HomeMy WebLinkAboutWQ0004972_Monitoring - 07-2022_20220901Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * July
Report Information
WQ0004972
Forest Lake Preserve ELS
Type *
NDMR, NDAR-1, NDAR-2, NDMLR
Confirmation Email Address:*
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2022
Upload Document*
Forest Lakes —July 22.pdf 1.97MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Jessica.Mize@pacelabs.com
Jessica Mize
jwd rA lip
Reviewer: Gerald, Wanda
9/1 /2022
This will be filled in automatically
Is the project number correct?* WQ0004972
Is the monitoring report accepted?* Yes No
Regional Office* Winston-Salem
Reviewer: _anonymous
Review Date: 10/4/2022
Page 1 of 2
NON -DISCHARGE WASTE WATER MONITORING REPORT
PERMIT NUMBER: W00004972 MONTH: Julv YEAR: 2022
FACILITY NAME: Forest Lakes Preserve ELS COUNTY: Davie
Flow Monitoring Point: Effluent: lyl Influent:
Parameter Monitoring
Point: Effluent: I Influent: I I S ace Water isW :
SW Code/Name:
Was There
Effluent Flow for this Month Generated
At This Facility: Yes: N
Opemmr
W050
00400
50060
W310
00610
own
31616
0060
00625
own
Now 00620
70300
WS"10
B
A
*
r
AMval
Muse
24M
Cloa
Opendor
Them
Siu
ORC
on
site?
Davy pate
(19.)into
TnNaruent
Sysmn
pH
H.klul
Ouoinr
Boo
26C
NHLN
TSS
Feral
car.
(Gooumir
Mon)
Taal
PMs
Taal
Njddiul
Ni mgM
NO2-NW
Tool Ninale
Nanun NO3.N
Tool
Dixsalvol
Solids
CNadde
HRS
YIN
GPD
UNITS
mgrL
M iL
St
MG,1.
tlOUML
0=
MGL
61G,1.
Mr✓L MGr
h1GL
61GrL
CMINuws
ml y
onl y
m y
mt v
.gyp,
1
0915
0.25
B
12555
6.0
<0.01
2
18,620
71
3
18.620
+
1
1
1
18.620
thnlidav --- -----
5
1605
0.25
B
18,620
1 6.3
<0.01
6
1524
0.25
Y
11.1125
6.1
<0.01
1509
0.25
Y
11.179
6.2
<0.01
S
1059
0.50
Y
121580
6.1
<0.01
0
18,009
10
18,009
D
1600
0.25
B
18,009
6.1
<0.01
12
1600
0.25
B
12,336
6.0
<0.01
13
0700
0.25
Y
IIA53
6.0
<0.01
W.
0740
0.25
Y
IIMIN
6.0
<0.01
is
0716
0.25
Y
12,066
6.1
<0.01
6
15,929
15,929
Is
11719
0.25
Y
15,929
6.1
<0.01
19
11733
0.25
V
11,128
6.0
<0.01
20
6741
0.25
1
12.396
6.0
<0.01
21
0810
1.25
Y
12,144
6.0
<0.01
2.0
88.4
5.3
2420
11.1
104
<0.040
104
<0.040
362
68.2
22
0755
0.25
Y
11.921
6.0
<0.01
23
14,733
24
14,733
25
1520 1
0.25 1
Y
14.733
6.2
<0.01
26
1315
0.25
a
13.693
6.1
<0.01
n
1620
0.25
B -
12,004
6.1
<0.01
28
1420
0.25 1
B
12,219
6.1
<0.01
79
0950
0.25
13
12.088
6.0
<0.01
3o
15,111
15.111
.Avempe
Uaily Maxiummum
14.275
18.620
6.3
70.01
<0.01
-.11
2421)
11.1
0
<0.040
I
< ,
362
681
-.II
5.3
2420
I L I
0'
q).1140
<0.040
62
b8_2
Daily Minim
11,008
6.0
<0.01
2.0
88.4
5.3
2420
11.1
1 104
<0.040
104
<0.040
362
68.2
Monthly Limits Is)
24400
Composite 0 / Grab IG)
*FLOWS ESTIMATED, FLOW METER INOPERABLE MAY 1st - MAY 20th
Operator in Responsible Charge (ORC): Glenn Price Grade: II Phone: 336-996-2841
Check Box if ORC Has Changed: 11 ORC Certification Number: 987931/20771
Certified Laboratories (1): Pace Analytical Serivees (2): .
