 3461309 Matrix: Water Associated Lab Samples: 92569918001, 92569918002, 92569918003, 92569918004, 92569918005, 92569918006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ng/L ND 0.50 11/18/2113:04 METHOD BLANK: 3461310 Matrix: Water Associated Lab Samples: 92569918001, 92569918002, 92569918003, 92569918004, 92569918005, 92569918006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ng/L ND 0.50 11/18/2113:43 METHOD BLANK: 3461311 Matrix: Water Associated Lab Samples: 92569918001, 92569918002, 92569918003, 92569918004, 92569918005, 92569918006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ng/L ND 0.50 11/18/2115:01 LABORATORY CONTROL SAMPLE: 3461312 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ng/L 5 4.94 99 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3461313 3461314 MS MSD 92569918001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury ng/L ND 25 25 21.1 21.1 83 83 71-125 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657606 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92569918005 METHOD BLANK: 3447194 Associated Lab Samples: 92569918005 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Qualifiers Antimony ug/L ND 5.0 11/05/2119:02 Arsenic ug/L ND 10.0 11/05/2119:02 Barium ug/L ND 5.0 11/05/2119:02 Cadmium ug/L ND 1.0 11/05/2119:02 Calcium ug/L ND 100 11/05/2119:02 Chromium ug/L ND 5.0 11/05/2119:02 Cobalt ug/L ND 5.0 11/05/2119:02 Copper ug/L ND 5.0 11/05/2119:02 Lead ug/L ND 5.0 11/05/2119:02 Magnesium ug/L ND 100 11/05/2119:02 Nickel ug/L ND 5.0 11/05/2119:02 Potassium ug/L ND 5000 11/05/2119:02 Selenium ug/L ND 10.0 11/05/2119:02 Silver ug/L ND 5.0 11/05/2119:02 Sodium ug/L ND 5000 11/05/2119:02 Thallium ug/L ND 10.0 11/05/2119:02 Vanadium ug/L ND 5.0 11/05/2119:02 Zinc ug/L ND 10.0 11/05/2119:02 LABORATORY CONTROL SAMPLE: 3447195 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 500 480 96 80-120 Arsenic ug/L 500 472 94 80-120 Barium ug/L 500 474 95 80-120 Cadmium ug/L 500 492 98 80-120 Calcium ug/L 5000 4750 95 80-120 Chromium ug/L 500 483 97 80-120 Cobalt ug/L 500 471 94 80-120 Copper ug/L 500 488 98 80-120 Lead ug/L 500 486 97 80-120 Magnesium ug/L 5000 4820 96 80-120 Nickel ug/L 500 494 99 80-120 Potassium ug/L 5000 4780J 96 80-120 Selenium ug/L 500 462 92 80-120 Silver ug/L 250 237 95 80-120 Sodium ug/L 5000 4720J 94 80-120 Thallium ug/L 500 465 93 80-120 Vanadium ug/L 500 476 95 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 LABORATORY CONTROL SAMPLE: 3447195 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Zinc ug/L 500 484 97 80-120 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3447196 3447197 MS MSD 92570483021 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Antimony ug/L ND 500 500 519 500 104 100 75-125 4 Arsenic ug/L ND 500 500 518 498 104 100 75-125 4 Barium ug/L 99.7 500 500 610 584 102 97 75-125 4 Cadmium ug/L ND 500 500 530 510 106 102 75-125 4 Calcium ug/L 13800 5000 5000 20200 19200 129 108 75-125 5 M1 Chromium ug/L 10.9 500 500 521 501 102 98 75-125 4 Cobalt ug/L ND 500 500 501 481 100 96 75-125 4 Copper ug/L 61.7 500 500 590 567 106 101 75-125 4 Lead ug/L ND 500 500 516 497 103 99 75-125 4 Magnesium ug/L 8930 5000 5000 15000 14300 122 108 75-125 5 Nickel ug/L 5.9 500 500 528 504 104 100 75-125 5 Potassium ug/L 4070J 5000 5000 9450 9090 108 100 75-125 4 Selenium ug/L ND 500 500 544 521 109 104 75-125 4 Silver ug/L ND 250 250 257 250 103 100 75-125 3 Sodium ug/L 5840 5000 5000 11400 10800 111 100 75-125 5 Thallium ug/L ND 500 500 490 475 97 94 75-125 3 Vanadium ug/L 34.4 500 500 542 523 102 98 75-125 4 Zinc ug/L 19.5 500 500 542 520 105 100 75-125 4 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 659038 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92569918001, 92569918002, 92569918004, 92569918006 METHOD BLANK: 3454139 Matrix: Water Associated Lab Samples: 92569918001, 92569918002, 92569918004, 92569918006 Blank Reporting Parameter Units Result Limit Analyzed Antimony ug/L ND 5.0 11/12/2102:01 Arsenic ug/L 5.9J 10.0 11/12/2102:01 Barium ug/L ND 5.0 11/12/2102:01 Cadmium ug/L ND 1.0 11/12/2102:01 Calcium ug/L ND 100 11/12/2102:01 Chromium ug/L ND 5.0 11/12/2102:01 Cobalt ug/L ND 5.0 11/12/2102:01 Copper ug/L ND 5.0 11/12/2102:01 Lead ug/L ND 5.0 11/12/2102:01 Magnesium ug/L ND 100 11/12/2102:01 Nickel ug/L ND 5.0 11/12/2102:01 Potassium ug/L ND 5000 11/12/2102:01 Selenium ug/L ND 10.0 11/12/2102:01 Silver ug/L ND 5.0 11/12/2102:01 Sodium ug/L ND 5000 11/12/2102:01 Thallium ug/L ND 10.0 11/12/2102:01 Vanadium ug/L ND 5.0 11/12/2102:01 Zinc ug/L ND 10.0 11/12/2102:01 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 3454140 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 506 101 80-120 Arsenic ug/L 500 493 99 80-120 Barium ug/L 500 509 102 80-120 Cadmium ug/L 500 497 99 80-120 Calcium ug/L 5000 4820 96 80-120 Chromium ug/L 500 468 94 80-120 Cobalt ug/L 500 481 96 80-120 Copper ug/L 500 518 104 80-120 Lead ug/L 500 501 100 80-120 Magnesium ug/L 5000 4780 96 80-120 Nickel ug/L 500 498 100 80-120 Potassium ug/L 5000 4890J 98 80-120 Selenium ug/L 500 478 96 80-120 Silver ug/L 250 243 97 80-120 Sodium ug/L 5000 5160 103 80-120 Thallium ug/L 500 459 92 80-120 Vanadium ug/L 500 487 97 80-120 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 LABORATORY CONTROL SAMPLE: 3454140 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Zinc ug/L 500 466 93 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3454141 3454142 MS MSD 92569194002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Antimony ug/L 3.6J 518 524 1 Arsenic ug/L ND 515 520 1 Barium ug/L 205 704 698 1 Cadmium ug/L 0.64J 515 519 1 Calcium ug/L 61900 5000 5000 67200 66600 106 93 75-125 1 Chromium ug/L ND 473 478 1 Cobalt ug/L 51.3 535 540 1 Copper ug/L ND 529 532 1 Lead ug/L ND 507 510 1 Magnesium ug/L 17000 5000 5000 21800 22000 97 101 75-125 1 Nickel ug/L 14.5 507 511 1 Potassium ug/L 6530 5000 5000 11400 11500 98 99 75-125 0 Selenium ug/L ND 540 546 1 Silver ug/L 7.2 253 253 0 Sodium ug/L 32000 5000 5000 37300 36900 107 99 75-125 1 Thallium ug/L ND 500 500 483 489 96 98 75-125 1 Vanadium ug/L 93.2 604 603 0 Zinc ug/L 14.7 487 492 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657346 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92569918001, 92569918002 METHOD BLANK: 3446006 Associated Lab Samples: 92569918001, 92569918002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/03/21 23:36 1,1,1-Trichloroethane ug/L ND 1.0 11/03/21 23:36 1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/03/21 23:36 1,1,2-Trichloroethane ug/L ND 1.0 11/03/21 23:36 1,1-Dichloroethane ug/L ND 1.0 11/03/21 23:36 1,1-Dichloroethene ug/L ND 1.0 11/03/21 23:36 1,1-Dichloropropene ug/L ND 1.0 11/03/21 23:36 1,2,3-Trichlorobenzene ug/L ND 1.0 11/03/21 23:36 1,2,3-Trichloropropane ug/L ND 1.0 11/03/21 23:36 1,2,4-Trichlorobenzene ug/L ND 1.0 11/03/21 23:36 1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/03/21 23:36 1,2-Dibromoethane (EDB) ug/L ND 1.0 11/03/21 23:36 1,2-Dichlorobenzene ug/L ND 1.0 11/03/21 23:36 1,2-Dichloroethane ug/L ND 1.0 11/03/21 23:36 1,2-Dichloropropane ug/L ND 1.0 11/03/21 23:36 1,3-Dichlorobenzene ug/L ND 1.0 11/03/21 23:36 1,3-Dichloropropane ug/L ND 1.0 11/03/21 23:36 1,4-Dichlorobenzene ug/L ND 1.0 11/03/21 23:36 2,2-Dichloropropane ug/L ND 1.0 11/03/21 23:36 2-Butanone (MEK) ug/L ND 5.0 11/03/21 23:36 2-Chlorotoluene ug/L ND 1.0 11/03/21 23:36 2-Hexanone ug/L ND 5.0 11/03/21 23:36 4-Chlorotoluene ug/L ND 1.0 11/03/21 23:36 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 11/03/21 23:36 Acetone ug/L ND 25.0 11/03/21 23:36 Benzene ug/L ND 1.0 11/03/21 23:36 Bromobenzene ug/L ND 1.0 11/03/21 23:36 Bromochloromethane ug/L ND 1.0 11/03/21 23:36 Bromodichloromethane ug/L ND 1.0 11/03/21 23:36 Bromoform ug/L ND 1.0 11/03/21 23:36 Bromomethane ug/L ND 2.0 11/03/21 23:36 v2 Carbon tetrachloride ug/L ND 1.0 11/03/21 23:36 Chlorobenzene ug/L ND 1.0 11/03/21 23:36 Chloroethane ug/L ND 1.0 11/03/21 23:36 Chloroform ug/L ND 1.0 11/03/21 23:36 Chloromethane ug/L ND 1.0 11/03/21 23:36 cis-1,2-Dichloroethene ug/L ND 1.0 11/03/21 23:36 cis-1,3-Dichloropropene ug/L ND 1.0 11/03/21 23:36 Dibromochloromethane ug/L ND 1.0 11/03/21 23:36 Dibromomethane ug/L ND 1.0 11/03/21 23:36 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 METHOD BLANK: 3446006 Associated Lab Samples: 92569918001, 92569918002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Dichlorodifluoromethane ug/L ND 1.0 11/03/21 23:36 Diisopropyl ether ug/L ND 1.0 11/03/21 23:36 Ethylbenzene ug/L ND 1.0 11/03/21 23:36 Hexachloro-1,3-butadiene ug/L ND 2.0 11/03/21 23:36 m&p-Xylene ug/L ND 2.0 11/03/21 23:36 Methyl-tert-butyl ether ug/L ND 1.0 11/03/21 23:36 Methylene Chloride ug/L ND 5.0 11/03/21 23:36 Naphthalene ug/L ND 1.0 11/03/21 23:36 o-Xylene ug/L ND 1.0 11/03/21 23:36 p-Isopropyltoluene ug/L ND 1.0 11/03/21 23:36 Styrene ug/L ND 1.0 11/03/21 23:36 Tetrachloroethene ug/L ND 1.0 11/03/21 23:36 Toluene ug/L ND 1.0 11/03/21 23:36 trans-1,2-Dichloroethene ug/L ND 1.0 11/03/21 23:36 trans- 1,3-Dichloropropene ug/L ND 1.0 11/03/21 23:36 Trichloroethene ug/L ND 1.0 11/03/21 23:36 Trichlorofluoromethane ug/L ND 1.0 11/03/21 23:36 Vinyl acetate ug/L ND 2.0 11/03/21 23:36 Vinyl chloride ug/L ND 1.0 11/03/21 23:36 Xylene (Total) ug/L ND 1.0 11/03/21 23:36 1,2-Dichloroethane-d4 (S) % 101 70-130 11/03/21 23:36 4-Bromofluorobenzene (S) % 99 70-130 11/03/21 23:36 Toluene-d8 (S) % 105 70-130 11/03/21 23:36 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 3446007 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 51.3 103 70-130 1,1,1-Trichloroethane ug/L 50 48.1 96 70-130 1,1,2,2-Tetrachloroethane ug/L 50 51.5 103 70-130 1,1,2-Trichloroethane ug/L 50 54.4 109 70-130 1,1-Dichloroethane ug/L 50 48.8 98 70-130 1,1-Dichloroethene ug/L 50 46.2 92 70-132 1,1-Dichloropropene ug/L 50 51.4 103 70-131 1,2,3-Trichlorobenzene ug/L 50 53.9 108 70-134 1,2,3-Trichloropropane ug/L 50 49.2 98 70-130 1,2,4-Trichlorobenzene ug/L 50 53.0 106 70-130 1,2-Dibromo-3-chloropropane ug/L 50 50.3 101 70-132 1,2-Dibromoethane (EDB) ug/L 50 54.4 109 70-130 1,2-Dichlorobenzene ug/L 50 50.0 100 70-130 1,2-Dichloroethane ug/L 50 47.3 95 70-130 1,2-Dichloropropane ug/L 50 52.1 104 70-130 1,3-Dichlorobenzene ug/L 50 49.7 99 70-130 1,3-Dichloropropane ug/L 50 51.0 102 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 LABORATORY CONTROL SAMPLE: Parameter 3446007 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,4-Dichlorobenzene ug/L 50 49.4 99 70-130 2,2-Dichloropropane ug/L 50 48.9 98 70-130 2-Butanone (MEK) ug/L 100 107 107 70-133 2-Chlorotoluene ug/L 50 49.9 100 70-130 2-Hexanone ug/L 100 105 105 70-130 4-Chlorotoluene ug/L 50 49.6 99 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 103 103 70-130 Acetone ug/L 100 97.9 98 70-144 Benzene ug/L 50 49.8 100 70-130 Bromobenzene ug/L 50 49.8 100 70-130 Bromochloromethane ug/L 50 49.5 99 70-130 Bromodichloromethane ug/L 50 49.8 100 70-130 Bromoform ug/L 50 53.0 106 70-131 Bromomethane ug/L 50 43.0 86 30-177 v3 Carbon tetrachloride ug/L 50 47.4 95 70-130 Chlorobenzene ug/L 50 48.0 96 70-130 Chloroethane ug/L 50 54.2 108 46-131 Chloroform ug/L 50 49.4 99 70-130 Chloromethane ug/L 50 43.4 87 49-130 cis-1,2-Dichloroethene ug/L 50 49.8 100 70-130 cis-1,3-Dichloropropene ug/L 50 53.1 106 70-130 Dibromochloromethane ug/L 50 54.6 109 70-130 Dibromomethane ug/L 50 48.3 97 70-130 Dichlorodifluoromethane ug/L 50 43.3 87 52-134 Diisopropyl ether ug/L 50 49.9 100 70-131 Ethylbenzene ug/L 50 48.2 96 70-130 Hexachloro-1,3-butadiene ug/L 50 51.9 104 70-131 m&p-Xylene ug/L 100 95.9 96 70-130 Methyl-tert-butyl ether ug/L 50 50.5 101 70-130 Methylene Chloride ug/L 50 50.4 101 68-130 Naphthalene ug/L 50 52.1 104 70-133 o-Xylene ug/L 50 47.7 95 70-130 p-Isopropyltoluene ug/L 50 50.2 100 70-130 Styrene ug/L 50 50.1 100 70-130 Tetrachloroethene ug/L 