WQ0004298_1998 Residuals Annual Report_19990217

err` 'Oki
ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit Number W QOaan q-'n C
Facility Name (as shown on rmit) Q ty �"' sc�
Land Application Operator ` �`i"'`K Fl f
�'� Phone #,
Lan application of residuals as allowed by the above permit occurred during the past
-- YES NO. If NO, skip' Part I and Part II and proceed to ft rt�ica ' not and applied, please attach an explanation on how the residuals were "6d� " n' Also, if residu
Part IW. _U
*Total number of application fields in permit. _}Ma i
•Total number of fields land application occurred d u=i=1grtkte y'ar�� f r
•Total amount of dry tons applied during the year for all al Jhca0.9 r% it s
PP
Year 1 99 %i
N
*Total number of acres land application occurred during the year. ~ L
Facility was compliant during calendar ye aaz M with all conditions of the land application permit
(inc ding but not limited to items 1-12 below) issued b the Division of Water
YES NO. Y Quality
� •but` y rft',•,^.
(III s+� f.-`.`•, ,
IF NO, PLEASE PROVIDE A WRITTEN DESCRIPTION WHY THE FACILITY WAS NOT COMPLIANT THE DATES AND
EXPLAIN CORRECTIVE ACTION TAKEN.
I. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil
PH of at least 6.0 or the limit specified in the permit. {
3. Annual soils analysis was performed on each site receiving residuals during the past calendar e
and three (3) copies of laboratory results are attached.
P year'.."
4. Annual TCLP analysis was performed.and three (3) copies of certified laboratory results are
attached.
5. All other monitoring was performed 'in accordance with the permit and reported durin the . year s
required and three (3) copies of certified laboratory results are attached. g Y as
6. The facility did not exceed any of the Pollutant Concentratioxi Limits in Table 1 of 40 CFR Part
503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13. (applicable to 40 CFR Part 503
re ated facilities)
7. All general requirements in 40 CFR Part 503.12 and management practices '
P in 40 CFR Part 503.14
were complied with. (applicable to 40 CFR Part 503 'regulated facilities)
8. All operations and maintenance requirements in the permit were complied with or, in the case of a
deviation, prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitorin well or
explanations of violations are attached to include appropriate actions and remediations.
10.Vegetative cover as specified in the permit was maintained on this site and the cro s own were
removed in accordance with the crop management plan. P
11.No rtmoff of residuals from the application sites onto adjacent
has occurred. property or nearby surface waters
12.All buffer requirements as, specified on the permit were maintained during each application
,of residuals.
"I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY KNOWLEDGE
AND BELIEF, TRUE, ACCURATE, AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR .
SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINES AND IMPRISONMENT FOR
KNOWING VIOLATIONS." r -
i4 I lid rw , OLAw-w t&M
Pe tee Name and Title (type or print)
Signature �bf Permittee Date
--gnature of Preparer Date
(if different from Pennittee)
Note: Preparer Is defined In 40 CFR Part 503.9(r)
Signature of Land Applier Date
Of different from Permittee and Preparer)
DEM FORM CF (10/94)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding laboratory analysis.
Please note that your permit may contain additional parameters to be analyzed than those requ
ked to be summarized on this form.
Permit Number
Facility Name
NPOES #
or WO # (residual only facHiffes)
WVVTP Name
CQ0 H Q 9 S
In n
LIS
Residual Analysis Data
Date Sampled (grab) or T77, T q.17
Laboraiorycar-'��1n V;q-dy1
2)
3)
x
"7 �- I- `-i�
(SIGNATURE OF PREPARER)
ATE
"I certify, under pansity of taw, that this docufnam was Pr@Pamd under my direction or supervision
In accordance with a systern
designed to assure - that qua'Wad Personnel property 9MMmW and OWuBt@d the Information submitted, .1 am -wars Vurt there are
.-significant penaltim.for submitting false Information, lncfucffng the po**Mft of fh"snd
Imprisonment for knowing violations."'
DEN FORM SSF (10194)
4
A

