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Home My WebLink AboutWQ0004222_1998 Annual Report_19990211MA`f-11-1999 09:43 BAXTER PURCHASING 828 756 7388 P.02/02 I.V. Systems Division Uaxtar Hsa[txare Corporation • 744-70-415t P.O. Box 1390 Marbnr North Carolina 28752 F •P^ iSAr —71 Mi March 2, 1999 NC Divivion of Water Quality P.O. Box 25535 Raleigh, NC 27626-0535 Lear Mr. Kevin Barnett, Per our conversation on March 2, 1999, onclosad are our sour test data sheets for January and February 4f 1998. we only land applied these two marit;hs. Also enclosed are Pace data sheets for the 2nd, 3rd and 4th quarters. These sheets contain fecal, coliform data: 1/20/96 4, 50O, 000 OAAK SA"-".G FLe TAA)--rz�3 "A*t v 4/16/98 12,000 CA" A-(N-1-0�3 7/29/98 157,000 11/25/98 40,Q00_ Log Mean 134,184 �f you have any questions, please give Walker Hodges a call at $28-7//56-6618 or Me a call at 828-756--6527. Phil. Castro Environmental Ma,n.ager PC/cw enclosures ..NORTH COVE TOTAL P.02 I.V. Systems Division Baxter Healthcare Corporation 704-756-4151 P.O. Box 1390 Marion, North Carolina 28752 Baxter February 11, 1999 � ��VE® NC Division of Water Quality P.O. Box 29535 ar Raleigh, NC 27626-0535i,Ll'I'r SEGilaPJ ,Dear Mr. Kevin Barnett, Enclosed are three copies of our Annual Land Application Report for 1998. An alternate sludge disposal method (landfilling) was begun in March, 1998. we no longer land apply sludge. The report covers the land application that Baxter did in 1998 which occurred in January and February 1998. If you have any questions, please give me a call at 828-756-6527. 4 Phil Castro Environmental Manager PC/cw ,enclosures NORTH COVE ANNUAL LAND APPLICATION CERTIFICATION FORM Permit Number WQ000422 Z County McDowell Year 1998 Facility Name (as shown on permit) Baxter Healthcare Corporation Land Application Operator Walker Hodges Phone # 828-756-6618 Land application of residuals as allowed by the above permit occurred during the past calendar year X YES NO. If NO, skip Part I and Part H and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part I Total number of application fields in permit. 8 *Total number of fields land application occurred during the year. 2 *Total amount of dry tons applied during the.,year for all application sites. 36.86 *Total number of acres land application occurred during the year. 32.2 Part II Facility was compliant during calendar year 1995 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Environmental Management X YES NO. IF NO, PLEASE PROVIDE A WRITTEN DESCRIPTION WHY THE FACILITY WAS NOT CONIPLLANT, THE DATES, AND EXPLAIN CORRECTIVE ACTION TAKEN. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 . (applicable to 40 CFR Part 503 regulated facilities) 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with. (applicable to 40 CFR Part 503 regulated facilities) 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization yeas -received from the Division of Environmental Management. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY KNOWLEDGE AND BELIEF, TRUE, ACCURATE, AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINES AND IMPRISONMENT FOR KNOWING VIOLATIONS." Permittee Name and Title (type or print) Signature of Preparer Date (if different from Pemittee) SignatureofPermittee Date G' CG - / / - Signature of Land Applier Date__ .__ (if different from Permittee and Preparer) Note: Preparer is defined in 40 CFR Part 503.9(r) DEM FORM CF (10/94) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding laboratory analysis. Please note that your permit may contain additional parameters to be analyzed than those,.'required to be summarized on this form. Permit Number Facility Name NPDES # or WQ N (residual only facilities) WWTP Name WQ0004222 Baxter Healthcarg Corp NC0006564 Baxter Healthcare Corp Residual Analysis Data Date Sampled (grab) or Date Com osited 1/20/98 Percent Solids 2.1 PARAMETERS (ma/ka dry welahtl Laboratory 1 ) Pace Laboratories Inc 2) 3) s Arsenic Cadmium ND Chromium ND Copper 260 Lead ND Mercury Molybdenum Nickel ND Selenium Zinc 400 TKN Ammonia -Nitrogen 72,000 Nitrate -Nitrogen ND Total Phosphorus 7,900 X---- rr _— L�>�----------------- 1 _� (SIGNATURE O,F PREPARER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision. In accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and Imprisonment for knowing violations." DEM FORM SSF (10194) PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A."N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. FACILITY NAME Baxter Healthcare Corporation PERMIT # WQ0004222 OWNER Baxter Healthcare Corp SITE # lA CATION EXCHANGE CAPACITY (non 503 regulated facilities only) OPERATOR Walker Hodges FIELD # 1 ACRES PERMITTED 10.2 ACRES UTILIZED 10.2 TOTAL DRY TONS APPLIED (ANNUAL) 3.04 DATE or MONTH Gallons /or Cubic Yards (specify) Dry Tons Per Acre Residual Source % Solids Nola Oa fsol USe,Akerages Mineralization Rale Application Method (surface or Injection) I[ robortIt by inpnth keep the§e .flail records on st(e Crop Total per Acre P InchasFlelnlail po6i 24 Hrs. Site Conditions •(Dry, Moist, Wet) 1/98 24,000 2353 .20 Digester 2.03 SurfaCE Fescue 2 98 12,000 I i Lime Application DATE I LBS/ACRE TOTALS: PAN P As Cd Cr Cu Pb Hg Mo Ni Se Zn Annual E 2.18 0 (Cumulative 1 .04011 5.55 1.47 ..582 .112 7.405 Permit Limit lbs./acre/ ear - 1st Crop / 2nd Crop 50 Permitted Cumulative Pollutant Loading Rate (lbs./acre) 4.5 125 500 125 250 (SI ATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false