WQ0004298_2002 Residuals Annual Report_20030218

Year:
PLAIN UAL LAND APPLICATION CERTIFIC"'rION FORM
.. - hermit#: (ZQ6004aA `b inty: 48af1;
Facility Name (as shown on permit)• T-
I otr�r► c��' I���� W: \1
Land Application Operator Phone: �� _
�i„ ,A 1 L5
Land application of residual solids as allowed by the permit occurred during the past calender year?
❑ Yes 0 No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Total number of application fields in permit:
a'
Total number of fields land application occurred during the year:
Total amount of dry tons applied during the year for all application sites:
FT
Total number of acres land application occurred during the year:
I
VW--tr62JH
Facility was compliant during calendar year 100with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Quality.. @j Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
.6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment fo knowing violations."
�-� ��
r o —TO
ermittee Name and Title (type or print) , L_B Signature of Permittee Date
Signature of Preparer*
Date Signiture of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Pmrf RM o i�x DENR FORM ACF (7120.02)

NUAL DISTRIBUTION AND MAR_K_FTING/ SURFA DISPOSAL CERTIFICATION AND SUMMARY FO]
PERMIT #: !LUQ600q} S ,�, FACILITY NAME: I owv� S m� r 5 'A\
PHONE: (a-�)C,jq _ q cg50 COUNTY: me A , -scon OPERATOR: y �r
FACILITY TYPE (please check one): 0 Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only and Part C)
0 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Q( Yes rlNo Nn If Nn ekin Wade A R r .—A .--4-:r— e » L
Part A*:
Part B*:
Month
January
Sources s (include NPDES # if
applicable)
Volume (dry tons)
Admendment/ �
Bulking Agent Residual In Product Out
g
Recipient Information
NameVolume (dry
s) Intended use(s)
tons)
February
March
—
April
May
June
July
r 51 -AjCeO I l
ilov►
-7, Q
August
September
October
November
December
Totals:
Annual (dry tons
dmendment s use
* Tf mnrP er,ara +l,.�n rritrcn in rnn,,;ro�
,,,10.,�� .,++.,..1..,,7,7:+:,....,.� �l
g gents used:
...__-'•: _ -�- _ �i_�
.-„
_.. .
..r..vv .11a.1..a 5-- — 1V.i lALL VLL, iJ1VCL0L1
Part C:
II I IUI.WaLIWI SUGCLIS). L_I necx Dox lI aQaitlonat slleet(s) are attached
Facility was compliant during calendar year ap0Q with all conditions of the permit (including but not limited to items 1-3 below) issued by t",
Division of Water Quality. Cf Yes 0 No If No, please provide a written description why the facility was not co mpliant.
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the *Division of Water
Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best, of my knowledge and belief, true, accurate and complete. I am aware
that there are significant penalties for submitting false informaiton, incluAing the possibility of fines and imprisonment for knowing..violations."
'1-03
Signature of Permittee Date 'Signature of Preparer** Date
(if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r)
DENR FORM DMSDF (7/2002)

