Loading...
HomeMy WebLinkAboutWQ0002857_Monitoring - 07-2022_20220901Monitoring Report Submittal Permit Number #* Name of Facility:* Month: * July Report Information WQ0002857 Piedmont Custom Meat WWTF Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address:* Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2022 Upload Document* Piedmont Custom_July 22.pdf 2.54MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Jessica.Mize@pacelabs.com Jessica Mize jwd rA lip Reviewer: Gerald, Wanda 9/1 /2022 This will be filled in automatically Is the project number correct?* WQ0002857 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 10/4/2022 Page 1 of 3 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: W00002857 MONTH: Julv YEAR: 2022 FACILITY NAME: Piedmont Custom Meats WWTF COUNTY: Caswell Flow Monitoring Point: Effluent: LJ Influent: Parameter Monitoring Point: Effluent: Influent: Surface Water (SW): U SW Code/Name: Was There Effluent Flow for this Month Generated At This Facility: Yes: LJ No: Operator wow W400 50060 00310 00610 005M 31616 70300 00620 1 00625 00940 W600 00665 D A -1' L Anval Time 2400 Clock Operator Time on S!m ORC on S4e9 Daily Rate (Flow)into Treatment Ssmm PH Residual Chlorine 60D-3 ITC NH-3N TSS Fecal Cottle. (Gm-memc M'W) DS NO.I-N IKN CModde r.Ni Ninoycn Inlol I'M1osphonrs HRS YIN GALLONS UNITS u,L x4GL NAG MU 100%u Mir %IGL SIGLL %161 %161, MGL 1 3,333 3,333 3 3,333 4 3,333 5 3,333 6 3,333 2 0730 2.011 Y 3,333 6.4 <0.01 8 0630 1.00 Y 1,894 9 1,894 6 1,894 0720 0.25 Y 1,894 6.3 <U01 3,605 13 3,605 14 1 1 1 3,605 1s 3,605 16 3,605 17 3,605 18 3,605 H' 3,605 20 1311 0.25 B 3,605 6.2 <0.01 21 2,199 2,199 23 2,199 24 1 2,199 2,199 26 IOUO 1.51) Y 2,199 63 <0.01 10.5 35.6 G9.1 443 459 0.58 46.0 138 47.6 0.48 27 4,007 28 4,007 29 4,0117. 30 4,007 st 4,007 M aroge 3,116 JIM <0.01 IDS 35.6 <3.1 44.3 459 0.58 46.0 138 47.6 OAS Daily Maximum 4,007 6.40 <0.01 105 35.6 <3.1 44.3 459 U.58 46.0 138 47.6 0.48 Daily 11, imum 1,894 6.20 <0.01 I0.5 35.6 <3.1 44.3 459 0.58 46.0 138 47.6 0.48 Monthly Limits ( Avg) 5000 Composite / Grab (G) Operator in Responsible Charge (ORC): Glenn Price Grade: SI Phone: 336-996-2841 Check Box if ORC Has Changed: F-1 ORC Certification Number: 987931/20771 Certified Laboratories (1): Pace Analytical Services (2) Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X �( DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHA Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the hest of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (512003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant (Y,N) 1. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permitee)* Date Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 9683 Kerr's Chapel Road Gibsonville. NC (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) PARAMETER CODES 31504 Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel (Position or Title) 336-582-8247 (Phone Number) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease W 09 PAN Plant Available 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 03/31/21 (Permit Exp. Date) 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data. * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 28.0506 (b) (2) (D). Page 2 of 3 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W00002857 MONTH: Julv YEAR: 2022 FACILITY NAME: Piedmont Custom Meats WWTF COUNTY: Caswell Formulas: Daily Loading (inches) = [Volume Applied (gallons) x 0.1336 (cubic feat/gallon) x 12 (inchesdoogl / [Area Sprayed (acres) x 43,560 (square feat/acm) or = [Volume Applied (gallons) / (Area Sprayed (acres) x 27,152 (gallonslaweinch). Maximum Hourly Leading(inches) =Daily Loading (inches)/[rime irrigated (minutes) 160(minutes/nour)] Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Total (inches) = Sum of this month's Monthly Loading (inches) and previous ll month's Monthly Loadings (Inches) Average Weekly Loading (inches) = [Monthly Loading (inches/month) I Number of days in the month (dayslmonth )I x 7 (daysAfeek) .. Irrigation Occur On This Field: nNo: El Permitted Yeady Raw (inches): �x 'weather Coder: C<ki r, PC -panty tloudy, C4elnudy, a-n a Sa-roan, Spsktl Spray Irrigation Operator in Responsible Charge(ORQ: Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit DENR Division of Water Quality 1617 Mail Service Center RALEIGH, NC 27699-1617 (SIGNATURE OF OPERATOR IN RESPONSIBLE CHA By this signature, I certify that this report is accurate and complete to the best of my knowledge. DENR Form NDAR-1 (5/2003) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been comaliant_ with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. 2. Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. S. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is non -compliant , please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." S- :5 ( — 2--� Baron Neal McDufe (Signature of Permitee)* 4V Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Aaent (Permittee-Please print or type) 9683 Kerr's Chapel Road Gibsonville. NC (Permittee Address) Field Services Director (Pace Analytical Services) (Position or Title) 336-582-8247 (Phone Number) 03/31/21 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). DENR Form NDAR-1 (5/2003) Page 3 of 3 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITES) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W00002857 MONTH: July YEAR: 2022 FACILITY NAME: Piedmont Custom Meats W WTF COUNTY: Caswell Formulas: Daily Loading(inches) =Nolume Applied (gallons) x 0.1336 (cubic feeVgallon)x 12(inchestlooQj/[Area Sprayed (acres) x 43,560(square feeVacre) or = [Volume Applied (gallons) / [Area Sprayed (acres) x 27,152 (gallons/acre4nch). Maximum Hourly Loading (inches) = Daily Loading (inches) / Time irrigated (minutes) 160 fminutesmour)) Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Tobal(inches) = Sum of this month's Monthly Loading (inches) and previous ll month's Monthly Loadings (inches) Average Weekly Loading (inches) =[Monthly Loading (inches/month)/Number of days in the month (daysrmonth)I x 7(daysNreek) E ' .... : 12 o: . Area Sprayed la� PennstakfRourly Rate (inches): � A m �i�1���llllllllllllllli ����i�� mlllllllli �� � ��lllllllllllll� ����� •Nether Codes: C-clear,P-pnrlly dandy, C4rloudy. R-rain. Snenow. Skim Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed:❑ Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit x DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality 1617 Mail Service Center RALEIGH, NC 27699-1617 By this signature, I certify that this report is accurate and complete to the best of my knowledge. DENR Form NDAR-1 (5/2003) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. 2. Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. 5. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." --s Baron Neal McDuffie (Signature of Permitee)* Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Agent (Permittee-Please print or type) 9683 Kerr's Chapel Road Gibsonville. NC (Permittee Address) Field Services Director ( Pace Analytical Services) (Position or Title) 336-582-8247 (Phone Number) 03/31/21 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). DENR Form NDAR-1 (5/2003) aceAnalytical e WWW.pacalaCs.tom i August 09, 2022 Larry Moore Piedmont Custom Meats 430 NC Highway 49 South Asheboro, NC 27205 RE: Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Dear Larry Moore: Pace Analytical Services, LLC 1377 South Park Drive Kernersvllle, NC 27284 (704)977-0981 Enclosed are the analytical results for sample(s) received by the laboratory on July 26, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, A"�� Stephanie Knott stephanie.knoft@pacelabs.com 704-977-0981 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 1 of 25 aceAnalytical www.pacolabs.com Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 VirginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Page 2 of 25 aluc; y ical www.pacelabscam SAMPLE ANALYTE COUNT Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92616646001 MW-1 SM 254OC-2015 AED 1 PASI-E EPA 350.1 Rev 2.0 1993 SRS 1 PASI-E EPA 353.2 Rev 2.0 1993 SRS 1 PASI-E SM 9222D-2015 MWF 1 PASI-E EPA 120.1-1982 YEG 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A SM 531OB-2014 MJP 1 PASI-A 92616646002 MW-4 SM 2540C-2015 AED 1 PASI-E EPA 350.1 Rev 2.0 1993 SRS 1 PASI-E EPA 353.2 Rev 2.0 1993 SRS 1 PASI-E SM 9222D-2015 MWF 1 PASI-E EPA 120.1-1982 YEG 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A