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HomeMy WebLinkAboutWQ0004972_Monitoring - 06-2022_20220901Monitoring Report Submittal Permit Number #* Name of Facility:* Month:* June Report Information WQ0004972 Forest Lake Preserve ELS Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address:* Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2022 Upload Document* Forest Lakes —June 22.pdf 1.65MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Jessica.Mize@pacelabs.com Jessica Mize jwd rA lip Reviewer: Gerald, Wanda 9/1 /2022 This will be filled in automatically Is the project number correct?* WQ0004972 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 10/4/2022 Page 1 of 2 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER:_ W00004972 MONTH: June YEAR: 2022 FACILITY NAME: Forest Lakes Preserve ELS COUNTY: Davie Flow Monitoring Point: Effluent: bd Influent: Parameter Monitoring Point: Effluent Iinfluent S ace Water SW : SW Code/Name: Was There Effluent Flow for this Month Generated At This Facility: N Ves: Dparalor 50050 004E W060 W310 W610 00530 31616 00665 00625 00630 00600 00620 70300 00940 B A '1' L Anal Time 24M cl,,& Operator Time on Sim ORD on Site? Daily Rate (19m)into T.".t S". pH R.M.1 (Tionac a00.5 20T NH-3 N TSS Fecal Colifmm D0 nxoc Mon.) Ta"l Pl- Toul xinAul Nie n NO2+NQ3 Taal N'ieaaea Ni.. NO3-N Tau) Divahr4 Solids alon& Has YIN GPD NITS m,L MGL 11C L NIGL 11111M1. MGL 11GL 61 'L MOL M iL FI IL >IC I. Con . lom7 .I 1, 1iN lunll4Y NIon1111Y \IcnIIJ. 11 fly 1 Y ont Y 1 1240 0.25 B 11,,169 6.1 <0.01 2 1530 0.25 B 12.298 6.6 <0.01 3 1005 0.25 B 11.102 6.4 <0.01 15.113 5 15,113 6 0755 11.25 Y 15,113 6.0 <0.01 7 1530 0.25 B 8,421 6.f: <0.01 a 1220 0.25 V 9,694 5.8 <0.01 9 1055 0.25 V 10,229 5A <0.01 10 1620 0.25 B 10.487 6.2 <11.01 II 14,862 12 14.862 13 1435 0.25 B 14,862 6.0 <0.01 IA 1455 0.25 B 11.127 6.1 <0.01 15 0915 0.25 Y 10368 6.0 QI.01 16 0740 0.50 V 91999 5.8 <0.01 <2.0 98.0 30.0 2420 14.1 114 0.046 114 <0.040 17 0950 0.25 B 9,824 5.8 <0.01 is 14.099 19 14.099 29 1115 0.25 B 14,099 6.1 <0.01 21 1350 0.25 B 10.261 5.9 <0.01 22 0710 0.25 1 10,188 5.9 <0.01 23 0704 0.25 y 10,003 5.8 <0.01 24 0708 0.25 1' 9,966 5.9 <0,01 25 15,334 26 15.334 27 0730 0.511 1' 15334 6.1 <0.01 28 1300 11.51) 1' 10399 6.0 <0.01 29 0950 0.25 Y 12,684 6.0 <11,111 30 1415 0.25 B 13,007 6.2 <0.01 Avenac' Daily ylavimom I2.315 15.334 6.6 <0.01 <0.01 < .11 A 1 . 30A) _I 2420 I4.1 14.1 114 0.046 114.11 114.1) -11.u411 <ILINII <�-0 . 6 Daib'3limmum 8521 5.9 <0.01 <2.0 98.0 30.0 2420 14.1 114 0.046 114.0 <U.U40 Monthly Limits N) 21400 Composite O I Grab (G) *FLOWS ESTIMATED, FLOW METER INOPERABLE MAY 1st - MAY 20th Operator in Responsible Charge (ORC): Glenn Price Grade: 11 Phone: 336-996-2841 Check Box if ORC Has Changed: 11 ORC Certification Number: 987931/20771 Certified Laboratories (1): Pace Analytical Serivices Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Nan -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant 1. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non -compliant , please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Flow Estimated Flow meter inoperable May 1 st - Mav 20th "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permitee)* v Date Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N Riverside Plaza , Suite 800 Chicago,11 60606 (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 31504 Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 3/31/21 (Permit Exp. Date) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease W 09 PAN Plant Available) 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting_ facility's permit for reporting data. * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 2 of 2 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMITNUMBER:_WQ004972 MONTH: June YEAR: 2022 FACILITY NAME: Forest Lakes Preserve ELS. COUNTY: Davie Formulas: Daily Loading (inches) =[Volume Applied (gallons) a 0.1336(cubic (eedgallon)a12(nchevToot)iI[Anne Sprayed (acres) x 43,560(square feeVacre) or = [Volume Applied (gallons) / [Area Sprayed (aces) a 27,152 (gallons/acrainch). Maximum Hourly Loading (inches) =Daily Loading (inches)/time imposed (minutes)/60(minuteslhour)I Monthly Loading (inches) =Sum of Daily Loading (inch") 12 Month Floating Total (inches) = Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = (Monthly Loading (inches/month) / Number of days in the month (days/month )i a r (daysAwl Did Irrigation Occur At This Fell Yes No❑ Did Irrigation Occur On This Feld: Ye No: ❑ Did Irrigation Occur On This Feld: YJ3 No: ❑ Feld Number. Field Number Area Sprayed (acres): 60 Area Sprayed (acres): Lover Crap: Cover Crop: ermm ou y to mches:0.11 Ferramediou y Rate (inches): D ;% 'f WEATHERCONDRIONS sta., "al Permitted Yearly Rate (inches): 46.8 Permitted Yearly Rate (inches): W®Ills eatle' ivnppnara el aralleali.m Preeipile- VAL- Banllaal Lime 4vt'ald nuily LeJiny Maximum Wart, LVNng vnlwne ArTid TLno ImpLW Dail, 4vdini Ma�immn nmrlf Mint, Frudwril I-F1 vCIM9 Ynt "Hill, -hoe l.h. Fallrnaonavallim'M -ho, I C 1 88 0 2.0 42,480 300 0.26 0.06 2 C 90 0 2.6 3 PC 73 0 2.4 42480 300 0.26 0.06 a 6 Cl 71 0 3.0 '/ PC 83 0 3.0 8 PC 82 0 2.6 33.984 240 0.21 0.06 9 PC 83 0 35 in C 82 0 3.3 It 12 13 C 93 0 x.,) 14 C 88 0 2.4 33.984 240 0.21 0.06 Is C 76 0 3.5 16 PC 72 0 3.2 16.992 120 0.10 0.06 tl C 83 0 3.4 B 9 20 C 72 0 2.8 21 C 85 0 2.4 33,994 240 0.21 0.06 22 PC 72 0 3.6 13 PC 76 0 3.4 24 Cl 1 71 0 3.2 ES 26 27 Cl 1 73 0 2.6 2s CI 84 0 2.4 29 PC 89 0 30 C 85 0 2.1 33.984 240 0.21 0.06 31 Tram camWfiewlaly Lwmnaaemm u stone Froo. rum namm Moral wukly lanai.; ouku) , . "- 1.46 "+ Eil 23.74 0.29 `Weather Coda: Cdear, PC -pack chludy, Ch Ir udy, R-raut, Svauon, S"hal Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed: Mail ORIGINAL and Two COPIES to: ATTN: Nan -Discharge Compliance Unit X _ DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the hest of my knowledge. RALEIGH, NC 27699.1617 DENR Form NDAR-1 (5/2003) NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. T Z Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. 5. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is non -compliant , please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permitee)* Date Baron Neal McDuffie (Authorized Aaent) (Permittee-Please print or type) 2N. Riverside Plaza, Suite 800 Chicago, Il 60606 (Permittee Address) Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 3/31 /2021 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). aceAna1XJca1a MWYLDiC818A92a111 i June 28, 2022 Tracy Overdurf Forest Lake 192 Thousand Trails Dr. Advance, NC 27006 RE: Project: Forest Lake Pace Project No.: 92610076 Dear Tracy Overdurf: Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 272a4 (704)977-0981 Enclosed are the analytical results for sample(s) received by the laboratory on June 16, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNUNELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie.knoft@pacelabs.com 704-977-0961 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 15 acAnAnaljd cal www.pacelabs.com 1 i Project: Forest Lake Pace Project No.: 92610076 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 VirginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 IueAnalyical www.pacelabs.com SAMPLE ANALYTE COUNT Project: Forest Lake Pace Project No.: 92610076 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92610076001 Effluent SM 254OD-2015 LRB 1 PASI-E EPA 353.2 Rev 2.0 1993 SRS 2 PASI-E SM 521OB-2016 MWF 1 PASI-E Colilert-18 SRS 1 PASI-E TKN+NO3+NO2 Calculation KDF1 1 PASI-A EPA 350.1 Rev 2.0 1993 NDS 1 PASI-A EPA 351.2 Rev 2.01993 MFO 1 PASI-A EPA 365.1 Rev 2.01993 SMT 1 PASI-A PAS I -A = Pace Analytical Services - Asheville PASI-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 15 acice Ana lQD www.pacelabs.com t ANALYTICAL RESULTS Project: Forest Lake Pace Project No.: 92610076 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: Effluent Parameters Lab ID: 92610076001 Collected: 06/16/22 08:59 Received: 06/16/22 10:10 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services - Eden