OIL &wKS'wFJ
EARTH ENVIRONMENTAL SERVICES OF ROBBINSVILLE
MICHAEL LADD
75 Bison Lane
Murphy, North Carolina 28906
Robbinsville Lab [phone]
Name and Address of Facility
Madison County Lab [phone]
Residence [phone] Date 9 / 19 /
9 8
Town of Mars Hill
Sample Collector RS
P.O. Box 368
Date and Time Sample Received 8/12/98
11 : 35 AM
8:50=
Mars Hill, NC 28754
Date and Time Sample Collected 8/12/98
9 : 30 AM
Name of ORC
Date and Time Sample Analyzed <MHT
Att : Robert Sams -
Land Application Analyses-Note:All results in Mg/Kg Dry Basis
TEST
Soil -Site #1
Soil -Site #2
Drying Bed Sludg
Aerobic Dige
ter.
089820•' •
089821--
089819
Sludge 08981
Manganese
270
160
710
560
mg/L
Acidity
5.6me!�/100g
0.4 mere/100
mg/L
.Cation Exchange
Capacity
17.9 me /100g
8.7 mea/100g
per
100ml
Corrosivity pH
5.3
6.7
units
40NIA
IOGEN
1680
1990
mg/L
NO2 & NO3-N
21
<280
mg/L
Total Kjeldahl
17000
83000
mg/L
-Nitro en
TOTAL
PHOSPOROLIS
384
21.2
10300
18300
mg/L
Base
K-5.4 mg-24.5
K-6.7mg-25.7
mg/L
%
Ca-39. 0 H-31 .0
Ca-63. 2 H-9, 5
_Saturation
% Total
88.5%
83.5%
13.2%
0.9%
mg/L
Solids
6alciuin
1800
220
14000
15000
mg/L
1/ Potassium
2300
1200
4400
<11000
mg/L
r
Sodium
1100
1400
2000
3000
mg/L
Magnesium 3000 1600 5300 4500 umho�
% Humic at er cm
!(Organic) 1.8% 2.6/ mg/L
rl-allu riva.Li-
able Nitrogen
LABORATORY ID # 352
ANALYZED BY !�
CERTIFIED BY
MICHAEL LADD, LABORATORY SUPERVISOR, EES OF ROBBINSVILLE
°C
Surface-5457 urface-25,298
Subsurface-6297 Oubsurface261293
PPM Dry Wt. PPM Dry Wt.
D009353.FDB

7 ( j 1,
1.1
IN
MI
Name and Address of Facility
Town of Mars Hill
P.O. Box 368
Mars Hill, NC 28754
Name of ORC
Att: Robert Sams
EARTH ENVIRONMENTAL SERVICES
MICHAEL LADD
115 Fall Branch Road
Murphy, North Carolina 28906
[phone]
[phone]
Date 9/19/98
RS
P
Date and Time Sample Received _8/12/98 11 : 35 AM
8:50-
Date and Time Sample Collected 8/ 12/ 9 3-9 : a e—T m
Date and Time Sample Analyzed4MHT
Sam le Collector
Land Application Analyses-Note:All results in Mg/Kg Dry Basis
TEST
Soil-gite #1
089820
Soil -Site #2
089821
Drying Bed SludgeAerobic
089819
Digester
Sludge. 08981
Arsenic
1.1
.{0.6
3.8
<56
mg/L
CADMIUM
1.1
11.2
<7.6
<110
mg/L
CHROMIUM
50
14
30
220
mg/L
COPPER
25
41.2
2500
670
mg/L
LEAD
34
36
76
'-""1100
mg/L
NICKEL
12
8.4
120
<560
mg/L
ZINC
46
37
910
1100
mg/L
alenium
0.56
<'0.6
4.6
Z5.6
mg/L
?rcury
0.058
0.044
2.1
<2.2
mg/L
ALUMINUM
19000
25000
17000
12000
mg/L
)lybdenu
18
20
-_38
< 560
mg/L
Analyzed By:
Laboratory: #352
;ertified By: ��✓e c
Michael Ladd, Laboratory Supervisor, EES
170930604

�; .. llient Available Nitrogen (PAN) calculations and land application area requirements;,
CONSTITUENTS
M -DRY WEIGHT
TIN
93 0 0 0
AMMONIA-N
NO3-NO2-N
O
1. Mineralization Rate.(MR) �-D
(These values -can be established for the specific residual or default values can be used for domestic wastewater trcatment
residuals. If actual value's arc established, attach the documentation, The default values am as follows):
Unstabilized Primary and Secondary Residuals 40%
Aerobically Digested Resduals 30%
Atuterobicalty Digested Residuals 20%
Composted Residuals 10%
(If the default values are used, attach an explanation as to why the specific chosen default value is appropriate.)
2. Com lete the following calculations for the application method proposed (Please note, the Mineralization
Rate [MR] should be utilized In the following calculations as a decimal):
PAN for Surface Application
PAN [(MR) x (TKN - NH3)) + ,S x (NH3) +. (NO3•No2-N)
FAN0 A( 53'000 - -���� )1+.5x(
PAN = 2 �5 1 Z 9 PPM My Weight
PAN for Subsurface Application
PAN - [(MR)x(TKN - NH3)l + (NH3) + (NO3-NO2-N)
PANet[ + 3' ,x( g3 o vo - )r5-,o)+ o
PAN a— 2(0). Z 93
PPM Dry Weight
3. Total PAN to be land applied per year
Total dry tons of residual to be land applied per year;

