HomeMy WebLinkAboutWQ0002857_Monitoring - 07-2022_20220901Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * July
Report Information
WQ0002857
Piedmont Custom Meat WWTF
Type *
NDMR, NDAR-1, NDAR-2, NDMLR
Confirmation Email Address:*
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2022
Upload Document*
Piedmont Custom_July 22.pdf 2.54MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Jessica.Mize@pacelabs.com
Jessica Mize
jwd rA lip
Reviewer: Gerald, Wanda
9/1 /2022
This will be filled in automatically
Is the project number correct?* WQ0002857
Is the monitoring report accepted?* Yes No
Regional Office* Winston-Salem
Reviewer: _anonymous
Review Date: 10/4/2022
Page 1 of 3
NON -DISCHARGE WASTE WATER MONITORING REPORT
PERMIT NUMBER: W00002857 MONTH: Julv YEAR: 2022
FACILITY NAME: Piedmont Custom Meats WWTF COUNTY: Caswell
Flow Monitoring Point: Effluent: LJ Influent:
Parameter Monitoring
Point: Effluent: Influent: Surface Water (SW): U SW Code/Name:
Was There
Effluent Flow for this Month Generated At This Facility: Yes: LJ No:
Operator
wow
W400
50060
00310
00610
005M
31616
70300
00620
1 00625
00940
W600
00665
D
A
-1'
L
Anval
Time
2400
Clock
Operator
Time on
S!m
ORC
on
S4e9
Daily Rate
(Flow)into
Treatment
Ssmm
PH
Residual
Chlorine
60D-3
ITC
NH-3N
TSS
Fecal
Cottle.
(Gm-memc
M'W)
DS
NO.I-N
IKN
CModde
r.Ni
Ninoycn
Inlol
I'M1osphonrs
HRS
YIN
GALLONS
UNITS
u,L
x4GL
NAG
MU
100%u
Mir
%IGL
SIGLL
%161
%161,
MGL
1
3,333
3,333
3
3,333
4
3,333
5
3,333
6
3,333
2
0730
2.011
Y
3,333
6.4
<0.01
8
0630
1.00
Y
1,894
9
1,894
6
1,894
0720
0.25
Y
1,894
6.3
<U01
3,605
13
3,605
14
1
1
1 3,605
1s
3,605
16
3,605
17
3,605
18
3,605
H'
3,605
20
1311
0.25
B
3,605
6.2
<0.01
21
2,199
2,199
23
2,199
24
1
2,199
2,199
26
IOUO
1.51)
Y
2,199
63
<0.01
10.5
35.6
G9.1
443
459
0.58
46.0
138
47.6
0.48
27
4,007
28
4,007
29
4,0117.
30
4,007
st
4,007
M aroge
3,116
JIM
<0.01
IDS
35.6
<3.1
44.3
459
0.58
46.0
138
47.6
OAS
Daily Maximum
4,007
6.40
<0.01
105
35.6
<3.1
44.3
459
U.58
46.0
138
47.6
0.48
Daily 11, imum
1,894
6.20
<0.01
I0.5
35.6
<3.1
44.3
459
0.58
46.0
138
47.6
0.48
Monthly Limits ( Avg) 5000
Composite / Grab (G)
Operator in Responsible Charge (ORC): Glenn Price Grade: SI Phone: 336-996-2841
Check Box if ORC Has Changed: F-1 ORC Certification Number: 987931/20771
Certified Laboratories (1): Pace Analytical Services (2)
Person(s) Collecting Samples: Glenn Price
Mail ORIGINAL and Two COPIES to:
ATTN: Non -Discharge Compliance Unit X �(
DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHA
Division of Water Quality By this signature, I certify that this report is accurate and
1617 Mail Service Center complete to the hest of my knowledge.
RALEIGH, NC 27699-1617
DENR Form NDAR-1 (512003)
NON DISCHARGE WASTEWATER MONITORING REPORT
FACILITY STATUS:
Please answer the following question: Compliant (Y,N)