Michael Ladd
75 Bison Lane
Murphy, NC 28906
Robbinsville Lab [phone]
Madison County Lab [phone]
• Residence [phone]
Name and Address of Facility: Date: 1/13/03
Town of Mars Hill WWTP Sample Collector: RS
P.O. Box 368 Date and Time Sample Received: 12/4/03 11:35 AM
Mars Hill, NC 28754 Date and Time Sample Collected: 12/3 & 4/02
Aft: Robert Sams Date and Time Sample Analyzed: < MHT
Land Application Analyses - Note: All results in mg/Kg Dry Basis unless othenndse noted.
Test
Aer. Dig Sludge
Dry Bed Sludge
Soil Site #1
Soil Site #2
Report Limit
Method
Units
ACIDITY
0.1 meq/100g
0.9 meq/100g
2.0
SM5210B
mg/L
TOTAL SUSPENDED RESIDUE
1.0
SM2540D
mg/L
CATION EXCHANGE CAPACITY
9.2 meq/100g
8.8 meq/100g
1
SM9222D
per 100ml
pH
6.6
6.5
6.9
6.3
0-14
SM4500H+
units
AMMONIA NITROGEN
52.6
18.7
0.5
SM4500NH3F
mg/L
NO2 + NO3-n
< 1.00
< 1.00
1.0
SM6520B
mg/L
TOTAL KJELDAHL NITROGEN
703
5000
SCA
mg/L
TOTAL PHOSPHOROUS
199
916
174
51
SCA
mg/L
PERCENT TOTAL RESIDUE
1.37%
5.11%
84.3%
83.7%
1.0
SM2540B
mg/L
%HUMIC MATTER
3.0%
3.30/6
1.0
SM2130B
NTU
%BASE SATURATION - K
3.7
28.8
1.0
SM2540C
mg/L
- H
1.4
10.6
- Nlg
30.3
25.6
-Ca
63.6
34.0
PLANT AVAILABLE (surface)
221.4
1503.8
10
SM2510B
umhos/cm
NITROGEN- PPM DRY WT (subsurf)
247.7
1513.1
0.1
SM4500CIG
mg/L
TEMPERATURE
SM2550B
deg C
MIXED LIQUOR SUPSPENDED SOLIDS
1.0
NIA
mg/L
MAGNESIUM
12200
5230
1390
2460
SCA
mg/L
SODIUM
11500
3030
< 58.1
< 56.9
SCA
mg/L
CADMIUM
< 71.5
< 18.6
< 1.16
< 1.14
SCA
mg/L
CHROMIUM
86
37.4
51.8
39.5
SCA
mg/L
COPPER
1070
399
27.6
15.3
SCA
mg/L
LEAD
172
67.3
13.3
10.2
SCA
mg/L
NICKEL
< 71.5
26.2
11.9
10.0 '
SCA
mg/L
ZINC
2350
822
61.2
43.7
SCA
mg/L
CALCIUM
52900
15900
2030
644
SCA
mg/L
POTASSIUM
12500
3600
738
3570
SCA
mg/L
ALUMINUM
52500
20700
SCA
mg/L
ARSENIC
E 71.6
< 19.6
< 1.16
< 1.14
SCA
mg/L
SELENIUM
< 143
< 37.4
< 2.33
< 2.27
SCA
mg/L
OLOLYBDENUM
< 71.6
< 18.6
< 1.16
< 1.14
SCA
mg/L
1WERCURY
< 7.30
< 1.96
< 0.12
< 0.12
SCA
mg/L
N.C. Laboratory ID# 352
Lab Supervisor: Michael J. Ladd; EES-Robbinsville
Analyzed By MB
Certified By: �Q

L
1 HIAc- Vl r
i
ry
C . Plant Available Nitrogen (PAN) calculations and land application area requirements;
CONSTITUENTS
M K - DRY WEIGHT
TKN
Si5 sq
AMMONIA,-N
,
NO3-NO2-N
1. Mineralization Rate (MR)
30
(These values. can be established for the specific residual or default values can be used for domestic wastewater treatment
residuals. If actual values are establlsbed, attach the documentation, The default values are as follgws):
Unstabilized Pritnsry and Secondary Residuals 40%
Aerobically Olgested Residuals 30%
Aaaerobically Dlgestcd Residuals 20%
Composted Residuals 10%
(If the default values are used, attach an explanation as to why the specific chosen default value is appropriate.)
2. Complete the following calculations for the application method proposed (Please note, the Mineralization
Rate [MR] should be utilized in the following calculations as a decimal):
PAN for Surface Application
PAN = [(MR) x (TKN - N143)1 + ,S x (NH3) + (NO3-NO2-N)
FAN( , �0 x( .SO&Z� 1 8r1 )]+.sx( G5, 7 )+
PAN PPM Dry Weight
PAN for Subsurface Application
PAN = l(MR)x(TKN - NH3)] + (NH3) + (NO3-NO2-N)
PAN-[ ,33 x( <5 ��0 �9-7 )]+( �0 `7
PAN = -513 -"1 PPM Dry Weight
3. Total PAN to be land applied per year �........
Total dry tons of residual to be land applied per year,

