WQ0005763_Application_20011229

vIVISION OF WATER QUALITY
GROUNDWATER SECTION
December 29, 2001
MEMORANDUM
To: Kim Colson
cc: .La Davfdson— Asheville(WS=RO--' —
Through: Debra Watts 1,7 -(
11
From: Brian Wootton Z01`
Subject: Tuckaseigee Water & Sewer Authority
Plant 1
Jackson County
WQ0005763 / GWO1214
The Groundwater Section has reviewed the subject renewal permit application for the continued
operation and production of Class A residuals derived from the Tuckaseigee Water & Sewer Authority
(Plant 1, Plant2, and Plant 3) to be applied on farm pastures. The residuals generated at Plants 2 & 3 are
trucked in liquid form to the digestor at Plant # I where they are combined with the residuals generated at
Plant #1. The residuals are then dewatered and treated with lime to meet the requirement of the permit
and 503 regulations. The rejiduals are stored on a concrete pad with a leachate collection, minimizing
any potential adverse impact to groundwater. The Groundwater Section recommends reissuance of the
permit with the following conditions:
1) Applicable Boundaries:
a) The COMPLIANCE BOUNDARY for the disposal system is specified by regulations in 15A
NCAC 2L, Groundwater Classifications and Standards. The Compliance Boundary for the
disposal system individually permitted after December 31, 1983 is established at either 250 feet
from the waste disposal area, or 50 feet within the property boundary, whichever is closest to the
waste disposal area. An exceedance of Groundwater Oualitv Standards at or beyond the
Compliance Boundary is subject to immediate remediation action according to
.0106(d)(2).
15A NCAC 2L
b) The REVIEW BOUNDARY is established around the disposal systems midway between the
Compliance Boundary and the perimeter of the waste disposal area. Any exceedance of standards
at the Review Boundary shall require action in accordance with 15A NCAC 2L .0106(d)(1).
2) Additional Requirements:
Any groundwater quality monitoring, as deemed necessary by the Division, shall be provided.
If there are any questions please call Brian Wootton at [phone].
GW01214.doc Page 1 of 1 GW01214.doc

�F, il� I- I "Lill Full, P V
MEMORANDUM:
TO: Brian Wootton
THROUGH: Landon Davidso �
9
FROM: Kay Dechant
DATE: December 19, 2001
SUBJECT: Permit Renewal
Tuckaseigee Water and Sewer Authority
GW01214 WQ0005763
Jackson County
Tfiis office has reviewed the subject permit renewal application and has no obicclion to renewal.
The permit renewal is 1'or land application of residuals with bulk distribution on farm pastures.
The residuals are treated by pasteurization and alkaline stabilization. Residuals are stored on a
concrete pad with leachate collection. No adverse impact to groundwater is anticipated.
Please contact me at [phone] if you have any comments or questions.

DIVISION OF WATER QUALITY
GROUNDWATER SECTION
TO: Z n no�5�—�`
o ,eC;- -� Regional Office
FROM: ,UryQ��
SUBJECT: Application for �Perndt Renewal,
New Permit
CO:1filfEWTS:
...
,'
_ 7 2001
DEC a
_ p 1
Permit Amendment
Repah-1,Alteration of Exist. Disposal System IDEH/
Facility Name: / . , N
T
County: ✓�GIC SO
Type of Project:
APPLICABLE PEFLN'IIT NO.s: WQ ��Q S �%,�5 GW O lal -{ .
DEH
EPA (CONST. GRANTS)
ANIMAL WASTE (D%VQ)
AtoC
The Groundwater Section has received 01SLY O\F (hill copy of the referenced permit application. A cop)' of the
application should have been sent to )'our Regional Water. Qualit}' Supervisor, so please use that cop)' for
vour review - IF A COPY HAS NOT BEEN RECEIVED IN' THE REGIO\AL. OFFICE, PLEASE LET ME
KNOW.
The Groundwater Section has received ONLY ONE. (11 copy of the referenced permit application. A copy of the
application should have been sent to ; DEH's Regional Soil Specialist, so please use
that copy for your review - IF A COPY HAS KNOT BEEN RECEIVED IN THE REGIONAL OFFICE, PLEASE
LET ME KNOW.
V//Tie Groundwater Section received two (2) copies of the referenced permit application. One copy of the
we received is attached.
application documents
Please review the application mate pals f r completeness. If you feel additional information is necessary, please
let me know no later than A copy of any formal request for additional information
%vill be forwarded to you.
If you do not need a additional information to complete your review, please provide your final comments
by��� f . If you request and/or receive additional information, vour tin11 comments
\9-98TRAN.SHL (rev. 9129198)

Division of Env* nmental Management
Da e
IUVWOIO ANO1 1
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To:Wag Supervisor
o
n
Permits & Compliance Unit
o
`Y N
Groundwater Section
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ca
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��s6i
From:--,— l Project_ Engineer
Permits & Engineering Unit
Water Quality Section
cn
Subject: Groundwater Review 0 yl � D T 7 /
Non -Discharge Application No. U 1p
Facility Name: _ �(� G/
County:
(GW #
Attached you will find plans, specifications, and supporting information
for the above project.
Please let me know whether you will or will not be conducting an
extensive review of the subject project by
If I can provide additional infonnation, please contact. me at ext. : �
........................ 0 0 • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • .
CKzwill
(1) The Groundwater Section El will not* conduct an e iv
review of the subject.
* Groundwater Section will not review application for the reason
listed below:
(2) A request for additional information will be forwarded to you by the
reviewer listed below.
GW Reviewer: VV Date:
9/6/90

w
TABLE OF CONTENTS
(1) Non -Discharge Permit Application Form
U C
(2)(a) Materials Handling Overview fy.
(b) Annual Distribution and Marketing Summary �'
(c) Information sheet supplied to users
(3)(a) TCLP Analysis
(b) Pollutant and Nutrient Analysis
(c) Fecal Coliform Analysis

SECTION ONE
NON -DISCHARGE PERMIT
APPLICATION FORM

I
State of North 'Carolina
Department of Environment, Health and T .--ural Resources
Division of Environmental Management
1. T T t n. A
lvun-�isc ua1�C rCrlrui rippiication Form
(THIS FORW MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL)
DISTRIBUTION OF RESIDUAL SOLIDS
This application is intended for facilities which are to be regulated under 40 CFR Part 503
GENERAL INFORMATION:
1. Applicant's name (please specify the name of the municipality, corporation indiddual, etc.):
2. Print owners or
3
4.
siSUZ 2 official's name and title (the person who is legally responsible for the facility and its compliance):
Mailing address:. ©X 6 D,51
City:
State: Zip:
Telephone Number:( Eyhl(�--n 1,
ong)
Application Date:
1
5. Fee Submitted: S [The permit processing fee should be as specified in 15A NCAC 2H .0205(c)(5).,
6. Specify how these residuals will be distributed: sold or giver. away in bags or other containers: lawn (bulk);
t f. /`__� Cn �
home garden (bulk); ._ other,
7. If the alternative for residual disposal consists of "surface disposal" as defined under 40 CFR Part 503. please complete the
-.:F.
application titled "SURFACE DISPOSAL OF RESIDUAL SOLIDS. Please identify iiF here is any storage of residuals in u
a surface impoundment or disposal thru landfilling. Explain:
S. Is the residual process facility also the generator? Yps; Nol j
v A� p� of residual process facility
9. Latitude: �1� a� P 5c) Longitude:
to Y local aovernment;
10. Specify whether the process facility is owned by: federal; private,
11. County where facility is located: Lqq(qc-k
II. PERMIT INFORMATION:
1. Application No. (will be completed by DEivf):
2. Specify whether project is: new; X— renewal*; modification
* For renewals, complete all sections included in the application. Engine,-
Signature and Seal not required for
renewals or if there is not any construction involved with the subject proj&,-'t-
3. If this application is being submittea a result of a renewal or m0fiaication to an xisting permit, list the existing permit
I / , � -(� �12
number.
�] Q' 3 and its ;-.,tee date D
FORivTDKS 06/94 Page 1 of 8