1. Does all monitoring data and sampling frequencies meet permit requirements?
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its
permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach
additional sheets if necessary.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permitee)* Date
Baron Neal McDuffie (Authorized Agent)
(Permittee-Please print or type)
9683 Kerr's Chapel Road
Gibsonville. NC
(Permittee Address)
01002 Arsenic
01022 Boron
00310 BOD5
01027 Cadmium
00916 Calcium
00940 Chloride
50060 Chlorine, Total
Residual
01034 Chromium
00340 COD
Baron Neal McDuffie
(Name of Signing Official -Please print or type)
Field Services Director (Pace Analytical Services)
PARAMETER CODES
31504
Coliform, Total
00094
Conductivity
01042
Copper
00300
Dissolved Oxygen
31616
Fecal Coliform
01051
Lead
00927
Magnesium
71900
Mercury
00610
NH3 as N
01067
Nickel
(Position or Title)
336-582-8247
(Phone Number)
00600 Nitrogen, Total
00630 NO2 & NO3
00620 NO3
00556 Oil & Grease
W 09 PAN Plant Available
00400 pH
32730 Phenols
00665 Phosphorus, Total
00937 Potassium
00545 Settleable Matter
03/31/21
(Permit Exp. Date)
00929 Sodium
00931 SAR
00745 Sulfide
00515 TDS
00010 Temperature
00625 TKN
00680 TOC
00530 TSS/TSR
00076 Turbidity
01092 Zinc
Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529.
The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 28.0506 (b) (2) (D).
Page 2 of 3
NON -DISCHARGE APPLICATION REPORT
SPRAY IRRIGATION SITE(S)
THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED
PERMIT NUMBER: W00002857 MONTH: Julv YEAR: 2022
FACILITY NAME: Piedmont Custom Meats WWTF COUNTY: Caswell
Formulas:
Daily Loading (inches) = [Volume Applied (gallons) x 0.1336 (cubic feat/gallon) x 12 (inchesdoogl / [Area Sprayed (acres) x 43,560 (square feat/acm) or
= [Volume Applied (gallons) / (Area Sprayed (acres) x 27,152 (gallonslaweinch).
Maximum Hourly Leading(inches) =Daily Loading (inches)/[rime irrigated (minutes) 160(minutes/nour)] Monthly Loading (inches) =Sum of Daily Loading (inches)
12 Month Floating Total (inches) = Sum of this month's Monthly Loading (inches) and previous ll month's Monthly Loadings (Inches)
Average Weekly Loading (inches) = [Monthly Loading (inches/month) I Number of days in the month (dayslmonth )I x 7 (daysAfeek)
.. Irrigation Occur On This Field:
nNo: El
Permitted Yeady Raw (inches):
�x
'weather Coder: C<ki r, PC -panty tloudy, C4elnudy, a-n a Sa-roan, Spsktl
Spray Irrigation Operator in Responsible Charge(ORQ: Glenn Price Phone: 336-996-2841
ORC Certification Number: 987931/20771 Check Box if ORC
Mail ORIGINAL and Two COPIES to:
ATTN: Non -Discharge Compliance Unit
DENR
Division of Water Quality
1617 Mail Service Center
RALEIGH, NC 27699-1617
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHA
By this signature, I certify that this report is accurate and
complete to the best of my knowledge.
DENR Form NDAR-1 (5/2003)
FACILITY STATUS:
Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been comaliant_
with the following permit requirements: (Note: If a requirement does not apply to your facility put
(NA) in the
compliant box.)
Compliant (Y,N)
1. The application rate(s) did not exceed the limit(s) specified in the permit.
2. Adequate measures were taken to prevent wastewater runoff from the site(s).
3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit.
4. All buffer zones as specified in the permit were maintained during each application.
S. The freeboard in the treatment and/or storage lagoon(s) was not less than the
limit(s) specified in the permit.
If the facility is non -compliant , please explain in the space below the reason(s) the facility was not in compliance with its
permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach
additional sheets if necessary.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
S- :5 ( — 2--� Baron Neal McDufe
(Signature of Permitee)* 4V Date (Name of Signing Official -Please print or type)
Baron Neal McDuffie (Authorized Aaent
(Permittee-Please print or type)
9683 Kerr's Chapel Road
Gibsonville. NC
(Permittee Address)
Field Services Director (Pace Analytical Services)
(Position or Title)
336-582-8247
(Phone Number)
03/31/21
(Permit Exp. Date)
* If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D).