Information, Including the possibility of fines and Imprisonment for knowing violations." DEM FORM FSF (2/95) • I - PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. FACILITY NAME Baxter Healthcare Corporation PERMIT # WQ0004??? OWNER Baxter Healthcare Corp SITE # lA CATION EXCHANGE CAPACITY (non 503 regulated facilities only) OPERATOR 'Baxter Heal thcare Corp FIELD, # 2 ACRES PERMITTED 22 _ ACRES UTILIZED 22 TOTAL DRY TONS APPLIED (ANNUAL) 33.82 DATE or MONTH Gallons /or Cubic Yards (specify) Dry Tons per Acre Residual Source % Solids Nole, oa h1o' U.Ai—VOAIDA Mineralization not. Application Method (surtace or Injection) II rcportmg by monih keep these' 3 , ;..dell records on ite Crop Total per Acre Inchasnalntall past 24 )Its. Site Conditions (Dry, Moist, Wet) 1/98 216,000 9818 .91 Di ester 7.21 SurfaCE Fescue 2/98 186,000 8455 .63 i i i mcmunt'-KINt.. ,,.",•'.�-.,b+ rdai'- `-..F .s�z'4sr�'a, 11� .: Lime Application DATE I LBSJACRE x , ii +` �h fr yt"e i rye *• t . !•+''ir1�, Permit Limit (lbs./acre ear) - 1st . • . • • `4, y g.,'.rE�,ta' . lj ., % .y, w •. r ��', ` .e r „ €' L d.. t a 4 ' `Irt ?�$+;•. . i.1. `Y,• �.-. �.., f t : F..Permitted Cumulative Pollutant Loading Rate (lbs./acre) 7o (SIGN TURE OF LAND APPLIER) DATE "i certify, under penalty of law, that this document was prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gathered and evaluated the Information submitted. I am aware that there are significant penalties for submitting false Information, Including the possibility of fines and Imprisonment for knowing violations." DEM FORM FSF (2/95) PATHOGEN REDUCTION AND VECTOR ATTRACTION CERTIFICATION Per conversation with Lou Polletta on February 23, 1996, attached are the Fecal Coliform data on Pathogen Reduction Class B }Cy,�,•�v�w alternative land Vector Attraction option 4. 1 did not receive a form for this data in my packet. SOUR TEST Pace mg/g/hr Baxter mg/g/hr 1 /20/98 0.504 1 /19/98 0.64 1 /20/98 0.66 1 /26/98 0.67 2/16/98 1.06 StJu�Lj; --- I IO L,. 0,5 SLUDGE DXSPOSAL REPORT ' 'QTE, HEALTHCARE CORPORATION NORTH COVE FACILITY PL,NIT NUMBER 0004222 - DDATE: SIGNATURE OF OPERA TOP SITE NO. IA-1 BANTER HEALTHCARE CORP. IA-2 BARTER HEALTHCARE CORP IA-3 BAX'TER HEALT-HCARE CORD 2-2 HENRY BROWN 2-5 HENRY BROWN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES (I) IMETHOD OF APPLICATION: INJE, C T ION SURFACE APPLICATION 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 72.9 (2) WEATEEER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP:HAY CORN PASTURE (5) LOADS HAULED (6,000 ALILOAD) _ l4 (6) APPLICATION SITE: SI'I E AND 7ILEB NO. --� a. SITE ANTD I'l—VILB NO. � � _� GALLONS d (JZ� #I S b. SITE AND YIELD NO. GALLONS y #IS c. SITE AND GALLONS #IS POUNDS DRY WEIGH SOT LDS X 8.34 X MILLION MG GALLONS SIGNATURE OF OPERATOR: SITENO. ®. IA-1 BAXTER HEALTHCARE CORP. IA-2 BAXTER HEALTHCARE CORP IA-3 BAXTER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES (1) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 72.9 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUD' CLOUD' (3) SOIL CONDITIONS: WET. DRY: (4) CROP: HAS' CORN PASTURE (5) LOADS MAULED (6,000 GALTOAD) -1 (6) APPLICATION SITE: SITE AND FILED No. ZA -2 a. SITE AND FIELD NO. — GALLONS �2vj' #' S c-2Y137 b. SITE AND FIELD T O. GALLONS #' S c. SITE AND GALLONS #' S POUNDS DRY X 3.34 X MILLION MG GALLONS DATE: SIG A TURE OF OPERATOR: 1A-1 BAXTER HEALTHCARE CORP. IA-2 BAXTER HEALTHCARE CORP IA-3 BAXTER HEALTHCARE CORP 2-? HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 72.9 (I) I-VIETHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR _ CLOUDY (3) SOIL CONDITIONS: WET (4) CROP: HAY V CORN DRY: PARTLY CLOUDY PASTURE (j) LOADS HAULED (6,000 GAI_.1LOAD) y - (6) APPLICATION SITE: SITE AND FILED NO. I A --2- a. SITE AND FIELD NO. f GALLONS 'I dD1 #'S b. SITE AND FIELD NO. GALLONS #'S �. SITE r,.ND FIEi:D GALLONS #' S POUNDS DRY WEIGHT SOLIDS X 8.34 X MILLION MG GALLONS. SLUDGE DISPOSAL. REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PE IT NUMBER WQ0004222 - - DAT SIGNATURE OF OPERATOP: . /J" (Y/ SITE NO. ACRES IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5. 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES 72.9 (1) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLODDY (3) SOIL CONDITIONS: WET DRY: Y (4) CROP: HAY / CORN PASTURE (5) LOADS HAULED (6,000 GAL\LOAD) G (6) APPLICATION SITE: SITE AND FILED NO. _ a. SITE AND FIELD NO. A GALLONS #' S b. SITE AND FIELD NO. GALLONS #'S e. SITE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS 3.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT B TER HEALTHCARECORPORATION NORTH COVE FACILITY - PERMIT - ER WQ0004222 DATE: �— f SIGNA7VRE OF OPERATOR: SITE NO. -ACRES 1A-1 BAXTER HEALTHCARE CORP. ' 22.0 IA-2 BARTER HEALTHCARE CORP 10.2 lA-3 BARTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5. 4-4 b DEAN CHAPMAN 6.7 _ 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES 72.9 (I) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY, _ (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN PASTURE j (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. l ' a. SITE AND FIELD NO. (jT'`� GALLONS �` d'd ! #' S �� r b. SITE AND FIELD NO. GALLONS pv #' S c. SITE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = PI'M SOLIDS X 8.3=1 X MILLION MG GALLONS Wyo SLUDGE DISPOSAL ;; f s. Ir,`•'t_ .i? REPORT ce. i :.; .