SM 531OB-2014 MJP 1 PASI-A 92616646003 MW-5 SM 254OC-2015 AED 1 PASI-E EPA 350.1 Rev 2.0 1993 SRS 1 PASI-E EPA 353.2 Rev 2.01993 SRS 1 PASI-E SM 9222D-2015 MWF 1 PASI-E EPA 120.1-1982 YEG 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A SM 531OB-2014 MJP 1 PASI-A 92616646004 Effluent SM 254OC-2015 AED 1 PASI-E SM 2540D-2015 DAW 1 PASI-E EPA 353.2 Rev 2.01993 SRS 2 PASI-E SM 521OB-2016 MWF 1 PASI-E Colilert-18 LRB 1 PASI-E TKN+NO3+NO2 Calculation MDW 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A EPA 350.1 Rev 2.01993 KDF1 1 PASI-A EPA 351.2 Rev 2.01993 MFO 1 PASI-A EPA 365.1 Rev 2.01993 SMT 1 PASI-A PASI A = Pace Analytical Services - Asheville PASI-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 25 aceAnalytical www.pacelabscam ANALYTICAL RESULTS Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Sample: MWA Lab ID: 92616646001 Collected: 07/26/22 09:49 Received: 07/26/22 11:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 352 mg/L 25.0 1 07/29/22 10:47 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Ammonia ND mg/L 0.10 1 07/27/22 10:54 7664-41-7 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 21.0 mg/L 0.40 10 07/26/22 16:00 14797-55-8 MBIO 92220 Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms ND CFU/100 mL 1.0 1 07/26/22 15:06 07/27/22 14:25 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services -Asheville Specific Conductance 523 umhos/cm 10.0 1 08/09/2210:35 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Qual Chloride 58.5 mg/L 1.0 1 07/29/22 00:31 16887-00-6 M1 Sulfate 3.6 mg/L 1.0 1 07/29/22 00:31 14808-79-8 5310B TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 07/29/22 00:28 7440-44-0 Date: 08/09/2022 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 25 (�5a'cuceAnalXical www.pacelabscom ANALYTICAL RESULTS Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Sample: MW-4 Lab ID: 92616646002 Collected: 07/26/22 10:16 Received: 07/26/22 11:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 549 mg/L 25.0 1 07/29/22 10:47 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Ammonia ND mg/L 0.10 1 07/2712210:53 7664-41-7 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 1.9 mg/L 0.040 1 07/26/22 15:55 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms 42.0 CFU/100 mL 1.0 1 07/26/22 15:06 07/27/22 14:25 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services -Asheville Specific Conductance 1020 umhos/cm 10.0 1 08/09/22 10:39 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 212 mg/L 5.0 5 07/29/2216:12 16887-00-6 Sulfate 2.4 mg/L 1.0 1 07/29/22 01:15 14808-79-8 5310B TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 07/29/22 02:14 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, L.L.C. Page 5 of 25 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: MW-5 Lab ID: 92616646003 Collected: 07/26/22 10:32 Received: 07/26/22 11:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 154 mg/L 25.0 1 07/29/22 10:47 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Ammonia ND mg/L 0.10 1 07/27/2211:17 7664-41-7 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 0.11 mg/L 0.040 1 07/26/22 15:56 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms ND CFU/100 mL 1.0 1 07/26/22 15:06 07/27/22 14:25 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services -Asheville Specific Conductance 249 umhos/cm 10.0 1 08/09/22 10:41 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 36.2 mg/L 1.0 1 07/29/22 01:30 16887-00-6 Sulfate ND mg/L 1.0 1 07/29/22 01:30 14808-79-8 5310E TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 07/29/22 03:09 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 25 ace AnalyNoI www.pacelabs.com ANALYTICAL RESULTS Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: Effluent Parameters Lab lD: 92616646004 Collected: 07/26/22 09:38 Results Units Report Limit DF Received: 07/26/22 11:45 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 459 mg/L 25.0 1 07/29/22 10:47 2540D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services - Eden Total Suspended Solids ND mg/L 3.1 1 07/27/22 16:10 353.2 NO2JN03 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, NO2 plus NO3 1.6 mg/L 0.040 1 07/26/22 15:53 Nitrogen, Nitrate 0.58 mg/L 0.040 1 