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WQ0004222_1997 Annual Report_19980211
I.V. Systems Division Baxter Healthcare Corporation 704.756-4151 P.O. Box 1390 Marion, North Carolina 28752 A February 11, 1998 NC Division of -Environmental Management Water Quality Section -,Facilities Assessment Unit P.O. Box 29535 Raleigh, NC 2762670535 Reference: Annual Report Permit No. WQ0004222 Enclosed are three copies of our Annual Monitoring and Reporting Requirements of permit number WQ0004222 Baxter Healthcare Corporation Land Application of Sludge McDowell County for 1997. If you have any questions, please call me at 704-756-6527. Sincerely, Phil Castro PC/cw Enclosures FEB 2 5 1998 TION ��,iER QUA1-1�Y SEC ion pisChAe It NORTH COVE' ANNUAL LAND APPLICATION CERTIFICATION FORM County f�T�PnTTFT T-^ Year 1997 Permit Number WQ0004222 - tY _ Facility Name (as shown on permit) BAXTER HEALTHCARE CORPORATION Land Application Operator WALKER HOD Ems— Phone tt 704-756-6618 Land application of residuals as allowed by the above permit occurred during the past calendar year X YES NO. If NO, skip Part I and Part II and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part I • Total number of application fields in permit. 8 -Total number of fields land application occurred during the year. 4 -Total amount of dry tons applied during the year for all application sites. 167.5 Total number of acres land application occurred during the year. 44.8 Part II Facility was compliant during calendar year 1993 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Environmental Management X YES NO. IF NO, PLEASE PROVIDE A WRITTEN DESCRIPTION WHY TIE FACILITY WAS NOT COMPLLkNT, THE DATES, AND EXPLAIN CORRECTIVE ACTION TAKEN. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the pen -nit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. Al. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 . (applicable to 40 CFR Part 503 regulated facilities) 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with. (applicable to 40 CFR Part 503 regulated facilities) 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Environmental Management. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. ed on the permit were maintained during each application 12. All buffer requirements, as specifi of residuals. "I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY KNOWLEDGE AND RE ARE SIGNIFICANT PENALTIE UBMIETTINTRUE, ALS�E INFORMATION, INCLUDING THE POSSIBILITY OF FINES AND IMPRISONMENT FOR S FOR KNOWING VIOLATIONS." Permittee Name and Title (type or print) tA�of p()a4C�' � - / � - SignatuparerDate (if different from Permittee) Note: Preparer is defined in 40 CFR Part 503.9(r) Signature of Pemaittee Date �— Date Signature of Land A.pplier (if different from Permittee and Preparer) DEM FORM CF (10/94) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding laboratory analysis. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number Facility Name NPDES # or WO H (residual only facilities) WWTP Name W 0004222 BAXTER HEALTHCARE CORP NC0006564 BAXTER HEALTHCARE CORP liesicival Analysis Uaia Date Sampled (grab) or Date Com osited 1/22/97 4/21/97 7/14/97 11/4/97 Percent Solids 1.5 1 1.6 1 1.4 1 1.6 PARAMETERS (mq/kq dry welght) Laboratory 1 ) PACE LABORATORIES, INC. 2) 3) -- Arsenic Cadmium ND 53 ND ND Chromium 80 82 ND 62 Copper 270 580 ND 47 Lead ND 340 ND ND Mercury Molybdenum Nickel ND ND ND ND Selenium Zinc 370 830 500 560 TKN 76,800 68,000 59,000 110,000 Amrnonia-Nitro en 310 690 5 500 250 Nitrate -Nitrogen 1,440 15,600 73 ND Total Phosphorus 3 , 800 11,200 13,200 4,200 X--------- Ai� --- --�------ ------ --- (SIGNATUREOPARER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gatherod and evaluated the Informallon submlllod. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." t, DEM FORM SSF (10/94) ANNUAL LAND APPLIGA r rr-IN FIELD SUMMARY FUHM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE CC -TED AND SUBMITTED FOR EACH APPLICATION FIELD. Row PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. FACILITY NAME BAXTER HEALTHCARE CORPORATION OWNER BAXTER HEALTHCARE CORP SITE # 2 OPERATOR WALKER HODGES FIELD # 5 TOTAt DRY TONS APPLIED (ANNUAL) 13.58 PERMIT N WQ0004222 CATION EXCHANGE CAPACITY (non 503 regulated facilities only) 6.7 ACRES PERMITTED 5.5 ACRES UTILIZED 5.5 DATE or MONTH Gallons /or Cubic Yards (specify) Dry Tons per Acre Residual Source % Solids Noie Do IJo t,ei@A�aragos Mineralization Rate Application Molhod (surrace or Injection) I[re�orhnfl by month koep heso' ;,dell recar * on Crop Total per.Acre Inchesnalntall paet 24 tire. Silo Conditions (Dry, Molsr, wet) 1/97 210,000 38,182 2.47 DIGESTOR 1.5 SURFACI ESQUE Lime A llcallon DATE LBSIACRE 4 1 7 800 IA Permit Limit (Ibs./acre/year) - 1st Crop / 2nd Cro Permitted Cumulative Pollutant Loading Rate (Ibs./a X----- --- --� ---- - -- - - - - - - - - ----- ---- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penally of law, that this document was prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gathered and evaluated the Information submitted. I am aware that thoro are significant penalties for submitting false Information, Including the possibility of fines and Imprisonment for knowing violations." K DEM FORM FSF (2/95) ANNUAL LHINU HYt'LIUA t It JrN t-ItLU SUIVIMf1MT t-UtiM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE CI ETED AND SUBMITTED FOR EACH APPLICATION FIELD. 'TV PLACE A "N/A" IN A BLANK Old BOX WHEN NOT APPLICABLE. ' FACILITY NAME BAXTER HEALTHCARE CORPORATION _ PERMIT If WQ0004222 OWNER BAXTER HEALTHCARE CORP SITE # 2 CATION EXCHANGE CAPACITY (non 503 regulated facilities only) 7.0 OPERATOR WALKER HODGES FIELD # 2 ACRES PERMITTED 7.1 ACRES UTILIZED 7.1 TOTAIL DRY TONS APPLIED (ANNUAL) _19.56 DATE or MONTH Gallons /or Cubic Yards (specify) Dry Tons per Acre Residual Source % Solids No a Do Nol 40e Mo6t gns Mlnmliarlon nato Application Mothod (surmco or oouon In I ) If;:r2potUr9 by month dalf recatds keop`iheSe: on ICe Crop Total per Acre Inchos noloAno Paer 24 lire. Silo Conditions Dry, Molsl,. Wot) 1/97 54,000 7,606 .47 FESCUE 4/97 108,000 15,211 .98 1.55 5/97 150,000 21,127 1.30 1.48 Lime Apllcallon DATE I LBSJACRE r `3{ 5 � � , ^ � , u; ���. t "rt�- . t �,��' vrr4a„r,o-�'c� �i� yjtt',L r�� �k" �i���=i.. • � ----�2 XPPLIER) ----------(SIGNATURE OFLADATE "I certify, under penalty of law, that this document was prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gathered and evaluated the Information submitted. I am aware that there are significant penalties for submitting false Information, Including the possibility of fines and Imprisonment for knowing violations." k DEM FORM FSF (2/95) ANNUAL LANU At VLIGA I IUN I-ItLU SUMMAHY 1-UHM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE C( ETED AND SUBMITTED FOR EACH APPLICATION FIELD. ® PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. FACILITY NAME BAXTER HEALTHCARE CORPORATION _ _ PERMIT # WQ0004222 OWNER BAXTER HEALTHCARE CORP SITE If _ lA CATION EXCHANGE CAPACITY (non 503 regulated facilities only) 6.8 OPERATOR WALKER HODGES FIELD # 2 ACRES PERMITTED 10.2 ACRES UTILIZED 10.2 TOTAt DRY TONS APPLIED (ANNUAL) 100.14 DATE or MONP-I Gallons /or Cubic Yards (specify) Dry Tons per Acre Residual Source % Solids Qb Do blot Use A'J)Fi?gos Mineralization Rate Application Mothod (Surtace or Injection) I( repothnq by moritfi keepstheso;; Bail` recerds on silo> Crop Total per Acre 1-liosnalnlull pant 24 ttre. Sito Conditions (Dry, Moist, WWI 1/97 100,000 9,804 .62 DIGESTOR 1 2Z97 31-8,000 31,177 1.62 1.25 3/97 192,000 18,824 1.44 1.84 4/97 42,000 4,118 .28 1.64 5/97 120,000 11,765 .84 1.70 6/97 90,000 8,824 .61. 1.67 7/97 186,000 18,235 1.12 1.48 8/97 186,000 18,235 1.08 1.42 9/97 132,000 12,941 .62.1 1.16 11/97 48,000 4,706 .31 1.58 12/97 144,000 14,118 1.28 2.17 TOTALS: Annual Wiali Cumulative Permit Limit (Ibs./acre/year) - 1st Permitted Cumulative Pollutant Low DEM FORM FSF (2/95) +' "t, �r Fir M ti; 1 • • Lime A Ilcatlon DATE L©SJACRE 4111 1000 Mo I NI I - Se I Zn 0 1 1 16.84 / 2nd Crop50 Rate (Ibs./acre) 4.5 C 125 500 125 250 X--- - ---- -� --------------.:2 (SIGNATURE OF LAND APPLIER) DATE "I cortlfy, under penalty of law, that this document was prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gathered and evaluated the Information submitted. I am aware that there are significant penalties for submitting false Information, Including the possibility of fines and Imprisonment for knowing violations." ANNUAL LANU AVVLIL;A t IHN I-ItLU SUMMARY I-UHM PLEASE MAKE A COPY OF THIS BANK FORM TO BE C( ETED AND SUBMITTED FOR EACH APPLICATION FIELD. . PLACE A "N/A" IN A BLANK 011 t30X WHEN NOT APPLICABLE. FACILITY NAME BAXTER HEALTHCARE CORPORATION _ PERMIT fl _00004222 OWNER BAXTER HEALTHCARE CARP SITE # lA CATION EXCHANGE CAPACITY (non 503 regulated facilities only) 7.1 OPERATOR WALKER HODGES __ FIELD # 1 ACRES PERMITTED 22.0 ACRES UTILIZED 22.0 TOTAL DRY TONS APPLIED (ANNUAL) 34.21 DATE or MONTH Gallons /or Cubic Yards (specify) Dry Tons per Acre Residual Source % Solids Noie bo fdol UsA Av6Ao Mineralization Rala Application Mothod (surface or Inioction) If^rAporhng by month K s ,:dail records keep thes3 on sttai> Crop Total per Acre Inchosnolnlall Pont 24 fire. Sito Conditions (Dry, Moist, We() 1/97 6,000 273 .016 DIGESTER 1.4 SURFACI FESCUE 2 97 24,000 109 1 5/97 24,000 1091 .080 1.8 6/97 48,000 2182 .165 1.8 9/97 12,000 546 1 .028 1.2 10/97 276,000 12,546 .693 1.3 11 97 1 14000 5182 .416 1.9 12/97 24,000 1091 .100 2.2 A DATE I LBSJACRE TOTALS: PAN P As Cd Cr Cu Pb Hg Mo NI Se Zn Annual 528,000 24,002 1.56 87 25.2 .70 .26 0 1.76 Cumulative ORIMMINIM .04011 5.55 1.40 .'582 .112 7.295 Permit Limit lbs./acre/ ear - 1st Crop / 2nd Crop Permitted Cumulative Pollutant Loading Rate (lbs./acre) n 1 4.5 125 500 125 250 X Vim" (SIGNATURE OF D APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gathered and evaluated the Information submitted. I am aware that there are significant penalties for submitting false Information, including the posslblllty of fines and Imprisonment for knowing violations." DEM FORM FSF (2/95) PATHOGEN REDUCTION AND VECTOR ATTRACTION CERTIFICATION Per conversation with Lou Polletta on February 23, 1996, attached are the Fecal Coliform data on Pathogen Reduction Class B alternative land Vector Attraction option 4. 1 did not receive a form for this data in my packet. FECAL COLIFORM FROM ATTACHED PACE DATA SHEETS MPN/Ig 1 /22/97 1,100,000 4/21/97 160,000 7/14/97 1,200,000 1' 1 /4/97 100,000 FC (geometric mean) 381,219 SOUR TEST PACE AND BAXTER Pace mg/g/hr 1/22/97 1.01 4/21 /97 0.83 7/14/97 1.41 11 /4/97 0.67 Baxter mg/g/hr 3/10/97 0.88 3/17/97 0.55 4/1 /97 2.13 4/15/97 0.65 4/21 /97 0.65 5/5/97 0.73 5/12/97 0.74 5/19/97 1.14 6/2/97 1.38 6/23/97 0.81 7/14/97 1.04 7/28/97 1.51 8/11 /97 1.22 8/25/97 1.6 9/8/97 0.58 9/22/97 0.92 10/6/97 1.26 10/13/97 0.92 11/4/97 0.63 12/1/97 0.56 SLUDGE DISPOSAL REPORT EAXTER HEALTHCARE CORPORATION NORTH CODE FACILITY PERMIT NUMBER WQO004222 DATE: I - - -7 SIGNATURE OF OPERA TOR: SITE NO. ACRE.S IA-1 BARTER 1EALTHCARE CORP. 22.0 IA-2 BA.=R HEALTHCARE CORP 10.2 IA-3 B AXTER HE ALTHC ARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH 9.1 7.5 'AL AVAILABLE.ACRES :. _ .. 72.9.. METHOD OF_ APPLICATION: SURFACE APPLICATION WEATHER CONDITIONS: CLEAR '--! PARTLY CLOUDY LrITTMV- SOIL CONDITIONS: WET DRY: CROP: HAY CORN PASTURE LOADS HAULED (6,000 GALII.OAD) cl APPLICATION SITE: SITE AND FILED NO. �--' - SITE AND FIELD NO. GALLONS -57'YVO C #' S b. SITE AND FIELD NO. GALLONS #'S - SITE AND- FIELD NO. GALLONS #' S NDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS ` SLUDGE DISPOSAL REPORT EAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE:- q% ;SIGNATURE OF OPERATOR: zaz 9-aZ2�� SITE NO. ACRES IA-1 BANTER HEALTHCARE CORP. 22.0 IA-2 BARTER HEALTHCARE CORP 10.2 IA-3 BAD ER HEALTrICARE CORP 4.8 2-2 HENiRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAP VIAN (2) WEATHER CONDITIONS: CLEAR _ CLOUDY (3) SOIL CONDITIONS: WET DRY: PARTLY CLOUDY (4) CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) 7 - (6) APPLICATION SITE: SITE AND FILED NO. _ a. SITE AND FIELD NO. —� GALLONS �° O #' S- b. SITE AND FIELD NO. GALLONS #' S c. SITE AND FIELD NO. .,GALLONS #' S F POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X NIILLION MG GALLONS �� %S�^ �� 7 SLUDGE DasPosat SPORT BAxTER HEALTHCARE coxPoRATiox NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE: SIGNATURE OF OPERA TOR: r/ SITE NO. ACRES 1A-1 DA,=R HEALTHCARE CORP. 22.0 -ER CORP 10.2 IA-2 BAX 1A-3 BAXTER HE ALTHCARE CORP 4.8 2-2 HENRY BROWNi 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 -.-,--CLOUDY, -,:�:--:�;<: ..: (3) SOIL CONDITIONS: WET (¢) CROP: HAY : -CORN (5) LOADS HAULED (6,000 G_ LTOAD) DRY: PASTURE (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. 6�2_ S GALLONS i dC) Je7 b. SITE AND. FIELD NO. GALLONS . . c. SITE AND FIELD NO.- GALLONS ' : . #S U #IS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS %l �d ' SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COTE FACILITY PERMIT NUIMER WQ0004222 DATE: - SIGNATURE OF OPERATOR: . 5, SITE NO. ACRES IA-1 BAX-FER rEALTHCARE CORP. 22.0 1A-2 BA=L R HEALTHCARE CORP 10.2 1A-3 BAXTER- HE.: THC, RE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWNN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 - 5-5 b ROM ENGLISH 7.5 TOTAL'AVAILABLE. ACRE S- 72.9 (I) METHOD OF APPLICATION INJECTION -- SLTRFACE'APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY . ....CLOITDY . (3) SOIL CONDITIONS: WET -DRY: (4) CROP: HAY CORN PASTURE - (S) LOADS HAULED (6,000 GALILOAD) - (6) APPLICATION SITE: --SITE AND FILED NO. a. SITE -AND FIELD NO. �� - - GALLONS b. SITE AND FIELD NO. GALLONS`.— #' S c. SITE AND. FIELD NO: = GALLONS - - ` #, S POUNDS DRY WEIGHT — PPM SOLIDS X 8.34 X NU LLION MG GALLONS SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE. SIGNATURE OF OPERA TO SITE NO. ACRES 1A-1 BA,=R �IEALTHCARE CORP. 22.0 1A-2 BA=R HEALTHCARE CORP 10.2 IA-3 BAXTLP. HEALTHCARE CORD 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY ---- - - CLOUDY. -- (3) SOIL CONDITIONS: WET DRY: (4) CROP:: HAY CORN PASTURE (J) LOADS HAULED (6,000 GALCLOAD) (6) APPLICATION SITE: SITE -AND FILED NO.' a. SITE AND FIELD NOGALLONS S I Y� -- b. SITE AND FIELD NO. GALLONS #'S - c. SITE AND FIELD NO: GALLONS'. - #' S POUNDS DRY WEIGHT = PPM SOLIDS X 3.34 X MILLION MG GALLONS d Vpx F.7Y/K/Yi2� (3) SOIL CONDITIONS: WET . (4) CROP: HAY CORN (5) LOADS HAULED (6,000 GAL)\LOAD) SLUDGE DISPOSAL REPORT B.TER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT ITT ER WQ0004222 DATE: c SIGNATURE OFOPERA TOR: SITE NO. lA-1 Bil-K TER �ALTHCARE CORP. IA-2 B,' R HEALTHCARE CORP 1A-1 D_- ;i Ll,1 r.-' -iCARE C 0 R P 2-2 HENRY BROW 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES (1) METHOD OF APPLICATION: INJECTION - SURFACE APPLICATION (') WEAVE CONDITIONS: CLEAR CLOUDY _ DRY: Z" ICILi��y 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7S PARTLY CLOUDY PASTURE (6) APPLICATION SITE: SITE AND FILED NO. ZZ - A;�- 2 'S a. SITE AND FIELD NO. q ( GALLONS �f ova #'S /Yam b. SITE AND FIELD NO. / GALLONS _ a #'S c. SITE AND FELD NO. GALLONS o'' #'S POUNDS DRY WEIGHT = PPM SOLIDS X 3.34 X MILLION MGoGALLONS ,14� x�x SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE C O RPO RATIO N NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE: -' SIGNATURE OF OPER4TOR: .SITE NO. ACRES 1A-1 BAXIER=t— LTHCARE CORP. 22.0 IA-2 BA.XTEER HEALTHCARE CORP 10.2 1 A-3) BA X I ER r .Al—THCARE CORP 4.8 2-2 HENTRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES . 72.9 (�) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION !/ (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY. - (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN PASTURE (S) LOADS HAULED (6,000 GALILOAD) Gl (6) APPLICATION SITE: SITE AND FILED NO. ` a. SITE AND FIELD NO.' GALLONS 60 #'S b. SITE AND FIELD NO. GALLONS #' S c.' SITE AND FIELD NO. GALLONS #' S - POUNDS DRY WEIGHT = FPM SOLIDS X 8.34 X MILLION MG GALLONS �oZ� SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PEM IT NIAMRR WQ0004222 DATE: % 7-7 5 SIGNATURE OF OPERA TOR: SITE No. AGES 1A-1 B.A—XLR HEALTHCARE CORP. 22.0 IA-2 BA-XTER =kLTHCARE CORP 10.2 IA-3 B A.:KTER HE,7' L T HCARE C 0RP 4.3 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES 72.9 (I) 'METHOD OF APPLICATION: INJECTION J SURFACE APPLICATION (?) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY (3) SOIL CONDITIONS- WET DRY: (4) CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. 1`2 GALLONS �� #'S b. SITE AND FOLD NO. GALLONS #' S c. SITE AND FIELD NO. GALLONS #'S POUNDS DRY WEIGHT= PP-M SOLIDS X 8.34 X Iffi LION MG G,/ALLON�SQ�773 SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE PACMI'i`Y PERMIT NUMBER WQ0004222 DATE. /- 3 0 - r1'7 SIGNATURE OF OPERATOI? SITE NO. ACRES lA-1 BAXTER �ALTHCARE CORP. 22.0 IA-2 B AXTER HEALTHC, PRE CORP 10.2 1A-3 BAXTEr, R HEALTHCARE C0RP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 ® 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES 72.9 (I) METHOD.OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. y a. SITE AND FIELD NO. GALLONS oZ 6U0 #' S y(' } b. SITE AND FIELD NO. GALLONS #IS c. SITE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COTE FACILITY PERMIT NI7M13ER WQ0004222 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 B A,K=R BEALTHCARE CORP. 22.0 IA-2 BA=L R HEALTHCARE CORP 10.2 lA-3 BASER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 (2) WEATHER CONDITIONS: CLEAR `f PARTLY CLOUDY - h CLOUDY -_ -- - - •�° � -= . - .. _:.. . �. : � ...::- �. (3) SOIL CONDITIONS:, WET DRY: (4) CROP: HAY .CORN . (S) LOADS HAULED (6,000 GALILOAD) PASTURE (6) APPLICATION SITE: SITE AND FILED NO. f%l �— I a. SITE AND FIELD NO. Z— GALLONS #' S /.33"6"t" b. _ SITE AND.FIELD NO.. GALLONS'S _ SITE AND FIELD-NO.GALLONS = r , UNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONkx SLUDGE DISPOSAL. REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERsMIT NUMBER WQ0004222 DATE: - r - / I. SIGNATURE OF OPERATOR: f ` l SITE NO. ACRES IA-1 BANTER HEALTHCARE CORP. 22.0 IA-2 BAXiER HEALTHCARE CORP 10.2 IA-3 BAnl ER HEALTHCARE CORP 4.3 2-2 h'ENTRY BROWN" 7.1 2-5 HENRY BROWNT 5.5 4-4 b DEAN CHAPMAN 6.7 :.... _ CLO ,3) SOIL CONDITIONS: WET D (4) CROP: HAY`--y CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. Z149, a. SITE AND FIELD NO. r- GALLONS,�?�/� #'S b. SITE AND FIELD NO. GALLONS #'S _ c. SITE AND FIELD NO. GALLONS #'S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY'. PERMIT NUMMER WQ0004222 DATE. SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BANTER HEALTHCARE CORP. 22.0 IA-2 BARTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5-5 4-4 b _- DEAN CHAPMAN 6.7 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP:: HAY CORN'-:-' PASTURE (5) LOADS HAULED (6,000 GAL\LOAD) 3 (6) APPLICATION SITE:` SITE AND FILED NO. a. SITRAND FIELD NO. GALLONS s b. SITE AND FIELD NO.. GALLONS # S: C.: SITE AiVI)FIELD NO. GALLONS POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS o,1eX;z,;jrX -12 7L SLUDGE DISPOSAL REPORT - EAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY = PERMIT DER WQ0004222 DATE: a2 SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BA,=RHEALTHC.ARE CORP. 22.0 IA-2 BA,=R HEALTHCARE CORP 10.2 1A-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENTRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7' (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: -HAY :' - _ .CORN - :PASTURE - - -. (5) LOADS HAULED (6,000 GALILOAD) A2(6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND. FIELD ONS S NO. o`- ° GALL�4! dd #' ` b. SITE AND FIELD NO. GALLONS #' Q `-i c. SITEAND FIELD -NO..