III. FACILITY INFORMATION (attach additional pages for additional (?urces of residuals):
1 %T- -.n �,f resid-als are =cratc cr prepW-ed:'�P _
2. Facility permit number: facility permit holder: G�J e 1
3. Specify whether facility in Section IIL 1 is owned by: federal; private; state; JL
local government;
4. Specify facility design flow: 1 ®5 mod; facility average daily flow: mgd;
Type of residual storage: _ fi:Q-N-0 hi C C. 40 d ;
Volume of residual storage: ,, (» C�,j
Length of residuals storage at facility: - days (the Division requires a minimum 30 days storage in units that
are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.);
Estimated volume of residuals: 9 '� -5 (dry tons/yr.);
5. If the residual process facility is not the same as the generator, please specify delivery frequency and quantity of residual to
be processed:
6. Facility contact (person familiar with residuals preparation): ���Qr, �/� ►�
7. Facility contact's telephone number:(
8. Location of treatment facility: N041-, PQQJiWQ1 State; County
9. Mailing address:
10. Specify the source of the residuals: 7x— treatment of domestic wastewater; treatment of industrial wastewater;
other (explain):
Attach an explanation of either the treatment process, manufacturing process, or how the waste is generated. Provide full
and complete details of the entire process.
11. Does the facility which generates the residuals have an approve[ pretreatment program? Yes; � No.
This includes facilities which are classified as a "Class I" facility (any publicly owned treatment works required, under 40
CFR 403.8, to have an approved, pretreatment program or any facility treating domestic sewage that is classified as "Class
I" by the appropriate federal or State authority)
IV. RESIDUALS INFORMATION (attach additional pages for additional sources of residuals):
1. Information for Hazardous Waste (RCRA) Determination. The information requested on the limitations specified below
pertain only to those residuals that are generated from a municipal wastewater treatment facility with industrial contribution
or active pretreatment program and from any other treatment facility with wastewater sources that include industrial sources.
a. Are any of the residuals covered by this application listed in 40 CFR 261.31-261.33? Yes, X No. If Yes.
list the number(s):
b. Do the residuals exhibit any of the four characteristics defined by 40 CFR 261.21-261.24? Yes; 4No.
Attach laboratory results for the Toxicity Characteristic Leaching Procedure Analyses, Reactivity, Ignitability, and
Corrosivity for each residual.
FORM: DRS 06/94 Page 2 of 8

Y
Note: If the following constituent levels (as determined by the Toxicity Characteristic Leaching Procedure Analyses) are
exceeded in the residuals or if the pH of the residual is not within the range listed below, the residual is by
definition a Hazardous waste. Chemical analyses must be made to Minimum Detection Levels.
PPM
_ PPM
Arsenic
5.0
Barium
100.0
Benzene
0.5
Cadmium
1.0
Carbon tetrachloride
0.5
Chlordane
0.03
Chlorobenzene
100.0
Chloroform
6.0
Chromium
5.0
o-Cresol
200.0
m-Cresol
200.0
p-Cresol
200.0
Cresol
200.0
2,4-D
10.0
1,4-Dichlorobenzene
7.5
1,2-Dichloroethane
0.5
1,1-Dichloroethylene
0.7
2,4-Dinitrotoluene
0.13
Endrin
0.02
Heptachlor (and its hydroxide)
0.008
Hexachlorobenzene
0.13
Hexachloro-1,3-butadiene
0.5
Hexachloroethane
3.0
Lead
5.0
Lindane
0.4
Mercury
0.2
Methoxychlor
10.0
Methyl ethyl ketone
200.0
Nitrobenzene
2.0
Pentachlorophenol
100.0
Pyridine
5.0
Selenium
1.0
Silver
5.0
Tetrachloroethylene
0.7
Toxapbene
0.5
Trichloroethylene
0.5
2,4,5-Trichlorophenol
400.0
2,4,6-Trichlorophenol
2.0
2,4,5-TP (Silvex)
1.0
Vinyl chloride
0.2
pH (2:1 vol./wt.): >2.0 s.u. - <12.5 s.u.
NOTE: IF ANY OF THE RESIDUALS MEET THE DEFINITIONS OF A
HAZARDOUS WASTE,
AS NOTED IN
EITHER "A" OR "B"
ABOVE, A PERMIT CANNOT BE ISSUED FOR
THAT MATERIAL AND IT SHOULD NOT BE INCLUDED
AS PART OF THIS
APPLICATION.
2. For each residual, please attach
a complete chemical analysis
of the material. This analysis T7 must be comprehensive enough
to completely characterize the
residual and must be based upon a review of the process that generates the material. If the
facility that will generate the
residual is not yet in operation, the characterization must be
based on similar existing
facilities and projection based
on the type of facility. The analysis must include a minimum
of the following parameters
and any other known and suspected
contaminants that are tributary
to the system.
Arsenic
Molybdenum
Calcium
Phosphorus
Cadmium
Nickel
-Magnesium
Potassium
Chromium
Selenium
Nitrate -Nitrite Nitrogen
Sodium
Copper
Zinc
% Total Solids
TTKN
Lead
Aluminum
pH
Mercury
Ammonia -Nitrogen
Plant Available Nitrogen
(by calculation)
FORM: DRS 06/94 Page 3 of 8

3. Wastewater residuals cannot be sold or given away if -the concentration of any pollutant in the residuals exceeds the ceiling
concentrations specified in the table below. Specify the pollutant concentration of these residuals (attach Iab analysis):
Pollutant
Pollutant Ceiling Concentration (ma/kg)
Pollutant Concentration (mg/kg)
Dry Weight Basis
Dry Wei htBasis
Arsenic
75
Cadmium
85
CI 9
e
Chromium
3000
Copper
4300
14
Lead
840
Mercur •
57
0
Molybdenum
75
Nickel
420
0 O
Selenium
100
W1-7
Zinc
7500
4. Provide, all applicable pilot studies and any bench scale tests performed on each residual source and the results, including
the approximate fertilizer equivalent.
5. Wastewater residuals can't be sold or given away in bags or other- containers for application to the land unless one of the
following options is satisfied.
Specify either A or B. Please be advised, if the residuals are to be sold or given away in bulk for application to
lawn or home garden then Option A is the only option.
A . The pollutant concentration of the residuals must be less than Pollutant Monthly Average Concentrations
listed in the table below.
A
Monthly Average Concentraton
PollutantConcentration
Pollutant
Dry Weight Basis (mg/kg)
Dry Weight Basis (m g/k) .
Arsenic
41
1.9
Cadmium
39
Chromium
1200
Copper
1500
Lead
300
Mercury
17
Nickel
420
Selenium
36
Zinc
2800
B . The product of the concentration of each pollutant in the residual and the annual whole residual application
rate for the residual shall not cause the Annual Pollutant Loading Rate to be exceeded.
In order for the Annual Whole Residual Application Rate (AWRAR) to be calculated the Annual Pollutant
Loading Rate (APLR) is divided by the pollutant concentration (PC) times 0.001 (a conversion factor) as
follows:
AWRAR = APLR
PC * 0.001
FORM: DRS 06/94 Page 4 of 8
i