Person(s) Collecting Samples:
Glenn Price
Mail ORIGINAL and Two COPIES to:
ATTN: Non -Discharge Compliance Unit
X
H�a.�---�
DENR
v
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
Division of Water Quality
By this signature, I certify that this report is accurate and
1617 Dfail Service Center
complete to the bat of my knowledge.
RALEIGH, NC 27699-1617
DENR Form NDAR-1 (5/2003)
NON DISCHARGE WASTEWATER MONITORING REPORT
FACILITY STATUS:
Please answer the following question: Compliant N)
1. Does all monitoring data and sampling frequencies meet permit requirements? L*_j
If the facility is non -compliant , please explain in the space below the reason(s) the facility was not in compliance with its
permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach
additional sheets if necessary.
Flow Estimated, Flow meter inoperable May 1 st - May 20th
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
" 3 1 ` 2 Baron Neal McDuffie
(Signature of Permitee)* Date (Name of Signing Official -Please print or type)
Baron Neal McDuffie (Authorized Agent)
(Permittee-Please print or type)
2N Riverside Plaza , Suite 800
Chicago, Il 60606
(Permittee Address)
01002 Arsenic
01022 Boron
00310 BOD5
01027 Cadmium
00916 Calcium
00940 Chloride
50060 Chlorine, Total
Residual
01034 Chromium
00340 COD
31504
Coliform, Total
00094
Conductivity
01042
Copper
00300
Dissolved Oxygen
31616
Fecal Coliform
01051
Lead
00927
Magnesium
71900
Mercury
00610
NH3 as N
01067
Nickel
Field Services Director (Pace Analytical Services)
(Position or Title)
3/31/21
(Permit Exp. Date)
00600 Nitrogen, Total
00630 NO2 & NO3
00620 NO3
00556 Oil & Grease
W 09 PAN(Plant Available)
00400 pH
32730 Phenols
00665 Phosphorus, Total
00937 Potassium
00545 Settleable Matter
00929 Sodium
00931 SAR
00745 Sulfide
00515 TDS
00010 Temperature
00625 TKN
00680 TOC
00530 TSS/TSR
00076 Turbidity
01092 Zinc
Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529.
The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting
* If signed by other than the Permittee, delegation of signatory authority must be on rile with the state per 15A NCAC 213.0506 (b) (2) (D).
Page 2 of 2
NON -DISCHARGE APPLICATION REPORT
SPRAY IRRIGATION SITE(S)
THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED
PERMIT NUMBER: W0004972 MONTH: Julv YEAR: 2022
FACILITY NAME: Forest Lakes Preserve ELS. COUNTY: Davie
Formulas:
Daily Loading (inches) =(Volume Applied (gallons) x 0.1336(cubic feeVgagen)x12(inchedfoli(Area Sprayed (acres) x 43.560(square feevacre)or
= [Volume Applied (gallons) I (Area Sprayed (acres) x 27,152 (gallonslacre4nch).
Maximum Hourly Loading (inches) =Daily Loading (Inches)/[rime irrigated (minutes) 160(mimunshtur)l Monthly Loading (inches) =Sum of Daily Loading (inches)
12 Month Floating Total (inches) =Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches)
Average Weekly Loading (inches) = [Monthly Loading (incheslmonth) I Number of days in the month (daysrmonth )1 x 7 (daysvoeek)
Did Irrigation Occur At This Facility:
Yes No❑
Did Irrigation Occur On This Feld:
Y No: ❑
Did Irrigation Occur On This Feld:
Ye❑ No:
Field
Number:
Feld Number:
Area Sprayed (aces):
6.0
Area Sprayed (acres):
Cover Crop:
Cover Crop:
ermine au
y to mches :
0.11
Permitted Hourly Rate (inches):
D
A
T
H+
WEATHER
CONDMONS
sioage
1<9ran
Permined Yearly Rate (inches):
46.8
Permitted Yearly Rate (inches):
WmNv
Cade'
TanpMlue
.I
am'iulirn
lomate .
r
v,awnc
Arrr¢1
nee
lin"ol
aib-
tmJmr
M-nwn
nw,
Immna
vmn,k
A,I.W
Ti
_",al
L.'h2c
6hamwn
L"li['
Fe Kure
1"FI
IwMs
cell •n
ixhw
uµLs
rall..n
ind."
