WQ0004298_2001 Residuals Annual Report_20020219

ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit NumberCounty^ t_tA i c\ Year
Facility Name (as shown on A�?�t) �►a ��a nt r(11" r, 1 l l
Land Application Operator I!C0 ,cjE M S0,T\_ Phone
Land application of residuals as allowed by the above permit occurred during the past calendar year
_/ YES NO. If NO, SKIP PART I, AND PART 11 AND PROCEED TO THE CERTIFICATION. ALSO, IF RESIDUALS WERE
GENERATED BUT NOT LAND APPLIED, PLEASE ATTACH AN EXPLANATION ON HOW THE RESIDUALS WERE HANDLED.
Part I
• Total number of application fields in permit.
• Total number of fields land application occurred during the year.
• Total amount of dry tons applied during the year for all application sites. 406
• Total number of acres land application occurred during the year. t
Part II
Facilitywas compliant during calendar ear 200 cOA r p g y L with all conditions of the land application permit (indlndlr�g�b�t not limited to
items 1=12 below) issued by the Division of Water Quality c O,•
t YES / NO. IF NO, PLEASE PROVIDE A WRITTEN DESCRIPTION WHY THE FACILITY WAS NOT COMPLY t, E
DATES, AND EXPLAIN CORRECTIVE ACTION TAKEN.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit. -
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are
attached.
i. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
.:opies of certified laboratory -results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant
Loading Rates in Table 2 of 40 CFR part 503.13. (applicable to 40 CFR Part 503 regulated facilities)
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with.
(applicable to 40 CFR Part 503 regulated facilities)
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
IO.VeQetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance
with the crop management plan.
I LNo runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12.All buffer requirements as specified oi, the permit were maintained during each application of residuals.
"I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF NIY KNOWLEDGE AND BELIEF,
TRUE, ACCURATE, AND COIIPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBDIITTING FALSE
L\FORMATION, riCLUDING THE POSSIBILITY OF FLNES AND LNIPRISON.N ENT FOR I0VOWING NIOLATIONS"
Per
*ttee Name and title (type or print)
TE4 )an ( re
Ar,0,4 a "01 " ©off
a//3%av
Signature of Permittee Date
Signature of Preparer Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
rg
i. FEB 1 9 7002
Note: Preparer is defined in 40 CFR Part 503.9(r) I ± DEM FORM CF (1/2002)

INUAL DISTRIBUTION' AND MARKETING/ SURFACE DISPOSAL CER ATION AND SUMMARY FORM
- C M 11 f�JQr:�oo4a9�
FACILITY NAME -T6 U) d�_ C] M.
? PERMIT # W700 5 1 IS ( COUNTY _
FACILITY TYPE (please check one): Surface Disposal (complete Part A (Source(s) and "Residual IN" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A. B, and C)
OPERATOR in :ScA r -,S
PHONE Nat r'61 • 9 9 J
WAS THE FACILITY IN OPERATION DURING THE PAST CALENDAR YEAR? YES NO. If NO, skip Parts A, B, and C and certify form below.
Part A'
Part B'
Month
Sources(s)
(Include NPDES N If appllcable
Volume (dry tons)
Recipient
Information
Admendment/
Bulking Agent IN
Residual IN
Product OUT
Name(s)
Volume
dry tons
Intended uses)
January
February
March
k Q s -1 is
April
May
June
July
N C,o6 1151
August
September
5
October
tv r. (,c 5-1 (Cj'
November
December
Totals:
• Annual (dry tons)
Admendment s used: Bulkinq AQ3nt(s) used:
If more space Is required than given, please use the comment space provided below or attach additional sheel(s). Check box If additional sheel(s) are attached.
Comments:
Part C
Facility was compliant during calendar year 2001 with all conditions of the permit (including but not limited to items 1-3 below) Issued by the
Division of Water Quality Vf YES NO. If NO, please provide a written desription why the facility was not compliant.
1. All monitoring was performed In accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached.
2. All operations and maintenance requirements were compiled with or, In the case of a deviation, prior aulhorizatlon was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY KNOWLEDGE AND BELIEF, TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT
THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSS LITY OF FINES AND IMPRISONMENT FOR KNOWING VIOLATIONS."
SIGNA RE OF PERMITTEE DATE SIGNATURE OF PREPARER' ATE
(If different from Permlttee) 'Preparer Is defined In 40 CFR Part 503.9(r)
DEM FORM DMSD (1/2002)