Pollutant
Pollutant
Concentration
llry 1A'ei?ht Basis
(ma)
Annual Pollutant
Loading Rates
(APLR)
kJhectare
Annual Whole Residual
Application Rate
(AWRAR)
kg/hectare
Arsenic
2.0 "
Cadmium
1.9
Chromium
150
Copper
75
Lead
15
Mercury
0.85
Nickel
21
Selenium
5.0
Zinc
140
The AWRAR for the residual is the lowest AWRAR calculated. This is the maximum rate at which the
subject residual can be applied (to convert kg/hectare to lbs/acre multiply by 0.8924). Please specify
kg/hectare or lbs/acre:
FAVATZINVE
V . PATHOGEN AND VECTOR ATTRACTION REDUCTION INFORMATION (attach additional pages for
additional sources of residuals):
1. In order for the residuals Lobe Class A, in accordance with the pathogen requirements in 40 CFR 503.32(a), either Past a or
Part b D-d one of the options in Part c must be completed (please submit all lab analysis, test results and calculations):
a. A Fecal coliform density less than 1000 Most Probable Number per gram of total dry solids, or
b. A Salmonella sp. density less than 3 Most Probable Number per 4 grams of total dry solids.
c. In addition to Part a or Part b being met one of the following alternatives must also be completed. Please
specify 1, 2, 3, 4, 5a, 5b, 5c, 5d, 5e, 5f. 5g or 6 below being met:
1, time/temperature - an increased residuals temperature should be maintained for a prescribed period of time, in
accordance with the following guidelines. The results (D) shall be the amount of time, in days, that the residuals
shall remain at the given temperature:
T;..,n anri TPmrwrntnrP (;niriP1inee
Total Solids
Temperature (t)
Minimum Time
Equation
Notes
No heating of small
> or = 7%
> or = 500 C
> or = 20 minutes
D = 131,700,000
particles by warmed
100.14 t
gases or immiscible
liquid.
> or = 7%
> or = 500 C
> or = 15 seconds
D = 131,700,000
Small particles heated by
100.14 t
warmed gases or
immiscible liquid.
< 7%
> or = 500 C
> or =15 seconds
D=131,700,000
to
100.14 t
< 30 minutes
< 7%
> or = 500 C
>or = 30 minutes
D = 50,070,000
100.14 t
• FORM: DRS 06/94 Pace 5 of 8

2. &112Jine treatment - the pH of the residuals is raised to greater than 12 for'at least 72 hours. During this time, the
temperature of the residuals should be greater than 520 C for at least 12 hours. In addition, after the 72 hou:
period; the residuals are to be air dried to at least 50% total solids.
prior testing for Enteric Virus/Viable Helmin h Ova - the residuals are analyzed for the presence of enteric viruses
(Plaque -forming units) [pfu] and viable helminth ova. If the residuals are analyzed before the pathogen reduction
process and found to have densities of enteric. virus <1 pfu/4 grams of total solids and viable helminth ova <1/4g
total solids, the residuals are Class A with respect to enteric virus and viable helminth ova until the next
monitoring episode. If the residuals are analyzed before.the pathogen reduction process and found' to have densities
of enteric virus > or = 1 pfu/4 g total solids or viable helminth ova > or = 1/4 g total solids, and tested again after
processing and found to meet the enteric virus and viable helminth ova levels listed under "4" below, then the
processed residuals will be Class A with respect to enteric viruses and viable helminth ova when the operating
parameters for the pathogen reduction process are monitored and shown to be consistent with the values or ranges
of values documented
4. Dprior testing for Enteric Viols/Viable. H iminth Ova - if the residuals are not analyzed before pathogen reduction
processing for enteric viruses and viable helminth ova, the density of enteric viruses must be less than 1 pfu/4 g of
total dry solids and the density of viable helminth ova must be less than 1/4 g of total dry solids, or the residuals
must be treated by a "Process to Further Reduce Pathogens" or a "Process to Further Reduce Pathogens" equivalent .
process.
5. The "Processes to Further Reduce Pathogens" (PFRP) are described as follows:
a. Composting - using either the -within -vessel or static aerated pile composting methods, the temperature of the
residuals are raised to 550 C or higher for three days. Using the windrow composting method, the residuals are
raised to 550 C or higher for fifteen days. During the high temperature period, there will be a minimum of five
turnings of the windrow.
b. Heat Drying - residuals are dried by direct or indirect contact with hot gases to reduce the moisture content of
the residuals to 10% or lower. Either the temperature of the gas in contact with the residuals exceeds 800 C or
the wet bulb temperature of the gas in contact with the residuals, when the residuals leave the dryer, exceeds
800 C.
c. Heat Treatment - liquid residuals are heated to a temperature of 1800 C or higher for thirty minutes.
d. Thermopbilic Aerobic Digestion -liquid residuals are agitated with air or oxygen to n,?intain aerobic conditions
at residence times of ten days at temperatures of 550 C to 600 C.
e. Beta Rav Irradiation - residuals are irradiated with beta rays from an accelerator at dosages of at least 1.0
megarad at room temperature (ca. 200 Q.
f. Gamma Rav Irradiation - residuals are irradiated with gamma rays from certain isotopes such as 60Co and
137Ce, at dosages of at least 1.0 megarad at room temperature (ca. 200 Q.
Pasteurization - the temperature of the residuals is maintained at 700 C or higher for at least thirty minutes.
6. The residuals shall be treated in a process that is equivalent to a "Processes to Further Reduce Pathogens" (PFRP),
as determined by the permitting authority based on evaluations of the recommendations provided by the Pathogen
Equivalency Committee.
2. When residuals are to be sold or given away, one of the following vector attraction reduction requirements (a, b, c, d, e, f,
g, or h) described below must be met.
FSpecify the letter of the vector attraction reduction requirement that has been met (submit lab results, test results and
calculations). Any variation of the below must be described in full detail and attached.
a...: Aerobic or Anaerobic Digestion -The mass of volatile solids are reduced by at least 38%. Volatile solids reduction is
measured between the residuals, prior to stabilization, and the residuals ready for use or disposal. This criterion should
be readily met by properly designed and operated anaerobic digestors, but not as readily met by aerobic digestors.
Treatment facilities with aerobic digestors may need to meet the vector attraction reduction requirement through 19c or
19d.
FORM: DRS 06/94 Page 6 of 8