aL.�
C
78
0
3.1
3
4
5
C
89
0
2.0
33.984
240
0.21
0.06
6
R
92
0.4
1 3.0
7
Cl
93
0
2.7
R
Cl
83
0
2.4
42,480
300
0.26
0.06
9
11)
u
PC
81
0
23
33984
240
0.21
0.06
12
C
90
0
3.2
u
Cl
74
0
3.0
14
PC
72
0
2.9
33,984
240
0.21
0.06
15
PC
72
0
3.9
16
17
Is
R
72
0.2i
2.8
19
R
74
0.50
16
20
CI
71
0
1.4
21
PC
73
0
2.1
42,481)
300
0.26
0.06
22
PC
70
0
3.1
z3
2
25
Cl
86
0
2.6
26
Cl
89
0
2.2
n
C
92
- 0
2.1
00
0.26
0.06
29
C
93
1)
2.1
42,481)
300
0.26
0.06
z9
C 1
79 1
0
2.9
3e
31
Total Calloml,11i Lmde¢Iii
o Memh Floaloa rout lio[hetl
Avmae%Vmkll' L.aatlbF an[Gnl
i
1.67
=
22.00
0.42
;ak'
0
'we&Ihor C W6: C-cli rC-part, [loud). CHIouOr, Whom 50-foox, sFskel
Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841
ORC Certification Number: 987931/20771 Check Box if ORC Has Changed:
Mail ORIGINAL and Two COPIES to:
ATTN: Non -Discharge Compliance Unit X. ec
DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHAROf
Division of Water Quality By this signature, I certify that this report is accurate and
1617 Mail Service Center complete to the best of my knowledge.
RALEIGH, NC 27699-1617
DENR Form NDAR-1 (5/2003)
NON -DISCHARGE APPLICATION REPORT
SPRAY IRRIGATION SITE(S)
FACILITY STATUS:
Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been comaliant
with the following permit requirements: (Note: If a requirement does not apply to your facility put
(NA) in the
compliant box.)
Compliant (Y,N)
1. The application rate(s) did not exceed the limit(s) specified in the permit.
C�
2. Adequate measures were taken to prevent wastewater runoff from the site(s).
�—
3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit.
C
4. All buffer zones as specified in the permit were maintained during each application.
S. The freeboard in the treatment and/or storage lagoon(s) was not less than the
`--�
limit(s) specified in the permit.
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its
permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach
additional sheets if necessary.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
.11" L—< • 3 t • .2-7' Baron Neal McDuffie
(Signature of Permitee)* Date (Name of Signing Official -Please print or type)
Baron Neal McDuffie (Authorized Agent)
(Permittee-Please print or type)
2N. Riverside Plaza, Suite 800
Chicago,11 60606
(Permittee Address)
Field Services Director (Pace Analytical Services)
(Position or Title)
3/31 /2021
(Permit Exp. Date)
* If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D).