Test merieca.
I N C O R P O R A T E D
ANALYTICAL REPORT
TESTAMERICA-ASHEVILLE 5781 o Lab Number: 02-A199987
DINAH TRAMMEL x�` �"� Sample ID: EES #120224
122 LYMAN STREET (�`� Sample Type: Soil
ASHEVILLE, NC 28801 /16 Site ID:
`
-2;' '�Z
Date
Time
Collected:
Collected:
12/ 3/02
7 : 45
Project: �Q
Date
Received:
12/ 6/02
Project Name: ��
Sampler:
Time
Page:
Received:
1
9:00
Report
Dil
Analyse
------------------------
Result
-----------
Units
------
Limit
------
Factor
------
Date
--------
Time
-----
Analyst
----------
Method
---------
Batch
-----
*METALS*
Aluminum
52500
mg/kg
717.
1
12/13/02
1:23
C.Johnson
6010B
700
Arsenic
ND
mg/kg
71.5
1
12/23/02
1:23
C.Johnson
6010E
700
Cadmium
ND
mg/kg
71.5
1
12/13/02
1:23
C.Johnson
6010B
700
Calcium
52900
mg/kg
717.
1
12/13/02
1:23
C.Johnson
6010E
700
Chromium
86.
mg/kg
71.5
1
12/13/02
1:23
C.Johnson
6010E
700
Copper
1070
mg/kg
71.5
1
12/13/02
1:23
C.Johnson
6010E
700
Lead
172.
mg/kg
71.5
1
12/23/02
1:23
C.Johnson
6010D
700
Magnesium
12200
mg/kg
717.
1
12/13/02
1:23
C.Johnson
6010B
700
Mercury
ND
mg/kg
7.30
1
12/11/02
15:04
K.Hatchett
7471A
2053
Molybdenum
ND'
mg/kg
71.5
1
12/13/02
1:23
C.Johnson
6010E
700
Nickel
ND
mg/kg
71.5
1
12/13/02
1:23
C.Johnson
6010E
700
Potassium
12500•
mg/kg
3580
1
12/13/02
1:23
C.Johnson
6010E
700
Selenium
ND
mg/kg
143.
1
12/13/02
1:23
C.Johnson
6010E
700
Sodium
11500
mg/kg
3580
1
12/13/02
1:23
C.Johnson
6010E
700
Zinc
2350.
mg/kg
717.
1
12/13/02
1:23
C.Johnson
"6010B
700
*GENERAL CHEMISTRY PARAMETERS*
PH
6.60
pH units
12/ 7/02
21:15
S.
Self
9045
9357
Dry Weight
1.37
12/11/02
0:00
K.
Keller
CLP
9,339
Nitrite-N as N
ND
mg/kg
1.0
1
12/ 9/02
23:31
S.
Overton
9056
1287
Nitrate-N as N
ND
mg/kg
1.00
1
12/ 9/02
23:31
S.
Overton
9056
1287
Ammonia Nitrogen as N
52.6
mg/kg
1.00
1
12/13/02
23:00
S.
Prayter
350.1M
5391
Phosphorus as P
199.
mg/kg
10.0
1
12/15/02
23:00
G.
Baun
365.4 M
5477
Kjeldahl Nitrogen as N
703.
mg/kg
10.0
1
12/ 9/02
13:00
S.
Prayter
SM450ONC
1963
Sample report continued . . .
Onczn s.......... , n.............— n....... i M . ........ . .. M&I 0-7nnn i a1c vna nI'77 i c... a:: Boa nnCZn i onn'7ar, nnon

m rice.
�est e
I N C O R P D R A T E D
ANALYTICAL REPORT
TESTAMERICA-ASHEVILLE
DINAH TRAMMEL
122 LYMAN STREET
ASHEVILLE, NC 28801
Project:
Project Name:
Sampler:
5781
X0
Q
d�
Lab Number: 02-A199988
Sample ID: EES #120225
Sample Type: Soil
Site ID:
Date Collected: 12/ 4/02
Time Collected: 7:45
Date Received: 12/ 6/02
Time Received: -9:00
Page: 1
Report Dil
Analyte Result Units Limit Factor Date Time Analyst Method Batch
------------------------ - ----------- ------ ------ -------------- ----- ---------- ------- -----
*METALS*
Aluminum
20700
mg/kg
187.
1
12/13/02
1:23
C.Johnson
6010B
700
Arsenic
ND
mg/kg
18.6
1
12/13/02
1:23
C.Johnson
60108
700
Cadmium
ND
mg/kg
18.6
1
12/13/02
1:23
C.Johnson
6010E
700
Calcium
15900
mg/kg
187.
1
12/13/02
1:23
C.Johnson
6DiDB
700
Chromium
37.4
mg/kg
18.6
1
12/13/02
1:23
C.Johnson
6010E
700
Copper
399.
mg/kg
18.6
1
12/13/02
1:23
C.Johnson
6010E
7D0
Lead
67.3
mg/kg
18.6
1
12/13/02
1:23
C.Johnson
6010E
700
Magnesium
5230
mg/kg
187.
1
12/13/02
1:23
C.Johnson
6010B
700
Mercury
ND
mg/kg
1.96
1
12/11/02
15:04
K.Hatchett
7471A
2053
Molybdenum
ND
mg/kg
18.6
1
12/13/02
1:23
C.Johnson
6010E
700
Nickel
26.2
mg/kg
18.6
1
12/13/02
1:23
C.Johnson
6010E
700
Potassium
3600
mg/kg
933.
1
12/13/02
1:23
C.Johnson
6010E
700
Selenium
ND
mg/kg
37.4
1
12/13/02
1:23
C.Johnson
6010B
700
Silver
59.7
mg/kg
18.6
1
12/13/02
1:23
C.Johnson
6010B
700
Sodium
3030
mg/kg
933.
1
12/13/02
1:23
C.Johnson
6010B
700
zinc
822.
mg/kg
187.
1
12/13/02
1:23
C.Johnson
6010E
700
*GENERAL CHEMISTRY
PARAMETERS*
pH
6.50
pH units
12/ 7/02
21:20
S. Self
9045
9357
W Dry Weight
5.11
12/11/02
0:00
K. Keller
CLP
9339
Nitrite-N as N
ND
mg/kg
1.0
1
12/ 9/02
23:31
S. Overton
9056
1287
Nitrate-N as N
ND
mg/kg
1.00
1
12/ 9/02
23:31
S. Overton
9056
1287
Ammonia Nitrogen as
N 187.
mg/kg
10.0
10
12/12/02
8:45
S. Prayter
350.1M
1954
Phosphorus as P
916.
mg/kg
20.0
2
12/15/02
23:00
G. Baun
365.4 M
5477
Sample report continued . . .
')QAh Pilwrvu (`ovueumnrc nDIwv / N.+ein•ii i v TN .'17911A / AI R-77R-I1177 / R.:x• R17,-79R-f)AR4 / Rf10-7RR-1)ARfl