50 49.3 99 70-130 Toluene ug/L 50 47.3 95 70-130 trans-1,2-Dichloroethene ug/L 50 47.7 95 70-130 trans- 1,3-Dichloropropene ug/L 50 52.1 104 70-130 Trichloroethene ug/L 50 51.8 104 70-130 Trichlorofluoromethane ug/L 50 45.6 91 61-130 Vinyl acetate ug/L 100 105 105 70-140 Vinyl chloride ug/L 50 46.8 94 59-142 Xylene (Total) ug/L 150 144 96 70-130 1,2-Dichloroethane-d4 (S) % 99 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 96 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3446008 3446009 MS MSD 92569678001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 22.3 20.5 112 103 70-135 8 1,1,1-Trichloroethane ug/L ND 20 20 23.8 22.7 119 114 70-148 5 1,1,2,2-Tetrachloroethane ug/L ND 20 20 20.7 19.7 104 98 70-131 5 1,1,2-Trichloroethane ug/L ND 20 20 23.9 22.7 119 113 70-136 5 1,1-Dichloroethane ug/L ND 20 20 24.3 23.4 121 117 70-147 4 1,1-Dichloroethene ug/L ND 20 20 23.2 22.5 116 112 70-158 3 1,1-Dichloropropene ug/L ND 20 20 24.7 23.5 123 118 70-149 5 1,2,3-Trichlorobenzene ug/L ND 20 20 22.8 21.9 114 110 68-140 4 1,2,3-Trichloropropane ug/L ND 20 20 19.9 19.2 100 96 67-137 4 1,2,4-Trichlorobenzene ug/L ND 20 20 22.2 22.4 111 112 70-139 1 1,2-Dibromo-3-chloropropane ug/L ND 20 20 22.1 20.0 111 100 69-136 10 1,2-Dibromoethane (EDB) ug/L ND 20 20 23.5 22.4 117 112 70-137 5 1,2-Dichlorobenzene ug/L ND 20 20 22.3 21.3 111 106 70-133 5 1,2-Dichloroethane ug/L ND 20 20 21.8 20.8 109 104 67-138 4 1,2-Dichloropropane ug/L ND 20 20 24.4 22.5 122 113 70-138 8 1,3-Dichlorobenzene ug/L ND 20 20 22.5 21.6 112 108 70-133 4 1,3-Dichloropropane ug/L ND 20 20 22.0 20.9 110 105 70-136 5 1,4-Dichlorobenzene ug/L ND 20 20 22.2 21.5 111 108 70-133 3 2,2-Dichloropropane ug/L ND 20 20 24.7 24.2 124 121 52-155 2 2-Butanone (MEK) ug/L ND 40 40 43.6 44.5 109 111 61-147 2 2-Chlorotoluene ug/L ND 20 20 23.5 22.5 117 112 70-141 4 2-Hexanone ug/L ND 40 40 41.9 39.7 105 99 67-139 6 4-Chlorotoluene ug/L ND 20 20 23.1 22.1 116 110 70-135 5 4-Methyl-2-pentanone (MIBK) ug/L ND 40 40 40.2 37.3 101 93 67-136 8 Acetone ug/L ND 40 40 39.7 38.5 99 96 55-159 3 Benzene ug/L ND 20 20 23.3 21.1 116 106 67-150 10 Bromobenzene ug/L ND 20 20 23.2 22.1 116 110 70-134 5 Bromochloromethane ug/L ND 20 20 23.1 22.7 115 113 70-146 2 Bromodichloromethane ug/L ND 20 20 22.4 21.4 112 107 70-138 5 Bromoform ug/L ND 20 20 20.5 19.4 102 97 57-138 5 Bromomethane ug/L ND 20 20 25.1 22.4 126 112 10-200 11 Carbon tetrachloride ug/L ND 20 20 23.2 21.7 116 109 70-147 7 Chlorobenzene ug/L ND 20 20 22.8 21.5 114 108 70-137 6 Chloroethane ug/L ND 20 20 27.5 27.3 138 136 51-166 1 Chloroform ug/L ND 20 20 23.0 22.7 115 113 70-144 1 Chloromethane ug/L ND 20 20 21.6 21.4 108 107 24-161 1 cis-1,2-Dichloroethene ug/L ND 20 20 23.3 21.9 117 109 67-148 6 cis-1,3-Dichloropropene ug/L ND 20 20 23.2 21.4 116 107 70-142 8 Dibromochloromethane ug/L ND 20 20 22.5 20.7 112 103 68-138 8 Dibromomethane ug/L ND 20 20 22.5 21.0 112 105 70-134 7 Dichlorodifluoromethane ug/L ND 20 20 20.2 18.4 101 92 43-155 9 Diisopropyl ether ug/L ND 20 20 20.9 20.5 105 103 65-146 2 Ethylbenzene ug/L ND 20 20 23.4 22.1 117 110 68-143 6 Hexachloro-1,3-butadiene ug/L ND 20 20 26.3 23.9 131 120 62-151 9 m&p-Xylene ug/L ND 40 40 46.4 44.3 116 111 53-157 5 Methyl-tert-butyl ether ug/L ND 20 20 22.5 20.6 112 103 59-156 9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3446008 3446009 MS MSD 92569678001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Methylene Chloride ug/L ND 20 20 23.8 22.9 119 115 64-148 4 Naphthalene ug/L ND 20 20 21.9 21.2 109 106 57-150 3 o-Xylene ug/L ND 20 20 23.0 21.9 115 109 68-143 5 p-Isopropyltoluene ug/L ND 20 20 22.9 22.2 115 111 70-141 3 Styrene ug/L ND 20 20 22.5 21.3 112 107 70-136 5 Tetrachloroethene ug/L ND 20 20 23.4 21.5 117 107 70-139 9 Toluene ug/L ND 20 20 22.5 21.2 113 106 47-157 6 trans-1,2-Dichloroethene ug/L ND 20 20 24.8 21.8 124 109 70-149 13 trans- 1,3-Dichloropropene ug/L ND 20 20 21.5 20.6 107 103 70-138 4 Trichloroethene ug/L ND 20 20 24.1 22.6 120 113 70-149 6 Trichlorofluoromethane ug/L ND 20 20 23.6 22.7 118 113 61-154 4 Vinyl acetate ug/L ND 40 40 42.4 41.7 106 104 48-156 2 Vinyl chloride ug/L ND 20 20 23.3 22.2 117 111 55-172 5 Xylene (Total) ug/L ND 60 60 69.4 66.2 116 110 66-145 5 1,2-Dichloroethane-d4 (S) % 102 105 70-130 4-Bromofluorobenzene (S) % 96 98 70-130 Toluene-d8(S) % 97 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657547 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92569918004, 92569918005, 92569918006 METHOD BLANK: 3446849 Matrix: Associated Lab Samples: 92569918004, 92569918005, 92569918006 Blank Parameter Units Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/08/21 13:00 1,1,1-Trichloroethane ug/L ND 1.0 11/08/21 13:00 1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/08/21 13:00 1,1,2-Trichloroethane ug/L ND 1.0 11/08/21 13:00 1,1-Dichloroethane ug/L ND 1.0 11/08/21 13:00 1,1-Dichloroethene ug/L ND 1.0 11/08/21 13:00 1,1-Dichloropropene ug/L ND 1.0 11/08/21 13:00 1,2,3-Trichlorobenzene ug/L ND 1.0 11/08/21 13:00 1,2,3-Trichloropropane ug/L ND 1.0 11/08/21 13:00 1,2,4-Trichlorobenzene ug/L ND 1.0 11/08/21 13:00 1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/08/21 13:00 1,2-Dibromoethane (EDB) ug/L ND 1.0 11/08/21 13:00 1,2-Dichlorobenzene ug/L ND 1.0 11/08/21 13:00 1,2-Dichloroethane ug/L ND 1.0 11/08/21 13:00 1,2-Dichloropropane ug/L ND 1.0 11/08/21 13:00 1,3-Dichlorobenzene ug/L ND 1.0 11/08/21 13:00 1,3-Dichloropropane ug/L ND 1.0 11/08/21 13:00 1,4-Dichlorobenzene ug/L ND 1.0 11/08/21 13:00 2,2-Dichloropropane ug/L ND 1.0 11/08/21 13:00 2-Butanone (MEK) ug/L ND 5.0 11/08/21 13:00 2-Chlorotoluene ug/L ND 1.0 11/08/21 13:00 2-Hexanone ug/L ND 5.0 11/08/21 13:00 4-Chlorotoluene ug/L ND 1.0 11/08/21 13:00 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 11/08/21 13:00 Acetone ug/L ND 25.0 11/08/21 13:00 Benzene ug/L ND 1.0 11/08/21 13:00 Bromobenzene ug/L ND 1.0 11/08/21 13:00 Bromochloromethane ug/L ND 1.0 11/08/21 13:00 Bromodichloromethane ug/L ND 1.0 11/08/21 13:00 Bromoform ug/L ND 1.0 11/08/21 13:00 Bromomethane ug/L ND 2.0 11/08/21 13:00 Carbon tetrachloride ug/L ND 1.0 11/08/21 13:00 Chlorobenzene ug/L ND 1.0 11/08/21 13:00 Chloroethane ug/L ND 1.0 11/08/21 13:00 Chloroform ug/L ND 1.0 11/08/21 13:00 Chloromethane ug/L ND 1.0 11/08/21 13:00 cis-1,2-Dichloroethene ug/L ND 1.0 11/08/21 13:00 cis-1,3-Dichloropropene ug/L ND 1.0 11/08/21 13:00 Dibromochloromethane ug/L ND 1.0 11/08/21 13:00 Dibromomethane ug/L ND 1.0 11/08/21 13:00 IH v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 METHOD BLANK: 3446849 Matrix: Associated Lab Samples: 92569918004, 92569918005, 92569918006 Blank Parameter Units Result Water Reporting Limit Analyzed Dichlorodifluoromethane ug/L ND 1.0 11/08/21 13:00 v2 Diisopropyl ether ug/L ND 1.0 11/08/21 13:00 Ethylbenzene ug/L ND 1.0 11/08/21 13:00 Hexachloro-1,3-butadiene ug/L ND 2.0 11/08/21 13:00 m&p-Xylene ug/L ND 2.0 11/08/21 13:00 Methyl-tert-butyl ether ug/L ND 1.0 11/08/21 13:00 Methylene Chloride ug/L ND 5.0 11/08/21 13:00 Naphthalene ug/L ND 1.0 11/08/21 13:00 o-Xylene ug/L ND 1.0 11/08/21 13:00 p-Isopropyltoluene ug/L ND 1.0 11/08/21 13:00 Styrene ug/L ND 1.0 11/08/21 13:00 Tetrachloroethene ug/L ND 1.0 11/08/21 13:00 Toluene ug/L ND 1.0 11/08/21 13:00 trans-1,2-Dichloroethene ug/L ND 1.0 11/08/21 13:00 trans- 1,3-Dichloropropene ug/L ND 1.0 11/08/21 13:00 Trichloroethene ug/L ND 1.0 11/08/21 13:00 Trichlorofluoromethane ug/L ND 1.0 11/08/21 13:00 Vinyl acetate ug/L ND 2.0 11/08/21 13:00 Vinyl chloride ug/L ND 1.0 11/08/21 13:00 Xylene (Total) ug/L ND 1.0 11/08/21 13:00 1,2-Dichloroethane-d4 (S) % 106 70-130 11/08/21 13:00 4-Bromofluorobenzene (S) % 101 70-130 11/08/21 13:00 Toluene-d8 (S) % 101 70-130 11/08/21 13:00 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 3446850 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 55.3 111 70-130 1,1,1-Trichloroethane ug/L 50 54.8 110 70-130 1,1,2,2-Tetrachloroethane ug/L 50 54.2 108 70-130 1,1,2-Trichloroethane ug/L 50 53.3 107 70-130 1,1-Dichloroethane ug/L 50 53.3 107 70-130 1,1-Dichloroethene ug/L 50 53.2 106 70-132 1,1-Dichloropropene ug/L 50 56.9 114 70-131 1,2,3-Trichlorobenzene ug/L 50 52.2 104 70-134 1,2,3-Trichloropropane ug/L 50 59.2 118 70-130 1,2,4-Trichlorobenzene ug/L 50 54.4 109 70-130 1,2-Dibromo-3-chloropropane ug/L 50 56.4 113 70-132 1,2-Dibromoethane (EDB) ug/L 50 54.3 109 70-130 1,2-Dichlorobenzene ug/L 50 52.8 106 70-130 1,2-Dichloroethane ug/L 50 51.8 104 70-130 1,2-Dichloropropane ug/L 50 54.5 109 70-130 1,3-Dichlorobenzene ug/L 50 52.9 106 70-130 1,3-Dichloropropane ug/L 50 54.0 108 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 LABORATORY CONTROL SAMPLE: Parameter 3446850 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,4-Dichlorobenzene ug/L 50 54.3 109 70-130 2,2-Dichloropropane ug/L 50 56.4 113 70-130 2-Butanone (MEK) ug/L 100 123 123 70-133 2-Chlorotoluene ug/L 50 54.9 110 70-130 2-Hexanone ug/L 100 115 115 70-130 4-Chlorotoluene ug/L 50 53.3 107 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 116 116 70-130 Acetone ug/L 100 108 108 70-144 Benzene ug/L 50 52.8 106 70-130 Bromobenzene ug/L 50 53.4 107 70-130 Bromochloromethane ug/L 50 51.8 104 70-130 Bromodichloromethane ug/L 50 54.2 108 70-130 Bromoform ug/L 50 56.1 112 70-131 Bromomethane ug/L 50 73.4 147 30-177lH Carbon tetrachloride ug/L 50 54.4 109 70-130 Chlorobenzene ug/L 50 53.8 108 70-130 Chloroethane ug/L 50 48.9 98 46-131 Chloroform ug/L 50 54.7 109 70-130 Chloromethane ug/L 50 51.2 102 49-130 v2 cis-1,2-Dichloroethene ug/L 50 52.9 106 70-130 cis-1,3-Dichloropropene ug/L 50 57.7 115 70-130 Dibromochloromethane ug/L 50 55.4 111 70-130 Dibromomethane ug/L 50 50.2 100 70-130 Dichlorodifluoromethane ug/L 50 50.0 100 52-134 v2 Diisopropyl ether ug/L 50 55.7 111 70-131 Ethylbenzene ug/L 50 55.1 110 70-130 Hexachloro-1,3-butadiene ug/L 50 55.2 110 70-131 m&p-Xylene ug/L 100 112 112 70-130 Methyl-tert-butyl ether ug/L 50 56.2 112 70-130 Methylene Chloride ug/L 50 50.8 102 68-130 Naphthalene ug/L 50 53.4 107 70-133 o-Xylene ug/L 50 54.9 110 70-130 p-Isopropyltoluene ug/L 50 55.8 112 70-130 Styrene ug/L 50 56.2 112 70-130 Tetrachloroethene ug/L 50 52.7 105 70-130 Toluene ug/L 50 52.9 106 70-130 trans-1,2-Dichloroethene ug/L 50 53.6 107 70-130 trans- 1,3-Dichloropropene ug/L 50 56.7 113 70-130 Trichloroethene ug/L 50 53.6 107 70-130 Trichlorofluoromethane ug/L 50 50.8 102 61-130 Vinyl acetate ug/L 100 133 133 70-140 Vinyl chloride ug/L 50 54.1 108 59-142 Xylene (Total) ug/L 150 166 111 70-130 1,2-Dichloroethane-d4 (S) % 102 70-130 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3446851 3446852 MS MSD 92570420003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 23.0 22.4 115 112 70-135 3 1,1,1-Trichloroethane ug/L ND 20 20 23.5 23.1 118 116 70-148 2 1,1,2,2-Tetrachloroethane ug/L ND 20 20 22.5 21.5 113 108 70-131 5 1,1,2-Trichloroethane ug/L ND 20 20 22.5 22.4 112 112 70-136 1 1,1-Dichloroethane ug/L ND 20 20 22.8 22.5 114 112 70-147 1 1,1-Dichloroethene ug/L ND 20 20 23.0 22.4 115 112 70-158 3 1,1-Dichloropropene ug/L ND 20 20 22.5 22.2 112 111 70-149 1 1,2,3-Trichlorobenzene ug/L ND 20 20 22.4 21.7 112 109 68-140 3 1,2,3-Trichloropropane ug/L ND 20 20 21.5 20.9 107 104 67-137 3 1,2,4-Trichlorobenzene ug/L ND 20 20 21.7 21.5 109 108 70-139 1 1,2-Dibromo-3-chloropropane ug/L ND 20 20 21.9 21.7 110 108 69-136 1 1,2-Dibromoethane (EDB) ug/L ND 20 20 22.6 21.7 113 109 70-137 4 1,2-Dichlorobenzene ug/L ND 20 20 22.4 22.1 112 111 70-133 1 1,2-Dichloroethane ug/L ND 20 20 21.9 21.3 109 107 67-138 2 1,2-Dichloropropane ug/L ND 20 20 22.7 22.8 114 114 70-138 0 1,3-Dichlorobenzene ug/L ND 20 20 22.1 22.0 111 110 70-133 0 1,3-Dichloropropane ug/L ND 20 20 22.0 21.4 110 107 70-136 3 1,4-Dichlorobenzene ug/L ND 20 20 22.5 22.2 112 111 70-133 1 2,2-Dichloropropane ug/L ND 20 20 22.8 22.2 114 111 52-155 3 