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HomeMy WebLinkAboutWQ0004972_Monitoring - 07-2022_20220901Monitoring Report Submittal Permit Number #* Name of Facility:* Month: * July Report Information WQ0004972 Forest Lake Preserve ELS Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address:* Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2022 Upload Document* Forest Lakes —July 22.pdf 1.97MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Jessica.Mize@pacelabs.com Jessica Mize jwd rA lip Reviewer: Gerald, Wanda 9/1 /2022 This will be filled in automatically Is the project number correct?* WQ0004972 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 10/4/2022 Page 1 of 2 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: W00004972 MONTH: Julv YEAR: 2022 FACILITY NAME: Forest Lakes Preserve ELS COUNTY: Davie Flow Monitoring Point: Effluent: lyl Influent: Parameter Monitoring Point: Effluent: I Influent: I I S ace Water isW : SW Code/Name: Was There Effluent Flow for this Month Generated At This Facility: Yes: N Opemmr W050 00400 50060 W310 00610 own 31616 0060 00625 own Now 00620 70300 WS"10 B A * r AMval Muse 24M Cloa Opendor Them Siu ORC on site? Davy pate (19.)into TnNaruent Sysmn pH H.klul Ouoinr Boo 26C NHLN TSS Feral car. (Gooumir Mon) Taal PMs Taal Njddiul Ni mgM NO2-NW Tool Ninale Nanun NO3.N Tool Dixsalvol Solids CNadde HRS YIN GPD UNITS mgrL M iL St MG,1. tlOUML 0= MGL 61G,1. Mr✓L MGr h1GL 61GrL CMINuws ml y onl y m y mt v .gyp, 1 0915 0.25 B 12555 6.0 <0.01 2 18,620 71 3 18.620 + 1 1 1 18.620 thnlidav --- ----- 5 1605 0.25 B 18,620 1 6.3 <0.01 6 1524 0.25 Y 11.1125 6.1 <0.01 1509 0.25 Y 11.179 6.2 <0.01 S 1059 0.50 Y 121580 6.1 <0.01 0 18,009 10 18,009 D 1600 0.25 B 18,009 6.1 <0.01 12 1600 0.25 B 12,336 6.0 <0.01 13 0700 0.25 Y IIA53 6.0 <0.01 W. 0740 0.25 Y IIMIN 6.0 <0.01 is 0716 0.25 Y 12,066 6.1 <0.01 6 15,929 15,929 Is 11719 0.25 Y 15,929 6.1 <0.01 19 11733 0.25 V 11,128 6.0 <0.01 20 6741 0.25 1 12.396 6.0 <0.01 21 0810 1.25 Y 12,144 6.0 <0.01 2.0 88.4 5.3 2420 11.1 104 <0.040 104 <0.040 362 68.2 22 0755 0.25 Y 11.921 6.0 <0.01 23 14,733 24 14,733 25 1520 1 0.25 1 Y 14.733 6.2 <0.01 26 1315 0.25 a 13.693 6.1 <0.01 n 1620 0.25 B - 12,004 6.1 <0.01 28 1420 0.25 1 B 12,219 6.1 <0.01 79 0950 0.25 13 12.088 6.0 <0.01 3o 15,111 15.111 .Avempe Uaily Maxiummum 14.275 18.620 6.3 70.01 <0.01 -.11 2421) 11.1 0 <0.040 I < , 362 681 -.II 5.3 2420 I L I 0' q).1140 <0.040 62 b8_2 Daily Minim 11,008 6.0 <0.01 2.0 88.4 5.3 2420 11.1 1 104 <0.040 104 <0.040 362 68.2 Monthly Limits Is) 24400 Composite 0 / Grab IG) *FLOWS ESTIMATED, FLOW METER INOPERABLE MAY 1st - MAY 20th Operator in Responsible Charge (ORC): Glenn Price Grade: II Phone: 336-996-2841 Check Box if ORC Has Changed: 11 ORC Certification Number: 987931/20771 Certified Laboratories (1): Pace Analytical Serivees (2): . Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X H�a.�---� DENR v (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, I certify that this report is accurate and 1617 Dfail Service Center complete to the bat of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant N) 1. Does all monitoring data and sampling frequencies meet permit requirements? L*_j If the facility is non -compliant , please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Flow Estimated, Flow meter inoperable May 1 st - May 20th "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." " 3 1 ` 2 Baron Neal McDuffie (Signature of Permitee)* Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N Riverside Plaza , Suite 800 Chicago, Il 60606 (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 31504 Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel Field Services Director (Pace Analytical Services) (Position or Title) 3/31/21 (Permit Exp. Date) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease W 09 PAN(Plant Available) 