N A i
' h Anil r'. S. D � sti ", If 38% volatile solids reduction cannot be achieved. vector attraction reducuon can be
demonstrated by further digesting a portion of the previously digested residuals in a bench scale unit for an additional
40 days at 3U' C to 371 C. If, at the end of the 40 days, the volatile solids are reduced by less than 17%, vector
attraction reduction is achieved.
Aerobic Dim nn - If 38% volatile solids reduction cannot be achieved, vector attraction reduction can be demonstrated
by further digesting a portion of the previously digested residuals that have a solids content of 2% or less in a bench
scale unit for an additional 30 days at 200 C. If, at the end of the 30 days, the volatile solids are'reduced by less than
15%, vector atrraction reduction is achieved.
d- Aerobic Digestion - The specific oxygen uptake rate (SOUR) shall be equal to or less titan 1.5 milligrams of oxygen
per hour per gram of total dry solids at 200 C.
e. Aerobic Processes - The temperature of the residuals for at least 14 days shall be greater than 400 C. During this time,
�,he average temperature shall be greater than 450 C.
Alk ine S abi�i anon - The pH of the residuals is raised to 12 or higher by alkali addition and, without the addition of
more alkali, remains at 12 or higher for 2 hours and then at 11.5 or higher for an additional 22 hours.
g. Drying (stabilize solids) -The total solids of residuals that do not contain unstabilized.solids, and which are generated
in a primary wastewater treatment process, shall be equal to or greater than 75%. Blending with other materials is not
allowed to achieve the total solids percentage.
h. � ine (unstabi zed solids) - The total solids of residuals that contains unstabilized solids, and which are venerated in a
primary wastewater treatment process, shall be equal to or greater than 9017c. Blending with other materials is not
allowed to achieve the total solids percentage.
V I. GENERAL INFORMATION:
1. Please provide a brief narrative concerning materials handling, including the following:
a. How will the materials will be handled and transported from where the residuals were produced to where it will be
treated?
b. Where will the residuals be stored until processed?
c. How will leacate collection be handled?
d. What will be the duration of treatment?
e. Where will the 5 nal product be stored?
f. How long will the final product be stored before being distributed?
o. How will the final product be distributed (packaging)?
Please attach a marketability statement detailing destinations and approximate amounts of the final product to be
distributed.
3. Please provide either a label which shall be affixed to the bagged processed residual or an information sheet which shall be
provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the
following information:
a. The name and address of the person who prepared the residual that is sold or given away in a bag or other container for
application to the land.
b. A statement that application of the residual to the land is prohibited except in accordance with the instructions on the
label or information sheet.
c. A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
d A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
e. Information on all applicable buffers including a 10 foot buffer between application site and any public or private water
supply source (including wells) and any stream, lake, river, or natural drainage way.
f. The Annual Vr"nole Residual Application Rate (AWRAR) for the residual that does not cause any. of the annual
pollutant loading rates to be exceeded (if necessary).
FORM: DRS 06; 94 Page 7 of

Name and Complete Address of Engineering FL-m:
State:
Telephone Number: (-
n
Professional Engineer's Certification:
I, , attest that this application for
Zip:
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge.
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of t,`'is submitta'
package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have
reviewed this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
I, Q r) -� r Y-) attest that this application for (F-'
has been reviewed by me and is accurate and complete to the At of my knowledge. I understand that if all required parts of this
application are not completed and that if all required supporting information and attachments are not included, this application package
will be returned to me//s incomplety?
Signa
Date 0 - /01
THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND
MATERIALS, SHOULD BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
WATER QUALITY SECTION
PERMITS AND ENGINEERING UNIT
POST OFFICE BOX 29535
RALEIGH, NORTH CAROLINA 27626-0535
TELEPHONE NUMBER: [phone]
FORM: DRS 06/94 Paac 8 of 8

SECTION TWO
(a) MATERIALS HANDLING OVERVIEW
(b) ANNUAL DISTRIBUTION AND
MARKETING SUMMARY
(c) INFORMATION SHEET SUPPLIED TO
USERS

Materials Handling Overview
Tuckaseigee Water & Sewer Authority
Residuals are being generated at the following locations:
TWSA Plant #1(NC0039578)
97.48 dry tons*
TWSA Plant 42(NC0020214)
29.82 dry tons*
TWSA Plant #3(NC0063321)
19.04 dry tons*
*residuals production for the year 2000
All residuals generated at TWSA Plants 2 & 3 were trucked in liquid form to the digestor
at Plant #1 where they were combined with the residuals generated at Plant #1. This
residual source was then sampled for TCLP and then dewatered and treated with lime to
meet the requirements of the permit and 503 regulations.
Residuals thus treated are then stored on a concrete pad at the facility. Leachate and
runoff from this pad are returned to the head of the plant for treatment. The length of time
residuals are stored varies due to the time of year. Farmers using the product typically use
more at the start of the growing season and in the fall after hay has been harvested.
The product is usually distributed in bulk in user supplied spreader trucks. The annual
distribution and marketing summary for the year 2000 is attached with the application for
your review.

TWSA PLANT # 1
ANNUAL DISTRIBUTION AND MARKETING SUMMARY
2000
PART A
VOLUME IN DRY TONS
MONTH
ADMENDMENT/
BULKING AGENT IN
RESIDUAL
IN
PRODUCT
OUT
January
D
Februa
D
March
D
April
15-74
10.67
26.41
Ma
D
June
D
Jul
D
August
D
September
18.56
14.76
33-32
October
3.85
2.83
6.68
November
D
December
D
Annual Dry Tons
38.15
28.26
66.41
PART B
RECIPIENT INFORMATION
DATE
NAMES
VOLUME wet tons
INTENDED USE
2/23/00
John Frady
1
lawn & garden
3/1/00
Tim Crowe
3
pasture
3111/00
Smoky Mtn. Golf Club
40
ciolf course
3/23100
Tim Crowe
1
pasture
3/31/00
Jim Rhineheart
10
pasture
411/00
Jim Rhineheart
40
pasture
rM6/00
Dee Mull
14
ha field
Total109 ton x 54% solids= 58.9 dry tons