Feb 12 02 11:48P
Earth Jironmental Svcs
j ai i i Environmental Services
Michael Ladd
75 Bison Lane
Murphy, NC 28906
Robbinsville Lab [phone]
Madison County Lab (828) 649-92S0
Residence (828) 837•9543
1-828 '-17-9543
Name and Address of FacTiiy_ Date: 2111102
Town of Mars Hill WWTP Swwlecolleew. RS
P.Q. BOX 368 Date and Time Sample ReoekeM 11/28/01 115$AM
Rtt: Robert S
Mall Hill, S DBIe and Time Sample CDIWCW.- 11127 & 28MI
amsms Date and Time Sample AnaNZW.
Land A013kallan Anahme. _ Ntie• All ., S MHT
P.1
_ ... _ _--•-
ESL
-....,�...�.�.� .,m.a a.mcaao171C(N�21Cn00:0=
_
Aer. Dig Sludge My 9ed Sludge Sol Sile #1 Sol $Re �
Repofl UMh
MrAhod
Unim
CIDr1Y
I
a. D
SM52108
m9A.OTAL
0 7 rneg1100q 0.5 meq/100g
SUSPENDED RMIOUE
CATION EXCHANGE CAPACITY
1.0
SM25400
11.0 mey/100g 7.6 mety100g
1
SM9222D
oaf looml
H
1"wO2
6 6 6.8 6.6 6.6
0-14
SIYIA500H+
u"Ift
AMMONIA NITROGEN
s3.8 M0 963
+ NO3.n
0-5
SM4500NH3F
mg(.
17A mg/1 31.5
1.0
SM5920B
m L
TOTAL KJEL12AHL NITROGEN
322 mqA 4293
TOTAL PHOSPHOROUS
201 mall
SCA
24.2 2A.3 71.7
SCA
ntglL
TOTAL RESIDUE
'l,
12430 mgH
2V/,
80%
83%
1.0
SM2540B
mgR
HUMIC MATTER
3.2%
4.49.
1.0
SM2130133- ..'
-wu
% "SE SAT URATION - K
4.1
62
1.0
SM2540C
mg/L
- H
5.9
5.9
- Mg
30.4
33.1
Ca
68.9
5a.1
PLANT AVAILABLE (surface)
1970.2
1492
10
SM2510B
NITROGEN. PPM DRY WT (aubaurf)
2445
1923.5
umhodem
0.1
SIN45DOCIG
m9/L
Trw1NPERATURE
sM2s50B
MIitED LIQUOR SUPSPENDED SOLIDS
aey c
1.0
ItUA
MAGNESIUM
70 mmA
5265
895.5
514
SCA
mall.
SODIUM
62.5 mo
493
< 13.3
< 12.2
SCA
m
CADMIUM
0.0027 mgn
6.73
< 1.33
c 1.22
SCA
SCA
mg/L
CHROMIUM
0.104 man
28.9
ii6.3
141
COPPER
2.569 mgA
402
30.4
30•4
SCA
mglL
malt
LEAD
SCA
0.346 M911
511.7
11.2
10.2
NICKEL
0.112 mgn
15.4
15A
24.6
SCA
mg/t
ZINC
3.667 mg1l
5.9
48.1
a"
SCA
mg/L
CALCIUM
103.5 mall
13270
1242
760
SCA
malt
POTASSIUM
129.1 mall
4516
679
192
SCA
ALUMINUM
84.6 mall
16335
OIL
AI7SENIC
SCA
SCA
jn
0.0YZ m l
< ads
< 1.33
c 721
SELENIUM
0.040 mgn
10.6
133
c 1.22
SCA
SCA
e+9lt
M DENUM
< 0.010 mall
< 6.08
< 133
c 1,22
a 0,0002 man
0.8g5
< 0.133
a 0.122
M.:...,vRY
SCA
rnglt
N.C_ LAhyar�.. IMM -2
- -- r+nanyzeo ay; M8
Lab SupeMscr_ Michael J. Ladd; EES-Robbinsville Certified Br ' f! /