iest = merle
I N C O R P O R A T E D
ANALYTICAL REPORT �
Laboratory Number: 02-AI999`88
Sample ID: EES #120225
Project
Page 2
Report
Dil
Analyte
------------------------
Result Units
----------- ------
Limit
------
Factor
------
Date Time Analyst Method Batch
-------- -------- ------- --------- -----
Kjeldahl Nitrogen as N
5000 mg/kg
200.
20
12/ 9/02 13:00 S. Prayter SM45CONC 1963
LABORATORY COMMENTS:
ND = Not detected at the report limit.
B = Analyte was detected in the method blank.
J - Estimated Value below Report Limit.
E - Estimated Value above the calibration limit of the instrument.
# = Recovery outside Laboratory historical or method prescribed limits.
All reported results for metals or Organic analyses have been corrected for dry weight.
End of Sample Report.
)QRfI R11c•ruu Puu•v:irrnw Muni, / Nn�ucniu TN R7gnA / F,1r,-79R-f1177 / Rati• AlN-77R-nfigA / Rfin-7AR-nQA0

I
Test merica
I N C O R P O R A T E D
ANALYTICAL REPORT
TESTAMERICA-ASHEVILLE 5781 S
DINAH TRAMMEL X
122 LYMAN STREET o
ASHEVILLE, NC 28801
Project:
Project Name:
Sampler:
�1
C
Lab Number: 02-A199989
Sample ID: EES.4120226
Sample Type: Soil
Site ID:
Date Collected: 12/ 4/02
Time Collected: 14:00
Date Received: 12/ 6/02
Time Received: 9:00
Page: 1
Report Dil
Analyte Result Units Limit Factor Date Time Analyst Method Batch
------------------------ ----------- ------ ------ ------ -------- --------------- --------- -----
*METALS*
Cadmium
ND
mg/kg
1.16
1
12/12/02
13:31
G.McCord
6010B
2160
Calcium
2030
mg/kg
11.6
1
12/12/02
13:31
G.McCord
6010B
2160
Chromium
51.8
mg/kg
1.16
1
12/12/02
13:31
G.McCord
6010E
2160
Copper
27.6
mg/kg
1.16
1
12/12/02
13:31
G.MCCord
6010B
2160
Lead
13.3
mg/kg
1.16
1
12/12/02
13:31
G.McCord
6010E
2160
Magnesium
1390
mg/kg
11.6
1
12/12/02
13:31
G.McCord
6010E
2160
Mercury
ND
mg/kg
0.12
1
12/11/02
15:04
K.Hatchett
7471A
2053
kolybdenum
ND
mg/kg
1.16
1
12/12/02
13:31
G.McCord
6010E
2160
Nickel
11.9
mg/kg
1.16
1
12/12/02
13:31
G.McCord
6010E
2160
Potassium
738.
mg/kg
58.1
1
12/12/02
13:31
G.McCord
6010E
2160
Selenium
ND
mg/kg
2.33
1
12/12/02
13:31
G.McCord
6010E
2160
Silver
ND
mg/kg
1.16
1
12/12/02
13:31
G.McCord
6010B
2160
Sodium
ND
mg/kg
58.1
1
12/12/02
13:31
G.McCord
6010B
2160
Zinc
61.2
mg/kg
11.6
1
12/12/02
13:31
G.McCord
6010E
2160
*GENERAL CHEMISTRY
PARAMETERS*
PH
7.20
pH units
12/ 7/02
11:20
S. Self
9045
9357
1r Dry Weight
84.3
12/11/02
15:00
K. Keller
CLP
553
! Sample report continued . . .
9 A R 0 Fn nw..P (:Iw1(:u•rnn' Munn: / NACI11•II I u TN 179nd / A F_79R_n1 77 / P.%%. A 1,-,- 7 9 A_n Q :d / Ann- 7AF-no An