NGDA'A Dlvtsionr<:.4.08.
r. nomie
p
5
Gro:uer; Tucicaseigee Water & Sewer Copies To;
PO Box 1051
Sylva, NC 28779
��" •jpG�f41p.lJl'�'::p;
Wste nil sis e ort
y
5/ 9/01
Jackson County
S'iin le In >_
p -Re�ill,ts;,< arts,: er.mill '• ` � � J L
( ions'tin('e.$s,ofil��t'�745,�;no.te(1)+..;,-
L./ , ,.,, ,
,hah�n►f
� .� , l .. ,.
Sample 1D;
N
P K Ca M S Fe Un Zn Cu P NO U G'
Tolal 15634
5843 1799 201847 2712 2355 -4524 229 205 136 13.8
IN -N
---iste Corte;
-All14
,s
NO3
_
Na Ni Cd Pb Al Se Li pH SS C,N DAP6 CM6 ALS(lorrs)
Description:
OR-N
483 3.65 0.65 6.82 11.64 51.62 75.00 2.30
Munid al (Lime stab.)
Urea
.. :. F v: ,, ,'e:. :'': C.r E.. ..: ,::. .,C i,. r�:l", ..:.i. ":. .r,. IL , s >•', , viegT
Re it 1� {S
n {Q
'er:I lerti Lbs,to„- Grrsls
of etulaova,+.:�u
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il ! . ,U I.F 'r9. .L l
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.,!„ ,,. IP,2Qg... IA2Q ,. a �:....h1 i,4, S. v J ('e. .I}l/r,,..l� G,t s 13.: A:, A(o�t' -Cl L Y
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J.-.,. r( ,Nr .,Gr 'PG
fJ '
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J. - 'd.... J i r 1 tf:�4tL µF 1 �i.. :..JJ Yij,i114 5LF ,tl F{.P t, FJ .A ':): V: R T 1.
t �.:'S r Jt
•
7- :i , -.t. ..�'i.. : Y- V 1.: Ill{n".! • .. i
i , ,7: i :,w, I,t
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1. _. I . .:: l.. 4 -�:I;i
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{' l4;ll'iL�IG; Il Vll IVI IIilJ. tl"Ill'11-IIG IA II'HIIGIII 'a,''N�LI c'1NI1L YJ '1 '.\ IS{AVI 1 'V:U�:tll J11 t{'p l:?I'.ti1G�;�lIV_ti IG.N {V'.111VI1 + V I, /.IL IV.;111 US1L15 114L4:1H I -'• :1 - UN I Jl4 NIVQ;: 1 y!{llll V, I+111- � -v..A. Ih?1.4:.;1-Vl N 1 •IV'V .\J �11,V �11�,11 L,II LI,I - tt..,, �. v,
i
....1, : :.:: .,
�>ne.ton of ngrieull11M lrme,
- 5 c , .i, ty r %' .IS' 1 . !',. � ..L. _f .iii,,,: { ,':R I r 7t �•.,:. ,i a• s
These municipal waste residuals were prepared By: Tuckaseigee Water and Sewer Authority
1971 North River Rd,
Sylva. NC 28779
ph: 928-586-9318
fared under authority of North Carolina Dept, of Environment, Health and Natural Resources, (Division of Water Quality) Permit 4 WQ0005763
Application of this product to the land is prohibited except in accordance with the instructions on this information sheet.
(I) A minimum ten foot. buffer between application site and any public or private water supply (including wells) and any stream, lake, or river.
(2) Product shall not be applied to any site that. is flooded, frozen or snow covered:
(3) Adequate procedures shall be, provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters.
(4) Soil tests are recommended to identify optimum application rates.

SECTION THREE
(a) TCLP ANALYSIS
(b) POLLUTANT AND NUTRIENT
ANALYSIS
(c) FECAL COLIFORM ANALYSIS

ace Analytical m
www.pacelabs.cvm
aseigee Water & Sewer Auth
Po Box 1051
Sylva, NC 28779
Lab Project Number: 9319594
Client Project ID: TCLP
Pace Analytical Services, Inc.
54 Ravenscro(t Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Attn: Mr. Stan Bryson
Phone: [phone]
Solid results are reported on a dry weight basis
Lab Sample .6`. �' 93838647 Project Sample Number: 9319594-001 Date Collected: 04/11/01 00:00
Client Sam e �ID: RAW SLUDGE Matrix: Soil Date Received: 04/11/01 14:00
Parameters Results Units PRL Analyzed Analyst CAS# Ftnote Limit
Metals
RCRA Metals, ICP. TCLP Leach.
Method: EPA 6010
Arsenic
ND
mg/l
Barium
5.2 mg/l
Cadmium
NO
mg/l
Chromium
ND
mg/l
Lead
ND
mg/l
lenium
ND
mg/l
lver
ND
mg/l
Date Digested
Mercury, CVAAS. TCLP Leachate
Method: EPA 7470
Date Digested
Mercury. CVAAS. TCLP Leachate
Method: EPA 7470
Mercury
ND
mg/l
Wet Chemistry
Percent Moisture
Method: X Moisture
Percent Moisture
79.3
X
Paint Filter Liquids Test
Method: EPA 9095
Free Liquids
ND
ml/5min
Date: 05/03/01
Prep
Method:
EPA 3010
0.50
04/18/01
TRW
7440-38-2
0.10
04/18/01
TRW
7440-39-3
0.010
04/18/01
TRW
7440-43-9
0.020
04/18/01
TRW
7440-47-3
0.10
04/18/01
TRW
7439-92-1
0.10
04/18/01
TRW
7782-49-2
0.050
04/18/01
TRW
7440-22-4
04/13/01
Prep Method: EPA 1311
04/13/01
Prep Method: EPA 7470
0.00020 04/19/01 TRW 7439-97-6
04/13/01 AAB
Prep Method: EPA 9095
1.0 04/12/01 WWB
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

aceAnalyticafm
www.pacelabs.com
Lab Project Number: 9319594
Client Project ID: TCLP
PARAMETER FOOTNOTES
NO Not Detected
NC Not Calculable
PRL Pace Reporting Limit
Date: 05/03/01
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone. [phone]
Fax: [phone]
Page: 2
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

aceAnalytical m
www.pacelabs.com
Tuckaseigee Water & Sewer
Sytva, NC 28779
Attn: Mr. Stan Bryson
Solid results are reported on a dry weight basis
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax. [phone]
Lab Project Number: 9222096
Client Project ID: Tuckaseegee W&S/9319594
Lab Sample No: 93838647 Project Sample Number: 9222096-001 Date Collected: 04/11/01 00:00
Client Sample ID: RAW SLUDGE Matrix: Other Date Received: 04/11/01 14:00
Parameters Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
Metals
Volatile Organics, TCLP Leach.
Date Leached
GC VoLatiles
Pesticides, TCLP Leachate
Chlordane (Technical)
Endrin
Heptachlor
Heptachlor epoxide
gamma-BHC (Lindane)
Methoxychlor
Toxaphene
DecachLorobiphenyL (S)
Tetrachloro-m-xylene (S)
Date Extracted
Acid Herbicides, TCLP Leachate
4-n
2,4,5-TP (Silvex)
2,4-DCPA (S)
Date Extracted
GC/MS VoLatiles
Volatile Organics, TCLP Leach.
Vinyl chloride
Date: 04/24/01
Method: EPA
8260
Prep Method:
EPA
1311
0.00
1.0
04/17/01
LYS
Method: EPA
8081
Prep Method:
EPA
3510
ND
mg/l
0.00050
1.0
04/16/01
TSG
57-74-9
ND
mg/l
0-00050
1.0
04/16/01
TSG
72-20-8
ND
mg/l
0.00050
1.0
04/16/01
TSG
76-44-8
ND
mg/L
0.00050
1.0
04/16/01
TSG
1024-57-3
ND
mg/L
0.00050
1.0
04/16/01
TSG
58-89-9
ND
mg/l
0.00050
1.0
04/16/01
TSG
72-43-5
ND
mg/l
0.00050
1.0
04/16/01
TSG
8001-35-2
60
%
1.0
04/16/01
TSG
2051-24-3
55
%
1.0
04/16/01
TSG
877-09-8
04/14/01
Method: EPA
8151
Prep Method:
EPA 3510
ND
ma/l
2.0
2.0
04/20/01
TSG
94-75-7
ND
mg/l
0.20
2.0
04/20/01
TSG
93-72-1
122
%
1.0
04/20/01
TSG
19719-28-9
04/17/01
Method: EPA
8260
Prep Method:
EPA 8260
ND
mg/l
0.020
1.0
04/18/01 02:23
RPJ
75-01-4
Page: 1
'_aboratory Certification IDs Laboratory Certification IN
NC Wastewater 12 REPORT OF LABORATORY ANALYSISLaboratory
Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

