NC0027006_Renewal (Application)_20221003

STATE
ROY COOPER
Governor
ELIZABETH S.BISER
Secretary
RICHARD E.ROGERS,JR. NORTH CAROLINA
Director Environmental Quality
October 03, 2022
MPLX Terminals, LLC
Attn: Angela Brown, VP
539 S Main St
Findlay, OH 45840-3229
Subject: Permit Renewal
Application No. NC0027006
Selma Terminal
Johnston County
Dear Applicant:
The Water Quality Permitting Section acknowledges the October 3, 2022, receipt of your permit renewal application and
supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW permitting
branch. Per G.S. 150E-3 your current permit does not expire until permit decision on the application is made.
Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The
permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a
timely manner to requests for additional information necessary to allow a complete review of the application and renewal
of the permit.
Information regarding the status of your renewal application can be found online using the Department of Environmental
Quality's Environmental Application Tracker at:
https://deq.nc.gov/permits-regulations/permit-guidance/environmental-application-tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
Sincerel
Xitiin 4 43
Wren Thedford
Administrative Assistant
Water Quality Permitting Section
cc: Robert Jarabeck
ec: WQPS Laserfiche File w/application
E Q� No th Ca o4na Department of EnvUonental Qua 1 Division of Water Resources
0.akigh Regional Office 3800 Barrett mDrtve Rallityeigh North Carotlna 27609
9t9.791.4200

MPLx
MPLX Terminals LLC
539 South Main Street
Findlay,OH 45840
RECEIVED
September 30, 2022 OCT a 3 2022
NCDEQIDWR/NPDES Sent Via Overnight Mail
NC DENR
Division of Water Resources—NPDES Unit
1617 Mail Services Center
Raleigh,NC 27699-1617
RE: MPLX Terminals LLC—Selma West Oak Terminal
NC0027006 Permit Renewal Application
2555 West Oak Street
Selma, North Carolina 27576
MPLX Terminals LLC (MPLXT) owns and operates the Petroleum Bulk Storage and
Distribution Terminal located at the above referenced location. The facility is currently covered
under NPDES Permit NC0027006. The permit is set to expire March 31, 2023. MPLXT is
requesting that the permit be renewed. Included in this renewal is the following:
• EPA Application Form 1
o Attachment A
• Topological Map showing location of Terminal and Outfall 002
• EPA Application Form 2C
o Attachments
• Section 2.1 —Line Drawing
• Attachment A—Request for Waiver—Table A Pollutants
• Attachment B —Analytical Results—Table A, B, C, and D Applicable
Pollutants and Whole Effluent Testing (WET) Analysis
If you have any questions or require additional information, I can be reach by phone at 440-465-
2365 or via email at [e-mail].
Sincerely,
bU(4— YO-iratactc_
I cm
Robert Jarabeck
Senior Environmental Professional

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000825505 NC00270006 MPLX Terminals LLC-Selma West OMB No.2040-0004
Form U.S.Environmental Protection Agency
1 : EPA Application for NPDES Permit to Discharge Wastewater
NPDES GENERAL INFORMATION
SECTION 1.ACTIVITIES REQUIRING AN NPDES PERMIT(40 CFR 122.21(f)and(f)(1))
1.1 Applicants Not Required to Submit Form 1
Is the facility a new or existing publicly owned Is the facility a new or existing treatment works
1.1.1 12
treatment works? 1. . treating domestic sewage?
If yes,STOP.Do NOT complete E No If yes,STOP.Do NOT No
Form 1.Complete Form 2A. complete Form 1.Complete
Form 2S.
1.2 Applicants Required to Submit Form 1
1.2.1 Is the facility a concentrated animal feeding 1.2.2 Is the facility an existing manufacturing,
operation or a concentrated aquatic animal commercial,mining,or silvicultural facility that is
CD
n- production facility? currently discharging process wastewater?
o ❑ Yes 4 Complete Form 1 2 No © Yes 4 Complete Form No
a and Form 2B. 1 and Form 2C.
1.2.3 Is the facility a new manufacturing,commercial, 1.2.4 Is the facility a new or existing manufacturing,
rn mining,or silvicultural facility that has not yet commercial,mining,or silvicultural facility that
commenced to discharge? discharges only nonprocess wastewater?
Yes 4 Complete Form 1 El No ❑ Yes 4 Complete Form 2 No
co
and Form 2D. 1 and Form 2E.
1.2.5 Is the facility a new or existing facility whose
discharge is composed entirely of stormwater
associated with industrial activity or whose
discharge is composed of both stormwater and
non-stormwater?
❑ Yes 4 Complete Form 1 No
and Form 2F
unless exempted by
40 CFR
122.26(b)(14)(x)or
b 15 .
SECTION 2.NAME, MAILING ADDRESS,AND LOCATION (40 CFR 122.21(f)(2))
2.1 Facility Name
MPLX Terminals LLC-Selma West Oak Street Terminal
2.2 EPA Identification Number
o NCD000825505
J
2.3 Facility Contact
d Name(first and last) Title Phone number
v Robert Jarabeck Sr.Env Engineer [phone]
Email address
[e-mail]
2
2.4 Facility Mailing Address
£ Street or P.O.box
2555 West Oak Street
City or town State ZIP code
Selma NC 27576
EPA Form 3510-1(revised 3-19) Page 1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000825505 NC00270006 MPLX Terminals LLC-Selma West OMB No.2040-0004
y g 2.5 Facility Location
. Street,route number,or other specific identifier
Q o 2555 West Oak Street
a o County name County code(if known)
u Johnston
d -0
E a City or town State ZIP code
z Selma NC 27576
SECTION 3.SIC AND NAICS CODES(40 CFR 122.21(f)(3))
3.1 SIC Code(s) Description(optional)
5171 Petroleum Bulk Stations and Terminals
fa
N
a
0
U
3.2 NAICS Code(s) Description(optional)
a
424710 Petroleum Bulk Stations and Terminals
co
SECTION 4.OPERATOR INFORMATION(40 CFR 122.21(f)(4))
4.1 Name of Operator
MPLX Terminals LLC
0 4.2 Is the name you listed in Item 4.1 also the owner?
o ✓❑ Yes El No
__
4.3 Operator Status
❑ Public—federal ❑ Public—state ❑ Other public(specify)
0 Private ❑ Other(specify)
4.4 Phone Number of Operator
[phone]
4.5 Operator Address
r Street or P.O.Box
539 South Main Street
o 2
City or town State ZIP code
$ V Findlay OH 45840
m
Email address of operator
0
SECTION 5.INDIAN LAND(40 CFR 122.21(f)(5))
0 0 5.1 Is the facility located on Indian Land?
12 J ❑Yes ❑✓ No
EPA Form 3510-1(revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000825505 NC00270006 MPLX Terminals LLC-Selma West OMB No.2040-0004
SECTION 6,EXISTING ENVIRONMENTAL PERMITS(40 CFR 122.21(f)(6))
6.1 Existing Environmental Permits(check all that apply and print or type the corresponding permit number for each)
❑✓ NPDES(discharges to surface © RCRA(hazardous wastes) ❑ UIC(underground injection of
c water) fluids)
y
o u) NC0027006 SQG NCD000825505
� E
a ❑ PSD(air emissions) ❑ Nonattainment program(CM) ❑✓ NESHAPs(CM)
= 09330R21
w ❑ Ocean dumping(MPRSA) ❑ Dredge or fill(CWA Section 404) ❑ Other(specify)
SECTION 7.MAP(40 CFR 122.21(f)(7))
7.1 Have you attached a topographic map containing all required information to this application?(See instructions for
specific requirements.)
❑Yes ❑ No ❑CAFO—Not Applicable(See requirements in Form 2B.)
SECTION 8. NATURE OF BUSINESS(40 CFR 122.21(f)(8))
8.1 Describe the nature of your business.
Bulk Petroleum Storage Facility.Petroleum fuels are received via pipeline,stored,and blended to specification at
co tanker truck loading rack for wholesale.
y I
C)
N
m
Q
C)
tC
SECTION 9,COOLING WATER INTAKE STRUCTURES(40 CFR 122.21(f)(9))
9.1 Does your facility use cooling water?
❑ Yes ❑ No 4 SKIP to Item 10.1.
9.2 Identify the source of cooling water.(Note that facilities that use a cooling water intake structure as described at
40 CFR 125,Subparts I and J may have additional application requirements at 40 CFR 122.21(r).Consult with your
a NPDES permitting authority to determine what specific information needs to be submitted and when.)
SECTION 10.VARIANCE REQUESTS(40 CFR 122.21(f)(10))
10.1 Do you intend to request or renew one or more of the variances authorized at 40 CFR 122.21(m)?(Check all that
apply.Consult with your NPDES permitting authority to determine what information needs to be submitted and
when.)
❑ Fundamentally different factors(CWA ❑ Water quality related effluent limitations(CWA Section
cc Section 301(n)) 302(b)(2))
❑ Non-conventional pollutants(CWA ❑ Thermal discharges(CWA Section 316(a))
Section 301(c)and(g))
ElNot applicable
EPA Form 3510-1(revised 3-19) Page 3

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000825505 NC00270006 MPLX Terminals LLC-Selma West OMB No.2040-0004
SECTION 11.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d))
11.1 In Column 1 below,mark the sections of Form 1 that you have completed and are submitting with your application.
For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority. Note
that not all applicants are required to provide attachments.
Column 1 Column 2
❑✓ Section 1:Activities Requiring an NPDES Permit ❑ w/attachments
❑✓ Section 2: Name, Mailing Address,and Location ❑ w/attachments
© Section 3: SIC Codes ❑ w/attachments
❑✓ Section 4: Operator Information ❑ w/attachments
❑✓ Section 5: Indian Land ❑ w/attachments
❑✓ Section 6: Existing Environmental Permits ❑ w/attachments
w/topographic
Section 7: Map ❑✓ map ❑❑✓ w/additional attachments
cn
o ❑✓ Section 8:Nature of Business ❑ w/attachments
❑✓ Section 9:Cooling Water Intake Structures ❑ w/attachments
-a
❑✓ Section 10:Variance Requests ❑ w/attachments
❑✓ Section 11:Checklist and Certification Statement ❑ wl attachments
Y
d 11.2 Certification Statement
U
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system,or those persons
directly responsible for gathering the information, the information submitted is,to the best of my knowledge and
belief,true,accurate,and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fine and imprisonment for knowing violations.
Name(print or type first and last name) Official title
Angela Brown Vice President,MPLX Terminals LLC
Signature Date signed
)(/&lad-4j (AAJV‘ —QC1".
EPA Form 3510-1(revised 3-19) Page 4

Attachment A: Topological Map

,' ( >i \ ,,,` _ice 1 o— ��
��is ! I ,. \ 3- �`'i -- (,,
t .
tom/
9 is x.. P. 1111.„. - • ' y_\ 1^.~--1 ''tr?r. ems.. �a-., i—_
`S • i
�. .tip JL^"� _ -r.._• - • --'-` */ , , �\` .,- f -- . '''' � �
1 J. ''''lk _ Pits r i 1, r p
li t i '7 ��i •
, , ;/' ;sopj,„,
/ Sand and Gravel i • •
^" \) its
�.. •
-',=-- •. � Approximate Facility Boundary
'' i
r, - ,. \ •f f fP4.0Jping love , /_.
YnM e •
i
� �' \ �' ins . l'a -•�
`` .
r ,. Mill Creek �. ' f, t ; n,
r
--. • ._k ,-.. .....\ .:‘ : .4 -
_ f (ft«-,r •.�tst) ' Outfa11001 �.
\., ((flows south)
C re.twv�6 •. .. . -
_---uto t `� tat:35°33'02" N ._
f t,�C_ �` Long:78°18'44" W /
It„
-,/,.
4\''\ .I
i \ I,...'',\'/ ,k.
_ I.%.w Sewage—_,i _
West Noble Street f :0
Buffalo Road
%/111‘1 ..'''•• ''''..11j*IP1411:11,'
\)I • �: •NYiIV••
/I i' .J / a 10•i•^
/ 1 < - --
i2 , 7 . 7
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..., fr..
�.`",�.. • asp A ,, •
, dig .
1
�-, ? • II Memorial rr .
tiC. /fit} - I <‘.._ 'e• 4101:04 .�QP
MPLX Terminals LLC Facility
Selma Terminal Location
USGS Quad: Selma.NC Sub-Basin: 03-04-02 not to scale
Permitted Flow: Episodic--not limited Stream Class: WS-IV;NSW
Receiving Stream: UT of Mill Creek Stream Segment: 27-40 NPDES Permit NC0027006
Drainage Basin: Neuse River Basin WIC: 03020201 North
Johnston County