`R BAXTER HEALTHCARE CORPORATION' NORTH COVE FACMITY PERMIT NUMBER WQ0004222 ty 1 ' { O SITE 1°PTO. 1A-1 BAXTERHEALTHCARE CORP. IA-2 BARTER HEALTHCARE CORP IA-3 BARTER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES (1) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR_ CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN (s) LOADS HAULED (s,000 GAL\LOAD) Y 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 72.9 PARTLY CLOUDY .PASTURE (6) APPLICATION SITE.: SITE AND PILED NO. 14 a. SITE AND FIELD NO. GALLONS M-6 #' S d 6 76 5 b. SITE AND FIELD NO. GALLONS #' S SITE r.ND = %:D 111 o. GALLONS #7 S POUNDS DRY WEIGHT = ?FM SOLEDS X S.')4 X MILLION MG GALLONS /� S �0a�7a Y��3Y�,i=-. DATA'. S'IGNAYURE OF OPERATOR: SITE NO. 1A-1 BAXTER HEALTHCARE CORP. IA-2 BAXTER HEALTHCARE CORP IA-3 BAXTER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES (1) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATEEER CONDIT16NS: CLEAR_ CLOUDY (3) SOIL, CONDITIONS: WET DRY: (4) CROP: HAY / CORN ACMES 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 72.9 PARTLY CLOUDY (5) LOADS HAULED (6,000 GAL�LOAD) 1 (6) APPLICATION SITE: SITE AND FILED NO. /T a. SITE AND FIELD NO. � GALLONS D2d #IS b. SITE AND FIELD NO. GALLONS #IS SITE AND FUEL!) v!) �0. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS � Yi, SITE NO. IA-1 BAXTER HEALTHCARE CORP. 1A-2 BAXTER HEALTHCARE CORP IA-3 BAXTER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES (I) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR _ CLOUDY W-6 .y 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 72.9 PARTLY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: RAY 1/ CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. GALLONS o� #, S b. SITE AND FIELD NO. GALLONS #' S e. SITE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = MOM SOLIDS Y MG GALLONS SLUDGE F3ISP➢SAI. REPORT BAXTER HEALTHCARE CORPORATIOlU NORTH COS FACII.ITY PEIT NUMBER WQ0004222 --- SIGNATURE OF OPERATOR: SITE NO. IA-1 BAXTER HEALTHCARE CORP. IA-2 BAXTER HEALTHCARE CORP 1A-3 BAXTER HEALTHCARE CORD 2-2 HENRY BROWN 2-5 HENRY BROWN 44 b DEAN CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH 1ce��iIL-111 \: ImmosM (1) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR_ CLOUDY ACRES 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 72.9 PARTLY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) Z (6) APPLICATION SITE: SITE AND PILED NO. I a. SITE AIND FIELD NO. / GALLONS 24 dJb #I S p4Co2 S-5-- b. SITE AND FIELD NO. GALLONS #IS c. SITE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 3.34 X 141ILLION MG GALLON �Ov2l �� jx °� � SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPoRA3'IOIV _ I@TORTFI COS FACIF.ITH PERMIT NUMBER WQOO-04222 DATE: SIGNATURE OF OPERATOR: - SITE NO. ACRES IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5. 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES 72.9 (1) METHOD OF APPLICATION: INJECTION / SURFACE APPLICATION / (2) WEATHER CONDITIONS: CLEAR P---' PARTLY CLOUDY CLOUDY (3) SOIL CONDITIONS: WET DRY: ✓ (4) CROP: RAY CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) y (6) APPLICATION SITE: SITE AND FILED NO. r" 1 a. SITE AND FIELD NO. _� GALLONS �y 6O #I S dCX5'y— b. SITE AND FIELD NO. GALLONS #' S c. SITE AND F11 D No. GALLONS #I S POUNDS DRY ` EI-C- E _ P I SOLIDS X 8.34 X MILLION MG GALLONS �- y� DATE: b'-- SIGNATURE OF OPERATOR: SITE NO. , IA-1 BAXTER HEALTHCARE CORP. IA-2 BAXTER HEALTHCARE CORP IA-3 BAXTER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES (I) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 72.9 ✓l_ (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY (3) SOH, CONDITIONS: WET DRY: (4) CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) 9 (6) APPLICATION SITE.: SITE AND FILED NO. a. SITE AND FIELD NO. �,/ry 'r GALLONS dick #1S b. - SITE AND FIELD NO. GALLONS ' #'S c. SITE AND F- T--D NO. O. GALLONS #7 S POUNDS DRY WEIGHT = PFNI SOLIDS ti 3.34 X MILLION MG GALLONS ��.,�Q SIGNATURE OF OPER,4TOR: SITE NO. ACRES 1A--1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES (1) I TTHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR _ CLOUDY 72.9 PARTLY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: RAY CORN PASTURE (5) LOADS MAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FMED NO. 2- a. SITE AND FIELD NO. --�' � -- �� GALLONS #' S b. SITE AND FIELD NO. GALLONS #' S c. SITE AND E=LD NO. GALLONS #'S POUNDS DRY WEIGHT = `?FM SOLIDS X 3.34 X MILLION MG GALLONS DATE: SIGNATURE OF OPERA TO SITE NO. 1A-1 BARTER HEALTHCARE CORP. IA-2 BARTER HEALTHCARE CORP IA-3 BARTER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES (I) TMETHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR_ CLOUDY !3CllE 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 72.9 PARTLY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY ✓ CORN PASTURE (5) LOADS HAULED (6,000 GAL�LOAD) ,r (6) APPLICATION SITE: SITE AND FILED NO. a. STTE AND FIELD NO. / GALLONS W S b. SITE AND FIELD NO. GALLONS #IS �. SITE AND GALLONS #IS POUNDS DRY WSOLIDS X 3.34 X MILLION MG GALLONS � � = - / 0 3 -KF� ��y SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT MJMBER W90004222 - - - DATE: fix /f SIGNATURE OF OPERATOR: ; SITE NO. AGES IA-1 BARTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES (I) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION 72.9 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY / CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD td0. '- GALLONS -3° )_T #' S %1� 3 /� b. SITE AND FIELD NO. GALLONS #' S c. SITE AND FUILD NO. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS r ;,r; *_, . n SLUDGE DISPOSAL REPORT BAXTER E T C CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ0004222 ------ ---- SIGNATURE OF OPERATO-7?: SITE NO. ACES IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES 72.9 (1) INM' TROD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR _ CLOUDY (3) SOIL CONDITIOiv S: WET (4) CROP: HAY CORV1 PARTLY CLOUDY DRY: PASTURE z� (s) LOADS HAULED (6,060 G_ LILOAD) i3 (6) APPLICATION SITE: SITE .-D FILED O. /14 a. SITE AND EIE LD 'I'10.2-- b. SITE AND FIELD NO. c. SITE AND I:+= =lu- GALLONS IPOC-) #' S GALLONS #'S GALLONS #' S POUNDS DRY WEIGHT = ap "1 SOLED S 8.3 ? X MILLION MG GALLONS r` SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY' PERMIT NUMBER WQ0004222 =- . -- DATE: SIGNATURE OF OPERATOR: 2 SITE NO. ACRES 1A-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES 72.9 (1) INEETHOD OF APPLICATION: INJECTION SURFACE APPLICATION � (2) WEATHER CONDITIONS: CLEAN _ CLOUDY (3) SOIL. CONDITIONS: WET PARTLY CLOUDY (4) CROP: RAY CORN PASTURE (5) LOADS HAULED (6,000 GAL\LOAD) 4- (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. GALLONS ,ZSGOU #' S b. SITE AND FLELD r 10. _ GALLONS #' S c. SITE AND GALLONS #' S POUNDS DRY W E ICE = _': _>i:` _a= ..`_ 3.34 X MILLION MG GALLONS 3 y%� SLUDGE DISPOSAL REPORT BAXTER HEA.LTHCARE CORPORATION NORTH COVE FAMITY PE .1 IT NUMBER WQ0004222 - SIGNATURE OF OPERA TOR: 1A-1 BA;K TER HEALTHCARE CORP. IA-2 BAXTER HEALTHCARE CORP IA-3 BAXTER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES ACRES 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 72.9 (1)IVIEETHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY (3) SOIL CONDITIONS: WET DRY: ./ (4) CROP: HAY ./` CORN PASTURE (5) LOADS HAULED (6,000 GAL\LOAD) (6) APPLICATION SITE: SI i E+ AND ~ILED a. SITE AND F ALD t�i �). GALLONS 3" O -)� #' S b. SITE IND A IEL:-D NO. GALLONS #IS � �. SITE AND i> O. GALLONS #' S POUNDS D eY " lGE,—1 _ 4 1�=M SOLMS X 8.34 X MILLION MG GALLONSAr- . 6 "LUD E DISPOSE REPORT BAXTER HEALTHCARE CORPORATION FORTH COVE FACMIT Y PERMIT ZUMBERWQ0004222 -. DATE: SIGNATURE OF OPERATOR: IA-1 BAX'>TER HEALTHCARE CORP. 22.0 1A-2 BAXTI'ER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES 72.9 (I) METHOD OF APPLICATION: INJECTION / SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY _ (3) SOIL CONDITIONS: WET DRY: / (4) CROP: HAY / CORN PASTURE (5) LOADS HAULED (6,000 GAL\LOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. ��- GALLONS #, s b. SITE AND F ELD NO. GALLONS � #IS c. SITE AND F =LD NO. GALLONS #' S POUNDS DRY WEIGHT = PP14 SOLIDS X o.34 X TvHLLION MG 3AX/7�3/ /mod DATE: SIGNATURE OF OPERATOR: SITE NO. IA-1 BAXTER HEALTHCARE CORP. IA-2 BAXTER HEALTHCARE CORP IA-3 BAXTER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES (I) TVIEETHOD OF APPLICATION: INJECTION SURFACE APPLICATION 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 72.9 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY _ (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN t PASTURE (5) LOADS HAULED (6,000 GALILOAD) J (6) APPLICATION SITE: SITE AND FILED NO. a. SITE .AND FIELD NO. �°✓ GALLONS 19-f iWX #' S b. SITE AND FIELD NO. GALLONS #'S c. SITE AN-1) FIELD NO. GALLONS #'S POUNDS DRY WEIGHT = PP'q SOLIDS 3.3-1 Xl MILLION MG GALLON 1998 BAXTER HEALTHCARE CORPORATION (PASTURE FESCUE) SITE 1A-1 TOTALS DATE GALLONS 1/29/98 24,000 2/2/98 JAN FEB 10.2 ACRES mg/I D.W.Ibs. 20,258 4,055 12,000 20,258 2,027 GALLONS % SOLIDS D.W. lbs. 24,000 2.03 4,055 12,000 2.03 2,027 36,000 6,082 3.04 TONS 1998 BAXTER HEALTHCARE CORPORATION (PASTURE FESCUE) SITE 1A-2 TOTALS 22 ACRES DATE GALLONS mg/I D.W.Ibs. 1/5/98 24,000 24,197 4,843 1/6/98 24,000 24,197 4,843 1/12/98 24,000 20,458 4,095 1/13/98 24,000 24,197 4,843 1/14/98 24,000 24,197 4,843 1/20/98 24,000 20,709 4,145 1/21/98 24,000 20,586 4,120 1/26/98 24,000 20,258 4,055 1/30/98 24,000 20,258 4,055 2/3/98 6,000 20,258 1,014 2/9/98 30,000 19,311 4,832 2/10/98 30,000 19,311 4,832 2/13/98 18,000 19,311 2,899 2/20/98 24,000 17,350 3,473 2/24/98 30,000 16,431 4,111 2/26/98 30,000 16,431 4,111 2/27/98 18,000 16,431 2,467 GALLONS % SOLIDS D.W. Ibs. JAN 216,000 2.21 39,842 FEB 186,000 1.79 27,793 402,000 67,635 Site 1A2 33.82 TONS Site 1A1 3.04 Total 36.86 PER REQUIREMENT OF 11.4 LIME ADDITION IN 1998 The following lime additions were made in March 10, 1998: Site 1A-2 .5T acre Site 2-5 AT acre Note: lime additions for 1999 will be based on soil sample analysis when received from the state lab Pace Analytical Services, Inc. Pare A nalytiral A Ravine, C Drive /-� Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 February 05, 1998 Mr. Phil Castro Baxter Healthcare Corporation P.O. Box 1390 Highway 221 North Marion, NC 28752 RE: PACE Project No. A80120.601 Client Reference: Sludge And Other Samples Dear Mr. Castro: Enclosed is the report of laboratory analyses for samples received January 20, 1998. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel free to contact us. Sincerely, Walter L. Miller Project Manager Enclosures Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravensctoft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 Baxter Healthcare Corporation February 05, 1998 P.O. Box 1390 PACE Project Number: A80120601 Highway 221 North Marion, NC 28752 Attn: Mr. Phil Castro Client Reference: Sludge And Other Samples NC Wastewater Lab Cert. #40 NC Drinkingwater Lab Cert. #37712 SC Lab Cert. #99030 PACE Sample Number: 93 0513867 93 0513875 Date Collected: 01/20/98 01/20/98 Date Received: 01/20/98 01/20/98 Client Sample ID: Kitchen Leachate Tap Digester Parameter Units PRL BA1 Sludge (1) INORGANIC ANALYSIS 8 RCRA METALS - LEACHATE Barium, Leachate mg/L 0.010 - 0.10 Cadmium, Leachate mg/L 0.010 - ND Chromium, Leachate mg/L 0.010 - ND Lead, Leachate mg/L 0.100 - ND Silver, Leachate mg/L 0.005 - 0.038 Arsenic, Leachate mg/L 0.0050 - ND Selenium, Leachate mg/L 0.0050 - ND Mercury, Leachate mg/L 0.0002 - ND. 0 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace Analytical Service's, Inc. Pace Analytical Services, Inc. 54 R shevilleille, Pace Analytical Asheville, C Drive AsNC 28801 Tel: 704-254-7176 Fax:704-252-4618 Mr. Phil Castro February 05, 1998 Page 2 PACE Project Number: A80120601 Client Reference: Sludge And Other Samples PACE Sample Number:. 93 0513859 Date Collected: 01/20/98 Date Received: 01/20/98 Client Sample ID: Digester Parameter Units PRL Sludge INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Cadmium mg/kg 24 ND Calcium mg/kg 2400 13000 Chloride mg/kg 480 6100 Chromium mg/kg 48 ND Copper mg/kg 23 260 .Corrosivity pH Units 0.1 6.8 Fecal Coliform in Solids by MPN_ MPN/g 1 4,300.000 Lead mg/kg 240 0 — Magnesium mg/kg 240 4500 Nickel mg/kg 120 ND Nitrogen, Ammonia mg/kg 100 1000 Nitrogen, Plant Available mg/kg 1.0 21800 Phosphorus, Total mg/kg 240 7900 Potassium mg/kg 2400 7900 Sodium mg/kg 240 8600 Solids, Percent Total % 0.01 C2.1 Sulfate mg/kg 480 4800 Zinc mg/kg 23 400 SOUR TEST Sour test mg/g/hr 0.01 0.50.4 Solids, Total Suspended mg/L 1.0 27000 Solids, Total Volatile Suspended mg/L 1.0 27000 (2)' NITROGEN, TOTAL Nitrogen, Kjeldahl mg/kg 12000 72000 Nitrogen, Nitrate plus Nitrite mg/kg 48 ND Nitrogen, Total mg/kg 12484 72000 1-4,3 X rpG Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 Mr. Phil Castro Page 3 Client Reference: Sludge And Other Samples These data have been reviewed and are approved for release. wam vsl� Walter L. Miller Operations Manager February 05, 1998 PACE Project Number: A80120601 Laboratory Certification IDs Laboratoryy Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 . This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 Without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 Mr. Phil Castro FOOTNOTES February 05, 1998 Page 4 for pages 1 through 3 PACE Project Number: A80120601 Client Reference: Sludge And Other Samples ND Not detected at or above the PRL. PRL PACE Reporting Limit (1) All analysis performed on Toxic Characteristic Leachate. (2) possible matrix interference. used the tss value of less than or equal to the tvss value. Laboratoryy Certification IN Laboratory Certification IN NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02960 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NG 28801 Tel: 704-254-7176 Fax:704-252-4618 DATE: 02/04/98 PAGE: 1 Baxter Healthcare Pace Project Number: 85987 P. 0. Box 1390 Client Project ID: A80120.601 Marion, NC 28752 Attn: Mr. Phil Castro Solid results are reported on a wet weight basis Pace Sample No: 85102986 Date Collected: 01/20/98 Matrix: Soil Client Sample ID: 93 051385.9/ DIGESTER SLUDGE Date Received: 01/21/98 Parameters Results Units PRL App. DF Analyzed Analyst CAS# Footnotes Organics, Prep Volatiles, TCLP Leach, Solid Method: EPA 8260 Prep Method: EPA 1311 Date Leached 0.00 0 1.00 01/27/98 DMEN GC -- Semi -VOA Pesticides, TCLP Leachate Method: EPA 8080 Prep Method: EPA 3510 Chlordane NO mg/L 0.006 0.20 01/30/98 SPIN 57-74-9 Endrin ND mg/L 0.004 0.20 01/30/98 SYIN 72-20-8 Heptachlor ND mg/L 0.0016 0.20 01/30/98 SYIN ' 76-44-8 Toxaphene ND mg/L 0.1 0.20 01/30/98 SYIN 8001-35-2 gamma-BHC (Lindane) ND mg/L 0.08 0.20 01/30/98 SYIN 58-89-9 Methoxychlor ND mg/L 2 0.20 01/30/98 SYIN 72-43-5 Decachlorobiphenyl (S) 100 % 1.00 01/30/98 SYIN 2051-24-3 Tetrachloro-meta-xyiene (S) 64 % 1.00 01/30/98 SYIN '877-09-8 Date Extracted 01/28/98 Herbicides, TCLP Leachate Method: EPA 8150 Prep Method: EPA 8150 _ 2,4-D ND mg/L 0.02 1.00 01/30/98 SYIN 94-75-7 2,4,5-TP(Silvex) NO mg/L 0.0075 1.00 01/30/98 SYIN 93-72-1 Dichlorophenyl Acetic Acid (S) 49 % 1.00 01/30/98 SYIN 19719-28-9 Date Extracted 01/28/98 GC/MS -- VOA Volatiles, TCLP Leach, Solid Method: EPA 8260 Prep Method: EPA 8260 Vinyl Chloride ND mg/L 0.1 10.0 01/28/98 TSHA 75-01-4 1,1-Dichloroethene ND mg/L 0.05 10.0 01/28/98 TSHA 75-35-4 Laboratory Certification IDs Laboratoryt Certification IDs TN Drinking Water 02980 FL Environmental 96317 without NC Wastewater 40 REPORT OF LABORATORY ANALYSIS NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 DATE: 02/04/98 PAGE: 2 Pace Project Number: 85987 Client Project ID: A80120.601 Pace Sample No: 85102986 Date Collected: 01/20/98 Matrix: Soil Client Sample ID: 93 051385.9/ DIGESTER SLUDGE Date Received: 01/21/98 Parameters Results Units PRL App. DF Analyzed Analyst CAS# Footnotes Chloroform ND mg/L 0.05 10.0 01/28/98 TSHA 67-66-3 1,2-Dichloroethane ND mg/L 0.05 10.0 01/28/98 TSHA 107-06-2 2-Butanone ND mg/L 10 10.0 01/28/98 TSHA 78-93-3 Carbon Tetrachloride ND mg/L 0.05 10.0 01/28/98 TSHA 56-23-5 Trichloroethene ND mg/L 0.05 10.0 01/28/98 TSHA 79-01-6 Benzene ND mg/L 0.05 10.0 01/28/98 TSHA 71-43-2 Tetrachloroethene ND mg/L 0.05 .10.0 01/28/98 TSHA 127-18-4 Chiorobenzene ND mg/L 0.05 10.0 01/28/98 TSHA 108-90-7 Toluene-d8 (S) 98 % 1.00 01/28/98 TSHA 2037-26-5 4-Bromofluorobenzene (S) 104 % 1.00 01/28/98 TSHA 460-00-4 Dibromofluoromethane (S) 108 % 1.00 01/28/98 TSHA 1868-53-7 GC/MS -- Semi -VOA Semivolatile, TCLP, Solid Method: EPA-8270 Prep Method: EPA 3510 1,4-Dichlorobenzene ND mg/L 0.020 0.50 01/28/98 VHEB 106-46-7 2-M'ethylphenol ND mg/L 0.020 0.50 01/28/98 VHEB 95-48-7 3-Methylphenol ND mg/L 0.020 0.50 01/28/98 VHEB 108-39-4 4-Methylphenol ND mg/L 0.020 0.50 01/28/98 VHEB 106-44-5 Nitrobenzene ND mg/L 0.020 0.50 01/28/98 VHEB 98-95-3 Nexachlorobutadiene ND mg/L 0.020 0.50 01/28/98 VHEB 87-68-3 ;2,4,6-Trichlorophenol ND mg/L 0.020 0.50 01/28/98 VHEB 88-06-2 2,4,5-Trichlorophenol ND mg/L 0.050 0.50 01/28/98 VHEB 95-95-4 2,4-Dinitrotoluene ND mg/L 0.020 0.50 01/28/98 VHEB 121-14-2 Hexachlorobenzene ND mg/L 0.020 0.50 01/28/98 VHEB 118-74-1 PentachLorophenol ND mg/L 0.050 0.50 01/28/98 VHEB 87-86-5 Pyridine ND mg/L 0.020 0.50 01/28/98 VHEB 110-86-1 Hexachloroethane ND mg/L 0.020 0.50 01/28/98 VHEB 67-72-1 Nitrobenzene-d5 (S) 76 % 1.00 01/28/98 VHEB 4165-60-0 2-Fluorobiphenyl (S) 90 % 1.00 01/28/98 VHEB 321-60-8 Terphenyl-d14 (S) 106 % 1.00 01/28/98 VHEB 1718-51-0 Phenol-d6 (S) 22 % 1.00 01/28/98 VHEB 13127-88-3 2-Fluorophenol (S) 43 % 1.00 01/28/98 VHEB 367-12-4 2,4,6-TribromophenoL (S) 40 % 1.00 01/28/98 VHEB 118-79-6 Date Extracted 01/28/98 Laboratory Certification IDs Laboratoryy Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 DATE: 02/04/98 PAGE: 3 Pace Project Number: 85987 Client Project ID: A80120.601 PARAMETER FOOTNOTES ND Not Detected NC Not Calculable PRL Pace Reporting Limit (S) Surrogate App. DF Applied Dilution Factor Laboratoryy Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 Baxter Healthcare P. 0. Box 1390 Marion, NC 28752 Attn: Mr. Phil Castro QC Batch ID: 1266 Analysis Method: EPA 8080 Associated Pace Samples: 85102986 METHOD BLANK: 85110039 Associated Pace Samples: 85102986 QUALITY CONTROL DATA Pace Project Number: 85987 Client Project ID: A80120.601 QC Batch Method: EPA 3510 Analysis Description: Pesticides, TCLP Leachate Method Blank Parameter Units Result PRL Footnotes Chlordane mg/L NO 0.003 Endrin mg/L NO 0.002 Heptachlor mg/L NO 0.0008 Toxaphene mg/L NV 0.05 gamma-BHC (Lindane) mg/.L ND 0.04 "-`tioxychlor mg/L ND 1 ichlorobiphenyl (S) % 164 .--.-achloro-meta-xylene (S) % 84 DATE: 02/04/98 PAGE: 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 8578601 8578619 Matrix Matrix Spike Spike Spike Spike Sp. Dup. Dup Parameter Units 8554420 Conc. Result % Rec' Result % Rec RPD Footnotes Endrin mg/L 0 0.00 0.004450 89.0 0.004500 90.0 1 Heptachlor mg/L 0 0.00 0.004500 90.0 0.004800 96.0 6 gamma-BHC (Lindane) mg/L 0 0.00 0.004150 83.0 0.004350 87.0 5 Methoxychlor mg/L 0 0.00 0.004650 93.0 0.004400 88.0 6, Decachlorobiphenyl (S) 117 101 Tetrachloro-meta-xylene (S) 76. 62 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consenlof Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 QUALITY CONTROL DATA DATE: 02/04/98 PAGE: 5 Pace Project Number: 85987 Client Project ID: A80120.601 LABORATORY CONTROL SAMPLE: 8567331 Spike LCS Spike Parameter Units Conc. Result % Rec Footnotes Endrin mg/L 0.00 0.004700 94.0 Heptachlor mg/L 0.00 0.004650 93.0 gamma-BHC.(Lindane) mg/L 0.00 0.004250 85.0 Methoxychlor mg/L 0.00 0.005200 104 Decachlorobiphenyl (S) 127 Tetrachloro-meta-xylene (S) 80 LABORATORY CONTROL SAMPLE: 8575318 Parameter Endrin. Heptachlor gamma-BHC (Lindane) Methoxychlor Decachlorobiphenyl (S) Tetrachloro=meta-xylene (S) Spike LCS Units Conc. Result mg/L 0.00 0.004750 mg/L 0.00 0.003700 mg/L 0.00 0.003700 mg/L 0.00 0.004550 LABORATORY CONTROL SAMPLE: 85110047 imeter Units Endrin mg/L Heptachlor mg/L gamma-BHC (Lindane) mg/L Methoxychlor mg/L Decachlorobiphenyl (S) Tetrachloro-meta-xylene (S) Spike LCS Conc. Result 0.00 0.0005250 0.00 0.0004950 0.00 0.0004600 0.00 0.0005950 Spike Rec 95.0 74.0 74.0 91.0 133 83 Spike Rec 105 99.0 92.6 119 169 77 Footnotes Footnotes Laboratory Certification IDs Laboratoryy Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace. Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical A RavensDrive Asheville, INCNC 28801 Tel: 704-254-7176 Fax:704-252-4618 Baxter Healthcare P. 0. Box 1390 Marion, NC 28752 Attn: Mr. Phil Castro QC Batch ID: 1267 Analysis Method: EPA 8150 Associated Pace Samples: 85102986 METHOD BLANK: 85115160 Associated Pace Samples: 85102986 Parameter Units ------- ------------------------------- 2,4-D mg/L 2,4,5-TP(Silvex) mg/L Dichlorophenyl Acetic Acid (S) QUALITY CONTROL DATA Pace Project Number: 85987 Client Project ID: A80120.601 QC Batch Method: EPA 8150 Analysis Description: Herbicides, TCLP Leachate Method Blank Result PRL Footnotes ND 20 ND 7.5 81 DATE: 02/04/98 PAGE: 6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 8580128 8580136 Matrix Matrix Spike Spike Spike Spike Sp. Dup. Dup _.