DENR Form NDAR-1 (5/2003)
Page 3 of 3
NON -DISCHARGE APPLICATION REPORT
SPRAY IRRIGATION SITES)
THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED
PERMIT NUMBER: W00002857 MONTH: July YEAR: 2022
FACILITY NAME: Piedmont Custom Meats W WTF COUNTY: Caswell
Formulas:
Daily Loading(inches) =Nolume Applied (gallons) x 0.1336 (cubic feeVgallon)x 12(inchestlooQj/[Area Sprayed (acres) x 43,560(square feeVacre) or
= [Volume Applied (gallons) / [Area Sprayed (acres) x 27,152 (gallons/acre4nch).
Maximum Hourly Loading (inches) = Daily Loading (inches) / Time irrigated (minutes) 160 fminutesmour)) Monthly Loading (inches) =Sum of Daily Loading (inches)
12 Month Floating Tobal(inches) = Sum of this month's Monthly Loading (inches) and previous ll month's Monthly Loadings (inches)
Average Weekly Loading (inches) =[Monthly Loading (inches/month)/Number of days in the month (daysrmonth)I x 7(daysNreek)
E '
.... : 12 o:
.
Area Sprayed la�
PennstakfRourly
Rate (inches):
�
A
m
�i�1���llllllllllllllli
����i��
mlllllllli
��
�
��lllllllllllll�
�����
•Nether Codes: C-clear,P-pnrlly dandy, C4rloudy. R-rain. Snenow. Skim
Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841
ORC Certification Number: 987931/20771 Check Box if ORC Has Changed:❑
Mail ORIGINAL and Two COPIES to:
ATTN: Non -Discharge Compliance Unit x
DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
Division of Water Quality
1617 Mail Service Center
RALEIGH, NC 27699-1617
By this signature, I certify that this report is accurate and
complete to the best of my knowledge.
DENR Form NDAR-1 (5/2003)
FACILITY STATUS:
Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant
with the following permit requirements: (Note: If a requirement does not apply to your facility put
(NA) in the
compliant box.)
Compliant (Y,N)
1. The application rate(s) did not exceed the limit(s) specified in the permit.
2. Adequate measures were taken to prevent wastewater runoff from the site(s).
3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit.
4. All buffer zones as specified in the permit were maintained during each application.
5. The freeboard in the treatment and/or storage lagoon(s) was not less than the
limit(s) specified in the permit.
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its
permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach
additional sheets if necessary.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
--s Baron Neal McDuffie
(Signature of Permitee)* Date (Name of Signing Official -Please print or type)
Baron Neal McDuffie (Authorized Agent
(Permittee-Please print or type)
9683 Kerr's Chapel Road
Gibsonville. NC
(Permittee Address)
Field Services Director ( Pace Analytical Services)
(Position or Title)
336-582-8247
(Phone Number)
03/31/21
(Permit Exp. Date)
* If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D).
DENR Form NDAR-1 (5/2003)
aceAnalytical e
WWW.pacalaCs.tom
i
August 09, 2022
Larry Moore
Piedmont Custom Meats
430 NC Highway 49 South
Asheboro, NC 27205
RE: Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Dear Larry Moore:
Pace Analytical Services, LLC
1377 South Park Drive
Kernersvllle, NC 27284
(704)977-0981
Enclosed are the analytical results for sample(s) received by the laboratory on July 26, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Eden
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
A"��
Stephanie Knott
stephanie.knoft@pacelabs.com
704-977-0981
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.I.C.