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West OMB No.2040-0004
Form U.S.Environmental Protection Agency
2C .SEPA Application for NPDES Permit to Discharge Wastewater
NPDES EXISTING MANUFACTURING,COMMERCIAL,MINING,AND SILVICULTURE OPERATIONS
SECTION 1.OUTFALL LOCATION(40 CFR 122.21(g)(1))
1.1 Provide information on each of the facility's outfalls in the table below.
o Numbelr Receiving Water Name Latitude Longitude
ii —
U
.J 001 Unnamed Tributary of 35° 33' 02" N 78° 18' 44" W
is
3 Mill Creek " "
3
0
SECTION 2.LINE DRAWING(40 CFR 122.21(g)(2))
a, 2.1 Have you attached a line drawing to this application that shows the water flow through your facility with a water
c 3 balance?(See instructions for drawing requirements.See Exhibit 2G-1 at end of instructions for example.)
J tE6
o ❑✓ Yes ❑ No
SECT1011 3.AVERAGE FLOWS AND TREATMENT(40 CFR 122.21(g)(3))
3.1 For each outfall identified under Item 1.1,provide average flow and treatment information.Add additional sheets if
necessary.
**Outfall Number** 001
Operations Contributing to Flow
Operation Average Flow
process waters(spills cleaned up prior to discharge) N/A mgd
c
E storm water*precipitation dependent(avg past 12 months) (0.123)* mgd 1
m
m
i— hydrostatic test waters**(project dependent if required) **N/A mgd
c
H mgd
3
Treatment Units
O Description Code from Final Disposal of Solid or
(includesize, throughtreatment
d flow rate each treamen unit, Table 2C-1 Liquid Wastes Other Than
> retention time,etc.) by Discharge
load rack OWS(10,000 gal)* no option reclamation/recycle
tank field OWS(10,000 gal)* no option reclamation/recycle
*flow rate/retention time not known,no documentation ave
EPA Form 3510-2C(Revised 3-19) Page 1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West OMB No.2040-0004
3.1 "Outfall Number**
cont. Operations Contributing to Flow
Operation Average Flow
mgd
mgd
mgd
mgd
Treatment Units
Description Code from Final Disposal of Solid or
(include size,flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
retention time,etc.) by Discharge
-o
d
0
U
w
E
io
F--
"Outfall Number**
Operations Contributing to Flow
o Operation Average Flow
ri
a, mgd
tv
> mgd
mgd
mgd
Treatment Units
Description Code from Final Disposal of Solid or
(include size,flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
retention time,etc.) by Discharge
3.2 Are you applying for an NPDES permit to operate a privately owned treatment works?
d ❑ Yes ❑✓ No 4 SKIP to Section 4.
n 3.3 Have you attached a list that identifies each user of the treatment works?
❑ Yes ❑ No
EPA Form 3510-2C(Revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West OMB No.2040-0004
SECTION 4.INTERMITTENT FLOWS(40 CFR 122.21(g)(4))
4.1 Except for storm runoff,leaks,or spills,are any discharges described in Sections 1 and 3 intermittent or seasonal?
❑� Yes ❑ No 4 SKIP to Section 5.
4.2 Provide information on intermittent or seasonal flows for each applicable outfall.Attach additional pages,if necessary.
Outfall Operation Frequency Flow Rate
Number (list) Average Average Long-Term Maximum Duration
Days/Week Months/Year Average Daily
Hydro-test waters * days/week * months/year mgd * mgd * days
001 (project dependent)* days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
a.�
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
SECTION 5. PRODUCTION(40 CFR 122.21(g)(5))
5.1 Do any effluent limitation guidelines(ELGs)promulgated by EPA under Section 304 of the CWA apply to your facility?
❑ Yes ❑✓ No 4 SKIP to Section 6.
u) 5.2 Provide the following information on applicable ELGs.
w ELG Category ELG Subcategory Regulatory Citation
a)
co
.Q
0-
a
5.3 Are any of the applicable ELGs expressed in terms of production(or other measure of operation)?
❑ Yes ❑ No 4 SKIP to Section 6.
0
;g 5.4 Provide an actual measure of daily production expressed in terms and units of applicable ELGs.
Outfall Operation,Product,or Material Quantity per Day Unit of
-0 Number Measure
0
CO
O
d
EPA Form 3510-2C(Revised 3-19) Page 3

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West OMB No.2040-0004
SECTION 6. IMPROVEMENTS(40 CFR 122.21(g)(6))
6.1 Are you presently required by any federal,state,or local authority to meet an implementation schedule for constructing,
upgrading,or operating wastewater treatment equipment or practices or any other environmental programs that could
affect the discharges described in this application?
❑ Yes ❑✓ No 4 SKIP to Item 6.3.
6.2 Briefly identify each applicable project in the table below.
Affected Final Compliance Dates
Brief Identification and Description of Outfalls Source(s)of
cu
Project (list outfall Discharge Required Projected
a. number)
E
� I
w
L i
a)
a.
6.3 Have you attached sheets describing any additional water pollution control programs(or other environmental projects
that may affect your discharges)that you now have underway or planned?(optional item)
❑ Yes ❑ No ✓❑ Not applicable
SECTION 7.EFFLUENT AND INTAKE CHARACTERISTICS(40 CFR 122.21(g)(7))
See the instructions to determine the pollutants and parameters you are required to monitor and,in turn,the tables you must
complete. Not all applicants need to complete each table.
Table A.Conventional and Non-Conventional Pollutants
7.1 Are you requesting a waiver from your NPDES permitting authority for one or more of the Table A pollutants for any of
your outfalls?
❑✓ Yes ❑ No 4 SKIP to Item 7.3.
7.2 If yes,indicate the applicable outfalls below.Attach waiver request and other required information to the application.
Outfall Number 001 Outfall Number Outfall Number
u 7.3 Have you completed monitoring for all Table A pollutants at each of your outfalls for which a waiver has not been
requested and attached the results to this application package?
No;a waiver has been requested from my NPDES
✓❑ Yes ❑ permitting authority for all pollutants at all outfalls.
Table B.Toxic Metals,Cyanide,Total Phenols,and Organic Toxic Pollutants
Y 7.4 Do any of the facility's processes that contribute wastewater fall into one or more of the primary industry categories
listed in Exhibit 2C-3?(See end of instructions for exhibit.)
❑ Yes ✓❑ No 4 SKIP to Item 7.8.
• 7.5 Have you checked"Testing Required"for all toxic metals,cyanide,and total phenols in Section 1 of Table B?
w ❑ Yes ❑ No
7.6 List the applicable primary industry categories and check the boxes indicating the required GC/MS fraction(s)identified
in Exhibit 2C-3.
Primary Industry Category Required GC/MS Fraction(s)
(Check applicable boxes.)
❑Volatile 0 Acid 0 Base/Neutral ❑Pesticide
0 Volatile 0 Acid ❑Base/Neutral 0 Pesticide
❑Volatile 0 Acid ❑ Base/Neutral 0 Pesticide
EPA Form 3510-2C(Revised 3-19) Page 4

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West OMB No.2040-0004
7.7 Have you checked"Testing Required"for all required pollutants in Sections 2 through 5 of Table B for each of the
GC/MS fractions checked in Item 7.6?
❑ Yes ❑ No
7.8 Have you checked"Believed Present"or"Believed Absent"for all pollutants listed in Sections 1 through 5 of Table B
where testing is not required?
❑✓ Yes ❑ No
7.9 Have you provided(1)quantitative data for those Section 1,Table B,pollutants for which you have indicated testing is
required or(2)quantitative data or other required information for those Section 1,Table B,pollutants that you have
indicated are"Believed Present"in your discharge?
✓❑ Yes ❑ No
7.10 Does the applicant qualify for a small business exemption under the criteria specified in the instructions?
❑ Yes 4 Note that you qualify at the top of Table B, 0 No
a th
en SKIP to Item 7.12.
7.11 Have you provided(1)quantitative data for those Sections 2 through 5,Table B,pollutants for which you have
o determined testing is required or(2)quantitative data or an explanation for those Sections 2 through 5,Table B,
pollutants you have indicated are"Believed Present"in your discharge?
❑✓ Yes ❑ No
Table C.Certain Conventional and Non-Conventional Pollutants
Es 7.12 Have you indicated whether pollutants are"Believed Present"or"Believed Absent"for all pollutants listed on Table C
crs
for all outfalls?
❑✓ Yes ❑ No
c 7.13 Have you completed Table C by providing(1)quantitative data for those pollutants that are limited either directly or
indirectly in an ELG and/or(2)quantitative data or an explanation for those pollutants for which you have indicated
"Believed Present"?
❑✓ Yes ❑ No
w Table D.Certain Hazardous Substances and Asbestos
7.14 Have you indicated whether pollutants are`Believed Present"or`Believed Absent"for all pollutants listed in Table D for
all outfalls?
✓❑ Yes ❑ No _
7.15 Have you completed Table D by(1)describing the reasons the applicable pollutants are expected to be discharged
and(2)by providing quantitative data,if available?
❑✓ Yes ❑ No
Table E.2,3,7,8-Tetrachlorodibenzo-p-Dioxin(2,3,7,8-TCDD)
7.16 Does the facility use or manufacture one or more of the 2,3,7,8-TCDD congeners listed in the instructions,or do you
know or have reason to believe that TCDD is or may be present in the effluent?
❑ Yes 4 Complete Table E. ❑✓ No 4 SKIP to Section 8.
7.17 Haveyou completed Table E byreporting qualitative data for TCDD?
P P 9
❑ Yes ❑ No
SECTION 8.USED OR MANUFACTURED TOXICS(40 CFR 122.21(g)(9))
8.1 Is any pollutant listed in Table B a substance or a component of a substance used or manufactured at your facility as
an intermediate or final product or byproduct?
❑ Yes ❑� No 4 SKIP to Section 9.
mg 0 8.2 List the pollutants below.
ro 1. 4. 7.
0
2. 5. 8.
3. 6. 9.
EPA Form 3510-2C(Revised 3-19) Page 5

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West OMB No.2040 0004
SECTION 9.BIOLOGICAL TOXICITY TESTS(40 CFR 122.21(g)(11))
9.1 Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made
within the last three years on(1)any of your discharges or(2)on a receiving water in relation to your discharge?
❑✓ Yes ❑ No 4 SKIP to Section 10.
" 9.2 Identify the tests and their ourposes below.
Submitted to NPDES
. Test(s) Purpose of Test(s) Date Submitted
Permitting Authority?
0
I-
To WET-Whole Effluent Permit Requirement ✓❑ Yes El No 09/28/2022
Testing
0
m ❑ Yes ❑ No
❑ Yes ❑ No
SECTION 10.CONTRACT ANALYSES(40 CFR 122.21(g)(12))
10.1 Were any of the analyses reported in Section 7 performed by a contract laboratory or consulting firm?
❑✓ Yes ❑ No 4 SKIP to Section 11.
10.2 Provide information for each contract laboratory or consulting firm below.
Laboratory Number 1 Laboratory Number 2 Laboratory Number 3
Name of laboratory/firm PACE Analytical Services,LLC ETT Environmental Inc
Laboratory address
co
Huntersville,NC 28708 Greer,SC
29650
R
Phone number
04 •0•
Pollutant(s)analyzed
all but WET Toxicity WET Toxicity
SECTION 11.ADDITIONAL INFORMATION(40 CFR 122.21(g)(13))
11.1 Has the NPDES permitting authority requested additional information?
❑ Yes ❑✓ No 4 SKIP to Section 12.
O
E 11.2 List the information requested and attach it to this application.
0
1. 4.
0
2. 5.
3. 6.
EPA Form 3510-2C(Revised 3-19) Page 6