;estl= M'erioca-
I N C O R P O R A T E D
ANALYTICAL REPORT -
1
TESTAMERICA-ASHEVILLE
5781
Lab Number: 02-A199990
DINAH TRAMMEL
122 LYMAN STREET
Sample ID: EES #120227
Sample Type: Soil
ASHEVILLE, NC 28801
C) v
Site ID:
t7
Q)
Date Collected:
12/ 4/02
Project:
_IX J�
Time Collected:
14:10
Project Name:
�%
�
Date Received:
Time Received:-
12/ 6/02
9:00
Sampler:
�4S
�-
�
Page: 1
Report.
Dil
Analyte
------------------------
Result
-----------
Units
------
Limit
------
Factor
------
Date
--------
Time
-----
Analyst
----------
Method
---------
Batch
-----
*METALS*
Cadmium
ND
mg/kg
1.14
1
12/12/02
23:31
G.McCord
6010B
2160
Calcium
644.
mg/kg
11.4
1
12/12/02
13:31
G.Mccord
6010E
2160
Chromium
39.5
mg/kg
1.14
1
12/12/02
13:32
G.McCord
6010E
2160
Copper
15.3
mg/kg
1.14
1
12/12/02
13:31
G.McCord
6010B
2160
Lead
10.2
mg/kg
1.14
1
12/12/02
13:31
G.MCCord
6010E
2160
Magnesium
2460
mg/kg
11.4
1
12/12/02
13:31
G.McCord
6010B
2160
Mercury
ND
mg/kg
0.12
1
12/11/02
15:04
K.Hatchett
7471A
2053
Molybdenum
ND
mg/kg
1.14
1
12/12/02
13:31
G.McCord
6010B
2160
Nickel
10.0
mg/kg
1.14
1
12/12/02
13:31
G.McCord
6010E
2260
Potassium
3570
mg/kg
56.9
1
12/12/02
13:31
G.McCord
6010B
2160
Selenium
ND
mg/kg
2.27
1
12/12/02
13:31
G.McCord
6010E
2160
Silver
ND
mg/kg
1.14
1
12/12/02
13:31
G.McCord
6010B
2260
Sodium
ND
mg/kg
56.9
1
12/12/02
13:31
G.McCord
6010E
2160
Zinc
43.7
mg/kg
11.4
1
12/12/02
13:31
G.McCord
6010E
2160
*GENERAL CHEMISTRY
PARAMETERS*
PH
6.20
pH units
12/ 7/02 11:25 S. Self 9045 9357
t Dry Weight
83.7
Fr
12/11/02 15:00 K. Keller CLP 553
Sample report continued . . .
n0/-,n v.......... . I. ................ n...... I i m......... ... mnt n�nnA 1 04r inn n417P7 i n... eIr_ 17nn nne:A i 01111 qQG 11n00

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: (� Q Cj ®® a a 00
Facility Name:
NPDES # or
wQ#: N ®Q 5 15 1
WWTP Name: 16 ��
Residual Analysis Data
Sample or
Composite Date
I
30
L43t
8" Q
5-
( ��
L r� —
Percent Solids
f ' a.
Arsenic
a
Cadmium
Chromium
-7 -3a
Copper
`7-�0<
Lead
1 3 1 -
Mercury
< 3$ .4
Molybdenum
< 37
Nickel
Selenium
Zinc
TKNQ_0
C�
Ammonia-Nitroge
Nitrate and Nitriteko
71
l otal Phosphorus 11799
voo A-
-1 20 41
"I certify, under penalty of law,1
designed to assure that qualifie
significant penalties for submithngiaiac mxui-m.nu- I
Signature of Preparer
Laboratory: 1) E20` + G) ; �� �, ►i Y1 � Y1�Q.t 'lc
3)
4)
5)
vas prepared under my direction or supervision in accordance with a system
gathered and evaluated the information submitted. I am aware that there are
, including the possibility of fines and imprisonment for knowing violations."
a ®G-Q3
Date
DENR FORM RSSF (7/2002)