Page 1 of 25
aceAnalytical
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Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Page 2 of 25
aluc; y ical
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SAMPLE ANALYTE COUNT
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92616646001
MW-1
SM 254OC-2015
AED
1
PASI-E
EPA 350.1 Rev 2.0 1993
SRS
1
PASI-E
EPA 353.2 Rev 2.0 1993
SRS
1
PASI-E
SM 9222D-2015
MWF
1
PASI-E
EPA 120.1-1982
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
2
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92616646002
MW-4
SM 2540C-2015
AED
1
PASI-E
EPA 350.1 Rev 2.0 1993
SRS
1
PASI-E
EPA 353.2 Rev 2.0 1993
SRS
1
PASI-E
SM 9222D-2015
MWF
1
PASI-E
EPA 120.1-1982
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
2
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92616646003
MW-5
SM 254OC-2015
AED
1
PASI-E
EPA 350.1 Rev 2.0 1993
SRS
1
PASI-E
EPA 353.2 Rev 2.01993
SRS
1
PASI-E
SM 9222D-2015
MWF
1
PASI-E
EPA 120.1-1982
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
2
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92616646004
Effluent
SM 254OC-2015
AED
1
PASI-E
SM 2540D-2015
DAW
1
PASI-E
EPA 353.2 Rev 2.01993
SRS
2
PASI-E
SM 521OB-2016
MWF
1
PASI-E
Colilert-18
LRB
1
PASI-E
TKN+NO3+NO2 Calculation
MDW
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.01993
KDF1
1
PASI-A
EPA 351.2 Rev 2.01993
MFO
1
PASI-A
EPA 365.1 Rev 2.01993
SMT
1
PASI-A
PASI A = Pace Analytical Services - Asheville
PASI-E = Pace Analytical Services - Eden
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 25
aceAnalytical
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ANALYTICAL RESULTS
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Sample: MWA Lab ID: 92616646001 Collected: 07/26/22 09:49 Received: 07/26/22 11:45 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No.
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
352 mg/L 25.0
1
07/29/22 10:47
350.1 Ammonia EDN
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Ammonia
ND mg/L 0.10
1
07/27/22 10:54 7664-41-7
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
21.0 mg/L 0.40
10
07/26/22 16:00 14797-55-8
MBIO 92220 Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
ND CFU/100 mL 1.0
1
07/26/22 15:06 07/27/22 14:25
120.1 Specific Conductance
Analytical Method: EPA 120.1-1982
Pace Analytical Services -Asheville
Specific Conductance
523 umhos/cm 10.0
1
08/09/2210:35
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Qual
Chloride 58.5 mg/L 1.0 1 07/29/22 00:31 16887-00-6 M1
Sulfate 3.6 mg/L 1.0 1 07/29/22 00:31 14808-79-8
5310B TOC Analytical Method: SM 531 OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon ND mg/L 1.0 1 07/29/22 00:28 7440-44-0
Date: 08/09/2022 03:52 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 25
(�5a'cuceAnalXical
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ANALYTICAL RESULTS
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Sample: MW-4 Lab ID: 92616646002 Collected: 07/26/22 10:16 Received: 07/26/22 11:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
549 mg/L 25.0
1
07/29/22 10:47
350.1 Ammonia EDN
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Ammonia
ND mg/L 0.10
1
07/2712210:53 7664-41-7
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
1.9 mg/L 0.040
1
07/26/22 15:55 14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
42.0 CFU/100 mL 1.0
1
07/26/22 15:06 07/27/22 14:25
120.1 Specific Conductance
Analytical Method: EPA 120.1-1982
Pace Analytical Services -Asheville
Specific Conductance
1020 umhos/cm 10.0
1
08/09/22 10:39
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
212 mg/L 5.0
5
07/29/2216:12 16887-00-6
Sulfate
2.4 mg/L 1.0
1
07/29/22 01:15 14808-79-8
5310B TOC
Analytical Method: SM 531 OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
07/29/22 02:14 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, L.L.C.
