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HomeMy WebLinkAboutWQ0000957_Monitoring - 07-2022_20220815W r August 9, 2022 Department of Environment & Natural Resources Division of Water Resources — Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: Valley Proteins, Inc. — Wadesboro Division, Permit #WQOOOO957 DARLING INGREDIENTS a _ V.� a Enclosed please find the Quarterly Monitoring Wells Report for our Wadesboro, North Carolina Division. If you require any additional information or wish to discuss the information in this report, please feel free to call me at (704) 694-3701. Sincerely, Mike Craumer General Manager 1 GW-59A COMPLIANCE REPORT FORM Permit # (Submit one each monitoring period with GW_59 forms.) VV00000957 1 Enter date monitoring results were due. ( 8/31/2022 ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was an required information missingon the GW-59 report forms? YES NO IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)'df the answer is "YES", contact to Regional Office for guidance 4 Are any monitoring constituents equal to or above the established standards? YES I NO If the answer to question 4 is "NO', skip to section 8. If the answer to question 4 is "YES'list the affected wells individually with constituents(s) and concenlratiori exceeding standards in the space provided below: MW# 1, 2, 3, 5, and 9 exceed ground water standards for Total Dissolved Solids. MW# 1, 2, 3, 5, and 9 exceed for chlorides. MW#1 & 2 exceeds for nitrate. 5 For the same constituents identified in question 4 above, have standards been exceeded previously for the YES i NO same constituents(s) in the same wells(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES"Dist in the space provided below, each well with constituent(s) exceeding standards, concentra6on(s) reported, and sample collection date for each occurrence (for the last two years). See Report enclosed. 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? 4 YES NO If the answer is "YES", a groundwater quality problem may be occuring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO'> ontact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permitteee to a Notice of Violation fines, and/or penalties. Piezometers were placed in the irrigation fields to determine water quality . Total Dissolved Solids and Chlorides were determined to be naturally high in this area. Sprinkler heads were purposely capped off near monitoring well #1 as instructed by Jim Barber (Regional Engineer) to see if the nitrate level will change in the well. An anoxic pond was put in place to reduce nitrates. 8 The Person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. Signature of Permittee (or Authorized Agent) Date GW-59A 12/8/2003 SUBMIT FORM ON YELLOW PAPER ONLY EPARTMENT OF ENVIRONMENT,& NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 06/30/2023 Facility Name: Valley Proteins Non -Discharge W00000957 UIC NPDES Other Permit Name (if different): Facility Address: 656 Little Duncan Road TYPE OF PERMITTED OPERATION BEING MONITORED Wadesboro NC 28170 County Anson ❑ Lagoon ❑ Remediation: Infiltration Gallery 91 Spray Field ❑ Remediation: Contact Person: Mike Craumer Telephone#: 704-694-3701 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Behind Field #9 No. of wells to be sampled: 8 ❑ Water Source Heat Pump ❑ Other: from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW#1 Date sample collected: 07/20/2022 FIELD ANALYSES: WAS Well Depth: 33 ft. Well Diameter: 2 in. pH 7.1 units Temp. 17.8 °C DRY at Depth to Water Level: 16.89 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 1668 µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor None check Volume of water pumped/bailed before sampling: 11.0 gallons Appearance _ Murky here: ❑ Samples for metals were collected unfiltered: El YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 07/20/ thru 07/25/2022 Laboratory Name: PACE Analytical Certification No. #12 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal ND /100ml Nitrate (NO3) as N 13.9 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P 10 mg/I (Note' Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 974 mg/I Al - Aluminum mg/I pH (when analyzed) 7.4 units Ba - Barium mg/I TOC 1.4 mg/I Ca - Calcium mg/I Chloride 339 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 29.1 