NCG030694_2022 DMR_20220725

hart 07,,N-44mhickman
SMARTER ENVIRONMENTAL SOLUTIONS
Via Online Portal & 2"1' Day FedEx
July 21, 2022
North Carolina Department of Environmental Quality
Division of Energy, Mineral and Land Resources
450 West Hanes Mill Road, Suite 300
Winston-Salem, North Carolina 27105
Re: DMR June 2022 — NCG030694 — LLFIex, LLC
Oracle Flexible Packaging, Inc. (Former)
1300 Cunningham Avenue
Winston-Salem, Forsyth County
H&H Project No. LLF-007
Dear Madam/Sir:
On behalf of LLFIex, LLC (LLFIex), Hart & Hickman, PC (H&H) is submitting the enclosed
quarterly storinwater Discharge Monitoring Report (DMR) for the site referenced above in
accordance with the industrial stormwater permit (NCG030694). There were no benchmark value
exceedances in samples from this quarterly monitoring period.
Should you have any questions or need any additional information, please feel free to contact
me.
Sincerely,
Hart & Hickman, PC
a,
Gregory Kanellis, PE
Project Manager
Enclosures
CC: Mr. Jason Caple, LLFIex (PDF via email)
Mr. Shawn Sylvester, LLFIex (PDF via email)
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847A241 main

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG030000
Metal Fabrication
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG03 0694
Person Collecting Samples: Glenn Price (Pace Analytical)
Facility Name: Former Oracle 200 Facility
Laboratory Name: Pace Analytical
Facility County: Forsyth
Laboratory Cert. N o•: Asheville, NC(40}. Eden. NC (633). Huntersville, NO (12), Ormond Beach (667)
Discharge during this period:
Yes
No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances?171 Yes MNo
If so, which Tier (I, 11, or lil)?
A copy of this DMR has been uploaded electronically via https:Hedocs.deg,tic.gov/Forms/SW-DMR Yes No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities - Benchmarks in (Red)
Parameter
Parameter
Outfall SD01
Outfall SD02
Outfall SD03
Outfall SD04
Outfall SD05
Code
N/A
Receiving Stream Class
C
C
C
C
C
N/A
Date Sample Collected MM/DD/YYYY
06/27/2022
06/27/2022
06/27/2022
06/27/2022
06/27/2022
46529
24-Hour Rainfall in inches
1.2
1.2
1.2
1.2
1.2
C0530
TSS in mg/L (100 or 50*)
3.3
3.7
3.4
3.8
3.6
pH in standard units (6.0-9.0 FW,
00400
6.88
6.71
6.54
6.69
6.68
6.8-8.5 SW)
Copper, total recoverable in mg/L
01119
<0.0050
<0.0050
<0.0050
<0.0050
<0.0050
(0,010 FW, 0.0058 SW
Lead, total recoverable in mg/ L
01051
<0.0050
<0.0050
<0.0050
<0.0050
<0.0050
(0,075 FW, 0.22 SW
Zinc, total recoverable in mg/ L (0.126
01094
FW, 0.095 SW)
<0.010
<0.010
<0.010
<0.010
<0.010
Chemical Oxygen Demand (COD) in
00340
mg/L (120)
<25.0
<25.0
<25.0
<25.0
<25.0
00552
Non -Polar Oil & Grease in mg/L (15)
<5.0
<5.1
<5.1
<5.1
<5.1
* Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L
FW (Freshwater) SW (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, orthose persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, including the poVibility of fines and imprisonment for knowing violations."
Signature of Permittee or Lfelegated Authorized Individual
[e-mail]
Email Address
Date �l
336-803-1655
Phone Number
Page 28 of 28

aceAnalytical
www.pactlabs.com
July 08, 2022
Greg Kanellis
Hart & Hickman
3921 Sunset Ridge Rd.
Suite 301
Raleigh, NC 27607
RE: Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
Dear Greg Kanellis:
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on ,tune 28, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Paco Analytical Services -Asheville
- Pace Analytical Services - Charlotte
- Pace Analytical Services - Eden
• Pace Analytical Services - Kernersville, NC
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
1(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 28

laneAnalyfical"
www.pacetabs.com
Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory 10: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification M 37738
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification M 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 28