- - GALLONS:: :-- #'S f ra POUNDS DRY 'WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACMITY - PERMIT NUMBER WQ0004222 DATA': SIGNATUREGF GRLRATOR SITE NO. ACRES IA-1 BA,=R HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10-2 IA-3 BARTER HEALTHCARE CORP 4.8 2-2 HE?14-RY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY _.. -CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP:. HAY CORN PASTURE {$) LOADS HAiJLED (6,000 GALILOAD) -: (6) APPLICATIQN SITE:- SITE AND FILED NO. = �� `a- SITE AND FIELD NO. �-- GALLONS r # S b: SITE AND FIELD NO. GALLONS Ws SITE SITE AND FIELD NO. GALLONS.-.-.-.' #'S '� ,POUNDS CRY WEIGHT = PPM SOLIDS X 8.34 Y MILLION MG GALLONS �6� Si,I7DCzE DISP(3SAL REPORT BA7LTER HEALTHCARE CORPORATION NORTH COVE FACIY.ITY PERMIT NUMBER WQ0004222 DATE: e? • 7- 97 SIGNATURE OF OPERATOR: 4'k../ SITE NO. ACRES IA-1 BA,=R HEALTHCARE CORP. 22.0 1A-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXI E R HEALTHCARE CORP 4.8 2-2 HE BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 (2) WEATHER CONDITIONS: CLEAR - = CLOUDY:.::... (3) SOIL CONDITIONS: WET DRY: PARTLY CLOUDY (4) CROP: HAY CORN PASTURE - (5) LOADS HAULED (6,000 GALLOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. GALLONS #'S zi� - b. SITE AND FIELD NO. GALLONS. #'S c. SITE AND FIELD NO. - - GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLON) SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE: SIGNATURE OF ORLRATOR.• SITE NO. ACRES IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 B AX i. ER HEALTHCARE CORP, 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAP -MAN 6-7 5-1 b ROM ENGLISH 9.1 SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY--._._.. -::• _,.. .:_ - ---._. .. .- (3) SOIL CONDITIONS: WET (4) CROP: HAS' CORN (S) LOADS HAULED (6,000 GALTOAD) (6) APPLICATION SITE: SITE AND FILED NO. DRY PASTURE a. SITE AND FIELD NO. GALLONShc b. SITE AND FIELD NO. GALLONS FI c. SITE AND ELD NO. - GALLONS POUNDS DRY WEIGHT = FFId-I SOLIDS X 8.34 X MILLION ���� j� S7-7 SLUDGE DISPOSAL REPORT RAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY. ERMIT NUM13ER WQ0004222 DATE: SIGNATURE OF OPERATOR: SITE NO. I ACRES IA-1 BARTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORD 10.2 1 A- B a YTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 (6) APPLICATION SITE: SITE AND FILED a SITE AND" FIELD NO. ` _ _ GALLONS Dv #' S- ® b. SITE AND FIELD NO. _ GALLONS #' S c. STTE ANI3 FIELD NO. _: : =GALLONS #'S :X POUNDS DRY. WEIG$T = PPM SOLIDS8 34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COTE FACILITY . PERMIT NU ER WQ0004222 DATE. - ,Q SIGNATURE OF OPERA MR: SITE NO. ACRES lA-1 BAX'TER =ALTHCARE CORP. 22.0 IA-2 B Al- i ER 1EALTHCARE CORP 10.2 IA-3 B AlY i ER HEALTHCARE CORP 4.8 2-2 FT..ENT.Y BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 (2) WEATHER CONDITIONS: CLEAR (3) SOIL CONDITIONS: WET DRY: PARTLY CLOUDY (4) CROP: HAY ` CORN PASTURE (J) LOADS HAULED (6,000 GAL�LOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. GALLONS aV 3 #'S /,33 b. SITE AND FIELD NO. GALLONS c. SITE AND FIEELD NO. GALLONS #'S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS o�YXF?YX 4� -7 - � a \ SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUJ ER WQ0004222 DATA`: .SIGNATURE OF OPERATOR: SITE NO. r f ACES 1A-1 BAXTERHEALTHCARE CORP. 22.0 lA-2 BARTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b . DEAN CHAPMAN 6.7 SURFACE APPLICATION (4) CROP: HAY (5) LOADS HAULED (6,000 GALILOAD) L (6) APPLICATION SITE: SITE AND FILED NO. a;z a. SITE AND FIELD NO. (/91 GALLONSp V c7 b. SITE AND FIELD NO. GALLONS c. SITE AND FIELD NO. GALLONS �./ CORN PASTURE #2S 333 #' S #I S . POUNDS DRY WEIGHT = PP1YI SOLIDS X 8.34 X .M I.,.LION MG GALLONS SLUDGE DISPOSAL REPORT PAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PEIUAIT NUMBER WQO0O4222 DATE. �' 19-- SIGNATURE QF OPE RA'' OR .% SITE NO. IA-1 Bt%,X=R HEALTHCARE CORP. 1A-2 B.XI'ER HEALTHCARE CORP 1A-3 B A-XTER HEALTHC:,�RE CORP 2-2 HENRY BRO«Ni 2-5 HENRY BROWN ACRES 22'.0 10.2 4.8 7.1 5.5 4-4 b DEAN CHAPMAN 6.7 I 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLEACRES 72 9 (1) METHOD OF APPLICATION: -INJECTION SURFACE. APPLICATION 1 (2) WEATIEER CONDITIONS: CLEAR PARTLY CLOUDY . � CLOUDY. (3) SOIL CONDITIONS: WET (4) CROP: HAY CORN (5) LOADS HAULED (6,000 GAL\LOAD) DRY: t// PASTURE (6) APPLICATION SITE: SITE AND FILED NO.� a. SITE AND FIELD NO. IA,)- GALLONS #'S 13'211s 4 b. SITE AND FIELD NO. GALLONS #'S c. SITE A.N D FIELD NO. GALLONS- #' S POUNDS DRY WEIGHT = FPM SOLIDS X 8.34 X MILLION MG GALLONS �Gvs �o f�XF/3 DATE: SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY . - PERMIT NUM13ER WQ0004222 �- /9 I `7 SIGNATURE OF OPERA TO-.'?: i SITE 17Os ACRES IA-1 BARTER HEALTHCARE CORP. 22.0 IA-2 BAXIER ZEAL iHCARE C0RP 10.2 l A-3 B A. TER HEALTHC-ARE CORP 4.8 2-2 HEENTRY BROWNN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 2 WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY.,_.- (3) SOIL CONDITIONS: WET DRY: 4 O CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 GAL\LOAD) (6) APPLICATION SITE: SITE AND FILED NO. ` =. a. SITE AND FIELD NO. l�I C GALLONS #'S s�S b. SITE AND FIELD NO. GALLONS #,S c. SITE AND FIELD NO. GALLONS #'S - P = POUNDS DRY WEIGHT � P11�I SOLIDS � &.34 X MILLION MG GALLONS �. 7�/�`� - p3X - SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE. --2 2e -,FZ SIGNATURE OF ORLRATOR: SITE NO. IA-1 B X-EER HEALTHCARE CORP. IA-2 BA-XTER HEALTHCARE CORP IA-3 3AXTER HEALTrICARE CORD 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN (2) WEATHER CONDITIONS: CLEAR_ CLOUDY (3) SOH. CONDITIONS: WET (4) CROP: HAY 41-1� CORN DRY: ACRES 22.0 10.2 4.8 7.1 5.5 6.7 PARTLY CLOUDY PASTURE (5) LOADS HAULED (6,000 GALILOAD) . (6) APPLICATION SITE: STTE AND I'TT.FD NO. 21 a. SITE AND FIELD NO. �— GALLONS b. SITE ANrD FIELD NO. GALLONS #, S c. SITE AND FIELD NO. GALLONS #7S POUNDS DRY WEIGHT = DP.Nf SOLIDS X 8.34 X MILLION MG GATLONS z 9 SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUM13ER WQ0004222 DATE: cP ai 577 SIGNATURE OF O ER,4T0.1�: SITE NO. AGE'S IA-1 BA, -,-'TER HEALTHCARE CORP. 22.0 IA-2 BARTER HEALTHCARE CORP 10.2 IA-3) B,\XTER HEALTHCARE CORD 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL. AVAILABLE ACRES = _ 72.9 (I):-MIJTHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR _ CLOUDY (3) SOIL CONDITIONS: WET PARTLY CLOUDY DRY: L�— - (4) CROP: HAY tl� CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. Z/4 �— a. SITE AND FIELD NO. z— GALLONS /PG o #I S b. SITE AND FIELD NO. GALLONS #' S c. SITE AND FIELD NO. GALLONS #7S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X IfILLION MG GALLONS 9 SLUDGE DISPOSAL REPORT BARTER HEALTHCARE C O RPO RATIO N NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE: - SIGNATURE OF OPERATOR c� SITE NO. IA-1 BA=R HEALTHCARE CORP. IA-2 BAXTER HEALTHCARE CORP 1A-3 BANTER HEALTHCARE CORP 2-2 HENRY BROW 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN ACRES 22.0 10.2 4.8 7.1 5.5 5-1 b ROM ENGLISH 9.1 SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY (3) SOIL CONDITIONS: WET (4) CROP: HAY CORN (5) LOADS HAULED (6,000 GAL`LOAD) DRY: PASTURE (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. GALLONS b. SITE AND FIELD NO. GALLONS c. SITE AND FIELD NO. GALLONS #IS y #' S #' S - POUNDS DRY WEIGHT = aPM SOLIDS X 8.34 X MILLION MG GALLONS DATE: - ] UDGE DISPOSAL. REPORT B.r XTER HEALTHCARE CORPORATION NORTH COVE FACILITY PEFall ' NUMBER WQ0004222 3- f=,?'_i . / SIGNATURE OF OP TOR: SITE NO. 1A-1 BAX-FE'R=ALTHC.A E CORP. lA-2 B.-�,.=_'R THEALTHCARE CORP ER _HEALTi-iC.-kRE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN A C ES 22.0 10.2 4.8 7.1 5.5 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES 72.9.. . (I) M ETHODvOF APPLICATION:. INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY - (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN PASTURE (S) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. LIA a. SITE AND FIELD NO. GALLONS,' 4 00 #' S b. SITE AND FIELD NO. GALLONS #'S c. SITE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X INIILLION MG GALLONS SLUDGE DISPOSAL REPORT BA TER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ00O4222 DATE: -7 SIGNATURE OF OPERA TOR: SITE NO. ACRES IA-1 BA'--=R HEALTHCARE CORP. 22.0 IA-2 BA.�R HEALTHCARE CORP 10.2 1A-3 BA.x i ER HEALTHCARE CORP 4.8 2-2 HE��RY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR CLOUDY (3) SOIL CONDITIONS: WET �/~ DRY: (4) CROP: HAY CORN PARTLY CLOUDY PASTURE (5) LOADS HAULED (6,000 GALILOAD) �7 (6) APPLICATION SITE: SITE AND FILED NO. Illf a. SITE AND FIELD NO. GALLONS a' b CD' #'S l(A52�1 -- b. SITE AND FIELD NO. GALLONS #'S - c. SITE AND FIELD NO. GALLONS #'S POUNDS DRY WEIGHT = ?P-Nl SOLIDS X 8.34 X MILLION MG GALLONS �;�bl,-�� SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NU ER W Q 0004222 DATE: %`7 SIGNATURE OF OPERATOR: TOR: SITE NO. '� ACRES IA-1 B A:=R T P ALTHCARE CORP. 22.0 IA-2 BA==R 11EALTHCARE CORP 10.2 IA-3 BA TER HEALTHCARE CORD 4.8 2-2 HENTRY BROWN- 7.1 2-5 HENTRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN (5) LOADS HAULED (6,000 GAL\LOAD) N PASTURE (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. I / GALLONS Yid #' S b. SITE AND FIELD NO. GALLONS #'S . c. SITE AND FIELD NO. `' GALLONS #'S .-- POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS � ��� SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH CODE FACILITY - PERMIT NUMBER WQ0004222 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BAXTER=ALTHCARE CORP. 22.0 IA-2 BANTER HEALTI CARE CORP 10.2 1A-3 BANTER HEALTHCARE CORD 4.8 2-2 HENRY BROWN 7.1 2-5 HENTRY BROWN 5.5 4-4 b DEAN 'CHAPMAN 6.7 v 5-1 b ROM ENGLISH 9.1 5-5 b . ROM ENGLISH 7.5 (2) WEATHER CONDITIONS: CLEAR _ CLOUDY PARTLY CLOUDY (3) SOH., CONDITIONS: WET DRY: (4) CROP: •HAY-- CORN PASTURE . (5) LOADS HAULED ,(6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. GALLONS CU O #' S N76 � b. *SITE AND FIELD NO- GALLONS #' S c. SITE AND FIELD NO. GALLONS #'S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACMITY PERMIT NUM3ER WQ0004222 DATE. 3 SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BAD'-=IR liE.UTHCARE CORP. 22.0 IA-2 BAXTEERIHEALTHCARE CORP 10.2 IA-3 B,AXTIER h7EALT11CARE CORP 4.8' 2-2 HENNRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 L " (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY w. (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY -CORN—* PASTURE (5) LOADS HAULED (6,000 GA-L\LOAD) (6). . APPIJCATTON.SnE: SITE AND FILED NO. A a. SITE AND FIELD NO.: 114 GALLONS �V,6 b SITE AND FIELD NO. GALLONS C. SITE. AND FIELD .NO:. GALLONS 7s. rr #9S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALWO C76 SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY = . PERMIT NI `MBER WQ0004222 DATE: 2)/_,�7 SIGNATURE OF OPERATOR: SITE NO. ACRES 1A-1 BANTER HEALTHCARE CORP. 22.0 IA-2 B AX T ER 19EALTHCARE CORP 10.2 !A-3 B AXTER HEALTHC ARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 (2) WEATHER CONDITIONS: CLEAR V� PARTLY CLOUDY .,r (3) SOIL CONDITIONS: WET DRY: 4) CROP: HAY,;-- _ �l CORN: PASTURE (5) LOADS HAULED (6,000 GAL\LOAD) (6) APPLICATION SITE:.- SITE AND FILED NO. a. SITE AND iZFLD NO: �� GALLONS 02 Oo v #'SY'=� Y b. SITE AND FIELD. NO. = GALLONS :#7S= •- �, _ - c. SITE'AND FIF.LD.NO - GALLONS POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X IU LLION MG GALLONS »u: SLUDGE DISPOSAL REPORT IN TER HEALTHCARE CORPORATION NORTH COVE FACIL E IT ER WQ 04222 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BAXTERHEALTHCARE CORP. 22.0 IA-2 BAXTERHEALTHCARE CORP 10.2 IA-3 BAX'TER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 Albx 5-1 b ROM ENGLISH 9.1 - 5-5 b ROM ENGLISH 7.5 -. TOTAL AVAILABLE ACRES _: _ __-.:_:72.9 (1). ;METHOD ®F APPLICATION:. INJECTION:: SURFACE APPLIC ON (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY { _ CLOUDY. (3) SOIL CONDITIONS: WET DRY: (4) CROP:. HAAY CORN - PAST`YJRE (5) LOADS HAULED (6,000 GALTOAD) (6) APPLICATION SITE:_. SITE AND FILED No. 3U: a. SITE AND FIEiD N®: l -GALLONS �� : - #, S b. SITE AND FIELD NO: GALLONS- #'S - _ c. ' SITE AND TIELD---NO.'' -_GALLONS :. # S..: POUNDS DRY_ WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS % SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY - _ PERMIT NUMBER WQ0004222 DATE: c/ 17 SIGNATURE OF OPERATOR: SITE NO. ACRES 'T IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BSA _=R HEALTHCARE CORP 10.2 1A-3 BA.'�CTER HEALTcICARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b : DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5.b-.. ROM ENGLISH - _ -:TOTAL "AVAMABLE---ACRES- - LS�:ti: +•.c-_"` '� -�-_ - _ �-�xMiY'?�==.-_.. - --- � - -= ..":J��:�� —'s ¢ti �'c_ .:�. sc�--.xy"�-a ��• - _ (I) `METHOD .OF -APPLICATION: -:INJECTION`S _- SURFACE APPLICATION D. J11l' APf!J XMJ' JJ'IN V. LYKLLV1 U - -_- _ c.-- ID SITE"A"FIELD NO." ,__ _ - GALLONS S - _ POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X NU LLION MG GALLONS �f SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION' NORTH COVE FACILITY'-'.'-. PERMIT NUMBER WQ0004222 DATE: SIGNA TURE OF OPERATOR: SITE NO. IA-1 B A.=,R HEALTHCARE CORP. IA-2 BAXTERBEALTHCARE CORP IA-3 BAXTER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b ..DEAN CHAPMAN ACRES 22.0 10.2 4.8 7.1 5.5 6.7 5-1 b ROM ENGLISH 9.1 5-5 b. -ROM ENGLISH.F 7.5 _.7.-ACRES:,-`---*"- �---TOTAL:AVAELABLE .9- 1):-I6 THOV-DF`".P L C ONi"'INJECTION.- SURFACE APPLICATION WEATHER CONDITIONS: CLEAR PARTLY CLOUDY (3) SOIL CONDITIONS: WET DRY: :CORN ___�_'PA. TURE S 4 CROP: HAS';` LOADS HAULED (6,000 GA LOAD) (6) APPLICAT16N SITE: SITE AND FILED NO. - a*:'SITE AND thELD NO. 97 - b SrrE AND _FEELD NO. GALLONS: #'S SITE AND.T-IELD NO.--- GALLONS POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL. REPORT BARTER HEALTHCARE CORPORATION NORTH COTE FACILITY SATE: PERMIT ER WQ0004222 . — �T_� SIGNATURE OF OPERATOR: SITE NO. ACMES IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 B AXTER HEALTHCARE CORD 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 - 5-5 b ROM ENGLISH 7.5 �:.:.. .:.....TOTAL. ACRES ::: ._ .- _..,72.9. (1) METHOD, OF APPLICATION: -INJECTION - SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY, (3) SOIL -CONDITIONS: WET DRY: (/ (4) CROP: HAY c� CORN - - (5) LOADS HAULED (6,000 GAL\LOAD) (6) APPLICATlbN SITE: SITE AND FILED NO. _ a.� SITE AND FIELD NO. i q b.. SITE AND FIELD NO. c.. SITE AND FIELD NO. PASTURE . GALLONS� S GALLONS #' S GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 5.34 X INULLION MG GALLONS /3 �� SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE C O RPO RATIO N NORTH COVE FACILITY :." PERMIT NUM3ER WQ0004222 DATE: SIGNATURE OF OPERAR: zcw SITE NO. ACRES IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 1A-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5- l . b = ROM ENGLISH - 9.1 5-5 b ROM ENGLISH 7.5 " :._TOTAL::AVAlI;ABLE:ACRES- -' - _ �72.9 - �= _METHOD OFAPPJ_ICATION::- SURFACEAPPLICATION v - (2) WEATHER CONDITIONS: CLEAR = PARTLY CLOUDY- = (3) SOIL CONDITIONS WET DRY ! _ (4) CROP:: HAzi''::: •`: = = `CORN _ . :..__ _ (5) LOADS HAULED' (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. • -_ - ... _.. __ - _ .�- - - - -'--- -- =.. _ ._ _- __ .... --- --- ---- -_ -_,ram a. SITE AND FIELD NO. =•Z=V GALLONS = G� #_'S S �4 b. SITE AND FIELD NO.- >:.. GALLONS = c. SITE• AND: FIELD NO - : GALLONS .: w..,._ POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X IIIIC.LION MG GALLO S SLUDGE DISPOSAI. REPORT EAXTER HEALTHCARE CORPORATION NORTH COVE FACMITY' - PERMIT NUMBER WQ0004222 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES 1A=1 BAXTER=ALTHCARE CORP. 22.0 IA-2 BAX T ER HEALTHCARE CORP 101 1A-3 BAXTER HEALTHCARE CORP 4.8 ?-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 - 5-5 b ROM ENGLISH 7.5 :. TOTAL AVAILABLE ACRES. ;_... : 72.9 . - - - j Y 3 'METTHOD-_OF. PPLICATION. INJECTION :- SURFACE APPLICATION l (�) WEATHER CONDITIONS: CLEAR t/ PARTLY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN PASTURE (�) LOADS -HAULED (6,000 GALILOAD) / (6) APPLICATION STTE: SITE AND FILED NO. = a: SITE •AND'FIELD NO. - GALLONS t ?JOB #IS A55��-/ "- = b. SITE AND FIELD NO. GALLONS #IS SITE AND FIELD. NO. GALLONS #IS . POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLLO�N SLUDGE DISPOSAL REPORT PAXTER HEALTHCARE CORPORATION NORTH COVE FACMITY PERMIT NVUBMER WQ0004222 DATE: 16- q SIGN ATUJ?E OF OPERATOR: SITE NO. ACRE IA-1 BAXTER �IEALTHCARE CORP. 22.0 1A-2 BA_=RHEALTHC.kRE COPP 10.2 1A-3 BARTER HEALTHCARE CORP 4.8 2-2 hIENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 ,CLOUDY (3) SOIL CONDrrIONS: WET (4) CROP: HAY CORN DRY: PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. -GALLONS 3 b. SITE AND FIELD NO. GALLONS c. SITE AND FIELD NO. GALLONS #' S #' S #' S POUNDS DRY WEIGHT = DPM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT RAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATA': 5- j-97 SIGNATURE OF OPIERATOR: r SITE NO. ACRES IA-1 B AX-IER r1�ALTHCARE CORP. 22.0 IA-2 BA1�ER HEALTHCARE CORP 10.2 IA-3 BA.,`t'TER 19EALT1CARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 (2) WEATHER CONDITIONS: CLEAR (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN (5) LOADS HAULED (6,000 GALTOAD) 6 PARTLY CLOUDY. PASTURE (6) APPLICATION SITE: SITE AND FILED NO. z-- �— a. SITE AND FIELD NO. Z— 2— GALLONS 36"rG #'S b. SITE AND FIELD NO. GALLONS #'S c. SITE AND FIELD NO. GALLONS #'S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE: 5'a SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 B AXTER HEALTHCARE CORP 10.2 lA-3 BAXTER FlEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAII.ABLE: ACRES - -. SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY: (3) SOIL CONDITIONS: WET DRY: (4) CROP: -.HAY CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. :2— GALLONS` `�a °O d . ws b. SITE AND YIELD NO. GALLONS :_ #1 S": c. SITE AND FIELD NO: GALLONS #'S >'• -- POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X ?vlILLION MG GALLONS`-'_ �-L DATE: SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE PAC ITY PERIVET NUMBER W 04222 `S - ,7 ,. SIGNATURE OF OPERA TOP.: SITE NO. ACRES IA-1 BA:iiERrE.,�LTIHICARE CORP. 22.0 lA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BA.XTER HE.-\LTHCARE C0RP 4.8 2-2 HENRY BROWN- 7.1 2-5 HENRY BROw'tiT 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 -TOTAL AVAILABLE ACRES 'F.:• - _ t_,t-.1 .3_ rPy V t. _ - _ _ - ___z _' _ __ __ d:L' _- _ _ 'may. _:.- n�'f ..� (1) ._ METHOD..OF.APPLiCATION: INJECTION - _ SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY .-- CLOUDY -- - . . ' (3) SOIL CONDITIONS: WET DRY: 4 CROP: HAY : CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (9 (6) APPLICATION. SITE: SITE AND FILED NO. _ a. SITE AND FIELD NO: - GALLONS �� #' S b. SITE AND FIELD NO. GALLONS #IS c. SITE AND FIELD' NO. GALLONS .#IS - - POUNDS DRY WEIGHT= PPM SOLIDS X 8.34 X IMMLION MG GALLONS ,636X3 yxl5�l C� SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVEFACILITY PERMIT lTVJMER WQ0004222 DATE: SIGNATURE OF OPERATOR: / .SITE NO. ACRES IA-1 BAX-=R HEALTHCARE CORP. 22.0 1A-2 B A,=R HEALTHCARE CORP 10.2 1A-3 BARTER HEALTrICARE CORD 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 F _� 5-1 b ROM ENGLISH 9.1 (4) CROP: HAY CORN (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. PASTURE a. SITE AND FIELD NO. J GALLONS _ #' S b. SITE AND FIELD NO. GALLONS #' S c. SITE AND FIELD NO. GALLONS #'S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X A11ILLION MG GALLONS SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION _ NORTH COVE FACILITY- DATE: .SIGMA ,SITE NO. ACRES IA-1 BAXTERAEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 102 1 A-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 j 5-1 b _ ROM ENGLISH 9.1 - 5-5 b ROM ENGLISH 7.5 :. ... TOTAL -_Ay. AILABIE.ACRES _ _ . ._... ...._... .J...r . n.. .� .s...__.,._..r,J:• ft.:..:-:�•=�-^^_,"' - - ..-a?•t:. - a` •b.. - — t3''+.-�{:i#��`''=.�..�^`.1.'<�".+�. _ . I -N ETHOD OF APPLICATION: ,INJECTION •-= _.- --:: ,��� _. SURFACE APPLICATION T (2) WEATHER CONDITIONS:. CLEAR PARTLY CLOUDY ' ( 1 - - - " l H - - .. (3) SOIL CONDITIONS: WET DRY:. -r (¢):=.CROPS=HAS';-..- - . .-CORN `PAST`CTRE - __ (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICAT10 SITE;'°SITE AND FILEDNO. SITE ANI9 FIELD NO - - GALLONS s - - ..- b. SITE AND-TULD NO.t`' :GALLONS # S c. -SITE` AI�TID FIEf10. NO:.: = - GALLONS Vs - _ - = PPM SOLIDS X 8.34 X MILLION MG GALLONS - POUNDS DRY.WEIGHT a �.�--. • ::-. _ :_ . . SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERT NUMBER WQ00O4222 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES h IA-1 BANTER HEALTHCARE CORP. 22.0 1A-2 BANTER HEALTHCARE CORP 10.2 1A-3 BAXTI ER 1HE. L-E-ICARE C0RP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 (4) CROP: HAY - PASTURE _ .. (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE. AND FILED NO: a. SITE AND FIELD NO.' GALLONS # S b. SITE AND FIELD NO. GALLONS c. SITE AND FOLD NO. GALLONS-- POUNDS DRY WEIGHT = PPM SOLIDS X 3.34 X iIULLION MG GALLON6 � � CORN. SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY I'ERUAI`I' ER WQ0004222 DATA': Sr'1 SIGNATURE OF OPEF.ATO R: SITE NO. IA-1 3-k t E r+EALTrICARE CORP 1A-2 B.A.X'I'ER HEALTHCARE CORP IA-3 BA; TER HEALTHC.-kRE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN .., 5-1 b 5-5 b DEAN CHAPMAN ROM ENGLISH ROM ENGLISH ACRES 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY. CORN PASTURE L (5) LOADS HAULED (6,000 GALTOAD) (6) APPLICATION SITE: SITE AND FILED NO. l - a. SITE AND FINO. O. ! GALLONS 1 #' S �S/ b. SITE AND FIELD NO. GALLONS #' S c. SITE AND FIELD .NO. GALLONS #'S - - POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS �6 6 �aYX��Y�i�7-5-17 3 SLUDGE DISPOSAL REPORT BANTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE: SIGNATURE OF OPERATOR: -� . &—Zlf SITE NO. A CRES 1A-1 BAX'I'ER I4EALTHCARE CORP. 22.0 !A'-2 BAR HEALTHCARE CORP 10.2 IA-3 BASER HEALTHCARE CORD 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 - 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES 72.9 - ,- _ - - - (1) METE[OD_ OF-APPLICATION:..INJECTION -. E - - SURFACE APPLICATION (2) WEATE R CONDITIONS: CLEAR PARTLY CLOUDYCLOUDY - • (3) SOIL CONDITIONS: 'VET DRY: (4) CROP: HAY -CORN PASTURE (5) LOADS HAULED (6,000 GAL\LOAD) :- - - (6) .APPLICATION SITE: SITE AND FILED NO. _.._ .. a. SITE AND FIELD NO: l GALLONS �b�/ #'S b. SITE AND FIELD NO:: GALLONS #' S -c. SITE AND FIELD NO:: GALLONS = #'S - - - POUNDS DRY. WEIGHT = PNULL SOLIDS X 8.34 X ULLION MG GALLONS 3� � oa Yx Fri ?x 17517= "!':'3IrUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACMITY PERT NUM3ER WQ0004222 DATE. SIGNA TURE OF OPERA TOR: SITE NO. ACRIL,II IA-1 BA,=P, I-=-ALTHCAR.E CORP. T 22.0 IA-2 B ^ � R HEALTHCARE CORP 10.2 1A-3 BARTER I EALTl-ICARE C0RP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CI- APMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY ::CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: RAY CORN " PASTURE ✓ (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. 4 -2 GALLONS �/✓ D 5� #' S b. SITE AND FIELD NO. GALLONS #'S c. SITE AND FIELD NO. GALLONS #'S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X lffiLLION MG GALLONS r17= 3,G"' � SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE. FACILITY PERMIT NUMER WQ0004222 DATE. -7 SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BA—XTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 - .5-5 b ROM ENGLISH - 7.5 TOTAL AVAILABLE ACRES 72.9 (1) METHOD_.©1C+':APPLICATION: -:INJECTION::_ _-- SURFACE APPLICATION t/ (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY - CORN: PASTURE: (�) LOADS HAULED (6,000 GALILOAD) (6) A.PPEICATION SITE: SITE AND FILED NO.. a. SITE AND FIELD NO. l GALLONS v`LY60� #'S %L%/% - im • b. SITE AND FIELD NO. GALLONS .#'S - c. SITE AND FIELD NO. • GALLONS #' S. POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS�X'� ACRES 7 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY.-'* - PERMIT NUMER WQ0004222. DATE: SIGNATURE OF OPERATOR. , SITE NO. 1A-1 BAX"IER HEALTHCARE CORP. IA-2 B AXTER HEALTHCARE CORP 1A-3 BAXTER HEALTHCARE CORP 2-2 HENT Y BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN 57.1 b.. ROM ENGLISH 5-5 b .._::_:. ROM ENGLISH - ,:TOTAL- AYAILABL:E ACRES APPLICATION: -INJECTION==-�s--�—i= =_�•_- _,: - - = - - :.= -- - SURF SCE APPI,IOATION= 4 .:. • . h' - . . (2) WEATIiER CONDITIONS: CLEAR PARTLY CLOUDY- .._ t f : CLOUDY~- - (3) SOEL CONDITIONS: WET DRY: 4 CROP: `=.HAY _ C - _ - ORN __ -- PASTURE - (S) LOADS HAULED (6,000 GALILOAD) - -. - .._ (6) APPLICATION SITE: ' SITE AND FILED NO:.-- - -= -- - - - �7 4' a:': -SITE A-Np.FIELD N-7 O.-.-GALLONS - b. STTE.AND_FIELDNO, _GALLONS.- - - - SITE ANDrFIEI:Ti Ir'Q: = -. GALLO_ NS. POUNDS DRY. WEIGHT PPM SOLIDS X 8.34 X MILLION MG GALLONy�`L`��� SLUDGE DISPOSAL REPORT BA TER HEALTHCARE CORPORATION NORTH COVE FACMITY PEP IT NUMBER WQ0004222 DATE: SIGNATURE OFOPEAI?ATOR: SITE E NO. A CR 1J lA-1 BAXTER HEALTHI CARE CORP. 22.0 1A-2 BA:LjERHEALTHCARE CORP 10.2 lA-3) BAl TER FEALTHC.A E CORP 4.8 2-2 HENRY BROW i 7.1 2-5 HENRY BRO'"Ni 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 . .' TOTAL AVAILABLE ACRES 72.9 (1) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY 3 f (3) SOIL CONDITIONS: WET DRY: C (4) CROP: HAY CORN PASTURE (J) LOADS HAULED (6,000 GALILOAD) (6) _APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. /-T GALLONS b. SITE AND FIELD NO. GALLONS c. SITE AND FIELD NO... GALLONS #IS #' S #' S POUNDS DRY WEIGHT = PPM SOLIDS K 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PER IT NUMBER WQ0004222 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 1A-3 BAXTER h7EALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN, 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH . 9.1 5-5 b _ .....:::_ ROM ENGLISH 7.5 _TOTAL AVAILABLE ACRES:. _. 72.9 ': .. - - - (X) ::METHOD-:OF=APPLICATION:,L INJECTION �_--_--,:.,,, , :....;Y :.-_�/:. •, t _ SURFACE APPLICATION / 2 WEATHER CONDITIONS:. CLEAR PARTLY CLOUDY .` ^ 3 SOIL CONDITIONS: WET DRY.y^ �/ .. (¢) CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. ^ - . a. SITEAND FIELD NO. ` GALLONS-'" b. SITE AND FIELD NO... -'.GALLONS #I S GALLONS D # S - C.- SITE ANFIELD NO.. _ FOUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS 7- � = SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACMITY PERMIT DER WQ0004222 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BAXTER i-lEALTHC ARE C ORP . 22.0 1A-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HE ALT-HC ARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 (4) CROP: HAY CORN (5) LOADS HAULED (6,000 GALILOAD) 5 PASTURE (6) APPLICATION SITE: SITE AND FILED NO. v� a. SITE AND FIELD NO. -,z GALLONS D Y d #, S - . b. SITE AND FIELD NO. GALLONS #, S c.. SITE AND FIELD NO. GALLONS #IS POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS 6 � ��%/S1-7 SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY - ` IT NUMBER WQO0O4222 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES 1 A-1 B ER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 1A-3 BA TER HEALTHCARE CORP 4.8 2-2 HENRY BRO'�N'N 7.1 2-5 HENRY BROWN 5.5 - 4-4 b DEAN CHAP -MAN 6.7 5-1 b ROM ENGLISH 9.1 - 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES - _ 72 9 a. (1) METHOD OF. APPLICATION: INJECTION— -- SURFACE APPLICATION 2 WEATHER CONDITIONS: CLEAR PARTLY CLOUDY C LOUDY (3) SOIL CONDITIONS: 'VET DRY: (4) CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 GAL\LOAD) L (6) APPLICATION SITE: SITE AND FILED NO. _ a. SITE AND HELD NO. GALLONS �% d 1 #' S� b. SITE AND FIELD NO. GALLONS #'S c. STTE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X INU LLION MG GALLONS s � °� -- SLUDGE DISPOSAL, REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUER WQ0004222 DATE: 7---F 27 SIGNATURE OF OPERA T OR: SITE NO. ACRES IA-1 BAR,-X,HEALTHCARE CORP. 22.0 IA-2 BAX -Ir TER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORD 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 9 (2) WEATHER CONDITIONS: CLEAR :� PARTLY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) . CROP:: HAY :_ ._ CORN (5) LOADS HAULED (6,000 GAL\LOAD) (6) APPLICATION SITE: SITE AND FILED NO.: a. -SITE AND FIELD NO..- `GALLONS- yz:�Q U #'S b. SITE AND.FEELD NO.: GALLONS #'S = SITE AND FIELD NO. GALLONS • #' S POUNDS DRY WEIGHT = PP_'VI SOLIDS X 8.34 X MILLION MG GALLONS /cw I BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMT NUMBER WQ0004222 DATE: SIGNATURE OF OPERATOR: SITE NO. 1 A-1 IA-2 IA-3 2-2 2-5 4-4 b BAXTER HEALTHCARE CORP. 22.0 BANTER HEALTHCARE CORP 10.2 BAXTER HEALTHCARE CORP 4.8 HENRY BROWN 7.1 HENRY BROWN 5.5 DEAN CHAPMAN 6-7 ' 5-1 b =. ROM ENGLISH 9.1 - 5-5 b::_.:-.'ROMENGLISH:.: 7.5 r 72 9 TOTAI AVAILABLE ACRES - '' -a i` _ .ri^ sc. tc r•cn. � _-.- -Fey+ ^'-"TMy �� x.• :r ^'�'- *s..,;.,i .� "'.'�-- u' -ti — '� r �'-_ ' +�'ft" S. �-�'"`�.,,,. I i�YETHOD OF APPLICATION , RYJEC'IT03�t - -- - - - - k _. - _ - - --: SURFACE APPLICATION - • ` - - - . -. - - -.lam PARTLY CLOUDY (2) WEATHER CONDITIONS: CLEAR, _ -- CLOUDY _ (3) -.SOIL CONDITIONS: WET D :. (4) CROP: HAY -- ..: CORN -- - PASTURE S LOADS HAULED(6 000 GAL\LOAD) (b) APPLICATION STTE: -SITE AID FILED NO - SITE AND FIELD NO -G''2 GALLONS #,S b. SITE AND FIELD NO..: GALLONS - #'S - GALLLONS c. SITE AND FIELD NO. _ . POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS c k�3 5-7 SLUDGE DISPOS21, REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE -FACILITY �i SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 lA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 (4) CROP:. HAY CORN - PASTURE ✓ (5) LOADS HAULED (6,000 GAL\L.OAD) (6) APPLICATION SITE:. SITE AND FILED NO.: a. SITE -AND FIELD NO. / . 1 a GALLONS r�b `� #;S )3 -7 b. SITE AND FIELD NO. —�— ,GALLONS #'S c.: SITE AND FIELD NO. ;= ' GALLONS = #' S -- POUNDS DRY WEIGHT = P PM SOLIDS X 8.34 X MILLION MG GALLONS %,14 SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NLTbMER WQ0004222 DATE: - l i 17 SIGNATURE OF OPEERATOR: % SITE NO. IA-1 BA1`=HEALTHCARE CORP. IA-2 B AXTER HEALTHCARE CORP lA-3 BAXI'ER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN . ACRES 22.0 10.2 4.8 7.1 5.5 6.7 -WEATHER CONDITIONS: CLEAR PARTLY CLOUDY { CLOUDY.-;:, mm CONDITIONS: WET _ DRY:-- 1/ ROP: HAY l/ CORN .= -PASTURE ADS HAULED (6,000 GAL\LOAD) PUCATION SITE: - SITE AND FILED NO. rND FION FIELD NO. /� 2— GALLS ,Z-/OGC, #? E AS .-13 3s 'I')g AND FIELD NO. - GALLONS = #' S 4 AND Fir LD NO: - GALLONS �'Y WEIGHT = PPIM SOLIDS X 8.34 X 1-vIILLION MG GALLON % ! SLUDGE DISPOSAL, REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ 0042.22 DATE. - S GNA l QJ R 0177 Oi E111-1 O-,'?. SITE NO. ACRES IA-1 BA%-IER 1- EALTHCARE CORP. 22.0 IA-2 BAXTI ER HEALTHCARE CORP 10.2 1A-3 BAXTEP_ I EALTHI CARE CORP 4.8 2-2 HEiv-RY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY - .CLOUDY (3) SOIL CONDITIONS: WET DRY: , (4) CROP: HAY'- ' - .- PASTURE (S) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. _ _� GALLONS .:2Y C-0 b.. SITE AND FIELD NO. GALLONS - c. SITE AND -PULD -NO. --GALLONS POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MII,LION MG GALLONS #, s /3 q3S #' S #' S SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACMITY PERMIT NITER WQ0004222 DATE. SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY iCLO- -_ (3) SOIL, CONDITIONS: 'VET DRY: (4) CROP: HAY CORN PASTURE (S) LOADS HAULED (6,000 GAL�LOAD) (6) APPLICATION SITE: SITE AND FILED NO. ZA�— a. SITE AND FIELD NO. GALLONS � ecf0 #'SX.3 b. SITE AND FIELD NO. GALLONS #'S : c. SITE AND FIELD NO. GAi,LONS #'S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS 3 %� SLUDGE DISPOSAL. REPORT BA TER HEALTHCARE CORPORATION NORTH COVE FACILITY EM IT NUM13ER WQ0004222 DATE: SIGNATURE Cad' GRERATOR: SITE NO. ACRES IA-1 B_-\R HEALTHCARE. CORP. 22.0 IA-2 B AX T ER HEALTHCARE C ORP 10.2 1 A-3 B X TER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL. AVAILABLE. ACRES - - :.:_ ."72:9 :.. (I) METHOD OF APPLICATION:_ INJECTION SURFACE APPLICATION Z WEATHER CONDITIONS: CLEAR PARTLY CLOUDY LOTJ (3) SOLI. CONDITION S: WET DRY: (4) .CROP: HAY-. - ✓ CORN PASTURE- .. - (5) LOADS HAULED (6,000 GALILOAD) All (6) APPLICATION SITE: SITE AND FILED NO..: a. SITE AND FIELD NO. GALLONS,�j b. SITE AND:FIELD NO. - -GALLONS #'S c. SITE AND FIELD NO.-- -GALLONS"'.'-.:-----' #'S - - -- POUNDS DRY WEIGHT = PPM SOLIDS X 9.34 X MILLION MG GALLONS s SLUDGE DISPOSAL REPORT AXTER HEALTHCARE CORPORAT = NORTH COVE FACMIT PERMIT NUMBER WQ0004222 - DATE: 3/- cl% SIGNATURE Off' ORLRATOJT. . SITE NO. ACRES IA-1 BA -,"=ER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 B.AXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 - 5-1 b f ROM ENGLISH 9.1 5-5, b :ROM ENGLISH 7.5 . _TOTAL_AVAIL.;ABLE:ACRES-: -: ._�__-. 72.9 - (1) 14ZETHOD,OYAPPLICATION.-INJECTION : SURFACE APPLICATION .:i (2) WEAATHER CONDITIONS: CLEAR PARTLY CLOUDY . CL (3) _.SOIL-CONDTTIONS: WET DRY: -CROP: HAY"=: "<' ... - - .CORN PASTURE (5)�`LOADS HAULED (6,000 GALTOAD) [� (6).-- APPLICATION SITE: SITE AND FILED NO. - - - SITE AND FIELD NO.':.. : GALLONS avv #'S - -_ b. SITE'AND FIELD NO." .:GALLONS #' S : • _ _. = :: SITE AND FIELD NOS `- GALLONS: ##'S : POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS ^ .3 SLUDGE DISPOSAL RFPORT ExAt.XTER HEALTHCARE CORPORATION FIORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE: 9-7- q7 SIGNATURE OF �3 l ,ems SM tea-'-„'e'�,:��?%�'` •1 • � 1 }mot ^^✓.9 t t 1 1 1 • z..'."s" wml '� t »F t ` .•t. i � �,.v xr YL. 5c1r" �7� .mot s +� � � a c ,.ry.s �o,t r•a-o"- :kt -'7` n u�+'} ..r���y��`.. �,�'k•y� x, = `Lr.2� t'.�`9 , 4 �'sS-t. � �r e � u+'�"�' ' � SLUDGE DISPOSAL REPORT BAX'-.PE'R HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE: F 9:7-'�7 .SIGNA7V RE OF GPERA MR SITE, NO. ACRES lA-1 B - —I Et ALTHCARE CORP. 22.0 IA-2 BAX—,rER ALTHC:-ARE CORP 10.2 IA-3 BA R z'lEA .T=+-iCARE CORP 4.8 2-2 HEM-:Y BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 -' (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. / GALLONS S b. SITE AND FIELD NO. GALLONS #' S c. SITE AND FIELD NO. GALLONS #I S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS ��,� 75 �.-.. s ; i f SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUM3ER WQ0004222 DATA. S'IGNATUPE OF OPERATOR � SITE NO. ACRES 1A-1 BA-KTFR 1H LTHC.4RE CORP. 22.0 1 A-2 BAXTER �IEALTHCARE CORP 10.2 IA-3 BAXTER-EEALITHCARE CORP 4.8 -2 HENRY BROWN 7.1 2-5 HENRY BROWN . 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES (1) IYIETHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR _ CLOUDY (3) SOIL CONDITIONS: WET 72.9 PARTLY CLOUDY DRY: r/ _tea, (4) CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 G_4LILOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. i/r' �� GALLONS 12i)PJ #'S ® b. SITE AND FIELD NO. GALLONS �- #'S c. SITE AND FIELD NO. GALLONS #IS POUNDS DRY WEIGHT = PPIM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER BER Q0004222 SIGNATURE OF OPERA TO--'?: SITE No. ACRES IA-1 B AXTER HEALTHCARE CORP. 22.0 IA-2 BAXTER FEALTHC. RE CORP 10.2 IA-3 BA -1'LRiIEALiHC.ARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4--4 b DEAN CHAPMAN 6.7 (2) WEATHER CONDITIONS: CLEAR _ CLOUDY ;- (3) SOIL CONDITIONS: WET PARTLY CLOUDY Z� DRY: (4) CROP: HAY CORN PASTURE (S) LOADS HAULED (6,000 GALILOAD) 3 {6)- APPLICATION SITE: SITE AND FILED NO. - - a. SITE AND FIELD NO. GALLONS YO #'S 13 ?Y5 b -SITE AND.FIELD NO. GALLONS #'S - r 6 SITE A,biD FOLD NO. GALLONS Mz i4K7 *` Pt?UINDS DRY'WEIGH T = PP-vT SOLIDS X 8.34 X MILLION MG GALLONS 7 �� �3 � � ',;Zr, 67 ' SLUDGE DISPOSAL REPORT BAXTER HEALTHCARIE COIQPORATIOId YdOfl2TH COVE FACFE.ITY ail ��'4i�IT ER WQ0�4222 DATE: �"" SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BA XTIER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 (2) WEATHER CONDITIONS: CLEAR — CLOUDY (3) SOIL CONDITIONS: WET J PARTLY CLOUDY ..DRY: (4) CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION.SITE: ' SITE AND FILED NO. a. SITE AND FIELD NO. GALLONS �1�U b. SITE AND FIELD -NO. GALLONS c. SITE AND FIELD —NO., GALLONS #1S/3 �yS #, S #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT BAXT ER HEALTHCARE CORPORATION NORTH COVE FACMIT'Y P PERMIT NUM13ER WQ0004222 SIGNATURE OF OPERATOR: SITE NO. ACRES 1A-1 BARTER i-MALTHCARE CORP. 22.0 1A-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORD 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 (3) SOIL, CONDITIONS: WET DRY: / () 4 CROP: HAY CORN PASTURE / (S) LOADS HAULED (6,000 GALILOAD) 6() APPLICATION SITE: SITE AND FILED NO. ` a. SITE AND FIELD NO.' GALLONS ) #' S 6 3 b. SITE AND FIELD NO. - GALLONS #' S c. SITE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X NU LLIbOa MG GALLL`03Sys'_ ���,} ' SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE COY2POI2ATIOYV NORTH. COVE FACILITY PERMIT N�Tfl�EF2 WQ 4222 DATE: �S �,T SIGNATURE OF OPERATOR: SITE NO. 1 A-1 BAXTER HEALTHCARE CORP. 1A-2 BAXTER HEALTHCARE CORP IA-3 BAXTER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN ' 5-1 b 5-5 b DEAN CHAPMAN ROM ENGLISH ROM ENGLISH ff"re-6m. 22.0 10.2 4.8 7-1 5.5 6.7 9.1 7.5 TOTAL AVAILABLE ACRES 72.9 v _(I) METHOD OF APPLICATION: INJECTION - SURFACE APPLICATION 2 WEATHER CONDITIONS: CLEAR — / PARTLY CLOUDY () _... - CLOUDY (3) SOIL CONDITIONS: WET (4) CROP: HAY'. COIGN (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. DRY: c/ PASTURE. a. SITE AND FIELD NO. 2 GALLONS d b. SITE AND FIELD NO. GALLONS c. SITE AND FIELD NO.