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia ND mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total) Mn -Manganese mg/I ,method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Mike Craumer (General Manager) Permiftee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 1/2007 SUBMIT FORM ON YELLOW PAPER ONLY ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: Valley Proteins Permit Name (if different): Facility Address: 656 Little Duncan Road Wadesboro NC 28170 County Anson act Person: Mike Craumer Location/Site Name: Behind Field #4 Telephone#: 7 04-6 94-3 7 01 No. of wells to be sampled: 8 )EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES NVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 PERMIT Number: Expiration Date: 06/30/2023 Non -Discharge W00000957 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW#2 Date sample collected: 07/20/2022 FIELD ANALYSES: WAS Well Depth: 30 ft. Well Diameter: 2 in. pH 7.1 units Temp. 18.1 °C DRY at Depth to Water Level: 10.82 ft. below measuring point Screened Interval: ft. to _ft. Spec. Cond. 1925 µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor None check Volume of water pumped/bailed before sampling: 11.25 gallons Appearance Murky here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO sample analyzed: 07/20/ thru 07/25/2022 Laboratory Name: PACE Analytical Certification No. #12 ;AMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal ND /100ml Nitrate (NO3) as N 10.8 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P .074 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 1210 mg/I Al - Aluminum mg/I pH (when analyzed) 7.2 units Ba - Barium mg/I TOC ND mg/I Ca - Calcium mg/I Chloride 402 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 8.3 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia ND mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen: NH3as N, Ammonia Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 1/2007 ;Date) SUBMIT FORM ON YELLOW PAPER ONLY EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: Niff'6117 (VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 06/30/2023 Facility Name: Valley Proteins Non -Discharge W00000957 UIC NPDES Other Permit Name (if different): Facility Address: 656 Little Duncan Road TYPE OF PERMITTED OPERATION BEING MONITORED Wadesboro NC 28170 County Anson ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: Contact Person: Mike Craumer Telephone#: 704-694-3701 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Behind Field #1 No. of wells to be sampled: 8 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPUNG INFORMATION If WELL WELL ID NUMBER (from Permit): MW#3 Date sample collected: 07/20/2022 FIELD ANALYSES: WAS Well Depth: 29.2 ft. Well Diameter: 4 in. pH 7.1 units Temp. 18.9 °C DRY at Depth to Water Level: 15.81 ft. below measuring point Screened Interval: ft. to — ft. Spec. Cond. 1949 µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor None check Volume of water pumped/bailed before sampling: 8•5 gallons Appearance Murky here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 07/20/ thru 07/25/2022 Laboratory Name: PACE Analytical Certification No. #12 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal ND /100m1 Nitrate (NO3) as N 3.6 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P ND mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 1220 mg/I Al - Aluminum mg/I pH (when analyzed) 7.4 units Ba - Barium mg/I TOC ND mg/I Ca - Calcium mg/I Chloride 474 mg/1 Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/1 (Specify test and method #. ATTACH LAB REPORT.) Sulfate 106 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia ND mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N mg/1 Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: and that the laboratory analytical data ilit of fines and im nsonment for knc Mike Craumer (General Manager) Permittee (or Authorized Agent) Name and Title - Please print or type mg/L VOC Removal% AV ,;� ;Date) GW-59 Rev.1/2007 SUBMIT FORM ON YELLOW PAPER ONLY EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: ]VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM - 517 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 06/30/2023 Facility Name: Valley Proteins Non -Discharge W00000957 UIC Permit Name (if different): NPDES Other Facility