Page 5 of 25
aceAnalytical
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ANALYTICAL RESULTS
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Sample: MW-5 Lab ID: 92616646003 Collected: 07/26/22 10:32 Received: 07/26/22 11:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
154 mg/L 25.0
1
07/29/22 10:47
350.1 Ammonia EDN
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Ammonia
ND mg/L 0.10
1
07/27/2211:17
7664-41-7
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
0.11 mg/L 0.040
1
07/26/22 15:56
14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
ND CFU/100 mL 1.0
1
07/26/22 15:06 07/27/22 14:25
120.1 Specific Conductance
Analytical Method: EPA 120.1-1982
Pace Analytical Services -Asheville
Specific Conductance
249 umhos/cm 10.0
1
08/09/22 10:41
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
36.2 mg/L 1.0
1
07/29/22 01:30
16887-00-6
Sulfate
ND mg/L 1.0
1
07/29/22 01:30
14808-79-8
5310E TOC
Analytical Method: SM 531 OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
07/29/22 03:09
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 25
ace AnalyNoI
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ANALYTICAL RESULTS
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Sample: Effluent
Parameters
Lab lD: 92616646004 Collected: 07/26/22 09:38
Results Units Report Limit DF
Received: 07/26/22 11:45 Matrix: Water
Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
459 mg/L 25.0 1
07/29/22 10:47
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analytical Services - Eden
Total Suspended Solids
ND mg/L 3.1 1
07/27/22 16:10
353.2 NO2JN03 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
1.6 mg/L 0.040 1
07/26/22 15:53
Nitrogen, Nitrate
0.58 mg/L 0.040 1
07/26/22 15:53 14797-55-8
5210B BOD, 5 day EDN
Analytical Method: SM 521OB-2016 Preparation Method:
SM 521OB-2016
Pace Analytical Services - Eden
BOD, 5 day
10.5 mg/L 2.0 1
07/27/22 16:28 08/01 /22 14:55 B2
Colilert-18 Fecal Coliform EDN
Analytical Method: Colilert-18 Preparation Method: Colilert-18
Pace Analytical Services - Eden
Fecal Coliforms
44.3 MPN/100ml- 1.0 1
07/26/22 14:27 07/27/22 08:37
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
Total Nitrogen
47.6 mg/L 0.040 1
08/04/22 18:43
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
138 mg/L 3.0 3
07/29/2216:27 16887-00-6
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
35.6 mg/L 1.0 10
08/08/22 14:56 766441-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Kjeldahl, Total
46.0 mg/L 2.5 5
08/01/22 17:32 08/02/22 05:31 7727-37-9
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
0.48 mg/L 0.050 1
08/03/2218:08 08/04/2-217:07 7723-14-0
REPORT OF LABORATORY ANALYSIS
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Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 25
aceAnalytr`cal
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QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 713584
Analysis Method: SM 2540C-2015
QC Batch Method: SM 2540C-2015
Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92616646001, 92616646002, 92616646003, 92616646004
METHOD BLANK: 3720477
Matrix: Water
Associated Lab Samples: 92616646001, 92616646002,
92616646003, 92616646004
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Dissolved Solids
mg/L
ND 25.0 07/29/22 10:47
LABORATORY CONTROL SAMPLE:
3720478
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids
mg/L
250 248 99 90-110
SAMPLE DUPLICATE: 3720479
92616646001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Dissolved Solids
mg/L
352 355 1
SAMPLE DUPLICATE: 3720480
92617332002 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Dissolved Solids
mg/L
98.0 90.0 9
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 25
QD
5a'uce1�
AnalXical
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QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QC Batch: 713210
Analysis Method: SM 2640D-2015
QC Batch Method: SM 254OD-2015
Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92616646004
METHOD BLANK: 3718581
Matrix: Water
Associated Lab Samples: 92616646004
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 07/27/22 16:09
LABORATORY CONTROL SAMPLE: 3718582
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 234 94 90-110
SAMPLE DUPLICATE: 3718584
92616746002 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
47.9 41.4 15
SAMPLE DUPLICATE: 3718887
92616753001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
32.2 31.2 3
Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 25
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QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 713144
Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993
Analysis Description: 350.1 Ammonia, EDN
Laboratory: Pace
Analytical Services - Eden
Associated Lab Samples: 92616646001, 92616646002, 92616646003
METHOD BLANK: 3718285
Matrix: Water
Associated Lab Samples: 92616646001, 92616646002, 92616646003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Ammonia mg/L
ND 0.10
07/27/22 10:42
LABORATORY CONTROL SAMPLE: 3718286
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Ammonia mg/L
5 5.0
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3718287 3718288
MS MSD
92616597001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Ammonia mg/L ND
5 5 4.9
4.9 99 99
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3718289 3718290
MS MSD
92616753002
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Ammonia mg/L ND
5 5 4.9
4.9 98 98
90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 25
la 'uc ice;Affllytical
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QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 712800
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92616646001, 92616646002, 92616646003, 92616646004