Feb 12 02 11:43p
E17/22/1996 14:57
C
fly
Earth wironmental Svcs
78425164.,t
1-82E 37-8543 p.l
PAGE ©1
7
C- Plant Available Nitrogen (PAN) calculations and land applicSIIOA area requirem6its:--
EAAONSF TUEwTB M • DRY WE16KT
TIN � rt .3
MMONLA-N �.
NO3-NO2-N! h _5
{These valuescan be established for *6 apeeifie residual or dnfauU values Ca be used (or domestic wasrmgcr trcatta mg
itsiduaia. if equal values anc estabtiehtd� attach the dow�nreatatioe, ?Irt: default value$ a� es lollpurs):
Unwaboilized l'rittrety and Sccottdery Residuals d0%
AmbiQUY 04PSted Residuals 30
AnsocabkWIY Dil eatad Residuals 20%
Composted Residuals 10%
(I[ the dcfauk ualueb are used, AU04h an eagtaoadan as to wby the sPOcirIc cbosee default value is appropriate.)
lem
2. Rae (M,R] sshhoUld be utilized in tale ofOr wing calculadons a$ aUcadOn d�ira a ease note, the �1r�inetalizatxon
1-
PAN fur Surface Application
PAN ffi (p4iR) x ('tICN - NH j?I + ,S x (Nli3) + (NO3-M2,N)
PAN 7 1 • PPK DryWeight
PAN for Subsurface Application
.PAN IQdRX71K.M - NK3H + (NM3) + W03-19o2-M
PAN _ —' 3 0 - x ( �l�'3 4� ) + 31 + S
PAN = 1 t'2 , PPM Dry Weight
3. Total PAN to be Iand applied per year
'torsi dry tons of residual 10 be land applied per year;

Earth jironmental Svcs
70425164__
Feb 12 02 11:43p
07122/1996 14.57
U1
CRQG..(���e,e
1-828 7-9543 p-4
PAGE 81
' VrJ - y-.•.�J
S} A,: cry. Ut1
48 Sis e, T'S.
U, ," S J. p4 f, ` 1:2,4-3 umy/ �
C, Plane Available Mtragen (PAN) calculations and land APPlicatlon area requiren��i��;�-•
EAAMM�ONIA-N
01rT871']T1111�Ti $ M MYW �IGEiT - -
TN SI �R!
f . �..
N034NO2-? �.�
(7 -bese w4luesean be established 1'oc ft Vuilic Residual or defauk values can be used for daw4suc waslcwatar prt ment
rraidoals. if actuel valua ate estabti&W4 at=b ft dowmasWom The default values are as follows):
U MI=dA=oWWWy y i idn� 40%
ARmaobWly Dig*ted Reg"Us 30%
CoMpWW Rc0ft m 209:
10%
Ur de ddfauk values ere use, strach an axglanWoti as to why tip speoltuc closet► default valae is a ppmpc au.)
2. Coetpleas the fOUQWing cakWadons for the app&aLdon MEW ptiop®sed �Plcwe note, the MiMrWlizadom
Rate CUR] should be utilimd In the Wowing calcW;WODs as a.de cirntd): .-
PAN for Surface Appliea;jon
PAN _ [0a) s (MN - NR3)] + .S x MP 4 IN%-NOZ-N)
PAN [ a c' x ( 51 �M aL b
PAN 70 ppm O y Weight �ij —7 04 ; 3:7
PAN for Subsurface Application
PAN = IM)xx(ZKe1- NH3)] (MM3) + IN% -NOS
PAN=(
PAN
..... PpM Dry Weight
3. Total pAK to be land appWd pa year

t
ROT ;IEEE LABORATORY
_ _:_1) a79.642e
MADISflN COUNTY LABORATORY EARTH ENVIRONMENTAL SERVICES
(V6) 649-W60 MICHAR 1AD&OWWR
RESIDENCE
(828) 837-9U3 P.O, BOX 1) 77 75 BISON LANE
"SHALL, NC28763 MURPHY, NC 28906
Client
Sam
Address
t---' -- Bill To:
P.O. i BIN Re!eregnce
Phone
4ddil-oval Comments
9 (l 1 t
CHAIN -OP -CUSTODY RECORD
r
Analytical Request
n
EL:S Client Na.
EES Project Manager
OCR o-,.._..,_ -- -