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting * If signed by other than the Permittee, delegation of signatory authority must be on rile with the state per 15A NCAC 213.0506 (b) (2) (D). Page 2 of 2 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W0004972 MONTH: Julv YEAR: 2022 FACILITY NAME: Forest Lakes Preserve ELS. COUNTY: Davie Formulas: Daily Loading (inches) =(Volume Applied (gallons) x 0.1336(cubic feeVgagen)x12(inchedfoli(Area Sprayed (acres) x 43.560(square feevacre)or = [Volume Applied (gallons) I (Area Sprayed (acres) x 27,152 (gallonslacre4nch). Maximum Hourly Loading (inches) =Daily Loading (Inches)/[rime irrigated (minutes) 160(mimunshtur)l Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Total (inches) =Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = [Monthly Loading (incheslmonth) I Number of days in the month (daysrmonth )1 x 7 (daysvoeek) Did Irrigation Occur At This Facility: Yes No❑ Did Irrigation Occur On This Feld: Y No: ❑ Did Irrigation Occur On This Feld: Ye❑ No: Field Number: Feld Number: Area Sprayed (aces): 6.0 Area Sprayed (acres): Cover Crop: Cover Crop: ermine au y to mches : 0.11 Permitted Hourly Rate (inches): D A T H+ WEATHER CONDMONS sioage 1<9ran Permined Yearly Rate (inches): 46.8 Permitted Yearly Rate (inches): WmNv Cade' TanpMlue .I am'iulirn lomate . r v,awnc Arrr¢1 nee lin"ol aib- tmJmr M-nwn nw, Immna vmn,k A,I.W Ti _",al L.'h2c 6hamwn L"li[' Fe Kure 1"FI IwMs cell •n ixhw uµLs rall..n ind." aL.� C 78 0 3.1 3 4 5 C 89 0 2.0 33.984 240 0.21 0.06 6 R 92 0.4 1 3.0 7 Cl 93 0 2.7 R Cl 83 0 2.4 42,480 300 0.26 0.06 9 11) u PC 81 0 23 33984 240 0.21 0.06 12 C 90 0 3.2 u Cl 74 0 3.0 14 PC 72 0 2.9 33,984 240 0.21 0.06 15 PC 72 0 3.9 16 17 Is R 72 0.2i 2.8 19 R 74 0.50 16 20 CI 71 0 1.4 21 PC 73 0 2.1 42,481) 300 0.26 0.06 22 PC 70 0 3.1 z3 2 25 Cl 86 0 2.6 26 Cl 89 0 2.2 n C 92 - 0 2.1 00 0.26 0.06 29 C 93 1) 2.1 42,481) 300 0.26 0.06 z9 C 1 79 1 0 2.9 3e 31 Total Calloml,11i Lmde¢Iii o Memh Floaloa rout lio[hetl Avmae%Vmkll' L.aatlbF an[Gnl i 1.67 = 22.00 0.42 ;ak' 0 'we&Ihor C W6: C-cli rC-part, [loud). CHIouOr, Whom 50-foox, sFskel Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed: Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X. ec DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHAROf Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been comaliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. C� 2. Adequate measures were taken to prevent wastewater runoff from the site(s). �— 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. C 4. All buffer zones as specified in the permit were maintained during each application. S. The freeboard in the treatment and/or storage lagoon(s) was not less than the `--� limit(s) specified in the permit. If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." .11" L—< • 3 t • .2-7' Baron Neal McDuffie (Signature of Permitee)* Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N. Riverside Plaza, Suite 800 Chicago,11 60606 (Permittee Address) Field Services Director (Pace Analytical Services) (Position or Title) 3/31 /2021 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). aceAnalXical anocpacelabs.eom I August 03, 2022 Tracy Overdurf Forest Lake 192 Thousand Trails Dr. Advance, NC 27006 RE: Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Dear Tracy Overdurf: Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27264 (764)977-0981 Enclosed are the analytical results for sample(s) received by the laboratory on July 21, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie.knoft@pacelabs.com 704-977-0981 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 24 5aceAnalXical www pacelabasom { Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, L.L.C. Page 2 of 24 aCLA; lylical `� j www.pacelaba.ecm i SAMPLE ANALYTE COUNT Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Lab ID Sample ID Method Analysts Analyses Reported Laboratory 