METHOD BLANK: 3716690
Matrix: Water
Associated Lab Samples: 92616646001, 92616646002,
92616646003, 92616646004
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L
ND 0.040 07/26/22 11:06
Nitrogen, NO2 plus NO3 mg/L
ND 0.040 07/26/22 11:06
LABORATORY CONTROL SAMPLE: 3716691
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L
1.5 1.5 97 90-110
Nitrogen, NO2 plus NO3 mg/L
2.5 2.4 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3716692 3716693
MS MSD
92616520001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate mg/L 5.8
1.5 1.5 7.1 7.1 88 85
90-110 1
Nitrogen, NO2 plus NO3 mg/L 5.8
2.5 2.5 8.1 8.1 94 92
90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 25
acice, Ana l
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QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
QC Batch: 713235 Analysis Method: SM 521OB-2016
QC Batch Method: SM 521OB-2016 Analysis Description: 5210B BOD, 5 day Final EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92616646004
METHOD BLANK: 3718790
Associated Lab Samples: 92616646004
Parameter Units
BOD, 5 day mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 08/01 /22 14:02
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
LABORATORY CONTROL SAMPLE: 3718791
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
BOD, 5 day mg/L 198 193 98 84.6-115
SAMPLE DUPLICATE: 3718793
92616817001 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day mg/L 933 893 4 R6
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
QC Batch: 713217 Analysis Method: SM 9222D-2015
QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform( MF)-EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92616646001, 92616646002, 92616646003
METHOD BLANK: 3718611 Matrix: Water
Associated Lab Samples: 92616646001, 92616646002, 92616646003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 07/27/22 14:25
SAMPLE DUPLICATE: 3718612
92616646001 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms CFU/100 mL ND ND
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 25
I
eAnalyiical�
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1
QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
QC Batch: 712973 Analysis Method: Colilert-18
QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92616646004
SAMPLE DUPLICATE: 3717703
92616596001 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms MPN/100mL ND ND
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 25
aceAnalj cal
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QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville. NC 27284
(704)977-0981
QC Batch: 715668
Analysis Method: EPA 120.1-1982
QC Batch Method: EPA 120.1-1982
Analysis Description: 120.1 Specific Conductance
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92616646001, 92616646002, 92616646003
METHOD BLANK: 3730853
Matrix: Water
Associated Lab Samples: 92616646001, 92616646002, 92616646003
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Specific Conductance
umhos/cm
ND 10.0 08/09/22 10:30
LABORATORY CONTROL SAMPLE:
3730854
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Specific Conductance
umhos/cm
1410 1420 100 90-110
SAMPLE DUPLICATE: 3730855
92616646001 Dup
Parameter
Units
Result Result RPD Qualifiers
Specific Conductance
umhos/cm
523 525 0
SAMPLE DUPLICATE: 3730856
92617494001 Dup
Parameter
Units
Result Result RPD Qualifiers
Specific Conductance
umhos/cm
49.1 47.7 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 25
aceAnalXical
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QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 713637
Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993
Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92616646001, 92616646002, 92616646003, 92616646004
METHOD BLANK: 3720961
Matrix: Water
Associated Lab Samples: 92616646001, 92616646002,
92616646003, 92616646004
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Chloride mg/L
ND 1.0
07/28/22 23:31
Sulfate mg/L
ND 1.0
07/28/22 23:31
LABORATORY CONTROL SAMPLE: 3720962
Spike LCS
LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Chloride mg/L
50 53.8
108 90-110
Sulfate mg/L
50 50.1
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3720963 3720964
MS MSD
92616646001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Chloride mg/L 58.5
50 50 87.4
88.5 58 60
90-110
1 M1
Sulfate mg/L 3.6
50 50 52.3
53.3 97 99
90-110
2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3720965 3720966
MS MSD
92615737021
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Chloride mg/L 14.0
50 50 66.6
65.8 105 104
90-110
1
Sulfate mg/L 89.5
50 50 128
135 78 90
90-110
5 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 25
acmnalOcal
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QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QC Batch: 715564
Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993
Analysis Description: 350.1
Ammonia
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92616646004
METHOD BLANK: 3730430
Matrix: Water
Associated Lab Samples: 92616646004
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Ammonia mg/L
ND 0.10
08/08/22 14:28
LABORATORY CONTROL SAMPLE: 3730431
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Ammonia mg/L
5 5.1
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3730432 3730433
MS MSD
92617423001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Ammonia mg/L 4.1
5 5 9.0
9.0 98 97
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3730434 3730435
MS MSD
92617446001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Ammonia mg/L 2330
5 5 2230
2320 -1980 -310
90-110 4 M1,P4
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services. LLC.