2-Butanone (MEK) ug/L ND 40 40 46.2 44.1 115 110 61-147 4 2-Chlorotoluene ug/L ND 20 20 22.5 22.1 113 110 70-141 2 2-Hexanone ug/L ND 40 40 42.2 40.4 105 101 67-139 4 4-Chlorotoluene ug/L ND 20 20 21.6 21.4 108 107 70-135 1 4-Methyl-2-pentanone (MIBK) ug/L ND 40 40 42.1 41.1 105 103 67-136 3 Acetone ug/L ND 40 40 43.2 42.1 108 105 55-159 3 Benzene ug/L ND 20 20 22.5 22.1 112 111 67-150 2 Bromobenzene ug/L ND 20 20 22.8 22.3 114 112 70-134 2 Bromochloromethane ug/L ND 20 20 23.4 22.6 117 113 70-146 4 Bromodichloromethane ug/L ND 20 20 22.4 21.8 112 109 70-138 3 Bromoform ug/L ND 20 20 21.5 20.8 107 104 57-138 3 Bromomethane ug/L ND 20 20 22.5 22.9 113 115 10-200 2 Carbon tetrachloride ug/L ND 20 20 22.9 23.1 115 115 70-147 1 Chlorobenzene ug/L ND 20 20 22.8 22.3 114 112 70-137 2 Chloroethane ug/L ND 20 20 25.0 25.3 125 126 51-166 1 Chloroform ug/L ND 20 20 24.2 23.4 121 117 70-144 3 Chloromethane ug/L ND 20 20 22.5 22.4 112 112 24-161 0 cis-1,2-Dichloroethene ug/L ND 20 20 23.1 22.7 116 113 67-148 2 cis-1,3-Dichloropropene ug/L ND 20 20 22.0 21.7 110 108 70-142 1 Dibromochloromethane ug/L ND 20 20 22.4 21.8 112 109 68-138 3 Dibromomethane ug/L ND 20 20 23.2 22.8 116 114 70-134 2 Dichlorodifluoromethane ug/L ND 20 20 25.1 24.7 126 123 43-155 2 Diisopropyl ether ug/L ND 20 20 21.0 20.7 105 103 65-146 2 Ethylbenzene ug/L ND 20 20 22.6 22.1 113 110 68-143 3 Hexachloro-1,3-butadiene ug/L ND 20 20 23.3 22.8 116 114 62-151 2 m&p-Xylene ug/L ND 40 40 45.0 44.5 113 111 53-157 1 Methyl-tert-butyl ether ug/L ND 20 20 21.9 21.3 109 106 59-156 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3446851 3446852 MS MSD 92570420003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Methylene Chloride ug/L ND 20 20 22.0 21.5 110 107 64-148 2 Naphthalene ug/L ND 20 20 22.2 21.8 111 109 57-150 2 o-Xylene ug/L ND 20 20 22.4 21.9 112 109 68-143 2 p-Isopropyltoluene ug/L ND 20 20 21.8 21.7 109 109 70-141 1 Styrene ug/L ND 20 20 15.4 15.6 77 78 70-136 1 Tetrachloroethene ug/L ND 20 20 22.5 22.1 112 111 70-139 2 Toluene ug/L ND 20 20 22.6 22.2 113 111 47-157 2 trans-1,2-Dichloroethene ug/L ND 20 20 23.3 22.6 116 113 70-149 3 trans- 1,3-Dichloropropene ug/L ND 20 20 21.7 20.9 109 105 70-138 4 Trichloroethene ug/L ND 20 20 23.1 22.7 115 113 70-149 2 Trichlorofluoromethane ug/L ND 20 20 22.0 21.8 110 109 61-154 1 Vinyl acetate ug/L ND 40 40 37.9 37.6 95 94 48-156 1 Vinyl chloride ug/L ND 20 20 25.3 25.0 126 125 55-172 1 Xylene (Total) ug/L ND 60 60 67.5 66.4 112 111 66-145 2 1,2-Dichloroethane-d4 (S) % 93 96 70-130 4-Bromofluorobenzene (S) % 101 100 70-130 Toluene-d8(S) % 99 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657830 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92569918007 METHOD BLANK: 3448080 Associated Lab Samples: 92569918007 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/09/21 18:05 1,1,1-Trichloroethane ug/L ND 1.0 11/09/21 18:05 1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/09/21 18:05 1,1,2-Trichloroethane ug/L ND 1.0 11/09/21 18:05 1,1-Dichloroethane ug/L ND 1.0 11/09/21 18:05 1,1-Dichloroethene ug/L ND 1.0 11/09/21 18:05 1,1-Dichloropropene ug/L ND 1.0 11/09/21 18:05 1,2,3-Trichlorobenzene ug/L ND 1.0 11/09/21 18:05 1,2,3-Trichloropropane ug/L ND 1.0 11/09/21 18:05 1,2,4-Trichlorobenzene ug/L ND 1.0 11/09/21 18:05 1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/09/21 18:05 1,2-Dibromoethane (EDB) ug/L ND 1.0 11/09/21 18:05 1,2-Dichlorobenzene ug/L ND 1.0 11/09/21 18:05 1,2-Dichloroethane ug/L ND 1.0 11/09/21 18:05 1,2-Dichloropropane ug/L ND 1.0 11/09/21 18:05 1,3-Dichlorobenzene ug/L ND 1.0 11/09/21 18:05 1,3-Dichloropropane ug/L ND 1.0 11/09/21 18:05 1,4-Dichlorobenzene ug/L ND 1.0 11/09/21 18:05 2,2-Dichloropropane ug/L ND 1.0 11/09/21 18:05 2-Butanone (MEK) ug/L ND 5.0 11/09/21 18:05 2-Chlorotoluene ug/L ND 1.0 11/09/21 18:05 2-Hexanone ug/L ND 5.0 11/09/21 18:05 4-Chlorotoluene ug/L ND 1.0 11/09/21 18:05 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 11/09/21 18:05 Acetone ug/L ND 25.0 11/09/21 18:05 Benzene ug/L ND 1.0 11/09/21 18:05 Bromobenzene ug/L ND 1.0 11/09/21 18:05 Bromochloromethane ug/L ND 1.0 11/09/21 18:05 Bromodichloromethane ug/L ND 1.0 11/09/21 18:05 Bromoform ug/L ND 1.0 11/09/21 18:05 Bromomethane ug/L ND 2.0 11/09/21 18:05 Carbon tetrachloride ug/L ND 1.0 11/09/21 18:05 Chlorobenzene ug/L ND 1.0 11/09/21 18:05 Chloroethane ug/L ND 1.0 11/09/21 18:05 Chloroform ug/L ND 1.0 11/09/21 18:05 Chloromethane ug/L ND 1.0 11/09/21 18:05 cis-1,2-Dichloroethene ug/L ND 1.0 11/09/21 18:05 cis-1,3-Dichloropropene ug/L ND 1.0 11/09/21 18:05 Dibromochloromethane ug/L ND 1.0 11/09/21 18:05 Dibromomethane ug/L ND 1.0 11/09/21 18:05 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 METHOD BLANK: 3448080 Associated Lab Samples: 92569918007 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Dichlorodifluoromethane ug/L ND 1.0 11/09/21 18:05 Diisopropyl ether ug/L ND 1.0 11/09/21 18:05 Ethylbenzene ug/L ND 1.0 11/09/21 18:05 Hexachloro-1,3-butadiene ug/L ND 2.0 11/09/21 18:05 m&p-Xylene ug/L ND 2.0 11/09/21 18:05 Methyl-tert-butyl ether ug/L ND 1.0 11/09/21 18:05 Methylene Chloride ug/L ND 5.0 11/09/21 18:05 Naphthalene ug/L ND 1.0 11/09/21 18:05 o-Xylene ug/L ND 1.0 11/09/21 18:05 p-Isopropyltoluene ug/L ND 1.0 11/09/21 18:05 Styrene ug/L ND 1.0 11/09/21 18:05 Tetrachloroethene ug/L ND 1.0 11/09/21 18:05 Toluene ug/L ND 1.0 11/09/21 18:05 trans-1,2-Dichloroethene ug/L ND 1.0 11/09/21 18:05 trans- 1,3-Dichloropropene ug/L ND 1.0 11/09/21 18:05 Trichloroethene ug/L ND 1.0 11/09/21 18:05 Trichlorofluoromethane ug/L ND 1.0 11/09/21 18:05 Vinyl acetate ug/L ND 2.0 11/09/21 18:05 Vinyl chloride ug/L ND 1.0 11/09/21 18:05 Xylene (Total) ug/L ND 1.0 11/09/21 18:05 1,2-Dichloroethane-d4 (S) % 91 70-130 11/09/21 18:05 4-Bromofluorobenzene (S) % 96 70-130 11/09/21 18:05 Toluene-d8 (S) % 103 70-130 11/09/21 18:05 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 3448081 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 52.5 105 70-130 1,1,1-Trichloroethane ug/L 50 47.3 95 70-130 1,1,2,2-Tetrachloroethane ug/L 50 49.8 100 70-130 1,1,2-Trichloroethane ug/L 50 51.4 103 70-130 1,1-Dichloroethane ug/L 50 46.1 92 70-130 1,1-Dichloroethene ug/L 50 46.5 93 70-132 1,1-Dichloropropene ug/L 50 48.9 98 70-131 1,2,3-Trichlorobenzene ug/L 50 55.5 111 70-134 1,2,3-Trichloropropane ug/L 50 49.7 99 70-130 1,2,4-Trichlorobenzene ug/L 50 54.9 110 70-130 1,2-Dibromo-3-chloropropane ug/L 50 54.9 110 70-132 1,2-Dibromoethane (EDB) ug/L 50 53.4 107 70-130 1,2-Dichlorobenzene ug/L 50 52.1 104 70-130 1,2-Dichloroethane ug/L 50 46.0 92 70-130 1,2-Dichloropropane ug/L 50 50.2 100 70-130 1,3-Dichlorobenzene ug/L 50 51.7 103 70-130 1,3-Dichloropropane ug/L 50 52.9 106 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 LABORATORY CONTROL SAMPLE: Parameter 3448081 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,4-Dichlorobenzene ug/L 50 52.1 104 70-130 2,2-Dichloropropane ug/L 50 48.6 97 70-130 2-Butanone (MEK) ug/L 100 101 101 70-133 2-Chlorotoluene ug/L 50 53.0 106 70-130 2-Hexanone ug/L 100 106 106 70-130 4-Chlorotoluene ug/L 50 50.0 100 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 105 105 70-130 Acetone ug/L 100 96.1 96 70-144 Benzene ug/L 50 49.2 98 70-130 Bromobenzene ug/L 50 53.2 106 70-130 Bromochloromethane ug/L 50 47.0 94 70-130 Bromodichloromethane ug/L 50 49.1 98 70-130 Bromoform ug/L 50 51.4 103 70-131 Bromomethane ug/L 50 49.7 99 30-177 Carbon tetrachloride ug/L 50 50.8 102 70-130 Chlorobenzene ug/L 50 50.2 100 70-130 Chloroethane ug/L 50 46.0 92 46-131 Chloroform ug/L 50 45.9 92 70-130 Chloromethane ug/L 50 45.8 92 49-130 cis-1,2-Dichloroethene ug/L 50 45.7 91 70-130 cis-1,3-Dichloropropene ug/L 50 51.6 103 70-130 Dibromochloromethane ug/L 50 54.0 108 70-130 Dibromomethane ug/L 50 48.7 97 70-130 Dichlorodifluoromethane ug/L 50 44.9 90 52-134 Diisopropyl ether ug/L 50 47.6 95 70-131 Ethylbenzene ug/L 50 50.0 100 70-130 Hexachloro-1,3-butadiene ug/L 50 57.4 115 70-131 m&p-Xylene ug/L 100 99.1 99 70-130 Methyl-tert-butyl ether ug/L 50 48.7 97 70-130 Methylene Chloride ug/L 50 47.5 95 68-130 Naphthalene ug/L 50 53.9 108 70-133 o-Xylene ug/L 50 50.3 101 70-130 p-Isopropyltoluene ug/L 50 53.1 106 70-130 Styrene ug/L 50 51.1 102 70-130 Tetrachloroethene ug/L 50 50.5 101 70-130 Toluene ug/L 50 47.5 95 70-130 trans-1,2-Dichloroethene ug/L 50 47.3 95 70-130 trans- 1,3-Dichloropropene ug/L 50 50.3 101 70-130 Trichloroethene ug/L 50 50.8 102 70-130 Trichlorofluoromethane ug/L 50 42.0 84 61-130 Vinyl acetate ug/L 100 112 112 70-140 Vinyl chloride ug/L 50 45.7 91 59-142 Xylene (Total) ug/L 150 149 100 70-130 1,2-Dichloroethane-d4 (S) % 88 70-130 4-Bromofluorobenzene (S) % 95 70-130 Toluene-d8 (S) % 97 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3448082 3448083 MS MSD 92570592004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 22.7 22.0 113 110 70-135 3 1,1,1-Trichloroethane ug/L ND 20 20 22.5 21.7 113 109 70-148 4 1,1,2,2-Tetrachloroethane ug/L ND 20 20 23.0 22.0 115 110 70-131 4 1,1,2-Trichloroethane ug/L ND 20 20 22.9 22.8 115 114 70-136 0 1,1-Dichloroethane ug/L ND 20 20 21.6 21.3 108 106 70-147 1 1,1-Dichloroethene ug/L ND 20 20 22.2 22.0 111 110 70-158 1 1,1-Dichloropropene ug/L ND 20 20 22.8 22.0 114 110 70-149 4 1,2,3-Trichlorobenzene ug/L ND 20 20 24.6 25.5 123 127 68-140 4 1,2,3-Trichloropropane ug/L ND 20 20 22.3 20.9 111 104 67-137 6 1,2,4-Trichlorobenzene ug/L ND 20 20 23.7 24.5 119 123 70-139 3 1,2-Dibromo-3-chloropropane ug/L ND 20 20 22.3 22.4 111 112 69-136 1 1,2-Dibromoethane (EDB) ug/L ND 20 20 22.8 22.5 114 113 70-137 1 1,2-Dichlorobenzene ug/L ND 20 20 23.0 23.3 115 116 70-133 1 1,2-Dichloroethane ug/L ND 20 20 20.5 20.7 102 103 67-138 1 1,2-Dichloropropane ug/L ND 20 20 22.7 22.6 113 113 70-138 0 1,3-Dichlorobenzene ug/L ND 20 20 23.2 23.3 116 117 70-133 0 1,3-Dichloropropane ug/L ND 20 20 23.3 22.7 116 113 70-136 3 1,4-Dichlorobenzene ug/L ND 20 20 23.4 23.8 117 119 70-133 2 2,2-Dichloropropane ug/L ND 20 20 22.4 22.3 112 111 52-155 1 2-Butanone (MEK) ug/L ND 40 40 44.5 41.3 111 103 61-147 7 2-Chlorotoluene ug/L ND 20 20 23.1 23.8 116 119 70-141 3 2-Hexanone ug/L ND 40 40 46.4 44.0 116 110 67-139 5 4-Chlorotoluene ug/L ND 20 20 22.6 22.8 113 114 70-135 1 4-Methyl-2-pentanone (MIBK) ug/L ND 40 40 43.8 42.4 109 106 67-136 3 Acetone ug/L ND 40 40 42.9 40.3 107 101 55-159 6 Benzene ug/L ND 20 20 23.0 22.7 115 113 67-150 1 Bromobenzene ug/L ND 20 20 23.1 23.5 116 117 70-134 2 Bromochloromethane ug/L ND 20 20 21.8 20.9 109 104 70-146 4 Bromodichloromethane ug/L ND 20 20 21.7 21.4 108 107 70-138 1 Bromoform ug/L ND 20 20 21.3 20.8 107 104 57-138 2 Bromomethane ug/L ND 20 20 24.3 24.2 122 121 10-200 0 v2 Carbon tetrachloride ug/L ND 20 20 24.1 23.1 121 116 70-147 4 Chlorobenzene ug/L ND 20 20 22.9 22.9 115 114 70-137 0 Chloroethane ug/L ND 20 20 22.5 23.7 112 118 51-166 5 Chloroform ug/L ND 20 20 21.4 21.8 107 109 70-144 2 Chloromethane ug/L ND 20 20 20.0 20.3 100 101 24-161 1 cis-1,2-Dichloroethene ug/L ND 20 20 21.2 20.8 106 104 67-148 2 cis-1,3-Dichloropropene ug/L ND 20 20 22.0 21.9 110 110 70-142 0 Dibromochloromethane ug/L ND 20 20 22.3 22.6 111 113 68-138 2 Dibromomethane ug/L ND 20 20 22.0 21.4 110 107 70-134 3 Dichlorodifluoromethane ug/L ND 20 20 20.6 20.4 103 102 43-155 1 Diisopropyl ether ug/L ND 20 20 20.4 20.0 102 100 65-146 2 Ethylbenzene ug/L ND 20 20 22.8 22.5 114 112 68-143 2 Hexachloro-1,3-butadiene ug/L ND 20 20 28.8 27.9 144 139 62-151 3 m&p-Xylene ug/L ND 40 40 45.0 45.4 112 114 53-157 1 Methyl-tert-butyl ether ug/L ND 20 20 20.9 20.8 104 104 59-156 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3448082 3448083 MS MSD 92570592004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Methylene Chloride ug/L ND 20 20 21.5 21.5 108 108 64-148 0 Naphthalene ug/L ND 20 20 22.9 22.9 115 114 57-150 0 o-Xylene ug/L ND 20 20 22.1 