aceAnalyticaf'
www.pacelabs.com
Lab Sample No: 93838647
Client Sample ID: RAW SLUDGE
Pace Analytical Services, Inc.
9800 Kincey Avenue. Sulte 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9222096
Client Project ID: Tuckaseegee W&S/9319594
Project Sample Number: 9222096-001 Date Collected: 04/11/01 00:00
Matrix: Other Date Received: 04/11/01 14:00
Parameters
Results
Units
PRL
Dilution Analyzed
Analyst CAS# Ftnote Limit
1,1-Dichloroethene
ND
mg/l
0.020
1.0
04/18/01
02:23
RPJ
75-35-4
2-Butanone (MEK)
ND
mg/l
0.40
1.0
04/18/01
02:23
RPJ
78-93-3
Chloroform
ND
mg/L
0.020
1.0
04/18/01
02:23
RPJ
67-66-3
1,2-Dichloroethane
ND
mg/L
0.020
1.0
04/18/01
02:23
RPJ
107-06-2
Carbon tetrachloride
ND
mg/l
0.020
1.0
04/18/01
02:23
RPJ
56-23-5
Benzene
ND
mg/l
0.020
1.0
04/18/01
02:23
RPJ
71-43-2
Trichloroethene
ND
mg/L
0.020
1.0
04/18/01
02:23
RPJ
79-01-6
TetrachLoroethene
ND✓
mg/L
0.020
1.0
04/18/01
02:23
RPJ
127-18-4
Chlorobenzene
ND
mg/L
0.020
1.0
04/18/01
02:23
RPJ
108-90-7
Dibromofluoromethane (S)
109
%
1.0
04/18/01
02:23
RPJ
1,2-DichLoroethane-d4 (S)
113
%
1.0
04/18/01
02:23
RPJ
17060-07-0
Toluene-d8 (S)
100
%
1.0
04/18/01
02:23
RPJ
2037-26-5
4-BromofLuorobenzene (S)
89
%
1.0
04/18/01
02:23
RPJ
460-00-4
Dioxin, High Resolution
Semivolatile Organics, TCLP
Method:
EPA 8270
Prep Method:
EPA 3510
Pyridine
ND`V
mg/l
0.50
1.0
04/17/01
18:55
YLJ
110-86-1
1,4-Dichlorobenzene
ND
mg/L
0.75
1.0
04/17/01
18:55
YLJ
106-46-7
2-MethylphenoL (o-Cresol)
ND
mg/l
20.
1.0
04/17/01
18:55
YLJ
95-48-7
Hexachloroethane
ND ✓
mg/l
0.30
1.0
04/17/01
18:55
YLJ
67-72-1
3&4-Methylphenol
ND
mg/l
200
10.0
04/17/01
18:55
YLJ
Nitrobenzene
ND✓
mg/L
0.20
1.0
04/17/01
18:55
YLJ
98-95-3
HexachLoro-1,3-butadiene
ND-"
mg/l
0.050
1.0
04/17/01
18:55
YLJ
87-68-3
2,4,6-TrichlorophenoL
ND ✓
mg/L
0.20
1.0
04/17/01
18:55
YLJ
88-06-2
2,4,5-TrichlorophenoL
ND J
mg/L
40.
1.0
04/17/01
18:55
YLJ
95-95-4
2.4-Dinitrotoluene
ND✓
mg/l
0.013
1.0
04/17/01
18:55
YLJ
121-14-2
Hexachtorobenzene
ND✓
mg/'t
0.013
1.0
04/17/01
18:55
YLJ
ii8-74-1
PentachlorophenoL
ND✓
mg/1
10.
1.0
04/17/01
18:55
YLJ
87-86-5
Nitrobenzene-d5 (S)
59
%
1.0
04/17/01
18:55
YLJ
4165-60-0
2-Fluorobiphenyt (S)
56
%
1.0
04/17/01
18:55
YLJ
321-60-8
TerphenyL-dl4 (S)
73
%
1.0
04/17/01
18:55
YLJ
1718-51-0
Phenol-d6 (S)
19
%
1.0
04/17/01
18:55
YLJ
13127-88-3
2-Fluorophenol (S)
28
%
1.0
04/17/01
18:55
YLJ
367-12-4
2,4,6-Tribromophenol (S)
73
%
1.0
04/17/01
18:55
YLJ
118-79-6
Date Extracted
04/14/01
Date: 04/24/01
Page: 2
NC Wastewater
Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs .
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

aczAnalyical'
www.pacelabs.com
PARAMETER FOOTNOTES
ND Not Detected
NC Not Calculable
PRL Pace Reporting Limit
(S) Surrogate
Date: 04/24/01
Pace Analytical Services, Inc.
9800 Kincey Avenue; Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9222096
Client Project ID: Tuckaseegee W&S/9319594
Page: 3
' aboratory Certification IN LaboratoryCertification IN
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Face` Anaw tical
AN
The Right Chet. y, The Right Solution®
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain-c stody is a LEGAL DOCUMENT. All relevant fields must be completed accLira
507631
Required Client Information: Section A Required Client Information: Section S Page: Ot To Be Completed by Pace Analytical and Client Section C
Com may, ,
To:
1�
Quote Reference:
�% JL•
�i
(j'L
S
Clilenit Information Checkquote/contract):
Addr
Invoice To:
Requested Due Date:
*TAT:
Project Manager:
Turn around times less than 14 days subject to
Project #:
laboratory and contractual obligations
Rush Turnaround Surcharge.
and may result in a
•
Pr6lect Name:
Profile
Turn Around Time (TAT) in calendar
days.
V
Phone ^
ax _ (�
Project Number:
Requested
Analysis
Section D Required Client Information:
Valid Matrix Codes
p
p
Preservatives
MATRIX
CODE
w
w
//��
S A M P L E I D
WATER
SOIL
WT
SL
w
O
w
¢ w
w 1"'
�_ w
�
OIL
OL
U
-J
-J
c
Z
One Character per box.
AIR WIPE
AR
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"
=
O
(A—Z, 0-9 / .—�
Sample IDs
TISSUE
TS
¢
(j
c
Oz
U
Co
�
F- MUST BE U�N7IQUE
OTHER
OT
�
mm / dd / yy
hh: mm a/p
�
�
_
_
=
z
Z
Remarks / Lab ID
y�
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.o
r�°
u n
•'�
T y'
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µ,b
�~
„.•"°'r
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?tt'"Yr
44'
t
:•y
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Un
• • •
•
•
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• • • • .
.
Temp in °C:
Y
Received on ICE:
Y / N
Sealed Cooler:
Y / N
Samples Intact:
Y / N
Additional Comments:
of SAMPLER:
PRIN
_
YA
9 •1
" \
t
SIGNATUR
S PLER:
DATE Sign M / D / W)
SEE REVERSE SIDE FOR INSTRUCTf a Pace Analytical Services, Inc. /ForVCOCOI.XLS 12/99
nRtrinlnl