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1�5a'(c',ice Analytical QD
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QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 714126
Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92616646004
METHOD BLANK: 3723127
Matrix: Water
Associated Lab Samples: 92616646004
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/L
ND 0.50
08/02/22 03:58
LABORATORY CONTROL SAMPLE: 3723128
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/L
10 10.1
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3723129 3723130
MS MSD
92616922001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/L 127
10 10 141
128 138 12
90-110 9 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3723131 3723132
MS MSD
92616922002
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/L 135
10 10 149
147 139 119
90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 25
1�5a'cucice Malytical QD
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t
1
QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 714540
Analysis Method: EPA 365.1 Rev 2.01993
QC Batch Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92616646004
METHOD BLANK: 3725401
Matrix: Water
Associated Lab Samples: 92616646004
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Phosphorus mg/L
ND 0.050 08104/2216:57
LABORATORY CONTROL SAMPLE: 3725402
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Phosphorus mg/L
2.5 2.5 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3725403 3725404
MS MSD
92615520002
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Phosphorus mg/L 0.17
2.5 2.5 2.8 2.7 103 101
90-110 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3725405 3725406
MS MSD
92615643001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Phosphorus mg/L 7.2
2.5 2.5 9.9 9.6 111 98
90-110 3 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 25
PualicceeAnalXical
( www.paCOIA COO
QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville. NC 27284
(704)977-0981
QC Batch: 713475
Analysis Method: SM 531OB-2014
QC Batch Method: SM 531 OB-2014
Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92616646001
METHOD BLANK: 3719804
Matrix: Water
Associated Lab Samples: 92616646001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
07/28/22 15:45
LABORATORY CONTROL SAMPLE: 3719805
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 23.8
95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3719806 3719807
MS MSD
92617003001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Total Organic Carbon mg/L 1.0
25 25 24.7
24.6 95 95
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3719808 3719809
MS MSD
92617003011
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Total Organic Carbon mg/L ND
25 25 23.6
23.6 94 94
90-110 0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services. LLC.
Page 20 of 25
aceAnalyNo/
www pacelabs.com
QUALITY CONTROL DATA
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville. NC 27284
(704)977-0981
QC Batch: 713476
Analysis Method: SM 531OB-2014
QC Batch Method: SM 531OB-2014
Analysis Description: 5310B TOC
Laboratory: Pace
Analytical Services -Asheville
Associated Lab Samples: 92616646002, 92616646003
METHOD BLANK: 3719819
Matrix: Water
Associated Lab Samples: 92616646002, 92616646003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
07/29/22 01:40
LABORATORY CONTROL SAMPLE: 3719820
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 23.8
95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3719821 3719822
MS MSD
92616646002
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Total Organic Carbon mg/L ND
25 25 23.7
24.1 94 96
90-110 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3719823 3719824
MS MSD
92616287002
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Total Organic Carbon mg/L ND
25 25 24.9
25.1 99 100
90-110 1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 08/09/2022 03:52 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC.
Page 21 of 25
ace Analytical
www.pacelabs.com
QUALIFIERS
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville. NC 27284
(704)977-0981
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TN I - The NELAC Institute.