•-imeter Units 8554420 Conc. Result % Rec Result % Rec RPD Footnotes 2,4-D ug/L 0 100 88.00 88.0 84.00 84.0 5 2,4,5-TP(Silvex) ug/L 0 10 8.200 82.0 7.900 79.0 4 Dichlorophenyl Acetic Acid (S) 113 114 LABORATORY CONTROL SAMPLE: 8567364 Parameter Units 2,4-D ug/L 2,4,5-TP(Silvex) ug/L Dichlorophenyl Acetic Acid (S) Spike LCS Conc. Result 100 102.0 10 7.900 Spike Rec Footnotes 102 79.0 134 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. //�� Pace Analytical Services, Inc. Pace Analytical Asheville, N oft Drive Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 QUALITY CONTROL DATA DATE: 02/04/98 PAGE: 7 Pace Project Number: 85987 Client Project ID: A80120.601 LABORATORY CONTROL SAMPLE: 8575250 Spike LCS Spike Parameter Units Cone. ------- Result ---------- % Rec Footnotes --------------- ------------------------------ 2,4-D ---------- ug/L 160 128.0 128 2,4,5-TP(Silvex) ug/L 10 8.500 85.0 Dichlorophenyl Acetic Acid (S) 124 LABORATORY CONTROL SAMPLE: 85100980 Spike LCS Spike Parameter Units Cone. Result % Rec Footnotes ------------------------------ 2,4-D ---------- ug/L ------- 100 ---------- 96.00 ----- ---------- 96.0 2,4,5-TP(Silvex) ug/L 10 8.900 89.0 Dichlorophenyl Acetic Acid (S) 56 TORY CONTROL SAMPLE: ,Spike LCS Spike Parameter Units Cone. Result ---------- % Rec Footnotes --------------- ------------------------------ ---------- 2,4-D ug/L ------- 100 82.60 82.6 2,4,5-TP(Silvex) ug/L 10 7.070 70.7 Dichlorophenyl Acetic Acid (S) 81 Laboratoryy Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 1 Baxter Healthcare P. 0. Box 1390 Marion, NC 28752 Attn: Mr. Phil Castro QC Batch ID: 1864 Analysis Method: EPA 8260 Associated Pace Samples: 85102986 METHOD BLANK: 85113355 Associated Pace Samples: 85102986 QUALITY CONTROL DATA Pace Project Number: 85987 Client Project ID: A80120.601 QC Batch Method: EPA 8260 Analysis Description: Volatiles, TCLP'Leach, Solid Method Blank Parameter Units Result PRL Footnotes Vinyl Chloride mg/L NO 0.01 1,1-Di.chloroethene mg/L NO 0.005 Chloroform mg/L NO 0.005 1,2-Dichloroethane mg/L NO 0.005 ,2-Butanone mg/L NO 1 r--5on Tetrachloride mg/L NO 0.005 :hloroethene mg/L NO 0.005 .:ene mg/L NO 0.005 Tetrachloroethene mg/L. NO 0.005 Chtorobenzene mg/L NO 0.005 Toluene-d8 (S) % 102 4-Bromofluorobenzene (S) % 104 Dibromofluoromethane (S) % 110 DATE: 02/04/98 PAGE: 8 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 8596215 8596223 Matrix Matrix Spike Spike.. Spike Spike Sp. Dup. Dup Parameter Units 8588915 Conc. Result % Rec Result % Rec RPD Footnotes 1,1-Dichloroethene mg/L 0 0.50 0.5200 104 0.5300 106 2 Trichloroethene mg/L 0 0.50 0.4200 84.0 0.4790 95.8 13 Benzene mg/L 0 0.50 0.5400 108 0.5420 108 0 Chlorobenzene mg/L 0 0.50 0.4800 96.0 0.4810 96.2 0 Toluene-d8 (S) 102 102 4-Bromofluorobenzene (S) 98 100 Laboratory Certification IDs Laboratoryy Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 QUALITY CONTROL DATA DATE: 02/04/98 PAGE: 9 Pace Project Number: 85987 Client Project ID: A80120.601 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 8596215 8596223 Matrix Matrix Spike Spike Spike Spike Sp. Dup. Dup Parameter Units 8588915 Conc. Result % Rec Result % Rec RPD Footnotes --------- --------------------------------------------------------- ----- -------- ----- --------------- Dibromofluoromethane (S) 104 95 LABORATORY CONTROL SAMPLE: 8596207 Spike LCS Spike Parameter Units Conc. Result % Rec Footnotes 1,1-Dichloroethene mg/L 0.50 0.4900 98.0 Trichloroethene mg/L 0.50 0.4600 92.0 Benzene mg/L 0.50 0.5100 102 Chlorobenzene mg/L 0.50 0.4525 90.5 LABORATORY CONTROL SAMPLE: 8598971 Spike LCS Spike Parameter Units Conc. Result % Rec Footnotes 1,1-Dichloroethene mg/L 0.05 0.04431 88.6 Trichloroethene mg/L 0.05 0.04500 90.0 Benzene mg/L 0.05 0.04586 91.7 Chlorobenzene mg/L 0.05 0.04723 94.5 I)RATORY CONTROL SAMPLE: 85103950 Spike LCS Spike Parameter Units Conc. Result % Rec Footnotes 1,1-Dichtoroethene mg/L 0.50 0.4444 88.9 Trichloroethene mg/L 0.50 0.3866 77.3 Benzene mg/L 0.50 0.4838 96.8 Chlorobenzene mg/L 0.50 0.4594 91.9 LABORATORY CONTROL SAMPLE: 85113363 S ike LCS S ike Parameter Units 1,1-Dichloroethene mg/L Trichloroethene mg/L Benzene mg/L Chlorobenzene mg/L P Conc. Result 0.50 0.5000 0.50 0.4960 0_50 0.5110 0.50 0.5100 p Rec Footnotes 100 99.2 102 102 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 Baxter Healthcare P. 0. Box 1390 Marion, NC 28752 Attn: Mr. Phil Castro QC Batch ID: 1868 Analysis Method: EPA 8270 Associated Pace Samples: METHOD BLANK: 85109874 Associated Pace Samples: Parameter 1,4-Dichlorobenzene 2-Methylphenol 3-Methylphenol 4-Methylphenol Nitrobenzene ..--Lachlorobutadiene �,6-Trichlorophenol ,,4,5-Trichlorophenol 2,4-Dinitrotoluene Hexachlorobenzene Pentachlorophenol Pyridine Nexachloroethane Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 85102986 85102986 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % QUALITY CONTROL DATA Pace Project Number: 85987 Client Project ID: A80120.601 QC Batch Method: EPA 3510 Analysis Description: Semivolatile, TCLP, Solid Method Blank Result ND ND NO ND ND ND NO ND ND ND ND ND NO 58 66 83 12 29 40 PRL Footnotes 10 10 10 10 10 10 10 25 10 10 25 10 10 DATE: 02/04/98 PAGE: 10 Laboratory Certification IDs Laboratoryy Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317. SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 QUALITY CONTROL DATA DATE: 02/04/98 PAGE: 11 Pace Project Number: 85987 Client Project ID: A80120.601 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 8599094 8599102 Matrix Matrix Spike Spike Spike Spike Sp. Dup. Dup Parameter Units ---------- 8582595 Conc. Result % Rec Result % Rec RPD Footnotes ------------------------------ 1,4-Dichlorobenzene ug/L ---------- 0 ------- 200 ---------- 68.00 ----- 34.0 ---------- 96.00 ----- 48.0 --------------- 34 2-Methylphenol ug/L 0 400 102.0 25.5 112.0 28.0 9 4-Methylphenol ug/L 104.0 400 174.0 17.5 172.0 17.0 3 1,1 Nitrobenzene ug/L 0 200 102.0 51.0 140.0 70.0 31 Hexachlorobutadiene ug/L 0 200 74.00 37.0 104.0 52.0 34 2,4,6-Trichlorophenol ug/L 0 400 312.0 78.0 326..0 81.5 4 2,4,5-Trichlorophenol ug/L 0 400 132.0 33.0 124.0 31.0 6 2,4-Dinitrotoluene ug/L 0 200 188.0 94.0 172.0 86.0 9 Hexachlorobenzene ug/L 0 200 128.0 64.0 