07/26/22 15:53 14797-55-8 5210B BOD, 5 day EDN Analytical Method: SM 521OB-2016 Preparation Method: SM 521OB-2016 Pace Analytical Services - Eden BOD, 5 day 10.5 mg/L 2.0 1 07/27/22 16:28 08/01 /22 14:55 B2 Colilert-18 Fecal Coliform EDN Analytical Method: Colilert-18 Preparation Method: Colilert-18 Pace Analytical Services - Eden Fecal Coliforms 44.3 MPN/100ml- 1.0 1 07/26/22 14:27 07/27/22 08:37 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 47.6 mg/L 0.040 1 08/04/22 18:43 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 138 mg/L 3.0 3 07/29/2216:27 16887-00-6 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 35.6 mg/L 1.0 10 08/08/22 14:56 766441-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 46.0 mg/L 2.5 5 08/01/22 17:32 08/02/22 05:31 7727-37-9 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 0.48 mg/L 0.050 1 08/03/2218:08 08/04/2-217:07 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 25 aceAnalytr`cal www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 713584 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92616646001, 92616646002, 92616646003, 92616646004 METHOD BLANK: 3720477 Matrix: Water Associated Lab Samples: 92616646001, 92616646002, 92616646003, 92616646004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 07/29/22 10:47 LABORATORY CONTROL SAMPLE: 3720478 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 248 99 90-110 SAMPLE DUPLICATE: 3720479 92616646001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 352 355 1 SAMPLE DUPLICATE: 3720480 92617332002 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 98.0 90.0 9 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 25 QD 5a'uce1� AnalXical www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 QC Batch: 713210 Analysis Method: SM 2640D-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92616646004 METHOD BLANK: 3718581 Matrix: Water Associated Lab Samples: 92616646004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 07/27/22 16:09 LABORATORY CONTROL SAMPLE: 3718582 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 234 94 90-110 SAMPLE DUPLICATE: 3718584 92616746002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 47.9 41.4 15 SAMPLE DUPLICATE: 3718887 92616753001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 32.2 31.2 3 Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 25 1�5a'uccice AnalX cal QD www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 713144 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia, EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92616646001, 92616646002, 92616646003 METHOD BLANK: 3718285 Matrix: Water Associated Lab Samples: 92616646001, 92616646002, 92616646003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 07/27/22 10:42 LABORATORY CONTROL SAMPLE: 3718286 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.0 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3718287 3718288 MS MSD 92616597001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 4.9 4.9 99 99 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3718289 3718290 MS MSD 92616753002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 4.9 4.9 98 98 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 25 la 'uc ice;Affllytical www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 712800 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92616646001, 92616646002, 92616646003, 92616646004 METHOD BLANK: 3716690 Matrix: Water Associated Lab Samples: 92616646001, 92616646002, 92616646003, 92616646004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.040 07/26/22 11:06 Nitrogen, NO2 plus NO3 mg/L ND 0.040 07/26/22 11:06 LABORATORY CONTROL SAMPLE: 3716691 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.5 97 90-110 Nitrogen, NO2 plus NO3 mg/L 2.5 2.4 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3716692 3716693 MS MSD 92616520001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 5.8 1.5 1.5 7.1 7.1 88 85 90-110 1 Nitrogen, NO2 plus NO3 mg/L 5.8 2.5 2.5 8.1 8.1 94 92 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 25 acice, Ana l www.pacelaba.ccrn QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 QC Batch: 713235 Analysis Method: SM 521OB-2016 QC Batch Method: SM 521OB-2016 Analysis