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West OMB No.2040-0004
SECTION 12.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d))
12.1 In Column 1 below,mark the sections of Form 2C that you have completed and are submitting with your application.
For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority.Note
that not all applicants are required to complete all sections or provide attachments.
Column 1 Column 2
❑� Section 1:Outfall Location ❑ w/attachments
❑✓ Section 2:Line Drawing ❑✓ w/line drawing ❑ w/additional attachments
im Section 3:Average Flows and wl list of each user of
ElTreatment wl attachments 0 privately owned treatment
works
❑� Section 4:Intermittent Flows ❑ w/attachments
❑✓ Section 5:Production ❑ w/attachments
w/optional additional
0Section 6:Improvements Elw/attachments ❑ sheets describing any
additional pollution control
plans
❑ w/request for a waiver and ❑ wl explanation for identical
supporting information outfalls
w/small business exemption w/other attachments
d 0 requestco 0
❑ Section 7: Effluent and Intake El Table A ❑✓ w/Table B
Characteristics
0
u ❑✓ w/Table C w/Table D
❑� wl Table E ❑ wl analytical results as an
attachment
Section 8:Used or Manufactured
❑✓ Toxics ❑ w/attachments
❑ Section 9: Biological Toxicity ❑ w/attachments
Tests
U
❑✓ Section 10:Contract Analyses ❑ w/attachments
❑✓ Section 11:Additional Information ❑ w/attachments
Section 12:Checklist and
❑ Certification Statement ❑� wl attachments
12.2 Certification Statement
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted.Based on my inquiry of the person or persons who manage the system,or those persons directly
responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the
possibility of fine and imprisonment for knowing violations.
Name(print or type first and last name) Official title
Angela Brown Vice President,MPLX Terminals LLC
Signatur Date signed
CA_gC1-�-
EPA Form 3510-2C(Revised 3-19) Page 7

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma Well001 OMB No.2040-0004
TABLE A.CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(iii))1
Effluent Intake
Waiver (Optional)
Pollutant Requested Units Maximum Maximum Long-Term
(specify) Daily Monthly Average Daily Number of Long-Term Number of
(if applicable) Discharge Discharge Discharge Analyses Average Value Analyses
(required) (if available) (if available)
❑ Check here if you have applied to your NPDES permitting authority for a waiver for all of the pollutants listed on this table for the noted outfall.
Biochemical oxygen demand Concentration
1' El(BOD5) Mass
2 Chemical oxygen demand ElConcentration
(COD) Mass
Concentration
3. Total organic carbon(TOC) ✓❑
Mass
Concentration
4. Total suspended solids(TSS) ❑
Mass 45.0 mg/I 5.0 mg/I N/A
Concentration
5. Ammonia(as N) ❑✓
Mass
6. Flow ❑ Rate N/A N/A N/A
Temperature(winter) ❑✓ °C °C
7.
Temperature(summer) ✓❑ °C °C
pH(minimum) ❑✓ Standard units s.u.
8.
pH(maximum) ❑✓ Standard units s.u.
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 9

1
This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term _
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long Number
Present Absent Daily Monthly Daily of Term of
D(reghreargd a (ifavailabl) Di Averageischarge
scharge Analyses Value Analyses
(if available)
❑ Check here if you qualify as a small business per the instructions to Form 2C and,therefore,do not need to submit quantitative data for any of the organic toxic pollutants in Sections
2 through 5 of this table. Note,however,that you must still indicate in the appropriate column of this table if you believe any of the pollutants listed are present in your discharge.
Section 1.Toxic Metals,Cyanide,and Total Phenols
Antimony,total Concentration
1.1 (7440-36-0) ❑ ❑ ❑ Mass
Arsenic,total Concentration
1.2 (7440-38-2) 0 0 Mass
Beryllium,total Concentration
1.3 (7440-41-7) Mass
Cadmium,total Concentration
1.4 (7440-43-9) 0 0 ❑ Mass
1.5 Chromium,total 0
0
❑ Concentration
(7440-47-3) Mass
Copper,total Concentration
1.6 (7440-50-8) ❑ El El
Mass
Lead,total Concentration
1.7 (7439-92-1) 0 El ❑ Mass
Mercury,total Concentration
1.8 (7439-97-6) ❑ ❑ El
Mass
1.9 Nickel,total 0
0
0
Concentration
(7440-02-0) Mass
Selenium,total Concentration
1.10 (7782-49-2) 0 0 0Mass
Silver,total Concentration
1.11 (7440-22-4) 0 0 0 Mass
EPA Form 3510-2C(Revised 3-19) Page 11

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))l
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
Dischargeaily of of
Discharge) DisDcharge Analyses AverageValue Analyses
(required) (if available (if available)
Thallium,total Concentration
1.12 (7440-28-0) CI CI 0 Mass
1.13 Zinc,total ❑ ❑ Concentration
(7440-66-6) Mass
1.14 Cyanide,total ❑ ❑ ❑ Concentration
(57-12-5) Mass
Concentration mg/I N/A ND<0.020 N/A 4/yr
1.15 Phenols,total 0 0 ❑
Mass
Section 2.Organic Toxic Pollutants(GC/MS Fraction—Volatile Compounds)
Acrolein Concentration
2.1 (107-02-8) ❑ ❑ ElMass
2.2 Acrylonitrile ❑ ❑ Concentration
(107-13-1) Mass
Benzene ❑ ❑ ❑ Concentration ug/I N/A ND<1.0 N/A 4/yr
2.3 (71-43-2) Mass
2 4 Bromoform ❑ ❑ ❑ Concentration
(75-25-2) Mass
2.5 Carbon tetrachloride ❑ ❑ Concentration
(56-23-5) Mass
Chlorobenzene Concentration
2.6 (108-90-7) CI CI ❑ Mass
Chlorodibromomethane Concentration
2.7 (124-48-1) ❑ CI 0 Mass
2.8 Chloroethane CI CI ❑ Concentration
(75-00-3) Mass
EPA Form 3510-2C(Revised 3-19) Page 12

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long-
Number
Present Absent Daily Monthly Daily of Term of
Discharge available)Discharge
Discharge Analyses Average
ee Analyses
(required) ( (if available)
2.9 2-chloroethylvinyl ether ❑ ❑ ❑ Concentration
(110-75-8) Mass
Concentration
2.10 Chloroform(67-66-3) 0 0 ❑✓ Mass
2.11 Dichlorobromomethane 0 0
❑ Concentration
(75-27-4) Mass
212 1,1-dichloroethane 0 0 ❑ Concentration
(75-34-3) Mass
2.13 1,2-dichloroethane 0 0
❑ Concentration
(107-06-2) Mass
2.14 1,1-dichloroethylene 0 ❑ ❑ Concentration
(75-35-4) Mass
2.15 1,2-dichloropropane 0 0
❑ Concentration
(78-87-5) Mass
2.16 1,3-dichloropropylene ❑ ❑ ❑ Concentration
(542-75-6) Mass
2.17 Ethylbenzene El ❑ 0
Concentration ug/l N/A ND<1.0 N/A
(100-41-4) Mass
2.18 Methyl bromide 0
0
0
Concentration
(74-83-9) Mass
2.19 Methyl chloride ❑ ❑ ❑ Concentration
(74-87-3) Mass
2.20 Methylene chloride ❑ 0
❑ Concentration
(75-09-2) Mass
2.21 1,1,2,2-tetrachloroethane 0
0
0
Concentration
(79-34-5) Mass
EPA Form 3510-2C(Revised 3-19) Page 13

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
( aily of of
Drequired)
favailabllee e) Discharge Analyses AverageValue Analyses
re cared
(if available)
Tetrachloroethylene Concentration
2.22 (127-18-4) Mass
2.23 Toluene ❑ ❑ Concentration ug/I N/A ND<1.0 N/A 4/yr
(108-88-3) Mass
2.24 1,2-trans-dichloroethylene 0 Concentration
El 1:1
(156-60-5) Mass
11,1-trichloroethane � Concentration
2.25 El 1:1
(71-55-6) Mass
1,1,2-trichloroethane � Concentration
2.26 0 ID
(79-00-5) Mass
2.27 Trichloroethylene Concentration
0 El El
(79-01-6) Mass
2.28 Vinyl chloride El
El
(75-01-4) Mass
Section 3.Organic Toxic Pollutants(GCIMS Fraction—Acid Compounds)
2-chlorophenol � � Concentration ug/I N/A ND<4.5 N/A 2/yr
3.1 (95-57-8) Mass
2,4-dichlorophenol Concentration ug/l N/A ND<4.5 N/A 2/yr
3.2 (120-83-2) Mass
2,4-dimethyiphenol Concentration ug/I N/A ND<9.1 N/A 2/yr
3.3 (105-67-9) Mass
4,6-dinitro-o-cresol ❑ ❑ ❑ Concentration ug/I N/A ND<9.1 N/A 2/yr
3.4 (534-52-1) Mass
3.5 2,4-dinitrophenol Concentration ug/I N/A ND<45.5 N/A 2/yr
El 0 El
(51-28-5) Mass
EPA Form 3510-2C(Revised 3-19) Page 14

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
of of
Discharge
o (if available) Di Dailyischarge Averageharge Analyses Value Analyses
(if
3.6 2-nitrophenol 0 Concentration ug/I N/A ND<4.5 N/A 2/yr
(88-75-5) Mass
4-nitrophenol 0 Concentration ug/I N/A ND<9.1 N/A 2/yr
3.7 El El
(100-02-7) Mass
3.8 p-chloro-m-cresol 0 Concentration ug/I N/A ND<4.5 N/A 2/yr
El 0
(59-50-7) Mass
Pentachlorophenol 0 Concentration ug/I N/A ND<9.1 N/A 2/yr
3.9 ID El
(87-86-5) Mass
Phenol 0 Concentration ug/I N/A ND<4.5 N/A 2/yr
3.10 (108-95-2) Mass
2,4,6-trichlorophenol 0 Concentration ug/I N/A ND<9.1 N/A 2/yr
3.11 (88 05 2) Mass
Section 4.Organic Toxic Pollutants(GCIMS Fraction—Base/Neutral Compounds)
4.1 Acenaphthene 0 Concentration ug/I N/A ND<4.5 N/A 2/yr
0 0
(83-32-9) Mass
4.2 Acenaphthylene 0 Concentration ug/I N/A ND<4.5 N/A 2/yr
0 0 •
(208-96-8) Mass
Anthracene 0 Concentration ug/I N/A ND<4.5 N/A 2/yr
4.3 1=I El
(120-12-7) Mass
Benzidine 0El 1:1 Concentration
4.4 (92 87 5) Mass
Benzo(a)anthracene 0 Concentration ug/I N/A ND <4.5 N/A 2/yr
4.5 (56-55-3) Mass
4,6 Benzo(a)pyrene Concentration ug/I N/A ND <4.5 N/A 2/yr
(50-32-8) Mass
EPA Form 3510-2C(Revised 3-19) Page 15