1 }
ace Analytical'
www.pacelabs.com
May 03, 2001
Mr. Stan Bryson`.
Tuckaseigee Water & Sewer Auth
PO Box 1051
Sylva;=NC 28779
RE: Lab Project Number: 9319620
Client Project ID: 1, ►► V-rve..,
Dear Mr. Bryson:
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Enclosed are the analytical results for sample(s)received by the laboratory on April 11, 2001. If you have any
questions concerning this report, please feel free to contact me. -
Sincerely,
Katherine Jimison
Project Manager
Enclosures
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

llacieAnalyficaf"
www.pacelabs.com
,:aseigee Water & Sewer Auth
Pb Box 1051
Sylva, NC 28779
Attn: Mr. Stan Bryson
Phone: [phone]
Lab Project Number: 9319620
Client Project ID: COMPOST
Solid results are reported on a dry weight basis
Lab Sample No:.. 93839439 Project Sample Number: 9319620-001
Client Sample ID: TWSA LIME RESIDUAL Matrix: Soil
Pace Analytical Services, Inc.
54 Ravenscroff Drive
Asheville, NC 28801
Phone: 828,254.7176
Fax: [phone]
Date Collected: 04/11/01 09:00
Date Received: 04/11/01 14:00
Parameters
Results
Units
PRL
Analyzed
Analyst CAS#
Metals
Metals, ICP, trace -level
Method:
EPA 6010
Prep
Method:
EPA 3050
Aluminum
10000
mg/kg
44.
04/23/01
TRW
7429-90-5
Arsenic
1.8
mg/kg
1.7
04/23/01
TRW
7440-38-2
Cadmium
0.99
mg/kg
0.17
04/23/01
TRW
7440-43-9
Calcium
280000
mg/kg
17.
04/23/01
TRW
7440-70-2
chromium
7.9
mg/kg
0.87
04/23/01
TRW
7440-47-3
pper
91.
mg/kg
0.87
04/23/01
TRW
7440-50-8
Lead
7.8
mg/kg
1.7
04/23/01
TRW
7439-92-1
Magnesium
3000
mg/kg
17.
04/23/01
TRW
7439-95-4
Molybdenum
2.3
mg/kg
0.87
04/23/01
TRW
7439-98-7
Nickel
4.0
mg/kg
0.87
04/23/01
TRW
7440-02-0
Potassium
1500
mg/kg
87.
04/23/01
TRW
7440-09-7
Sodium
400
mg/kg
44.
04/23/01
TRW
7440-23-5
Zinc
150
mg/kg
3.5
04/23/01
TRW
7440-66-6
Date Digested
04/17/01
Mercury, CVAAS
Mercury
Selenium, AAS Furnace
Selenium
Date Digested
Wet Chemistry
Percent Moisture
Percent Moisture
Date: 05/03/01
Method: EPA 7471
0.90 mg/kg
Method: EPA 7740
ND mg/kg
Method: % Moisture
42.8 %
Prep Method: EPA 7471
0.035 04/19/01 TRW 7439-97-6
Ftnote Limit
Prep Method: EPA 3050
0.87 (14/23/01 TRW 7782-49-2 1
04/17/01
04/13/01 AAB
Page: 1
Laboratory Certification IDS REPORT OF LABORATORY ANALYSIS Laboratory Certification IDS
NO Wastewater 40 TN Drinking Water 02980
NO Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

• / 1
aceAnalyticafm
www.pacelabs.com
Lab Sample No: 93839439
Client Sample ID: TWSA LIME RESIDUAL
Parameters Results
Pace Analytical Services, Inc.
54 Ravenscroff Drive
Asheville, NC 28801
Phone: [phone]
Fax; 828.254,4618
Lab Project Number: 9319620
Client Project ID: COMPOST
Project Sample Number: 9319620-001 Date Collected: 04/11/01 09:00
Matrix: Soil Date Received: 04/11/01 14:00
Units PRL Analyzed Analyst CAS# Ftnote Limit
Total Percent Solids
Method: EPA
160.3
Percent Solids
57.0 %
Ammonia, Soil
Method: EPA
350.3
Nitrogen, Ammonia
760.
mg/kg
Total.'Kjeldahl Nitrogen, Soil
Method: EPA
351.2
Nitrogen, Kjeldahl, Total
4370
mg/kg
Nitrogen, Nitrate plus Nitrite
Method: EPA
353.2
Nitrate -Nitrite (as N)
87.
mg/kg
Nitrogen, Nitrite, Soil
Method: EPA
354.1
Nitrite as N
NO
mg/kg
Phosphorus, Total, Soil
Method: EPA
365.2
"hosphorus
76.3
mg/kg
Fecal Coliform MPN Solid
Method: SM 92216/E
8.74
8.74
8.7
0.87
2.19
Coliform, Fecal ND 2
Nitrogen, Total Method: Standard Methods
Nitrogen 4500 mg/kg 1.0
Plant Available Nitrogen Method:
Nitrogen 960 mg/kg 1.0
Date: 05/03/01
Prep Method: EPA 160.3
04/13/01 AAB
Prep Method: EPA 350.3
04/25/01 JDA 7727-37-9
Prep Method: EPA 351.2
04/19/01 JDA
Prep Method: EPA 353.2
04/20/01 JDA 7727-37-9
Prep Method: EPA 354.1
04/30/01 AAB
Prep Method: EPA 365.2
04/13/01 MPS 7723-14-0
Prep Method: SM 922113/E
04/12/01 KAS
04/30/01 JDA 7727-37-9
04/26/01 JDA 7727-37-9
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 2
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

r �
ace Anaoyticafm
www.pacelabs.com
PARAMETER FOOTNOTES
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax.- 828.254.4618
Lab Project Number: 9319620
Client Project ID: COMPOST
ND Not Detected
NC Not Calculable
PRL Pace Reporting Limit
[1] Analyzed by —trace metals ICP, resulting in elevated PRL at 0.020 mg/l.
Date: 05/03/01
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 3
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

CHAIN -OF -CUSTODY, / Analytical Bequest uocumenz
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Paco— Ana'Mit1cal
The Right Chemistry, The Right SohationO
Rn-7r,'Ir,)
Page: Of
eJV f VJL.
Section C
Required Client Information: Section A
Required Client
Information:
Section B
To Be Completed by
Pace Analytical
and Client
Company ,
— X T-1
port To:
:'v(J ' —
j
'� J ! tYl
,—) ;� �
Client Information Check quote/contract):
Quote Reference:
Adcjr f�
/
Invoice To:
I
Requested Due Date:
'TAT:
Project Manager:
1
ifs
P.O.
Turn around times less than 14 days subject to
Project #:
laboratory and contractual obligations
Rush Turnaround Surcharge.
and may result in
a
O�
Project Name:
Profile
Turn Around Time (TAT) in calendar
days.
Phogs �, t �•••
flax 7 ��
•,,,
Project Number:
Requested nay I •\ ry ^'
_ 4 '
yam-
Section D
Required Client Information:
q
Valid Matrix Codes
o
o
Preservatives
MATRIX
WATER
CODE
WT
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w
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W
SAMPLE
ID
SOIL
SL
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¢
0 J
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One character per box.
OIL
WIPE
AIR
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f=
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(A—Z, 0-9 / .—)
TISSUE
TS
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/ Lab ID
IW_
Sample
IDS MUST BE UNIQUE
OTHER
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mm / dd / yy
hh: mm a/p
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< :
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Temp in IC:
` , `�
1!
%: ;r
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VI ` .Q
Received on ICE:
Y / N
Sealed Cooler:
Y / N
Samples Intact:
Y / N
Additional Comments:
w�
' NATQkE
IS
PRINT
Name oPL
SIGNATURE
of S
DATE Signed: (MM / DV/ YY)
SEE REVERSE SID, IR INSTRUCTIONS /Pace Analytical Services, Ind Fo JC01.XLS 12/99
0