r r < C ... Plant Available Nitrogen (PAN) calculations and land application area requirements., ,
CONSTITUENTS
M - DRY WEIGHT
TIN
/ 7 OD
AMMONIA-N
! �l
NO3-NO2-N
z
L. Mineralization Rate(MR) o %
Crhese values -can be established for the specific residual or default values can be used for domestic wastewatcruvatment
residuals..W actual value's are estabUsbed, attach the documentation. The default values are as follows);
UnstaWlized Primary and Secondary Residuals 40%
Aerobically )Digested Residuals' - 30%
Aaaaobically Dlgest A.Residuals 2096
Composted Residuals 10%
(If the default values are used, attach an oxelanation as to why die specific chosen default value is appropriate.)
2. Complete the following calculations for the applicadon method proposed (Please note, the Mineralization
Rate [MR] should be utilized in the following calculations as a decimal):
PAN for Surface Application
p�N . KW x (TKN - NH3)] .+ .5 x (NH3) + (1403-NO2-N)
FAN 1 r 30 'x( /Its 0 o A- 9-0)]+.5x( /��� )+ z 1
PAN = 5 4-5 ) PPM Dry weigbt
PAN for , Subsurface Application
PAN-1(MR)xC= = NH3)] + (NH3) + (NO3-NO2-N)
PAN=L # 3 0 x(
PAN = 2 7 PPM Dry Weight
3. Total PAN to be land applied per year
Total dry tons of residual to be land applied per year;
glp���

Pace Analytical Services Inc
Pace Analytical A shevilleRaven, villeC Drive
ANC 28801
54 Rovanacroft Orive 'xxP7H�2-at1t*
Mr. Michool Ladd
Earth Environrantal Services
7S aison Lana
Murphy, VC 28906
701868/EARTH ENVR.
Asheville, MC 28001
/honer (71K) ZU-7176
Fox: (71%) ZS2-4618
v�"e ` o p J;�,iu
1
9
k P [\1
.0 Jemi fer Jones
-1
The above charps are for the following "too:
SptA► 0eacription/client 10 Received
9321589 tttiA0e9a18-s/12/96 011/13/98
9321S97 EEfrNOg9a19-8/92/9E 08/13/98
08/31/98
Pace Anatyticat Services, Inc.
NM 8922
P.O. Box 1450
Minneapolis, MN 55485-8922
Cue Upon Receipt
2
L REPORT OF LABORATORY ANALYSIS L�'O�ry Certification IDs
R M�tM 40 TN Drinking Water 02980
NC Dnn#rp Millar 37712 This ah�l uob except �n full,FL Environmental 96317
SC Environmental tA8900 without"wridsn olm nt of Pace Maiytical S rvices, Inc.

Pace Analytical Services, Inc '
Pace AnniNlicel A Rsheville, avine. C Drive
ANC 2880 t
Tel. [phone]
Fax:[phone]
Aupwt 31, 19"
Mr. Micheal Ladd
Earth Envirartllental Services
75 Wson Lana
Murphy, MC 2M
RE: ►ste Project Mustier: M494
Client Project 10: Siudge Analysis
Dear Mr. Ladd:
Enclosed are the results of anslyses for saWlets) received by the laboratory on August 13, 1998. if you have any
questions concerning this report, please feel free to contact w.
Sincerely,
N4�v 0
Jennifer Jones
Project NwwWr
Enclosures
e L�waim
� � � Laboratory Certification Ids
,C arn�ano w 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
This report shall not bo FL Environmental 96317
� EiMronmsintal avo�oo po ral:roduoad, excap! in full,
without the written consent of Pace MalytIcal Services, Inc.

Pace Analytical Services, Inc
54 Ravenscroit Drive
Pace Aiielytlral Asheville, NC 28801
TO 704-254-7176
Al Fax. [phone]
arth Environamintat Services
5 Bison Lane
lurphy, NC 28906
,ttn: Mr. Michael Ladd
hone- [phone]
iolld results are reported on ■ dry weight basis
DATE: 05/31/98
PAGE: 1
Pace Project Number: 93494
Client Project ID: Sludge Analysis
,aca Sample No: 9321589 Date Collected: 08/12/98 Matrix: Soil
;lient Saitopte 10: EESM089818-8/12/98 Date Received: 08/13/98
parameters Results Units PRL Analysed Analyst CASH Footnote$
letal s
M , MCP
Method: EPA 6010
Prep Method: EPA 305D
,irxan
12000 mg/kg
1100
06/20/98
KEK 7429-90-5
iva
ND
mg/kg
110
08/20/96
KEK 7440-43-9
ciuR
15000 mg/kg
1100
08/20/98
KEK 7440-70-2
n
ND
me/ke
220
08/20/98
KEK 7440.47-3
670
mg/kg
110
08/20/98
KEK 7440.50.8
ND
mg/kg
1100
08/20/98
KEK 7439-92-1
us
tl�kk*L'i
4500
mg/kg
2200
00/20/98
KEK 7439.95-4
se
560
mg/kg
110
08/20/98
KEK 7439-96-5
nun
ND
me/kg
560
05/20/98
KEK 7439-98-7
ND
mg/kg
560
08120/98
KEK 7440-02-0
ssiva
ND
flog/kg
11000
08/20/98
KEK 7440-09-7
un
Re
3000
mg/kg
2200
08/20/98
KEK 7440.23-5
1100
mg/kg
110
08/20/98
KEK 7440-66-6
Date Digested
08/17/98
Ars c, AAS Furnace
Method: EPA 7060
Prep Method: EPA 3050
emit
ND
nog/kg
56
05/25/98
KEK 7440-38-2
Dote Digested
08/17/"
Nor ry, CVAAS
Method: EPA 7471
Prep Method: EPA 7471
*c ry
ND
mg/kg
2.2
08/24/98
KEK 7439-97.6
Setum, AAS Furnace
Method: EPA 7740
Prep Method: EPA 3050
S anion
ND
mg/kg
56
08/24/98
KEK 7782-49-2
Date Digested
00/17/98
at lstry
LA of Coafficoffigin on
Laboratory Car_rificatian IDs
ND ----A""'teir 40
REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Dunking VMNer 37712
SC EnwkwYoental go=
This report shag not be napr duced, except in full, FL Environmental 9F3t 7
WWWW the wrhlen ooneerst of Paoe Analytkal Services, Inc.