ROI 'PILLE LABORATORY
B) 479-WB
MADISON COUNTY LABORATORY
(3t6) 649.9250
RESIDENCE mm
(sea) 837-9543
Address
Phone d - f.-. ? I r.-5'u
EARTH ENVIRONMENTAL SERVICES
MICHAEL L40D-OWNER
EO, BOX 1177 75 BISON LANE
MARS HALL, INC 28763 MURPHY, NC 28906
ReportTo_ ab c'f-+
Bill To:
P.O. # + Billing Werenca
CHAIN -OF -CUSTODY RECORD
Analytical Request
EES Client No,
EES Project Manage► -
EES Projec 1 No.
OCe nCxfrnctr- c+ine rnn
rr
tv
rf
3
M
c
0
3
a
N
7
N
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tYf
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un

ANNUAL RESIDUAL SAMPLING SUMMARY FORM.
Attach this form to the corresponding laboratory analysis.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number
Facility Name
NPDES #
at WA it
WWTP Name
i'
NCC)o5-7 l
oo
Residual Analysis nntn
Laboratory Inc.
2)
3)
Date Sampled or
Date Composited
�c I
Percent Solids
PAPAUrTCDC hy.../1--1—
p
_�_ti■.
r.®v Nslut nW YIy Walut1U
••
milli
i
s.
/
x _. � 10
(SIGNATURE OF PREPARER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the Information submitted. 1 am aware that there are
significant penalties for submitting false Information, Including the possibility of fines and imprisonment for knowing violations."
DEM FORM SSF (1/2W2)

ANNUAL LAND APPLICATIc.. _ "IELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
` � 1 j PLACE A "N/A" IN A BLANK OR � ��M f N1N% i PPLICABLE.
FACILITY NAME E O v,� n O M r.+ [`� % 41 Q. � � PERMIT # Oct® a q T9 j,`� .
OWNER f` .a.,rr,,i SITE # CATION EXCHANGE CAPACITY (non 503 regulated facilities only) `)6
OPERATOR Q .i' YYl . "t FIELD # O t ACRES PERMITTED 1 / ct � ACRES UTILIZED
TOTAL DRY TONS APPLIED (ANNUAL),. 3�G
DATE or
MONTH
Gallons /or Cubic Yards
� s ecify
Dry Tons
per Acre
Residual Source
% Solids
(Do not
use
Averages)
g )
Mineral-
zatlon Rate
Applicatior
Method*
See Code
If reporting by month keep
these daily records on site
Crop
Total
per Acre
nches
Rainfall pas(Dr
Site Conditions
, Moist, Wet)
d Qci
( Lt ,
c)
D l lied S\
)0 o`
v a
`Dry
PCicae
S- ,
/�5,(5 06
t b-7 1,
% 9
0 �+k �� s�
aCJ $a
30 o
Sk��
Q
,�
Fe cl�
VCTc�tAQr
/ 6) LJ
a13 �I
0,
Qba�4
�0%
5't
IJY'
�`'C Lw-
Lime Application
DATE LBS./AC.
0,,,i a 15 19
* Code
S - Surface
I - Incorporation
IN - Injection
LBSJACRE
TOTALS:
AN
P As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
Annual �� 60Q ��;1 �� . i
ISM (�� Io
0. � �f�
Oo5os
f� 1�
3
YItJ��
11a�
0,3
OI�GKI„b
0.1�39
Cumulative
,69G
6,qC j
1,T1$
213
4. 32
0,01W
Q'415
'waif
1"1433 171509
Permit Limit lbs./acre/year) - 1 st Crop,!/ 2nd Cro
Permitted Cumulative_ Pollutant Loading Rate
I, �j
U 5
I C do
�D 45 0
X �1.17. 76� ;� W-0Y-0 a
(SIGNATURE OF LAND APPLIER) DATE
"I certify; under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
DEM FORM FSF 1/2002`designed to assure that qualified personnel properly gathered and evaluated the Information submitted. I am aware that there are
( ----11t_—A--_.____t._e.e1.__t.t____._Jt________—__L