92615985001 MW1 EPA 353.2 Rev 2.0 1993 SRS 1 PASI-E SM 9222D-2015 AED 1 PASI-E EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A EPA 350.1 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 SMT 1 PASI-A SM 531OB-2014 MJP 1 PASI-A 92615985002 MW2 EPA 353.2 Rev 2.0 1993 SRS 1 PASI-E SM 9222D-2015 AED 1 PASI-E EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A EPA 350.1 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 SMT 1 PASI-A SM 531OB-2014 MJP 1 PASI-A 92615985003 MW3 EPA 353.2 Rev 2.0 1993 SRS 1 PASI-E SM 9222D-2015 AED 1 PASI-E EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A EPA 350.1 Rev 2.01993 KDF1 1 PASI-A EPA 365.1 Rev 2.01993 SMT 1 PASI-A SM 531OB-2014 MJP 1 PASI-A 92615985004 MW4 EPA 353.2 Rev 2.0 1993 SRS 1 PASI-E SM 922213-2015 AED 1 PASI-E EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A EPA 350.1 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 SMT 1 PASI-A SM 531OB-2014 MJP 1 PASI-A 92615985005 Effluent SM 254OC-2015 MWF 1 PASI-E SM 254OD-2015 LRB 1 PASI-E EPA 353.2 Rev 2.0 1993 SRS 1 PASI-E SM 521OB-2016 MWF 1 PASI-E Colilert-18 SRS 1 PASI-E TKN+NO3+NO2 Calculation MDW 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A EPA 350.1 Rev 2.0 1993 KDF1 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 SMT 1 PASI-A PASI-A = Pace Analytical Services -Asheville PASI-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 24 aceAnalXical QD www.pacelabs.com ANALYTICAL RESULTS Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: MW1 Parameters Lab ID: 92615985001 Collected: 07/21/22 08:00 Results Units Report Limit DF Received: 07/21/22 11:00 Matrix: Water Prepared Analyzed CAS No. Qual 353.2 N021NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 0.35 mg/L 0.040 1 07/22/22 13:18 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 922213-2015 Pace Analytical Services - Eden Fecal Coliforms 1.0 CFU/100 mL 1.0 1 07/21/22 15:29 07/22/22 13:38 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 1.1 mg/L 1.0 1 07/26/22 09:36 16887-00-6 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 0.26 mg/L 0.10 1 08/03/22 10:39 7664-41-7 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 0.10 mg1L 0.050 1 07/29/2214:31 07/29/2219:16 7723-14-0 5310B TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon 2.1 mg/L 1.0 1 07/26/22 13:52 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 24 5ac ie A na /j dica I www.pacelabs.com ANALYTICAL RESULTS Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 Sample: MW2 Lab ID: 92615985002 Collected: 07/21/22 08:19 Received: 07/21/22 11:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 353.2 N021NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 0.95 mg/L 0.040 1 07/22/22 13:22 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms 5.0 CFU/100 mL 1.0 1 07/21/22 15:29 07/22/22 13:38 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 6.6 mg/L 1.0 1 07/26/22 09:55 16887-00-6 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia ND mg/L 0.10 1 08/03/22 10:41 7664-41-7 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 0.077 mg/L 0.050 1 07/29/2214:31 07/29/2219:18 7723-14-0 5310E TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 07/26/22 14:10 744044-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 24 acmnalytical www.pacelaDs.cam ANALYTICAL RESULTS Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: MW3 Lab lD: 92615985003 Collected: 07/21/22 08:41 Received: 07/21/22 11:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 353.2 N021NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 8.5 mg/L 0.080 2 07/22/22 13:34 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms 1.0 CFU/100 mL 1.0 1 07/21/22 15:29 07/22/22 13:38 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 26.0 mg/L 1.0 1 07/26/2210:14 16887-00-6 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia ND mg/L 0.10 1 08/03/22 10:42 7664-41-7 