ANNUAL LAND APPLICATION FIELD SUMMARY-F ORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: A ; `1 Permit #: WQ 6p ® tf a 9 $ Annual Dry Tons Applied:
Owner: 0. r '� ��r `� Operator: o �. ,
L 771 C e, °�, orb vrs Cation Exchange Capacity (non 503): 9,
me(A/ z
Site #: 0 j Field #: ( Acres Utilized: j L- 0 Acres Permitted: ► 4 n=
�,
q
7
o
Specify
Totals
Per
Acre
C43
o
Solids
As
Deci-
mal
.
11
Dry
Tons
Per
Acre
b,14
Residual
Sources
(Summarize)
;n
JI b1D 5g�kU
Cond.
Dry,
Wet
Moist
r
Inches
Precip.
Past 24
Hrs.
O
O
Appli-
cation
Meth-
od**
u
Voli-
tila-
zation
Rate*
�:5
O.3°f
©
Muier-
ala-
TKN
zation
Rate
30
30� ,
Ammo
ma-
Ni-
trogen
Od
, 1O
dd©
Ni-trate
Ni-
trogen
O
PAN i
-
)......_;. -.
C #
PAN 2
Must Se lect
Crop 1 or Crol
a
Gal.
cu.Yd.
Report
p
Totals
in Gal.
O0v�
O00
60
Crop 1
�s'>�0,1
escihe
COTALS: JQ35"7 .1 f 1
knnual lbs/acre
:urrent Cumulative lbs/acre
'rior Years Cumulative lbs/acre
'ermitted C. P. L. R.***
'ermit PAN Limit Ist/2nd Crop
'I certify. under nenalty of law-
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 P N 2
3 ��{ Q�? 7.5dO� f 13 l 7 38 <U.�%f 0, 5i� < j6
1, a 6� a 5 , 0 l 51. i MIS Q , y 55 a 9�5 33 59 � ..
0,,46 f 1,90% q3 , -3 I qJ33 6,0741 a,�f g S a , 0 4 Y ►a4 3 3 /7, S 09 ,
, .51QS 1500 t' a 5 2lSC�
that Chic rint-nman+ woe , „a,,,....
Lune
pp -
It . _
p
Date
*
i
-- - r--r-------------- �1 �+__—_w+_ va ouyvi vi-aun in uccurtiance wiTn a system
lesigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
ignificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
0 6 - 0 ,3' *Application Method: S - Surface, IN - Injection, INC - Incorp oration
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1 0
***C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (7/2002)

ANN L METALS FIELD LOADING SUM1V Y FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: -ro t JV) 1J Total Dry Tons Applied (Annual): V
Permit #: Waa0,0 ,)1h _ UC06c; -7 1 S 1 Cation Exchange Capacity (non 503 only): amp r�f 7�DY�a
Operator: Q1 06- E M. so' -MS Owner: �mre,/ Coyly `J T-
Acres Used: 14. o Acres Permitted: 14, o Site #: b i Field #: J
Residual Analysis Data (Heavy Metals and Total Phosphorus use m % Solids use
Total
Phos-
-phorusEEMENEENEENE1
Annual Heavy Metal Field Loadings Calculated in lbs/acre :
Total
Phos-
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
7 rcordance with a system designed to assure that qualified personnel properly gathered and evaluated the
'kformation submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
DENR FORM MFLSF (7/2002
Signature of Land Applier Date