.
ANNUAL LAND APPLICAT . _ FIELD SUMMARY FORM -
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD,
PLACE A "N/A" IN A BLANK OR BOX WHEN fVOT APPLICABLE.
FACILITY NAME ( ©Off 0!� ri� c� r � IiA Al tv) Q � C o 0 5 �' ' 1
PERMIT # � an(-Q q c� SITE # . CATION EXCHANGE CAPACITY (non 503 tAgulated tacllities only) -7
OPERATOR _ i a�(YZc,_ FIELD # 'OD ACRES PERMITTED . Cb ACRES UTILIZED
TOTAL DRY TONS APPLIED (ANNUAL) C�
DATE or
MONTH
Galin /or Cubic Yards
Pecifiv
Dry Tons
per Acre
Residual Source
916 Solids
Po not
use
Avera es)
9
Nneral-
radon par
0%
AppOcaffor
Method*
Sea Code
•J&JrPace
If reporting by month keep
these daily records on -site
Crop
p
keSC,ke
Total
Pe Acre
p
a7
n as
rtainrau pall
0
site Conditions
r , Moist, Wet
Lime Application
DATE LBS./AC.
1CY..0115 3 N
• code
S - Surface
I - Incorporation
IN!. Injection
TOTALS:
LM./AGRt
PAN � P As
Cd
Cr
Cu
Pb Hg
Mo
Ni Se
Zn
Annual J ()C)t' ej-wl
�� D,557c0Yig0Qi1SS
Q.619
9 `a i
f,3 o,c;267
14
0,364 0.Q'fi3$
(�i357
Cumu
�0, I9
0,'a 5?
0, q4 5
, (
, 9 3 (). 0-701
Q 4 ?6
1,1 aJf ° i `7
R 7a 9
Permit Limit Ibs./acre ear) -1st Cro*/ 2nd Cro
r}, 5
1, 5
inn
I'1 �,
C:_ ,1
Permitted Cumulative Pollutant Loading Rate
X� yYnY� �� �iQ7�o
(SIGNATURE OF LAND APPLIER) DATE
"I cerllty, under penalty of law, that this document was prepared under my direction or supervision In accordance with a system
DEM FORM FSF(1/2002l.
designed to assure that qualified personnel properly gathered and evaluated the Information submitted. I am aware that there are
d

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
F--:l;ry Name Permit Number 1_) CA 0 o o x t 01
1 PName lows 0� Mct.t-s WM W1RJ7 1 NPDES# N0005- 71 5 I
Monitoring Period: From _/ / TO
Pathogen Reduction (40 CFR 50332) - Please indicate level achieved and alternative performed
Class A
Alternative 1
Alternative 4
_Composting _Heat Drying
Class B
Alternative 1
:�1a
ZOO 014V��
Alternative 3 _
I Alternative 6
i Thermophilic _Beta Ray _Gamma Ray _Pasteurization
I
d Alternative 3
If applicable to alternative I Indicate "Process to Significantly Reduce Pathogens":
I_
Aerobic Digestion _ Ai Drying _ __.___ �obic Digestion _ Composting _ Lime Stabilization
If applicable to alternative performed (Class A or Class B) complete the followink monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Frequency of
SampleAnalytical
Minimum
Geo. Mean
Maximum
Units
Exceedence
Analysis
Type
Te hnique
Fecal Coliform
2 x 106 MPN
per gram of total
pp /l
ls,00Q
yCatont
5 1 , 000
30,600
solids or 2 x 106
CFU per gram
of total solids
1000 MPN
per gram of
total solid
(dry weight)
Salmonella
3 MPN per 4
bacteria (in
grams total
lieu of fecal
solid (dry
coliform)
wei ht
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed �,
Option 1 Option 2 Option 3 Option 4 (i Option 5
Option 6 Option 7 Option 8 Option 9 Option 10
No vector attraction reduction options were performed
CEICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met " (Please note if you check this statement attach an explanation why you have not met one
or both of the requirements.)
,'This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
ISc,6e_n 1 it I S4XYr% ` - �Oh1 C 1�1 rr�3 V
?re, Name and Title (type or print)
1-
_nature of Preparer Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
DEM FOR.Vl RF (1/2002)