Address: 656 Little Duncan Road TYPE OF PERMITTED OPERATION BEING MONITORED Wadesboro NC 28170 County Anson ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: Contact Person: Mike Craumer Telephone#: 704-694-3701 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Behind Pond #1 No. of wells to be sampled: 8 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW#5 Date sample collected: 07/20/2022 FIELD ANALYSES: WAS Well Depth: 29.2 ft. Well Diameter: 2 in. pH 6.7 units Temp. 18.6 °C DRY at Depth to Water Level: 10.64 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 2275 µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor None check Volume of water pumped/bailed before sampling: 9•75 gallons Appearance Murky here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 07/20/ thru 07/25/2022 Laboratory Name: PACE Analytical Certification No. #12 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal 1.0 /100ml Nitrate (NO3) as N .041 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P .11 mg/I (Note. use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 1310 mg/I Al - Aluminum mg/I pH (when analyzed) 7.0 units Ba - Barium mg/I TOC 1.8 mg/I Ca - Calcium mg/I Chloride 340 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 28.8 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia ND mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total) Mn -Manganese mg/I ,method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Mike Craumer (General Manager) Permiftee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 1/2007 of Permittee (or Authorized Agent) 'Date) SUBMIT FORM ON YELLOW PAPER ONLY EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: ffiffiff'617 (VISION OF WATER QUALITY-INFORMAnoN PROCESSING UNIT COMPLIANCE REPORT FORM MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 06/30/2023 Facility Name: Valley Proteins Non -Discharge W00000957 UIC Permit Name (if different): NPDES Other Facility Address: 656 Little Duncan Road TYPE OF PERMITTED OPERATION BEING MONITORED Wadesboro NC 28170 County Anson ❑ Lagoon ❑ Remediation: Infiltration Gallery K❑ Spray Field ❑ Remediation: Contact Person: Mike Craumer Telephone#: 704-694-3701 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Behind Field #20 No. of wells to be sampled: 8 ❑ Water Source Heat Pump ❑ Other: from permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW#6 Date sample collected: 07/20/2022 FIELD ANALYSES: WAS Well Depth: 45 ft. Well Diameter: 2 in. pH 6.6 units Temp. 18.3 °C DRY at Depth to Water Level: 9.81 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 200 µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor None check Volume of water pumped/bailed before sampling: 8•0 gallons Appearance Murky here: ❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: []YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 07/20/ thru 07/25/2022 Laboratory Name: PACE Analytical Certification No. #12 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal 4.0 /100ml Nitrate (NO3) as N ND mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P .34 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 147 mg/I Al - Aluminum mg/I pH (when analyzed) 7.4 units Ba - Barium mg/I TOC ND mg/I Ca - Calcium mg/I Chloride 17.0 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 9.0 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia ND mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen. NH,as N, Ammonia Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Mike Craumer (General Manager) Permittee (or Authorized Agent) Name and Title - Please print or type Siqnature of Permittee (or Authorized Aqent) ;Date) GW-59 Rev. 1/2007 SUBMIT FORM ON YELLOW PAPER ONLY EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: EN1617 (VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 06/30/2023 Facility Name: Valley Proteins Non -Discharge W00000957 UIC Permit Name (if different): NPDES Other Facility Address: 656 Little Duncan Road TYPE OF PERMITTED OPERATION BEING MONITORED Wadesboro NC 28170 County Anson ❑ Lagoon ❑ Remediation: Infiltration Gallery x❑ Spray Field ❑ Remediation: Contact Person: Mike Craumer Telephone#: 704-694-3701 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Behind Field #19 No. of wells to be sampled: 8 ❑ Water Source Heat Pump ❑ Other: from Pemrt SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW#7 Date sample collected: 07/20/2022 FIELD ANALYSES: WAS Well Depth: 52 ft. Well Diameter: 2 in. pH 7.2 units Temp. 18.5 °C DRY at Depth to Water Level: 21.33 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 543 µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor None check Volume of water pumped/bailed before sampling: 11.0 gallons Appearance Murky here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 07/20/ thru 07/25/2022 Laboratory Name: PACE Analytical Certification No. #12 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal 4.0 /100ml Nitrate (NO3) as N .27 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P ND mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 314 mg/I Al - Aluminum mg/I pH (when analyzed) 7.5 units Ba - Barium mg/I TOC ND mg/I Ca - Calcium mg/I Chloride 33.8 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 6.5 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia ND mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen, NH3asN. Ammonia Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Mike Craumer (General Manager) Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 1/2007 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: ,.IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date 06/30/2023 Facility Name: Valley Proteins Non -Discharge W00000957 UIC NPDES Other Permit Name (if different): Facility Address: 656 Little Duncan Road TYPE OF PERMITTED OPERATION BEING MONITORED Wadesboro NC 28170 County Anson ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: Contact Person: Mike Craumer Telephone#: 704-694-3701 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Behind Field #16 No. of wells to be sampled: 8 ❑ Water Source Heat Pump ❑ Other: (from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW#8 Date sample collected: 07/20/2022 FIELD ANALYSES: WAS Well Depth: 30 ft. Well Diameter: 2 in. pH 6.8 units Temp. 20.7 °C DRY at Depth to Water Level: 5.65 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 634 µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor None check Volume of water pumped/bailed before sampling: 11.0 gallons Appearance Murky here: ❑ Samples for metals were collected unfiltered: El YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 07/20/ thru 07/25/2022 Laboratory Name: PACE Analytical Certification No. #12 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal ND /100ml Nitrate (NO3) as N ND mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P .070 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 430 mg/I Al - Aluminum mg/I pH (when analyzed) 7.2 units Ba - Barium mg/I TOC ND mg/I Ca - Calcium mg/I Chloride 104 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 9.5 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia ND mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total) Mn -Manganese mg/I ,method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev. 1/2007 SUBMIT FORM ON YELLOW PAPER ONLY EPARTMENT OF ENVIRONMENT''$ NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT' COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER, RALEIGH, NC 22699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 06/30/2023 Facility Name: Valley Proteins Non -Discharge WQ0000957 UIC NPDES Other Permit Name (if different): Facility Address: 656 Little Duncan Road TYPE OF PERMITTED OPERATION BEING MONITORED Wadesboro NC 28170 County Anson ❑ Lagoon ❑ Remediation: Infiltration Gallery Spray Field ❑ Remediation: Contact Person: Mike Craumer Telephone#: 704-694-3701 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Behind Field #14 No. of wells to be sampled: 8 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW#9 Date sample collected: 07/20/2022 FIELD ANALYSES: WAS Well Depth: 30 ft. Well Diameter: 2 in. pH 6.8 units Temp. 17.9 °C DRY at Depth to Water Level: 11.70 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 1866 µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor None check Volume of water pumped/bailed before sampling: 9•0 gallons Appearance Murky here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 07/20/ thru 07/25/2022 Laboratory Name: PACE Analytical Certification No. #12 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal ND /100ml Nitrate (NO3) as N .54 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P .054 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 1050 mg/I Al - Aluminum mg/I pH (when analyzed) 7.2 units Ba - Barium mg/I TOC ND mg/I Ca - Calcium mg/I Chloride 501 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 26.6 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia ND mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen. NH3as N. Ammonia Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Mike Craumer (General Manager) Permittee (or Authorized Agent) Name and Title - Please print or type Siqnature of Permittee (or Authorized Aqent) ;Date) GW-59 Rev. 1/2007 Document Name: Field data Sheet Document hlumbtr. F-CAR-Fi D-001-rev.03 f Name and Affiliation (Sampler(s); troL Name and Affiliation (Inspector);_ Ili /A Well Information Well ID: M,W.-1 Well Diameter: oZ N -- Total Well Depth: Static Water Level: I Et Height of Water Column 16 - 30 ft Well Locked: Construction: NZ dd Data Sheet Review: Date: 9�yt 7-2i-ZZ NO / Flushmount ) Steel) Multi Factor'. m•Ib r(Radlue/12)2x3,14x7.4). Casing Votume gallons. Cal. 3 Volumes ' g — gajlons Pump Intake; Allk. ae: March 8, 2019 I of_ Pace Huntersville Quality. Office IAJ'�Vl?S . r� I'ur eg Info_imatiort Date Purged D-1 j ao Start:_ _p .13aa Purge Rate: Purging Method _ . G. �. Tot'al Volume'Purged: allo mis/L) Sampling Informatioln Date Collected;SL/w-22-- Time Collected: Sampling $quipment iJsed: 51 ,U_ InstruMent ID:_- Bottle Type Preservation Analysis Required .� 0h1)_ VOA ?hoC &Z fl 1— �•-t�s� ./Von/ E � %�-cA.� �ete;(1rons Sample Temp (°C): t Tim a: JU:! ..Turbidity (ntu): ` Timer Dias Oxy (ing/L). -- Tirane. — Fe 2+ mg/L.- Time Specific Cond. (us): _VQ_G-Tim& Res. © (mg/L)/(ug/L): Tirne . J Sample pH (s.u.): 7:L Tune: Z(As Od'or: .t 1D P Time: 6 cjc,! ReDox(mV): Time Appearance: Wtu.- Tom:_. /6 _ ReDox (EH value):YSI Proplus +200AIV -- Other: — ' Time: General/WeatherObservations: § cloudy/raitly) Temp (7 Wind a(mph) Sampler Signature Stabilization' Test Time Purged Temp. (°C) Dias Oxy. (mg/L) Spec.oume and ( pH (s.n.) ReDox (m� Turbidity () removed Water �OIW61s/ level (ft) Other a �-- — _ b 1.!2ceAna1X'Jlca1" www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Sprayfield Well Pace Project No.: 92615936 Sample: MW-1 Lab ID: 92615936001 Collected: 07/20/22 16:45 Received: 07/20/22 18:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by PACE 1 08/01/22 09:36 Collected By JJQ 1 08/01/22 09:36 Collected Date 07/20/22 1 08/01/22 09:36 Collected Time 16:45 1 08/01/22 09:36 pH 7.1 Std. Units 1 08/01/22 09:36 Temperature 17.8 deg C 1 08/01/22 09:36 Static Water Level 16.89 feet 1 08/01/22 09:36 Specific Conductance 1668 umhos/cm 1 08/01/22 09:36 Total Well Depth 33.19 feet 1 08/01/22 09:36 Odor None 1 08/01/22 09:36 Appearance Murky 1 08/01/22 09:36 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms ND CFU/100 mL 1.0 1 07/20/22 18:49 07/21/22 17:00 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Asheville Total Dissolved Solids 974 mg/L 50.0 1 07/25/22 12:02 4500H+ pH, Electrometric Analytical Method: SM 4500-H+B-2011 Pace Analytical Services -Asheville pH at 25 Degrees C 7.4 Std. Units 0.10 1 07/22/22 15:32 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 29.1 mg/L 1.0 1 07/22/2213:44 14808-79-8 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia ND mg/L 0.10 1 07/25/2212:40 7664-41-7 353.2 Nitrogen, NO2/1403 unpres Analytical Method: EPA353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate 13.9 mg/L 0.20 5 07/20/22 23:57 14797-55-8 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus 0.10 mg/L 0.050 1 07/25/22 17:46 07/25/22 21:22 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville Chloride 339 mg/L 15.0 15 07/22/2215:38 16887-00-6 Date: 08/02/2022 05:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. H3 Page 4 of 25 aceAnalytical www.pacslabs.com ANALYTICAL RESULTS Project: Sprayfield Well Pace Project No.: 92615936 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-1 Lab ID: 92615936001 Collected: 07/20/22 16:45 Received: 07/20/22 18:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310E TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon 1.4 mg/L 1.0 1 07/21/22 19:49 7440-44-0 Date: 08/02/2022 05:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 25 Document Name: Field data Sheet Date Issued: March 8 22019 �� c8 xal cam' pap.. I of Document Number. F-CAR-FLD-001-rev.03 bjv'ng Authority: Pace Run tersvi!!e Qua.Iitr• Office . Name aitd A.ttiliattion (Sampler(s); (9` , iC17 Name and Affiliation (inspector): N f Well Information Well ID: rA W — °� Well Locked: Well Diameter: r�tt Total Well Depth: 3 ft Static Water Level: ci • - ft Height of Water Column: 12. 