r -
,,AceAnalytical-
www. pacelabs. com
l_'aseigee Water & Sewer Auth
10 Box 1051
,yl va, NC 28779
,ttn: Mr. Stan Bryson
hone: [phone]
olid results are reported on a dry weight basis
ab Samp'le No: 93774685
lient Sample; -ID: TWSA LIME RESIDUAL
arameters Results
et Chemistry
Pace Analytical Services, Inc.
54 Ravenscrott Drive
Asheville, NC 28801
Phone: [phone]
Fax- 828.252.4618
Lab Project Number: 9317865
Client Project ID: TWSA LIME RESIDUAL
Project Sample Number: 9317865-001 Date Collected: 01/23/01 08:30
Matrix: Soil Date Received: 01/23/01 13:25
Units PRL Analyzed Analyst CAS# Ftnote Limit
Percent Moisture Method: X Moisture
Percent Moisture 44.8 t;
Fecal Coliform MPN Solid Method:.SM 9221B/E
Coliform, Fecal ND 2
v
Date: 01/30/01
r-,
_aboratory Certification IDs
UC Wastewater 40
VC Drinking Water 37712
O1/26/01 JMS
Prep Method: SM 9221B/E
01/23/01 KAS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

laneAnalyfical'"
www. pacelahs. cam
_�aseigee Water & Sewer Auth
0 Box 1051
ylva, NC 28779
ttn: Mr. Stan Bryson
hone: [phone]
olid results are reported on a dry weight basis
ab Sample No: 93799815
lient Sample ID: TWSA LIME RESIDUAL
arameters Results
et Chemistry
Percent Moisture
Percent Moisture
Fecal Coliform MPN Solid
Col iform. Fecal
413
Date: 03/05/01
Pace Analytical Services, Inc.
54 Ravenscroll Drive
Asheville. NC 28801
Phone. [phone]
Fax: 828,252.4618
Lab Project Number: 9318507
Client Project ID: TWSA LIME RESIDUAL
Project Sample Number: 9318507-001 Date Collected: 02/23/01 09:44
Matrix: Soil Date Received: 02/23/01 12:20
Units PRL Analyzed Analyst CAS# Ftnote Limit
Method: X Moisture
46.5 2
Method: SM 9221B/E
ND 2
02/28/01 AAB
- Prep Method: SM 9221B/E
02/23/01 KAS
Page: 1
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

mace Analytical "o
www pacelahs.com
iyckaseigee Water & Sewer Auth
PO Box 1051
Sylva, NC 28779
Attn: Mr. Stan Bryson
Phone: [phone]
Solid results are reported on a dry weight basis
Lab Sample No: 93820009
Client Sample ID: TWSA LIME RESIDUAL
Parameters Results
Wet Chemistry
Percent Moisture
Percent Moisture
Fecal Coliform MPN Solid
Coliform, Fecal
Date: 03/30/01
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax. [phone]
Lab Project Number: 9319068
Client Project ID: TWSA LIME RESIDUAL
Project Sample Number: 9319068-001 Date Collected: 03/21/01 10:00
Matrix: Soil Date Received: 03/21/01 16:37
Units PRL Analyzed Analyst CAS# Ftnote Limit
Method: X Moisture
47.7 X
Method: SM 922113/E
ND 2
03/27/01 TRW
Prep Method: SM 922113/E
03/22/01 KAS
Page: 1
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

ace Analytical
www.pacelabs.com
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9320539
Client Project ID: Effluent Analysis
Lab Sample No: 93874469 Project Sample Number: 9320539-002 Date Collected: 05/18/01 08:00
Client Sample ID: TWSA LIME RESIDUAL Matrix: Soil Date Received: 05/18/01 12:25
Parameters ,Results Units PRL Analyzed Analyst CAS# Ftnote Limit
Wet Chemistry
Fecal Coliform.MPN Solid
Col iform,: Fecal
Date: 05/30/01
Method: SM 922113/E Prep Method: SM 92218/E
ND 2 05/18/01 KAS
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 2
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

kttn. Mr. Stan Bryson
phone: [phone]
Solid results are repoi
_ab Sample No: t`.-�93913853
:lient Sample 'ID: TWSA LIME RESIDUAL
parameters Results
let Chemistry
Percent Moisture
Percent Moisture
Fecal Coliform MPN Solid
Coliform, Fecal
Date: 07111JOl
aboratory Certification IDS
,JC Wastewater 40
NC Drinking Water 37712
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone_ 828.254.7176
fax.- 828.254.4618
Lab Project Number: 9321567
Client Project ID: LIME RESIDUAL FECAL
on a dry weight basis
Project Sample Number: 9321567-001 Date Collected: 06/28/01 12:00
Matrix: Soil Date Received: 06/28/01 15:44
Units PRL Analyzed Analyst CAS# Ftnote Limit
Method: % Moisture
45.6 %
Method: SM 9221B/E
ND
07/09/01 AAB
Prep Method: SM 9221B/E
2 06/29/01 KAS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N �CoN
D�
Page: 1
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

4ttn: Mr. Stan Bryson
phone: [phone]
iolid results are repo
_ab Sample No
:lient Sample
Jet Chemistry
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9321807
Client Project ID: TWSA LIME RESIDUAL
on a dry weight basis
93921765 Project Sample Number: 9321807-001 Date Collected: 07/12/01 08:00
TWSA LIME RESIDUAL Matrix: Soil Date Received: 07/12/01 09:08
Results Units Report Limit —_ Analyzed CAS No. Ftnote Rea limit
Percent Moisture Method: X Moisture
Percent Moisture 47.7 % 07/16/01 AAB
Fecal Coliform MPN Solid Prep/Method: SM 9221B/E / SM 9221B/E
Coliform, Fecal ND 2 07/12/01 KAS
Date: 07/20/01
Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
..«oq
Page: 1
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone. [phone]
Fax. [phone]
Lab Project Number: 9322813
Client Project ID: TWSA LIME RESIDUAL
Attn: Mr. Stan Bryson
Phone: [phone]
Solid results are reported on a dry weight basis
Lab Sample No_ `-'93957645 Project Sample Number: 9322813-001 Date Collected: 08/21/01 07:00 .
Client Sample =ID: TWSA LIME RESIDUAL Matrix: Soil Date Received: 08/21/01 12:04
Wet' Chemi stry
Percent Moisture
Percent Moisture
Fecal Coliform MPN Solid
Coliform, Fecal
Date: 09/03/01
` Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Method: % Moisture
41.0 % 08/27/01 AAB
Prep/Method: SM 9221B/E / SM 9221B/E
ND 2 08/21/01 KAS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
aC[o9
S
Page: I
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030