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West ow. OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v)p
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
Discharge Discharge Daily of Average of
(required) (if available) Discharge Analyses Value Analyses
(if available)
3,4-benzofluoranthene Concentration ug/I N/A ND<4.5 N/A 2/yr
4.7 (205-99-2) Mass
4.8 Benzo(ghi)perylene Concentration ug/l N/A ND<4.5 N/A 2/yr
(191-24-2) Mass
4.9 Benzo(k)fluoranthene ❑ ❑ Concentration ug/l N/A ND<4.5 N/A 2/yr
(207-08-9) Mass
Bis(2-chloroethoxy)methane 0 Concentration ug/I N/A ND<9.1 N/A 2/yr
4.10 (111-91-1) Mass
4.11 Bis(2-chloroethyl)ether Concentration ug/I N/A ND<4.5 N/A 2/yr
(111-44-4) Mass
4.12 Bis(2-chioroisopropyl)ether Concentration
(102-80-1) Mass
4.13 Bis(2-ethylhexyl)phthalate Concentration ug/l N/A ND<4.5 N/A 2/yr
El El 0
(117-81-7) Mass
4.14 4-bromophenyl phenyl ether Concentration ug/I N/A ND<4.5 N/A 2/yr
0 El El
(101-55-3) Mass
4.15 Butyl benzyl phthalate Concentration ug/l N/A ND<4.5 N/A 2/yr
El El 0
(85-68-7) Mass
4.16 2-chloronaphthalene Concentration ug/I N/A ND<4.5 N/A 2/yr
El El 0
(91-58-7) Mass
4.17 4-chlorophenyl phenyl ether Concentration ug/I N/A ND<4.5 N/A 2/yr
(7005-72-3) Mass
4.18 Chrysene Concentration ug/I N/A ND<4.5 N/A 2/yr
(218-01-9) Mass
4.19 Dibenzo(a,h)anthracene Concentration ug/l N/A ND<4.5 N/A 2/yr
(53-70-3) Mass
EPA Form 3510-2C(Revised 3-19) Page 16

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))l
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
aily of of
Discharge (if availablee) Discharge Analyses
AverageValue Analyses
(required)
(if available)
1,2-dichlorobenzene � Concentration
4.20 El El
(95-50-1) Mass
1,3-dichlorobenzene Concentration
4.21 (541-73-1) Mass
4.22 1,4-dichlorobenzene Concentration
(106-46-7) Mass
4.23 3,3-dichlorobenzidine Concentration ug/l N/A ND<9.1 N/A 2/yr
(91-94-1) Mass
Diethyl phthalate Concentration ug/I N/A ND<4.5 N/A 2/yr
4.24 (84-66-2) Mass
4.25 Dimethyl phthalate 0 ElConcentration ug/l N/A ND<4.5 N/A 2/yr
(131-11-3) Mass
Di-n-butyl phthalate Concentration ug/I N/A ND<4.5 N/A 2/yr
4.26 (84-74-2) Mass
2,4-dinitrotoluene 0 0 0 Concentration ug/I N/A ND<4.5 N/A 2/yr
4.27 (121-14-2) Mass
4.28 2,6-dinitrotoluene ❑ ❑ Concentration ug/l N/A ND<4.5 N/A 2/yr
(606-20-2) Mass
4.29 Di-n-octyl phthalate Concentration ug/l N/A ND<4.5 N/A 2/yr
(117-84-0) Mass
4.30 1,2-Diphenylhydrazine 0 0 Concentration
(as azobenzene)(122-66-7) Mass
Fluoranthene ❑ ❑ ❑ Concentration ug/I N/A ND<4.5 N/A 2/yr
4.31 (206-44-0) Mass
Fluorene Concentration ug/I N/A ND<4.5 N/A 2/yr
4.32 (86-73-7) Mass
EPA Form 3510-2C(Revised 3-19) Page 17

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Long-Term
Long-
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge
Discharge Analyses AverageValue Analyses
(required) (if available) (if available)
4.33 Hexachlorobenzene Concentration ug/I N/A ND<4.5 N/A 2/yr
(118-74-1) Mass
4.34 Hexachlorobutadiene Concentration ug/I N/A ND<4.5 N/A 2/yr
(87-68-3) Mass
4.35 Hexachlorocyclopentadiene Concentration ug/I N/A ND<9.1 N/A 2/yr
(77-47-4) Mass
4.36 Hexachloroethane Concentration ug/l N/A ND<4.5 N/A 2/yr
(67-72-1) Mass
4.37 Indeno(1,2,3-cd)pyrene Concentration ug/I N/A ND<4.5 N/A 2/yr
0 0 0
(193-39-5) Mass
4.38 Isophorone Concentration ug/I N/A ND<9.1 N/A 2/yr l El0
(78-59-1) Mass
Naphthalene Concentration ug/I N/A ND<4.5 N/A 2/yr
4.39 (91-20-3) 0 ❑ 0 Mass
4.40 Nitrobenzene El ❑ Concentration ug/I N/A ND<4.5 N/A 2/yr
(98-95-3) Mass
4.41 N-nitrosodimethylamine ElConcentration ug/I N/A ND<4.5 N/A 2/yr
El 0(62-75-9) Mass
4.42 N-nitrosodi-n-propylamine Concentration ug/I N/A ND<4.5 N/A 2/yr
(621-64-7) Mass
4.43 N-nitrosodiphenylamine CIConcentration ug/I N/A ND<9.1 N/A 2/yr
El 0(86-30-6) Mass
4.44 Phenanthrene Concentration ug/I N/A ND<4.5 N/A 2/yr
(85-01-8) Mass
Pyrene Concentration ug/I N/A ND<4.5 N/A 2/yr
4.45 (129-00-0) 0 CI 0 Mass
EPA Form 3510-2C(Revised 3-19) Page 18

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number LOng. Number
Present Absent Daily Monthly Term
( of
required)
Discharge Df availabllee) DischargeDaily Analyses AverageValue Analyses
re cared
(if available)
1,2,4-trichlorobenzene Concentration ug/I N/A ND<4.5 N/A 2/yr 2/yr
4.46 (120-82-1) Mass
Section 5.Organic Toxic Pollutants(GC/MS Fraction—Pesticides)
5.1 Aldrin Concentration
(309-00-2) Mass
a-BHC Concentration
5.2 (319-84-6) Mass
R-BHC Concentration
5.3 (319-85-7) Mass
y-BHC Concentration
5.4 (58 89 9) Mass
6-BHC Concentration
5.5 (319-86-8) Mass
Chlordane Concentration
5.6 (57-74-9) Mass
4,4'-DDT Concentration
5.7 0 0 0
(50-29-3) Mass
4,4'-DDE Concentration
5.8 0 0 0
(72-55-9) Mass
4,4'-DDD Concentration
5.9 (72-54-8) Mass
Dieldrin Concentration
5.10 0 0 0
(60-57-1) Mass
a-endosulfan Concentration
5.11 0 0 0
(115-29-7) Mass
EPA Form 3510-2C(Revised 3-19) Page 19

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Testing Units Long-Term
Long-
(and CAS Number,if available) Required Believed Believed Maximum Maximum q (specify) Average Number Number
Present Absent Daily Monthly Term
ischaischarge
®requ'ed a Daily
availablle) Discharg Analyses Averag
Valuee Analyses
(if available}e
13-endosulfan ❑ ❑ ❑ Concentration
5.12 (115-29-7) Mass
Endosulfan sulfate ❑ ❑ ❑ Concentration
5.13 (1031-07-8) Mass
Endrin ❑ ❑ ❑ Concentration
5.14 (72 20 8) Mass
Endrin aldehyde 0 ❑ ❑ Concentration
5.15 (7421-93-4) Mass
Heptachlor ❑ ❑ ❑ Concentration
5.16 (76-44-8) Mass
Heptachlor epoxide Concentration
5.17 (1024-57-3) ❑ ❑ 0
Mass
PCB-1242 Concentration
5.18 (53469-21-9) 0 ❑ ✓❑ Mass
PCB-1254 Concentration
5.19 (11097-69-1) 0 0 0 Mass
PCB-1221 Concentration
5.20 (11104-28-2) 0 ❑ 0 Mass
PCB-1232 Concentration
5.21 (11141-16-5) 0 0 ❑✓ Mass
PCB-1248 Concentration
5.22 (12672-29-6) 0 0 0 Mass
PCB-1260 Concentration
5.23 (11096-82-5) 0 0 0 Mass
PCB-1016 Concentration
5.24 (12674-11-2) 0 0 0 Mass
EPA Form 3510-2C(Revised 3-19) Page 20

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
Dreq(required) (if available) DisDchargofe Analyses of
ischarge DischargeAValuee Analyses
(if available)
Toxaphene Concentration
5.25 (8001-35-2) 0 0 0 Mass
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 21

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West ow. OMB No.2040-0004
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence
(check one) Effluent Intake
(Optional)
Units
Pollutant Maximum Long-Term
Believed Believed (specify) Maximum Daily Monthly Average Daily Number of Long-Term Number of
Present Absent Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) (if available) Value
❑ Check here if you believe all pollutants on Table C to be present in your discharge from the noted outfall.You need not complete the"Presence or Absence"column of Table C for
each pollutant.
❑ Check here if you believe all pollutants on Table C to be absent in your discharge from the noted outfall.You need not complete the"Presence or Absence"column of Table C for
each pollutant.
1 Bromide ❑ ❑ Concentration
(24959-67-9) Mass
Chlorine,total Concentration
2' residual ❑ ❑ Mass
3. Color ElConcentration
Mass
Concentration
4. Fecal coliform 0 0 Mass
5 Fluoride Concentration
(16984-48-8) ❑ 0 Mass
6 Nitrate-nitrite 0 0
Concentration
Mass
Nitrogen,total Concentration
7. organic(as N) ElMass
Concentration mg/I N/A ND<4.9 N/A 4/yr
8. Oil and grease 0 ❑
Mass
Phosphorus(as ✓ Concentration
g' P),total(7723-14-0) ❑ Mass
10. Sulfate(as SO4) 0 0 Concentration
(14808-79-8) Mass
11. Sulfide(as S) ❑ 0 Concentration
Mass
EPA Form 3510-2C(RevisedPage 23
3-19)

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence Intake
(check one) Effluent (Optional)
Units
Pollutant Maximum Long-Term
Believed Believed (specify) Maximum Daily Monthly Average Daily Number of Long-Term Number of
Present Absent Discharge Discharge Discharge Analyses Average Analyses
(required)
(if available) (if available) Value
Sulfite(as SO3) Concentration
12. (14265-45-3) ❑ a
Mass
Concentration
13. Surfactants 0 ❑✓ Mass
14. Aluminum,total ❑ ✓❑ Concentration
(7429-90-5) Mass
Barium,total ❑ El Concentration
15. (7440-39-3)
Mass
16. Boron,total ❑ ❑✓ Concentration
(7440-42-8) Mass
17 Cobalt,total El ❑ Concentration
(7440-48-4) Mass
18 Iron,total ❑ 0Concentration
(7439-89-6) Mass
19. Magnesium,total ❑ ❑ Concentration
(7439-95-4) Mass
Molybdenum, Concentration
20. total 0 ❑✓
(7439-98-7) Mass
21 Manganese,total ❑ ✓❑ Concentration
(7439-96-5) Mass
22. Tin,total 0 0Concentration
(7440-31-5) Mass
23. Titanium,total ❑ ❑✓ Concentration
(7440-32-6) Mass
EPA Form 3510-2C(Revised 3-19) Page 24