(�IacleAnalytical
www.patolabs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huniersville, NC 28078
[phone]
Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
Analyses
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92611918001 Outfall SDO1
SM 2540D-2015
LRB
1
PASI-E
EPA 1664E
REL
1
PASI-C
EPA 200.7 Rev 4.4 1994
RUT
3
PASI-A
KRG
4
PASI-KR
SM 5220D-2011
DMN
1
PASI-A
92611918002 Outfall SD02
SM 2540D-2015
DAW
1
PASI-E
EPA 1664B
REL
1
PASI-C
EPA 200.7 Rev 4.4 1994
RUT
3
PASI-A
KRG
4
PASI-KR
SM 5220D-2011
DMN
1
PASI-A
92611918003 Outfall SD03
SM 2540D-2015
DAW
1
PASI-E
EPA 1664E
REL
1
PASI-C
EPA 200.7 Rev 4.4 1994
RUT
3
PASI-A
KRG
4
PASI-KR
SM 5220D-2011
DMN
1
PASI-A
92611918004 Outfall SD04
SM 2540D-2015
DAW
1
PASI-E
EPA 1664B
REL
1
PASI-C
EPA 200.7 Rev 4.4 1994
RUT
3
PASI-A
KRG
4
PASI-KR
SM 5220D-2011
DMN
1
PASI-A
92611918005 Outfall SDOS
SM 2540D-2015
DAW
1
PASI-E
EPA 1664E
REL
1
PASI-C
EPA 200.7 Rev 4.4 1994
RUT
3
PASI-A
KRG
4
PAS]-KR
SM 5220D-2011
DMN
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
PASWR = Pace Analytical Services - Kernersville, NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 28

aceAnalytical
www.pacelabs.corn
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704}875-9092
Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
Sample: Outfall SD01 Lab ID: 92611918001 Collected: 06/27/22 15:03 Received: 06/28/22 10:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analytical Services - Eden
Total Suspended Solids
3.3 mg1L 2.7
1
06/29/22 09:47
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mglL 5.0
1
06/30/22 01:00
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Copper
ND mglL 0.0050
1
06/30/22 07:57 06/90/22 17:57 7440-50-8
Lead
ND mg1L 0.0050
1
06/30/22 07:57 06/30/22 17:57 7439-92-1
Zinc
ND mg1L 0.010
1
06/30/22 07:57 06/30/22 17:57 7440-66-6
Field Data Kernersville
Analytical Method:
Pace Analytical Services - Kernersville, NC
Performed by
Pace
1
06/27/22 15:03
Collected By
Glenn
1
06/27/22 15:03
Price
pH
6.88 Std. Units
1
06/27/22 15:03
Temperature
22.7 deg C
1
06/27/22 15:03
5220D COD
Analytical Method: SM 52200-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
ND mg/L 25.0
1
06/30/22 12:53 07/01/22 15:05
Date: 07108/2022 08:15 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
withwt the written consent of Pace Analytical Services, LLC.
Page 4 of 28

(�IacieAnalytical
www.pacolabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
Sample: Outfall SD02 Lab ID: 92611918002 Collected: 06/27/22 15:11 Received: 06/28/22 10:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analytical Services - Eden
Total Suspended Solids
3.7 mg/L
2.7
1
06/29/22 14:36
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.1
1
06/30/22 01:00
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4A 1994
Pace Analytical Services -Asheville
Copper
ND mg/L
0.0050
1
06/30/22 07:57 06/30/22 18:00 7440-50-8
Lead
ND mg/L
0.0050
1
06/30/22 07:57 06/30/22 18:00 7439-92-1
Zinc
ND mg/L
0.010
1
06/30/22 07:57 06/30/22 18:00 7440-66-6
Field Data Kernersville
Analytical Method:
Pace Analytical Services - Kernersville,
NC
Performed by
Pace
1
06/27/22 15:11
Collected By
Glenn
1
06/27/22 15:11
Price
pH
6.71 Std. Units
1
06/27/22 15:11
Temperature
21.9 deg C
1
06/27/22 15:11
5220D COD
Analytical Method: SM 522OD-2011
Preparation
Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
ND mg1L
25.0
1
06/30/22 12:63 07/01/22 15:05
Date: 07/08/2022 08:15 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 28