Total Suspended Solids 30.0 mg/L 10.9 1 06/21/22 09:32 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, NO2 plus NO3 0.046 mg/L 0.040 1 06/16/22 16:23 Nitrogen, Nitrate ND mg/L 0.040 1 06/16/22 16:23 14797-55-8 5210B BOD, 5 day EDN Analytical Method: SM 521OB-2016 Preparation Method: SM 521OB-2016 Pace Analytical Services - Eden BOD, 5 day ND mg/L 2.0 1 06/16/22 17:46 06/21/22 14:35 B2 Colilert-18 Fecal Coliform EDN Analytical Method: Colilert-18 Preparation Method: Colilert-18 Pace Analytical Services - Eden Fecal Coliforms 2420 MPN/100mL 1.0 1 06/16/22 15:52 06/17/22 11:17 El Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 114 mg/L 0.040 1 06/28/2215:51 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 98.0 mg/L 1.0 10 06/24/22 14:04 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 114 mg/L 5.0 10 06/23/22 14:41 06/24/22 06:43 7727-37-9 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 14.1 mg/L 0.50 10 06/27/22 18:56 06/28/22 00:21 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/28/2022 04:00 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 15 ;a'Ucce-aAna1j6ca1 ! www.pacelabs com QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92610076 Pace Analytical Services, LLC 1377 South Park Drive Kernersville. NC 27284 (704)977-0981 QC Batch: 705585 Analysis Method: SM 2544D-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92610076001 METHOD BLANK: 3681503 Matrix: Water Associated Lab Samples: 92610076001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 06/21/22 09:25 LABORATORY CONTROL SAMPLE: 3681504 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 258 103 90-110 SAMPLE DUPLICATE: 3681505 92609890001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 265 287 8 SAMPLE DUPLICATE: 3681506 92610237002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 26.1 27.6 6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/28/2022 04:00 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 15 acice. AnalXical www.pacelabs.ccm 1 QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92610076 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 705044 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92610076001 METHOD BLANK: 3679100 Matrix: Water Associated Lab Samples: 92610076001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.040 06/16/22 16:21 Nitrogen, NO2 plus NO3 mg/L ND 0.040 06/16/22 16:21 LABORATORY CONTROL SAMPLE: 3679101 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.4 94 90-110 Nitrogen, NO2 plus NO3 mg/L 2.5 2.4 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3679102 3679103 MS MSD 92610076001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L ND 1.5 1.5 1.4 1.3 92 89 90-110 3 Nitrogen, NO2 plus NO3 mg/L 0.046 2.5 2.5 2.4 2.4 94 93 90-110 1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/28/2022 04:00 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 15 aceAnalJ6011 www.pacelabs.com i QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92610076 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 QC Batch: 705032 Analysis Method: SM 521OB-2016 QC Batch Method: SM 521OB-2016 Analysis Description: 5210B BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92610076001 METHOD BLANK: 3679019 Matrix: Water Associated Lab Samples: 92610076001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 06/21/22 13:35 LABORATORY CONTROL SAMPLE: 3679020 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 174 88 84.6-115 SAMPLE DUPLICATE: 3679022 92610169002 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 111 115 3 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/28/2022 04:00 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 15 laCcAcemalytical www.patelabi.com QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92610076 QC Batch: 705217 Analysis Method: Colilert-18 QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92610076001 SAMPLE DUPLICATE: 3679827 92610150003 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms MPN/100mL 28.2 25.9 9 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/28/2022 