° GALLONS POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X IVIILLION MG GALLONS #' S IV T UDGE DISPOSAL RETORT .B°I'E HEALTHCARE CORPORATION NORTH COVE FACILITY PEM, IIT D ER WQ0004222 DATE: SIGNATURE OF OPERA TOR: SITE NO. ACRES 1A-1 BAX—J--R,--i ALL-HCARE CORP. 22.0 R � 71 THCARE CORP 10.2 IA-2 B'Lir IA-3 BAIT ER 1 cf T,TI-ICARE CORP 4.8 2-2 i-!E-"\T Y B1?10�'i-N 7.1 2-5 HENRY BROWN 5.5 4-4 b 'DEAN CHAPMAiN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES (7) METHOD OF APPLICATION: INJECTION - SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR _ CLOUDY (3) SOIL CONDITIONS: WET (4) CROP: HAY (5) LOADS HAULED (6,000 GALILOAD) 9.1 7.5 PARTLY CLOUDY DRY: PASTURE (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. 2-- GALLONS #'S / Sa b. SITE AND FIELD NO. GALLONS #' S c. SITE AND FIlLD NO. GALLONS #'S POUNDS DRY 'WEIGHT = PPM jOLIDS X 8.34 X _-NU LION MG GALLONS /aaS'l�`�QO Y�� SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATA. �- /6^i-,-� (7 ]� j �yT7J ]' g /� 0 � T DCJ i.3��17�1 Vd� �1'�'V'�dd-i.�� �3�. SITE NO. ACRES 1A-1 BAX! R PLEALTHCARE CORP. 22.0 IA-2 BA;�ER HEALTHCARE CORP 10.2 lA-3 BA,.'TER HEALTHCARE CORP 4.8 -2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 (?) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY UDY- (3) SOIL CONDITIONS: WET DRY: (4) -CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (b) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. - GALLONS •2` . d)73 #IS b. SITE AND FIELD NO. GALLONS #IS c. SITE AND FIELD NO. GALLONS' #' S - - - POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACMITY PET IT NUM13ER WQ0004222 DATE. -f � ' 7 SIGNATURE OF OPERATOR: SITE NO. 1A-1 BA�"TER HEALTHCARE CORP. IA-2 BAXTER HEALTHCARE CORP 1A-3 BAXTER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN ' 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH (2) WEATHER CONDITIONS: CLEAR_ CLOUDY (3) SOIL CONDMONS: WET (4) CROP: HAY_ CORN (J) LOADS HAULED (6,000 GALILOAD) 22.0 10.2 4.8 7.1 5.5 6.7 9.1 - 7.5 PARTLY CLOUDY DRY: PASTURE (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND' FIELD NO. f i2 GALLONS,9 y� #' S b. SITE AND FIELD NO. GALLONS #IS c. SITE AND 7FIELD NO. GALLONS #7S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X. MILLION MG GALLONS SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY - PERMIT NUMBER WQ0004222 DATE: �' / -� �)r IAlz SIGNATURE OF OPERATOR SITE NO. 1A-1 BAXTER HEALTHCARE CORP. IA-2 BAXTER HEALTHCARE CORP IA-3 BAXTER HEALTHCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN CLOUDY (3) SOIL CONDITIONS: WET DRY: AC E►S` 22.0 10.2 4.8 7.1 5.5 6.7 (4) CROP: HAY CORN PASTURE (S) LOADS HAULED .(6,000 GALILOAD) t (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. GALLONS 2�_ #IS b. SITE AND FIELD NO. GALLONS #IS c. STTE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X N ULLION MG GALLONS ����� SLUDGE DISPOSAL REPORT EIM R HEALTHCARE CORPORATION NORTH COVE FACILITY- PERMIT IVT3 ER WQ0004222 DATE: - ,SIGNATURE OF OPERATOR: 0� SITE NO. ACRES IA-1 BANTER HEALTHCARE CORP. 22.0 IA-2 BARTER HEALTHCARE CORP 10.2 lA-3 BANTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 r (2) WEATHER CONDITIONS:. CLEAR PARTLY CLOUDY z CLOUDY-� SOIL CONDITIONS: WET DRY: (4) ..CROP: -.HAY - , ' . CORN- = :. ____ . ` PASTURE - 5) LOADS HAULED (6,000 GAL`LOAD)l (6) APPLICATION SITE:. SIy'E'.AND =D'NO. SITE AND FIELD NO - A' - - GALLONSS/, Dd #' S- _. b:: SITE AND FIELD NO: - , - - -. GALLONS _ # S °-- -- _ -.: SITE AND FIELD NO:: :GALLONS, = .... �.. :: - Vs" POUNDS DRY WEIGHT' PPM SOLIDS X 8.34 X MILLION MG GALLONS � �3 � ���� l as n'?,v 9X//;r _ - SLUDGE DISPOSAL REPORT RAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY'PERMIT NUMBER W 0004222 DATE: SIGNATURE OF OPERATOR: .SITE NO. ACRES IA-1 BA,=R HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAIXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY � ill OUDY -� Y - (3) SOIL CONDITIONS: WET DRY (4) CROP: HAY ---•. - - CORN - : PASTURE (�) LOADS HAULED (6,000 GALILOAD) (6) -APPLICATION SITE: SITE AND FILED NO. — - r Z. a.. STTE=AND FIELD NO.''= GALLONS `l/�d°� :.I b. SITE AND _FIELD NO. - -L ... :.: GALLONS 1 #I S =. SITE ANFIEIiID;NO:=-_ .: -:. _... D' _:.; :;_GALLONS -.-. #,S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT ` . BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT DER WQ0004222 DATE.- SIGNATURE- � SITE NO. ACRE` IA-1RT�ALTHCARE CORP. 22.0 IA-2 BAXiER 1-IEALTHCARE CORP 10.2 IA-3 BAXTER CORP 4.8 2-2 HENvRY BROWN 7.1 2-5 HP,NRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 (4) CROP: ' HAY CORN (5) LOADS HAULED (6;000 GALILOAD) PASTURE (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. ' GALLONS �y�a b. SITE AND FIELD NO. GALLONS c: SITE AND KELD NO.- GALLONS POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS�� a 0o2Y� � SLUDGE DISPOSAL REPORT 13AXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUN3ER WQ0004222 DATE: SIGNAYVRE OF OPERATOR: SITE NO. ACRES 1A-1 BA:r ir-R-HEALTHCARE CORP. 22.0 IA-2 B AX 17,R -HE ALTHCARE- C 0RP 10.2 IA-3 BANTER HEALTHCARE CORP 4.8 2-2 HENRY BROWNN 7.1. 2-5 HENRY BROWN 5.5 4-4 b DEAI�t CHAPMAN 6.7 5-I b ROM ENGLISH 9.1 ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES _ 72:9 - - .4.ztiFx., . n 1 :� 'ta'� "c --=-�.�.�,e+ ";':> ✓. { tom-^.-- _ r ry J _ .a (I)' --METHOD OF APPLICATION : 'INJECTION - SURFACE`APPLICATION :-' (2) WEATHER CONDITIONS: CLEAR t/ PARTLY CLOUDY CLOL-DY_ ' (3) SOIL CONDMONS: WET DRY: (4) CROP: HAY_..'y CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) -APPLICATION STTE: SITE AND FILED NO. _ - ':: - - a. SITE AND FIELD NO."GALLONS d�U ` : #' S b. SITE AND FIELD NO. �1 = GALLONS #' S C. SITE AND FIELD NO. GALLONS POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS _, ys� �C7o�� ��v-3� ��. SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE PACMITY PERMIT NUN3ER WQ0004222 DATA': SIGNATU OF OPERATOR: SITE NO. ACRES iA-1 BAXTER iEALTHCARE CORP. 22.0 IA-2 BAR HEALTITICARE CORP 10.2 1A-3 BARTER HEALTHCARE CORD 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES 72.9 = (I) IM ETHOD OF APPLICATION: - INJECTION _ SURFACE APPLICATION (2) FEATHER CONDITIONS: CLEAR / PARTLY CLOUDY ----CLOUDY. () 3 SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN PASTURE L (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO, GALLONS �yi a #' S 13 ff a 3 b. SITE AND FIELD NO. GALLONS #' S c. SITE AND FIELD NO. GALLONS POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X NULLION MG a UDGE DISPOSAL, REPORT BARTER HEALTHCARE CORPORATION_ NORTH COVE FACMITY PERMIT YUMBER WQ0004222 SIGNATURE OF OP-F -TOR: SITE NO. ACRES lA-1 B.AXTER HEALTHCARE CORP. 22.0 IA-2 B A-XER HEALTHCARE CORP 10.2 1A-3 BA-:KTER HEALTHCARE CORP 4.8 2-2 HENRY BROWNT 7.1 2-5 HENRY BROWN 5.5 I 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES )_' i�T'HOD:OF;APPLICATION -_-INJECTION;- . - SURFACE-APPLICATTON SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUER WQ0004222 DATE: SIGN,4—TUP, OF 0 E 4 T 0J?: r SITE INTO. A C S T IA-1 B a2 tP_ .P=-=HCARE CORP. 22.0 IA-2 BA1�ER -HEALTHCARE CORP 10.2 1 A-3 3AXi ER IHEALTHC ARE. CORP 4.8 2-2 HE'-� 1+i Y BR01; N 7.1 2-5 HENIRY BROWN 5.5 4-4 b DEAN CHAPNLAN (2) WEATHER. CONDITIONS: CLEAR_ CLOUDY (3) SOIL CONDITIONS: WET (4) CROP: HAY CORN 6.7 PARTLY CLOUDY DRY: PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AIND FIELD NO. �_ GALLONS #'S b. SITE AND FIELD NO. GALLONS #IS c. SITE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS /6 c� �1,�3f�X /Z�6- SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT i7J ER Q0004222 DATE: �-17-47 SIGNA TURE OF OPEWATOR: SITE NO. ACRES 1 A-1 B-A=TER HEALTHCARE CORP. 22.0 IA-2 BAXTER H—EALTHC ARE C0RP 10.2 1 A-3 BAX i ER 1HEALTTriC AR.E CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEANI CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES - (1) : METHOD OF APPLICATION: INJECTION SURFACE APPLICATION 6.7 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY _ = CLOUDY. (3) SOL-L CONDITIONS: WET DRY: ; (4) CROP: HAY CORN (5) LOADS HAULED (6,000 GALILOAD) PASTURE (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. -- GALLONS #'S / b. SITE AND FIELD NO. GALLONS #' S c. SITE AND FIELD -NO. GALLONS #'S POUNDS DRY WEIGHT = FPM SOLIDS X 3.34 X MILLION MG GALLONS Sa 5 a�Y BAXTERlb2rU:iALTHCARE O O NORTH COVE FACILITY SIGNATURE OF OPERATOR: OR: IV SITE No. ACAS 11 IA-1 BA,=R IMALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 (1) i�TR�I2 ®F APP: ,SURFACE APPLICATION .=_ 2 WEATRER'CONDTTIONS: CLEAR PARTLY CLOUDY SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUM13ER WQ0004222: DATE: fd -1-2 3- 2 7 SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BA,=R HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 B AFTER HEALTHCARE C ORP 4.8 2-2 HENT R Y BROWN 7.1 2-5 HENRY BROWN 5.5 4=4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 =5b;___.:::::;;:: _...ROM ENGLISH = - 7.5:__ - _ - :TOTAL; AVAi1JABLEJAGRES 72.9 _- _ _ p*-��+n�1'?:a,�.yai� +s .�`r-:r .. ���ra�i-_r�ss�r�z.;.-'--.-eA �n-x--•� -f+ �.,-�.o-,-xti, .+«,,�q.•q-'�r.:�.3F-- �J- � � �;er�' 11 - _4 , (1) METHOD OF P.LICATION: ;INJECTION -SURFACE'A.PPLICATION WEATHER --CONDITIONS: CLEAR -- PARTLY CLOUDY-:-:= (3) SOIL CONDITIONS: 'WET. - - DRY:`= _ - -- 4 - =- - - `- - _ - .. PASTURE O. OP•.y:HAY.' CORN - - (S) LOADS HAULED: (6,000 GALILOAD) -• (6)-APPLICATI®N: STTE , SITE AND FILE NO ...5_Ls_.:.: � fig se.._-:._.- _: -,---; .--le- ,,v. s-•�t� _ _ _ - -- _ - - - . _ :..:. _ - a: STTE AND FIELD NO . F = - GALLONS �.`t� d#'S - _�.— b SITE-AND`FIELD: NO _ __ GALLO - _ SITE ANC FIELD= O _ - = _ -. - :GALLONS: , ..-- = _.#IS- :. POUNDS DRY WEIGHT PPM SOLIDS X 8.34 X MILLION MG GALLONS G'Y� SLUDGE DISPOSAL REPORT AXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT YUMBER WQ0004222. DATA': /1"', SIGNATURE OF OP1'RATOR: l SITE NO. ACRES 1A-1 BAX-17-:R HE ALTHCARE CORP. 22.0 IA-2 B Axe R E ALTHC.ARE C ORD 10.2 1 A-3 BAD i ER i�c��.LTHCARE CORP 4.3 2-2 INN Y BROWN 7.1 2-5 HENRY FROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 (2) WEATHER CONDITIONS: CLEAR (3) SOIL CONDITIONS: ' WET (4) CROP: HAY r/ CORN PARTLY CLOUDY DRY: �% PASTURE (5) LOADS HAULED (6,000 GAL\LOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. -� GALLONS o cJ #, S b. SITE AND FIELD NO. GALLONS #IS c. SITE AND FIELD NO. GALLONS #IS POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS 4 OY SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE: SIGNATURE OF OPERATOR: ,SI E NO. ACRES 1A-1 BARTER HEALTHCARE CORP. 22.0 IA-2 BARTER HEALTHCARE CORP 10.2 IA-3 BA."TER HEALTHCARE CORD 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 - 5-5 b ROM ENGLISH 7.5 =-...TOTAL' AVAIIr L:72.9' - _ - - /- - N -—�i�.yy_r - � ..iF-:,n: m' .;+::-._ve. .__'^: �..`<r S..i6 :u��.:'1R.i�J=zl�•1'i. aRw<_ _ }.. 1 J1 �METU[®I)_OFAPPLI..CATION: INJECTi®N - - ... � SURFACE APPLICATION- .. .. _ . - ......7. .. SITE AND FIELD NO::::_:' L GALLONS";/d S —_ b..: SITE AND FIELD NO.. GALLONS #' S c. SITE AND FIELD NO. - , G . ALLONS � #'S . POUNDS DRY'WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLON �� DATA: SLUDGE DISPOSAL, REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERAUT DER W00004222 f ' - /%f�/ SITE NO. Jv I ACRE IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 �irJ •v iJA ili2Si1 \..+V1\LLi1V1\V. vi++-+i aim -------^ --- -- — , -...:. __. CLOUD - - _ (3) SOIL CONDITIONS. WET DRY: (4) CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO.Z4�/ ' a. SITE AND FIELD NO. :- GALLONS-Apl� b. SITE AND FIELD NO. GALLONS c. SITE AND FIELD NO.: GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONSfs SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY = PEM IT NUMBER WQ0004222 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES 1A-1 B_A TERrir.ALTHCARE CORP. 22.0 IA-2 BAX I -ER HEALTHCARE CORP 10.2 1 A-3 BAX i ER T--lE.ALTHC.kRE C0RP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH 7.5 OTAL AVAILABLE ACRES - - - - - = - 72.9.- — _ �- - 1),j THOD OF APPLICAT ON: INJECTION - -_ --__ -`SURFA.CE-APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY (3) ,SOIII:CONDIIIONS-:- WET s -DRY: - ✓ - -- - ___ . (4) .CROP: HAY'" CORN: :.PASTURE (5) :LOADS HAULED (6,000 GALILOAD) (6) APPLICATION SITE: SITE AND FILED NO. - tco y -'SITE AND FIELD �NO.::=-`` GALLONS .`v2 b #'S _ b SITE:AND FIELD NO. GALLONS #'S . c. STIE_AND FIELD=NO.. -: ;:: GALLONS = - _ #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS 3 - SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION - NORTH COVE FACILITY. := PERMIT ER � ®®®4222 ' 3l1�SY131 ltl 1! 6lYJ3L1i 49 �!G T6l+6 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES T IA-1 B A.XTER i-lEALTHC ARE CORP. IA-2 B AX T ER HEALTHCARE CORP IA-3 BAXTER HE.,XJ—THCARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b _ DEAN CHAPMAN - 5-1 b _' ROM ENGLISH _ ..--5-5 b:.=_.:.::- .-::;:;._.::;ROM_ENGLISH-=- =:TOTAI AVAII ABLE=ACRES (2) WEA=R.CONDITIONS:...CLEAR= t/ - PARTLY, -CLOUDY zrs_ -i' - � � ,.-.v., ,. .--- ems.. `� *� '�- ''�-S ra1a T _ ' •Kia.� . �- XN • �- �r ,c sxi .0 ._:.:..-.. .....•:..-.-:::..�.:.�. .-. �'........ w.._-.-v... .._...-. _. �-• ___.__�__. .-a :F.. ..-.�.?�.-aw�_1-� .hic_t.2�—. .L - '. tia-aaz _.. ._t U-- =-• - - (3) SOIL CONDITIONS." WET.' ` = _.__.DRY: _ 4 CROE = HAS':' :. CORN : - - - _ O :- - - - - - (5) " LOADS HAULED (6,000 GALII.OAD) - _- (6} °APPLICATION SITE==aSITE_AND FILED NO. l -- .._y- r {/ - --2 .-� •�Y :�� T � . .ate.. ..__. .'.-: '_' _ i_ .- ••u sS GALLONS #,.,� ADFIELD`SITE NO _ - b.:-. SITE AND FIELD NO = :; - - _ GALLONS - _ . ;a : S� c STTEID =AN'FLELD'NO. GALLONS - - - #_ S POUNDS DRY WEIGHT:= PPM SOLIDS X 8.34 X MILLION MG GALLOl SS..., a9' 9j SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PEST DER WQ0004222 DATE: //l SIGNATURE OF OPERATOR: V_�1cev SITE NO. ACRES 7 IA-1 BAXTERriEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 1A-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY -st Z F (3) SOIL- CONDITIONS: WET DRY: 4 CROP:' HAY CORN PASTURE a/ _ (S) LOADS HAULED (6,000 GAL\LOAD) (6) APPLICATION SITE: SITE AND FILED NO. �� - -- -- a. SITE AND'FIELD NO. GALLONS rZ U # S4_- b.. SITE AND FIELD NO. GALLONS #, S - _ - c. SITE AND FIELD NO. GALLONS-: #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS SI,IJDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILI'I`Y PERMIT NUMBER VVQ0004222 DATE SIG,-VATURE OF OPEP,4 TOR: SITE NO. ACRES IA-1 BAXiER HEALTHCARE CORP. 22.0 IA-2 B AXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAP -MAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b,-- ROM ENGLISH -- 7.5 ...... - ... . TOTAL -AVAIL := - ::. __._ _ ..- :_ ..:::: = 729 _ - _ INJECTION ... - . -- _ -_ - -- -- (1),•MXTHOD, OF APPLICATION: - SURFACEAPPLICATION (2) WEATHER CONDITIONS:. CLEAR PARTLY CLOUDY - - _ - (3) SOIL CONDITIONS: WET - DRY:, (4) CROP: HAY :-.. - .: CORN (5) _LOADS HAULED (6,000 GALILOAD) _ ... (6) APPLICATION SITE: SITE AND FILED NO. - - : - - a. SITE AND FIELD NO. GALL 01il, _All` b.. SITE AND FIELD NO. - - GALLONS c. SITE AND FIELD NO. _ _ : - GALLONS .. #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS 71`1 SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUM3ER WQ0004222 DATE: Z SIGNATURE OF OPEP,4 TOR: SITE NO. ACRES IA-1 BAf=P, HEALTHCARE CORP. 22.0 IA-2 B AXTLER HEALTHCARE CORP 10.2 IA-3 BARTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 SURFACE APPLICATION (2) WEATHER CONDITIONS: - CLEAR PARTLY CLOUDY CLOUDY" . (3) SOIL CONDITIONS: WET DRY:. (4) CROP: HAY CORN PASTURE 7 (5) LOADS HAULED (6,000 GAL\LOAD) (6) APPLICATION SITE: SITE AND FILED NO. SITE AND FIELD NO. "GALLONS /od #IS b. -SITE AND :FIELD NO. GALLONS #'s c. SITE. AND FIELD NO. GALLONS POUNDS DRY WEIGHT = DLPM SOLIDS X 8.34 X INULLION MG GALLONS SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY.",` PERt-dIT NUMBER WQ0004222 . - DATE: c SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 BAXILTR HEALTHCARE CORP 10.2 lA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b 5-5 b :TOTAL AVMI (2) INJECTIONZ, SURFACE APPLICATION WEATHER CONDITIONS: _ CLEAR PARTLY CLOUDY RR ` _ " � •.:ya.. o . aa. s r � r - - -s �s*r+ .c-.r,.... - w.s (3) SOIL CONDITIONS WET DRY. (4) CROP: _HAY= _.: r._ -CORN: PASTURE - (5) LOADS HAULED (61,000 GAL\LOAD) (b) APPLICATTON SITE: -'SITE AND FILED NO. SITE AND FIELD NO: - - GALLONS*� = b. SITE AND FIELD NO..: - - GALLONS ., ..- --- c.. SITE AND. F'IEL.D NO. - . GALLONS - -_ #'. S r:- POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER W00004222 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES 1A-1 BARTER IqEALTHCARE CORP. 22.0 IA-2 BA,XTER HEALTHCARE CORP 10.2 IA-3 BA TER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7•5 TOTAL `AVAILABLE -ACRES = _. '.'4i."wi. - _ _ - al-'lYie•..s..._:a:.;.`i.-'t.�:..._' .__ _ _ _ P:c...'r.•—_":.T=�'': .Y`i-:t•-:�^.t,= _ - - _ ..3.r.--.e.--5 _ _ - (�) METHOD: O� APPLICATION -,.INJECTION-: -- -_ - ;. SURFACEAPPLICATION <x (2) WEATHER CONDITIONS:. CLEAR - - �PARTLY CLOUDY (3) SOIL CONDITIONS: -- WET DRY: (4), CROP:HAY CORN PASTURE . _..:. :.. 6 000 GAL\I,OAD (S) LOADS HAULED (6,000 } -. (6) APPLICATION SITE: SITE AND FILED NO. ` a SITE AND -FIELD NO. - GALLONS : `s # 1S b. SITE AND FIELD NO. - GALLONS'S: c. SITE AND FIELD NO: GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY - PERMIT INT ER WQ0004222 DATE: X7 SITE NO. O. ACRES IA-1 B,-X i R �EALTHC AR.E CORP. 22.0 1A-2 B, XTEER11-1FALTHC'RE CORP 10.2 IA-3 B A.`--_ 1 ER iir.ALTHC ARE CORP 4.8 2-2 HE'��RY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN PASTURE (5) LOADS HAULED (6,000 GAL\LOAD) (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. /Q _ GALLONS yQ °y #' S b. SITE AND FIELD NO. GALLONS #'s c. SITE AND FIELD NO. GALLONS - #'S " ;' POUNDS DRY WEIGHT = DP -NI SOLIDS X 8.34 X IHLLION MG GALLONS� SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY - PERMIT tVMER WQ0004222 DATE: SIGNATURE OF OPERA TOR: SITE NO. ACRES IA-1 BA1XIE13, HEALTHCARE CORP. 22.0 IA-2 BAXTER HEALTHCARE CORP 10.2 IA-') B AX i ER liE.UTTrIC ARE CORP 4.8 2-2 HENTRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b I DEAN CHAPMAN 6.7 .; (2) WEATHER CONDITIONS: CLEAR .--PARTLY CLOUDY CLOUDY- - - (3) SOIL CONDITIONS; WET DRY: 1.(4) . CROP: HAY CORN. PASTURE- (5) LOADS -HAULED (6,000 GAL\LOAD) ` (6) APPLICATION SITE: SITE AND FILED NO: a: - STTE AND FIELD NO. GALLONS #' S. b.:;:SITE AND FIELD -NO.- . GALLONS #'S SITE AND FIELD NO. � GALLONS :: = #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS D 3 0 SLUDGE DISPOSAL REPORT BAXTER HEALTHCARE CORPORATION NORTH COVE FACILITY PEMAMT NUMBER WQ0004222 DATE: %) — ;2' F �, SIGNATURE OF OPERATOR: ► lTE NO® IA-1 BAX-IT-RrT'r.ALTHCARE CORP. IA-2 BAXTER HEALTHCARE CORP !A-3 BAXTER HEAT THC ARE CORP 2-2 HENRY BROWN 2-5 HENRY BROWN 4-4 b DEAN CHAPMAN 5-1 b ROM ENGLISH 5-5 b ROM ENGLISH TOTAL AVAILABLE ACRES (1) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 72.9 ly (?) WEATHER CONDITIONS: CLEAR _ PARTLY CLOUDY CLOUDY (3) SOIL CONDITIONS: WET (4) CROP: HAY CORN (5) LOADS HAULED (6,000 GALILOAD) DRY: �� PASTURE (6) APPLICATION SITE: SITE AND FILED NO. % a. SITE AND FIELD NO. �� �_ GALLONS b. SITE AND FIELD NO. GALLONS #'S - c. SITE AND FIELD NO. GALLONS #'S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS 0 a?,K tFtZW- SLUDGE DISPOSAL REPORT BAXT R HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER W90004222 DATE: SIGNATURE OF OPERATOR: c` SITE NO. ACRES 1 A-1 BAXTER HEALTHCARE CORP. 22.0 IA-2 B AXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL AVAILABLE ACRES _ . 