Description: 5210B BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92616646004 METHOD BLANK: 3718790 Associated Lab Samples: 92616646004 Parameter Units BOD, 5 day mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 08/01 /22 14:02 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3718791 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 193 98 84.6-115 SAMPLE DUPLICATE: 3718793 92616817001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 933 893 4 R6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 25 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 QC Batch: 713217 Analysis Method: SM 9222D-2015 QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform( MF)-EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92616646001, 92616646002, 92616646003 METHOD BLANK: 3718611 Matrix: Water Associated Lab Samples: 92616646001, 92616646002, 92616646003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/27/22 14:25 SAMPLE DUPLICATE: 3718612 92616646001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL ND ND Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 25 I eAnalyiical� www.pacelabs.com 1 QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 QC Batch: 712973 Analysis Method: Colilert-18 QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92616646004 SAMPLE DUPLICATE: 3717703 92616596001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms MPN/100mL ND ND Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 25 aceAnalj cal www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kernersville. NC 27284 (704)977-0981 QC Batch: 715668 Analysis Method: EPA 120.1-1982 QC Batch Method: EPA 120.1-1982 Analysis Description: 120.1 Specific Conductance Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92616646001, 92616646002, 92616646003 METHOD BLANK: 3730853 Matrix: Water Associated Lab Samples: 92616646001, 92616646002, 92616646003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Specific Conductance umhos/cm ND 10.0 08/09/22 10:30 LABORATORY CONTROL SAMPLE: 3730854 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Specific Conductance umhos/cm 1410 1420 100 90-110 SAMPLE DUPLICATE: 3730855 92616646001 Dup Parameter Units Result Result RPD Qualifiers Specific Conductance umhos/cm 523 525 0 SAMPLE DUPLICATE: 3730856 92617494001 Dup Parameter Units Result Result RPD Qualifiers Specific Conductance umhos/cm 49.1 47.7 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 25 aceAnalXical www.pacelabsccm QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 713637 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92616646001, 92616646002, 92616646003, 92616646004 METHOD BLANK: 3720961 Matrix: Water Associated Lab Samples: 92616646001, 92616646002, 92616646003, 92616646004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 1.0 07/28/22 23:31 Sulfate mg/L ND 1.0 07/28/22 23:31 LABORATORY CONTROL SAMPLE: 3720962 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 50 53.8 108 90-110 Sulfate mg/L 50 50.1 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3720963 3720964 MS MSD 92616646001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 58.5 50 50 87.4 88.5 58 60 90-110 1 M1 Sulfate mg/L 3.6 50 50 52.3 53.3 97 99 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3720965 3720966 MS MSD 92615737021 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 14.0 50 50 66.6 65.8 105 104 90-110 1 Sulfate mg/L 89.5 50 50 128 135 78 90 90-110 5 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 25 acmnalOcal www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 QC Batch: 715564 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92616646004 METHOD BLANK: 3730430 Matrix: Water Associated Lab Samples: 92616646004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 08/08/22 14:28 LABORATORY CONTROL SAMPLE: 3730431 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.1 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3730432 3730433 MS MSD 92617423001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 4.1 5 5 9.0 9.0 98 97 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3730434 3730435 MS MSD 92617446001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 2330 5 5 2230 2320 -1980 -310 90-110 4 M1,P4 