WQ0004298_2000 Residuals Annual Report_20010219

Uj a 0 OANN UAL L ND APPLICATION CERTIFICATION FORM
Permit Number nn Coun c c.0 Year Q 0 0
Facility Name (as shown on rmit) c' -
Land Application Operator_J_ n er `,�s��� Phone,# 30
Land application of residuals as allowed by the above permit occurred during the past calendar year
YES NO. If NO, skip Part I and Part II and proceed to the.certification. Also, if residuals were generated but
not land applied, please attach an explanation on how the residuals were-liandledj
Part I
*Total number of application fields in permit.
*Total number of fields land application occurred during
*Total amount of dry tons applied during the year for all
•Total number of acres land application occurred durin the ear
Part II 4'
Facility was compliant during calendar year )LOcOwith all conditions of the land appli, ? erifde
(incl ding but not limited to items 1-12 below) issued by the Division of Water Quality 'A,19�Trr,' . ��
YES NO. 0
IF NO, PLEASE PROVIDE A WRITTEN DESCRIPTION WHY THE FACILITY WAS NOT COMPLIANT, THE DATE$1l l
EXPLAIN CORRECTIVE ACTION TAKEN. ��
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil
PH of at least 6.0 or the limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year
and three (3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are
attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as
=cility
ed and three (3) copies of certified laboratory results are attached.
6. did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part -
503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13. (applicable to 40 CFR Part 503
regulated facilities)"
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14
were complied with. (applicable to 40 CFR Part 503 regulated facilities)
8. All operations and maintenance requirements in the permit were complied with or, in the case of a
deviation, prior authorization was received from the Division of Water Quality. .
9. No contravention of Ground Water Quality Standards occurred at a monitorinwell or
explanations of violations are attached to 'include appropriate actions and remediations.
10.Vegetative cover as specified in the permit was maintained on this site and the crops grown were
removed in accordance with the crop management plan.
11.No runoff of residuals from the application sites onto adjacent property or nearby surface waters
has occurred.
12.All buffer requirements as specified on the permit were maintained during each application
of residuals.
"I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY KNOWLEDGE
AND BELIEF, TRUE, ACCURATE, AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR
SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINES AND IMPRISONMENT FOR
KNOWING VIOLATIONS."
rkw % —800
:Pe&rm*eeName and Title (type or print)
Signature of Preparer Date
(if different from Permittee)
C5.;2 ��-
Signature of Permittee Date
Signature of Land Applier Date
(if different from Penmittee and Preparer)
Note: Preparer is defined in 40 CFR Part 503.9(r) DEM FORM CF (10/94)
t

ANNUAL RESIDUAL SAMPLING SLwmARy FORAM
Attach this form to the corresponding laboratory analysis.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number
Facit)ty Name
WIVES #
of wo a (teddm G* two"
WViPTP Name
O H Qq 40,
I�ex
i o wY, 0 liic`
Residual Analysis Data .
Date Sued (grab) or
Date Convcsiled I I
I Percent Solids I ! • "/C I
PAt�AMETEFiS (Mato dry welahtl
Laboratory 1
REM
X
. SK31V111URE OF -
t pREFARERI DATE
• 1 CwW, WNW putatty of taw, that We dmmmt was prepared UWW my t kwftn at sapwvlelan to Wcordenw wMt a "atom
==qmMW peraonnet pwpwV gathered and wtwted the t ftm at." au mawd. I am wrap that Htene tma bralu rep wee hdorm norh httdttdbw the possIbmy of ftoea and htprimor rut fix krom g aohtiom...
.
DEM FORM Sar 10f'94)