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus ND mg/L 0.050 1 07/2912214:31 07/29/2219:19 7723-14-0 5310E TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 07/26/22 14:27 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 24 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Sample: MW4 Lab ID: 92615985004 Collected: 07/21/22 09:06 Received: 07/21/22 11:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen. Nitrate 0.058 mg/L 0.040 1 07/22/22 13:24 14797-55-8 M1310 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms 2.0 CFU/100 mL 1.0 1 07/21/22 15:29 07/22/22 13:38 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 3.4 mg/L 1.0 1 07/26/2211:11 16887-00-6 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia ND mg/L 0.10 1 08/03/22 10:43 7664-41-7 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus ND mg/L 0.050 1 07/29/2214:31 07/29/2219:20 7723-14-0 5310E TOC Analytical Method: SM 531OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 07/26/22 14:44 7440-44-0 Date: 08/03/2022 04:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 24 aceAnalytical www.pacelabs.cem ANALYTICAL RESULTS Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: Effluent Parameters Lab ID: 92615985005 Collected: 07/21/22 08:09 Results Units Report Limit DF Received: 07/21/22 11:00 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 362 mg/L 50.0 1 07/25/22 10:46 2540D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services - Eden Total Suspended Solids 5.3 mg/L 2.5 1 07/26/22 08:58 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate ND mg/L 0.040 1 07/22/22 13:21 14797-55-8 5210E BOD, 5 day EDN Analytical Method: SM 521OB-2016 Preparation Method: SM 521OB-2016 Pace Analytical Services - Eden BOD, 5 day 2.0 mg/L 2.0 1 07/22/22 12:08 07/27/22 13:47 Colilert-18 Fecal Coliform EDN Analytical Method: Colilert-18 Preparation Method: Colilert-18 Pace Analytical Services - Eden Fecal Coliforms 2420 MPN/100mL 1.0 1 07/21/22 15:12 07/22/22 09:15 El Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 104 mg/L 0.040 1 08/02/22 19:06 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 68.2 mg/L 1.0 1 07/26/2211:30 16887-00-6 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 88A mg/L 5.0 50 08/03/22 11:44 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 104 mg/L 5.0 10 07/28/22 17:24 07/29/22 03:55 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 ND mg/L 0.040 1 08/02/22 10:50 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.01993 Pace Analytical Services -Asheville Phosphorus 11.1 mg/L 0.25 5 07129/2214:31 07/29/2219:21 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 24 aceAnalytical o www.pacelabs.com QUALITY CONTROL DATA Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersvitle, NC 27284 (704)977-0981 QC Batch: 712602 Analysis Method: SM 254OC-2015 QC Batch Method: SM 254OC-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92615985005 METHOD BLANK: 3715393 Matrix: Water Associated Lab Samples: 92615985005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 07/25/22 10:44 LABORATORY CONTROL SAMPLE: 3715394 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 244 98 90-110 SAMPLE DUPLICATE: 3715395 92615481002 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 93.0 93.0 0 SAMPLE DUPLICATE: 3715396 92616069001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 1770 1730 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 24 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 712596 Analysis Method: SM 2540D-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92615985005 METHOD BLANK: 3715363 Matrix: Water Associated Lab Samples: 92615985005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 07/26/22 08:55 LABORATORY CONTROL SAMPLE: 3715364 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 242 97 90-110 SAMPLE DUPLICATE: 3715365 92615564001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 