laceAnalytical"
www.plcolabs.com
ANALYTICAL RESULTS
Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
Sample: Outfall SD03 Lab ID: 92611918003 Collected: 06/27/22 15:19 Received: 06/28/22 10:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analytical Services - Eden
Total Suspended Solids
3.4 mg1L
2.8
1
06/29/22 14:37
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.1
1
0613012201:00
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Copper
ND mg/L
0.0050
1
06/30/22 07:57 06/30/22 18:03 7440-50-8
Lead
ND mg/L
0.0050
1
06/30/22 07:57 06/30/22 18:03 7439-92-1
Zinc
ND mg/L
0.010
1
06/30/22 07:57 06/30/22 18:03 7440-66-6
Field Data Kernersville
Analytical Method:
Pace Analytical Services - Kernersville,
NC
Performed by
Pace
1
06/27/22 15:19
Collected By
Glenn
1
06/27/22 15:19
Price
pH
6.54 Std. Units
1
06/27/22 15:19
Temperature
22.4 deg C
1
06/27/22 15:19
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
ND mg/L
25.0
1
06/30/22 12:53 07/01/22 15:06
Date: 07/08/2022 08:15 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 28

(�IaneAnalXical"
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
Sample: Outfall SD04 Lab ID: 92611918004 Collected: 06/27/22 1526 Received: 06/28/22 10:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analytical Services - Eden
Total Suspended Solids
3.8 mg/L
2.8
1
06/29/22 14:37
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg1L
5.1
1
06/30/22 01:00
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Copper
ND mglL
0.0050
1
06/30/22 07:57 06/30/22 18:07 7440-50-8
Lead
ND mg1L
0.0050
1
06/30/22 07:57 06/30/22 18:07 7439-92-1
Zinc
ND mglL
0.010
1
06/30/22 07:57 06/30/22 18:07 7440-66-6
Field Data Kernersville
Analytical Method:
Pace Analytical Services - Kernersville,
NC
Performed by
Pace
1
06/27/22 15:26
Collected By
Glenn
1
06/27/22 15:26
Price
pH
6.69 Std. Units
1
06/27/22 15:26
Temperature
22.6 deg C
1
06/27/22 15:26
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method:
SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
ND mglL
25.0
1
06/30/22 12:53 0710l/22 15:06
Date: 07/08/2022 08:15 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 28

leAnaVical
www.picllabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
Sample: Outfall SD05
Lab ID: 92611918005 Collected: 06/27/22 15:35
Received: 06/28/22 10:20 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No, Qual
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analytical Services - Eden
Total Suspended Solids
3.6 mg1L 2.8
1
06/29/22 14:38
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg1L 5.1
1
06/30/22 01:00
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
ND mg1L 0.0050
1
06/30/22 07:57 06/30/22 18:10 7440-50-8
Lead
ND mg/L 0.0050
1
06/30/22 07:57 06/30/22 18:10 7439-92-1
Zinc
ND mg/L 0.010
1
06/30/22 07:57 06/30/22 18:10 7440-66-6
Field Data Kernersville
Analytical Method:
Pace Analytical Services - Kernersville, NC
Performed by
Pace
1
06/27/22 15:35
Collected By
Glenn
1
06/27/22 15:35
Price
pH
6.68 Std. Units
1
06/27/22 15:35
Temperature
22.8 deg C
1
06/27/22 15:35
5220D COD
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
ND mg/L 25.0
1
06/30/22 12:53 07101/22 15:06
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07108/2022 08:15 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 28