Laulh Lhrilloomental selvices
! Michael Ladd
! 75 Bison Lane
Murphy, NC 28906
f Robbinsville Lab [phone]
Madison County Lab [phone]
Residence [phone]
i ..-
Namp and Address of Facility:
Date: 1/4/01
T6Wn'of Mars Hill WWTP '
Sample Collector: RS
P.010 BOX 368
Date and Time Sample Received: 11/29/00 12:20 PM
Mars Hill, NC 28754
Date and Time Sample Collected: 11/27 & 29/00
Att: Robert Sams
Date and Time Sample Analyzed: < MHT
Land!Application Analyses - Note: All results in
mg/Kg Dry Basis unless otherwise noted.
Test
Aer. Dig Sludge
Dry Bed Sludge
Soil Site #1
Soil Site #2
Report Limit
Method
Units
ACIDITY
1.0 meq/100g
0.3 meq/100g
2.0
SM5210B
mg/L
TOTAL SUSPENDED RESIDUE��,
.
1.0
SM2540D
mg/L
CATION EXCHANGE CAPACITY
,1,ff
9.4 meq/100g
5.8 meq/1009
1
SM9222D
per 100m1
PH ;j,
6.5
iJ, 6.7 f
6.3
6.6
0-14
SM4500H+
units
AMMONIA NITROGEN
59.8 mg/I
I 959
0.5
SM4500NH3F
mg/L
NO2[ NO3-n'' "`
19.6 mg/l
, 35.0 I
1.0
SM5520B
mg/L
TOTALXJELDAHL NITROGEN
358 mg/l
t
4770 1 I
SCA
mg/L
TOTAL PHOSPHOROUS
223 mg/1
26.9 I j
27
13
SCA
mg/L
TOTAL RESIDUE
797 mg/I
18% (�
79%
82%
1.0
SM2540B
mg/L
% HUMIC MATTER
j 1
1.6%
2.9%
1.0
SM2130B
NTU
% BASE SATURATION - K
!
4.2
4.7
1.0
SM2540C
mg/L
-H
f. j
10.6
5.9
- Mg
f
23.4
30.4
- Ca
!i 1 j
61.8
59.0
PLANT AVAILABLE (surface)
3126.7
i 1657.8 i
10
SM2510B
umhos/cm
NITROGEN- PPIVI DRY WT (subsurf)
3799.4
11, 2137.3 •I
0.1
SM4500CIG
mg/L
TEMPERATURE
14 1 I
SM2550B
deg C
MIXED LIQUOR SUPSPENDED SOLIDS
(1 i ;!
1.0
NIA
mg/L
MAGNESIUM
77.5 mg/I
5850 I 1
995
571
SCA
mg/L
SODIUM
69.5 mgll
i 540
< 12.6
< 11.7
SCA
mg/L
CADMIUM
0.0030 mg/I
! 7.48 ?
< 1.25
1.17
SCA
mg/L
CHROMIUM
I
0.116 mg/I
29.9
73.7
167
SCA
mg/L
COPPER
2.855 mg/I
1 447 I
33.8
33.8
SCA
mg/L
LEAD
0.386 mg/I
j + 65.2
12.5
11.4
SCA
mg/L
NICKEL
0.125 mg/I
1 17.1 I t
19.6
27.3
SCA
mg/L
ZINC;
4.076 mg/1
I 6.6 I;
63.4
44.3
SCA
mg/L
CALCIUM
115.0 mg/I
i j 13400 1
1380
844
SCA
mg/L
POTASSIUM
143.5 mg/I
4J 5020
754
213
SCA
mg/L
ALUMINUM
94.0 mg/I
1 1 16500 I
SCA
mg/L
ARSENIC
0.025 mg/1
d l < 5.34
< 1.25
<1.17
SCA
mg/L
SELENIUM
0.045 mg/I
I 1 11.8 j
< 1.25
< 1.17
SCA
mg/L
MI DENUM
< 0.010 mg/l
, ;, < 5.34 ?
< 1.25
< 1.17
SCA
mg/L
MI RY
< 0.0002 mg/I
,� 0.989
< 0.125
< 0.122
SCA
mg/L
N.C. Laboratory ID# 352 Analyzed�By' MB
Lab Supervisor: Michael J. Ladd; EES-Robbinsville Certified By: 17itAa , l"

awl
i
M
_
• '
1�7iii'Lr�
1
l DATE i LWACM 1
. ..
TOTALS: PAN P
As.
1w
cr At
�•,w.�T-�N:T
Pb
^�.wwni�i
Kb
.•Ti1V;�}Uy1P�LL'R'FiF�++C-AYF��.uc.�ly
t
se
h
AMW
Icuffal3 s 3 s o a 5a 5 J o °1 4.30 Qa F o
Q.oa,9
0. l y- J,
o a 4
v.cc
<a oQ
o, ©L$
v, a
5�9
3 ►9
0 :� t 3�I.q
�,50g
0,e57
<9.36
I �7 E�
0�10
17
OEM FORM FBF 0")
(SiONAIUM OF LAND APPUEP4 — - - DATE
1 089". under PWAIW of kw. 09 tbb dOOMMA Im prepared under my die d1w dr supsmWm in amordaaea with a sy stm
dadptsd w =me that gmUsd pwoomd pmpe t>r QammW and swebawd Ow k torprom submu" t sm-a"m that awe are
Pia for WAMUft On blomWion, Meingi" tfts pussibit of fkm and imprbmamd twr tnwM bg vblstbna."