4ft AK- 1d Data Sheet Review: Date: /�_97,2 / Fluslu ount ) Construction Steel/Stainless Steel) Multi Factor*: !?. b 3 l*(Radi„s/12)2 x 3.1! z 7.48j. Casing Volume: �� gallons Cal. 3 Volumes: " �E%,ff gallons Pump Intake: P r a Ihforinati'ort Date Purged�o�/ _/-Start: 1 Finish_) ao Purge lZate Purging Method: Q W10 Soo Total Volume Pnr ed: g --.�� Ilo cols/L) QA5. B ht- C_t C- SainpIing Information Date Collected:. 6 /2V 39- Time Collected:- i b �- Sampling $quipmentUsed:_ &AIhC - Instrumentm: z Sl fo Bottle Type Preservatiin Analysis Required b%IDCC t �� 2 Sam— i2t� • �-- I�mL �{zgpµ -u:,t. _.....-�_��i'9�2'?t.- Sample Teatp (°C): �(g Time: [W-0 Turbidity (ntu); Titne: Digs Oxy (gig/L)= — Tine Pe 2+ mg/L: Specific Cond. (oS): Time: r (o S-O . Res. CI (mg/L)/(µg/i,): Sample pH (S•u_): d� Time: _Od'or: .. /)n�'1 P Time: l ReDox (mV): Time: Appearance:Time:, "I k22­0_ ReDox (EH value):YSI ProPlus +200r1tV Other: Time: General/Weather Observations:. ttit v 1- - . soli cloudy/rairty) Temp-10—(T) Wind gLID (mph) Sampler Signature Stabilization Test Spec., Cond.( ,, . o � - MMR�® I1DG ®ems®�-�_� aceAnalytical / www.pacelabs.com ANALYTICAL RESULTS Project: Sprayfield Well Pace Project No.: 92615936 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-2 Lab ID: 92615936002 Collected: 07/20/22 16:20 Received: 07/20/22 18:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Performed by Collected By Collected Date Collected Time pH Temperature Static Water Level Specific Conductance Total Well Depth Odor Appearance MBIO 9222D Fecal Coliform CHT Fecal Coliforms 2540C Total Dissolved Solids Total Dissolved Solids 4500H+ pH, Electrometric pH at 25 Degrees C 300.0 IC Anions 28 Days Sulfate 350.1 Ammonia Nitrogen, Ammonia 353.2 Nitrogen, N021NO3 unpres Nitrogen, Nitrate 365.1 Phosphorus, Total Phosphorus 4500 Chloride Chloride Date: 08/02/2022 05:19 PM Analytical Method: Pace Analytical Services - Charlotte PACE 1 08/01/22 09:37 JJC1 1 08/01/22 09:37 07/20/22 1 08/01/22 09:37 16:20 1 08/01/22 09:37 7.1 Std. Units 1 08/01/22 09:37 18.1 deg C 1 08/01/22 09:37 10.82 feet 1 08/01/22 09:37 1925 umhos/cm 1 08/01/22 09:37 33.16 feet 1 08/01/22 09:37 None 1 08/01/22 09:37 Murky 1 08/01/22 09:37 Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte ND CFU/100 mL 1.0 1 07/20/22 18:49 07/21/22 17:00 Analytical Method: SM 254OC-2015 Pace Analytical Services - Asheville 1210 mg/L 50.0 1 07/25/2212:02 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 7.2 Std. Units 0.10 1 07/22/22 15:25 H3 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville 8.3 mg/L 1.0 1 07/22/2214:00 14808-79-8 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville ND mg/L 0.10 1 07/26/2213:02 7664-41-7 Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 10.8 mg/L 0.20 5 07/20/22 23:56 14797-55-8 Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville 0.074 mg/L 0.050 1 07/25/22 17:46 07/25/22 21:23 7723-14-0 Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville 402 mg/L 20.0 20 07/22/2215:38 16887-00-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 25 aceAna'1XJca1 11 www.pacelabs.com ANALYTICAL RESULTS Project: Sprayfield Well Pace Project No.: 92615936 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-2 Lab ID: 92615936002 Collected: 07/20/22 16:20 Received: 07/20/22 18:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310E TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services - Asheville Total Organic Carbon ND mg/L 1.0 1 07/21/22 21:35 744044-0 Date: 08/02/2022 05:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 25 Document Name; Field data Sheet Date leeued: March 8, 2019 �. C9 MWlj�dAEAl' Page: 1 of Document Number. KAR-FLD-001-rev.03 issuing Authority: Pace Huntersvtfle Quality, tom, Name alid Affiliation (Sampler(s); Name -and Affiliation (Inspector):_ , Ilt Well Information Well ID: Well Diameter: Total Well Depth: 2 � 3 t Static Water Gevel:.J, �ft Height of Water Columnft Office . Field Data Sheet Review: Date:.? - 2- (' . 