120.0 60.0 6 Pentachlorophenol ug/L 0 400 376.0 94.0 340.0 85.0 10 Hexachloroethane ug/L 0 200 62.00 31.0 96.00 48.0 43 Nitrobenzene-d5 (S) 55 71 2-FluorobiphenyL (S) 62 66 TerphenyL-d14 (S) 75 67 Phenol-d6 (S) 26 32 2-FLuorophenoL (S) .22 33 2,4,6-Tribromophenol (S) 74 65 LABORATORY CONTROL SAMPLE: 8596652 Spike LCS Spike D--meter Units ---------- Conc. ------- Result '--------- % Rec Footnotes -------------------------- Dichlorobenzene ug/L 200 136.0 --------------- 68.0 2-MethylphenoL ug/L 400 106.0 26.5 4-Methylphenol ug/L 400 176.0 44.0 1 Nitrobenzene ug/L 200 180.0 90.0 Hexachlorobutadiene ug/L 200 144.0 72.0 2,4,6-Trichlorophenol ug/L 400 1580 395 2,4,5-Trichlorophenol ug/L 400 150.0 37.5 2,4-Dinitrotoluene ug/L 200 200.0 100 Hexachlorobenzene ug/L 200 168.0 84.0 Pentachlorophenol ug/L 400 560.0 140 Hexachloroethane ug/L 200 140.0 70.0 LABORATORY CONTROL SAMPLE: 85109882 Spike LCS Spike Parameter Units Conc. Result % Rec Footnotes --------------------------------------------------------- --------------- 1,4-Dichlorobenzene ug/L 100 59.00 59.0 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 QUALITY CONTROL DATA DATE: 02/04/98 PAGE: 12 Pace Project Number: 85987 Client Project ID: A80120.601 LABORATORY CONTROL SAMPLE: 85109882 Spike LCS Spike Parameter Units Conc. Result % Rec Footnotes ------------------------------ 2-MethylphenoL ---------- ug/L ------- 200 ---------- 49.00 ----- ---------- 24.5 4-Methylphenot ug/L 200 84.00 42.0 1 Nitrobenzene ug/L 100 70.00 70.0 Hexachlorobutadiene ug/L 100 63.00 63.0 2,4,6-TrichlorophenoL• ug/L 200 152.0 76.0 2,4,5-TrichlorophenoL ug/L 200 70.00 35.0 2,4-Dinitrotoluene ug/L 100 88.00 88.0 Hexachlorobenzene ug/L 100 75:00 75.0 . Pentachlorophenol ug/L 200 221.0 ill Hexachloroethane ug/L 100 59.00 59.0 Laboratory Certification IDs Laboratory Certification IDs. NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL Environmental 96317 SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 DATE: 02/04/98 PAGE: 13 Pace Project Number: 85987 Client Project ID: A80120.601 QUALITY CONTROL DATA PARAMETER FOOTNOTES Consistent with EPA guidelines unrounded concentrations are displayed and have been used to calculate % Rec and RPD values. ND Not Detected NC Not Calculable PRL Pace Reporting Limit RPD Relative Percent Difference (S) Surrogate Ell Due to co -elution, the value in 4-Methylphenol represents the total value for both 4-Methylphenol and 3-Methylphenol.. 4 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 FL Environmental 96317 SC Environmental 99030 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. CHAIN -OF -CUSTODY RECORD Analytical Request f 0 / / rl f'7 Turn around Time - 7 / , v Client , .:;+ r r Report To: • t. U' S - �' 4 ❑ 24 Hours Pace Client No. / ' Address v %' `� fU Bill To: ❑ 48 Hours ❑ 3-5 Days ❑ 1 Week 2 Weeks El Normal 14-Days Pace Project Manager t P.O. # / Billing Reference Pace Project No. C' Phone Project Name / No. [ v.i? :';` ;r, "Requested Due Date: 5ampiea by (I -KIN 1): Sampler Signature j Date Sampled ITEM NO. SAMPLE DESCRIPTION o 3 ; 4 5 6 7 8 Additional Comments �3 oU'C W PRESERVATIVES ANALYSES REQUEST _ z tiIvEL z _ 0 _ °> z ca \' ' .j �� rt TIME MATRIX PACE • - z ; l`� REMARKS �-p ', X �\ 7 r -a 7 715 F a t �' w e _ u .i r '"% i:. -� ! / . U � L�,�✓t--•' r`� !� se -tew-•�-t,. - U k {d x l .:J t✓ ,..--SAMPLE CONDITION °C Received on Ice: YJ N Sealed Cooler: Y / N Samples Intact: Y SEE REVERSE SIDE FOR INSTRUCTIONS , _ __-_-- _ .-- -- - _-- -- __-- - _ ----------- -- _ -- - instructions for completing Chain of C_ust®dy (ZCC)-___-_. - - - - --1. -Complete all Client ;Inf6ematr®n -at top of sheet: - ramie,-adde ss, -"phone;-contact (person -to whom-- _. be sent`-and'contact_can_be. made if-_questions.arise),,_1 iIling-information-if different from...- ,,, client, PU#, Projeet Name and/or Project Number as it_will.,appear, on the report. ,Z? Pace -Client No., Project Mana_ ger and -Project -No. will bet-com' pleted by Pace.____ ,.3', A separate COC rrrust,be;filied out for eacli-day of sample collection. 4:• Sampler should print their name in the space ;provided, and;sign their name followed by the date of -the, sampling event. - stir = =� 5. Complete Sample Description as itwill appear on the laboratory report; include time of sampling, - - - - sample matrix,'no.-of'coritainers and container types. - - - -- 6. Analysis Requested-—Completeanalysis-on-the lines -provided -and -place -a -check in the column for the samples- requiring the _anal ysis4 It tnay be necessary_ to_ use the space provided for additional comments or include attachments for extended lists''of parameters. 7. Indicatemethod of shipment used for return of samples and date sent. , �- _ 8._ Submission_ of samples to laboratory: indicate Item Number of those -samples being transferred, sign relinquished by, and' include your affiliation. *'IMPORTANT- NOTE: -- 1 1 , -,' Standard Turnaround Time. is 2 weeps: -if this does not satisfy your requirements, arrangements - - - -must be made -prior -to samples -being submitted to -the laboratory. Contact your project manager. -- - -_ - - Special --Project Rebuirements- such as -Low Level Detection Limits or level of QC reported must -- - - be indicated on -the- chain of custody {Use -Additional Comments Section.) 1998 DIGESTER MONTH TEMP pH 1 14.6 6.96 2 13.2 6 3 16.4 6.76 4 19.5 5.89 5 23.2 5.8 6 26.3 6.34 7 27.2 6.84 8 28.0 6.15 9 24.0 4.81 10 21.6 11 16.5 6.79 12 21.0 6.87 Avg 21.00