ANNUAL LAND APPLICATk, ,, FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: T� w� oar u
Owner: (_arv-y C.<rJV Operator: 9?,1,
Site #: O Field #: 6 a
Permit
Acres Utilized: L�
Annual Dry Tons Applied: 'a , 9
Cation Exchange Capacity (non 503): 100
Acres Permitted: q . g
14
ar
Specify
Totals
Per
Acre
o
Solids
As
Dec'-
mal
Dom'
Tons
Per
Acre
Residual
Sources
(Summarize)
NCd©5715 I
Cond.
Dry,
wet
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od**
Voli-
tila-
zation
Rate*
Miner-
ala-
zation
Rate
TKN
Ammo
ma-
Ni-
tro en
g
Ni-trate
Ni-
trogen
PAN 1
PAN 2
Must Select
Crop 1 or Crol
2
Gal.
-
cu.Yd.
..:
?
Report
Totals
in Gal.
rop 1
)Crop,
1 a
ooc�
313
6 a5
5.1 I
1 I
i
Dn • be'
I
yMoist
Vr
��
O
O
(1
SiAAult
SlAAC,
O 1 S
O, 5
00�1
5®
®
-
a a
F� i Mot
09 W
7 S 0,0
P5 6 a
• , 11
1
0-T1
Oq V�
D„ ° - 5
D t 5
r
�N
O
����.
v�r�C►
y 5c
. J
d
3d afo
�,
`7
C�
of
r .tu
COTALS:
annual lbs/acre
�urrent Cumulative lbs/acre
'rior Years Cumulative lbs/acre
'ermitted C. P. L. R. * * *
'ermit PAN Limit l st/2nd Crop
`I certify under penalty of law
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PA 2
6,04 CO,479 . b7 0 g 19, 37 1 ' .1i , 1-7
'p, 9 , gq6$ `, � � � �.Y,534 ff 6 a 1,956 7�{ $ , 'g6 �1, f d
<611919 0,,Q52 d, N S a 5. 1 9 ,943 0, 0 01
,rj 00
..... ....:.....:... .... . a 5�
that this document was re d d d'
Lime Applied
11
Date
0
> > p p e Lan et my erection or supervision in accordance with a system.
lesigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
ignificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
"d - r1l.a -06-03 *Application Method: S - Surface, IN - Injection INC - Incorporation
J �
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
Author Daryl D. Merritt DENR FORM FSF (712002)

AM L METALS FIELD LOADING SUMU W FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: j� .1 n � f-S N ;1 i O tk) t 'P Total Dry Tons Applied (Annual): Q .9
Permit #:00,(5O0 4 '1 � � p1V'GC�O�i 15 1 Cation Exchange Capacity (non 503 only): R . � mac / !p 0 @
Operator: . �,�, Y�l , Barns Owner: /- . V - r v Co -
Acres Used: l , �� Acres Permitted: 1� , Site #: A ` Field #: _
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent f:
posite
Date 'monsoon
11111
,
a ME
,.
Phos-
lphoms�E'NEENEEEENE
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
C=
i
' I
In-_------.---_-
Total
p
..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includi the possibility of fines and imprisonment for knowing violations"
A�,,//IV,AL a, -p (- p J DENR FORM MFLSF (7/2
Signature of Land AppiicP natty

- ___ r XICJ 11.J1.1VjXf-j111U-1L.1yl DIN J,(_EjjUUjlU1V 11URM
Facility Name: Jowly\ O Moss U JI Permit Number: (,��
WWTP Name: a � Maf, y. (;3 �� NPDES Number: NC-06r, 71,51
Monitoring Period: Fromn�a��r ad0a To
.r
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative nerfnrmed!
Class A: Alternative 1 ❑
Alternative 2 ❑ Alternative 3 ❑
Alternative 4❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic
Beta Ray ❑
Gamma Ray El
Pasteurization
Class B:
Alternative 1
Alternative 2 ❑
Alternative 3 ❑ .
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
time Stabilization. ❑ Air Drying❑ Composting ❑ jAerobic Digestion 0'
Anaerobic Digestion❑
If applicable to alte ativ erformed (Class A or Class B) complete the following monitoring data:
Parameter
Level in
Pathogen Density
um er o
Excee-
requency
Sample
ca
inlmu
Geo. Mean
aximu
Units
dences
of
Analysis
Type
Tech-
ni ue
x o e
power MPN per
5'POO
36j000
3 S,000
Cvlart�ea
P �T-
gram of total
solids or 2 x 10 to
Fecal Coliform
the 6th power
CFU er am of
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
3 MPN per 4
(in lieu of fecal
grams total solid
coliform)
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ❑ Option 2 ❑ Option 3 ❑ Option 4 Option 5 ❑
Option 6 ❑ Option 7 ❑ Option 8 ❑ 7 Option 9 '❑ Option 10
No vector attraction reduction options were performed ❑
/'ITTTT�TIY
w-ju-njL it i%,t, x tviv a 1 A 1 Emim'N t (please check the appropriate statement)
"I certify, under penalty.of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
U "IL certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Prep er N e and Title type or print)
03
Signature of Preparer Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable)
Date
M RF !7/gnnq)
DENR FOR