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services. LLC. Page 17 of 25 1�5a'(c',ice Analytical QD www.pacelaba.ccm QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 714126 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92616646004 METHOD BLANK: 3723127 Matrix: Water Associated Lab Samples: 92616646004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 08/02/22 03:58 LABORATORY CONTROL SAMPLE: 3723128 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10.1 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3723129 3723130 MS MSD 92616922001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 127 10 10 141 128 138 12 90-110 9 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3723131 3723132 MS MSD 92616922002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 135 10 10 149 147 139 119 90-110 1 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 25 1�5a'cucice Malytical QD www.pacelabs.com t 1 QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 714540 Analysis Method: EPA 365.1 Rev 2.01993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92616646004 METHOD BLANK: 3725401 Matrix: Water Associated Lab Samples: 92616646004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 08104/2216:57 LABORATORY CONTROL SAMPLE: 3725402 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3725403 3725404 MS MSD 92615520002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.17 2.5 2.5 2.8 2.7 103 101 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3725405 3725406 MS MSD 92615643001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 7.2 2.5 2.5 9.9 9.6 111 98 90-110 3 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 25 PualicceeAnalXical ( www.paCOIA COO QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kernersville. NC 27284 (704)977-0981 QC Batch: 713475 Analysis Method: SM 531OB-2014 QC Batch Method: SM 531 OB-2014 Analysis Description: 5310E TOC Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92616646001 METHOD BLANK: 3719804 Matrix: Water Associated Lab Samples: 92616646001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 07/28/22 15:45 LABORATORY CONTROL SAMPLE: 3719805 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 23.8 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3719806 3719807 MS MSD 92617003001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L 1.0 25 25 24.7 24.6 95 95 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3719808 3719809 MS MSD 92617003011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L ND 25 25 23.6 23.6 94 94 90-110 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services. LLC. Page 20 of 25 aceAnalyNo/ www pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 QC Batch: 713476 Analysis Method: SM 531OB-2014 QC Batch Method: SM 531OB-2014 Analysis Description: 5310B TOC Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92616646002, 92616646003 METHOD BLANK: 3719819 Matrix: Water Associated Lab Samples: 92616646002, 92616646003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 07/29/22 01:40 LABORATORY CONTROL SAMPLE: 3719820 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 23.8 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3719821 3719822 MS MSD 92616646002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L ND 25 25 23.7 24.1 94 96 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3719823 3719824 MS MSD 92616287002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L ND 25 25 24.9 25.1 99 100 90-110 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 08/09/2022 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC. Page 21 of 25 ace Analytical www.pacelabs.com QUALIFIERS Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TN I - The NELAC Institute. ANALYTE QUALIFIERS B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated for the dilution using the most amount of sample. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. P4 Sample field preservation does not meet EPA or method recommendations for this analysis. R6 The RPD between valid sample dilutions exceeded 30%. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 25 aceArWytical www.pacelabs.com I QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Piedmont Custom Meats-MW/Eff Pace Project No.: 92616646 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Lab ID Sample ID QC Batch Method QC Batch Analytical Analytical Method Batch 92616646001 MW-1 SM 254OC-2015 713584 92616646002 MW-4 SM 254OC-2015 713584 92616646003 MW-5 SM 2540C-2015 713584 92616646004 Effluent SM 254OC-2015 713584 92616646004 Effluent SM 254OD-2015 713210 92616646001 MW-1 EPA 350.1 Rev 2.0 1993 713144 92616646002 MW-4 EPA 350.1 Rev 2.0 1993 713144 92616646003 MW4 EPA 350.1 Rev 2.0 1993 713144 92616646001 MW-1 EPA 353.2 Rev 2.0 1993 712800 92616646002 MW-4 EPA 353.2 Rev 2.0 1993 712800 92616646003 MW-5 EPA 353.2 Rev 2.0 1993 712800 92616646004 Effluent EPA 353.2 Rev 2.0 1993 712800 92616646004 Effluent SM 521OB-2016 713235 SM 521 OB-2016 713746 92616646001 MW-1 SM 9222D-2015 713217 SM 9222D-2015 713218 92616646002 MW-4 SM 9222D-2015 713217 SM 9222D-2015 713218 92616646003 MW-5 SM 9222D-2015 713217 SM 922213-2015 713218 92616646004 Effluent Colilert-18 712973 Colilert-18 712978 92616646001 MW-1 EPA 120.1-1982 715668 92616646002 MW-4 EPA 120.1-1982 715668 92616646003 MW-5 EPA 120.1-1982 715668 92616646004 Effluent TKN+NO3+NO2 715160 Calculation 92616646001 MW-1 EPA 300.0 Rev 2.1 1993 713637 92616646002 MW-4 EPA 300.0 Rev 2.1 1993 713637 92616646003 MW-5 EPA 300.0 Rev 2.1 1993 713637 92616646004 Effluent EPA 300.0 Rev 2.1 1993 713637 92616646004 Effluent EPA 350.1 Rev 2.01993 715564 92616646004 Effluent EPA 351.2 Rev 2.0 1993 714126 EPA 351.2 Rev 2.0 1993 714278 92616646004 Effluent EPA 365.1 Rev 2.0 1993 714540 EPA 365.1 Rev 2.0 1993 714846 92616646001 MW-1 SM 531OB-2014 713475 92616646002 MW-4 SM 531OB-2014 713476 92616646003 MW-5 SM 531OB-2014 713476 Date: 08/09/2022 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 23 of 25 D O O Q a 3 y.�� a ¢tom to o ., a:s� CCRpi II /� a�a C G G U e^? iLA :-f S cd iM rn it 4 t3 • V 6 C CD a 4�J 0 C Z \�1/ fffl� 3 E k k t�i C to .- G uO�41' U ! u .t". E \ O r. >m u u as C .fit ; 2i to G V3 �., p�.�u� t=a .. L x_ REdCiCiE +Cs = to _ r a reGco um03 :; i3 041 0 w O 0 0 c r o cs O a OL u� •- w s men ►.mw �u p.as LA r- I- u ca v u c� --:• '^ 0 2 m .r c. a. is C. 1 z d Gtsd2 xrok w-04 inla � e a m mRa io as • • �" "••- (� Q .L` .7 J a O. O J cis V, ni 0,4 M ; = 0 m £i ` rs C Q jj I♦� r� all Z V '.• m C d LU u E w ++t e x 'd lelQl 'N lBIol N-£HN C, n R �- ¢ ►•- c R 3 Q to o = SON `aP!J0140 'sOl 'ssl '00suj c/I � 3 `7- ,� ? a w' R N T t� ✓ ?• mom. 2 Q ti ~ H z ¢ C .•• -•• N-CHNXXX t wl U3 ? LA c�i. a N o (O-09Z9) OOAl ! o �.N E u O A> O c Li T W E :301 4 w a '`�• oLL o E Puo3 'S01 't7OS t£ON 'aPfaolUO, } � `� to a5.z XXX f100"A z �{ W O G 1 C U a u CID GQ 00 LO v w i^1 c w u M1' O CJ rcD tw ` c p to u �- m Q m a ° Z a, z° az O GZ m to — u - --- .. m w R JE O" F= .. N w c� � r al O a J } w v� u cr E :2 m a u aj3 o- > w v to Q ,� C � y, � u .2 eo e 3 I— m a C p 0 E o v > �. N a m .. N M 0 J ,l ¢ 0 �° u •� tts ,, >g j o� °� n a a tL tsa an u C 0 to-- L x a 0. z et Q H aco u o m V •� at :R u {�� ` �* ei ai m - = Li { 1 CPA to d tJJ in i/] QU. .0 Q o 3 m u ... I ro m ss �% 3 o a0:: m ¢ E` O Q U 0 L fn .� 1 m a c a f� fn coz c� o E -- x LA c x tv O :3 a a V E U tea' c O °'� � 3 u m s y 3 y 7 y 7 � in a CJ x tm i7i 0)0 $ a A O Edcpu cC mm0 �- `L� 5� dHc uCm c • a al c Z qi `- � ... f6 G O�E sn to Q mOG. .Q co w)`'� 'a' u w. a cstu w C :: aJ Q t a L O o C Oo �— LO Efl-$m=Lo a oaoi o u 3 u L a w o u o u a¢x u 24 R5 to -...- W a ' DCT Title: NV-FP.1�!-HU.d1-0Ud4 V01 Tech Spec Sam Condition !.. � � it — _ �on i /mac JE Upon Receipt " E;,ectiv: Data: CS;t'.2o__ "' i i!_ mar: ter pal' cf c c x it a„4, cr is veriria'j any tine ran for presariation samples. TCC, Cil 3-_ : t33:2. C=:! °� S ;s;:�•' CC�. act:-- ;; F a If cf b 0 x is to list nurnbCr of Ea►.,ems *"WChack a'l unpres_rrec' r4i„ates fcr chfcrine PH Adjustment log for Preserved Samples Sample 10 Type of PreserIIative pH upon receipt Care Fr_sero;don -adjusted Time preser,ation Amount of Preservative Lot # adjusted added J I iota: V,ha^ever t`ere is a d;5crepanc-/ of -2=ir& Ncr.1 Carolina CCrnpiiarca sarnpfe5. 3 Copy Of thii f_rr1 w'•il is se -It to t^e Nor; Carotira DFr.i4!1 Cer:f:C3:ian rti:C? (i.e. Out of hold, incorrect presarv3tive, out of tamp, incorrect Containers) Qualtrax Document ID: 70677 Page 2 of 2 Page 25 of 25