65.3 72.9 11 SAMPLE DUPLICATE: 3715854 92616062001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 29.5 29.7 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 24 aceAnalXical www pacelabs.ccm QUALITY CONTROL DATA Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park drive Kemersville, NC 27284 (704)977-0981 QC Batch: 712296 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.01993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005 METHOD BLANK: 3714093 Matrix: Water Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.040 07/22/22 13:15 LABORATORY CONTROL SAMPLE: 3714094 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.4 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3714095 3714096 MS MSD 92615985001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 0.35 1.5 1.5 1.8 1.8 93 94 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 24 (�5a'ce Analytical www.pacelabs.com QUALITY CONTROL DATA Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 QC Batch: 712309 Analysis Method: SM 521OB-2016 QC Batch Method: SM 5210B-2016 Analysis Description: 521013 BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92615985005 METHOD BLANK: 3714148 Matrix: Water Associated Lab Samples: 92615985005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 07/27/22 13:01 LABORATORY CONTROL SAMPLE: 3714149 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 192 97 84.6-115 SAMPLE DUPLICATE: 3714151 92616002001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 893 892 0 R6 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 24 ace7malytical 0 www.pacelabs.ccm QUALITY CONTROL DATA Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Parts Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 712146 Analysis Method: SM 9222D-2015 QC Batch Method: SM 922213-2015 Analysis Description: 9222D Fecal Coliform( MF)-EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004 METHOD BLANK: 3713521 Matrix: Water Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/22/22 13:38 METHOD BLANK: 3713523 Matrix: Water Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/22/22 13:38 SAMPLE DUPLICATE: 3713522 92615985001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL 1.0 1.0 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 24 ace;malytical www.pacelabs.com QUALITY CONTROL DATA Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 QC Batch: 712164 Analysis Method: Colilert-18 QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92615985005 SAMPLE DUPLICATE: 3713682 92616005002 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms MPN1100mL ND ND Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 24 5a'ucceArralXicaI www.pacelabscom QUALITY CONTROL DATA Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 712541 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005 METHOD BLANK: 3715185 Matrix: Water Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 1.0 07/26/22 06:07 LABORATORY CONTROL SAMPLE: 3715186 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 50 54.7 109 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3715187 3715188 MS MSD 92614788008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 96.2 50 50 125 120 57 48 90-110 4 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3715189 3715190 MS MSD 92616114001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 18.5 50 50 71.1 71.6 105 106 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 24 /�5a'neAnalXical j www.pecolabs.com QUALITY CONTROL DATA Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 QC Batch: 714350 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005 METHOD BLANK: 3724172 Matrix: Water Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 08/03/22 10:14 LABORATORY CONTROL SAMPLE: 3724173 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 4.9 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3724174 3724175 MS MSD 