Pace Analytical Services. Inc
54 Ravenscroft Drive
Asheville, NC 28601
QJ
L '
'ace Semple No: 9321589
A i ent Sample 10: L'Ellti089818.8/12/90
Tel: [phone]
Fax:[phone]
DATE: 08/31/98
PACE: 2
Pace Project Number: 93494
Client Project ID: Sludge Analysis
Date Collected: 08/12/98 Matrix: Soil
Date Received: 08/13/98
ammeters
Rer:ulto Units PAL
......... ..........
Analyzed
........
Analyst CAS#
----- ..........
Footnotes
...........
................................
Percent Moisture
..........
Method: % Moisture
Prep Method:
Percent Moisture
99.1 %
08/17/98
KEK
Tota Percent Solids
Method: EPA 160.3
Prep Method: EPA
160.3
Cent Solids
0.9 %
08/14/98
KEK
is, Sof•l
Method: EPA 350.3
Prep Method: EPA
350.3
Itrogen, Ammonia
1990 mg/kg 200
08/19/98
TRW 7727-37-9
To ta Kjeldehl Nitrogen, Soil
Method: EPA 351.3
Prep Method: EPA
351.3
rogen, Kjeldahl, Total
83M mg/kg 35000
08/24/98
eSP
Nitri:JW, Nitrate plus Nitrite
Method: EPA 353.2
Prep Method: EPA
353.2
ste-Nitrite (as N)
ND mg/kg 290
08/24/98
HP 7727-37-9
Phoa50orus, Total, Soil
osphorus
Method: EPA 365.2
18300 mg/kg 6"
Prep Method: EPA 365.2
00/21/98 MPS 7723-14-0
LA of womeam REPORT OF LABORATORY ANALYSIS TN 1)fi torn Water
I 0
NL ---- � TN Drinking Water 02980
NC DdrildSC Erv*o w VV9 M 37712 This �n shall not be nW d. except in full, FL Enviianmental 96317
g9010 without the written ooneent of Pepe Anafy foal Services, 1 no.

Pace Analytical Services. Inc
54 Ravenscroll Drive
Asheville. NC 28801
pit tiD Tel- 704.254-7176
Fax:[phone]
liJ ( DATE: 08/31/98
PAGE: 3
Pace Project Number: 93494
,• 9� ` Ctlent Project 10: Sludge Anstyais
Pace Sseple No: 9321597 Data t:011ecteds 00/12/98 Matrix: Soil
:Bent Sample 1D.- ECIOM819-8/12/" Date Received: 08/13/98
,aramleters Results Units PRL Analyzed Analyst CAS: Footnotes
................................ ........ ........ -...- ---------- ----------
totals
Metals, 1CP
At i ww
ium
cim
allu
mar
LIi
at
W um
US
Date Digeated
Are ic, AAS Furnace
sonic
Date Digested
Merc y, CVAAS
ircury
Selen us, AAS Furnace
enium
Date Digested
let Chemistry
Percent Moisture
Percent Moisture
Tots Percent Solids
rcent Solids
e, sail
trowm, Aemonis
Method: EPA 6010
Prep
Method: EPA 3050
17M
mg/kg
76
08/20/98
KEK
7429-90-5
NO
mg/kg
7.6
08/20/98
KEK
7440-43-9
14000
mg/kg
76
08/20/98
KEK
7440-70-2
30
mg/kg
15
08/20/98
KEK
7440-47-3
2500
me/kg
7.6
08/ZO/98
KEK
7440-50-0
76
mg/kp
76
08/20/98
KEK
7439-92-1
5300
mg/kV
ISO
Oa/20/98
KEK
7439-95-4
710
m4/kg
7.6
08/20/98
KEK
7439-96-5
ND
mg/kip
38
08/20/98
KEK
7439-95-7
120
etp/kg
38
08/20/98
KEK
7440.02-0
4400
mg/kp
760
08/20/98
KEK
7440-09.7
2000
mp/kp
ISO
OB/20/98
KEK
7440-23-5
910
otq/kg
7.6
08/20/96
KEK
7440-66-6
08/17/98
Method:
EPA 7060
Prep
Method: EPA 3050
ND
me/kg
3.a
08/25/98
KEK
7440-38-2
08/17/98
Method: EPA 7471
2.1 me/kp 0.15
Method: EPA 7740
4.6 map/kg 3.8
Method: X Moisture
86.8 %
Method: EPA 160.3
13.2 3
Method: EPA 350.3
11680 mg/kg 19
Prep Method: EPA 7471
08/17/98 KEK 7439-97-6
Prep Method: EPA 3050
08/24/98 KEK 7782-49-2
08/17/98
Prep Method:
08/17/96 KEK
Prep Method: EPA 160.3
08/14/98 KEK
Prep Method: EPA 350.3
06/19/98 TRW 7727-37-9
xcslmcmogazb Laboratory Certification IDs
REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC ID**bV Welar 37712 FL Environmental 96317
SID EnvRonmenW go= This report shah not be raproduced, except in full.
without the wrftn awwarrt of Pace Ans"cai Services, Inc_