72.9 - , (I) METHOD OP APPLICATION:. INJECTION . SURFACE APPLICATION 2() WEATHER CONDITIONS:` CLEAR PARTLY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN (5) LOADS HAULED (6,000 GALTOAD) PASTURE (6) APPLICATION SITE: SITE AND FILED NO. z/4 - a. SITE AND FIELD NO. '2 GALLONS W ood #'S 6&Z, % b. SITE AND FIELD NO. GALLONS #' S c. SITE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8'.3.4 X MILLION MG GALLONS SLUDGE DISPOSAL REPORT[' BARTER HEALTHCARE CORPORATION NORTH COVE FACMITY . DATA: ,122-5-97 SIGNATURE OF OPERATOR: A,D SITE NO. ACRES IA-1 BANTER =ALTHC ARE CORP. 22.0 IA-2 B AX i ER HEA.LTHC ARE CORP 10.2 IA-3 BA TER HEALTHCARE CORP 4.8 ?-2 hTENT?Y BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 +O APPLICATION: - INJECTION . ` SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY (3) SOIL CONDITIONS: WET (4) CROP: HAY r/ CORN (5) LOADS HAULED (6,000 GALTOAD) DRY: PASTURE (6) APPLICATION SITE: SITE AND FILED NO. a. SITE ANb FIELD NO. GALLONS #'S oZ/f7� b. SITE AND FIELD NO. GALLONS #IS - c. SITE AND FLELD NO.' GALLONS #' S . POUNDS DRY WEIGHT = PPM SOLIDS X-8.34 X MILLIO MG GALLONS c� 63 SLUDGE DISPOSAL REPORT BAXTEH HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUKBER WQ0004222 DATE: SIGNATURE OF OPERATOJ?: SITE NO. 1A-1 BAXTERHEALTHCARE CORP. IA-2 BARTER HEALTHCARE CORD lA-- BARTER HEALTHCARE CORP 3_2 HENRY BROWN 2-5 HENRY BROWN, 4-4 b DEAN CHAPMAN 5-1 b ROM ENGLISH - 5-5 b ROM ENGLISH 22.0 10.2 4.8 7.1 5.5 6.7 9.1 7.5 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN (5) LOADS HAULED (6,000 GALILOAD) PASTURE (6) APPLICATION SITE: SITE AND FILED NO. ' f ,4 - a. SITE AND FIELD NO. l GALLONS a<J� #' S b. SITE AND FIELD NO. GALLONS #IS c. SITE AND FIELD NO. GALLONS #' S -. POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS �. _ S�54p3 SLUDGE DISPOSAL REPORT BARTER HEALTHCARE CORPORATION NORTH COVE FACILITY PERMIT NUMBER WQ0004222 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BA=RHEALTHCARE CORP. 22.0 lA-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTERHEALTHCARE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 (2) WEATHER CONDITIONS: CLEAR PARTLY CLOUDY CLOUDY (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY CORN (5) LOADS HAULED (6,000 GALTOAD) PASTURE (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. �7 • GALLONS #' S b. SITE AND FIELD NO. GALLONS #' S c. SITE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X iVIa,LION MG GALLONS 1,76 SLUDGE DISPOSAY, REPORT BAXTEI2HEALTHCARE CORPORATION NORTH COVE FACYi.ETY PE3u°'rYIT NiTiViBEgt W90004222 DATE: SIGNATURE OF OPERATOR: SITE NO. ACRES IA-1 BA -`_TER HEALTHCARE CORP. 22.0 1A-2 BAXTER HEALTHCARE CORP 10.2 IA-3 BAXTER HEALTHCARE CORD 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH., 7.5 TOTAL AVAILABLE ACRES - y 72.9 (1) METHOD OF APPLICATION: INJECTION SURFACE APPLICATION ' () 2 WEATHER CONDITIONS: CLEAR y PARTLY CLOUDY CLOUDY _ (3) SOIL CONDITIONS: WET DRY: / (4) CROP: HAY (5) LOADS HAULED (6,000 GALILOAD) 5" PASTURE (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. LA d , GALLONS �,� #' S �d b. SITE AND FIELD NO. GALLONS #' S c. SITE AND FIELD NO. GALLONS #'S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X AULLION MG GALLONS y SLUDGE DISPOSAL REPORT Bz'LXTER HEALTHCARIE CORPORATION NORTH COVE FACILITY PERMIT NUMER WQ0004222 DA?'L: //i_ iS- �I . SIGNATURE OF OPEJ TOR: SITE NO. ACRE, IA-1 B R l=A THC.-.RE CORP. 22.0 IA-2 B AX—IFER zIEALTHC ARE CORP 10.2 1A-3 BANTER =` ALTHC:-\RE CORP 4.8 2-2 HENRY BROWN 7.1 2-5 HENRY BROWN 5.5 4-4 b DEAN CHAPMAN 6.7 5-1 b ROM ENGLISH 9.1 5-5 b ROM ENGLISH 7.5 TOTAL. AVAILABLE ACRES 72.9 - (I) , METHOD OF APPLICATION: INJECTION SURFACE APPLICATION (2) WEATHER CONDITIONS: CLEAR J PARTLY CLOUDY .CLOUDY - (3) SOIL CONDITIONS: WET DRY: (4) CROP: HAY COMN PASTURE (5) LOADS HAULED (6,000 GALILOAD) ` (6) APPLICATION SITE: SITE AND FILED NO. a. SITE AND FIELD NO. - GALLONSX- MO #' S b. SITE AND FIELD NO. GALLONS #'S c. SITE AND FIELD NO. GALLONS #' S POUNDS DRY WEIGHT = PPM SOLIDS X 8.34 X MILLION MG GALLONS 1997 % BAXTER HEALTHCARE CORPORATION (PASTURE FESCUE) SITE 1A-1 22 ACRES DATE GALLONS mg/I D.W.Ibs. 1/27/97 6,000 14,280 715 2/7/97 24,000 12,494 2,501 5/29/97 24,000 17,517 3,506 6/6/97 24,000 18,087 3,620 6/7/97 24,000 18,087 3,620 9/27/97 12,000 12,243 1,226 10/2/97 24,000 12,243 2,451 10/7/97 24,000 13,023 2,607 10/13/97 24,000 12,509 2,504 10/16/97 : 24,000 12,509 2,504 10/17/97 24,000 12,509 2,504 10/21/97 6,000 12,509 626 10/23/97 24,000 12,509 2,504 10/24/97 24,000 12,509 2,504 10/28/97 24,000 14,455 2,893 10/29/97 30,000 14,455 3,617 10/30/97 24,000 14,455 2,893 10/31/97 24,000 14,455 2,893 11/7/97 24,000 15,842 3,171 11/17/97 24,000 20,184 4,040 ` 11/18/97 24,000 20,184 4,040 11/20/97 24,000 20,184 4,040 11/21/97 18,000 20,184 3,030 12/2/97 24,000 21,997 4,403 TOTALS GALLONS % SOLIDS D.W. lbs. JAN 6,000 1.43 715 FEB 24,000 1.25 2,501 MAY 24,000 1.75 3,506 JUNE 48,000 1.81 7,240 SEPT 12,000 1.24 1,226 OCT 276,000 1.33 30,500 NOV 114,000 1.93 18,321 DEC 24,000 2.2 4,403 528,000 68,412 34.21 TONS 1997 BAXTER HEALTHCARE CORPORATION (PASTURE FESCUE) SITE 1A-2 10.2 ACRES DATE GALLONS mg/I D.W.Ibs. 1 /27/97 12,000 14,280 1,429 1/28/97 24,000 14,280 2,858 1/29/97 30,000 14,280 3,573 1/30/97 24,000 13,466 2,695 1/31/97 18,000 13,466 2,022 2/2/97 24,000 13,539 2,710 2/3/97 18,000 12,494 1,876 2/5/97 24,000 12,494 2,501 2/6/97 24,000 12,494 2,501 2/10/97 30,000 11,333 2,836 2/11/97 30,000 11,333 2,836 2/12/97 24,000 11,333 2,268 2/13/97 24,000 11,333 2,268 2/18/97 24,000 13,215 2,645 2/19/97 30,000 13,215 3,306 2/20/97 24,000 13,215 2,645 2/21/97 18,000 13,215 1,984 2/25/97 24,000 15,539 2,710 3/5/97 24,000 18,258 3,654 3/6/97 24,000 18,258 3,655 3/11/97 24,000 18,700 3,743 3/13/97 24,000 18,700 3,743 3/18/97 24,000 18,230 3,649 3/21/97 24,000 18,230 3,649 3/27/97 24,000 18,230 3,649 3/28/97 24,000 18,230 3,649 4/3/97 24,000 16,378 3,278 4/4/97 18,000 16,378 2,459 5/12/97 24,000 16,296 3,262 5/13%97 24,000 16,296 3,262 5/19/97 24,000 17,517 3,506 5/20/97 24,000 17,517 3,506 5/27/97 24,000 17,517 3,506 6/10/97 24,000 18,087 3,620 6/12/97 24,000 18,087 3,620 6/13/97 18,000 18,087 2,715 6/24/97 24,000 12,807 2,563 7/8/97 18,000 12,807 1,923 7/10/97 24,000 13,935 2,789 7/15/97 24,000 13,935 2,789 7/17/97 24,000 13,935 2,789 7/22/97 24,000 13,935 2,789 7/25/97 24,000 16,361 3,275 7/29/97 24,000 16,361 3,275 7/31/97 24,000 16,361 3,275 1997 BAXTER HEALTHCARE CORPORATION (PASTURE FESCUE) SITE 1A-2 cont. 10.2 ACRES DATE GALLONS mg/I D.W.Ibs. 8/7/97 24,000 16,361 3,275 8/8/97 24,000 16,361 3,275 8/12/97 24,000 13,845 2,771 8/14/97 18,000 13,845 2,078 8/19/97 24,000 13,845 2,771 8/21/97 24,000 13,845 2,771 8/25/97 24,000 12,500 2,502 8/28/97 24,000 12,500 2,502 9/16/97 24,000 10,997 2,201 9/18/97 24,000 10,997 2,201 9/19/97 24,000 10,997 2,201 9/22/97 24,000 12,243 2,451 9/27/97 12,000 12,243 1,226 9/30/97 24,000 12,243 2,451 11/6/97 24,000 15,842 3,171 11/11/97 24,000 15,842 3,171 12/3/97 24,000 21,997 4,403 12/5/97 24,000 21,997 4,403 12/8/97 24,000 21,997 4,403 12/9/97 18,000 21,997 3,302 12/16/97 30,000 21,080 5,274 12/18/97 24,000 21,080 4,219 TOTALS GALLONS % SOLIDS D.W. lbs. JAN 108,000 1.4 12,577 FEB 318,000 1.25 33,086 MAR 192,000 1.84 29,391 APR 42,000 1.64 5,737 MAY 120,000 1.7 17,042 JUN 90,000 1.67 12,518 JULY 186,000 1.48 22,904 AUG 186,000 1.42 21,945 SEPT 132,000 1.16 12,731 NOV 48,000 1.58 6,342 DEC 144,000 2.17 26,004 1,566,000 200,277 100.14 TONS 1997 BAXTER HEALTHCARE CORPORATION (HAY FESCUE) SITE 2-2 TOTALS 7.1 ACRES DATE GALLONS mg/I solids D.W. lbs. 1/14/97 54,000 14,952 6,734 4/14/97 42,000 15,481 5,423 4/15197 42,000 15,481 5,423 4/16/97 24,000 15,481 3,097 5/1/97 30,000 15,382 3,849 5/2/97 42,000 15,382 5,388 5/5/97 36,000 14,160 4,251 5/6/97 42,000 14,160 4,960 JAN APR MAY GALLONS % SOLIDS D.W. Ibs. 54,000 1.5 6,734 108,000 1.55 13,943 150,000 1.48 18,448 312,000 39,125 19.56 TONS 1997 BAXTER HEALTHCARE CORPORATION (HAY FESCUE) SITE 2-5 5.5 ACRES DATE GALLONS ppm solids D.W. lbs. 1/15/97 42,000 14,952 5,237 1/20/97 60,000 16,528 8,271 1/21/97 42,000 16,582 5,789 1/22/97 48,000 14,280 5,717 1/27/97 18,000 14,280 2,144 TOTALS GALLONS % SOLIDS D.W. Ibs. JAN 210,000 1.55 27,158 13.58 TONS PER REQUIREMENT OF 11.4 LIME ADDITION IN 1997 The following lime additions were made in 1997: Site 1A-1 No lime required Site 1A-2 .5T acre Site 1A-3 No lime required Site 2-2 No lime required Site 2-5 .4T acre Site 4-4 No lime required Site 5-1 1AT acre Site 5-5 No lime required The following lime additions -are scheduled for 1998: Site 1A-1 No lime Site 1A-2 .5T acre Site 2-2 No lime Site 2-5 AT acre Groruer: Baxter Ilealthco PO Box 1390 Marion, NC 28752 Soil est Rohort ray m. --Nhffn� 11/26/97 SERVING N.C. CITIZENS FOR OVER 50 YEARS Yr T/A Crop or Year 1st Crop: Fes/OG/Tim,M 2nd Crop: McDowell Coun Corp. Copies to: Lime N R05 RO Mg Cu Zn .6T 120-200 0 0-20 0 0 0 C -- 12 Mn See Note 0 12 Test Results Soil Class HM% W/V CEC BS% Ac pH P-I . K I Ca% Mg% Mn-I Mn-AI (1)Mn-AI (2) Zn-1 Zn-AI Cu-I S-I SS -I NQj-N Mh-N Na MIN 0.6 1.23 7.1 85.0 1.1 5.2 125 70 54.0 26.0 269 178 119 119 188 63 0.1 l~�el°d Iriforni�.ti®n � . ,. 3.: .' X1eclLime ReconnmenclatYons, m , Crop or Year .....NNW Lime x r N R05 RO Mg Cu Zn B Mn z See Note Sample No. Last Crop Mo Yr T/A 12 Fes/OG/Pim,E 1st Crop: Fes/OG/Tim,M .3T 120-200 60-80 70-90 0 0 0 0 12 2nd Crop: Test Results Soil Class HM% W/V CEC BS% Ac pH P-I K I Ca% Mg% Mn-1 Mn-AI (1)Mn-AI (2) Zn-1 Zn-AI Cu-I S-I SS-1 N0,1-N AVh-N Na MIN 0.56 1.19 6.8 87.0 0.9 5.7 27 27 62.0 22.0 761 474 65 65 91 43 0.1 vie l ' Inftrrznation . , <•.:.. = hed Lmte Recorn nendationsgH Sample No. Last Crop Mo Yr T/A Crop or Year Lime N R05 RO Mg Cu Zn B Mn See Note 22 Fes/OG/I'im,E 1st Crop: Fes/OG/Tim,M 0 120-200 100-120 90-I10 0 0 0 0 12 2nd Crop: Test Results Soil Class IIM% W/V CEC BS% Ac pH P-I K 1 Ca% Mg% Mn-I Mn-AI (1)Mn-AI (2) Zn-1 Zn-AI Cu-1 S-1 SS -I NQj-N AU-N Na MIN 0.41 1.17 7.0 90.0 0.7 6.0 14 21 59.0 29.0 479 304 48 48 107 38 0.2 E'ield -lnforar ti cif i a l;i a n Ft. 5, b l-: -0i *ontYn ` riclati .1 . Sample No. Last Crop Mo Yr T/A Crop or Year Lime N R05 RO Mg Cu Zn B Mn See Note 25 Fes/OG/Pim,E 1st Crop: Fes/OG/I'im,M .3T 120-200 70-90 90-110 0 0 0 0 12 2nd Cro : Test Results Soil Class HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% Mn-I Mn-AI (1)Mn-AI (2) Zn-I Zn-AI Cu-I S-1 SS-1 NQf-N AVh-N Na MIN 0.51 1.14 6.7 88.0 0.8 5.7 25 22 56.0 31.0 444 283 47 47 108 64 0.2 Sample No. Last Crop Ho Yr T/A Crop or Year Lime N R05 KO Mg Cu Zta B Mn See Note 44 Fes/OG/ h-n,E 1st Crop: Fes/OG/I'im,M 0 120-200 80-100 100-120 0 0 0 0 12 2nd Crop: Test Results Soil Class HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% Mn-1 Mn-AI (1)Mn-AI (2) Zn-1 Zn-AI Cu-I S-I SS -I NQt-N AU-N Na MIN 0.76 1.25 7.7 92.0 0.6 6.1 19 14 63.0 29.0 318 206 55 55 155 26 0.1 J ? Field>Inforrnation .,, ^ ,.. lied %une n . attons. . Recomme `d" Crop or Year Lime ... , ..: N R05 K. 0 Mg Cu Zn 1 B Mn See Note Sample No. Last Crop Ko Yr T/A 51 Alfalfa, E 1st Crop: Alfalfa, M 1T 0.0 0 120-140 0 0 0 2.0 0 12 2nd Crop - Test Results Soil Class HM% W/V CEC BS% Ac pH P-I K I Ca% Mg% Mn-I Mn-AI (1)Mn-AI (2) Zn-1 Zn-AI Cu-I S-1 SS-1 NQt-N AU-N Na MIN 0.71 1.12 6.4 83.0 1.1 5.6 82 27 55.0 26.0 236 151 8 98 96 32 0.1 Field.XYlformatxon 11ed,:Lime Recornmeandatl011 ;- „.:.. '... .:, l S 4. .i x £ 3) ,ow Sample No. Last Crop Ho Yr T/A Crop or Year Lime N R05 RO Mg Cu Zn B Mn See Note 55 Fes/OG/Pim,E 1st Crop: Fes/OG/I'im,M 0 120-200 60-80 100-120 0 0 0 0 12 2nd Crop: Test Results Soil Class IIM°o W/V CEC BS°o Ac pH P-I KI Ca% Mg% Mn-1 Mn-AI (1)Mn-AI (2) Zn-I Zn-AI Cu-1 S-I SS -I NQ3-N NIA-N Na 0.51 1.6 7 6.4 27 1 63.0 30.0 227MIN 147 33 33 127 24 0.1 NCDA Agronomic Division 4300 Reedy Creek Rd Raleigh, NC 27607-6465 (9I)) 733-2655 k� T es t Report ' gr nuon.i UfiderstandingtheSo2 FORAGE/PASTURE CROPS(Crop Codes o40 oGo) Soil pH and the amount of line required for optimum yields are crucial parts of the soil test report. Low soil pH and low phosphorus cause more yield losses than any other factors in forage production. Excessive soil acidity (low pH) reduces the capacity of forage crops to Utllizc applied fertilizer nutrients. lime recommendations are based on pH, amount of acidity, and desired pH for the designated crop. Establishment and maintenance of legumes depend very heavily on maintaining the proper pH. For best results, recommended lino and fertilizer should be mixed into the top 6 to 8 --.inches of the soil before establishment. Although most foage crops show no response to r phosphorus and potassium above an index of 50, some fertilization will be recommended for certain crops. Recommendations for nitrogen, phosphorus and, potassium are for annual application. Depending on the crop, climate and soils, split applications of nitrogen and potassium may be required. Past experience, management level and economics will influence rates and time of application. For additional information, sec Note 12 "Forage and Pasture Crops" that accompanies your soil test report. The table below shows the relationship between soil test level and response to applied nutrients. Soil Test Index Crop Response to Nutrient Application Range Rating llbospbows Potassium Manki;anese Zinc Copper 0-10 Very Low Very High Very High Very High Very High Very High 11-25 Low High High high High High 26-50 Medium Medium * Medium "` None None None 51-100 High None Low -None None None None 100+ Very High None None None None None Abbreviations MIN mineral soil M-0 mineral -organic soil 0 ` 61vu is oil: IN% percent huniic matter W%V weight/vghilue of soil i3S% potent of CCC occupied by bases Ac acidity (decreases.as p1i increases) P-T p iospltorus index K-L potassium index Ca c lc.luni Mg magnesium mangaiiescindex Mn-Al ` manganese avahi6ility index /n I zuic.liilex 7n_Ai mnravnilalvlihrrrirtnr VU A S-I l.VI/FJL'1.I11UGh 'sulfur index SS-1 . soluble silt index; NO3 N nitrate nitrogen (ppin) Nisi N alninoiiitiiii nitrogen (ppm) N sodnun KO.potash P,05 pliosplia(e t3 6oron ` * Response decreases as soil test index increases. 20,000 copies were printed at a cost of $4.31.22 or $0.02 per copy. Pace Analytical Services, Inc. 54 Ravenscroft Drive a g G Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 February 07, 1997 Mr. Phil Castro Baxter Healthcare Corporation P.O. Box 1390 Highway 221 North Marion, NC 28752 RE: PACE Project No. A70122.602 Client Reference: Quarterly Dear Mr. Castro: Enclosed is the report of laboratory analyses for samples received January 22, 1997. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel free to contact us. Sincerely, Walter L. Miller Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive. Fare Anse#ical Asheville, NC28801 Tel: 704-254-7176 Fax: 704-252-4618 Baxter Healthcare Corporation P.O. Box 1390 Highway 221 North Marion, NC 28752 Attn: Mr. Phil Castro Client Reference: Quarterly PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter Units PRL INORGANIC ANALYSIS 8 RCRA METALS - LEACHATE February 07, 1997 PACE Project Number: A70122602 93 0338194 01/22/97 01/22/97 Digestor Sludge Leachate (1) Barium, Leachate mg/L 0.010 0.144 Cadmium, Leachate mg/L 0.010 0.013 Chromium, Leachate mg/L 0.010 ND Lead, Leachate mg/L 0.100 ND Silver, Leachate mg/L 0.005 0.057 Arsenic, Leachate mg/L 0.0050 ND Selenium, Leachate mg/L 0.0050 0.0779 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Asheville, NC28801 Tel: 704-254-7176 Fax:704-252-4618 Mr. Phil Castro February 07, 1997 Page 2 PACE Project Number: A70122602 Client Reference: Quarterly PACE Sample Number: 93 0338186 Date Collected: 01/22/97 Date Received: 01/22/97 Client Sample ID: Digester Parameter Units PRL Sludge INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Cadmium. mg/kg 33 ND Calcium mg/kg 330 13600 Chloride mg/kg 670 9470 Chromium mg/kg 67 80 Copper mg/kg 33 270 Corrosivity pH Units 0.1 6.8 Fecal Coliform in Solids by MPN MPN/g 13000 1100000 Lead mg/kg 330 ND Magnesium mg/kg 330 3500 Nickel mg/kg 170 ND Nitrogen, Ammonia mg/kg 67 310 Nitrogen, Plant Available mg/kg 1.0 24500 Phosphorus, Total mg/kg 170 3800 Potassium mg/kg 3300 3700 Sodium mg/kg 330 10000 Solids, Percent Total % 0.01 1.5 Sulfate mg/kg 2670 14100 Zinc mg/kg 33 370 SOUR TEST Sour test mg/g/hr 0.01 1.01 Solids, Total Suspended mg/L 1 20750 Solids, Total Volatile Suspended mg/L 1 18650 NITROGEN, TOTAL Nitrogen, Kjeldahl mg/kg 16700 76800 Nitrogen, Nitrate plus Nitrite mg/kg 330 1440 Nitrogen, Total mg/kg 17030 78240 • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. • LJ Pace Analytical Services, Inc. p 54 Ravenscroft Drive race t i c a 9 Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 Mr. Phil Castro Page 3 Client Reference: Quarterly These data have been reviewed and are approved for release. Diane M. Davis Supervisor, Laboratory Operations February 07, 1997 PACE Project Number: A70122602 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. Ease Anal lical 54venDrive Ashheeville,,NC 28801 Tel: 704-254-7176 Fax:704-252-4618 Mr. Phil Castro FOOTNOTES February 07, 1997 Page 4, for pages 1 through 3 PACE Project Number: A70122602 Client Reference: Quarterly ND Not detected at or above the PRL. PRL PACE Reporting Limit (1) All analysis performed on Toxic Characteristic Leachate. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive E a s e Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 February 07, 1997 Report No.: 00058660 Section A Page 1 LABORATORY ANALYSIS REPORT CLIENT NAME: BAXTER HEALTHCARE CORP. ADDRESS: P.O. BOX 1390 MARION, INC 28752- ATTENTION: PHIL CASTRO SAMPLE ID: 93 033818.6/ SLUDGE SAMPLE NO: H443725 SAMPLE MATRIX: SLUDGE LIMS CLIENT: 0719 0597 PACE PROJECT: A70122602 PACE CLIENT: 000593 P.O. NO: VERBAL DATE SAMPLED: 22-JAN-97 DATE RECEIVED: 24-JAN-97 PROJECT MANAGER: Katren Jenkins ------------------------------------------------------------------------------------------------------------------------------- TEST DILUTION LN ------------------------------------------------------------------------------------------------------------------------------- CODE DETERMINATION FACTOR RESULT UNITS 1 OVZHE Volat'iles - ZHE/Part 261 1,1-DichLoroethylene 1 < 0.005 mg/L 1,2-Dichloroethane 1 < 0.005 mg/L Benzene 1 < 0.005 mg/L Carbon tetrachloride 1 < 0.005 mg/L Chlorobenzene 1 < 0.005 mg/L Chloroform 1 < 0.005 mg/L Methyl ethyl ketone 1 < 0.010 mg/L Tetrachloroethylene 1 < 0.005 mg/L Trichloroethylene 1 < 0.005 mg/L Vinyl chloride 1 < 0.010 mg/L 3 S904 TCLP ZHE Leaching Procedure Done 4 S903 TCLP Bottle Leaching Procedure Done 5 G150L TCLP Semivolatiles (40CFR Part 261) 1,4-Dichlorobenzene 1 < 0.01 mg/L 2,4,5-TrichLorophenol 1 < 0.01 mg/L 2,4,6-TrichlorophenoL 1 < 0.01 mg/L 2,4-Dinitrotoluene 1 < 0.01 mg/L Hexachlorobenzene 1 < 0.01 mg/L Hexachlorobutadiene 1 < 0.01 mg/L Hexachloroethane 1 < 0.01 mg/L Nitrobenzene 1 < 0.01 mg/L PentachlorophenoL 1 < 0.05 mg/L Pyridine 1 < 0.02 mg/L m-Cresol 1 < 0.01 mg/L o-Cresol 1 < 0.01 mg/L p-Cresol 1 < 0.01 mg/L 7 G121L TCLP Organochlorine Pesticides Chlordane 10 < 10 ug/L Endrin 10 < 0.5 ug/L Heptachlor 10 < 0.5 ug/L Heptachlor epoxide 10 < 0.5 ug/L Lindane 10 < 0.5 ug/L Methoxychlor 10 < 0.5 ug/L Toxaphene 10 < 50 ug/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2ar-tP Analytical 54veDrive Ashheevillee,,NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 February 07, 1997 Report No.: 00058660 Section A Page 2 LABORATORY ANALYSIS REPORT CLIENT NAME: BAXTER HEALTHCARE CORP. SAMPLE ID: 93 033818.6/ SLUDGE SAMPLE NO: H443725 ------------------------------------------------------------------------------------------------------------------------------- TEST DILUTION LN CODE DETERMINATION FACTOR RESULT UNITS ------------------------------------ I G130L TCLP Chlorinated Herbicides 2,4,5-TP (SiLvex) 10 < 2.5* ug/L 2,4-0 10 < 2.5* ug/L COMMENTS: Analysis performed by Pace Analytical Services, Inc., Houston, Texas. * Sample was re -extracted outside of hold -time due to Low surrogate recovery. The results confirmed these original extract results. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive rare Analytical Asheville, NC28801 Tel: 704-254-7176 Fax: 704-252-4618 February 07, 1997 Report No.: 00058660 Section A Page 3 LABORATORY ANALYSIS REPORT CLIENT NAME: BAXTER HEALTCARE CORP. ADDRESS: P.O. BOX 1390 MARION, NC 28752- ATTENTION: WALT MILLER SAMPLE ID: 93 033819.4/ SLUDGE LEACHATE SAMPLE NO: H443726 SAMPLE MATRIX: LEACHATE LIMS CLIENT: 0719 0597 PACE PROJECT: A70122602 PACE CLIENT: 000593 P.O. NO: VERBAL DATE SAMPLED: 22-JAN-97 DATE RECEIVED: 24-JAN-97 PROJECT MANAGER: Katren Jenkins ------------------------------------------------------------------------------------------------------------------------------- TEST DILUTION LN CODE DETERMINATION FACTOR RESULT UNITS ------------------------------------------------------------------------------------------------------------------------------- 16 AHGL Mercury, Leachable (Hg) COMMENTS: Analysis performed by Pace Analytical Services, Inc., Houston, Texas. 1 0.0002 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. out 'seotmgS leoilAleuV aced JO luasuoo ualppM ay; Inogl!m 'Hnj w Idaoxe 'paonpadaj aq Lou pegs }jodaj siyl SISAIVN`d ANOMOB` I JO AUM salepdn pue 986L •AoN 'pa pu£ 'alseM piloS 6utlenleA3 uo; spo paW Zsal-Vd3 6L aouauapS ainlejalll poylaW Ml 13WOOL V 0 W L 26-Ntlr-O£ VOLV-6L VN 0660L 06602 l9HV 9L 31VHOV31 39anis /7'6L8££0 £6 :0I 3ldWVS 9ZL£477H :ON 3ldWVS VSWO9 Or 078L L6-NVr-OE SORS -6L W V 0060 L6-NVr-62 8OLS£-6L LSL8-6L 0280L 7£SOL 6£60L L£60L I05L9 IO£L9 S 6 OOL£00 dd0 £S02 L6-83J-£0 LSL9-6L W V 0060 L6-NVr-62 W V 0060 L6-NVr-6Z BUS£-6L L750L L760L 120 L 09£589 d30 559L L6-Ntlr-LE 0808-6L VN ££869 ££869 £06S 7 S39 008L L6-NVr-SZ LL£L-6L VN S£869 S£869 706S £ S39 OOBL L6-NVr-52 LL£L-6L VN £LOLL 950LL 3HZAO L ASW09 Or OLLZ L6-NVr-O£ e0728-6L SZL£77H :ON 3ldWVS 39anis /9.8L8££0 £6 =0I 3ldWVS ----------------------------------------------------------------- ------------------------------------------ lN3wnsiSNI 1SAIVNV 3WI1/31V0 00H13W-SI lSAIVNV 3WI1/31V0 0OH13W-Ml 08W/SW H31 VS 3003 NI ISR SISAIVNV 3ldWVS------------- NOIIVIIVd3ad 3ldWVS------------- SW/dna i3SOl -------------------------------------------------------------------------------------- NO I lVRO3 N I IV1N3W31ddns L a6ed 8 UOLIOaS 09985000 :-ON liodaa L�6� 'Lp Auenuga3 819ti-ZSZ-ti0L :xe j 9LLLIGZ-bOL :lal L089Z ON `811lA8gSV anua 40JOSuane�j tq •Oul 'SaOwaS IKIIAIeuy 808d Pace Analytical Services, Inc. 54 Ravenscroft Drive e l t i Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 February 07, 1997 Report No.: 00058660 Section C Page 1 SURROGATE STANDARD RECOVERY ---------------------------------------------------------------------------- TEST PERCENT ACCEPTANCE LN CODE SURROGATE COMPOUND RECOVERY LIMITS REF LN ---------------------------------------------------------------------------------- SAMPLE NO: H443725 SAMPLE ID: 93 033818.6/ SLUDGE 1 2 $VOAW GC/MS Volatiles Surrogates 98 _ 4-Bromofluorobenzene 101 - Dibromofluoromethane 104 - Toluene-d8 5 6 $BNAL GC TCLP 40 CFR 261 BNA Surrogates 75 2,4,6-TribromophenoL 74 - 2-FLuorobiphenyl 44 - 2-Fluorophenol 72 - Nitrobenzene-d5 33 - Phenol-d5 p-TerphenyL-d14 7 8 $PSTW Pesticides Surrogate 133 - Decachlorobiphenyl 86 - Tetrachloro-m-xylene 9 10 $HRBRW Herbicides Surrogate 64 - 2,4-Dich,lorophenylacetic acid REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive a c (� Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 February 07, 1997 Report No.: 00058660 Section D Page 1 LABORATORY CONTROL SAMPLE RECOVERY -------------------------------------------------------------------------------------- TEST LCS % ACCEPTANCE CODE DETERMINATION RECOVERY LIMITS BATCH NO: 70937 SAMPLE NO: H381405 G130L TCLP Chlorinated Herbicides 2,4,5-TP (Silvex) 39 _ 2,4-D 33 - BATCH No: 70939 SAMPLE NO: H381409 G150L TCLP Semivolatiles (40CFR Part 261) 1,2,4-Trichlorobenzene 73 1,4-Dichlorobenzene 72 2,4-Dinitrotoluene 80 2-Chlorophenol 65 - 4-Nitrophenol 28 Acenaphthene 77 - Pentachlorophenol 70 - Phenol 33 - Pyrene 86 74 - n-Nitrosodi-n-propylamine p-Chloro-m-cresol 67 BATCH No: 70941 SAMPLE NO: H381413 G121L TCLP Organochlorine Pesticides Endrin 88 _ Heptachlor 88 Heptachlor epoxide 86 Lindane 84 - Methoxychlor 93 BATCH NO: 70990 SAMPLE NO: H381496 AHGL Mercury, Leachable (Hg) 102.0 - BATCH NO: 71056 SAMPLE NO: H381602 OVZHE Volatiles - ZHE/Part 261 103 - 1,1-DichLoroethylene Benzene 1 105 - - Chlorobenzene 105 - Toluene 106 - Trichloroethylene REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace A almlical Asheville, NC28801. ���= Tel: 704-254-7176 Fax: 704-252-4618 February 07, 1997 Report No.: 00058660 section E Page 1 METHOD BLANK DATA ------------------------------------------------------------------------------------------------------------------------------- TEST CODE DETERMINATION RESULT UNIT SAMPLE NO: H379706 BATCH No: 69833 S903 TCLP Bottle Leaching Procedure Done SAMPLE NO: H381406 " BATCH NO: 70937 G130L TCLP Chlorinated Herbicides < 0.5 ug/L 2,4,5-TP (Silvex) < 0.5 ug/L 2,4-D SAMPLE NO: H381410 BATCH NO: 70939 G150L TCLP semivolatiles (40CFR Part 261) < 0.01 mg/L 1,4-Dichlorobenzene < 0.01 mg/L 2,4,5-TrichlorophenoL < 0.01 mg/L 2,4,6-Trichlorophenol < 0.01 mg/L 2,4-Dinitrotoiuene < 0.01 mg/L Hexachlorobenzene < 0.01 mg/L HexachLorobutadiene < 0-.01 mg/L Hexachloroethane < 0.01 mg/L Nitrobenzene < 0.05 mg/L Pentachlorophenol < 0.02 mg/L Pyridine < 0.01 mg/L m-Cresol < 0.01 mg/L o-Cresol < 0.01 mg/L p-Cresol SAMPLE NO: H381414 BATCH NO: 70941 G121L TCLP Organochlorine Pesticides < 1 ug/L Chlordane < 0.05 ug/L Endrin < 0.05 ug/L Heptachlor < 0.05 ug/L. Heptachlor epoxide < 0.05 ug/L Lindane < 0.05 ug/L Methoxychlor < 5 ug/L Toxaphene SAMPLE NO: H381497 BATCH N0: 70990 AHGL Mercury, Leachable (Hg) < 0.0002 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. .54 Ravenscroft Drive le -Analytical Asheville, NG 28801 Tel: 704-254-7176 Fax:704-252-4618 February 07, 1997 Report No.: 00058660 Section E Page 2 METHOD BLANK DATA -------------------------------------------------------------- TEST RESULT UNIT CODE DETERMINATION ---------------------------------------------------------- ------ SAMPLE NO: H381603 BATCH NO: 71056 OVZHE Volatiles - ZHE/Part 261 < 0.005 mg/L 1,1-Dichloroethylene < 0.005 mg/L 1,2-Dichtoroethane < 0.005 mg/L Benzene < 0.005 mg/L Carbon tetrachloride < 0.005 mg/L Chlorobenzene < 0.005 mg/L Chloroform < 0.010 mg/L Methyl ethyl ketone < 0.005 mg/L Tetrachtoroethylene < 0.005 mg/L TrichLoroethylene < 0.010 mg/L Vinyl chloride REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace l i c a l Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 February 07, 1997 Report No.: 00058660 Section F Page 1 DUPLICATE AND MATRIX SPIKE DATA ------------------------------------------------------------------------------------------------------------------------------- TEST ORIGINAL DUPLICATE RANGE / MS MS % CODE DETERMINATION RESULT RESULT UNITS RPD RESULT RCVRY ------------------------------------------------------------------------------------------------------------------------------- BATCH NO: 70990 SAMPLE NO: H443800 AHGL Mercury, Leachable (Hg) < 0.0002 < 0.0002 mg/L --- 0.0043 107.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive ace nap tica0 Asheville, NC28801 Tel: 704-254-7176 Fax:704-252-4618 February 07, 1997 Report No.: 00058660 Section H Page 1 MATRIX SPIKE AND MATRIX SPIKE DUPLICATE DATA ------------------------------------------------------------- MS PCT MSD PCT TEST DETERMINATION MS RESULT MSD RESULT UNITS RPD RCVRYRCVRY CODE ------------ ------------------------------------------------------------- SAMPLE NO: H442514 BATCH No: 70534 G130W Chlorinated Herbicides 10.5 7.36 ug/L 34.8 105 74 2,4,5-T 7.23 4.94 ug/L 37.7 72 49 2,4,5-TP (Silvex) 6.29 4.31 ug/L 37.3 63 43 2,4-D SAMPLE NO: H442508 BATCH NO: 70541 G120WR Organochlorine Pesticides and PCBs 1.64 1.64 ug/L 0 82 82 4,4' DDD 1.55 1.52 ug/L 3 78 76 4,4' DDE 1.57 1.56 ug/L 2 79 78 D 4,4' DDT 1.18 1.09 ug/L 8 59 54 ALdrinin 1.60 1.59 ug/L 2 80 79 DieLdrEndosulfan 1.57 1.59 ug/L 2 78 79 I 1.64 1.64 ug/L 0 82 82 Endosulfan II 1.6 1.61 ug/L 1 80 81 Endosulfan sulfate 1.68 1.68 ug/L 0 84 84 Endrin Endrin aldehyde 1.62 1.62 ug/L 0 5 81 65 81 62 Heptachlor 1.30 1.25 ug/L 2 78 79 a Heptachlor epoxide 1.57 1.58 1.57 ug/L ug/L 0 78 78 Methoxycor 1.57 1.57 1.57 ug/L 3 76 78 alpha-BHC 1.63 1.65 ug/L 2 81 82 beta-BHC 1.62 1.64 . ug/L 2 81 82 delta-BHC 1.58 1.60 ug/L 2 79 80 gamma-BHC SAMPLE NO: H443466 BATCH N0: 70820 G150L TCLP Semivolatiles (40CFR Part 261) 62.6 ug/L 5.81 60 70 1,2,4-Trichlorobenzene 67.9 67.8 ug/L 63 68 1,4-Dichlorobenzene 76.2 76.2 77.8 ug/L 2.P1 2.13 76 79 2,4-Dinitrotoluene 119 127 ug/L 6.99 60 64 2-ChLorophenol 62.5 62.4 ug/L 0.29 32 31 4-Nitrophenol 72.1 74.8 ug/L 3.70 72 75 Acenaphthene 68.1 71.8 ug/L 5. 68 72 N-Nitrosodi-n-propylamine ug/L 1. 38 67 68 Pentachlorophenol. 67.4 72.1 .1 ug/L 6.84 34 36 Phenol .4 85.6 85.1 ug/L 0.60 85 85 Pyrene p-Chloro-m-cresol 130 133 ug/L 2.15 65 66 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive E a c e ) f t l c a l Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 February 07, 1997 Report No.: 00058660 Section H Page 2 MATRIX SPIKE AND MATRIX SPIKE DUPLICATE DATA ------------------------------------------------------------------------------------------------------------------------------- TEST MS MSD MS PCT MSD PCT CODE DETERMINATION ------------------------------------------------------------------------------------------------------------------------------- RESULT RESULT UNITS RPD RCVRY RCVRY BATCH N0: 71013 SAMPLE NO: H442084 OVTCWD Volatiles by 8260 - Subtitle D 1,1-Dichtoroethene 40.1 36.3 ug/L 9.95 101 91 Benzene 40.8 36.6 ug/L 10.8 102 92 Chtorobenzene 40.1 36.6 ug/L 11.1 102 91 Toluene 40.1 35.5 ug/L 11.4 100 89 Trichloroethene 40.1 37.2 ug/L 9.96 102 93 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 00%0%1 350526 CHAIN -OF -CUSTODY RECORD FF n f Analytical Request 1" I ' (. T Client �_����--Y : f c� -� /�(✓ L=% —�-� Re�c S %� �� Pace Client No. port To: �y I O J Address , !L' Bill To: �°�a )C�� / Pace Project Manager ° //<, P.O. # / Billing Reference Pace Project No. A —2(9 Phone S Project Name / No. UDC', , �� , �i, 'Requested Due Date: Sampled By (PRINT): U) ANALYSES /`� w PRESERVATIVES REQUEST ✓ k: l Cam'., Z Sampler Signature Date Sampled z u, \J} • ITEM. SAMPLE • 2 2 1� 0 0� REMARKS l F; „•, 3 44L 33�j�,y 4 ,' 7 € 3r s 8 ' • . • • •" ITEM • 1 • 1 1 1�,�AETW*ED/DAT'E BY 4WILIAtI614 DATE 4 Additional Comments �h a / 6. SEE REVERSE SIDE FOR INSTRUCTIONS- - Pace Analytical Services, Inc. 54 Ravenscroft Drive LD-Ce Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 May 15, 1997 Mr. Phil Castro Baxter Healthcare Corporation P.O. Box 1390 Highway 221 North Marion, NC 28752 RE: PACE Project No. A70421.601 Client Reference: Sludge And TTHMs Dear Mr. Castro: Enclosed is the report of laboratory analyses for samples received April 21, 1997. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel free to contact us. S inc erely; Walter L. Miller Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 3axter Healthcare Corporation May 15, 1997 P.O. Box 1390 PACE Project Number:.A70421601 Highway 221 North Marion, NC 28752 Attn: Mr. Phil Castro Client Reference: Sludge And TTHMs PACE Sample Number: 93 0379087 Date Collected: 04/21/97 Date Received: 04/21/97 Digester Parameter Units PRL Sludge (1) INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Cadmium mg/kg 31 53 Calcium mg/kg 310 17000 Chloride mg/kg 625 8660 Chromium mg/kg 63 82 Copper mg/kg 31 580 Corrosivity pH Units 0.1 5.0 `.Fecal Coliform in Solids by MPN MPN/g 12000 160000 Lead mg/kg 310 340 Magnesium mg/kg 310 4200 Nickel mg/kg 160 ND Nitrogen, Ammonia mg/kg 62 690 Nitrogen, Plant Available mg/kg 625 36100 Phosphorus, Total mg/kg 313 11200 Potassium mg/kg 3100 9100 Sodium mg/kg 0.10 10000 Solids, Percent Total % 0.01 1.6 Sulfate mg/kg 2500 12400 Zinc mg/kg 31 830 SOUR TEST Sour test mg/g/hr 0.01 0.83 Solids, Total Suspended mg/L 1.0 15000 Solids, Total Volatile Suspended mg/L 1.0 12000 NITROGEN, TOTAL Nitrogen, Kjeldahl mg/kg 15600 68000 Nitrogen, Nitrate plus Nitrite mg/kg 3125 15600 '83600 Nitrogen, Total mg/kg 18725 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive E-9-r.e.Alla1yt1r l Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 Mr. Phil Castro Page 2 Client Reference: Sludge And TTHMs These data have been reviewed and are approved for release. Walter L. Miller Operations Manager May 15, 1997 PACE Project Number: A70421601 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Parm Analylical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 Mr. Phil Castro FOOTNOTES May 15, 1997 Page 3 for pages 1 through 2 PACE Project Number: A70421601 Client Reference: Sludge And TTHMs ND Not detected at or above the PRL. PRL PACE Reporting Limit (1) All analysis performed on Toxic Characteristic Leachate. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 May 14, 1997 Report No.: 00061253 Section A Page 1 LABORATORY ANALYSIS REPORT CLIENT NAME: Baxter Healthcare Corporation LIMS CLIENT: 701050 ADDRESS: P.O. Box 1390 Hwy 221 North PACE PROJECT: A70421601 Marion, NC 28752 PACE CLIENT: 000592 ATTENTION: Mr. Phil Castro P.O. NO: VERBAL SAMPLE ID: 93 037908.7/10.9/ DIGESTER SLUDGE DATE SAMPLED: 21-APR-97 SAMPLE NO: H449443 DATE RECEIVED: 23-APR-97 SAMPLE MATRIX• SLUDGE PROJECT MANAGER: Debbie Proctor ------------------------------------------------------------------------------------------------------------------------------- TEST DILUTION LN CODE DETERMINATION ------------------------------------------------------------------------------------------------------------------------------- FACTOR RESULT UNITS 2 S904 TCLP ZHE Leaching Procedure Done 3 OVZHE VolatiLes - ZHE/Part 261 1,1-DichLoroethylene 1 < 0.005 mg/L 1,2-DichLoroethane 1 < 0.005 mg/L Benzene 1 0.007 mg/L Carbon tetrachloride 1 < 0.005 mg/L Chlorobenzene 1 < 0.005 mg/L Chloroform 1 < 0.005 mg/L Methyl ethyl ketone 1 0.010 mg/L TetrachLoroethylene 1 < 0.005 mg/L Trichloroethylene 1 < 0.005 mg/L Vinyl chloride 1 < 0.010 mg/L 5 G150L TCLP SemivolatiLes (40CFR Part 261) 1,4-Dichlorobenzene 5 < 0.05 mg/L 2,4,5-TrichlorophenoL 5 < 0.05 mg/L 2,4,6-TrichlorophenoL 5 < 0.05 mg/L 2,4-Dinitrotoluene 5 < 0.05 mg/L HexachLorobenzene 5 < 0.05 mg/L HexachLorobutadiene 5 < 0.05 mg/L HexachLoroethane 5 < 0.05 mg/L Nitrobenzene 5 < 0.05 mg/L PentachlorophenoL 5 < 0.05 mg/L Pyridine 5 < 0.05 mg/L m-Cresol 5 < 0.05 mg/L o-Cresol 5 < 0.05 mg/L p-Cresol 5 < 0.05 mg/L 7 G121L TCLP Organochlorine Pesticides Chlordane < 1.0 ug/L Endrin < 0.05 ug/L Heptachlor < 0.05 ug/L Heptachlor epoxide < 0.05 ug/L Lindane < 0.05 ug/L Methoxychlor < 0.05 ug/L Toxaphene < 5.0 ug/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive E a rm Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 May 14, 1997 Report No.: 00061253 Section A Page 2 LABORATORY ANALYSIS REPORT CLIENT NAME: Baxter Healthcare Corporation SAMPLE ID: 93 037908.7/10.9/ DIGESTER SLUDGE SAMPLE NO: H449443 ------------------------------------------------------------------------------------------------------------------------------- TEST DILUTION LN ------------------------------------------------------------------------------------------------------------------------------- CODE DETERMINATION FACTOR RESULT UNITS 9 G130L TCLP Chlorinated Herbicides 2,4,5-TP (Silvex) 1 < 0.5 ug/L 2,4-D 1 < 0.5 ug/L 11 S903 TCLP Bottle Leaching Procedure Done 14 AASL Arsenic, Leachable (As) 1 < 0.1 mg/L 15 ABAL Barium, Leachable (Ba) 1 0.6 mg/L 16 ACDL Cadmium, Leachable (Cd) 1 < 0.005 mg/L 17 ACRL Chromium, Leachable (Cr) 1 < 0.01 mg/L 18 APBL Lead, Leachable (Pb) 1 < 0.05 mg/L 19 AHGL Mercury, Leachable (Hg) 1 < 0.0002 mg/L 20 ASEL Selenium, Leachable (Se) 1 < 0.1 mg/L 21 AAGL Silver, Leachable (Ag) 1 < 0.01 mg/L COMMENTS: * Analysis peformed at Pace Analytical Services, Houston Laboratory. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 May 14, 1997 Report No.: 00061253 Section B Page 1 SUPPLEMENTAL INFORMATION ------------------------------------------------------------------------------------------------------------------------------- LCSR DUP/MS------------- SAMPLE PREPARATION ------------- -------------- SAMPLE ANALYSIS --------------- TEST BLNK MS/MSD LN CODE BATCH BATCH LR-METHOD DATE/TIME ANALYST LR-METHOD DATE/TIME ANALYST INSTRUMENT ------------------------------------------------------------------------------------------------------------------------------- SAMPLE ID: 93 037908.7/10.9/ DIGESTER SLUDGE SAMPLE NO: H449443 2 S904 73735 73735 NA 19-1311 23-APR-97 1700 JLJ 005EPE 3 OVZHE 73847 73847 NA 19-8240B 28-APR-97 1558 MH GCMSB 11 S903 73734 73734 NA 19-1311 23-APR-97 1700 JLJ 001EPE 19 AHGL 73839 73839 NA 19-7470A 29-APR-97 0857 D A 100MET 7 G121L 73782 73372 19-3520B 25-APR-97 1200 S M 19-8080 01-MAY-97 1312 S Z 0031GC 9 G130L 73784 73784 19-8151 28-APR-97 0900 S M 19-8151 30-APR-97 1938 S Z 0031GC 5 G150L 73763 74052 19-3510B 25-APR-97 0900 S M 19-8270B 09-MAY-97 1717 MSH 02ITSD 14 AASL 73801 73801 19-3010A 28-APR-97 1200 M P 19-6010A 28-APR-97 1729 CCJ 700MET 15 ABAL 73801 73801 19-3010A 28-APR-97 1200 M P 19-6010A 28-APR-97 1729 CCJ 700MET 16 ACDL 73801 73801 19-3010A 28-APR-97 1200 M P 19-6010A 28-APR-97 1729 CCJ 700MET 17 ACRL 73801 73801 19-3010A 28-APR-97 1200 M P 19-6010A 28-APR-97 1729 CCJ 700MET 18 APBL 73801 73801 19-3010A 28-APR-97 1200 M P 19-6010A 28-APR-97 1729 CCJ 700MET 20 ASEL 73801 73801 19-3010A 28-APR-97 1200 M P 19-6010A 28-APR-97 1729 CCJ 700MET 21 AAGL 73800 73800 19-7760A 28-APR-97 1600 M P 19-7760A 29-APR-97 1118 D A 300MET LR Method Literature Reference 19 EPA -Test Methods for Evaluating Solid Waste, 3rd ed, Nov. 1986 and updates REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Ease lical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 May 14, 1997 Report No.: 00061253 Section C Page 1 SURROGATE STANDARD RECOVERY ------------------------------------------------------------------------------------------------- TEST PERCENT ACCEPTANCE LN CODE SURROGATE COMPOUND RECOVERY LIMITS REF LN ---------------------------------------------------------------------------------------------------- SAMPLE ID: 93 037908.7/10.9/ DIGESTER SLUDGE 4 $VOAW GC/MS Volatiles Surrogates 4-Bromofluorobenzene DibromofLuoromethane Toluene-d8 6 $BNAL GC TCLP 40 CFR 261 BNA Surrogates 2,4,6-Tribromophenol 2-FLuorobiphenyL 2-Fluorophenol Nitrobenzene-d5 Phenol-d5 p-TerphenyL-d14 8 $PSTW Pesticides Surrogate DecachlorobiphenyL TetrachLoro-m-xylene 10 $HRBRW Herbicides Surrogate 2,4-Dichlorophenylacetic acid SAMPLE NO: H449443 3 93 - 95 - 95 - 5 88 - 54 - 50 - 53 - 59 - 61 - 7 107 - 57 - 9 27 - REPORT OF LA13OMTORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive E!ace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 May 14, 1997 Report No.: 00061253 Section D Page 1 LABORATORY CONTROL SAMPLE RECOVERY ------------------------------------------------------------------------------------------------------------------------------- TEST LCS % LCSD % ACCEPTANCE CODE ------------------------------------------------------------------------------------------------------------------------------- DETERMINATION RECOVERY RECOVERY LIMITS RPD BATCH NO: 73763 SAMPLE NO: H385860 G150L TCLP SemivolatiLes (40CFR Part 261) 1,4-DichLorobenzene 67 - 2,4,5-TrichlorophenoL 83 - 2,4,6-TrichlorophenoL 78 - 2,4-Dinitrotoluene 81 - Hexachlorobenzene 68 - Hexachlorobutadiene 66 - Hexachloroethane 69 - Nitrobenzene 94 - PentachlorophenoL 77 - m-Cresol 62* - o-Cresol 63 - p-Cresol * - * The compounds m-cresol and p-cresol co -elute. The reported result is the sum of the two. BATCH NO: 73782 SAMPLE NO: H385892 G121L TCLP Organochlorine Pesticides Chlordane - Endrin 82 - Heptachlor 73 - Heptachlor epoxide 91 - Lindane 69 - Methoxychlor 93 - Toxaphene - G121L TCLP Organochlorine Pesticides Chlordane - Endrin 93 - Heptachlor 93 - Heptachlor epoxide 93 - Lindane 93 - MethoxychLor 93 - Toxaphene - BATCH NO: 73784 SAMPLE NO: H385896 G130L TCLP ChLorinated Herbicides 2,4,5-TP (Silvex) 63 2,4-D 67 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive are Anci1ytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 May 14, 1997 Report No.: 00061253 Section D Page 2 LABORATORY CONTROL SAMPLE RECOVERY ------------------------------------------------------------------------------------------------------------------------------- TEST LCS % LCSD % ACCEPTANCE CODE ------------------------------------------------------------------------------------------------------------------------------- DETERMINATION RECOVERY RECOVERY LIMITS RPD BATCH NO: 73800 SAMPLE NO: H385924 AAGL Silver, Leachable (Ag) 102.0 - BATCH NO: 73801 SAMPLE NO: H385926 AASL Arsenic, Leachable (As) 104.4 - ABAL Barium, Leachable (Ba) 105.1 - ACDL Cadmium, Leachable (Cd) 98.4 - ACRL Chromium, Leachable (Cr) 98.4 - APBL Lead, Leachable (Pb) 107.1 - ASEL Selenium, Leachable (Se) 104.5 - BATCH NO: 73839 SAMPLE NO: H385979 AHGL Mercury, Leachable (Hg) 96.9 - BATCH No: 73847 SAMPLE NO: H385993 OVZHE Volatiles - ZHE/Part 261 1,1-Dichloroethene 88 - Benzene 101 - Chlorobenzene 99 - Toluene 100 - Trichloroethylene 101 - REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Ece Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 May 14, 1997 Report No.: 00061253 Section E Page 1 METHOD BLANK DATA ------------------------------------------------------------------------------------------------------------------------------- TEST CODE DETERMINATION RESULT UNIT --------------------------------------------------------------------------------------------------------------------------- BATCH NO: 73763 SAMPLE NO: H385861 G150L TCLP Semivolatiles (40CFR Part 261) 1,4-Dichlorobenzene < 0.01 mg/L 2,4,5-TrichLorophenoL < 0.01 mg/L 2,4,6-TrichlorophenoL < 0.01 mg/L 2,4-DinitrotoLuene < 0.01 mg/L Hexachlorobenzene < 0.01 mg/L Hexachlorobutadiene < 0.01 mg/L HexachLoroethane < 0.01 mg/L Nitrobenzene < 0.01 mg/L PentachLorophenol < 0.01 mg/L Pyridine < 0.01 mg/L m-Cresol < 0.01 mg/L o-Cresol < 0.01 mg/L p-Cresol < 0.01 mg/L BATCH NO: 73782 SAMPLE NO: H385893 G121L TCLP OrganochLorine Pesticides Chlordane < 1.0 ug/L Endrin < 0.05 ug/L Heptachlor < 0.05 ug/L Heptachlor epoxide < 0.05 ug/L Lindane < 0.05 ug/L Methoxychlor < 0.05 ug/L Toxaphene < 5.0 ug/L G121L TCLP Organochlorine Pesticides Chlordane < 1.0 ug/L Endrin < 0.05 ug/L Heptachlor < 0.05 ug/L Heptachlor epoxide < 0.05 ug/L Lindane < 0.05 ug/L Methoxychlor < 0.05 ug/L Toxaphene < 5.0 ug/L BATCH NO: 73784 SAMPLE NO: H385897 G130L TCLP ChLorinated Herbicides 2,4,5-TP (Silvex) < 0.5 ug/L 2,4-D < 0.5 ug/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Earm CY����s��� Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 May 14, 1997 Report No.: 00061253 Section E Page 2 METHOD BLANK DATA ------------------------------------------------------------------------------------------------------------------------------- TEST CODE DETERMINATION RESULT UNIT ------------------------------------------------------------------------------------------------------------------------------- BATCH NO: 73800 AAGL Silver, Leachable (Ag) BATCH NO: 73801 AASL Arsenic, Leachable (As) ABAL Barium, Leachable (Ba) ACDL Cadmium, Leachable (Cd) ACRL Chromium, Leachable (Cr) APBL Lead, Leachable (Pb) ASEL Selenium, Leachable (Se) BATCH NO: 73839 AHGL Mercury, Leachable (Hg) BATCH NO: 73847 OVZHE Volatiles - ZHE/Part 261 1,1-Dichloroethylene 1,2-Dichloroethane Benzene Carbon tetrachloride Chlorobenzene Chloroform Methyl ethyl ketone Tetrachloroethylene Trichloroethylene Vinyl chloride SAMPLE NO: H385925 < 0.01 mg/L SAMPLE NO: H385927 < 0.1 mg/L < 0.1 mg/L < 0.005 mg/L < 0.01 mg/L < 0.05 mg/L < 0.1 mg/L SAMPLE NO: H385980 < 0.0002 mg/L SAMPLE NO: H385994 < 0.005 mg/L < 0.005 mg/L < 0.005 mg/L < 0.005 mg/L < 0.005 mg/L < 0.005 mg/L < 0.010 mg/L < 0.005 mg/L < 0.005 mg/L < 0.010 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace, Analylica Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 May 14, 1997 Report No.: 00061253 Section F Page 1 DUPLICATE AND MATRIX SPIKE DATA ------------------------------------------------------------------------------------------------------------------------------- TEST ORIGINAL DUPLICATE RANGE / MS MS CODE ------------------------------------------------------------------------------------------------------------------------------- DETERMINATION RESULT RESULT UNITS RPD RESULT RCVRY BATCH No: 73800 SAMPLE NO: H449443 AAGL Silver, Leachable (Ag) < 0.01 < 0.01 mg/L --- 0.12 * 60.0 * Recovery of the matrix spike indicates the presence of a matrix interference. This should be considered in evaluating the data. BATCH NO: 73801 SAMPLE NO: H449443 AASL Arsenic, Leachable (As) < 0.1 < 0.1 mg/L --- 2.0 100.0 ABAL Barium, Leachable (Ba) 0.6 0.7 mg/L 15.4 2.6 100.0 ACDL Cadmium, Leachable (Cd) < 0.005 < 0.005 mg/L --- 0.045 90.0 ACRL Chromium, Leachable (Cr) < 0.01 0.01 mg/L --- 0.17 85.0 APBL Lead, Leachable (Pb) < 0.05 < 0.05 mg/L --- 0.45 90.0 ASEL Selenium, Leachable (Se) < 0.1 < 0.1 mg/L --- 2.0 100.0 BATCH NO: 73839 SAMPLE NO: H449456 AHGL Mercury, Leachable (Hg) < 0.0002 < 0.0002 mg/L --- 0.0020 100.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive P-19ce ���I�,t���N Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 May 14, 1997 Report No.: 00061253 Section H Page 1 MATRIX SPIKE AND MATRIX SPIKE DUPLICATE DATA ------------------------------------------------------------------------------------------------------------------------------- TEST MS MSD MS PCT MSD PCT CODE ------------------------------------------------------------------------------------------------------------------------------- DETERMINATION RESULT RESULT UNITS RPD RCVRY RCVRY BATCH NO: 73372 SAMPLE NO: H448775 G121L TCLP Organochlorine Pesticides Chlordane < 1 < 1 ug/L Endrin 1.78 1.80 ug/L 1.1 89 90 Heptachlor 1.42 1.48 ug/L 4.1 71 74 Heptachlor epoxide 1.50 1.50 ug/L 0.0 75 75 Lindane 1.68 1.49 ug/L 12.6 84 74 MethoxychLor 1.89 1.88 ug/L 0.0 94 94 Toxaphene < 5 < 5 ug/L BATCH NO: 73784 SAMPLE NO: H449390 G130L TCLP Chlorinated Herbicides 2,4,5-TP (SiLvex) 3.23 3.21 ug/L 0.0 32 32 2,4-D 5.66 3.89 ug/L 3.4 57 39 BATCH NO: 74052 SAMPLE NO: H449990 G150L TCLP Semivolatiles (40CFR Part 261) 1,4-Dichlorobenzene 0.062 0.054 mg/L 6.9 62 54 2,4,5-Trichlorophenol 0.070 0.084 mg/L 8.7 70 84 2,4,6-Trichlorophenol 0.068 0.072 mg/L 2.8 68 72 2,4-Dinitrotoluene 0.074 0.087 mg/L 8.2 74 87 HexachLorobenzene 0.082 0.073 mg/L 6.0 82 73 HexachLorobutadiene 0.065 0.058 mg/L 5.2 65 58 HexachLoroethane 0.063 0.052 mg/L 9.6 63 52 Nitrobenzene 0.085 0.083 mg/L 1.2 85 83 PentachLorophenoL 0.072 0.065 mg/L 5.3 72 65 m-Cresol 0.34* 0.27* mg/L 11.1 127 93 o-Cresol 0.18 0.15 mg/L 9.6 127 95 p-Cresol * * mg/L * The compounds m-cresol and p-cresol co -elute. The reported result is the sum of the two. REPORT OF LASORATORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Client s �� k /' �' / z // h a ,. Address-,nq Phone —7yY G i. Sampled By (PRINT): / .t k' Sampler Additional Comments 371116 a CHAIN -OF -CUSTODY RECORD Analytical Request Report To: �'j I / ��� Ira a Pace Client No. Bill To: 8 K 7' P i Pace Project Manager P.O. # / Billing Reference Pace Project No. /1 7,7 Date Sampled INU� - �. � - '1 7 Project Name / No. VUay -I- r PRESERVATIVES ANALYSES REQUEST ~w z M O w u- w O IL OU) O Q p z N z O z D I'1 'Requested Due Date: 5 , ?gto,9 t Y 77, 2 SEE REVERSE SIDE FOR INSTRUCTIONS Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 August 04, 1997 Mr. Phil Castro Baxter Healthcare Corporation P.O. Box 1390 Highway 221 North Marion, NC 28752 RE: PACE Project No. A70714.600 Client Reference: Sludge And Other Samples Dear Mr. Castro: Enclosed is the report of laboratory analyses for samples received July 14, 1997. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel free to contact us. Sincerely, Walter L. Miller Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive rfar.AnalyliAsheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 ;axter Healthcare Corporation August 04, 1997 P.O. Box 1390 PACE Project Number: A70714600 Highway 221 North Marion, NC 28752 Attn: Mr. Phil Castro Client Reference: Sludge And Other Samples NC Wastewater Lab Cert. #40 NC Drinkingwater Lab Cert. #37712 SC Lab Cert. #99030 PACE Sample Number: 93 0423990 Date Collected: 07/14/97 Date Received: 07/14/97 Client Sample ID: Sludge Parameter Units PRL Leachate (1) INORGANIC ANALYSIS 8 RCRA METALS - LEACHATE Barium, Leachate mg/L 0.010 0.30 Cadmium, Leachate mg/L 0.010 0.02 Chromium, Leachate mg/L 0.010 ND Lead, Leachate mg/L 0.100 ND Silver, Leachate mg/L 0.01 0.08 Arsenic, Leachate mg/L 0.0050 0.006 Selenium, Leachate mg/L 0.0050 ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace AD Jyl i c a p Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 Mr. Phil Castro Page 2 August 04, 1997 PACE Project Number: A70714600 Client Reference: Sludge And Other Samples PACE Sample Number: 93 0423981 Date Collected: 07/14/97 Date Received: 07/14/97 Client Sample ID: Sludge Parameter Units PRL INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Cadmium mg/kg 36 ND Calcium mg/kg 360 27000 Chloride mg/kg 710 11100 Chromium mg/kg 71 ND Copper mg/kg 36 ND Corrosivity pH Units 0.1 5.5 Fecal Coliform in Solids by MPN col/g 14000 1200000 Lead mg/kg 360 ND Magnesium mg/kg 360 5000 Nickel mg/kg 180 ND Nitrogen, Ammonia mg/kg 71 5500 Nitrogen, Plant Available mg/kg 1.0 18900 Phosphorus, Total mg/kg 714 13200 Potassium mg/kg 3600 5400 Sodium mg/kg 360 12000 Solids, Percent Total % 0.01 1.4 Sulfate mg/kg 2900 13600 Zinc mg/kg 36 500 SOUR TEST Sour test mg/g/hr 0.01 1.4 Solids, Total Suspended mg/L 1.0 11000 Solids, Total Volatile Suspended mg/L 1.0 10000 NITROGEN, TOTAL Nitrogen, Kjeldahl mg/kg 18000 59000 Nitrogen, Nitrate plus Nitrite mg/kg 72 73 Nitrogen, Total mg/kg 18071 59073 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 Mr. Phil Castro Page 3 Client Reference: Sludge And Other Samples These data have been reviewed and are approved for release. ct� Walter L. Miller Operations Manager August 04, 1997 PACE Project Number: A7O7146OO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Rare alyt9cal Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 Mr. Phil Castro FOOTNOTES August 04, 1997 Page 4 for pages 1 through 3 PACE Project Number: A70714600 Client Reference: Sludge And Other Samples NO Not detected at or above the PRL. PRL PACE Reporting Limit (1) All analysis performed on Toxic Characteristic Leachate. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services. !nc. 54 Ravenscroft Drive Pace Analal Asheville. NC 28801 Tel: /04-254-/176 Fj iO4-"S2-4618 August 1, 17 Report No.: 00063331 Section A Page 1 LABORATORY ANALYSIS REPORT CLIENT NAME: BAXTER HEALTHCARE CORP. ADDRESS: P. 0. BOX 1390 MARION, NC 28752 ATTENTION: PHIL CASTRO SAMPLE ID: 93 042398.1/SLUDGE SAMPLE NO: 9454542 SAMPLE MATRIX: SLUDGE LIMS CLIENT: 0719 0597 PACE PROJECT: A70714600 PACE CLIENT: 000593 P.O. NO: VERBAL DATE SWLED: 14-JUL-97 DATE RECEIVED: 16-JUL-97 PROJECT MANAGER: Debbie Pr-octor ------------------------------------------------------------------------------------------------------------------------------- TEST DILUTION LN ------------------------------------------------------------------------------------------------------------------------------- CODE DETERMINATION FACTOR RESULT UNITS 1 OVZHE Votatiles - ZHE/Part 261 1,1-Dichloroethylene 1,2-DichLoroethane 10 < 0.05 mg/L Benzene 10 < 0.05 mg/L Carbon tetrachloride 10 < 0.05 mg/L Chlorobenaene 10 < 0.05 RG/L Chloroform 10 < 0.05 mg/L Methyl ethyl ketone 10 < 0.10 mg/L TetrachLoroethytow .10 < 0.05 mVL TrichloroethyLem 10 < 0.05 mwL vinyl chloride 10 < 0.10 mg/L 3 $904 TCLP ZHE leaching Procedure Dona 4 6903 TCLP Bottle Leaching Procedure Dane 16 AHGL Mercury, Leachable (fig) 1 < 0.0002 mg/L 23 9121L TCLP Orgenochlorine Pesticides Chtordam 1 < 10.0 ug/L Endrin . 1 < MO ug/L Reptachlor 1 r 0.50 ug/L. Heptachlor epoxide 1 < 0.50 ug/L. Linden 1 < 0.50 ug/L Methexychlor 1 < 0.50 ug/L Toxapherle 1 < 50.0 USA 25 0130L TCLP Chlorinated Herbicides 2,4,5-TP (Silvex) 1 < 5 ug/L 2,4-0 1 < 5 ug/L 27 OTCLP Semi-volatiles - TCLP/Part 261 T,4-Dichlorobenzene 1 < 0.01 Mg/L 2,4,5-Trichtorophenot 1 < 0.01 mg/L 2,4,6-Trichtorophenol 1 < 0.01 mg/L 2,4-Dinitratotuene 1 < 0.01 matt. HeXachtarobenzene • 1 < 0.01 mg/L Hexachlorofxrtadiene 1 < 0.01 mg/L Mexachlorcethane 1 < 0.01 mg/L Nitrobenzene 1 < 0.01 mg/L Pentachlorophenol 1 < 0.01 ng/L REPORT OF LABORATORY ANALYSIS This report shall riot be reproduced, exoept in fluff, WOW the written omwent of Pace Analytical Servicass, Ina Pace Analytical Services. inc. Asheville. INC28801 Tel: 704-254-7175 Fax: 7 04i, ')-.1b18 August 01, 7 Reflort No.: 00063331 Section A Page 2 LABORATORY ANALYSIS REPORT CLIENT NAME: BAXTER HEALTHCARE CORP. SAMPLE ID: 93 042398.1/SLUDGE SAMPLE NO: H454542 -- TEST --------;---------------------------------------------- DILUTICp LM =E DETERMINATION ------------------------------------------------------------------------------------------------------------------------------- FACTOR. RESULT UNITS Pyridine 1 < O.pT cg/L m-Cresol 1 < 0.01 Van a -Cresol T < 0.01 ng/L p-Cresol 1 < 0.01 ag/L COMMENTS: * Anetysis peformed by Pace Analytical Services, Inc., HCuston Laboratory. REPORT OF LABORATORY ANALYSIS This repot shall not be reproduced, except in full, without the written consent of Pace Anaiytical Services, Inc. FEB-14-1917 2:09 FROM PACE ANALYTICRL TO 17042524618 P.004i011 Pace Analytical Services, Inc. goo Gemini Avenue Analy i �, a{ Houston, Tx T7058 pa C p Tel. 281-488-1810 I= 281-488-4661 August 12, 1997 Report' No.: 00063331 Section 0 Page 1 SUPPLEMENTAL INFORMATION -------------------------------------------------------------- tCSR 'DUP/F1s --- SAMPLE PREPARATION ------------ -------------- SAMPLE ANALYSIS --------------- TEST BLNK BATCH MS/MSD BATCH LR-METHOD DATE/TIME ANALYST LR-METHOD DATE/TIME ANALYST I-I---t£N- LN CODE SAMPLE NO: H454W SAMPLE ID: 93 042398.USLUDGE 19-82400 08-AUG-97 0014 MH GCMSB 1 OVZHE 76497 76676 NA 19-1311 •18-dUL-97 1400 D M 005EPE 3 S904 76046 76046 NA 19-1311 18-JUL-97 1400 D M 001EPE 4 S903 76047 76047 NA 19-7470A 22-JUL-97 18" D A 100MET 16 AHGL 16175 76096 76175 76096 NA 19-35208 21-JUL-97 0800 J A 19-8080 23=JUL-97 1252 WZ 5693GC 23 25 G121L G130L 76099 75069 19-8151 21-JUL-97 0800 RDQ 19-8151 22-JUL-97 1636 A Y 0031GC 22-JUL-97.2220 MSH 021TSD 27 OTCLP 76100 75209 19-3510B 22-JUL-97 0900 J A 19-82708 lft Method Liter tore Reference for EVBluatim Solid Waste, 3rd ad, Noy. 1986 and updates 19 EPA -Test Methods REPORT OF LABORATORY ANALYSIS This report shau not berWoduced, except in NII, without the written consent of Pace Analytical Services. Inc. FEB-14-1917 2:09 FROM PACE ANALYTICAL TO 17042524618 P.005/011 Pace Analytical Services, Inc. 900 Gemini Avenue Pace. Analytical + Houston, TX 77058 Tel: 281-488-1810 Fax 261-488-4661 August 12, 1997 Report No.: 00063331 section C Page 1 SURROGATE STANDARD RECOVERY --------------------- TEST -................................................................................. ----------------------- PERCENT ACCEPTANCE LN ------------------------------------------------------------------------------------------------------------------------------- CODE 5MCGATE COMPOUND RECOVERY ' LIMITS REF LN SAMPLE ID: 93 042398.1/SLUDGF- SAMPLE NO: H454542 2 $VOAW GC/MS Votatiles surrogates 1 1,2-Dichtorcethane-d4 102 - 4-5romofLuorobenzena •96 - TOtuene-d8 95 - 24 $PSTW Pesticides Surrogate 23 Decachlorobiphenyt 243* - Tetrachloro-m-xyLerle 98 - *: Out of Limit due to the crystalization of DC8 in the spiking solution. 26 3HRBRW Herbicides Surrogate 25 2,4-Dichloro0enytacetic acid 25 - 28 SONAL GC TCLP 40 CPR 261 BNA Surrogates 27 2,4,6-Tribrcomphenol 75 - 2-Fluorobiphenyl 60 - 2-Flucrophenol 36 - Nitrobenzene-d5 5o - Phenot-415 23 - p-Terphenyt-d% 55 - REPORT OF LABORATORY ANALYSIS This report ShaA not be reproduced, except in full, without the written consent of Pace'Analytical Services, Inc. FEB-14-1917 2:09 FROM PACE ANALYTICAL TO 17042524618 P.006/011 Pace Analytical Services, Inc. No Gemini Avenue Houston, TX 77058 pace nabalical Tel: 281-488-1810 Fax: 281-488-4661 August 12, 1997 Report No.: 0006 I Section D PW 1 LABORATORY CONTROL SAMPC RECOVERY _ ---------------------------------- LCS x LCSD x ACCEPTANrF TEST' QETERMINATION RECOVERY RECOVERY LIMITS -HP CO DE -------------------------------------------------- -------------------------- -------- ------ SAMPLE No: H389450 HATCH NO: 76M G121L TCLP OrSanochLorine Pesticides 78 _ Endrin 74 - Heptachtor 84 - Heptachlor epoxide 8s _ Litldane 86 - Methoxychtor SAMPLE NO., MM456 BATCH N0: 76099 0130L TCLP Chlorinated Herbicides 68 _ 2,4,5-TP (S UVex) 51 _ Z,4-D 8AMPI-E N0: N�458 BATCH HQ: 76100 OTCLP Semi-votatiLes - TCLP/Part 261 77 - 1,4-pichlorobenzene 88 _ 2,4,5-Trichloropheno1 95 _ 2,4,6-Trichlorophenot 110 ' 2,4-Dinitrotoluene 67 - Hexachlorobenzene $0 - Hexachtorobutadiene 74 _ Hexachloroethane 78 Nitrobemene 99 - Pentwti orophenoL 50 . Pyridine - m-Cres*L 80 - a-Cresol- p-Cresol The compounds w-eresot and p-cresol co -elute- The reported result is the sum of the two.. SAMPLE NO: H389582 BATCH N0: 76175 99.4• _ AHGL Mercury, Leachable (Hg) SAMPLE No: B390086 BATCH NO: 76497 OVZHE Volatiles - ZHE/Part 261 92 _ 1,1-Qiohloroethylene 106 - Benzene 112 - �� Chlorobenzene REPORT OF LABORATORY ANALYSIS This report shall not be reproduce, except in full. without the written consent of Pace Anehltjcal Services. Inc. FEB-14-1917 2:10 FROM PACE ANALYTICAL TO 17042524618 P.008i011 Pace Analytical Services, Inc. 900 Gemini Avenue Pacr, ..