ANALYTE QUALIFIERS
B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
P4 Sample field preservation does not meet EPA or method recommendations for this analysis.
R6 The RPD between valid sample dilutions exceeded 30%.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/09/2022 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 25
aceArWytical
www.pacelabs.com
I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Piedmont Custom Meats-MW/Eff
Pace Project No.: 92616646
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical
Analytical Method Batch
92616646001
MW-1
SM 254OC-2015
713584
92616646002
MW-4
SM 254OC-2015
713584
92616646003
MW-5
SM 2540C-2015
713584
92616646004
Effluent
SM 254OC-2015
713584
92616646004
Effluent
SM 254OD-2015
713210
92616646001
MW-1
EPA 350.1 Rev 2.0 1993
713144
92616646002
MW-4
EPA 350.1 Rev 2.0 1993
713144
92616646003
MW4
EPA 350.1 Rev 2.0 1993
713144
92616646001
MW-1
EPA 353.2 Rev 2.0 1993
712800
92616646002
MW-4
EPA 353.2 Rev 2.0 1993
712800
92616646003
MW-5
EPA 353.2 Rev 2.0 1993
712800
92616646004
Effluent
EPA 353.2 Rev 2.0 1993
712800
92616646004
Effluent
SM 521OB-2016
713235
SM 521 OB-2016 713746
92616646001
MW-1
SM 9222D-2015
713217
SM 9222D-2015 713218
92616646002
MW-4
SM 9222D-2015
713217
SM 9222D-2015 713218
92616646003
MW-5
SM 9222D-2015
713217
SM 922213-2015 713218
92616646004
Effluent
Colilert-18
712973
Colilert-18 712978
92616646001
MW-1
EPA 120.1-1982
715668
92616646002
MW-4
EPA 120.1-1982
715668
92616646003
MW-5
EPA 120.1-1982
715668
92616646004
Effluent
TKN+NO3+NO2
715160
Calculation
92616646001
MW-1
EPA 300.0 Rev 2.1 1993
713637
92616646002
MW-4
EPA 300.0 Rev 2.1 1993
713637
92616646003
MW-5
EPA 300.0 Rev 2.1 1993
713637
92616646004
Effluent
EPA 300.0 Rev 2.1 1993
713637
92616646004
Effluent
EPA 350.1 Rev 2.01993
715564
92616646004
Effluent
EPA 351.2 Rev 2.0 1993
714126
EPA 351.2 Rev 2.0 1993 714278
92616646004
Effluent
EPA 365.1 Rev 2.0 1993
714540
EPA 365.1 Rev 2.0 1993 714846
92616646001
MW-1
SM 531OB-2014
713475
92616646002
MW-4
SM 531OB-2014
713476
92616646003
MW-5
SM 531OB-2014
713476
Date: 08/09/2022 03:52 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 25
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' DCT Title: NV-FP.1�!-HU.d1-0Ud4 V01 Tech Spec Sam Condition
!.. � � it
— _ �on i
/mac JE Upon Receipt "
E;,ectiv: Data: CS;t'.2o__ "' i i!_ mar: ter pal' cf c c x it a„4, cr
is veriria'j any tine ran for
presariation samples.
TCC, Cil 3-_ : t33:2. C=:! °� S ;s;:�•' CC�.
act:-- ;; F a If cf b 0 x is to list nurnbCr of Ea►.,ems
*"WChack a'l unpres_rrec' r4i„ates fcr chfcrine
PH Adjustment log for Preserved Samples
Sample 10 Type of PreserIIative pH upon receipt Care Fr_sero;don -adjusted Time preser,ation Amount of Preservative
Lot #
adjusted added
J
I
iota: V,ha^ever t`ere is a d;5crepanc-/ of -2=ir& Ncr.1 Carolina CCrnpiiarca sarnpfe5. 3 Copy Of thii f_rr1 w'•il is se -It to t^e Nor; Carotira DFr.i4!1 Cer:f:C3:ian rti:C? (i.e.
Out of hold, incorrect presarv3tive, out of tamp, incorrect Containers)
Qualtrax Document ID: 70677
Page 2 of 2
Page 25 of 25