EARTH ENVIRONMENTAL SERVICES
75 Bison Lane
Murphy, NC 28906
Residence — [phone]
Robbinsville Lab — [phone]
Marshall Lab — [phone]
Shelby Lab — [phone]'
E-Mail — earthenvser@,webworkz.com\
December, 14, 2002
NC ID9474, #352
Mr. Robert Sams
Town of Mars Hill
P.O. Box 36R
Mars Hill, NC 28754
Dear Mr. Sams -
Following is a report of laboratory analyses. for digester sludge samples received 12/4/02.
Colony Counts
!! Samnle Tlatr. Glifnrtn TlencitiPc lrnlnniec/oraml o/ Tntal Cn1Na 1 ml 01 —1 A Al —1
1
11/25/02
31,000 Colonies/Gram
0.83%
TNTC
26
4
2
11/26/02
28,000 Colonies/Gram
0.82%
TNTC
23
1
3
11/27/02
33,000 Colonies/Gram
0.81%
TNTC
27
4
4
11/30/02
25,000 Colonies/Gram
0.83%
TNTC
20
6
5
1212/02
35,000 Colonies/Gram
0.84%
TNTC
29
3
6
12/3/02
25,000 Colonies/Gram
0.82%
TNTC
20
5
7
12/4/02
35,000 Colonies/Gram
0.84%
TNTC
29
3
Geometric mean for all seven samples: 30,000 colonies/gram. Thank you for your
business. If you have any question or need additional sample analyses performed, please
call_
Respectfully submitted,
Michael J. Ladd
Laboratory Director

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxvoen Level
0
Slope:
Intercept:
Correlation Coefficient:
iaow Cl
oke L A c
0'-A t4o
Itn ' e q
0
pin
milliliters
Yo Dry Solids
iegrees Celsius
iegrees Celsius
Oxygen Uptake Rate: mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Average Temperature: degrees Celsius
Temperature Correction Factor:
Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

` j . .. • ► I..v. • � / � .� f V 0 Lill% C/�w
Sect 4-
11ti��5Cr/l env/ /
Specific Oxygen Uptake Rate
SOUR
to
8
F
7
3
11
All w-v.� y`I
Date /43° 32 Sample Location Ae-t:G (21yedI-fC Temperature 1 G
Time l F :]Wo-I
1 2 3 4 5 6 7 3 9 10 11 12 13 14 15
Time (Min)
PV Begin "temp / a' DG Average Temp l Z �" End Temp /'� �� �
(o Oxygen Uptake Rate (OUR) (SM 2710B)
OUR mg Oz /L /hr = Begin Dissolved Oxvgen - Egg Dissolyed QUgen * 60
y O'q 7 Elapsed Time
OUR = _ mg /L - mg /I ` 60 = m O /Uhr
Minutes g z

Specific Oxygen Uptake Rate (SOUR)
01P
Au
�v
NY
oeq
1. SOUR mg 02 /hr/g = OUR mg 02/Vhr
Total Solids ` 1000 g/L
Note: enter total solids are as a decimal, see S.M. 2540 G
SOUR = mg 02 /Uhr = mg 02 /hr/g
% Total Solids *1000 g/L
2• SOUR m OUR mg O /Uhr
9 02 /hr/g --- F �'r
Total Solids g/L � it my ()ZA'r- 5
Note: S.M. 2540D, except use evaporating dish instead of fiber filter.
SOUR = M9 02 /Uhr = _ ® mac 02 /hr/a
g/L
Total Solids g/L = Tot 1000 lid�9 g/L
�bg x I,-UO CT ern( . Gu "eGhfl✓1�e�
Temperature Adjustment 8 1s azj
SOUR = @ 20 °C = SOUR @ Average Temp ° Adjustment, or correction factor
Mg 02 /hr/g mg 02 /hr/g `
0 20 °C ® °C
Note: See Adjush-nent formula and correetlot, factors oon the next page.

Specific Oxygen Uptake Rate
Temperature Adjustment y
SOUR is determined at the digesters ambient temperature and then adjusted as follows.
SOUR = 0 20 °C = SOUR @ Average Temp * Adjustment, or correction factor
Where A =1.05 above 200
=1.07 below 20'
Those factors are good between 100 C and 300
Simplified
SOUR = 0 20° C = SOUR ® Average Temp ` Correction
Correction = A (21- Ambient Tempe)
Temp °C Correction
10 1.97
11* 1.84
12 1.72
13 1.6Q
14 1.50
15 1.40
16 1.31
17 1.22
18 1.14
19 1.07
20 1.00
21 0.95
...2-2..... 0.90
23 0.86
24 0.82
25 0.78
26 0.75
27 0.71
28 0.68
29 0.64
30 0.61