Pace Analytical Services, Inc
54 Ravenscrort Drive
Ashewlle, NC 28801
Tel: [phone]
"DX) Fax: [phone]
DATE: 08/31/98
PAGE: 4
Pace Project Nurber: 93494
Client Project ID: SLud9e Analysis
Pace Ssaple No: 9321597 Date Collectedt 08/12/98 Matrix: Scit
Client Sa k* ID: EEtiOM819-8/12/98 Date Received: 08/13/9a!
Paraoaters Results Units PAL Analysed Analyst CASs Footnotes
................................. .......... ......... .......... ........ ..... .......... .....
Total Kjeldaht Nitrogen, $olt Methods EPA 391.3 Prep Method: EPA 351.3
rogen, Kjeldahl, Total 17M me/kg 1900 08/24/" BSP
Nitroyin, Nitrate plus Nitrite Method: EPA 353.2
N ate-N(trite (as N) 21 mg/ke 19
Phos�iorus, Tots(, SOL
P sphorus
Method: EPA 365.2
10300 mg/kg 474
Prep Method: EPA 353.2
08/24/95 BSP 7727-37-9
Prep Method: EPA 365.2
08/21/98 MPS 7723-14-0
-- --Amster REPORT OF LABORATORY ANALYSIS Laboratory Drinking
Water
0 ID
0
TN Drinking Water 02980
NC Drkfldng V*W 37712 FL EmAronmental 96,417
SC EirrArower" 99030 This report Mug not be reproduced, except In full,
without the written of Psce Analytical Services. Inc.

Pace Analytical Services. Inc.
Drive
Pace _AnalvVina! As evi�lle,SNCt28801
Ted: 704.254-7176
Fax: [phone]
August 28, 199d
Mr. Michel Ladd
Earth Environmental Services
75 Bison Lane
Murphy, NC 26906
RE: Pace Project Nnwber: 9%93
client Project 10: Soil Ansysis
Dear Mr. Ladd:
Enclosed are the results of analyses for ssrepteCs) received by the laboratory on August 13, 1998. If you have any
questions concerning this report, plesse feat free to contact me.
sincerely,
�tw
Jemifer Jones
Project Manager
Enclosures
�r aborntory Certification IDa
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712 FL Environmental 98317
SC Environmental Now This report shall not be reproduced, except in full,
without the written consent of Pon "tical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscralt Drive
Psaf-o An alutinial Asheville, NC 28801
Earth Enoirornwntal Services
75 aison Lane
Murphy, Pic 28906
Attn: Mr. Michoet Ladd
Phone: [phone]
Solid results are reported on a dry weight basis
Tel: [phone]
Fall: 704-252-4618
DATE: 08/28/98
PAGE: 1
Pace Project Number: 93493
.1A Client Project ID: Soil Aneyais
5a
Pace Sample No: 9321563 Date Collected: 05/12/98 Matrix: Soil
Client Sample ID: EES0089820-8/12/98 Date Received: 08/13/98
Parameters Results units PRL Analyzed Analyst CASH Footnotes
................................. .......... ......... — ........ ........ ..... .......... ..........
Metats
..atals, 1CP
. -Atuminum
ium
cium
0lironm i um
apper
t�1
MaA rase
ybdenum
c�kkel
w" m um
Furn
nc
Date Digested
Arc, AAS Furnace
Mnic
Date Digested
Me;reCy, CVAAS
C'Y` curt'
Selenium, AAS furnace
Selenium
Date Digested
Method:
EPA 6010
Prep
Method: EPA 3050
19000
mg/kg
11
08/20/98
KEK
7429-90.5
ND
ag/kg
1.1
08/20/98
KEK
7440-43-9
1800
mg/kg
11
08/20/98
KEK
7440.70.2
50
mg/kg
2.3
08/20/98
KEK
7440-47-3
25
mg/kg
1.1
08/20/98
KEK
7440-50-8
34
mg/kg
11
08/20/98
KEK
7439-92.1
3000
mg/kg
23
08/20/98
KEK
7439-95-4
270
mg/kg
1.1
08/20/98
KEK
7439-%-S
18
mg/kg
5.6
08/2.0/98
KEK
7439.98-7
12
mg/kg
5.6
08/20/98
KEK
7440-02.0
2300
mg/kg
110
08/20/98
KEK
7440-09-7
1100
mg/kg
23
08/20/98
KEK
7440-23-5
46
mg/kg
1.1
08/20/98
KEK
7440-66-6
00/17/98
Method: EPA 7060
1.1 mg/kg 0.56
Method: EPA 7471
0.058 mg/kg 0.023
Method: EPA 7740
ND mg/kg 0.56
Prep Method: EPA 3050
08/25/98 KEK 7440-36-2
08/17/93
Prep Method: EPA 7471
08/17/98 KEK 7439-97-6
Prep Method: EPA 30SO
MUM KEK 7782-49-2
08/17/98
wet Chemistry
Lehoralory Certification IN
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712 This report shall clot t�:e reproduced. except in Sall, FL Envimt nmentat 96317
�� ti0030 wtlhout the written oongnt of Pape Analytical Services. Inc.