aceAnalXical
anocpacelabs.eom
I
August 03, 2022
Tracy Overdurf
Forest Lake
192 Thousand Trails Dr.
Advance, NC 27006
RE: Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Dear Tracy Overdurf:
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27264
(764)977-0981
Enclosed are the analytical results for sample(s) received by the laboratory on July 21, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Eden
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
stephanie.knoft@pacelabs.com
704-977-0981
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 24
5aceAnalXical
www pacelabasom
{
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, L.L.C. Page 2 of 24
aCLA; lylical `�
j www.pacelaba.ecm
i
SAMPLE ANALYTE COUNT
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Lab ID
Sample ID
Method
Analysts
Analyses
Reported
Laboratory
92615985001
MW1
EPA 353.2 Rev 2.0 1993
SRS
1
PASI-E
SM 9222D-2015
AED
1
PASI-E
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.0 1993
KDF1
1
PASI-A
EPA 365.1 Rev 2.0 1993
SMT
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92615985002
MW2
EPA 353.2 Rev 2.0 1993
SRS
1
PASI-E
SM 9222D-2015
AED
1
PASI-E
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.0 1993
KDF1
1
PASI-A
EPA 365.1 Rev 2.0 1993
SMT
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92615985003
MW3
EPA 353.2 Rev 2.0 1993
SRS
1
PASI-E
SM 9222D-2015
AED
1
PASI-E
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.01993
KDF1
1
PASI-A
EPA 365.1 Rev 2.01993
SMT
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92615985004
MW4
EPA 353.2 Rev 2.0 1993
SRS
1
PASI-E
SM 922213-2015
AED
1
PASI-E
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.0 1993
KDF1
1
PASI-A
EPA 365.1 Rev 2.0 1993
SMT
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92615985005
Effluent
SM 254OC-2015
MWF
1
PASI-E
SM 254OD-2015
LRB
1
PASI-E
EPA 353.2 Rev 2.0 1993
SRS
1
PASI-E
SM 521OB-2016
MWF
1
PASI-E
Colilert-18
SRS
1
PASI-E
TKN+NO3+NO2 Calculation
MDW
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.0 1993
KDF1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
KDF1
1
PASI-A
EPA 365.1 Rev 2.0 1993
SMT
1
PASI-A
PASI-A = Pace Analytical Services -Asheville
PASI-E = Pace Analytical Services - Eden
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 24
aceAnalXical QD
www.pacelabs.com
ANALYTICAL RESULTS
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Sample: MW1
Parameters
Lab ID: 92615985001 Collected: 07/21/22 08:00
Results Units Report Limit DF
Received: 07/21/22 11:00 Matrix: Water
Prepared Analyzed CAS No. Qual
353.2 N021NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
0.35 mg/L 0.040 1
07/22/22 13:18 14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation Method: SM 922213-2015
Pace Analytical Services - Eden
Fecal Coliforms
1.0 CFU/100 mL 1.0 1
07/21/22 15:29 07/22/22 13:38
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
1.1 mg/L 1.0 1
07/26/22 09:36 16887-00-6
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
0.26 mg/L 0.10 1
08/03/22 10:39 7664-41-7
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
0.10 mg1L 0.050 1
07/29/2214:31 07/29/2219:16 7723-14-0
5310B TOC
Analytical Method: SM 531 OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
2.1 mg/L 1.0 1
07/26/22 13:52 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 24
5ac ie A na /j dica I
www.pacelabs.com
ANALYTICAL RESULTS
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville. NC 27284
(704)977-0981
Sample: MW2
Lab ID: 92615985002 Collected: 07/21/22 08:19
Received: 07/21/22 11:00 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed
CAS No. Qual
353.2 N021NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
0.95 mg/L 0.040 1
07/22/22 13:22
14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation Method:
SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
5.0 CFU/100 mL 1.0 1
07/21/22 15:29 07/22/22 13:38
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
6.6 mg/L 1.0 1
07/26/22 09:55
16887-00-6
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10 1
08/03/22 10:41
7664-41-7
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
0.077 mg/L 0.050 1
07/29/2214:31 07/29/2219:18
7723-14-0
5310E TOC
Analytical Method: SM 531 OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0 1
07/26/22 14:10
744044-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 24
acmnalytical
www.pacelaDs.cam
ANALYTICAL RESULTS
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Sample: MW3
Lab lD: 92615985003 Collected: 07/21/22 08:41
Received: 07/21/22 11:00 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed
CAS No. Qual
353.2 N021NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
8.5 mg/L 0.080 2
07/22/22 13:34
14797-55-8
MBIO 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
1.0 CFU/100 mL 1.0 1
07/21/22 15:29 07/22/22 13:38
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
26.0 mg/L 1.0 1
07/26/2210:14
16887-00-6
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10 1
08/03/22 10:42
7664-41-7
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
ND mg/L 0.050 1
07/2912214:31 07/29/2219:19
7723-14-0
5310E TOC
Analytical Method: SM 531 OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0 1
07/26/22 14:27
7440-44-0
REPORT OF LABORATORY ANALYSIS