EARTH ENVIRONMENTAL SERVICES
75 Bison Lane
Murphy, NC 28906
Residence — [phone]
Robbinsville Lab — [phone]
Marshall Lab — [phone]
Shelby Lab — [phone]'
E-Mail — earthenvser(&webworkz.com\
NC ID#474, #352
Mr. Robert Sams
Town of Mars Hill
P.O. Box 368
Mars Hill, NC 28754
Dear Mr. Sams:
Following is a report of laboratory analyses for digester sludge samples received 11/28/01.
Colony Counts
Sample Date Coli#brm Densities (colonies/eram) % Total Solids 1 ml 0.1 ml 0.01 ml
1
11/19/01
24,000 Colonies/Gram
1.39%
TNTC
33
5
2
11/20/01
22,000 Colonies/Gram
1.36%
TNTC
30
3
3
11/21/01
20,000 Colonies/Gram
1.43%
TNTC
28
0
4
11/23/01
30,000 Colonies/Gram
1.48%
TNTC
45
2
5
11/26/01
18,000 Colonies/Gram
1.41%
TNTC
26
1
6
11/27/01
28,000 Colonies/Gram
1.41%
TNTC
40
1
7
11/28/01
25,000 Colonies/Gram
1.44%
TNTC
36
1
Geometric mean for all seven samples: 24,000 colonies/gram. Thank you for your
business. If you have any question or need additional sample analyses performed, please
call.
Respectfully submitted,
d), "-, J�- A4/
Michael J. Ladd
Laboratory Director

�11
I
ROBBINS' I !ABORATORY
(8,> a-6428
MADISON CUurviN LABORATORY
[phone]
RESIDENCE
[phone]
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Client l;W,� (�1L�5 Nil( !LC)i_&Tjd
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Address4-
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Phone
EARTH ENVIRON VTAL SERVICES
MICHAEL LADD-OWNER
P.O. BOX 1177 75 BISON LANE
MARSHALL, NC 28753 MURPHY, NC 28906
Report To:
Bill To:
P.O. # / Billing Reference
Project Name / No.
f 7
CHAIN -OF -CUSTODY RECORD
Analytical Request
EES Client No.
EES Project Manager
EES Project No.
'Requested Due Date-
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f
SarpRler Signature Date Sampled
ITEM SAMPLE DESCRIPTION TIME MATRIX EES. NO.
NO.
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NINE
SHIPMENT METHOD
COOLER NOS. BAILERS OUT/DATE, RETURNED i DATE
ITEM
NUMBER
TIME
RELINQUISHED BY AFFILIATION
ACCEPTED BY / AFFILIATION DATE
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1
!�dditional Comments
SEE REVERSE SIDE FOR INSTRUCTIONS

reb 12 02 11:38p
Earth Environmental Suns
1-82P-037-9543
p.3
SpBcific Oxygen Uptake Rate
Temperature Adjustment
SOUR is determined at the digester's ambient temperature and Ihen adjusted as follows.
SOUR = 0 20 OC = SOUR 0 Average Temp " Adjustment, or correction factor
Where A =1.05 above 200
=1.07 below 20°
These f�!clars are between Ino C and 300
Simplified
SOUR = ® 20° C A SOUR 0 Average Temp ° Correction
Correction - A t20- AmN*nt Tampa)
Tamp °C
Correction
10
1.97
11
1.B4-
i2
1.72.
13
1.60
14
1.50
15
1.40
16
1.31
17
1.22
18
1,1.4
19
1.07
20
1.00
21
U,95
22..
4.90
23
0.86
24
0.82
25
0.78
26
0.75
27
0.71
28
d.68
29
0.64
30
0.61

Feb 12 02 11:38p Earyh,_Fnvironmental Svcs
SPec is Oxygen Uptake Rate (SOUR)
1-821'�937-9543 p,2
7. SOUR mg 02 /hr/g — OUR Mg O /L/hr
% Total Solids • 1 OOD g/L
Note: enter total solids are as a decimal, see S_M, 2540 G
SOUR M Osi /Lft _
Mg OZ ft/
% Total Solids • low g/L
Lo
SOUR mg O6 /hr/g =OUI� m Oy/Uhr 0�c%X % C'_. Enc�`resr
Total Solids cyL
tl Note; SM. ?.saOD, except use evaporating dish inSgd of fiber f ker_f
SOUR := m 02 /L./hr =
mg 02 1hda .
Total Solids gA- - imt—sot (s mgf,
1000 mg/g
Temperature Adjustment
SOUR = ® 20 "C s SOUR 0 Averogc TemP 0 Adjustment, or correction factor
mg 02 /hdg --_—_,_mg 02 thr/g
0 20 °C oC
Notes: Seri Ailjlist�l2r�tiufl��Ula and cones..,:
�.uoii lectors ao�1 tho iiam page.