� T
Pie Analvti al
v
LVoC
7
Pace Analytical Services, Inc.
54 Ravenscrolt Dive
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
DATE: 08/28/90
PACE: 2
Pace Project NueEsr: 93493
Client Project 10: Soil Aneysis
Pace Sampte No: 9321S63 Date Collecteds 08/12/98 Matrix: Soft
Client Sample ID: EE:MOd9a2o-9/12/9a Data Recetvedt 0013/98
Parameters Results Units PRl. Anslyaed Analyst CAS! Footnotes
...•..... .......... .......... .......... -------- --- ........--
Perce Moisture Method: S Moisture Prep Method:
Cent Moisture 11.5 % 09/17/98 KEK
Phoa us, Total, Soil Method: EPA 365.2 Prep Method: EPA 365.2
osphorus 384 mg/kV 14.1 08/21/9a MPS 7723-14.0
NC Wrrs:ewate► 40 REPORT OF LABORATORY ANALYSIS TNLr g Water"`029880
NC Odr>Itiny Water 37712
SC Environmental pp03o This report shall not be reproduced, except in full, FL Environmental 96317
without the written consent of Peas kwMical Services, Inc.
J

Pace Sample No: 9321571
Client Sample ID: EEW89821-8/12/93
Pace Analytical Services. Inc.
54 Ravenscrott Drive
Asheville, NC 28801
Tel: [phone]
Fax:[phone]
DATE: 08/28/98
PAGE: 3
Pace Project Nurbert 93493
Client Project ID: Soil Anaysis
Date Collected: 08/12/98 Matrix: 'Soil
Date Received: 03/13/98
Parameters ResuLts Units PRL Analyzed AnsLyst CASS Footnotes
Metals
ICP
Meta ,
umi num
um
fum
romium
r
L
nesium
smartest
Est
enum
11 ium
um
Z nc
Date Digested
Ars c, MS Furnace
enic
Date Digested
Marc y, CVAAS
cury
Sete i um, AAS Furnace elenium
Date Digested
Wet Chemistry
Pe rc Moisture
Pnt Moisture
Phoziorus, Total, Soil
osphorus
Method: EPA 6010
1
Prep Method: EPA 3050
25000
mg/ko
12
08/20/98
KEK
7429.90-5
No
mg/kg
1.2
08/20/98
KEK
7440-43-9
220
mg/kg
12
00/20/98
KEK
7440-70-2
14
rag/kg
2.4
08/20/98
KEK
7440-47-3
NO
mg/kg
1.2
08/20/98
KEK
7440-50.3
36
mg/kg
12
08/20/98
KEK
7439-92-1
1600
mg/kg
24
08/20/98
KEK
7439.99-4
160
mg/kg
1.2
08/20/98
KEK
7439.96-S
20
mg/kg
6
03/20/98
KEK
7439.98-7
8.4
ag/ka
6
08/20/98
KEK
7440.02.0
1200
sg/kg
120
09/20/95
KEK
7440.09-7
1400
mg/kg
24
08/20/98
KEK
7440.23-5
37
mo/kg
1.2
06/20/98
KEK
7440-66-6
081171"
Method: EPA 7060
ND mg/kg 0.6
Method: EPA 7471
0.044 mg/kg 0.024
Method: EPA 7740
NO mp/kg 0.6
Method: 11 Moisture
16.5 %
Method: EPA 365.2
27.2 mg/kg 0.748
Prep Method: EPA 3050
08/25/98 KEK 7440-38.2
08/17/98
Prep Method: EPA 7471
08/17/98 KEK 7439.97-6
Prep Method: EPA 3050
06/24/9a KEK 7M-49-2
08/17/98
Prep Method:
08/17/98 KEK
Prep Method: EPA 365.2
08/21/98 MPS 7723-14-0
LaDoral=CeMcation IDs
NC wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712
This report shall notba except ' FL Environmental 96317
SC EnvlronmenW a!P030 ttlproduoad, sxa m full,
without the wrNlen eoneeet of Paoss Analytical Services, Inc.