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Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Sample: MW4 Lab ID: 92615985004 Collected: 07/21/22 09:06 Received: 07/21/22 11:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen. Nitrate
0.058 mg/L 0.040 1
07/22/22 13:24
14797-55-8
M1310 9222D Fecal Coliform EDN
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
2.0 CFU/100 mL 1.0 1
07/21/22 15:29 07/22/22 13:38
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
3.4 mg/L 1.0 1
07/26/2211:11
16887-00-6
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10 1
08/03/22 10:43
7664-41-7
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
ND mg/L 0.050 1
07/29/2214:31 07/29/2219:20
7723-14-0
5310E TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0 1
07/26/22 14:44
7440-44-0
Date: 08/03/2022 04:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 24
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ANALYTICAL RESULTS
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Sample: Effluent
Parameters
Lab ID: 92615985005 Collected: 07/21/22 08:09
Results Units Report Limit DF
Received: 07/21/22 11:00 Matrix: Water
Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
362 mg/L 50.0 1
07/25/22 10:46
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analytical Services - Eden
Total Suspended Solids
5.3 mg/L 2.5 1
07/26/22 08:58
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
ND mg/L 0.040 1
07/22/22 13:21 14797-55-8
5210E BOD, 5 day EDN
Analytical Method: SM 521OB-2016 Preparation Method: SM 521OB-2016
Pace Analytical Services - Eden
BOD, 5 day
2.0 mg/L 2.0 1
07/22/22 12:08 07/27/22 13:47
Colilert-18 Fecal Coliform EDN
Analytical Method: Colilert-18 Preparation Method: Colilert-18
Pace Analytical Services - Eden
Fecal Coliforms
2420 MPN/100mL 1.0 1
07/21/22 15:12 07/22/22 09:15 El
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
Total Nitrogen
104 mg/L 0.040 1
08/02/22 19:06
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Chloride
68.2 mg/L 1.0 1
07/26/2211:30 16887-00-6
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
88A mg/L 5.0 50
08/03/22 11:44 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Kjeldahl, Total
104 mg/L 5.0 10
07/28/22 17:24 07/29/22 03:55 7727-37-9
353.2 Nitrogen, N021NO3 pros.
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, NO2 plus NO3
ND mg/L 0.040 1
08/02/22 10:50
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.01993
Pace Analytical Services -Asheville
Phosphorus
11.1 mg/L 0.25 5
07129/2214:31 07/29/2219:21 7723-14-0
REPORT OF LABORATORY ANALYSIS
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Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 24
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QUALITY CONTROL DATA
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersvitle, NC 27284
(704)977-0981
QC Batch: 712602
Analysis Method: SM 254OC-2015
QC Batch Method: SM 254OC-2015
Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92615985005
METHOD BLANK: 3715393
Matrix: Water
Associated Lab Samples: 92615985005
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Dissolved Solids
mg/L
ND 25.0 07/25/22 10:44
LABORATORY CONTROL SAMPLE: 3715394
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids
mg/L
250 244 98 90-110
SAMPLE DUPLICATE: 3715395
92615481002 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Dissolved Solids
mg/L
93.0 93.0 0
SAMPLE DUPLICATE: 3715396
92616069001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Dissolved Solids
mg/L
1770 1730 2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 712596
Analysis Method: SM 2540D-2015
QC Batch Method: SM 254OD-2015
Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92615985005
METHOD BLANK: 3715363
Matrix: Water
Associated Lab Samples: 92615985005
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 07/26/22 08:55
LABORATORY CONTROL SAMPLE: 3715364
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 242 97 90-110
SAMPLE DUPLICATE: 3715365
92615564001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
65.3 72.9 11
SAMPLE DUPLICATE: 3715854
92616062001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
29.5 29.7 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 24
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QUALITY CONTROL DATA
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 712296
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.01993
Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005
METHOD BLANK: 3714093
Matrix: Water
Associated Lab Samples: 92615985001, 92615985002,
92615985003, 92615985004, 92615985005
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L
ND 0.040 07/22/22 13:15
LABORATORY CONTROL SAMPLE: 3714094
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L
1.5 1.4 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3714095 3714096
MS MSD
92615985001
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L 0.35
1.5 1.5 1.8 1.8 93 94 90-110 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 24
(�5a'ce Analytical
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QUALITY CONTROL DATA
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QC Batch: 712309
Analysis Method:
SM 521OB-2016
QC Batch Method: SM 5210B-2016
Analysis Description:
521013 BOD, 5 day Final EDN
Laboratory:
Pace Analytical Services - Eden
Associated Lab Samples: 92615985005
METHOD BLANK: 3714148
Matrix: Water
Associated Lab Samples: 92615985005
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
BOD, 5 day
mg/L
ND
2.0 07/27/22 13:01
LABORATORY CONTROL SAMPLE: 3714149
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
BOD, 5 day
mg/L
198 192
97 84.6-115
SAMPLE DUPLICATE: 3714151
92616002001 Dup
Parameter
Units
Result Result
RPD Qualifiers
BOD, 5 day
mg/L
893
892 0 R6
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 24
ace7malytical 0
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QUALITY CONTROL DATA
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Parts Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 712146
Analysis Method: SM 9222D-2015
QC Batch Method: SM 922213-2015
Analysis Description: 9222D Fecal Coliform( MF)-EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004
METHOD BLANK: 3713521
Matrix: Water
Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL
ND 1.0 07/22/22 13:38
METHOD BLANK: 3713523
Matrix: Water
Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL
ND 1.0 07/22/22 13:38
SAMPLE DUPLICATE: 3713522
92615985001 Dup
Parameter Units
Result Result RPD Qualifiers
Fecal Coliforms CFU/100 mL
1.0 1.0 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 24
ace;malytical
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QUALITY CONTROL DATA
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
QC Batch: 712164 Analysis Method: Colilert-18
QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92615985005
SAMPLE DUPLICATE: 3713682
92616005002 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms MPN1100mL ND ND
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 24
5a'ucceArralXicaI
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QUALITY CONTROL DATA
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 712541 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005
METHOD BLANK: 3715185 Matrix: Water
Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride mg/L ND 1.0 07/26/22 06:07
LABORATORY CONTROL SAMPLE: 3715186
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chloride mg/L 50 54.7 109 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3715187 3715188
MS MSD
92614788008 Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Chloride mg/L 96.2 50 50 125 120 57 48
90-110 4 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3715189 3715190
MS MSD
92616114001 Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Chloride mg/L 18.5 50 50 71.1 71.6 105 106
90-110 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 24
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QUALITY CONTROL DATA
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville. NC 27284
(704)977-0981
QC Batch: 714350
Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993
Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005
METHOD BLANK: 3724172
Matrix: Water
Associated Lab Samples: 92615985001, 92615985002,
92615985003, 92615985004, 92615985005
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/L
ND 0.10 08/03/22 10:14
LABORATORY CONTROL SAMPLE: 3724173
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/L
5 4.9 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3724174 3724175
MS MSD
92616946002
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Nitrogen, Ammonia mg/L 0.22
5 5 4.9 4.8 93 93
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3724176 3724177
MS MSD
92616947001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Nitrogen, Ammonia mg/L 24.9
5 5 29.8 29.3 98 86
90-110 2 M1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 713457
Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92615985005
METHOD BLANK: 3719673
Matrix: Water
Associated Lab Samples: 92615985005
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/L
ND 0.50
07/29/22 02:25
LABORATORY CONTROL SAMPLE: 3719674
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/L
10 9.0
90 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3719675 3719676
MS MSD
92616182004
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/L 54.5
10 10 62.5
66.5 80 120
90-110 6 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3719677 3719678
MS MSD
92616182005
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/L 57.9
10 10 68.2
64.0 103 61
90-110 6 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
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ace Analytical
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QUALITY CONTROL DATA
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville. NC 27284
(704)977-0981
QC Batch: 714046
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite, preserved
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92615985005
METHOD BLANK: 3722701
Matrix: Water
Associated Lab Samples: 92615985005
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/L
ND 0.040 08/02/22 10:28
LABORATORY CONTROL SAMPLE: 3722702
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L
2.5 2.5 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3722703 3722704
MS MSD
92617604027
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 1.2
2.5 2.5 3.6 3.6 97 94
90-110 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3722705 3722706
MS MSD
92617604028