22.3 111 112 68-143 1 p-Isopropyltoluene ug/L ND 20 20 23.8 24.8 119 124 70-141 4 Styrene ug/L ND 20 20 22.9 22.5 115 113 70-136 2 Tetrachloroethene ug/L ND 20 20 22.7 22.4 114 112 70-139 1 Toluene ug/L ND 20 20 21.9 21.6 109 108 47-157 1 trans-1,2-Dichloroethene ug/L ND 20 20 22.5 22.5 112 113 70-149 0 trans- 1,3-Dichloropropene ug/L ND 20 20 21.4 21.6 107 108 70-138 1 Trichloroethene ug/L ND 20 20 23.4 22.9 117 115 70-149 2 Trichlorofluoromethane ug/L ND 20 20 20.5 20.4 102 102 61-154 0 Vinyl acetate ug/L ND 40 40 45.3 43.7 113 109 48-156 4 Vinyl chloride ug/L ND 20 20 21.3 21.6 107 108 55-172 1 Xylene (Total) ug/L ND 60 60 67.1 67.7 112 113 66-145 1 1,2-Dichloroethane-d4 (S) % 98 91 70-130 4-Bromofluorobenzene (S) % 97 97 70-130 Toluene-d8(S) % 98 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657257 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92569918001, 92569918002 METHOD BLANK: 3445139 Associated Lab Samples: 92569918001, 92569918002 Parameter Units 1,4-Dioxane (p-Dioxane) ug/L 1,2-Dichloroethane-d4 (S) % Toluene-d8 (S) % Matrix: Water Blank Reporting Result Limit Analyzed ND 2.0 11 /03/21 13:27 87 70-130 11/03/2113:27 89 66-133 11/03/2113:27 Qualifiers LABORATORY CONTROL SAMPLE: 3445140 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 19.3 97 70-130 1,2-Dichloroethane-d4 (S) % 87 70-130 Toluene-d8 (S) % 88 66-133 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3445141 3445142 MS MSD 92569908001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 19.6 19.2 98 96 64-141 2 1,2-Dichloroethane-d4 (S) % 87 90 70-130 Toluene-d8(S) % 90 90 66-133 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657574 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92569918004, 92569918005, 92569918006 METHOD BLANK: 3446979 Matrix: Water Associated Lab Samples: 92569918004, 92569918005, 92569918006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 11/04/21 13:35 1,2-Dichloroethane-d4 (S) % 99 70-130 11/04/21 13:35 Toluene-d8 (S) % 101 66-133 11/04/21 13:35 LABORATORY CONTROL SAMPLE: 3446980 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 19.4 97 70-130 1,2-Dichloroethane-d4 (S) % 96 70-130 Toluene-d8 (S) % 98 66-133 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3446981 3446982 MS MSD 40236135004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,4-Dioxane(p-Dioxane) ug/L 228 80 80 311 307 104 99 64-141 1 1,2-Dichloroethane-d4 (S) % 100 106 70-130 Toluene-d8(S) % 93 100 66-133 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657931 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92569918007 METHOD BLANK: 3448753 Matrix: Water Associated Lab Samples: 92569918007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 11/05/21 14:29 1,2-Dichloroethane-d4 (S) % 95 70-130 11/05/21 14:29 Toluene-d8 (S) % 96 66-133 11/05/21 14:29 LABORATORY CONTROL SAMPLE: 3448754 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane(p-Dioxane) ug/L 20 21.0 105 70-130 1,2-Dichloroethane-d4 (S) % 93 70-130 Toluene-d8(S) % 94 66-133 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3448755 3448756 MS MSD 92570731001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 19.1 18.9 95 95 64-141 1 1,2-Dichloroethane-d4 (S) % 105 97 70-130 Toluene-d8(S) % 96 93 66-133 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 58 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657076 Analysis Method: EPA 8270E QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92569918001, 92569918002 METHOD BLANK: 3444440 Associated Lab Samples: 92569918001, 92569918002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,2,4-Trichlorobenzene ug/L ND 10.0 11/02/21 18:02 1,2-Dichlorobenzene ug/L ND 10.0 11/02/21 18:02 1,3-Dichlorobenzene ug/L ND 10.0 11/02/21 18:02 1,4-Dichlorobenzene ug/L ND 10.0 11/02/21 18:02 1-Methylnaphthalene ug/L ND 10.0 11/02/21 18:02 2,2'-Oxybis(1-chloropropane) ug/L ND 10.0 11/02/21 18:02 2,4,5-Trichlorophenol ug/L ND 10.0 11/02/21 18:02 2,4,6-Trichlorophenol ug/L ND 10.0 11/02/21 18:02 2,4-Dichlorophenol ug/L ND 10.0 11/02/21 18:02 2,4-Dimethylphenol ug/L ND 10.0 11/02/21 18:02 2,4-Dinitrophenol ug/L ND 50.0 11/02/21 18:02 2,4-Dinitrotoluene ug/L ND 10.0 11/02/21 18:02 2,6-Dinitrotoluene ug/L ND 10.0 11/02/21 18:02 2-Chloronaphthalene ug/L ND 10.0 11/02/21 18:02 2-Chlorophenol ug/L ND 10.0 11/02/21 18:02 2-Methylnaphthalene ug/L ND 10.0 11/02/21 18:02 2-Methylphenol(o-Cresol) ug/L ND 10.0 11/02/21 18:02 2-Nitroaniline ug/L ND 20.0 11/02/21 18:02 2-Nitrophenol ug/L ND 10.0 11/02/21 18:02 3&4-Methyl phenol (m&p Cresol) ug/L ND 10.0 11/02/21 18:02 3,3'-Dichlorobenzidine ug/L ND 20.0 11/02/21 18:02 3-Nitroaniline ug/L ND 20.0 11/02/21 18:02 4,6-Dinitro-2-methyl phenol ug/L ND 20.0 11/02/21 18:02 4-Bromophenylphenyl ether ug/L ND 10.0 11/02/21 18:02 4-ChIoro-3-methyl phenol ug/L ND 10.0 11/02/21 18:02 4-Chloroaniline ug/L ND 20.0 11/02/21 18:02 4-Chlorophenylphenyl ether ug/L ND 10.0 11/02/21 18:02 4-Nitroaniline ug/L ND 20.0 11/02/21 18:02 4-Nitrophenol ug/L ND 50.0 11/02/21 18:02 Acenaphthene ug/L ND 10.0 11/02/21 18:02 Acenaphthylene ug/L ND 10.0 11/02/21 18:02 Aniline ug/L ND 10.0 11/02/21 18:02 Anthracene ug/L ND 10.0 11/02/21 18:02 Benzo(a)anthracene ug/L ND 10.0 11/02/21 18:02 Benzo(a)pyrene ug/L ND 10.0 11/02/21 18:02 Benzo(b)fluoranthene ug/L ND 10.0 11/02/21 18:02 Benzo(g,h,i)perylene ug/L ND 10.0 11/02/21 18:02 Benzo(k)fluoranthene ug/L ND 10.0 11/02/21 18:02 Benzoic Acid ug/L ND 50.0 11/02/21 18:02 Benzyl alcohol ug/L ND 20.0 11/02/21 18:02 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 METHOD BLANK: 3444440 Associated Lab Samples: 92569918001, 92569918002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed bis(2-Chloroethoxy)methane ug/L ND 10.0 11/02/21 18:02 bis(2-Chloroethyl) ether ug/L ND 10.0 11/02/21 18:02 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/02/21 18:02 Butylbenzylphthalate ug/L ND 10.0 11/02/21 18:02 Chrysene ug/L ND 10.0 11/02/21 18:02 Di-n-butylphthalate ug/L ND 10.0 11/02/21 18:02 Di-n-octylphthalate ug/L ND 10.0 11/02/21 18:02 Dibenz(a,h)anthracene ug/L ND 10.0 11/02/21 18:02 Dibenzofuran ug/L ND 10.0 11/02/21 18:02 Diethylphthalate ug/L ND 10.0 11/02/21 18:02 Dimethylphthalate ug/L ND 10.0 11/02/21 18:02 Fluoranthene ug/L ND 10.0 11/02/21 18:02 Fluorene ug/L ND 10.0 11/02/21 18:02 Hexachloro-1,3-butadiene ug/L ND 10.0 11/02/21 18:02 Hexachlorobenzene ug/L ND 10.0 11/02/21 18:02 Hexachlorocyclopentadiene ug/L ND 10.0 11/02/21 18:02 Hexachloroethane ug/L ND 10.0 11/02/21 18:02 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/02/21 18:02 Isophorone ug/L ND 10.0 11/02/21 18:02 N-Nitroso-di-n-propylamine ug/L ND 10.0 11/02/21 18:02 N-Nitrosodimethylamine ug/L ND 10.0 11/02/21 18:02 N-Nitrosodiphenylamine ug/L ND 10.0 11/02/21 18:02 Naphthalene ug/L ND 10.0 11/02/21 18:02 Nitrobenzene ug/L ND 10.0 11/02/21 18:02 Pentachlorophenol ug/L ND 20.0 11/02/21 18:02 Phenanthrene ug/L ND 10.0 11/02/21 18:02 Phenol ug/L ND 10.0 11/02/21 18:02 Pyrene ug/L ND 10.0 11/02/21 18:02 2,4,6-Tribromophenol (S) % 107 10-144 11/02/21 18:02 2-Fluorobiphenyl (S) % 99 10-130 11/02/21 18:02 2-Fluorophenol(S) % 64 10-130 11/02/21 18:02 Nitrobenzene-d5 (S) % 97 10-144 11/02/21 18:02 Phenol-d6 (S) % 47 10-130 11/02/21 18:02 Terphenyl-d14 (S) % 115 34-163 11/02/21 18:02 Qualifiers LABORATORY CONTROL SAMPLE: 3444441 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/L 50 37.8 76 18-130 1,2-Dichlorobenzene ug/L 50 33.2 66 20-130 1,3-Dichlorobenzene ug/L 50 31.5 63 18-130 1,4-Dichlorobenzene ug/L 50 32.3 65 18-130 1-Methylnaphthalene ug/L 50 45.5 91 29-130 2,2'-Oxybis(1-chloropropane) ug/L 50 48.6 97 28-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 60 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 LABORATORY CONTROL SAMPLE: Parameter 3444441 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,4,5-Trichlorophenol ug/L 50 56.1 112 35-130 2,4,6-Trichlorophenol ug/L 50 52.5 105 31-130 2,4-Dichlorophenol ug/L 50 47.5 95 35-130 2,4-Dimethylphenol ug/L 50 45.6 91 34-130 2,4-Dinitrophenol ug/L 250 209 83 10-153 v1 2,4-Dinitrotoluene ug/L 50 64.1 128 37-136 v1 2,6-Dinitrotoluene ug/L 50 62.5 125 33-136 2-Chloronaphthalene ug/L 50 50.3 101 26-130 2-Chlorophenol ug/L 50 40.3 81 37-130 2-Methylnaphthalene ug/L 50 44.4 89 29-130 2-Methylphenol(o-Cresol) ug/L 50 41.5 83 35-130 2-Nitroaniline ug/L 100 108 108 37-130 2-Nitrophenol ug/L 50 46.9 94 32-130 3&4-Methyl phenol (m&p Cresol) ug/L 50 45.0 90 34-130 3,3'-Dichlorobenzidine ug/L 100 110 110 34-136 3-Nitroaniline ug/L 100 123 123 37-138 4,6-Dinitro-2-methyl phenol ug/L 100 108 108 21-157 4-Bromophenylphenyl ether ug/L 50 51.7 103 38-130 4-ChIoro-3-methyl phenol ug/L 100 99.1 99 37-130 4-Chloroaniline ug/L 100 98.5 98 38-130 4-Chlorophenylphenyl ether ug/L 50 58.1 116 33-130 4-Nitroaniline ug/L 100 126 126 42-137 4-Nitrophenol ug/L 250 187 75 10-130 Acenaphthene ug/L 50 55.1 110 33-130 Acenaphthylene ug/L 50 54.4 109 35-130 Aniline ug/L 50 37.3 75 22-130 Anthracene ug/L 50 50.0 100 48-130 Benzo(a)anthracene ug/L 50 55.5 111 48-137 Benzo(a)pyrene ug/L 50 61.6 123 49-138 Benzo(b)fluoranthene ug/L 50 67.4 135 52-138 Benzo(g,h,i)perylene ug/L 50 61.6 123 48-140 Benzo(k)fluoranthene ug/L 50 64.5 129 48-139 Benzoic Acid ug/L 250 27.OJ 11 10-130 Benzyl alcohol ug/L 100 85.6 86 35-130 bis(2-Chloroethoxy)methane ug/L 50 49.2 98 34-130 bis(2-Chloroethyl) ether ug/L 50 47.3 95 36-130 bis(2-Ethylhexyl)phthalate ug/L 50 53.8 108 32-165 Butylbenzylphthalate ug/L 50 56.2 112 34-161 Chrysene ug/L 50 55.4 111 47-131 Di-n-butylphthalate ug/L 50 52.2 104 39-144 Di-n-octylphthalate ug/L 50 57.4 115 30-170 Dibenz(a,h)anthracene ug/L 50 61.8 124 49-138 Dibenzofuran ug/L 50 57.1 114 33-130 Diethylphthalate ug/L 50 59.5 119 38-131 Dimethylphthalate ug/L 50 58.5 117 37-130 Fluoranthene ug/L 50 55.1 110 46-137 Fluorene ug/L 50 58.5 117 37-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 61 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 LABORATORY CONTROL SAMPLE: Parameter 3444441 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Hexachloro-1,3-butadiene ug/L 50 32.5 65 11-130 Hexachlorobenzene ug/L 50 48.6 97 38-130 Hexachlorocyclopentadiene ug/L 50 37.5 75 10-130 Hexachloroethane ug/L 50 28.2 56 14-130 Indeno(1,2,3-cd)pyrene ug/L 50 63.5 127 41-130 Isophorone ug/L 50 46.9 94 33-130 N-Nitroso-di-n-propylamine ug/L 50 51.3 103 36-130 N-Nitrosodimethylamine ug/L 50 40.9 82 34-130 N-Nitrosodiphenylamine ug/L 50 47.5 95 37-130 Naphthalene ug/L 50 41.1 82 30-130 Nitrobenzene ug/L 50 46.7 93 36-130 Pentachlorophenol ug/L 100 98.0 98 23-149 Phenanthrene ug/L 50 50.8 102 44-130 Phenol ug/L 50 29.3 59 18-130 Pyrene ug/L 50 52.3 105 47-134 2,4,6-Tribromophenol (S) % 118 10-144 2-Fluorobiphenyl (S) % 107 10-130 2-Fluorophenol (S) % 68 10-130 Nitrobenzene-d5 (S) % 101 10-144 Phenol-d6 (S) % 56 10-130 Terphenyl-d14 (S) % 115 34-163 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3444748 MS 92565649015 Spike Parameter Units Result Conc. MSD Spike Conc. 3444747 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Qual 1,2,4-Trichlorobenzene ug/L ND 83.3 83.3 43.6 39.0 52 47 10-130 11 1,2-Dichlorobenzene ug/L ND 83.3 83.3 35.6 32.2 43 39 10-130 10 1,3-Dichlorobenzene ug/L ND 83.3 83.3 33.3 29.9 40 36 10-130 11 1,4-Dichlorobenzene ug/L ND 83.3 83.3 34.1 31.0 41 37 10-130 9 1-Methylnaphthalene ug/L ND 83.3 83.3 52.6 47.8 63 57 10-130 9 2,2'-Oxybis(1-chloropropane) ug/L ND 83.3 83.3 47.1 43.4 57 52 12-142 8 2,4,5-Trichlorophenol ug/L ND 83.3 83.3 14.9J 77.2 18 93 10-143 2,4,6-Trichlorophenol ug/L ND 83.3 83.3 7.2J 64.2 9 77 10-147 M1 2,4-Dichlorophenol ug/L ND 83.3 83.3 14.7J 47.9 18 57 10-138 2,4-Dimethylphenol ug/L ND 83.3 83.3 50.7 47.1 61 56 25-130 7 2,4-Dinitrophenol ug/L ND 417 417 ND 113 3 27 10-165 M1,v1 2,4-Dinitrotoluene ug/L ND 83.3 83.3 102 101 122 121 29-148 1 v1 2,6-Dinitrotoluene ug/L ND 83.3 83.3 97.0 93.7 116 