92616946002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 0.22 5 5 4.9 4.8 93 93 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3724176 3724177 MS MSD 92616947001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 24.9 5 5 29.8 29.3 98 86 90-110 2 M1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 24 aceAnalytical www.pacelabaxcm QUALITY CONTROL DATA Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 713457 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92615985005 METHOD BLANK: 3719673 Matrix: Water Associated Lab Samples: 92615985005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 07/29/22 02:25 LABORATORY CONTROL SAMPLE: 3719674 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.0 90 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3719675 3719676 MS MSD 92616182004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 54.5 10 10 62.5 66.5 80 120 90-110 6 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3719677 3719678 MS MSD 92616182005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 57.9 10 10 68.2 64.0 103 61 90-110 6 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 24 ace Analytical www.pacelaba.ccm QUALITY CONTROL DATA Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 QC Batch: 714046 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92615985005 METHOD BLANK: 3722701 Matrix: Water Associated Lab Samples: 92615985005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.040 08/02/22 10:28 LABORATORY CONTROL SAMPLE: 3722702 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3722703 3722704 MS MSD 92617604027 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 1.2 2.5 2.5 3.6 3.6 97 94 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3722705 3722706 MS MSD 92617604028 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L ND 2.5 2.5 2.3 2.4 94 95 90-110 2 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 24 QD I5acl 1� www.pacelabs.com I QUALITY CONTROL DATA Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 713647 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005 METHOD BLANK: 3720986 Matrix: Water Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 07/29/2219:10 LABORATORY CONTROL SAMPLE: 3720987 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.6 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3720988 3720989 MS MSD 92616629001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 3.3 2.5 2.5 5.8 5.9 103 104 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3720990 3720991 MS MSD 92615985001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.10 2.5 2.5 2.7 2.7 103 105 90-110 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 24 acicemalytical www.pacelaba.eom i QUALITY CONTROL DATA Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 712840 Analysis Method: SM 531OB-2014 QC Batch Method: SM 531OB-2014 Analysis Description: 5310E TOC Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004 METHOD BLANK: 3716800 Matrix: Water Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 07/26/22 12:26 LABORATORY CONTROL SAMPLE: 3716801 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 23.8 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3716802 3716803 MS MSD 92615824001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L ND 25 25 25.5 25.4 99 99 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3716804 3716805 MS MSD 92616363002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L ND 25 25 23.4 23.6 94 94 90-110 1 Results presented an this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 24 aceAnalX cal j www pacelabs.com I QUALIFIERS Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method based on the sample volume used. The true value is likely greater than the value reported. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R6 The RPD between valid sample dilutions exceeded 30%. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 24 aCone AnalX cal www.pacelabs.com t QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Forest Lakes MW/Effluent Pace Project No.: 92615985 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92615985005 Effluent SM 2540C-2015 712602 92615985005 Effluent SM 254OD-2015 712596 92615985001 MW1 EPA 353.2 Rev 2.0 1993 712296 92615985002 MW2 EPA 353.2 Rev 2.0 1993 712296 92615985003 MW3 EPA 353.2 Rev 2.0 1993 712296 92615985004 MW4 EPA 353.2 Rev 2.0 1993 712296 92615985005 Effluent EPA 353.2 Rev 2.0 1993 712296 92615985005 Effluent SM 521OB-2016 712309 SM 521OB-2016 712792 92615985001 MW1 SM 9222D-2015 712146 SM 9222D-2015 712147 92615985002 MW2 SM 9222D-2015 712146 SM 9222D-2015 712147 92615985003 MW3 SM 9222D-2015 712146 SM 9222D-2015 712147 92615985004 MW4 SM 9222D-2015 712146 SM 9222D-2015 712147 92615985005 Effluent Colilert-18 712164 Colilert-18 712166 92615985005 Effluent TKN+NO3+NO2 714526 Calculation 92615985001 MW1 EPA 300.0 Rev 2.1 1993 712541 92615985002 MW2 EPA 300.0 Rev 2.1 1993 712541 92615985003 MW3 EPA 300.0 Rev 2.1 1993 712541 92615985004 MW4 EPA 300.0 Rev 2.1 1993 712541 92615985005 Effluent EPA 300.0 Rev 2.1 1993 712541 92615985001 MW1 EPA 350.1 Rev 2.0 1993 714350 92615985002 MW2 EPA 350.1 Rev 2.0 1993 714350 92615985003 MW3 EPA 350.1 Rev 2.0 1993 714350 92615985004 MW4 EPA 350.1 Rev 2.0 1993 714350 92615985005 Effluent EPA 350.1 Rev 2.0 1993 714350 92615985005 Effluent EPA 351.2 Rev 2.0 1993 713457 EPA 351.2 Rev 2.0 1993 713670 92615985005 Effluent EPA 353.2 Rev 2.0 1993 714046 92615985001 MW1 EPA 365.1 Rev 2.0 1993 713647 EPA 365.1 Rev 2.0 1993 713869 92615985002 MW2 EPA 365.1 Rev 2.0 1993 713647 EPA 365.1 Rev 2.0 1993 713869 92615985003 MW3 EPA 365.1 Rev 2.0 1993 713647 EPA 365.1 Rev 2.0 1993 713869 92615985004 MW4 EPA 365.1 Rev 2.0 1993 713647 EPA 365.1 Rev 2.0 1993 713869 92615985005 Effluent EPA 365.1 Rev 2.0 1993 713647 EPA 365.1 Rev 2.0 1993 713869 92615985001 MW1 SM 531OB-2014 712840 92615985002 MW2 SM 531OB-2014 712840 92615985003 MW3 SM 531OB-2014 712840 92615985004 MW4 SM 531OB-2014 712840 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 24 n z V, Q4 00 I It 8 z T.- -L)o ENO= E E Q Q Q Q c x 2 m .0 10 m z 4.j J= L, Z > M tr C*4 72 :7 , C CL 7 U) =,tt, 0 cu amm� CO L ea on R A 0) 3 do cc cli 00. ri L4 'jai E -14 to Lw 75 LJ '7 Ln u .2 c m M j = 0 - uj ol *r_ =CL m C- o tA 75 SG i 'SS.!. (U S -1 —v '3 fu E 33 E J En co 4-A to to Lin Ln 4) LA Edci m m fu tia tz i7i u u i6 'c 41 Qj CL 0 A a6 X1 i ' spy q, LA QW) cc C(lu tj E aj 'C ILI UJ m 4j m V) IA C. CP LL 0) E lu C�. CL -72 W E E 0 U. C lu u p 23 df2-4 leI DC;# Title: ENV-FRINI-HUlNI-0034 v01_Tech Spec Sample Condition —Face' Upon Receipt .ol"cK oc•�J, I Ellective Dale: ti 9ill •r.,rr 'Check mark top half of k-cx if pH and/or dechlcrina: on is verired and wit, ;in the acceptance range for preservation samples. (� Excep.,ens. G'�M, Cc!i�.r1:1, T%-C' CII a,.,4 Gra3:2 Cn" •art u i..v lh�i_.1 �L`L. �_.�J *"bottom half of box is to list number of hctt;es -**Check all unpres_rved Nitrates for chiorjne I Z < z it v y u r'+ — _ G_ a _ 1. G �• �, �.• a v — �� �' 4, :, � C M G � to N � ` •••• .�, J Q J_ C G J L7 J c C c J c G G J a ` C r IN 1'..1 e4 en !� r � � "T 121 I NI N 1 1N\ I\ 1\1 12-1 Iz I I\I I NI I I 121 12 -IFI N I -1 N N 1\1 J1 I I2I2I�I I\NI I 1\ NINNI y 1 I I I[ \I I \ NIN J\ 1I 1\1 'NI - I I I\III I1\1 11N _31 1\1I I I\NI\NlI NI NNNI .0 1\1 I I NI\I\INI H NINNI F1'- \ I I INIKINNI I 1\1 Project rul L i~ G n pH Adjustment Log for Preserved Samples Sample IC I Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative I adjusted I added Lot 9 N:ta: Wherever ther'_ is a discra;ancy a:;eai, �g Nor ;it Carolina Compliance sariples, a copy of this fcr n wail be sent to the No%h Carolina GEH`i3 Cerif:ca:ion Cfiice (i.e. Gut of hold, incorrect pres2r43tive. out of tamp, inccrrect containers) Qualtrax Document ID: 70677 Page 2 of 2 Page 24 of 24