ANNUAL LAND APPL iON FIELD SUMMARY FORM
PLEASE MAKE A COPY OFTHIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A'N/A' IN A BLANK OR BOX WHEN OUCABI.E.
FACILITY NAME TO t/1 R� YY1(a I- s /YC o`TAPP
5� 5 l .
PERMIT # 000a q p
OWNER L4 r r-y Co r ii SITE # CATION EXCHANGE CAPACITY (non 503 regulated facilities only)
OPERATOR -2n P r'}' S rx m S FIELD # O ACRES PERMITTED O ACRES UTILIZED
TOTAL DRY TONS APPLIED (ANNUAL) 3
DATE or
MONTH
rte- a
Gallons /or Cubic Yards
s ecif
Dry Tons
'Per Acre
Residual Source
5►�
o
/o Solids
Not Do;
use'Avereges
%
Mineralization
Rate
°0
Application
Method
(surface or
Injection)
5u4
If.'reporting byY ^o th`keep"1he e`
smogh ry
" 'ldail-records•on site 1: 4".'
Crop
r
Total
-7 o
per Acre
Ind=Rainfal
pest 24 Hrs.
site CondlUons
(Dry, Moist, Wet)
Lime Application
DATE I LBS/ACRE
TOTALS: -
__ __- .. ... .............. :,,_ ,.._ ..a.o�Jha.ne'Y.r:;,,�:.t; .��. ."t7s�? '�?:'i'��8�'. �"' ":�::`�."•�,:o.e='
PAN P
rSe
Annual 70 —7 1- L4-73 V, I
As Cd Cr Cu
14 '7 b. 5 (1,o 1 (7 U 1�5 6062 0.983
Pb Hg
0,100
Mo Ni
0,01 i1 0,03
Zn
6.bi4 5
Cumulative
0597 0, 100 0,3269 675
1,593 0-0044,
,6259
3460,7706 G.3579
0,593
Permit Limit lbs./acre/ ear - 1st Crop / 2nd Crop
Permitted Cumulative Pollutant Loading Rate lbs./acre
a 5
50d
�a 5
a 5 0
(SIGNATURE F LAND APPLIE DATE
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
DEM FORM FSF (2/95) significant penaitles for submitting false information, including the possibility of fines and Imprisonment for knowing violations."

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name _ f au->Ijc, t' 1ca,r� ��►�� Permit Number WQnoci4 Q °I
WWTP Name T�y,),n ���yYi�,,� �I ;1� LA_l �T '� NPDES # N C 0 C) 51 I S 1
Monitoring Period: From 1 / 1 12000
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed
Class A
Alternative 1 Alternative 2 Alternative 3
Alternative 4 Alternative 5 Alternative 6
Class B V/_
Altemative 1 Alternative 2 Alternative 3
If applicable to alternative performed (class B only) indicate "Process to Significantly Reduce Pathogens":
s ,_ ✓ Aerobic Digestion _ Air Drying _ Anaerobic Digestion _ Composting _ Lime Stabilization
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
In Sludge
Pathogen Deity
Number of
Exceedences
Frequency of
Analysis
Sample
Analyyl
Technique
Minimum
Geo. Mean
Maximum
Units
Fecal Cordortn
per gram of total
solids or 2 x 106
� ( �
�� n
6 0-v a
of" .m
O
COX
/(`�Type
V R+.�
CFU per gram
of total sorids
1000 MPN
Per gram of
total solid
(dry weight)
salmonella
bacteria (n
lieu of fecal
coliform) I
3 MPN per 4
grams total
solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed
Option 1 Option 2 Option 3 Option 4 Option 5
Option 6 Option 7 Option 8 Option 9 Option 10
No vector attraction reduction options were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
°I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note If you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system'designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
�L(1Cl Ir�� 111, �1CA o� 1 LAY]'iC QOr z+ L1•(',
Pre er Na and Title (typrint) Land Applier Name and Title (if applicable)(type or print)
a5 o i
Signature of Preparer Date Signature of Land Applier (if applicable) .Date
DEM FORM RF (10/94)

Earth Environmental Services
ROBBINSVILLE LAB [phone]
MADISON COUNTY LAB [phone]
RESIDENCE [phone]
December 5, 2000
NC ID #474, #352
Mr. Robert Sams
Town of Mars Hill
P.O. Box 368
Mars Hill, NC 28754
Dear Mr. Sams:
Following is a report of laboratory analyses for digester sludge samples received 1 1/29/00:
Colony Counts
# Sample Date Coliform Densities (colonies/gram) Percent Total Solids 0.1 mL 0.01 mL 0.001 ml,
1
11/20/00
79,000 Colonies/Gram
1.25 %
104
5
0
2
11/21/00
78,000 Colonies/Gram
1.16 %
90
10
0
3
l 1/22/00
72,000 Colonies/Gram
1.37 %
89
16
4
4
11/24/00
86,000 Colonies/Gram
1.27 %
109
11
l
5
l 1/27/00
63,000 Colonies/Gram
1.27 %
75
13
1
6
11/28/00
80,000 Colonies/Gram
1.20 %
95
11
0
7
l 1/29/00
30,000 Colonies/Gram
1.46 %
44
0
0
Geometric mean for all seven samples: 67,000 colonies/gram. Thank you for your business. If you have
any questions or need additional sample analyses performed, please call.
Respectfully submitted,
a�'- -60V
Michael J. Ladd
Laboratory Director