REPORT NUMBER A&L EASTERN AGRICULTURAL LABORATORIES, INC.
R229-052 7621 Whitepine Road • Richmond, Virginia 23237 • [phone]
�) Fax No. [phone]
rs . �
i�a B p i � I 012 6 SAMPLES
SEND PACE LABORATORIES, INC. EARTH ENV I RO P0693 -00186 fUBMITTED
TO: 54 RAVENSCROFT DRIVE GROWER: BY:
ASHEVILLE NC 28801
DATE OF REPORT 08 / 18 / 98 PAGE
Umu W NInom 9L ENR
NUMBFDI
bnJA
850r899T 15456 1.8 62L
06
#089821 15457 2.6 90H
S* .0Z
ACCT s 45530
MICHAEL LADD
DATE RECEIVED 08/14/98
1 SOIL ANALYSIS REPORT DATE OF ANALYSIS 08/17/98
MFOiPF101NFs PMAiBwAr Maw /M ACEM C.E.C.
BRAY P1 BRAY P2 K fE0 CA M am IUFPER N
ppm RATE ppm RATE Wnf RATE ppnn RATE Wn RATE pm RATE pH o h00000 "MOMS
122 VH 196 VH 378 VH 528 VH 1400 L 5.3 n�6.4 5.6 17.9
PERCM S tiE SATMUUM
TZMME K of CA Nr
9089820 5.4 24.5 39.0,
$089821 1 6.7125.7163.2
8 VL 14 L 226 VH 268 VH 1100 H
WM>E I «,LM jl�
M M[/aal 0044
x pptn FATE 1 peon RATE ppm RATE_ on wn
31.0
4.5
Values on this report represent the plant available nutrients in the soil.
EVEONA
planation► of symbols: Values are expressed as % (percent). ppm (parts per million), or lbs/A (pounds per acre).
ting after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High).
- Estimated Nitrogen Release. C.E.C. — Cation Exchange Capacity.
convert to Ibs/A, multiply the results in ppm by 2.
6.71 6.91 0.41 8.7
now
:
CL
1111TEpptn ME Am RATE
This mW appaa to the swnple(s) tesred Sampes are reaw-d a
manrrrrn thirty days atim testing Son Mayan prepared by.
Aar4cmTuRAL L4SOKATORIEs, lqc.

ANNUAL LAND API TION FIELD SUMMARY FORM _
PLEASE MAKE A COPY OFTHIS BLANK FORM h, ca vJMPLETEDAND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A `WX IN A BLANK OR BOX WHEN NOT APPLICABLE
_ AltdOSi
FACILITY NAME � � r`� � PERMIT fl On COa249 �f.
OWNER v`1eo1ASITE # G CATION EXCHANGE CAPACITY (non'S03 regulated'facilitiss only)
OPERATOR 1`- FIELD it Q I ACRES PERMITTED / . ACRES UTILIZED
TOTAL DRY TONS APPLIED (ANNUAL) 17,
DATE or
MONTH
Gallons /or Cubic Yards
(specify)
Dry Tons
per Acre
Residual Source
% Solids
Niis ®Avoregea
W. Rule can
Application
Method
i iUwbu
If`ieporting, W orith:.keep these
W daii-recoils on sde -
Crop
Total
per Acre
�
site conditions
(Dry. Moist. Wet)
aoo
a a
a a6
r �. I
, a ,
so o
&
r,,
;26 cmp
!d 9 66
67
r �l 1
I ,a'yo
30"! .
X
0
=' D r�
W $
000
5 r%
-a. . ; �.
11CAnsa e -5a
0 R (/'n
�
Q
r
qr ,
16 13
Qy
/�
6 U
1 e-4e,-51
6 , ! D
30 0
/6/)319%1
11QM
q00
030
'D Siter 1
0. boa
°
c_
id f laA.10
1 1107 000
r, '
30
"r-
ri
I
el6
6
3 `7 7
D
Lime
DATE I LBSJACRE
lid/Ifll-v 5 319 I
TOTALS: �1 PAN P As Cd Cr -tj Pb Hg Mo Ni Se Zn
Annual �saq ! .17 36. • 7� . i9Qbi, 3ic�7q :-� : �,�9 S5 5_o•�G ®O1�°i a.��
Cumulative
Permit Limit IbsJacre/ ear 1st Crop / 2nd Cro [1
Permitted Cumulative Pollutant Loading Rate (it Jacre) / . ia5 506 j oL S
x-�•9 __
(SIGNATURE OF LAND APPUER) DATE -_
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the Information submitted. I am aware that there are
significant penalties for submitting false Information, including the possibility of fines and Imprisonment for knowing violations."
DEM FORM FSF (2195)