112 26-146 3 2-Chloronaphthalene ug/L ND 83.3 83.3 61.6 57.6 74 69 11-130 7 2-Chlorophenol ug/L ND 83.3 83.3 13.2J 37.2 16 45 10-133 2-Methylnaphthalene ug/L ND 83.3 83.3 51.2 46.5 61 56 13-130 10 2-Methylphenol(o-Cresol) ug/L ND 83.3 83.3 44.2 40.6 53 49 20-130 8 2-Nitroaniline ug/L ND 167 167 161 156 97 94 24-136 3 2-Nitrophenol ug/L ND 83.3 83.3 13.5J 44.4 16 53 10-153 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 62 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3444748 MS Parameter 3&4-Methyl phenol (m&p Cresol) 3,3'-Dichlorobenzidine 3-Nitroaniline 4,6-Din itro-2-methyl phenol 4-Bromophenylphenyl ether 4-ChIoro-3-methyl phenol 4-Chloroaniline 4-Chlorophenylphenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl alcohol bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Ethylhexyl)phthalate Butylbenzylphthalate Chrysene Di-n-butylphthalate Di-n-octylphthalate Dibenz(a,h)anthracene Dibenzofuran Diethylphthalate Dimethylphthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone N-Nitroso-di-n-propylamine N-Nitrosodimethylamine N-Nitrosodiphenylamine Naphthalene Nitrobenzene 92565649015 Spike Units Result Conc. ug/L ND 83.3 3444747 MSD Spike MS Conc. Result 83.3 47.5 MSD MS MSD % Rec Result % Rec % Rec Limits RPD Qual 43.2 57 52 16-130 10 ug/L ND 167 167 179 181 108 109 10-153 1 ug/L ND 167 167 197 190 118 114 22-151 3 ug/L ND 167 167 11.7J 119 7 72 10-180 M1 ug/L ND 83.3 83.3 80.3 77.9 96 93 25-130 3 ug/L ND 167 167 125 129 75 77 25-133 3 ug/L ND 167 167 109 102 65 61 14-132 6 ug/L ND 83.3 83.3 84.5 81.3 101 98 19-130 4 ug/L ND 167 167 209 202 125 121 29-150 3 ug/L ND 417 417 ND 224 2 54 10-130 M1 ug/L ND 83.3 83.3 73.1 69.4 88 83 16-130 5 ug/L ND 83.3 83.3 71.2 68.3 85 82 15-137 4 ug/L ND 83.3 83.3 37.8 35.3 45 42 10-130 7 ug/L ND 83.3 83.3 81.3 79.9 98 96 37-136 2 ug/L ND 83.3 83.3 90.6 89.9 109 108 40-145 1 ug/L ND 83.3 83.3 99.3 102 119 122 41-146 2 ug/L ND 83.3 83.3 108 107 130 128 39-151 1 ug/L ND 83.3 83.3 100 107 120 128 40-147 6 ug/L ND 83.3 83.3 99.3 104 119 125 40-146 5 ug/L ND 417 417 ND ND 0 0 10-130 M1 ug/L ND 167 167 95.3 82.0 57 49 25-130 15 ug/L ND 83.3 83.3 50.5 46.2 61 55 23-130 9 ug/L ND 83.3 83.3 48.3 43.2 58 52 25-130 11 ug/L ND 83.3 83.3 86.9 86.1 104 103 28-166 1 ug/L ND 83.3 83.3 90.6 89.7 109 108 33-165 1 ug/L ND 83.3 83.3 89.2 88.7 107 106 38-141 1 ug/L ND 83.3 83.3 88.0 84.7 106 102 32-153 4 ug/L ND 83.3 83.3 92.5 92.4 111 111 30-175 0 ug/L ND 83.3 83.3 99.6 106 120 127 39-148 6 ug/L ND 83.3 83.3 78.0 75.5 94 91 20-130 3 ug/L ND 83.3 83.3 93.3 92.7 112 111 28-142 1 ug/L ND 83.3 83.3 90.0 88.5 108 106 26-136 2 ug/L ND 83.3 83.3 93.1 91.3 112 110 39-143 2 ug/L ND 83.3 83.3 84.7 82.5 102 99 24-132 3 ug/L ND 83.3 83.3 37.2 32.8 45 39 10-130 12 ug/L ND 83.3 83.3 77.6 76.0 93 91 29-130 2 ug/L ND 83.3 83.3 41.6 39.2 50 47 10-130 6 ug/L ND 83.3 83.3 29.4 25.9 35 31 10-130 13 ug/L ND 83.3 83.3 101 107 121 128 39-148 6 ug/L ND 83.3 83.3 49.3 47.4 59 57 23-130 4 ug/L ND 83.3 83.3 52.9 47.7 63 57 25-130 10 ug/L ND 83.3 83.3 47.1 42.4 56 51 22-130 10 ug/L ND 83.3 83.3 76.1 74.6 91 90 26-134 2 ug/L ND 83.3 83.3 45.8 41.9 55 50 14-130 9 ug/L ND 83.3 83.3 47.9 45.6 57 55 25-130 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 63 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3444748 3444747 MS MSD 92565649015 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Pentachlorophenol ug/L ND 167 167 12.8J 128 8 77 10-175 M1 Phenanthrene ug/L ND 83.3 83.3 82.0 81.0 98 97 36-133 1 Phenol ug/L ND 83.3 83.3 21.6 32.5 26 39 10-130 40 R1 Pyrene ug/L ND 83.3 83.3 84.1 83.0 101 100 40-143 1 2,4,6-Tribromophenol (S) % 22 106 10-144 2-Fluorobiphenyl (S) % 74 68 10-130 2-Fluorophenol(S) % 7 39 10-130 SO Nitrobenzene-d5(S) % 59 57 10-144 Phenol-d6 (S) % 24 35 10-130 Terphenyl-d14(S) % 108 104 34-163 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 64 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657405 Analysis Method: EPA 8270E QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92569918005 METHOD BLANK: 3446149 Associated Lab Samples: 92569918005 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,2,4-Trichlorobenzene ug/L ND 10.0 11/04/21 15:50 1,2-Dichlorobenzene ug/L ND 10.0 11/04/21 15:50 1,3-Dichlorobenzene ug/L ND 10.0 11/04/21 15:50 1,4-Dichlorobenzene ug/L ND 10.0 11/04/21 15:50 1-Methylnaphthalene ug/L ND 10.0 11/04/21 15:50 2,2'-Oxybis(1-chloropropane) ug/L ND 10.0 11/04/21 15:50 2,4,5-Trichlorophenol ug/L ND 10.0 11/04/21 15:50 2,4,6-Trichlorophenol ug/L ND 10.0 11/04/21 15:50 2,4-Dichlorophenol ug/L ND 10.0 11/04/21 15:50 2,4-Dimethylphenol ug/L ND 10.0 11/04/21 15:50 2,4-Dinitrophenol ug/L ND 50.0 11/04/21 15:50 2,4-Dinitrotoluene ug/L ND 10.0 11/04/21 15:50 2,6-Dinitrotoluene ug/L ND 10.0 11/04/21 15:50 2-Chloronaphthalene ug/L ND 10.0 11/04/21 15:50 2-Chlorophenol ug/L ND 10.0 11/04/21 15:50 2-Methylnaphthalene ug/L ND 10.0 11/04/21 15:50 2-Methylphenol(o-Cresol) ug/L ND 10.0 11/04/21 15:50 2-Nitroaniline ug/L ND 20.0 11/04/21 15:50 2-Nitrophenol ug/L ND 10.0 11/04/21 15:50 3&4-Methyl phenol (m&p Cresol) ug/L ND 10.0 11/04/21 15:50 3,3'-Dichlorobenzidine ug/L ND 20.0 11/04/21 15:50 3-Nitroaniline ug/L ND 20.0 11/04/21 15:50 4,6-Dinitro-2-methyl phenol ug/L ND 20.0 11/04/21 15:50 4-Bromophenylphenyl ether ug/L ND 10.0 11/04/21 15:50 4-ChIoro-3-methyl phenol ug/L ND 10.0 11/04/21 15:50 4-Chloroaniline ug/L ND 20.0 11/04/21 15:50 4-Chlorophenylphenyl ether ug/L ND 10.0 11/04/21 15:50 4-Nitroaniline ug/L ND 20.0 11/04/21 15:50 4-Nitrophenol ug/L ND 50.0 11/04/21 15:50 Acenaphthene ug/L ND 10.0 11/04/21 15:50 Acenaphthylene ug/L ND 10.0 11/04/21 15:50 Aniline ug/L ND 10.0 11/04/21 15:50 Anthracene ug/L ND 10.0 11/04/21 15:50 Benzo(a)anthracene ug/L ND 10.0 11/04/21 15:50 Benzo(a)pyrene ug/L ND 10.0 11/04/21 15:50 Benzo(b)fluoranthene ug/L ND 10.0 11/04/21 15:50 Benzo(g,h,i)perylene ug/L ND 10.0 11/04/21 15:50 Benzo(k)fluoranthene ug/L ND 10.0 11/04/21 15:50 Benzoic Acid ug/L ND 50.0 11/04/21 15:50 Benzyl alcohol ug/L ND 20.0 11/04/21 15:50 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 65 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 METHOD BLANK: 3446149 Associated Lab Samples: 92569918005 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed bis(2-Chloroethoxy)methane ug/L ND 10.0 11/04/21 15:50 bis(2-Chloroethyl) ether ug/L ND 10.0 11/04/21 15:50 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/04/21 15:50 Butylbenzylphthalate ug/L ND 10.0 11/04/21 15:50 Chrysene ug/L ND 10.0 11/04/21 15:50 Di-n-butylphthalate ug/L ND 10.0 11/04/21 15:50 Di-n-octylphthalate ug/L ND 10.0 11/04/21 15:50 Dibenz(a,h)anthracene ug/L ND 10.0 11/04/21 15:50 Dibenzofuran ug/L ND 10.0 11/04/21 15:50 Diethylphthalate ug/L ND 10.0 11/04/21 15:50 Dimethylphthalate ug/L ND 10.0 11/04/21 15:50 Fluoranthene ug/L ND 10.0 11/04/21 15:50 Fluorene ug/L ND 10.0 11/04/21 15:50 Hexachloro-1,3-butadiene ug/L ND 10.0 11/04/21 15:50 Hexachlorobenzene ug/L ND 10.0 11/04/21 15:50 Hexachlorocyclopentadiene ug/L ND 10.0 11/04/21 15:50 Hexachloroethane ug/L ND 10.0 11/04/21 15:50 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/04/21 15:50 Isophorone ug/L ND 10.0 11/04/21 15:50 N-Nitroso-di-n-propylamine ug/L ND 10.0 11/04/21 15:50 N-Nitrosodimethylamine ug/L ND 10.0 11/04/21 15:50 N-Nitrosodiphenylamine ug/L ND 10.0 11/04/21 15:50 Naphthalene ug/L ND 10.0 11/04/21 15:50 Nitrobenzene ug/L ND 10.0 11/04/21 15:50 Pentachlorophenol ug/L ND 20.0 11/04/21 15:50 Phenanthrene ug/L ND 10.0 11/04/21 15:50 Phenol ug/L ND 10.0 11/04/21 15:50 Pyrene ug/L ND 10.0 11/04/21 15:50 2,4,6-Tribromophenol (S) % 87 10-144 11/04/21 15:50 2-Fluorobiphenyl (S) % 72 10-130 11/04/21 15:50 2-Fluorophenol(S) % 58 10-130 11/04/21 15:50 Nitrobenzene-d5 (S) % 83 10-144 11/04/21 15:50 Phenol-d6 (S) % 42 10-130 11/04/21 15:50 Terphenyl-d14 (S) % 109 34-163 11/04/21 15:50 Qualifiers LABORATORY CONTROL SAMPLE: 3446150 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/L 50 30.3 61 18-130 1,2-Dichlorobenzene ug/L 50 31.4 63 20-130 1,3-Dichlorobenzene ug/L 50 28.5 57 18-130 1,4-Dichlorobenzene ug/L 50 29.1 58 18-130 1-Methylnaphthalene ug/L 50 40.6 81 29-130 2,2'-Oxybis(1-chloropropane) ug/L 50 46.9 94 28-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 66 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 LABORATORY CONTROL SAMPLE: Parameter 3446150 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 2,4,5-Trichlorophenol ug/L 50 48.5 97 35-130 2,4,6-Trichlorophenol ug/L 50 46.8 94 31-130 2,4-Dichlorophenol ug/L 50 44.6 89 35-130 2,4-Dimethylphenol ug/L 50 43.1 86 34-130 2,4-Dinitrophenol ug/L 250 238 95 10-153 2,4-Dinitrotoluene ug/L 50 52.6 105 37-136 2,6-Dinitrotoluene ug/L 50 53.3 107 33-136 2-Chloronaphthalene ug/L 50 43.3 87 26-130 2-Chlorophenol ug/L 50 40.7 81 37-130 2-Methylnaphthalene ug/L 50 39.9 80 29-130 2-Methylphenol(o-Cresol) ug/L 50 40.5 81 35-130 2-Nitroaniline ug/L 100 106 106 37-130 2-Nitrophenol ug/L 50 43.0 86 32-130 3&4-Methyl phenol (m&p Cresol) ug/L 50 44.3 89 34-130 3,3'-Dichlorobenzidine ug/L 100 107 107 34-136 3-Nitroaniline ug/L 100 108 108 37-138 4,6-Dinitro-2-methyl phenol ug/L 100 99.2 99 21-157 4-Bromophenylphenyl ether ug/L 50 45.1 90 38-130 4-ChIoro-3-methyl phenol ug/L 100 94.5 95 37-130 4-Chloroaniline ug/L 100 94.2 94 38-130 4-Chlorophenylphenyl ether ug/L 50 48.1 96 33-130 4-Nitroaniline ug/L 100 116 116 42-137 4-Nitrophenol ug/L 250 163 65 10-130 Acenaphthene ug/L 50 46.3 93 33-130 Acenaphthylene ug/L 50 47.1 94 35-130 Aniline ug/L 50 44.6 89 22-130 Anthracene ug/L 50 49.4 99 48-130 Benzo(a)anthracene ug/L 50 52.3 105 48-137 Benzo(a)pyrene ug/L 50 53.9 108 49-138 Benzo(b)fluoranthene ug/L 50 58.1 116 52-138 Benzo(g,h,i)perylene ug/L 50 55.5 111 48-140 Benzo(k)fluoranthene ug/L 50 54.6 109 48-139 Benzoic Acid ug/L 250 121 48 10-130 Benzyl alcohol ug/L 100 86.9 87 35-130 bis(2-Chloroethoxy)methane ug/L 50 43.1 86 34-130 bis(2-Chloroethyl) ether ug/L 50 44.8 90 36-130 bis(2-Ethylhexyl)phthalate ug/L 50 55.0 110 32-165 Butylbenzylphthalate ug/L 50 59.4 119 34-161 Chrysene ug/L 50 52.2 104 47-131 Di-n-butylphthalate ug/L 50 50.7 101 39-144 Di-n-octylphthalate ug/L 50 55.1 110 30-170 Dibenz(a,h)anthracene ug/L 50 54.2 108 49-138 Dibenzofuran ug/L 50 47.9 96 33-130 Diethylphthalate ug/L 50 49.5 99 38-131 Dimethylphthalate ug/L 50 47.9 96 37-130 Fluoranthene ug/L 50 49.7 99 46-137 Fluorene ug/L 50 50.8 102 37-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 67 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 LABORATORY CONTROL SAMPLE: Parameter 3446150 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Hexachloro-1,3-butadiene ug/L 50 23.9 48 11-130 Hexachlorobenzene ug/L 50 45.8 92 38-130 Hexachlorocyclopentadiene ug/L 50 30.4 61 10-130 Hexachloroethane ug/L 50 25.5 51 14-130 Indeno(1,2,3-cd)pyrene ug/L 50 52.2 104 41-130 Isophorone ug/L 50 43.0 86 33-130 N-Nitroso-di-n-propylamine ug/L 50 46.1 92 36-130 N-Nitrosodimethylamine ug/L 50 34.8 70 34-130 N-Nitrosodiphenylamine ug/L 50 47.5 95 37-130 Naphthalene ug/L 50 37.5 75 30-130 Nitrobenzene ug/L 50 43.7 87 36-130 Pentachlorophenol ug/L 100 94.7 95 23-149 Phenanthrene ug/L 50 49.7 99 44-130 Phenol ug/L 50 26.7 53 18-130 Pyrene ug/L 50 50.0 100 47-134 2,4,6-Tribromophenol (S) % 105 10-144 2-Fluorobiphenyl (S) % 82 10-130 2-Fluorophenol (S) % 66 10-130 Nitrobenzene-d5 (S) % 89 10-144 Phenol-d6 (S) % 52 10-130 Terphenyl-d14 (S) % 106 34-163 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3446151 MS 92565649018 Spike Parameter Units Result Conc. MSD Spike Conc. 3446152 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Qual 1,2,4-Trichlorobenzene ug/L ND 50 50 31.8 32.7 64 65 10-130 3 1,2-Dichlorobenzene ug/L ND 50 50 27.2 28.7 54 57 10-130 5 1,3-Dichlorobenzene ug/L ND 50 50 25.1 26.5 50 53 10-130 6 1,4-Dichlorobenzene ug/L ND 50 50 29.3 30.4 49 51 10-130 4 1-Methylnaphthalene ug/L ND 50 