aceAnalytical
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QUALITY CONTROL DATA
Project: Hart 8 Hickman - Oracle 200
Pace Project No.: 92611918
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hurtersville, NC 28078
[phone]
QC Batch: 707470
Analysis Method:
SM 254OD-2015
QC Batch Method: SM 254OD-2015
Analysis Description:
2540D Total Suspended Solids
Laboratory:
Pace Analytical Services - Eden
Associated Lab Samples: 92611918001
METHOD BLANK: 3690096
Matrix: Water
Associated Lab Samples: 92611918001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 06/29/22 09:42
LABORATORY CONTROL SAMPLE: 3690097
Spike LCS
LCS % Roe
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 248
99 90-110
SAMPLE DUPLICATE: 3690098
92611794001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
521
529 2
SAMPLE DUPLICATE: 3690099
92611795001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
96.6
89.6 7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/08/2022 08:15 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 28

(�IaneAnalyficalo'
www.pacelab$.com
QUALITY CONTROL DATA
Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 707560
Analysis Method:
SM 254OD-2015
QC Batch Method: SM 2540D-2015
Analysis Description:
2540D Total Suspended Solids
Laboratory:
Pace Analytical Services - Eden
Associated Lab Samples: 92611918002, 92611918003, 92611918004, 92611918005
METHOD BLANK: 3690472
Matrix: Water
Associated Lab Samples: 92611918002, 92611918003, 92611918004, 92611918005
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND 2.5 06/29/22 14:32
LABORATORY CONTROL SAMPLE:
3690473
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 236
94 90-110
SAMPLE DUPLICATE; 3690568
92611891001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg1L
33.6 30.0 11
SAMPLE DUPLICATE: 3690569
92611952001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 5130 5190 1
Results presented on this page are in the units indicated py the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/08/2022 08:15 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 28

laceAnalyilca/
www.pacolabs.com
QUALITY CONTROL DATA
Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
QC Batch: 707827 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92611918001, 92611918002, 92611918003, 92611918004, 92611918005
METHOD BLANK: 3691970 Matrix: Water
Associated Lab Samples: 92611918001, 92611918002, 92611918003, 92611918004, 92611918005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons ni ND 5.0 06/30/22 01:00
LABORATORY CONTROL SAMPLE:
3691971
Parameter
Units
Total Petroleum Hydrocarbons
mg/L
MATRIX SPIKE SAMPLE:
3691972
Parameter
Units
Total Petroleum Hydrocarbons
mg/L
SAMPLE DUPLICATE: 3691973
Parameter
Units
Total Petroleum Hydrocarbons
mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
20 16.3 82 64-132
35727358001 Spike
Result Conc.
4.9U 19.6
35727360001 Dup
Result Result
4.8U ND
MS MS
Result % Rec
15.5 78
RPD Qualifiers
% Rec
Limits Qualifiers
64-132
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/08/2022 08:15 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 28

laeAnalytical
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QUALITY CONTROL DATA
Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
QC Batch: 707879 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92611918001, 92611918002, 92611918003, 92611918004, 92611918005
METHOD BLANK: 3692045
Matrix:
Water
Associated Lab Samples:
92611918001, 92611918002,
92611918003, 92611918004, 92611918005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Copper
mg/L
ND
0.0050
06KM/2217:50
Lead
mg/L
ND
0.0050
06/30/2217:50
Zinc
mg/L
ND
0.010
06130/2217:50
Pace Analytical Services, LLC
9800 Kincey Ave, Simile 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
3692046
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Copper
mg/L
0.5 0.51
101 85-115
Lead
mg/L
0.5 0.50
100 85-115
Zinc
mg/L
0.5 0.48
97 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3692047
3692048
MS
MSD
92611918004
Spike
Spike
MS
Parameter units
Result
Cone.
Cone.
Result
Copper mg/t_
ND
0.5
0.5
0.43
Lead mg/L
ND
0.5
0.5
0,42
Zinc mg/L
ND
0.5
0.5
0.58
MSD
MS
MSD
% Rec
Result
% Rec
% Rec
Limits RPD Qual
0.44
86
88
70-130 2
0.44
83
87
70-130 5
0.58
114
116
70-130 1
Results presented on this page are in the units indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/08/2022 08:15 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 28