11I�j
ANNUAL LAND APP. . TION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A'NIV IN A BLANK OR BOX WHEN NOT APPLICABLE
FACILITY NAME /C. Lilh " ►a` (' S t PERMIT tk 4
OWNER 1• V,Y` SITE # CATION EXCHANGE CAPACITY (non 503 regulated facilities only) o --7 me A��
OPERATOR E.�`� i5 FIELD # ACRES PERMITTED ACRES UTILIZED
TOTAL DRY TONS APPLIED (ANNUAL) � of
DATE or
MONTH
alv lOn . /or Cubic Yards
s ecif
Dry Tons
per Acre
Residual Source
% Solids
Note:-oo f�
u"se dia,ges
Mineraiization
Rate
Application
Method
(Surface or
Injection)
If reporting by month keep jh0se
�r a 'dWI -'records on site ,1
Crop
indmFUL td
iW 24 Hrs.
Site Conditions
(Dry, Moist, Wet)
Total
per Acre
9$
Il 9
a
q
q
ada
s o
.9 00
3a
$o©O
ZW3 19
����
1000
aOOO
6(-1-
-75. t 16,9Yr,
�a
so p ra IV
,07
Iota S t� f
0.9 ?0
O• %r
0.90/a
Q A11/6
ad"Zoo'
3cJ��0
S o'
15(d) ye
o4'
old`
O
O
O
+
• ,' tCAa
rV
rV
�
r 2
1. DATE I LBSJACRE 1
y 4 k A r5 LBSJACRE;
..
TOTALS: PAN P As Cd Cr Cu Pb H9 Mo Ni Se Zn
Annual 0,$o0 I la `C'9 16! 1-1 -1, riv X6 d. i 19d
Cumulative 14r r�07 t .4 s .04717 i.3 i5 O IS3� 33 ij 1 5-71
Permit Limit IbsJacre/ ear - 1st Crop / 2nd Crop
Permitted Cumulative Pollutant LoadingRate (IbsJacre) 4 1 5d® 1 5
X ---`?�-------- 2--�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are
significant penalties for submitting false Information, Including the possibility of fines and Imprisonment for knowing violations."
OEM FORM FSF (2/95)
1 - -_

r �
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name Y1 G� a-3 1 ` Permit Number_W�(�OOa°i`b
WWTP Name ( NPDES # IVCOOs 7 1 S 1
Monitoring Period: From __J__/ To / /
Pathogen .Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed
Class A
Alternative 1 Alternative 2 Alternative 3
Altemative 4 Alternative 5 Alternative 6
Class B
Alternative 1 Alternative 2 Alternative 3
If applicable to alternative performed (class i3 only) indicate "Process to Significantly Reduce Pathogens":
Aerobic Digestion _ Air Drying —Anaerobic Digestion _ Composting • _ Lime Stabilization
If applicable to altemative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
In Sludge
PatF►►ogen Density
Number of
ExDeedences
Frequency of
Analysis
Sample
Type
T 4b
Minimum
Goo.
G000. Mean
Maximum
Units
Fecal Colifonn
MPN
per gram of total
solids or 2 x 106
'416 t� 1
� G 0
lD 5�+' !
I 1mm
CFU per gram
of total solids
1000 MPN
•
pere
gram of
total olid
(dry weight)
Salmonella
bacteria (In
Neu of fecal
coliform
3 MPN per 4
grams total
solid (dry
wed ht
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option /performed
Option 1 Option 2 Option 3 Option 4 Option 5
Option 6 Option 7 Option Option 9 Option 10
No vector attraction reduction options were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, Under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the,vector,
attraction reduction requirement in 40 CFR 503.33 have been met."
"l certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note it you check
this statement attach an explanation why you have not met one or both of the requirements.)
'This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information Used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Pre er Na and Title(type or print) '
Signature of Preparer Date
Land Applier Name and Title (if applicable)(type or print),
Signature of Land Applier (if applicable) Date
DEM FORM RF (10/94)

EARTH ENVIRONMENTAL SERVICES
11.5 FALLS BRANCH RD.
MURPHX N.C. 28906
PH. -SUS. [phone]
PH: RES. (704) 837-SS43
February 1,1999
NC ID # 352 A74
Mr.Robert Sams
Town of Mars Hill
P.O. Box 368
Mare Hill, NC 28754
Dear Mr. Sams:
The following is a report of Laboratory analyses for sludge
samples received 10/14/98 and for SOUR test completed 12/30/98.
12/30/98-SOUR=0.03 mg 02 Consumption/hr/gram Total Solids.
Fecal Coli>:orm Densities % Total Solids
#1-10/14/98=41 669 colonies/gram
#2-10/7/98=6547 colonies/gram
#3-10/12/98=4000 colonies/gram
#4-10/8/98=41669 colonies/gram
#5-10/6/98=1453 colonies/gram
46-10/13/98=41669 colonies/gram
#7-10/9/98=5300 colonies/gram
0.54%
0.55%
0.45%
0.54%
0.62%
0.54%
0.51%
Thank you for your business. If you have any questions,please-
call me.
Respectfully. submitted,
Michael J. Ladd
TO 39~d' -1,11td31141.10aIAN3 Hl'� �'3 CtiS6-LC -VOL
TC :60 666 WCS T"AW