50 36.5 37.9 73 76 10-130 4 2,2'-Oxybis(1-chloropropane) ug/L ND 50 50 38.7 39.0 77 78 12-142 1 2,4,5-Trichlorophenol ug/L ND 50 50 46.9 48.9 94 98 10-143 4 2,4,6-Trichlorophenol ug/L ND 50 50 43.2 44.4 86 89 10-147 3 2,4-Dichlorophenol ug/L ND 50 50 39.1 40.6 78 81 10-138 4 2,4-Dimethylphenol ug/L ND 50 50 36.7 38.1 73 76 25-130 4 2,4-Dinitrophenol ug/L ND 250 250 276 268 110 107 10-165 3 v1 2,4-Dinitrotoluene ug/L ND 50 50 54.2 56.2 108 112 29-148 4 v1 2,6-Dinitrotoluene ug/L ND 50 50 51.3 53.4 103 107 26-146 4 2-Chloronaphthalene ug/L ND 50 50 39.6 40.1 79 80 11-130 1 2-Chlorophenol ug/L ND 50 50 34.2 35.2 68 70 10-133 3 2-Methylnaphthalene ug/L ND 50 50 36.4 37.3 73 75 13-130 2 2-Methylphenol(o-Cresol) ug/L ND 50 50 34.7 36.0 69 72 20-130 4 2-Nitroaniline ug/L ND 100 100 87.9 90.7 88 91 24-136 3 2-Nitrophenol ug/L ND 50 50 38.0 38.4 76 77 10-153 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 68 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 MATRIX SPIKE & MATRIX SPIKE DUPLICATE Parameter 3&4-Methyl phenol (m&p Cresol) 3,3'-Dichlorobenzidine 3-Nitroaniline 4,6-Din itro-2-methyl phenol 4-Bromophenylphenyl ether 4-ChIoro-3-methyl phenol 4-Chloroaniline 4-Chlorophenylphenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl alcohol bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Ethylhexyl)phthalate Butylbenzylphthalate Chrysene Di-n-butylphthalate Di-n-octylphthalate Dibenz(a,h)anthracene Dibenzofuran Diethylphthalate Dimethylphthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone N-Nitroso-di-n-propylamine N-Nitrosodimethylamine N-Nitrosodiphenylamine Naphthalene Nitrobenzene QUALITY CONTROL DATA 3446151 MS 92565649018 Spike Units Result Conc. ug/L ND 50 ug/L ND 100 ug/L ND 100 ug/L ND 100 ug/L ND 50 ug/L ND 100 ug/L ND 100 ug/L ND 50 ug/L ND 100 ug/L ND 250 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 250 ug/L ND 100 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 ug/L ND 50 MSD Spike Conc. 3446152 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits 50 37.0 39.8 74 80 16-130 100 83.1 89.1 83 89 10-153 100 90.7 93.3 91 93 22-151 100 101 99.7 101 100 10-180 50 43.1 43.1 86 86 25-130 100 85.5 88.4 86 88 25-133 100 76.9 79.1 77 79 14-132 50 46.3 47.6 93 95 19-130 100 102 106 102 106 29-150 250 217 228 87 91 10-130 50 41.8 43.2 84 86 16-130 50 42.1 43.9 84 88 15-137 50 33.6 34.3 67 69 10-130 50 41.3 41.1 83 82 37-136 50 47.7 47.0 95 94 40-145 50 50.0 48.7 100 97 41-146 50 54.6 53.9 109 108 39-151 50 46.2 47.4 92 95 40-147 50 52.3 49.7 105 99 40-146 250 64.6 40.1J 26 16 10-130 100 71.9 76.7 72 77 25-130 50 37.3 38.0 75 76 23-130 50 38.5 38.5 77 77 25-130 50 47.3 46.1 95 92 28-166 50 50.2 47.6 100 95 33-165 50 47.3 45.9 95 92 38-141 50 46.2 46.1 92 92 32-153 50 49.7 51.0 99 102 30-175 50 45.9 48.1 92 96 39-148 50 44.5 46.2 89 92 20-130 50 50.2 52.1 100 104 28-142 50 47.9 49.6 96 99 26-136 50 47.5 47.9 95 96 39-143 50 45.7 47.8 91 96 24-132 50 27.8 29.0 56 58 10-130 50 42.0 41.8 84 84 29-130 50 32.3 32.7 65 65 10-130 50 23.4 24.2 47 48 10-130 50 45.7 47.2 91 94 39-148 50 37.8 39.1 76 78 23-130 50 38.7 39.4 77 79 25-130 50 37.5 38.3 75 77 22-130 50 40.4 40.4 81 81 26-134 50 32.8 33.7 66 67 14-130 50 36.6 37.4 73 75 25-130 RPD Qual 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. 7 3 1 0 3 3 3 4 5 3 4 2 0 1 3 1 2 5 6 2 0 3 5 3 0 3 5 4 4 4 1 4 5 1 1 3 3 3 2 2 0 3 2 Page 69 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3446151 3446152 MS MSD 92565649018 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Pentachlorophenol ug/L ND 100 100 92.1 89.5 92 89 10-175 3 Phenanthrene ug/L ND 50 50 42.9 43.0 86 86 36-133 0 Phenol ug/L ND 50 50 30.3 31.5 61 63 10-130 4 Pyrene ug/L ND 50 50 47.0 43.6 94 87 40-143 7 2,4,6-Tribromophenol (S) % 96 95 10-144 2-Fluorobiphenyl (S) % 75 76 10-130 2-Fluorophenol(S) % 59 60 10-130 Nitrobenzene-d5(S) % 76 76 10-144 Phenol-d6 (S) % 54 56 10-130 Terphenyl-d14(S) % 106 97 34-163 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 70 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657801 Analysis Method: EPA 8270E QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92569918004, 92569918006 METHOD BLANK: 3447982 Associated Lab Samples: 92569918004, 92569918006 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,2,4-Trichlorobenzene ug/L ND 10.0 11/07/21 09:36 1,2-Dichlorobenzene ug/L ND 10.0 11/07/21 09:36 1,3-Dichlorobenzene ug/L ND 10.0 11/07/21 09:36 1,4-Dichlorobenzene ug/L ND 10.0 11/07/21 09:36 1-Methylnaphthalene ug/L ND 10.0 11/07/21 09:36 2,2'-Oxybis(1-chloropropane) ug/L ND 10.0 11/07/21 09:36 2,4,5-Trichlorophenol ug/L ND 10.0 11/07/21 09:36 2,4,6-Trichlorophenol ug/L ND 10.0 11/07/21 09:36 2,4-Dichlorophenol ug/L ND 10.0 11/07/21 09:36 2,4-Dimethylphenol ug/L ND 10.0 11/07/21 09:36 2,4-Dinitrophenol ug/L ND 50.0 11/07/21 09:36 2,4-Dinitrotoluene ug/L ND 10.0 11/07/21 09:36 2,6-Dinitrotoluene ug/L ND 10.0 11/07/21 09:36 2-Chloronaphthalene ug/L ND 10.0 11/07/21 09:36 2-Chlorophenol ug/L ND 10.0 11/07/21 09:36 2-Methylnaphthalene ug/L ND 10.0 11/07/21 09:36 2-Methylphenol(o-Cresol) ug/L ND 10.0 11/07/21 09:36 2-Nitroaniline ug/L ND 20.0 11/07/21 09:36 2-Nitrophenol ug/L ND 10.0 11/07/21 09:36 3&4-Methyl phenol (m&p Cresol) ug/L ND 10.0 11/07/21 09:36 3,3'-Dichlorobenzidine ug/L ND 20.0 11/07/21 09:36 3-Nitroaniline ug/L ND 20.0 11/07/21 09:36 4,6-Dinitro-2-methyl phenol ug/L ND 20.0 11/07/21 09:36 4-Bromophenylphenyl ether ug/L ND 10.0 11/07/21 09:36 4-ChIoro-3-methyl phenol ug/L ND 10.0 11/07/21 09:36 4-Chloroaniline ug/L ND 20.0 11/07/21 09:36 4-Chlorophenylphenyl ether ug/L ND 10.0 11/07/21 09:36 4-Nitroaniline ug/L ND 20.0 11/07/21 09:36 4-Nitrophenol ug/L ND 50.0 11/07/21 09:36 Acenaphthene ug/L ND 10.0 11/07/21 09:36 Acenaphthylene ug/L ND 10.0 11/07/21 09:36 Aniline ug/L ND 10.0 11/07/21 09:36 Anthracene ug/L ND 10.0 11/07/21 09:36 Benzo(a)anthracene ug/L ND 10.0 11/07/21 09:36 Benzo(a)pyrene ug/L ND 10.0 11/07/21 09:36 Benzo(b)fluoranthene ug/L ND 10.0 11/07/21 09:36 Benzo(g,h,i)perylene ug/L ND 10.0 11/07/21 09:36 Benzo(k)fluoranthene ug/L ND 10.0 11/07/21 09:36 Benzoic Acid ug/L ND 50.0 11/07/21 09:36 Benzyl alcohol ug/L ND 20.0 11/07/21 09:36 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 71 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 METHOD BLANK: 3447982 Associated Lab Samples: 92569918004, 92569918006 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed bis(2-Chloroethoxy)methane ug/L ND 10.0 11/07/21 09:36 bis(2-Chloroethyl) ether ug/L ND 10.0 11/07/21 09:36 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/07/21 09:36 Butylbenzylphthalate ug/L ND 10.0 11/07/21 09:36 Chrysene ug/L ND 10.0 11/07/21 09:36 Di-n-butylphthalate ug/L ND 10.0 11/07/21 09:36 Di-n-octylphthalate ug/L ND 10.0 11/07/21 09:36 Dibenz(a,h)anthracene ug/L ND 10.0 11/07/21 09:36 Dibenzofuran ug/L ND 10.0 11/07/21 09:36 Diethylphthalate ug/L ND 10.0 11/07/21 09:36 Dimethylphthalate ug/L ND 10.0 11/07/21 09:36 Fluoranthene ug/L ND 10.0 11/07/21 09:36 Fluorene ug/L ND 10.0 11/07/21 09:36 Hexachloro-1,3-butadiene ug/L ND 10.0 11/07/21 09:36 Hexachlorobenzene ug/L ND 10.0 11/07/21 09:36 Hexachlorocyclopentadiene ug/L ND 10.0 11/07/21 09:36 Hexachloroethane ug/L ND 10.0 11/07/21 09:36 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/07/21 09:36 Isophorone ug/L ND 10.0 11/07/21 09:36 N-Nitroso-di-n-propylamine ug/L ND 10.0 11/07/21 09:36 N-Nitrosodimethylamine ug/L ND 10.0 11/07/21 09:36 N-Nitrosodiphenylamine ug/L ND 10.0 11/07/21 09:36 Naphthalene ug/L ND 10.0 11/07/21 09:36 Nitrobenzene ug/L ND 10.0 11/07/21 09:36 Pentachlorophenol ug/L ND 20.0 11/07/21 09:36 Phenanthrene ug/L ND 10.0 11/07/21 09:36 Phenol ug/L ND 10.0 11/07/21 09:36 Pyrene ug/L ND 10.0 11/07/21 09:36 2,4,6-Tribromophenol (S) % 72 10-144 11/07/21 09:36 2-Fluorobiphenyl (S) % 40 10-130 11/07/21 09:36 2-Fluorophenol(S) % 44 10-130 11/07/21 09:36 Nitrobenzene-d5 (S) % 58 10-144 11/07/21 09:36 Phenol-d6 (S) % 35 10-130 11/07/21 09:36 Terphenyl-d14 (S) % 92 34-163 11/07/21 09:36 Qualifiers LABORATORY CONTROL SAMPLE: 3447983 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/L 50 22.0 44 18-130 1,2-Dichlorobenzene ug/L 50 20.0 40 20-130 1,3-Dichlorobenzene ug/L 50 18.7 37 18-130 1,4-Dichlorobenzene ug/L 50 19.5 39 18-130 1-Methylnaphthalene ug/L 50 27.0 54 29-130 2,2'-Oxybis(1-chloropropane) ug/L 50 28.5 57 28-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 72 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 LABORATORY CONTROL SAMPLE: Parameter 3447983 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 2,4,5-Trichlorophenol ug/L 50 38.0 76 35-130 2,4,6-Trichlorophenol ug/L 50 35.5 71 31-130 2,4-Dichlorophenol ug/L 50 33.1 66 35-130 2,4-Dimethylphenol ug/L 50 32.2 64 34-130 2,4-Dinitrophenol ug/L 250 179 72 10-153 2,4-Dinitrotoluene ug/L 50 38.6 77 37-136 2,6-Dinitrotoluene ug/L 50 38.5 77 33-136 2-Chloronaphthalene ug/L 50 30.3 61 26-130 2-Chlorophenol ug/L 50 28.5 57 37-130 2-Methylnaphthalene ug/L 50 26.5 53 29-130 2-Methylphenol(o-Cresol) ug/L 50 28.4 57 35-130 2-Nitroaniline ug/L 100 80.3 80 37-130 2-Nitrophenol ug/L 50 31.4 63 32-130 3&4-Methyl phenol (m&p Cresol) ug/L 50 26.2 52 34-130 3,3'-Dichlorobenzidine ug/L 100 85.7 86 34-136 3-Nitroaniline ug/L 100 76.3 76 37-138 4,6-Dinitro-2-methyl phenol ug/L 100 82.0 82 21-157 4-Bromophenylphenyl ether ug/L 50 37.7 75 38-130 4-ChIoro-3-methyl phenol ug/L 100 70.8 71 37-130 4-Chloroaniline ug/L 100 63.3 63 38-130 4-Chlorophenylphenyl ether ug/L 50 33.5 67 33-130 4-Nitroaniline ug/L 100 76.7 77 42-137 4-Nitrophenol ug/L 250 117 47 10-130 Acenaphthene ug/L 50 32.3 65 33-130 Acenaphthylene ug/L 50 33.2 66 35-130 Aniline ug/L 50 29.1 58 22-130 Anthracene ug/L 50 39.0 78 48-130 Benzo(a)anthracene ug/L 50 42.5 85 48-137 Benzo(a)pyrene ug/L 50 43.2 86 49-138 Benzo(b)fluoranthene ug/L 50 42.6 85 52-138 Benzo(g,h,i)perylene ug/L 50 39.4 79 48-140 Benzo(k)fluoranthene ug/L 50 43.5 87 48-139 Benzoic Acid ug/L 250 78.4 31 10-130 Benzyl alcohol ug/L 100 60.0 60 35-130 bis(2-Chloroethoxy)methane ug/L 50 31.5 63 34-130 bis(2-Chloroethyl) ether ug/L 50 30.9 62 36-130 bis(2-Ethylhexyl)phthalate ug/L 50 49.0 98 32-165 Butylbenzylphthalate ug/L 50 47.0 94 34-161 Chrysene ug/L 50 41.7 83 47-131 Di-n-butylphthalate ug/L 50 45.8 92 39-144 Di-n-octylphthalate ug/L 50 45.8 92 30-170 Dibenz(a,h)anthracene ug/L 50 40.1 80 49-138 Dibenzofuran ug/L 50 33.4 67 33-130 Diethylphthalate ug/L 50 37.2 74 38-131 Dimethylphthalate ug/L 50 35.2 70 37-130 Fluoranthene ug/L 50 41.1 82 46-137 Fluorene ug/L 50 35.1 70 37-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 73 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 LABORATORY CONTROL SAMPLE: Parameter 3447983 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Hexachloro-1,3-butadiene ug/L 50 18.2 36 11-130 Hexachlorobenzene ug/L 50 40.4 81 38-130 Hexachlorocyclopentadiene ug/L 50 22.0 44 10-130 Hexachloroethane ug/L 50 18.0 36 14-130 Indeno(1,2,3-cd)pyrene ug/L 50 38.4 77 41-130 Isophorone ug/L 50 31.9 64 33-130 N-Nitroso-di-n-propylamine ug/L 50 29.9 60 36-130 N-Nitrosodimethylamine ug/L 50 24.4 49 34-130 N-Nitrosodiphenylamine ug/L 50 38.1 76 37-130 Naphthalene ug/L 50 26.4 53 30-130 Nitrobenzene ug/L 50 32.5 65 36-130 Pentachlorophenol ug/L 100 76.6 77 23-149 Phenanthrene ug/L 50 38.4 77 44-130 Phenol ug/L 50 18.5 37 18-130 Pyrene ug/L 50 43.4 87 47-134 2,4,6-Tribromophenol (S) % 89 10-144 2-Fluorobiphenyl (S) % 54 10-130 2-Fluorophenol (S) % 42 10-130 Nitrobenzene-d5 (S) % 62 10-144 Phenol-d6 (S) % 34 10-130 Terphenyl-d14 (S) % 88 34-163 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3448007 MS 92570300001 Spike Parameter Units Result Conc. MSD Spike Conc. 3448008 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Qual 1,2,4-Trichlorobenzene ug/L ND 90.9 90.9 44.9 56.0 49 62 10-130 22 1,2-Dichlorobenzene ug/L ND 90.9 90.9 49.0 56.0 54 