(�IaceAnalyficale
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QUALITY CONTROL DATA
Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
QC Batch: 707921 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92611918001, 92611918002, 92611918003, 92611918004, 92611918005
METHOD BLANK: 3692121 Matrix: Water
Associated Lab Samples: 92611918001, 92611918002, 92611918003, 92611918004, 92611918005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 07/01/22 14:57
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 3692122
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg1L 750 770 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3692123 3692124
MS MSD
92611550001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 6330 100 100 5950 5900 -385 -428 90-110 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3692125 3692126
MS MSD
92611557002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 26.3 100 100 26.3 139 0 113 90-110 136 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in Full,
Date: 07/08/2022 08:16 AM without the written consent of Pace Analytical Services, LLC.
Page 13 of 28

acMnalytical
www.pactimbs.com
QUALIFIERS
Project: Hart & Hickman - Oracle 200
Pace Project No.: 92611918
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
INC. - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethyivinyl ether.
Aseparate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphanylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TN[ accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/08/2022 08:15 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 28

(�IaneAnalyfical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Hart & Hickman - Oracle 200
92611918
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92611918001
Outfall SD01
SM 2540D-2015
707470
92611918002
Outfall SD02
SM 254OD-2015
707560
92611918003
Outfall SD03
SM 2540D-2015
707560
92611918004
Outfall SD04
SM 2540D-2015
707560
92611918005
Outfall SD05
SM 2540D-2015
707560
92611918001
Outfall SD01
EPA 1664B
707827
92611918002
Outfall SD02
EPA 1664E
707827
92611918003
Outfall SD03
EPA 1664E
707827
92611918004
Outfall SD04
EPA 1664B
707827
92611918005
Outfall SD05
EPA 1664B
707827
92611918001
Outfall SD01
EPA 200.7 Rev 4.4 1994
707879
EPA 200.7 Rev 4.4 1994
707889
92611918002
Outfall SD02
EPA 200.7 Rev 4.4 1994
707879
EPA 200.7 Rev 4.4 1994
707889
92611918003
Outfall SD03
EPA 200.7 Rev 4.4 1994
707879
EPA 200.7 Rev 4.4 1994
707889
92611918004
Outfall SD04
EPA 200.7 Rev 4.4 1994
707879
EPA 200.7 Rev 4.4 1994
707889
92611918005
Outfall SD05
EPA 200.7 Rev 4A 1994
707879
EPA 200.7 Rev 4.4 1994
707889
92611918001
Outfall SD01
92611918002
Outfall SD02
92611918003
Outfall SD03
92611918004
Outfall SD04
92611918005
Outfall SD05
02611918001
Outfall SD01
SM 5220D-2011
707921
SM 5220D-2011
708275
92611918002
Outfall SD02
SM 5220D-2011
707921
SM 5220D-2011
708275
92611918003
Outfall SD03
SM 5220D-2011
707921
SM 5220D-2011
708275
92611918004
Outfall SD04
SM 5220D-2011
707921
SM 5220D-2011
708275
92611919005
Outfall SD05
SM 5220D-2011
707921
SM 5220D-2011
708275
Date: 07/08/2022 08:15 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 15 of 28

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page 16 of 28

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IS V2lifle� and L':It;Sln t;.e a,ce;.tance range far
preservation samples,
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Fide: L•iher2,;er t. ere is 3 d's:raparcy it irk N:r,'t Car:iina qlr rGarce ser-p{es. a C•oy Of t^is fCr-t w.il to s?f1t U the N]ryt7 Cariiira C.Ca?f7 C:r,f Ca-' CM cff Cot of hoH, Irticwrect pr2sarnt:ve, out of temp, incorrect container$) :c_ (i.e.
Qualtrax Document ID: 70377
Page 2 of 2
Page 17 of 28