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence
(check one) Effluent Intake
(Optional)
Pollutant Units Maximum Long-Term
Believed Believed (specify) Maximum DailyLong-Term
Present Absent Discharge Monthly Average Daily Number of Average Number of
Discharge Discharge Analyses Analyses
(required) Value
(if available) (if available)
24. Radioactivity
Concentration
Alpha,total ❑ 0
Mass
Concentration
Beta,total 0 ❑✓
Mass
Concentration
Radium,total ❑ ❑✓ Mass
Concentration
Radium 226,total 0 ❑✓ Mass
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e., methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 25

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
1. Asbestos 0 ❑✓
2. Acetaldehyde 0 ❑✓
3. Allyl alcohol 0 ✓❑
4. Allyl chloride 0 ❑✓
5. Amyl acetate 0 0
6. Aniline 0 0
7. Benzonitrile 0 ❑✓
8. Benzyl chloride ❑ 0
9. Butyl acetate 0 0
10. Butylamine 0 0
11. Captan 0 ❑✓
12. Carbaryl 0 0
13. Carbofuran 0 ❑✓
14. Carbon disulfide 0 ❑✓
15. Chlorpyrifos ❑ ❑✓
16. Coumaphos 0 0
17. Cresol 0 ❑✓
18. Crotonaldehyde 0 0
19. Cyclohexane 0 0
EPA Form 3510-2C(Revised 3-19) Page 27

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
20. 2,4-D(2,4-dichlorophenoxyacetic acid) ❑ ❑✓
21. Diazinon ❑ ✓❑
22. Dicamba ❑ ❑✓
23. Dichlobenil 0 0
24. Dichlone ❑ 0
25. 2,2-dichloropropionic acid 0 0
26. Dichlorvos 0 0
27. Diethyl amine 0 0
28. Dimethyl amine 0 0
29. Dintrobenzene 0 ❑✓
30. Diquat ❑ ❑✓
31. Disulfoton ❑ 0
32. Diuron ❑ 0
33. Epichlorohydrin 0 ❑✓
34. Ethion ❑ ❑✓
35. Ethylene diamine ❑ 0
36. Ethylene dibromide ❑ 0
37. Formaldehyde ❑ 0
38. Furfural ❑ ❑✓
EPA Form 3510-2C(Revised 3-19) Page 28

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
39. Guthion ❑ ❑✓
40. Isoprene ❑ ❑✓
41. Isopropanolamine ❑ ❑✓
42. Kelthane ❑ ❑✓
43. Kepone 0 ❑✓
44. Malathion 0 ❑✓
45. Mercaptodimethur 0 ❑✓
46. Methoxychlor 0 ❑✓
47. Methyl mercaptan 0 ❑✓
48. Methyl methacrylate ✓
ry
49. Methyl parathion ❑ ❑✓
50. Mevinphos 0 ❑✓
51. Mexacarbate 0 ❑✓
52. Monoethyl amine 0 ❑✓
53. Monomethyl amine 0 0
54. Naled 0 0
55. Naphthenic acid 0 ❑✓
56. Nitrotoluene 0 ❑✓
57. Parathion 0 0
EPA Form 3510-2C(Revised 3-19) Page 29

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
58. Phenolsulfonate 0 0
59. Phosgene ❑ 0
60. Propargite 0 0
61. Propylene oxide ❑ 0
62. Pyrethrins 0 0
63. Quinoline 0 0
64. Resorcinol 0 0
65. Strontium ❑ 0
66. Strychnine ❑ 0
67. Styrene 0 0
68. 2,4,5-T(2,4,5-trichlorophenoxyacetic ❑ 0
acid)
69. TDE(tetrachlorodiphenyl ethane) ❑ 0
70. 2,4,5-TP[2-(2,4,5-trichlorophenoxy) ❑ ❑
propanoic acid]
71. Trichlorofon 0 0
72. Triethanolamine ❑ 0
73. Triethylamine 0 0
74. Trimethylamine ❑ 0
75. Uranium 0 0
76. Vanadium 0 0
EPA Form 3510-2C(Revised 3-19) Page 30

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii)p
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
77. Vinyl acetate ❑ ❑✓
78. Xylene ❑✓ ❑ component of gasoline ND<3.0 ugh!-4/yr
79. Xylenol 0 0
80. Zirconium 0 ❑✓
I Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 31

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000825505 NC0027006 MPLX Terminals LLC-Selma West 001 OMB No.2040-0004
TABLE E.2,3,7,8 TETRACHLORODIBENZO P DIOXIN(2,3,7,8 TCDD)(40 CFR 122.21(g)(7)(viii))
TCDD Presence or
Congeners Absence
Pollutant Used or (check one) Results of Screening Procedure
Manufactured Believed Believed
Present Absent
2,3,7,8-TCDD 0 El 0
EPA Form 3510-2C(Revised 3-19) Page 33

Section 2
2.1 Line Drawing

Exhibit 2C-1. Line Drawing - Selma West Oak
Stormwater Stormwater Stormwater
Intermittent Intermittent Intermittent----
Load Rack, Ethanol Offload, Parking Lot Drains Tank Farm Dike Area
VRU Pad, Additive Offload,
Truck Pump Back
Waste Treatment - OWS # 2 Retention Holding Pond
Waste Treatment - OWS # 1 Retention Holding Pond Outfall 001
Outfall 001
Waste Treatment - OWS # 2 Small Unnamed Creek
Small Unnamed Creek
Neuse River
Retention Holding Pond Neuse River
Outfall 001
Small Unnamed Creek Schematic of Water Flow -- NC0027006
Marathon Petroleum
Neuse River 2555 West Oak St, Selma, NC 27576

Attachment A: Request for Waiver—Table A Pollutants

Attachment A: Request for Waiver—Table A Pollutants
Per Item 7.1 in Section 7,"Effluent and Intake Characteristics(40 CFR 12.21(g)(7)). MPLX
Terminals LLC (MPLXT) is requesting a waiver for the following Table A pollutants listed
below. The terminal has an existing NPDES permit,NC0036145 which does not require testing
for these pollutants. Additionally,the operations of this facility have not had a significant
change in operations since the existing permit was granted.
• Biochemical oxygen demand(BOD)—Table# 1.
• Chemical oxygen demand(COD)—Table#2.
• Total organic carbon(TOC)—Table#3
• Ammonia(as N)—Table# 5
• Temperature,winter and summer(degree C)Table#7
• pH min and max (su)Table#8

Attachment B
Analytical Results — Table A,B,C and D Applicable Pollutants
Analytical Results — Whole Effluent Testing (WET) Analysis

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville NC to 100
28078
wrnwedabston [phone]
September 13, 2022
Mr. Roger Lamberth
Marathon Blanchard Terminal
P.O. Box 248
3707 Buffalo Rd.
Selma, NC 27576
RE: Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
Dear Mr.Lamberth:
Enclosed are the analytical results for sample(s)received by the laboratory on August 17,2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
Some analyses were subcontracted outside of the Pace Network.The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
•Pace Analytical Services-Asheville
•Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Felix Jimenez-MPLX,Marathon Petroleum Corporation-
NC
Mallory Hay,Marathon Petroleum Corporation
Michael House,Marathon Blanchard Terminal
Bob Jarabeck,Marathon Petroleum
Cindi A.Matthews,Marathon Petroelum Company
/77,,,,,,-4%
i�� REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 26

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
ceAnalytical Huntersville,NC 28078
www.pioalabatoe [phone]
CERTIFICATIONS
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#:E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#:12 Louisiana DoH Drinking Water#:LA029
South Carolina Laboratory ID:99006 VirginiaNELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 2 of 26

Pace Analytical Services,LLC
aceAnalytical5 9800Huntersv Ile Kincey ; Suite
C 28078
wtww•paCNabs eon [phone]
SAMPLE ANALYTE COUNT
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92621038001 Outfall 001 EPA 1664B REL 1 PASI-C
EPA 625.1 PKS 58 PASI-C
EPA 624.1 SAS 10 PASI-C
SM 2130B-2011 DMN 1 PASI-A
SM 2540D-2011 MAB2 1 PASI-A
EPA 420.4 Rev 1.0 1993 KDF1 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 3 of 26

Pace Analytical Services,LLC 1
® 9800 KinceyAve. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacelabs.con [phone]
ANALYTICAL RESULTS
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
Sample: Outfall 001 Lab ID: 92621038001 Collected: 08/17/22 09:45 Received: 08/17/22 12:37 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method:EPA 1664B
Pace Analytical Services-Charlotte
Oil and Grease ND mg/L 4.8 1 08/19/22 01:00
625 RVE Analytical Method:EPA 625.1 Preparation Method:EPA 625.1
Pace Analytical Services-Charlotte
Acenaphthene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 83-32-9
Acenaphthylene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 208-96-8
Anthracene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 120-12-7
Benzo(a)anthracene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 56-55-3
Benzo(a)pyrene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 50-32-8
Benzo(b)fluoranthene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 205-99-2
Benzo(g,h,i)perylene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 191-24-2
Benzo(k)fluoranthene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 207-08-9
4-Bromophenylphenyl ether ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 101-55-3
Butylbenzylphthalate ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 85-68-7
4-Chloro-3-methylphenol ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 9.1 1 08/22/22 15:27 08/23/22 12:07 111-91-1
bis(2-Chloroethyl)ether ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 111-44-4
2-Chloronaphthalene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 91-58-7
2-Chlorophenol ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 95-57-8
4-Chlorophenylphenyl ether ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 7005-72-3
Chrysene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 218-01-9
Dibenz(a,h)anthracene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 53-70-3
3,3'-Dichlorobenzidine ND ug/L 9.1 1 08/22/22 15:27 08/23/22 12:07 91-94-1
2,4-Dichlorophenol ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 120-83-2
Diethylphthalate ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 84-66-2
2,4-Dimethylphenol ND ug/L 9.1 1 08/22/22 15:27 08/23/22 12:07 105-67-9
Dimethylphthalate ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 131-11-3
Di-n-butylphthalate ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 84-74-2
4,6-Dinitro-2-methylphenol ND ug/L 9.1 1 08/22/22 15:27 08/23/22 12:07 534-52-1
2,4-Dinitrophenol ND ug/L 45.5 1 08/22/22 15:27 08/23/22 12:07 51-28-5
2,4-Dinitrotoluene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 121-14-2
2,6-Dinitrotoluene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 606-20-2
Di-n-octylphthalate ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 117-84-0
bis(2-Ethylhexyl)phthalate ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 117-81-7
Fluoranthene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 206-44-0
Fluorene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 86-73-7
Hexachloro-1,3-butadiene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 87-68-3
Hexachlorobenzene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 118-74-1
Hexachlorocyclopentadiene ND ug/L 9.1 1 08/22/22 15:27 08/23/22 12:07 77-47-4
Hexachloroethane ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 67-72-1 L2
Indeno(1,2,3-cd)pyrene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 193-39-5
Isophorone ND ug/L 9.1 1 08/22/22 15:27 08/23/22 12:07 78-59-1
Naphthalene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 91-20-3
Nitrobenzene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 98-95-3
2-Nitrophenol ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 88-75-5
4-Nitrophenol ND ug/L 9.1 1 08/22/22 15:27 08/23/22 12:07 100-02-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 26