62 10-130 13 1,3-Dichlorobenzene ug/L ND 90.9 90.9 44.6 51.6 49 57 10-130 15 1,4-Dichlorobenzene ug/L ND 90.9 90.9 45.9 53.2 50 59 10-130 15 1-Methylnaphthalene ug/L 26.1 90.9 90.9 80.2 111 59 93 10-130 32 R1 2,2'-Oxybis(1-chloropropane) ug/L ND 90.9 90.9 77.0 91.2 85 100 12-142 17 2,4,5-Trichlorophenol ug/L ND 90.9 90.9 71.1 80.3 78 88 10-143 12 2,4,6-Trichlorophenol ug/L ND 90.9 90.9 65.8 62.0 72 68 10-147 6 2,4-Dichlorophenol ug/L ND 90.9 90.9 70.3 83.1 77 91 10-138 17 2,4-Dimethylphenol ug/L ND 90.9 90.9 73.8 91.3 81 100 25-130 21 2,4-Dinitrophenol ug/L ND 455 455 ND ND 3 2 10-165 M1 2,4-Dinitrotoluene ug/L ND 90.9 90.9 71.2 92.6 78 102 29-148 26 2,6-Dinitrotoluene ug/L ND 90.9 90.9 77.1 97.7 85 107 26-146 24 2-Chloronaphthalene ug/L ND 90.9 90.9 65.7 83.0 72 91 11-130 23 2-Chlorophenol ug/L ND 90.9 90.9 70.6 81.2 78 89 10-133 14 2-Methylnaphthalene ug/L 62.9 90.9 90.9 115 161 57 108 13-130 33 R1 2-Methylphenol(o-Cresol) ug/L ND 90.9 90.9 69.8 84.9 77 93 20-130 20 2-Nitroaniline ug/L ND 182 182 164 212 90 117 24-136 25 2-Nitrophenol ug/L ND 90.9 90.9 73.9 85.4 81 94 10-153 14 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 74 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3448007 MS Parameter 3&4-Methyl phenol (m&p Cresol) 3,3'-Dichlorobenzidine 3-Nitroaniline 4,6-Din itro-2-methyl phenol 4-Bromophenylphenyl ether 4-ChIoro-3-methyl phenol 4-Chloroaniline 4-Chlorophenylphenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl alcohol bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Ethylhexyl)phthalate Butylbenzylphthalate Chrysene Di-n-butylphthalate Di-n-octylphthalate Dibenz(a,h)anthracene Dibenzofuran Diethylphthalate Dimethylphthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone N-Nitroso-di-n-propylamine N-Nitrosodimethylamine N-Nitrosodiphenylamine Naphthalene Nitrobenzene 92570300001 Spike Units Result Conc. ug/L ND 90.9 3448008 MSD Spike MS Conc. Result 90.9 66.1 MSD MS MSD % Rec Result % Rec % Rec Limits RPD Qual 80.8 73 89 16-130 20 ug/L ND 182 182 155 196 85 108 10-153 ug/L ND 182 182 152 195 84 107 22-151 ug/L ND 182 182 62.3 40.7 34 22 10-180 ug/L ND 90.9 90.9 72.6 88.9 80 98 25-130 ug/L ND 182 182 138 183 76 101 25-133 ug/L ND 182 182 144 181 79 99 14-132 ug/L ND 90.9 90.9 66.0 85.1 73 94 19-130 ug/L ND 182 182 149 195 82 107 29-150 ug/L ND 455 455 88.9J 48.6J 20 11 10-130 ug/L ND 90.9 90.9 69.3 86.6 76 95 16-130 ug/L ND 90.9 90.9 73.3 91.2 81 100 15-137 ug/L ND 90.9 90.9 76.6 90.4 84 99 10-130 ug/L ND 90.9 90.9 74.9 96.4 82 106 37-136 ug/L ND 90.9 90.9 84.7 104 93 114 40-145 ug/L ND 90.9 90.9 84.2 105 93 115 41-146 ug/L ND 90.9 90.9 83.7 111 92 122 39-151 ug/L ND 90.9 90.9 81.5 102 90 112 40-147 ug/L ND 90.9 90.9 82.3 105 91 115 40-146 ug/L ND 455 455 ND ND 0 0 10-130 ug/L ND 182 182 150 184 82 101 25-130 ug/L ND 90.9 90.9 73.6 94.1 81 103 23-130 ug/L ND 90.9 90.9 78.9 91.8 87 101 25-130 ug/L ND 90.9 90.9 90.1 114 99 125 28-166 ug/L ND 90.9 90.9 89.8 117 99 128 33-165 ug/L ND 90.9 90.9 83.2 103 92 114 38-141 ug/L ND 90.9 90.9 81.1 103 89 114 32-153 ug/L ND 90.9 90.9 88.3 115 97 126 30-175 ug/L ND 90.9 90.9 79.4 100 87 110 39-148 ug/L ND 90.9 90.9 70.2 89.1 77 98 20-130 ug/L ND 90.9 90.9 70.7 90.3 78 99 28-142 ug/L ND 90.9 90.9 70.9 90.2 78 99 26-136 ug/L ND 90.9 90.9 76.7 100 84 110 39-143 ug/L ND 90.9 90.9 71.3 91.5 78 101 24-132 ug/L ND 90.9 90.9 33.9 41.1 37 45 10-130 ug/L ND 90.9 90.9 75.7 95.2 83 105 29-130 ug/L ND 90.9 90.9 39.4 49.0 43 54 10-130 ug/L ND 90.9 90.9 40.2 48.2 44 53 10-130 ug/L ND 90.9 90.9 76.5 97.6 84 107 39-148 ug/L ND 90.9 90.9 71.0 91.7 78 101 23-130 ug/L ND 90.9 90.9 73.8 91.7 81 101 25-130 ug/L ND 90.9 90.9 63.8 75.2 70 83 22-130 ug/L ND 90.9 90.9 77.6 95.1 85 105 26-134 ug/L 135 90.9 90.9 187 264 57 141 14-130 ug/L ND 90.9 90.9 30.5 104 34 114 25-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. 24 25 42 R1 20 28 23 25 27 22 22 16 25 20 22 28 23 24 M1 21 24 15 23 26 22 24 26 23 24 24 24 26 25 19 23 22 18 24 25 22 16 20 34 M1,R1 109 R1 Page 75 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3448007 3448008 MS MSD 92570300001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Pentachlorophenol ug/L ND 182 182 88.0 75.9 48 42 10-175 15 Phenanthrene ug/L ND 90.9 90.9 75.4 95.4 83 105 36-133 23 Phenol ug/L ND 90.9 90.9 49.4 57.4 54 63 10-130 15 Pyrene ug/L ND 90.9 90.9 85.9 106 94 116 40-143 21 2,4,6-Tribromophenol (S) % 80 90 10-144 2-Fluorobiphenyl (S) % 65 83 10-130 2-Fluorophenol(S) % 57 57 10-130 Nitrobenzene-d5(S) % 77 98 10-144 Phenol-d6 (S) % 48 55 10-130 Terphenyl-d14(S) % 90 116 34-163 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 76 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 658187 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92569918001, 92569918002 METHOD BLANK: 3449820 Matrix: Water Associated Lab Samples: 92569918001, 92569918002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 mg/L ND 5.0 11/08/21 15:07 LABORATORY CONTROL SAMPLE: 3449821 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 mg/L 50 50.9 102 80-120 LABORATORY CONTROL SAMPLE: 3449822 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 mg/L 50 52.2 104 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3449823 3449824 MS MSD 92570663004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 mg/L 22.7 50 50 69.1 66.4 93 87 80-120 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3449825 3449826 MS MSD 92569908002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 mg/L ND 50 50 59.9 55.9 110 102 80-120 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 77 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 658188 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92569918004, 92569918005, 92569918006 METHOD BLANK: 3449832 Matrix: Water Associated Lab Samples: 92569918004, 92569918005, 92569918006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 mg/L ND 5.0 11/08/21 18:02 LABORATORY CONTROL SAMPLE: 3449833 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 mg/L 50 52.9 106 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3449834 3449835 MS MSD 92570961001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 mg/L 67400 50 50 115 130 95 126 80-120 13 M1 ug/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3449836 3449837 MS MSD 92570961009 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 mg/L ND 50 50 52.1 53.0 101 102 80-120 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 78 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657150 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92569918001, 92569918002 METHOD BLANK: 3444687 Matrix: Water Associated Lab Samples: 92569918001, 92569918002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 11/03/21 10:30 LABORATORY CONTROL SAMPLE: 3444688 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 254 102 90-110 SAMPLE DUPLICATE: 3444689 92569404006 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 234 229 2 SAMPLE DUPLICATE: 3444690 92569918001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 494 493 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 79 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657465 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92569918004, 92569918005, 92569918006 METHOD BLANK: 3446348 Matrix: Water Associated Lab Samples: 92569918004, 92569918005, 92569918006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 11/04/21 10:57 LABORATORY CONTROL SAMPLE: 3446349 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 264 106 90-110 SAMPLE DUPLICATE: 3446350 92570447001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 97.0 100 3 SAMPLE DUPLICATE: 3446351 92569918005 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L ND 27.0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 80 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657040 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92569918001, 92569918002 METHOD BLANK: 3444363 Matrix: Water Associated Lab Samples: 92569918001, 92569918002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate mg/L ND 1.0 11/02/2123:15 LABORATORY CONTROL SAMPLE: 3444364 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate mg/L 50 50.1 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3444365 3444366 MS MSD 92569903001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfate mg/L 179 50 50 235 236 112 115 90-110 1 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3444367 3444368 MS MSD 92569911003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfate mg/L 238 50 50 294 294 112 112 90-110 0 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 81 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 657704 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92569918004, 92569918005, 92569918006 METHOD BLANK: 3447750 Matrix: Water Associated Lab Samples: 92569918004, 92569918005, 92569918006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate mg/L ND 1.0 11/04/2121:19 LABORATORY CONTROL SAMPLE: 3447751 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate mg/L 50 47.4 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3447752 3447753 MS MSD 92570488001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfate mg/L ND 50 50 48.4 49.7 96 99 90-110 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3447754 3447755 MS MSD 92569918004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfate mg/L 2.5 50 50 50.9 52.4 97 100 90-110 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 82 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 658891 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92569918001, 92569918002, 92569918004, 92569918005, 92569918006 METHOD BLANK: 3453301 Matrix: Water Associated Lab Samples: 92569918001, 92569918002, 92569918004, 92569918005, 92569918006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 1.0 11/10/2121:32 LABORATORY CONTROL SAMPLE: 3453302 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 20 21.2 106 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3453303 3453304 MS MSD 92569908001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 0.72J 10 10 11.3 11.1 106 104 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3453305 3453306 MS MSD 92569908002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 0.76J 10 10 11.3 11.2 105 104 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 83 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 QC Batch: 659921 Analysis Method: SM 531 OB-2014 QC Batch Method: SM 531 OB-2014 Analysis Description: 5310E TOC Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92569918001, 92569918002, 92569918004, 92569918005, 92569918006 METHOD BLANK: 3458044 Matrix: Water Associated Lab Samples: 92569918001, 92569918002, 92569918004, 92569918005, 92569918006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 11/16/21 03:49 LABORATORY CONTROL SAMPLE: 3458045 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 26.9 108 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3458046 3458047 MS MSD 92569911013 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L 0.76J 25 25 27.3 27.7 106 108 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3458048 3458049 MS MSD 92569911014 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L ND 25 25 26.7 26.9 106 106 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 84 of 90 Pace Analytical Services, LLC leac,yficalAnal2225 Riverside Dr. Asheville, NC 28804 www.pacelabs.com (828)254-7176 QUALIFIERS Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS B Analyte was detected in the associated method blank. BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the laboratory reporting limit. IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be considered an estimated value. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. SO Surrogate recovery outside laboratory control limits. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 85 of 90 lacmnalyfica(' www,pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Glatfelter Sludge Landfill 92569918 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92569918001 WQ0013419-SWP1 92569918002 WQ0013419-SWP2 92569918004 WQ0013419-Q06V09 92569918005 WQ001 3419-Q06V1 0 92569918006 WQ0013419-Q06V11 92569918001 WQ0013419-SWP1 EPA 3010A 659038 EPA 6010D 659155 92569918002 WQ0013419-SWP2 EPA 3010A 659038 EPA 6010D 659155 92569918004 WQ0013419-Q06V09 EPA 3010A 659038 EPA 6010D 659155 92569918005 WQ001 3419-Q06V1 0 EPA 3010A 657606 EPA 6010D 657691 92569918006 WQ0013419-Q06V11 EPA 3010A 659038 EPA 6010D 659155 92569918001 WQ0013419-SWP1 EPA 1631E 660581 EPA 1631E 660775 92569918002 WQ0013419-SWP2 EPA 1631E 660581 EPA 1631E 660775 92569918003 FIELD BLANK EPA 1631E 660581 EPA 1631E 660775 92569918004 WQ0013419-Q06V09 EPA 1631E 660581 EPA 1631E 660775 92569918005 WQ001 3419-Q06V1 0 EPA 1631E 660581 EPA 1631E 660775 92569918006 WQ0013419-Q06V11 EPA 1631E 660581 EPA 1631E 660775 92569918001 WQ0013419-SWP1 EPA 3510C 657076 EPA 8270E 657180 92569918002 WQ0013419-SWP2 EPA 3510C 657076 EPA 8270E 657180 92569918004 WQ0013419-Q06V09 EPA 3510C 657801 EPA 8270E 658090 92569918005 WQ001 3419-Q06V1 0 EPA 3510C 657405 EPA 8270E 657636 92569918006 WQ0013419-Q06V11 EPA 3510C 657801 EPA 8270E 658090 92569918001 WQ0013419-SWP1 EPA 8260D 657346 92569918002 WQ0013419-SWP2 EPA 8260D 657346 92569918004 WQ0013419-Q06V09 EPA 8260D 657547 92569918005 WQ001 3419-Q06V1 0 EPA 8260D 657547 92569918006 WQ0013419-Q06V11 EPA 8260D 657547 92569918007 TRIP BLANK EPA 8260D 657830 92569918001 WQ0013419-SWP1 EPA 8260D Mod. 657257 92569918002 WQ0013419-SWP2 EPA 8260D Mod. 657257 92569918004 WQ0013419-Q06V09 EPA 8260D Mod. 657574 92569918005 WQ001 3419-Q06V1 0 EPA 8260D Mod. 657574 92569918006 WQ0013419-Q06V11 EPA 8260D Mod. 657574 92569918007 TRIP BLANK EPA 8260D Mod. 657931 92569918001 WQ0013419-SWP1 SM 2320B-2011 658187 92569918002 WQ0013419-SWP2 SM 2320B-2011 658187 92569918004 WQ0013419-Q06V09 SM 2320B-2011 658188 92569918005 WQ001 3419-Q06V1 0 SM 2320B-2011 658188 92569918006 WQ0013419-Q06V11 SM 2320B-2011 658188 92569918001 WQ0013419-SWP1 SM 2540C-2015 657150 92569918002 WQ0013419-SWP2 SM 2540C-2015 657150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /19/2021 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 86 of 90 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Glatfelter Sludge Landfill Pace Project No.: 92569918 Lab ID Sample ID QC Batch Method QC Batch 92569918004 W00013419406VO9 SM 2540C-2015 657465 92569918005 W00013419406V10 SM 2540C-2015 657465 92569918006 W00013419406V11 SM 2540C-2015 657465 92569918001 WQ0013419-SWP1 EPA 300.0 Rev 2.1 1993 657040 92569918002 W00013419-SWP2 EPA 300.0 Rev 2.1 1993 657040 92569918004 WQ0013419-QO6VO9 EPA 300.0 Rev 2.1 1993 657704 92569918005 WQ0013419-Q06V10 EPA 300.0 Rev 2.1 1993 657704 92569918006 WQ0013419-006V11 EPA 300.0 Rev 2.1 1993 657704 92569918001 W00013419-SWP1 SM 4500-CI-E-2011 658891 92569918002 WQ0013419-SWP2 SM 4500-CI-E-2011 658891 92569918004 WQ0013419-QO6VO9 SM 4500-CI-E-2011 658891 92569918005 WQ0013419-Q06V10 SM 4500-CI-E-2011 658891 92569918006 WQ0013419-Q06V11 SM 4500-CI-E-2011 658891 92569918001 W00013419-SWP1 SM 531OB-2014 659921 92569918002 W00013419-SWP2 SM 531OB-2014 659921 92569918004 W00013419406VO9 SM 531OB-2014 659921 92569918005 W00013419406V10 SM 531OB-2014 659921 92569918006 W00013419406V11 SM 531OB-2014 659921 Date: 11/19/2021 04:40 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Method Analytical Batch Page 87 of 90 aceAnalytira!" I - Document Name: Sample Condition Upon Recelpt(SCUR) Document Rev(sed: October 28, 2020 Page 1 of 2 Document No.: F-CAR-CS-033-Rev.07 Issuing Authority: Pace Carolinas Quality Office Laboratory Whig samples: rec Asheville Eden[] Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville[-] Atlanta❑ Kernersville❑ Client Name: GIa e: e,l la Projectk: Courier: �❑F dEx��f❑UPS ❑USPS ❑Cllent ❑Commercial WpIce ❑Other._ Custody Seal Present? []Yes E No Seals Intact? [Yes []NO Packing Material: ❑Bubble Wrap I735ubble Bags ❑None ❑ Other Thermometer, ovet ❑Blue ❑IR Gun ID: Type of Ice: /L Correction Factor: Cooler Temp: — Add/Subtract ('C) 0 Cooler Temp Corrected ('C : USDA Regulated Soil ( N/A, water sample) Did samples originate in a. quarantine zone within the United States: CA, NY, or SC (check maps)? WO#:92569918 HIM 1111111111111111 92568818 Date/Initials Person Examining Contents! ls I It tD Biological Tissue Frozen? ❑Yes ❑eFX No UN/A ❑None Temp should be above freezing to VC []samples out of temp criteria. Samples on ice, cooling process hasbegun Did samplesoriginate (ram a foreign source (internationally, Including Hawaii and Puerto Rico)? []Yes ❑No ❑Yes ❑No Comments/Dlscrepancy:_ Chain of Custody Present? ZYYes ❑No ❑N/A i. Samples Arrived within Hold Time? IT'es []NO ❑N/A 2. _ Short Hold Time Analysis (c72 hr.)? [)Yes t!JNo ❑NIA 3. Rush Turn Around Time Requested? []Yes Zo ❑NIA 4..--.- Sufficient Volume? r-X��/es No ❑N!A S. Correct Containers Used? -Pace Containers Used? ,I j[ves Rryes ❑No ❑No ❑NIA N/A 6. _ Containers Intact? es No ❑NIA 7. Dissolved analysis: Samples Field Filtered? Dyes ❑No 12K/A 9- _ Sample Labels Match COC? -includes Date{Time/ID/Anatysis Matrix: Headspace m VOA Vials (>S-6mm)? Oes W _ _ ❑Yes ❑No �� LgNo ❑NIA ❑NIA 9. 10. Trip Blank Present? hip Blanl Ctitody Seals Present? ❑Yes ❑Yes No ONO ❑N/A Qi/A _ 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION{RESOLUTION Person contacted: _ Date/lime: Project Manager SCURF Review: _ Date: Project Manager SRF Review: _ _ Date: Field Data Required? ❑Yes ❑No Document Name: Document *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottles Revised: Issuing Authority: Pace Carolinas Quality Office Project # WO# : 92569918 PM: UP Due Date: 11/15/21 CLIENT: 93—Slatfelte a t1 O n Z Q n a 1O n e m m L 9 Z w z N z W ? Z „ Z N 4 Z > Q � V V n z Z a A i 2 a H WWc a w O 4 O c z O z a y o a m 1O� r R a c c ] v�i 2 Z n J E 4 v�i d > _ p, Z o ] J c v 2 ry 2 C na n = o E E a a E o a a q4q `u Y a• E a a o a n a a E C E ¢ E F. E E E E E w E i E E E E n E E of E E NN ry N ry yvy pE. N Q N V II J J V,1 J e1 ] JI Z N U 4 m M P N 0a1 < N N QNQ M G m rV: e~1 li > O 3 I M1 5 7 8 9 ID 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot N adjusted added Note: Whenever there Is a discrepancy affecting Noith Carolina compliance samples, a copy of this form win oe sent to the norm t.armma ucmvn lei m114606 vnuc u.�. Out of hold, incorrect preservative, out of temp, Incorrect containers. n v O W W J N N A W N ITEM #_ 3 fu « 3 B X c N 3 da n o r n D o A 4 0 0 o sre W m o 8 8 o S o z` > c, m p oOy m D m or ym S o' 3 yy <SN N 9 pp < Qppp1 Op < O D S N (m1 S N G J yY V O e1 O ° r R ITI a 0 0 `n r; 3t Fo_o 8 aa,. "e kFy�"-e.- x FX c se _q rt �n n ryv Wv �9+ se $ aO 90trnag0 U U u Fi -JO m z N e p G as 3 mre 0 v MATRIX CODE (see valid Odes to left) 9 u 3 re y Z SAMPLETYPE (G=GRAB C=COMP) t C g o p G O D A � 0 orso m O y y N y y m 3 C on p r D y A nv z 4 z N y O To'X m _— f? in i s D 0 — N 3 3 g C/ I`J O y y r' in m m N SAMPLE TEMP AT COLLECTION w 9 "s 9 n o v n — #OF CONTAINERS s � a � R s.e �. UnpfeSeNed 9 90 u p q� m0 3. `o ] H2SO4 A m z o IF 3 HNO3 m i o. 'g d ., J I —ij HCI m a NaOH r 7^ Na2S203 N 0 1 j Methanol o �JJ I O Olirer r7 �.0 / Analyses Test YIN Fy S 0 x x x x x Metals by 6010 X x % Alkalinity F 3 z % X x x % Chloride, Sul(ata or N n x x x x x TDS by 2540C q�q S x x x x x x Low Level Mercury 2 6 - -- x x x x x TOC X x x x VOC by 8260 +i ax x x x x x svoc 8270 N x Trip BLANK 3 x x x x x 1,4 Dioxane-8260 SIM n m' x Trip Blank 8260 SIM � W A � TEMP in C c tD Residual Chlorine (V/N) S r Received on Ice 9 D (YIN) se 3 sto y Z (� O Cooler V/N VX U Samples Intact (YIN) 3� N A m non J m = � de Z a o 0v o EP N W v as -4 Pero m FIT � r cu0y o Crn 3 n r N � Z M °c D N a as X m < ry a »� ry M � m y P 0 �1D C 03 3 m ^� d n n 6 c a AN 0. 0 co m a! T m6 0 0 130 > o It, 0 0 c 0 z 0 MATRIX CODE (see valid codes to 180) SAMPLETYPE (G=GRAB C=COMP) 0 0 �O me J7 It on to V 0 0 5 22 z z CIA 01 V - — >1 m > C Z . on m zo 0 z m z ,A T f 57' ro to In SAMPLE TEMP AT COLLECTION Ct— # OF CONTAINERS -b -b In> - 0 2 2 2 3 a It, 44 Uppmerved no a b2. 0 Y: H2SO4 W HNO3 3 o HCl NaOH Na2S203 Methanol ,,AIINIIOSS-TSI YIN n Metals by 6010 x x x x Ix Alkalinity on 0 x x x x x Chloride, S.W. x x x x TDS by 2540C x x x x x x Low Level Mercury TOC x x x x x VOC by 8260 x x SVOC 8270 Trip BLANK x x ix x x 1A Dio.ane- 8260 SIM ji x Trip Blank 8260 SIM TEMP in C LID Residual Chlorine (YIN) E R .... v.d on Ice Re (YIN) T.—st—.d—y— Sealed IYINI J Samples Intact '—N I (YIN) Li ?8C8:An:31X1C,71' 1 Document Name: Sample Condition Upon Recei t SCUR) Document Revised: October 29, 2020 Page t of 2 Document No.: F-CAR-CS-033-Rev.07 sluing Authority: Pace Carolinas quality Office Laboratory r elving samples: Asheville Eden❑ Greenwood ❑ Huntersville ❑ Ralelgh❑ Mechanicsville❑ Atlanta❑ Kernersville❑ Client Name: Project q: C-00,k e, VU( wary. Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client ❑Commercial ice ❑Other._ Custody Seal Present? ❑Yes .Q#o— Seals Intact? ❑Ycs Dale/Initials Person Examining Conte nIs: _a )- i ( 3 Packing Material: [—]Bubble Wrap ❑Bubble Bags ❑None O—Other Biological Tissue Frozen? Thermometer: ❑Yes ❑No �A R Gun ID: et ❑Blue ❑None 3 1 Type or Ice: �7 Correction Factor: Cooler Temp: —! ' L— Add/Subtract ('C) Temp should be above freezing to VC []samples out of temp criteria. Samples on ice, cooling process Cooler Temp Corrected('C): I A hasbegun USDA Regulated Soil ( P-N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internationally, ram.✓ tnrludino Haw.r andPuerto Ricoi?( Yes 1390 IJYes u Comments/Discrepancy: Cha In of Custody Present? -El`es ❑No N/A i. Samples Arrived within Hold Time? ,BYe5' ONO ❑N{A 2. _ Short Hold Time Analysis (e72 hr,)? Oyes eORo ❑NIA 3. Rush Turn Around Time Requested? _ Yes Na ❑N/A 4. Sufficient Volume? E31es ONO ❑N/A S. Correct Containers Used? -Pace Containers Used? 0<s des ONO ❑No ❑N/A ❑N/A 6. - Containers Intact? s ONO ❑N/A 7. Dissolved analysis: Samples Field Filtered? _ ONO QN9 R. _ Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: r❑'1�Yes g7ei �x- ONO ❑N/A 9. Headspace in VOA Vials (>5-6mm)? ❑Yes [Pro t0. Trip Blank Present? Trip Blank Custody Seals Present? -des s ❑No ❑No OWA Il. _ COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes (—]No Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: / Project Manager SCURF Review: _ Date: Project Manager SRF Review: Date: Document Name: Document Revised: October 28, 2020 Sample Condition Upon Recelpt(SCUR) Page 2 of 2 Document No.: Issuing Authority: f /,/7"i[GCHlktlytlGd! F-CAA-CS-033-Rev.07 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is Project # verified and within the acceptance range for preservation /1� m saples. ��[[JJ exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottles R v z a Q 4 a U J a Z Z a d N A ry Z Z 2 Z N C = ? 7 N _ a U 9 a 5 A Y z V 2 a 2 Z \ 6 Z. 3 Y n a 2 \ Z `—' v `� z Z m •yn c c c v n O Z L y" c O VI yO N V O Z a O N a > m v Z c J L 0 n u J _N Z Z m ? U L 2 v • Y d L p. aJ q iv J n o m T u n m 5 a n E a E. E o ¢ ¢ J a S y y `v w m E a < Y € a E¢ 4 a C a O> O O> a o- ,n '", n -� E E E E u E E E E m E E E m i0 E E o E E N Vl r( N1 NNy N � n •-, N N ° P q R Y b' v N N N 4 J J J v, Z (f U LL „ N y� T m a N N M J ° , to P M •( M 01 O~1 m 0 O (� > 6 C 6 U• a N > t% ° - 1 3 1 I l0 3 1 2 I l0 3 2 4 n 5 2 7 8 3 10 I1 12 pH Adjustment Log for Preserved Samples Sample lD Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot N adjusted added Note: Whenever there is a discrepancy affectindrimm carmma compnance samprce,. wvv vl,.:,o,— —.,•,,,,�­•, Outof hold, incorrect preservative, out of temp. Incorrect containers.