�;,� Houston, TX 77058 Tel: 28148$1810 Fax 281-488-4661 August 12, 1997 Report No.: 00063331 Section E Page 1 METHOD BLANK DATA -----------------------a•-----...------------.------........------....-------------•----------.---- ...........-------r...--- TEST RESULT' UNIT CODE DETERMINATION BATCH No: 76096 SAMPLE Ho; H389451 G121L TCLP Orasnochlorine Pesticides < 10.0 ug/L Chlordene < 0.50' ug/L Endrin < 0.50 ug/L Heptachlor < 0.50 ug/L Heptachlor tpoxide < ug/L Litkielx• .0.50 < ug/L Methonchlor < 50.0 ug/L Toxaphene BATCH NO: 76099 G130L TCLP Chlorinated Herbicides 2,4,5-TP (Silvex) 2,4-D BATCH N0: 76100 OTCLP Semi-voiatiles - TCLP/Part 261 1.4-DichLorobemme 2,45-TrichLoropheml. 2,4,6-Trichlorophenot 2,4-Dinitrotoluene Nexachtorobenzene Hexachlorobutsdiene Hexachloroethem Nitrobenzene pentach(oropttenol Pyridine M-Cresol o-cresol P-Cresol BATCH No- 76175 AHGL Mercury, Leachable (Hg) BATCH NO: 76497 OVZHE Volatiles - 2HE/Part 261 1,1-Dichloroethylene 1,2-Dichtaroethane Benzene SAMPLE NO: H389457 < 5 ugA. < 5 ug/L SAMPLE NO: H389459 < 0.01 m0l. < 0.01 tag/L < 0.01 mg/L < 0.01 mg/L < 0.01 Mj/L < 0.01 mg/L < 0.01 mg/L < 0.01 mg/L < 0.01 mg/L < 0.01 mg/L < 0,01 M/L < 0.01 mg/L < 0.01 mg/L SAMPLE 90: KRM83 < 0.0002 ag/L SAMPLE NO: H390 U < 0.005 Mg/L < 0.005 ra9/L < 0.005 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, without the written consent oi.PBpe Analogel Services, Ina FEB-14-1917 2:10 FROM PACE ANALYTICAL TO 17042524618 P.009i011 Pace Analytical Services, Inc. 900 Gemini Avenue h A Houston, TX 77058 Tel: 281-488-1810 Fa:c 281-488-4661 ALwxt 12, 1917 Report No.: 0006MI Section E Page 2 KETHW- UANK_D_I_LTA TFST CODE DETERMINATION --------------------------------------------------------------------------------------------------------------------------- RESULT UNIT Carbon tetrachloride < 0.005 mg/L Chlorobenzene < O.005 mg/L Chloroform' < 0.005 M/L Methyl ethyl ketom < 0.010 . mg1L TatrachLoroethyterw < 0.005 mg/L Trichicroethytene < 0.005 )WL Vinyt chtoride c 0.010 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be ra6r6duced, except in full, Without the written consent of Pace Analytical Services, Inc. FEB-14-1917 2:10 FROM PACE ANALYTICAL TO 17042524618 P.010i011 Pace Analytical Services, Inc. qq p 900 Gemini Avenue Houston, TX77058 Tel: 281-488-1810 I= 281488-4661 Augst IZ, 1997 Report lies 00063331 section F page 1 DUPLICATE AND' TRIX SPIKE DATA TEST rntIGIKAL DUPLICATE RANGE / AS HS X CODE DETERMINATION RESULT RESULT UNITS RP0 RESULT RCVRY BATCH NO: 76175 SAMPLE NO: H454542. AHGL Mercury, Leachable (HQ) C 0.0002 0.000E mg/L --- 0.0020 100 REPORT OF LABORATORY ANALYSIS This report shall not to reproduced, exoept in full, without the written consent of Pace Analytical Services, Inc. FEB-14-191? 2:11 FROM PACE ANALYTICAL TO 1?042524618 P.011i011 Pace Analytical Services, Inc. 900 Gemini Avenue Analytic 1 �yti i Houston, TX77058 Tel: 281-488-1810 Fax'281-488-4661 August 12, 1997 Report No.: 00063331 section H Pa9e 1 MATRIX SPIKE AND MATRIX SPIKE DUPLICATE DATA ------- ---- ------------------------------------------------------------------- TEST MS MSD Ms OCT MSD PCT CODE DETERMINATION RESULT RESULT UNITS RPD RCVRY RCVRY BATCH ND: 7$069 G130L TCLP Chlorinated Herbicides 2,4,5-TP (SiLvex) 4 4 2,4-D . 5 5 u9/L BATCH NU: 75209 G150L TCLP SemivolatileS (40CFR Part 261) 1,4-Uichtorobenzene 4.92 7.0 mg/L 2,4,5-Trichtorophenol 5.36 9.7 mD/L 2,4,6-Trichlorophenol 4.56 7.1 mg/L 2,4-Dinitrotoluene 7.47 12.9 mg/L Nexachtorobenzene 4.36 7.1 m!a/L Hexachlorobutediene 4.33 5.4 mg/L Hexechloraethene 4.11 5.5 m9/L Nitrobenzene 5.12 7.7 m9/L PentachLorophenol 20.74 24.4 mg/L Pyridine 14.43 21.3 m9/L m-Cresot 10.06 * 13.4 * m8/L o-Cresol 5.07 7.0 VQIL P-Cresol ' m8/L w The compounds m-cresol and p-cresol cc -elute. The reported result is the sum of the tiro. BATCH xo: 16M SAMPLE NO: H452243 0 84 84 1 91 90 SAMPLE NO: H452446 17.2 25 35 28.9 27 49 21.5 23 35 26.6 37 64 23.8 2Z 35 11.4 22 27 14.6 21 28 20.3 26 39 8.1 104 122 19.2 36 53 14.1• 13 35 16.1 25 35 sAMPLE ►tor B454542 G12iL TCLP Organochlorine Pesticides 4 91 88 Endrin 9,10 . 875 ugll 4 82 79 Heptachlor 8.21 7.87 ug/L 5 93 89 Heptachlor epoxide 9.33 8.91 ug/L 4 98 94. Lindane 9.79 9.43 ug/L 2 93 91 mathoxychtor 9.29 9.09 ug/L SAMPLE NO:. H455629 BATCH No: 76676 OVZHE Volatiles - ZHE/Part 261 1 112 113 1,1-Dichtoroathylene 45 45 tig/L 3 92 95 senzene 37 40 38 40 u9/L u9/L 1 101 100 Chlorobenzene 43 43 ug/L 0 107 106 Toluene 38 38 uB/L 1 95 96 Trichtoroethylene REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full, ....• ... r .�......:u.-.. n..w-a..+ _(C)era AnAlvnifal gPMCOS. Inc. TnT01 P O11 1 Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 February 11, 1998 Mr. Phil Castro Baxter Healthcare Corporation P.O. Box 1390 Highway 221 North Marion, NC 28752 RE: PACE Project No. A71104.602 Client Reference: Quarterly Dear Mr. Castro: Enclosed is the report of laboratory analyses for samples received November 04, 1997. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel free to contact us. Sincerely, Walter L. Miller Project Manager Enclosures Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 FL Environmental 96317 SC Environmental 99030 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive P@Ce A nglyliGal Asheville, NC 28801 i� Tel: 704-254-7176 Fax:704-252-4618 laxter Healthcare Corporation February 11, 1998 P.O. Box 1390 PACE Project Number: A71104602 Highway 221 North Marion, NC 28752 Attn: Mr. Phil Castro Client Reference: Quarterly PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter INORGANIC ANALYSIS 8 RCRA METALS - LEACHATE Units PRL NC Wastewater Lab Cert. #40 NC Drinkingwater Lab Cert. #37712 SC Lab Cert. #99030 93 0482520 11/04/97 11/04/97 Leachate (1) Barium, Leachate mg/L 0.010 0.36 Cadmium, Leachate mg/L 0.010 ND Chromium, Leachate mg/L 0.010 ND Lead, Leachate mg/L 0.100 ND Silver, Leachate mg/L 0.005 0.027 arsenic, Leachate mg/L 0.0050 ND Selenium, Leachate mg/L 0.0050 ND Mercury, Leachate mg/L 0.0005 ND Laboratory Certification IDS Laboratory Certification IDS NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 FL Environmental 96317 SC Environmental 99030 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. C •_ Pace Analytical Services, Inc. 54 Ravenscroft Drive !Ge�''�' �� ' Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 Ar. Phil Castro February 11, 1998 Page 2 PACE Project Number: A71104602 Client Reference: Quarterly PACE Sample Number: 93 0482376 Date Collected: 11/04/97 Date Received: 11/04/97 Client Sample ID: Digester Parameter Units PRL Sludge INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Cadmium mg/kg 31 ND Calcium mg/kg 160 19000 Chloride mg/kg 620 8400 Chromium mg/kg 62 62 Copper pp m k 9/ 9 31 47 Corrosivity pH Units 0.1 6.9 Fecal Coliform in Solids by MPN MPN/g 1 100000 Lead mg/kg 310 ND Magnesium mg/kg 1600 4100 Nickel mg/kg 310 ND Nitrogen, Ammonia mg/kg 62 250 Nitrogen, Plant Available mg/kg 1.0 33050 Phosphorus, Total mg/kg 620 4200 Potassium mg/kg 3100 ND Sodium mg/kg 1600 11000 Solids, Percent Total % 0.01 1.6 Sulfate mg/kg 625 11000 Zinc mg/kg 31 560 SOUR TEST Sour test mg/g/hr 0.01 0.67 (2) Solids, Total Suspended mg/L 1.0 16000 Solids, Total Volatile Suspended mg/L 1.0 15000 NITROGEN, TOTAL Nitrogen, Kjeldahl mg/kg 16000 110000 Nitrogen, Nitrate plus Nitrite mg/kg 62 ND Nitrogen, Total mg/kg 16062 110000 Laboratory Certification IDs Laboratory Certification IDs REPORT ®F LABORATORY ANALYSIS TN Drinking Water 02980 NC Wastewater 40 FL Environmental 96317 NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Ease al,ytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 Mr. Phil Castro Page 3 Client Reference: Quarterly These data have been reviewed and are approved for release. W)K&-) Walter L. Miller Operations Manager February 11, 1998 PACE Project Number: A71104602 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC DrinkingWater 37712 FL Environmental 96317 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Eace n ylical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 Mr. Phil Castro FOOTNOTES February 11, 1998 Page 4 for pages 1 through 3 PACE Project Number: A71104602 Client Reference: Quarterly ND PRL (1) (2) Not detected at or above the PRL. PACE Reporting Limit All analysis performed on Toxic Characteristic Leachate. client calculated change in dissolved oxygen for 15 minutes. Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 FL Environmental 96317 SC Environmental 99030 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive An ly$ecai Asheville, NC 28801 Tel: 704-254-7176 Fax:704-252-4618 November 18, 1997 Report No.: 00065858 Section A Page 1 LABORATORY ANALYSIS REPORT CLIENT NAME: BAXTER HEALTHCARE.CORP. ADDRESS: P. 0. BOX 1390 MARION, NC 28152 ATTENTION: MR.,PHIL CASTRO SAMPLE ID: 93 048252.0/ LEACHATE SAMPLE NO: H462624 SAMPLE MATRIX: LIQUID LIMS CLIENT: 0719 0597 PACE PROJECT: A71104602 PACE CLIENT: 000593 P.O. NO: VERBAL DATE SAMPLED: 04-NOV-97 DATE RECEIVED: 06-NOV-97 PROJECT MANAGER: Debbie Proctor ------------------------------------------------------------------------------------------------------------------------------- TEST DILUTION LN ------------------------------------------------------------------------------------------------------------------------------- CODE DETERMINATION FACTOR RESULT UNITS 1 OVZHE Volatiles - ZHE/Part 261 1,1-Dichloroethylene 10 < 0.05 mg/L 1,,,2-Dichloroethane 10 < 0.05 mg/L Benzene 10 < 0.05 mg/L Carbon tetrachloride 10 < 0.05 mg/L Chlorobenzene 10 < 0.05 mg/L Chloroform 10 < 0.05 mg/L Methyl ethyl ketone 10 < 0.10 mg/L Tetrachloroethylene 10' < 0.05 mg/L Trichloroethylene 10 < 0.05 mg/L Vinyl chloride 10 < 0.02 mg/L 3 S904 TCLP ZHE Leaching Procedure Done 4 S903 TCLP Bottle Leaching Procedure Done 7 G121L TCLP Organochlorine Pesticides Chlordane 1 < 5.0 ug/L Endrin 1 < 1.0 ug/L Heptachlor 1 < 0.5 ug/L Heptachlor epoxide 1 < 0.5 ug/L Lindane 1 < 0.5 ug/L Methoxychlor 1 < 5.0 ug/L Toxaphene 1 < 24.0 ug/L 9 G130L TCLP Chlorinated Herbicides 2,4,5-TP (Silvex) 1 < 5.0 ug/L 2,4-D 1 < 20.0 ug/L 22 OTCLP Semi-volatiles - TCLP/Part 261 1,4-Dichlorobenzene 1 < 0.01 mg/L 2,4,5-Trichlorophenol 1 < 0.01 mg/L 2,4,6-Trichlorophenol 1 < 0.01 mg/L 2,4-Dinitrotoluene 1 < 0.01 mg/L Hexachlorobenzene 1 < 0.01 mg/L Hexachlorobutadiene 1 < 0.01 mg/L Hexachloroethane 1 < 0.01 mg/L Nitrobenzene 1 < 0.01 mg/L Pentachlorophenol 1 < 0.05 mg/L Pyridine 1 < 0.01 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Ease Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 November 18, 1997 Report No.: 00065858 Section A Page 2 LABORATORY ANALYSIS REPORT CLIENT NAME: BAXTER HEALTHCARE CORP. SAMPLE ID: 93 048252.0/ LEACHATE SAMPLE NO: H462624 ------------------------------------------------------------------------------------------------------------------------------- TEST DILUTION LN CODE DETERMINATION FACTOR RESULT UNITS ------------------------------------------------------------------------------------------- ------------------------------- m-Cresol o-Cresol p-Cresol COMMENTS: Analysis performed by Pace Analytical Services, Inc. Houston Laboratory. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 1 < 0.01 mg/L 1 < 0.01 mg/L 1 < 0.01 mg/L Pace Analytical Services, Inc. 54 Ravenscroft Drive EaCe Aaaly ical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 November 18, 1997 Report No.: 00065858 Section B Page 1 SUPPLEMENTAL INFORMATION ------------------------------------------------------------------------------------------------------------------------------- LCSR DUP/MS ------------- SAMPLE PREPARATION ------------- ----- ------ SAMPLE ANALYSIS --------------- TEST BLNK MS/MSD LN CODE BATCH BATCH LR-METHOO DATE/TIME ANALYST LR~METHOD DATE/TIME ANALYST INSTRUMENT ------------------------------------------------------------------------------------------------------------------------------- SAMPLE ID: 93 048252.0/ LEACHATE SAMPLE NO: H462624 1 OVZHE 79548 79548 NA 19-8240B 11-NOV-97 1612 NZ GCMSY 3 S904 79463 79463 NA 19-1311 07-NOV-97 1200 D M 005EPE 4 5903 79464 79464 NA 19-1311 07-NOV-97 1200 D M 001EPE 7 G121L 79487 79403 19-35208 11-NOV-97 1300 S M 19-8080 12-NOV-97 0048 WZ 1248GC 9 G130L 79488 79404 19-8151 11-NOV-97 0900 S M 19-8151 13-NOV-97 1945 J M 0031GC 22. OTCLP 79486 79372 19-3510B 117NOV-97 1300 S M 19-8270B 13-NOV-97 1836 MSH 02ITSD LR Method Literature Reference 19 EPA -Test Methods for Evaluating Solid. Waste, 3rd ed, Nov. 1986 and updates REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. p 54 Ravenscroft Drive Pace Anal"'tip N Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 November 18, 1997 Report No.: 00065858 Section C Page 1 SURROGATE STANDARD RECOVERY ------------------------------------------------------------------------------------------------------------------------------- TEST PERCENT ACCEPTANCE LN ------------------------------------------------------------------------------------------------------------------------------- CODE SURROGATE COMPOUND RECOVERY LIMITS REF LN SAMPLE ID: 93 048252.0/ LEACHATE SAMPLE NO: H462624 2 $VOAW GC/MS VolatiLes Surrogates 1 4-Bromofluorobenzene 102 - Dibromofluoromethane 109 - Toluene-d8 100 - 8 $PSTW Pesticides Surrogate 7 DecachLorobiphenyL 83 - Tetrachloro-m-xylene 71 - 10 $HRBRW Herbicides Surrogate 9 2,4-Dichlorophenylacetic acid 121 - 23 $BNAL GC TCLP 40 CFR 261 BNA Surrogates 22 2,4,6-Tribromophenot 75 - 2-FluorobiphenyL 75 - 2-FLuorophenoL 49 - Nitrobenzene-d5 105 - PhenoL-d5 30 - p-TerphenyL-d14 90 - REPORT OF LA130RATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical 54RavensINIC 8 01 Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 November 18, 1997 Report No.: 00065858 Section D Page 1 LABORATORY CONTROL SAMPLE RECOVERY TEST LCS % LCSD % `ACCEPTANCE CODE DETERMINATION RECOVERY RECOVERY LIMITS RPD. ------------------------------------------------------------------------------------------------------------------------------- BATCH NO: 79486 OTCLP Semi-votatiles - TCLP/Part 261 1,4-Dichlorobenzene 46 2,4,5-Trichlorophenol 55 2,4,6-Trichlorophenol 55 2,4-Dinitrotoluene 75 Hexachlorobenzene 80 Hexachlorobutadiene 42 Hexachdoroethane 50 Nitrobenzene 70 P,entachlorophenol 65 Pyridine 35 m-Cresol 45* o-Cresol 46 p-Cresol * The compounds m-cresol and p-cresol co -elute. The reported result is the sum of the two. BATCH NO: 79487 G121L TCLP Organochlorine Pesticides Endrin 99 Heptachlor 104 Heptachlor epoxide 84 Lindane 91 Methoxychlor 143 BATCH NO: 79488 G130L TCLP Chlorinated Herbicides 2,4,5-TP (Silvex) 69 2,4-D 91 BATCH NO: 79548 OVZHE Volatiles - ZHE/Part 261 1,1-Dichloroethylene 105 Benzene ill Chlorobenzene, 104 Toluene 102 Trichloroethylene 102 SAMPLE NO: H394657 SAMPLE NO: H394659 SAMPLE NO: H394661 SAMPLE NO: H394772 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Ease Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 November 18, 1997 Report No.: 00065858 Section E Page 1 METHOD BLANK DATA ------------------------------------------------------------------------------------------------------------------------------- TEST CODE DETERMINATION RESULT UNIT BATCH NO: 79486 OTCLP Semi-volatiles - TCLP/Part 261 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dinitrotoluene Hexachlorobenzene Hexachlorobutadiene Hexachloroetharie Nitrobenzene Pentactilorophenol Pyridine m-Cresol o-Cresol p-Cresol BATCH NO: 79487 SAMPLE No: H394658 < 0.01 mg/L < 0.01 mg/L < 0.01 mg/L < 0.01 mg/L < 0.01 mg/L < 0.01 mg/L < 0.01 mg/L < 0.01 mg/L < 0.05 mg/L < 0.01 mg/L < 0.01 mg/L < 0.01 mg/L < 0.01 mg/L SAMPLE NO: H394660 G121L TCLP Organochlorine Pesticides Chlordane < 5.0 ug/L Endrin < 1.0 ug/L Heptachlor < 0.5 ug/L Heptachlor epoxide < 0.5 ug/L Lindane < 0.5 ug/L Methoxychlor < 5.0 ug/L Toxaphene < 24.0 ug/L BATCH NO: 79488 G130L TCLP Chlorinated Herbicides 2,4,5-TP (Sitvex) 2,4-D BATCH NO: 79548 SAMPLE NO: H394662 < 5.0 ug/L < 20.0 ug/L SAMPLE NO: H394773 OVZHE Volatiles - ZHE/Part 261 1,1-Dichloroethylene < 0.005 mg/L 1,2-Dichloroethane < 0.005 mg/L Benzene < 0.005 mg/L Carbon tetrachloride < 0.005 mg/L Chlorobenzene < 0.005 mg/L Chloroform < 0.005 mg/L Methyl ethyl ketone < 0.010 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive race An ixtscal Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 November 18, 1997 Report No.: 00065858 Section E Page 2 METHOD BLANK DATA ------------------------------------------------------------------------------------------------------------------------------- TEST CODE DETERMINATION RESULT UNIT ------------------------------------------------------------------------------------------------------------------------------- Tetrachloroethylene Trichloroethylene Vinyl. chloride REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. < 0.005 mg/L < 0.005 mg/L < 0.002 mg/L Pace Analytical Services, Inc. 54 Ravenscroft Drive 9 ace Analytical Asheville, NC 28801 9 Tel: 704-254-7176 Fax:704-252-4618 November 18, 1997 Report No.: 00065858 Section H Page 1 MATRIX SPIKE AND MATRIX SPIKE DUPLICATE DATA ------------ TEST -------------------•---------------------------- ---------------- MS MSD ------------------------------- --------------------- MS PCT MSD PCT CODE ------------------------------------------------------------------------------------------------------------------------------- DETERMINATION RESULT RESULT UNITS RPD RCVRY RCVRY BATCH NO: 79372 SAMPLE NO: H462307 OTCLP Semi-volatiles - TCLP/Part 261 1,4-Dichlorobenzene 0.14 0.06 mg/L 86** 70 28** 2,4,5-TrichlorophenoL 0.14 0.13 mg/L 7 70 65 2,4,6-TrichlorophenoL 0.14 0.12 mg/L 15 70 60 2,4-DinitrotoLuene 0.20 0.16 mg/L 22 100 80 Hexachlorobenzene 0.18 0.14 mg/L 25 90 70 HexachLorobutadiene 0.14 0.07 mg/L 64** 70 36** Hexachloroethane 0.12 0.15 mg/L 86** 60 24** Nitrobenzene 0.18 0.12 mg/L 40 90 60 Pentachlorophenol 0.14 0.13 mg/L 7 70 65 Pyridine 0.07 0.03 mg/L 78** 34 15 m-Cresol 0.25* 0.19* mg/L 25* 62* 48* o-Cresol 0.11 0.09 mg/L 20 55 45 p-Cresol * * mg/L * The compounds m-cresol and p-cresol co -elute. The reported result is the sum of the two. ** The MSD % recoveries are unacceptable. Acceptable method performance for these analytes have been demonstrated in the Laboratory control sample. BATCH NO: 79403 SAMPLE NO: H462571 G121L TCLP Organochlorine Pesticides Endrin 0.47 43 ug/L 8 47 43 Heptachlor 0.46 41 ug/L 8 46 41 Heptachlor epoxide 0.51 47 ug/L 4 51 47 Lindane 0.57 55 ug/L 4 57 55 Methoxychlor 0.85 78 ug/L 9 85 78 BATCH NO: 79404 SAMPLE NO: H462571 . G130L TCLP Chlorinated Herbicides 2,4,5-TP (Silvex) 37 36 ug/L 3 74 72 2,4-D 41 76 ug/L 60 81 151 BATCH NO: 79548 SAMPLE NO: H462624 OVZHE Volatiles - ZHE/Part 261 1,1-Dichloroethylene 498 443 ug/L 11 124 ill Benzene 418 385 ug/L 8 104 96 Chlorobenzene 373 348 ug/L 7 93 87 Toluene 384 365 ug/L 5 96 91 Trichloroethylene 354 339 ug/L 3 88 85 8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 1997 DIGESTER MONTH TEMP pH 1 19.9 6.74 2 19.8 6.06 3 18.8 6.82 4 17.0 5.57 5 19.7 6.54 6 23.0 6.19 7 26.5 5.60 8 25.0 6.53 9 23.6 4.80 10 20.6 6.33 11 14.2 6.18 12 11.7 6.65 Avg 19.98 n