Pace Analytical Services,LLC
Q/��.� �+�J® 9800 Kincey Ave. Suite 100
CG/'IIIR� i71�G1I Huntersville,NC 28078
rrYnr•Peul�lsson [phone]
ANALYTICAL RESULTS
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
Sample: Outfall 001 Lab ID: 92621038001 Collected: 08/17/22 09:45 Received: 08/17/22 12:37 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method:EPA 625.1 Preparation Method:EPA 625.1
Pace Analytical Services-Charlotte
N-Nitrosodimethylamine ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 62-75-9
N-Nitroso-di-n-propylamine ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 621-64-7
N-Nitrosodiphenylamine ND ug/L 9.1 1 08/22/22 15:27 08/23/22 12:07 86-30-6
2,2'-Oxybis(1-chloropropane) ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 108-60-1
Pentachlorophenol ND ug/L 9.1 1 08/22/22 15:27 08/23/22 12:07 87-86-5
Phenanthrene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 85-01-8
Phenol ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 108-95-2
Pyrene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 129-00-0
1,2,4-Trichlorobenzene ND ug/L 4.5 1 08/22/22 15:27 08/23/22 12:07 120-82-1 L2
2,4,6-Trichlorophenol ND ug/L 9.1 1 08/22/22 15:27 08/23/22 12:07 88-06-2
Surrogates
Nitrobenzene-d5(S) 79 % 10-120 1 08/22/22 15:27 08/23/22 12:07 4165-60-0
2-Fluorobiphenyl(S) 61 % 15-120 1 08/22/22 15:27 08/23/22 12:07 321-60-8
Terphenyl-d14(S) 118 % 11-131 1 08/22/22 15:27 08/23/22 12:07 1718-51-0
Phenol-d6(S) 25 % 10-120 1 08/22/22 15:27 08/23/22 12:07 13127-88-3
2-Fluorophenol(S) 9 % 10-120 1 08/22/22 15:27 08/23/22 12:07 367-12-4 SO
2,4,6-Tribromophenol(S) 11 % 10-137 1 08/22/22 15:27 08/23/22 12:07 118-79-6
624 Volatile Organics Analytical Method:EPA 624.1
Pace Analytical Services-Charlotte
Benzene ND ug/L 1.0 1 08/19/22 20:46 71-43-2
Ethylbenzene ND ug/L 1.0 1 08/19/22 20:46 100-41-4
Naphthalene ND ug/L 5.0 1 08/19/22 20:46 91-20-3
Toluene ND ug/L 1.0 1 08/19/22 20:46 108-88-3
Xylene(Total) ND ug/L 3.0 1 08/19/22 20:46 1330-20-7
m&p-Xylene ND ug/L 5.0 1 08/19/22 20:46 179601-23-1
o-Xylene ND ug/L 5.0 1 08/19/22 20:46 95-47-6
Surrogates
4-Bromofluorobenzene(S) 99 % 70-130 1 08/19/22 20:46 460-00-4
Toluene-d8(S) 107 % 70-130 1 08/19/22 20:46 2037-26-5
1,2-Dichloroethane-d4(S) 87 % 70-130 1 08/19/22 20:46 17060-07-0
2130B Turbidity Analytical Method:SM 2130B-2011
Pace Analytical Services-Asheville
Turbidity 1.2 NTU 1.0 1 08/18/22 14:56
2540D TSS,Low-Level Analytical Method:SM 2540D-2011
Pace Analytical Services-Asheville
Total Suspended Solids 1.4 mg/L 1.0 1 08/23/22 11:49
420.4 Phenolics,Total Analytical Method:EPA420.4 Rev 1.0 1993 Preparation Method:EPA420.4 Rev 1.0 1993
Pace Analytical Services-Asheville
Phenolics,Total Recoverable ND mg/L 0.020 1 08/23/22 12:56 08/24/22 07:53 64743-03-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 26

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacalab.cola [phone]
QUALITY CONTROL DATA
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
QC Batch: 718224 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM,Oil and Grease
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92621038001
METHOD BLANK: 3744239 Matrix: Water
Associated Lab Samples: 92621038001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 08/19/22 01:00
LABORATORY CONTROL SAMPLE: 3744240
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 37.2 93 78-114
MATRIX SPIKE SAMPLE: 3744241
35739312001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 1.1J 39.2 38.7 96 78-114
SAMPLE DUPLICATE: 3744242
35739310001 Dup
Parameter Units Result Result RPD Qualifiers
Oil and Grease mg/L 37.7 37.4 1
Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 26

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
rr Pac.laUftom [phone]
QUALITY CONTROL DATA
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
QC Batch: 718435 Analysis Method: EPA 624.1
QC Batch Method: EPA 624.1 Analysis Description: 624 MSV
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92621038001
METHOD BLANK: 3745006 Matrix: Water
Associated Lab Samples: 92621038001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Benzene ug/L ND 1.0 08/19/22 13:58
Ethylbenzene ug/L ND 1.0 08/19/22 13:58
m&p-Xylene ug/L ND 5.0 08/19/22 13:58
Naphthalene ug/L ND 5.0 08/19/22 13:58
o-Xylene ug/L ND 5.0 08/19/22 13:58
Toluene ug/L ND 1.0 08/19/22 13:58
Xylene(Total) ug/L ND 3.0 08/19/22 13:58
1,2-Dichloroethane-d4(S) % 87 70-130 08/19/22 13:58
4-Bromofluorobenzene(S) % 100 70-130 08/19/22 13:58
Toluene-d8(S) % 104 70-130 08/19/22 13:58
LABORATORY CONTROL SAMPLE: 3745007
Spike LCS LCS %Rec
%
Parameter Units Conc. Result Rec Limits Qualifiers
Benzene ug/L 20 18.9 95 70-130
Ethylbenzene ug/L 20 19.2 96 70-130
m&p-Xylene ug/L 40 39.2 98 70-130
Naphthalene ug/L 20 22.2 111 70-133
o-Xylene ug/L 20 20.0 100 70-130
Toluene ug/L 20 18.5 93 70-130
Xylene(Total) ug/L 60 59.2 99 70-130
1,2-Dichloroethane-d4(S) °Ao 91 70-130
4-Bromofluorobenzene(S) % 97 70-130
Toluene-d8(S) % 98 70-130
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3745008 3745009
MS MSD
92621038001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Benzene ug/L ND 20 20 20.4 20.2 102 101 75-125 1
Ethylbenzene ug/L ND 20 20 22.3 22.1 112 110 75-134 1
m&p-Xylene ug/L ND 40 40 44.2 44.6 111 112 53-157 1
Naphthalene ug/L ND 20 20 22.5 23.1 112 116 57-150 3
o-Xylene ug/L ND 20 20 22.2 22.5 111 113 68-143 2
Toluene ug/L ND 20 20 20.3 20.8 102 104 75-134 2
Xylene(Total) ug/L ND 60 60 66.4 67.1 111 112 66-145 1
1,2-Dichloroethane-d4(S) % 92 90 70-130
Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 26

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
rntvpocd�bfton [phone]
QUALITY CONTROL DATA 1
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3745008 3745009
MS MSD
92621038001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
4-Bromofluorobenzene(S) % 96 99 70-130
Toluene-d8(S) % 96 99 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 26

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
rrinta.pateNatbsan [phone]
QUALITY CONTROL DATA
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
QC Batch: 718693 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92621038001
METHOD BLANK: 3746180 Matrix: Water
Associated Lab Samples: 92621038001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,2,4-Trichlorobenzene ug/L ND 5.0 08/23/22 10:28
2,2'-Oxybis(1-chloropropane) ug/L ND 5.0 08/23/22 10:28
2,4,6-Trichlorophenol ug/L ND 10.0 08/23/22 10:28
2,4-Dichlorophenol ug/L ND 5.0 08/23/22 10:28
2,4-Dimethylphenol ug/L ND 10.0 08/23/22 10:28
2,4-Dinitrophenol ug/L ND 50.0 08/23/22 10:28
2,4-Dinitrotoluene ug/L ND 5.0 08/23/22 10:28
2,6-Dinitrotoluene ug/L ND 5.0 08/23/22 10:28
2-Chloronaphthalene ug/L ND 5.0 08/23/22 10:28
2-Chlorophenol ug/L ND 5.0 08/23/22 10:28
2-Nitrophenol ug/L ND 5.0 08/23/22 10:28
3,3'-Dichlorobenzidine ug/L ND 10.0 08/23/22 10:28
4,6-Dinitro-2-methylphenol ug/L ND 10.0 08/23/22 10:28
4-Bromophenylphenyl ether ug/L ND 5.0 08/23/22 10:28
4-Chloro-3-methylphenol ug/L ND 5.0 08/23/22 10:28
4-Chlorophenylphenyl ether ug/L ND 5.0 08/23/22 10:28
4-Nitrophenol ug/L ND 10.0 08/23/22 10:28
Acenaphthene ug/L ND 5.0 08/23/22 10:28
Acenaphthylene ug/L ND 5.0 08/23/22 10:28
Anthracene ug/L ND 5.0 08/23/22 10:28
Benzo(a)anthracene ug/L ND 5.0 08/23/22 10:28
Benzo(a)pyrene ug/L ND 5.0 08/23/22 10:28
Benzo(b)fluoranthene ug/L ND 5.0 08/23/22 10:28
Benzo(g,h,i)perylene ug/L ND 5.0 08/23/22 10:28
Benzo(k)fluoranthene ug/L ND 5.0 08/23/22 10:28
bis(2-Chloroethoxy)methane ug/L ND 10.0 08/23/22 10:28
bis(2-Chloroethyl)ether ug/L ND 5.0 08/23/22 10:28
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 08/23/22 10:28
Butylbenzylphthalate ug/L ND 5.0 08/23/22 10:28
Chrysene ug/L ND 5.0 08/23/22 10:28
Di-n-butylphthalate ug/L ND 5.0 08/23/22 10:28
Di-n-octylphthalate ug/L ND 5.0 08/23/22 10:28
Dibenz(a,h)anthracene ug/L ND 5.0 08/23/22 10:28
Diethylphthalate ug/L ND 5.0 08/23/22 10:28
Dimethylphthalate ug/L ND 5.0 08/23/22 10:28
Fluoranthene ug/L ND 5.0 08/23/22 10:28
Fluorene ug/L ND 5.0 08/23/22 10:28
Hexachloro-1,3-butadiene ug/L ND 5.0 08/23/22 10:28
Hexachlorobenzene ug/L ND 5.0 08/23/22 10:28
Hexachlorocyclopentadiene ug/L ND 10.0 08/23/22 10:28
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 26

Pace Analytical Services,LLC
le 9800 KinceyAve. Suite 100
aceAnalytical Huntersville,NC 28078
www.ouNols.cml [phone]
QUALITY CONTROL DATA
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
METHOD BLANK: 3746180 Matrix: Water
Associated Lab Samples: 92621038001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Hexachloroethane ug/L ND 5.0 08/23/22 10:28
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 08/23/22 10:28
Isophorone ug/L ND 10.0 08/23/22 10:28
N-Nitroso-di-n-propylamine ug/L ND 5.0 08/23/22 10:28
N-Nitrosodimethylamine ug/L ND 5.0 08/23/22 10:28
N-Nitrosodiphenylamine ug/L ND 10.0 08/23/22 10:28
Naphthalene ug/L ND 5.0 08/23/22 10:28
Nitrobenzene ug/L ND 5.0 08/23/22 10:28
Pentachlorophenol ug/L ND 10.0 08/23/22 10:28
Phenanthrene ug/L ND 5.0 08/23/22 10:28
Phenol ug/L ND 5.0 08/23/22 10:28
Pyrene ug/L ND 5.0 08/23/22 10:28
2,4,6-Tribromophenol(S) % 85 10-137 08/23/22 10:28
2-Fluorobiphenyl(S) % 74 15-120 08/23/22 10:28
2-Fluorophenol(S) % 63 10-120 08/23/22 10:28
Nitrobenzene-d5(S) % 79 10-120 08/23/22 10:28
Phenol-d6(S) % 46 10-120 08/23/22 10:28
Terphenyl-d14(S) % 104 11-131 08/23/22 10:28
LABORATORY CONTROL SAMPLE: 3746181
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,2,4-Trichlorobenzene ug/L 50 20.5 41 44-142 L2
2,2'-Oxybis(1-chloropropane) ug/L 50 29.0 58 36-166
2,4,6-Trichlorophenol ug/L 50 39.6 79 37-144
2,4-Dichlorophenol ug/L 50 36.3 73 1-191
2,4-Dimethylphenol ug/L 50 41.3 83 32-119
2,4-Dinitrophenol ug/L 250 140 56 1-181
2,4-Dinitrotoluene ug/L 50 45.5 91 39-139
2,6-Dinitrotoluene ug/L 50 46.5 93 50-158
2-Chloronaphthalene ug/L 50 34.9 70 60-118
2-Chlorophenol ug/L 50 35.9 72 23-134
2-Nitrophenol ug/L 50 36.6 73 29-182
3,3'-Dichlorobenzidine ug/L 100 97.1 97 1-262
4,6-Dinitro-2-methylphenol ug/L 100 87.1 87 1-181
4-Bromophenylphenyl ether ug/L 50 41.3 83 53-127
4-Chloro-3-methylphenol ug/L 100 75.4 75 22-147
4-Chlorophenylphenyl ether ug/L 50 38.3 77 25-158
4-Nitrophenol ug/L 250 114 46 1-132
Acenaphthene ug/L 50 38.0 76 47-145
Acenaphthylene ug/L 50 37.6 75 33-145
Anthracene ug/L 50 39.1 78 1-166
Benzo(a)anthracene ug/L 50 45.1 90 33-143
Benzo(a)pyrene ug/L 50 53.3 107 17-163
Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 26