f�T

Michael Ladd
75 Bison Lane
1 Murphy, NC 28906
Robbinsville Lab [phone]
Madison County Lab [phone]
I Residence [phone]
Namaland Address of Facility: Date: 1/4101
Town of Mars Hill WWTP Sample Collector: RS
P.O. Box 366 Date and Time Sample Received: 11/29/00 12:20 PM
Mars! Hill, NC 28754 Date and Time Sample Collected: 11/27 & 29/00
Aft: Robert Sams Date and Time Sample Analyzed:______ < MHT
Land Application Analyses - Note: All results in mg/Kg Dry Basis unless otherwise not d'��-`'\
Test !
Aer. Dig Sludge
Dry Bed Sludge,
-!Soil Site #1
Soil Slte,#2
Report Limit
Method
Units
ACIDITY
,
1.0 meq/100g
0.3 meq/1OOg
2.0
SM5210B
mg/L
TOTAL SUSPENDED RESIDUE
5r
1.0
SM2540D
mg/L
CATION EXCHANGE CAPACITY
9.4 meq/100g
5.8 meq/100g
1
SM9222D
per 100ml
OH .
6.5
6.7
j +
6.3
6.6 ',.
0-14
SM4500H+
units
AMIMONIA NITROGEN
59.8 mg/I
959 i 1
0.5
SM4500NH3F
m /L
NO2', 'NO3-n• -
19.6 mg/l
35.0 ,
1.0
SM5520B
mg/L
TOTAL'�KJELDAHL NITROGEN
358 mg/I
4770
!
SCA
mg/L
TOTAL PHOSPHOROUS
223 mg/I
26.9 ; 4
27
13
SCA
mg/L
TOTAL RESIDUE
797 mg/1
18% i
79%
82%
1.0
SM2540B
mg/L
% HUMIC MATTER
1.6%
2.9%
1.0
SM2130B
% BASE SATURATION - K
11
4.2
4.7
1.0
SM2540C
I -H
i
10.6
5.9
-Mg-
23.4
30.4
-Ca
61.8
59.0
PLANT AVAILABLE (surface)
3126.7
1 1657.8
10
SM2510B
umhos/cm
NITROGEN- PPM DRY WT (subsurf)
3799.4
2137.3
0.1
SM4500CIG
m IL
TEMPERATURE
SM2550B
deg C
MIXED LIQUOR SUPSPENDED SOLIDS
1.0
N/A
mg/L
MAGNESIUM
77.5 mg/I
5850
995
571
SCA
mg/L
SODIUM
69.5 mg/l
540
< < 12.5
< 11.7
SCA
mg/L
CADMIUM
0.0030 mg/l
7.48
? < 1.25
1.17
SCA
mg/L
CHROMIUM
0.116 mg/I
29.9
f 73.7
157
SCA
mg/L
COPPER
2.855 mg/I
447
33.8
33.8
SCA
mg/L
LEAD'
0.385 mg/I
66.2
; 12.5
11.4 j
SCA
mg/L
NICKEL
0.125 mg/I
17.1
19.6
27.3 _j
SCA
mg/L
ZINC
4.075 mg/l
6.6
53.4
44.3
SCA
mg/L
CALCIUM
115.0 mg/l
13400
f 1380
844
SCA
mg/L
POTASSIUM
143.6 mgll
5020
I 754
213 ;
SCA
mg/L
ALUMINUM
94.0 mg/I
16500
SCA
mg/L
ARSENIC
0.025 mg/I
< 6.34
j1 < 1.25
< 1.17
SCA
mg/L
SELENIUM
0.045 mg/I
11.8
i i < 1.25
< 1.17
SCA
mg/L
MC IENUM
< 0.010 mg/1
< 5.34
to < 1.25
< 1.17 f +
SCA
mg/L
ME tY
< 0.0002 mg/I
0.989
�< 0.125
< 0.122ji
SCA
mg/L
N.C. Laboratory ID# 352
Lab Supervisor: Michael J. Ladd; EES-Robbinsville
Analyzed By:1111,B/�
Certified By: %j%L.-, oho(?