04:00 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 15 aceAnalXical o www.pacelabs.com QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92610076 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 706583 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92610076001 METHOD BLANK: 3686396 Matrix: Water Associated Lab Samples: 92610076001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 06/24/22 11:45 LABORATORY CONTROL SAMPLE: 3686397 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 4.9 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3686398 3686399 MS MSD 92609816001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 1.3 5 5 6.2 6.2 98 97 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3686400 3686401 MS MSD 92610584001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.2 5.2 104 103 90-110 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/28/2022 04:00 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 15 acice; Ma/i4ical www.pacelabs.com QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92610076 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 QC Batch: 706493 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92610076001 METHOD BLANK: 3685636 Matrix: Water Associated Lab Samples: 92610076001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 06/24/22 05:53 LABORATORY CONTROL SAMPLE: 3685637 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.3 93 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3685638 3685639 MS MSD 92610434003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.2 10 10 10.7 9.8 94 86 90-110 8 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3685640 3685641 MS MSD 92610434004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.1 10 10 11.2 10.4 102 93 90-110 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/28/2022 04:00 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 15 5acicc;Analyticalo www.pacelabs.com I QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92610076 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 707206 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92610076001 METHOD BLANK: 3689057 Matrix: Water Associated Lab Samples: 92610076001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 06/27/22 23:57 LABORATORY CONTROL SAMPLE: 3689058 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3689059 3689060 MS MSD 92610076001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 14.1 2.5 2.5 16.6 16.6 102 98 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3689061 3689062 MS MSD 92610088001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 1.9 2.5 2.5 4.4 4.4 99 100 90-110 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/28/2022 04:00 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 15 1�5a'neAnalytical" www.pacelabsxom J I QUALIFIERS Project: Forest Lake Pace Project No.: 92610076 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated for the dilution using the most amount of sample. El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method based on the sample volume used. The true value is likely greater than the value reported. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/28/2022 04:00 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 15 aceAnalytical o www.pacelaba.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Forest Lake Pace Project No.: 92610076 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92610076001 Effluent SM 254OD-2015 705585 92610076001 Effluent EPA 353.2 Rev 2.0 1993 705044 92610076001 Effluent SM 521OB-2016 705032 SM 521 OB-2016 705161 92610076001 Effluent Colilert-18 705217 Colilert-18 705218 92610076001 Effluent TKN+NO3+NO2 707461 Calculation 92610076001 Effluent EPA 350.1 Rev 2.0 1993 706583 92610076001 Effluent EPA 351.2 Rev 2.0 1993 706493 EPA 351.2 Rev 2.0 1993 706695 92610076001 Effluent EPA 365.1 Rev 2.0 1993 707206 EPA 365.1 Rev 2.0 1993 707260 Date: 06/28/2022 04:00 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 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