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.oaetlabs con [phone]
QUALITY CONTROL DATA
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
LABORATORY CONTROL SAMPLE: 3746181
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Benzo(b)fluoranthene ug/L 50 57.8 116 24-159
Benzo(g,h,i)perylene ug/L 50 55.7 111 1-219
Benzo(k)fluoranthene ug/L 50 56.5 113 11-162
bis(2-Chloroethoxy)methane ug/L 50 37.8 76 33-184
bis(2-Chloroethyl)ether ug/L 50 38.8 78 12-158
bis(2-Ethylhexyl)phthalate ug/L 50 52.4 105 8-158
Butylbenzylphthalate ug/L 50 54.8 110 1-152
Chrysene ug/L 50 44.4 89 17-168
Di-n-butylphthalate ug/L 50 44.1 88 1-118
Di-n-octylphthalate ug/L 50 54.4 109 4-146
Dibenz(a,h)anthracene ug/L 50 55.3 111 1-227
Diethylphthalate ug/L 50 43.7 87 1-114
Dimethylphthalate ug/L 50 42.7 85 1-112
Fluoranthene ug/L 50 42.3 85 26-137
Fluorene ug/L 50 41.1 82 59-121
Hexachloro-1,3-butadiene ug/L 50 15.6 31 24-116
Hexachlorobenzene ug/L 50 41.7 83 1-152
Hexachlorocyclopentadiene ug/L 50 19.3 39 25-150
Hexachloroethane ug/L 50 17.2 34 40-113 L2
Indeno(1,2,3-cd)pyrene ug/L 50 56.2 112 1-171
Isophorone ug/L 50 37.3 75 21-196
N-Nitroso-di-n-propylamine ug/L 50 40.3 81 1-230
N-Nitrosodimethylamine ug/L 50 32.1 64 25-150
N-Nitrosodiphenylamine ug/L 50 45.2 90 25-150
Naphthalene ug/L 50 25.8 52 21-133
Nitrobenzene ug/L 50 35.1 70 35-180
Pentachlorophenol ug/L 100 87.4 87 14-176
Phenanthrene ug/L 50 42.8 86 54-120
Phenol ug/L 50 25.7 51 5-112
Pyrene ug/L 50 48.2 96 52-115
2,4,6-Tribromophenol(S) % 96 10-137
2-Fluorobiphenyl(S) % 71 15-120
2-Fluorophenol(S) % 62 10-120
Nitrobenzene-d5(S) % 75 10-120
Phenol-d6(S) % 48 10-120
Terphenyl-d14(S) % 104 11-131
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3746182 3746184
MS MSD
92617068010 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
1,2,4-Trichlorobenzene ug/L ND 100 100 40.4J 37.7J 40 38 44-142 MO
2,2'-Oxybis(1-chloropropane) ug/L ND 100 100 47.8J 44J 48 44 36-166
2,4,6-Trichlorophenol ug/L ND 100 100 66.5J 77.8J 66 78 37-144
2,4-Dichlorophenol ug/L ND 100 100 50.0 54.3 50 54 1-191 8
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 26

aceAnalytical® Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
Huntersville,NC 28078
wwr►•patedatbfton [phone]
QUALITY CONTROL DATA
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3746182 3746184
MS MSD
92617068010 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
2,4-Dimethylphenol ug/L ND 100 100 62J 69.1J 62 69 32-119
2,4-Dinitrophenol ug/L ND 500 500 ND 342J 45 68 1-181
2,4-Dinitrotoluene ug/L ND 100 100 88.5 95.1 89 95 39-139 7
2,6-Dinitrotoluene ug/L ND 100 100 81.8 84.8 82 85 50-158 4
2-Chloronaphthalene ug/L ND 100 100 53.5 56.7 54 57 60-118 6 M1
2-Chlorophenol ug/L ND 100 100 52.5 47.6J 52 48 23-134
2-Nitrophenol ug/L ND 100 100 55.2 60.1 55 60 29-182 9
3,3'-Dichlorobenzidine ug/L ND 200 200 159 196 80 98 1-262 21
4,6-Dinitro-2-methylphenol ug/L ND 200 200 154 193 77 97 1-181 22
4-Bromophenylphenyl ether ug/L ND 100 100 69.4 80.5 69 80 53-127 15
4-Chloro-3-methylphenol ug/L ND 200 200 124 140 62 70 22-147 13
4-Chlorophenylphenyl ether ug/L ND 100 100 63.9 71.0 64 71 25-158 10
4-Nitrophenol ug/L ND 500 500 186 242 37 48 1-132 26
Acenaphthene ug/L ND 100 100 55.1 64.3 55 64 47-145 15
Acenaphthylene ug/L ND 100 100 56.7 61.6 57 62 33-145 8
Anthracene ug/L ND 100 100 63.5 76.2 64 76 1-166 18
Benzo(a)anthracene ug/L ND 100 100 83.5 100 83 100 33-143 18
Benzo(a)pyrene ug/L ND 100 100 94.3 107 94 107 17-163 12
Benzo(b)fluoranthene ug/L ND 100 100 99.7 113 100 113 24-159 13
Benzo(g,h,i)perylene ug/L ND 100 100 87.9 97.3 88 97 1-219 10
Benzo(k)fluoranthene ug/L ND 100 100 92.2 111 92 111 11-162 19
bis(2-Chloroethoxy)methane ug/L ND 100 100 46.9J 49.2J 47 49 33-184
bis(2-Chloroethyl)ether ug/L ND 100 100 76.5 72.3 76 72 12-158 6
bis(2-Ethylhexyl)phthalate ug/L ND 100 100 113 133 113 133 8-158 16
Butylbenzylphthalate ug/L ND 100 100 127 147 127 147 1-152 15
Chrysene ug/L ND 100 100 80.2 95.9 80 96 17-168 18
Di-n-butylphthalate ug/L ND 100 100 93.3 111 93 111 1-118 18
Di-n-octylphthalate ug/L ND 100 100 119 140 119 140 4-146 17
Dibenz(a,h)anthracene ug/L ND 100 100 88.6 96.5 89 97 1-227 9
Diethylphthalate ug/L ND 100 100 83.2 96.0 83 96 1-114 14
Dimethylphthalate ug/L ND 100 100 72.0 82.3 72 82 1-112 13
Fluoranthene ug/L ND 100 100 72.8 84.4 73 84 26-137 15
Fluorene ug/L ND 100 100 63.9 69.9 64 70 59-121 9
Hexachloro-1,3-butadiene ug/L ND 100 100 32.3J 32.5J 32 33 24-116
Hexachlorobenzene ug/L ND 100 100 69.4 79.0 69 79 1-152 13
Hexachlorocyclopentadiene ug/L ND 100 100 39.5J 42.2J 39 42 25-150 1
Hexachloroethane ug/L ND 100 100 31.4J 25.4J 31 25 40-113 MO
Indeno(1,2,3-cd)pyrene ug/L ND 100 100 88.0 103 88 103 1-171 16
Isophorone ug/L ND 100 100 49.7J 54.5J 50 54 21-196
N-Nitroso-di-n-propylamine ug/L ND 100 100 60.0 59.1 60 59 1-230 1
N-Nitrosodimethylamine ug/L ND 100 100 40.5J 38.8J 40 39 25-150
N-Nitrosodiphenylamine ug/L ND 100 100 77J 87.8J 77 88 25-150
Naphthalene ug/L ND 100 100 48J 47.7J 41 41 21-133
Nitrobenzene ug/L ND 100 100 47.5J 50.6 48 51 35-180
Pentachlorophenol ug/L ND 200 200 150 182 75 91 14-176 19
Phenanthrene ug/L ND 100 100 73.2 85.8 73 86 54-120 16
Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 26

Pace Analytical Services,LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
rlrtw•ptieNatbs eaatt [phone]
QUALITY CONTROL DATA
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3746182 3746184
MS MSD
92617068010 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phenol ug/L 972 100 100 890 941 -82 -31 5-112 6 M1
Pyrene ug/L ND 100 100 85.6 103 86 103 52-115 18
2,4,6-Tribromophenol(S) % 79 88 10-137
2-Fluorobiphenyl(S) % 47 50 15-120
2-Fluorophenol(S) % 36 35 10-120
Nitrobenzene-d5(S) % 49 49 10-120 D3
Phenol-d6(S) % 30 31 10-120
Terphenyl-d14(S) % 91 108 11-131
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 26

Pace Analytical Services,LLC
aceAnalytical a 9800 Kin ey Ave. Suite100
Huntersville,NC 28078078
www•Malatbs.cati [phone]
QUALITY CONTROL DATA
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
QC Batch: 718152 Analysis Method: SM 2130B-2011
QC Batch Method: SM 2130B-2011 Analysis Description: 2130E Turbidity
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92621038001
METHOD BLANK: 3743650 Matrix: Water
Associated Lab Samples: 92621038001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Turbidity NTU ND 1.0 08/18/22 14:26
LABORATORY CONTROL SAMPLE: 3743651
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Turbidity NTU 10 9.9 99 90-110
SAMPLE DUPLICATE: 3743652
92621026001 Dup
Parameter Units Result Result RPD Qualifiers
Turbidity NTU 1.6 1.7 6
SAMPLE DUPLICATE: 3743653
92621034001 Dup
Parameter Units Result Result RPD Qualifiers
Turbidity NTU 5.9 6.2 5
Resultspresented on this page are in the units indicated bythe"Units"column except where an alternate unit ispresented to the right of the result.I p g p 9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 26

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
nmcpacelabs.eoe [phone]
QUALITY CONTROL DATA
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
QC Batch: 718828 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92621038001
METHOD BLANK: 3746983 Matrix: Water
Associated Lab Samples: 92621038001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 1.0 08/23/22 11:49
LABORATORY CONTROL SAMPLE&LCSD: 3746984 3747636
Spike LCS LCSD LCS LCSD %Rec Max
Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers
Total Suspended Solids mg/L 251 244 246 97 98 90-110 1 10
Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 26

Pace Analytical Services,LLC
0 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.paedaba.eon [phone]
QUALITY CONTROL DATA
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
QC Batch: 718760 Analysis Method: EPA 420.4 Rev 1.0 1993
QC Batch Method: EPA420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92621038001
METHOD BLANK: 3746604 Matrix: Water
Associated Lab Samples: 92621038001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenolics,Total Recoverable mg/L ND 0.020 08/24/22 07:39
LABORATORY CONTROL SAMPLE: 3746605
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Phenolics,Total Recoverable mg/L 0.05 0.046 92 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3746606 3746607 1
MS MSD
92619860001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phenolics,Total Recoverable mg/L ND 0.05 0.05 0.049 0.049 96 97 90-110 1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3746608 3746609
MS MSD
92620239001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phenolics,Total Recoverable mg/L ND 0.05 0.05 0.050 0.042 99 84 90-110 16 M1,R1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 26