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L ND
2.5 2.5 2.3 2.4 94 95
90-110 2
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 24
QD
I5acl
1�
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I
QUALITY CONTROL DATA
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 713647
Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005
METHOD BLANK: 3720986
Matrix: Water
Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004, 92615985005
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Phosphorus mg/L
ND 0.050 07/29/2219:10
LABORATORY CONTROL SAMPLE: 3720987
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Phosphorus mg/L
2.5 2.6 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3720988 3720989
MS MSD
92616629001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Phosphorus mg/L 3.3
2.5 2.5 5.8 5.9 103 104
90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3720990 3720991
MS MSD
92615985001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Phosphorus mg/L 0.10
2.5 2.5 2.7 2.7 103 105
90-110 2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 24
acicemalytical
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i
QUALITY CONTROL DATA
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
QC Batch: 712840
Analysis Method: SM 531OB-2014
QC Batch Method: SM 531OB-2014
Analysis Description: 5310E
TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92615985001, 92615985002, 92615985003, 92615985004
METHOD BLANK: 3716800
Matrix: Water
Associated Lab Samples: 92615985001, 92615985002,
92615985003, 92615985004
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
07/26/22 12:26
LABORATORY CONTROL SAMPLE: 3716801
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 23.8
95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3716802 3716803
MS MSD
92615824001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Total Organic Carbon mg/L ND
25 25 25.5
25.4 99 99
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3716804 3716805
MS MSD
92616363002
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Total Organic Carbon mg/L ND
25 25 23.4
23.6 94 94
90-110 1
Results presented an this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 24
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QUALIFIERS
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method
based on the sample volume used. The true value is likely greater than the value reported.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R6 The RPD between valid sample dilutions exceeded 30%.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 24
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Forest Lakes MW/Effluent
Pace Project No.: 92615985
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
(704)977-0981
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92615985005
Effluent
SM 2540C-2015
712602
92615985005
Effluent
SM 254OD-2015
712596
92615985001
MW1
EPA 353.2 Rev 2.0 1993
712296
92615985002
MW2
EPA 353.2 Rev 2.0 1993
712296
92615985003
MW3
EPA 353.2 Rev 2.0 1993
712296
92615985004
MW4
EPA 353.2 Rev 2.0 1993
712296
92615985005
Effluent
EPA 353.2 Rev 2.0 1993
712296
92615985005
Effluent
SM 521OB-2016
712309
SM 521OB-2016
712792
92615985001
MW1
SM 9222D-2015
712146
SM 9222D-2015
712147
92615985002
MW2
SM 9222D-2015
712146
SM 9222D-2015
712147
92615985003
MW3
SM 9222D-2015
712146
SM 9222D-2015
712147
92615985004
MW4
SM 9222D-2015
712146
SM 9222D-2015
712147
92615985005
Effluent
Colilert-18
712164
Colilert-18
712166
92615985005
Effluent
TKN+NO3+NO2
714526
Calculation
92615985001
MW1
EPA 300.0 Rev 2.1 1993
712541
92615985002
MW2
EPA 300.0 Rev 2.1 1993
712541
92615985003
MW3
EPA 300.0 Rev 2.1 1993
712541
92615985004
MW4
EPA 300.0 Rev 2.1 1993
712541
92615985005
Effluent
EPA 300.0 Rev 2.1 1993
712541
92615985001
MW1
EPA 350.1 Rev 2.0 1993
714350
92615985002
MW2
EPA 350.1 Rev 2.0 1993
714350
92615985003
MW3
EPA 350.1 Rev 2.0 1993
714350
92615985004
MW4
EPA 350.1 Rev 2.0 1993
714350
92615985005
Effluent
EPA 350.1 Rev 2.0 1993
714350
92615985005
Effluent
EPA 351.2 Rev 2.0 1993
713457
EPA 351.2 Rev 2.0 1993
713670
92615985005
Effluent
EPA 353.2 Rev 2.0 1993
714046
92615985001
MW1
EPA 365.1 Rev 2.0 1993
713647
EPA 365.1 Rev 2.0 1993
713869
92615985002
MW2
EPA 365.1 Rev 2.0 1993
713647
EPA 365.1 Rev 2.0 1993
713869
92615985003
MW3
EPA 365.1 Rev 2.0 1993
713647
EPA 365.1 Rev 2.0 1993
713869
92615985004
MW4
EPA 365.1 Rev 2.0 1993
713647
EPA 365.1 Rev 2.0 1993
713869
92615985005
Effluent
EPA 365.1 Rev 2.0 1993
713647
EPA 365.1 Rev 2.0 1993
713869
92615985001
MW1
SM 531OB-2014
712840
92615985002
MW2
SM 531OB-2014
712840
92615985003
MW3
SM 531OB-2014
712840
92615985004
MW4
SM 531OB-2014
712840
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2022 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 24
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Sample IC I Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative
I adjusted I added
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N:ta: Wherever ther'_ is a discra;ancy a:;eai, �g Nor ;it Carolina Compliance sariples, a copy of this fcr n wail be sent to the No%h Carolina GEH`i3 Cerif:ca:ion Cfiice (i.e.
Gut of hold, incorrect pres2r43tive. out of tamp, inccrrect containers)
Qualtrax Document ID: 70677 Page 2 of 2
Page 24 of 24