Pace Analytical Services,LLC
aceAnalyti to9800 Suite cal Huntersville,C28078
WWW.pICNaba.caa [phone]
QUALIFIERS
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
L2 Analyte recovery in the laboratory control sample(LCS)was below QC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 26

Pace Analytical Services,LLC
_ aceAnalytical® 9800 Kincey Ave. Suite 100
Huntersville,NC 28078078
www.pacelabs.com
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 2026 Blanchard Quarterly
Pace Project No.: 92621038
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92621038001 Outfall 001 EPA 1664B 718224
92621038001 Outfall 001 EPA 625.1 718693 EPA 625.1 718959
92621038001 Outfall 001 EPA 624.1 718435
92621038001 Outfall 001 SM 2130B-2011 718152
92621038001 Outfall 001 SM 2540D-2011 718828
92621038001 Outfall 001 EPA420.4 Rev 1.0 1993 718760 EPA 420.4 Rev 1.0 1993 719028
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/13/2022 01:15 PM without the written consent of Pace Analytical Services,LLC. Page 18 of 26

DC* Title: ENV-FRM-HUN1-0084 v01 Tech Spec Sample Condition
Ce. Upon Receipt
I wee Effective Date:05/12/2022
Laboratory receiving samples:
Asheville ❑ Eden ❑ Greenwood❑ Huntersviile❑ naleigh'llMechan)csviile❑ A/tllaln't�a❑ KernersvilleD
Sarnph'Condition Upon Client Name: 110#
V//621,038
He ceiP4 (, — c�� �fO�eCii>!: VV it
Courier OFed Ex UPS USPSCllent I❑Commercial e ['Other: 1 111t'1i111jj
92621038
Carrier Tracklng Number:` _ I )
�rf 1
Custody Seal Present? ❑Yes No Seals Intact? ❑Yes jla Date/InitialsPerson Examining Contents: a i1 In- i
I
Packing Material: OBubble Wrap eubble Bags ONone 0 Other Biological Tissue ?
C- i I
� •
i
/� ❑Yes ONo N/A i l
Thermometer: ❑IR Gun ID: a 015 J 5^ Type of Ice: wet 0 Blue Q None (
Cooler Temp CC): 14, \ Correction`action Factor:Add/Subtract CC) �J V i
Temp should be above freezing to Et
Corrected Cooler Temp(`C) ]Sampphas �out of temp criteria.Samples on Ice,coaling process F,
USDA Regulated Soli((TN/A,water sample) i
•
•
Did samples oripete In a quarantine zone within the United States:CA,NY,or SC(check maps)? Did samples originate from a foreign source(internationally,
:yes including Hawaii and Puerto Rico)?Des ;afro i ;
•
Comments/Discrepancy:
Chain of Custody Present? ONo ON/A 1. i 1}{j C
.Y Tu
i
Samples Arrived within Hold Time? ( Y s ❑No ON/A 2.
Short Hold Time Analysis(42 hr.)? /es ONo ON/A 3.
Rush Turn Around Time Requested? [Des /ffNo ON/A 4.
Sufficient Volume? Des ONo ON/A 5.
Correct Containers Used? f. es ONo ON/A 5.
-Pace Containers Used? Yes ONo ❑NIA
Containers intact? Yf"" ONo ON/A _7, j €
Dissolved analysis:Samples Field Filtered? Oyes Otto 8.o /A s
Sample Labels Match COG? Janis ON° ON/A 9. i
, j'(�
-Includes Date/Time/ID/Analysis Matrix: A✓v
- E
Headspace in VOA Vials(>5-6mm}? ONo ON/A 10.
Trip Blank Present? Dyes Ono .2/A 11.
Trip Blank•Custody Seals Present? Ores ONo pilrrA
COMMENTS/SAMPLE DISCREPANCY Field Data Required? Dyes ONo
Lot ID of split containers:
Temp Log:Temp must be maintained CLIENT NOTIFICATION/RESOLUTION
at<6 C during login,record temp
every 20 minutes.
Tithe opened: Temp:
Time: put in cooler •
Time: Temp:
Person Contacted: Date/11me: _ •
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
Qualtrax Document ID: 70677 Page 1 of 2
Page 19 of 26

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;',. eAaArt/ar CHAIN-OF-CUSTODY/Analytical Request Document a
The Chain-of-Custody is a LEGAL DOCUMENT.All relevant fields must be completed accurately.
Section A Section a Section C
Required Client irdormatlon: Required Project Information: Invoke Information: Page: 1 Of ,
Company: Marathon Petroleum Company-NC Report To: Lamberth•Ro
ger Attention:
Address: 3707 Buffalo Rd. Copy To: Company!sterna:
Selma,NC 2757E
Email: Purchase Order a: Address: n:;:,;.__^L.
Phone: Paco Quote: ""f c7i v .`..
IFS Put Name: 2028 Blanchard QuarterlyPace Project
oket Manager2 ola.Dalaii ceiabe.cam, x'�-• xF^�. `+r -
Requested Due Data: t`rUJe�t e:NC0088960 � C n, .. L.L_._^'SiaFr�sLroeaHpe. i-. .`:�.. ,.. .
Pace Profile#: 3222.1 NC
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(%4 877 e942, (800)e91-2325 Frec(864)977 6995
Shipping Address:4 Crafsman Ct,Greer,SC 29650
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State:AU� NPDES#: 450 "3'r`_ t1'baEaEmneotT Ore It
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�!' ��r. Acute !Chronic Test Orkonisms .l
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Date Time Relic uisi Oy"an"
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COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 16 hours
rate Proportional:I sample each hour for 24 hours.Equal volt',0.0 and 6.0°C.Samples must not be frozen.Use ratter ice in sealed bags. of sample collectionl(complction ofcomposite sample).
at minimum 1 sample every 4 hours over 24 hours. Sample may not be!used after 72 hours from sample collection.
rowProportional:As per instructions in NPDES

Et1[ . (664)8774942.rAx(864)877-6930
P.D.Box 16414.Greenvlle.SC 29606 4 Craftsman Court,Greer,5C 29650
Pimephales promelas 24 Hour Acute Definitive Test
EPA-821-R-02-012 Method 2000
Client: MARATHON PETROLEUM CO
Facility:BLANCHARD 2026 WEST OAK ST
NPDES#:NC0088960
Test Date: 18-Aug-22
Laboratory ID#:T62786
Test Reviewed and Approved By:
t✓4 total( �. (1A- w,z
Robert W.Kelley,Ph.D. Patrick D.Timms
President QA/QC Officer
Certification#E87819 SCDHEC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided samples. NCDENR Certification# 022 Page 23 of 26
Page 1 of 4

Effluent Toxicity Report Form-Chronic Pass/Fail and Acute LC50 Date 08-Sep-22
Facility: MARATHON PETROLEUM CO BLANCHARD NPDES#NC0088960 Pipe# 001 County: Johnston
Laboratory Performing Test: ETT Environmental. Inc. Comments
X
Signature of Operator in Responsible Charge
X
Signature of Laboratory Supervisor
MAIL ORIGINAL TO Environmental Sciences Branch
Div.of Water Quality
N.C.DENR
1621 Mail Service Center
Raleigh,North Carolina 27699-1621
North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results
Calculated t=
Critical Value=
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 %Reduction=
#Young Produced %Mortality Avg.Reprod.
Adult (L)ive (D)ead
Control Control
Effluent%
Treatment 2 Treatment 2
Control CV
TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
#Young Produced %3rd Brood PASS FAIL
Adult (L)ive (D)ead I l
Complete This for Either Test Test Start Date
Collection(Start)Date 18-Aug-22
pH 1st sample 1st sample 2nd sample Sample 1 17-Aug-22 Sample 2 NA
Control Sample Type(Duration)
Treatment 2 Grab Comp Duration 1st 2nd
Sample 1 X Tox Tox
Sample 2 Dilution Sample Sample
start end start end start end
D.O. 1st sample 1st sample 2nd sample Hardness(mg/L) 81.6
Control Spec.Cond.(pmhos) 311 42
Treatment 2 Chlorine(mg/L) <0.05
Sample Temp.at receipt(CC) 0.8
LC50/Acute Toxicity Test
(Mortality expressed as%,combining replicates)
0 6.25 12.5 25 50 100 Concentration
0 0 0 0 0 0 Mortality start/end start/end
LC50= >100 % Method of Determination 7.7 8.0 Control 8.5 8.5
95%Confidence Limits Moving Average Probit = 8.1 7.6 High Conc. 9.1 8.8
NA% NA % Spearman Karber Other X pH D.O.
Organism Tested PIMEPHALES PROMELAS I
DEM Form AT-1 Page 24 of 26
Page 2 of 4
I

24 Hour Acute Toxicity Test
Test Method:EPA 821 R-02-012; Method 20100 Pimephales promelas
Client: MARA I'HON PE IROLEUM CO Sample ID:BLANCHARD 2026 WEST OAK Si Lab ID#: T62786
Start Date: 08/18/22 Time: 03:00 PM Set By: JC
End Date: 08/19/22 Time: 02:29 PM Ended By: JC
Test Vessel Test Solution Volume Incubator Transfer Volume Dilution Water
Fathead Minnows 500 mL plastic cup 200 mL #1 0.5 mL MHSF
Randomization pattern per SOP !Neonates from common holding vessel Light: 50-100 ft-c.16 hr light/8 hr dark
TEST ORGANISMS
for Ceriodaphnia dubia Comments:
Date Removed: Between: and:
Pimephales promelas Source: ABS 8/10/22 lays old: 14 ORGANISMS HATCHED 8/4/22 1500-1630
Mysidopsis bahia Source: Days old:
Test Organisms Pre Fed b : JC Time: 12:45
MORTALITY DATA
Conn tn@ial# Cumulative Mortality Final Initial Final
Cond/ Cond/
Rep. organisms za nr ax n, zz n va' m'mwy Temp D 0 ®Salim ®®D O ®Salim
A 10 0 3 t i.
Control B 10 0
C
D 0% 24.4 8.5®_� 25.0 8.5 8.0_�
A 10 0
6.3% B 10 0
C
D 0% 24.4 8.7 7.8_� v 25.0 8.6 7.9_®
A 10 0
12.5% B 10 0
C
D 0% 24.4 8.7 7.8__:,,,::, 25.0 8.4 7.9_17
A 10 0
25.0% B 10 0
C
D 0% 2'4.4 8.8 7.9__ 25.0 ._.8.5 7.8__
A 10, 0 -�
50.0% B 10 0
C
D 0% 24.4 8.9 8.0__ 25.0 8.5®_®
A 10 0
100.0% B 10 0
C
D 0% 24.4 9.1 8.1 __ 25.0 8.8®__
A
B
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D °C ��_PPT _���_PPT _
Page 25 of 26
Page 3 of 4

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PO Box 16414,Greenville,SC 29806-7414. f
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Date Time Relin iris d !Organs tin i Received By/Organization Area Tonic°C Preserved?
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OMPOSITE SAa4PLING PROCEDURES URES TEMPER ITURE MONITORING PROCEDURES HOLD TIME PROCEDURES
omposite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For to�itit)resting the sample mustfirstbe used within 36 hours
I
me Proportional:]sample each hour for 24 hours.Equal vohn 0.0 and 6.0°C.Samples must not be fr rLen_Use water ice in sealed bags. of sample coilectioa(completion of composite sample).
at minimum 1 sample every 4 hours over 24 hours. p Sample may not be:used after 72 hours from sample collection.
ow Proportional:As per instructions in NPDES permit + i
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