2Z By C-c- (, Well.Locked: �,9/ NO / Flushmount ) Construction: 9!0�lSteel/Stainless Steel) Multi Factor'': 0. 653 r(Radius/12)2 x 3.11 ii 7,48). Casing Volume: _�_ gallons Cal. 3 Voluines: aa. goons Pump Intake: 2 ft Purge Information Date Purgers/�/�L Start: 13 ph 13 Purge hate: Purging Method: Total Volume'Purged: •� gallon /tn]s/L) Sapling Information Date Collectied:_. 17 ` T� Coy�ed:,���pm) �G; � 1 ' Sampling topment Used: ty� ^Instrument ID:- '� �?` � 3, (,, Bottle Type Preservation R GV wt E Me.►&A��n��r�t�,'O�� e:=ua lions Analysis Required Sample Temp (°C): 1 �S, _" _Time: 1 l .3� Turbidity (�); — Time'." — Dias OXY (I.g/L): Time: Pa 2+m L g/ • Time: Specific Cond. (u5): 1 �G 4� Time ,_ I G QRes. Cl (mg/Ly(ug/L): Tirne:. Sautple pH (s.u.): Time: 11,30� Od'or: N Time Rebox (mV); ^ ' Time: - Appearance: r",Y-4 Time: )��p ReDox (EH value):YSI ProPlus +2o0mV Other: Time: General/Weather Observations:. W1,1A) /rainy) Temp._Y0LrF) WJmdRt&_(mph) Sampler Sign Stabilization o N®R ON aceAnalytical www.pacolobs.com i ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: SPRAYFIELD WELL Pace Project No.: 92616227 Sample: MW-3 Lab ID: 92616227001 Collected: 07/21/22 11:30 Received: 07/21/22 17:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by PACE 1 08/01/22 09:40 Collected By JQ 1 08/01/22 09:40 Collected Date 07/21/22 1 08/01/22 09:40 Collected Time 11:30 1 08/01/22 09:40 pH 7.1 Std. Units 1 08/01/22 09:40 Temperature 18.9 deg C 1 08/01/22 09:40 Static Water Level 15.81 feet 1 08/01/22 09:40 Specific Conductance 1949 umhos/cm 1 08/01/22 09:40 Total Well Depth 27.31 feet 1 08/01/22 09:40 Odor None 1 08/01/22 09:40 Appearance Murky 1 08/01/22 09:40 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms ND CFU/100 mL 1.0 1 07/21/22 18:05 07/22/22 17:41 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services - Asheville Total Dissolved Solids 1220 mg/L 50.0 1 07/26/22 10:53 4500H+ pH, Electrometric Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville pH at 25 Degrees C 7.4 Std. Units 0.10 1 07/28/22 13:20 H3 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Asheville Total Nitrogen 4.0 mg/L 0.040 1 07/30/22 17:18 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 106 mg/L 3.0 3 07/24/22 08:40 14808-79-8 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Ammonia ND mg/L 0.10 1 07/26/22 14:15 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total NO mg/L 0.50 1 07/26/22 16:09 07/27/22 02:49 7727-37-9 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate 3.6 mg/L 0.040 1 07/22/22 01:24 14797-55-8 Date: 08/01/2022 05:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 34 11ceAna'Iyfical www.pacelabs.com I ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: SPRAYFIELD WELL Pace Project No.: 92616227 Sample: MW-3 Lab ID: 92616227001 Collected: 07/21/22 11:30 Received: 07/21/22 17:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus ND mg/L 0.050 1 07/25/22 17:46 07/25/22 22:14 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 474 mg/L 20.0 20 07/29/2213:25 16887-00-6 5310E TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services - Asheville Total Organic Carbon ND mg/L 1.0 1 07/25/22 17:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/01/2022 05:42 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 34 Document Name: Field data Sheet Date Issued-Mnrcti 8, 2019 �. CBAnafygcaf' Page: 1 ofJ Document Number. F-qAR-FLD-001-rev.03 E�& Authority: Pace Hunteryvine Quality. _1:Office . NamQ and AfiIiation (Sampler(s):—T9Q/e r -L f Name and Affiliation (Inspector): /�l y�— Well Information Well ID: , &W— 5 Well Diameter: —_ a -- Total Well Depth: ! . • 0 ft Static Water Level: l ..�a� -ft Height of Water Column:41 ft Well Locked: Field Data Sheet Review: 'l1a--1 f�Z Y '3- Date: -7 --z Q �z By: G C C ES 0 / FIushmount ) Construction: JG/Steel/StainlessSteel) Multi r(Radfus/12)2 x 3.14 z 7,481. Casing Vo)ume:� gallons. Cal. 3 Volumes: , 3 gallons Pump intake/� Et Purge Information Date Purged: D�_ b1Q ./ as Start:_ Finishes Purge hate: Purging Method: Total Volume'Purged: S� ( lib mis L Sampling Infoxmation Date Collected:. Q /ap jam_ Time Collected—_ ( /Ig Sampling 9quipment Used: 80- -t v, Instrument ID:_ Y 6•'r-'A` 39 6 Bottle Type Preservat4n Analysis Required G 1as 1�SUy Jigs Sample Teutp (°C); �� • Time:_ (n p ()Turbidity (ntu): Time: Dins Oxy (mg/L): Time: '� Fe 2+ mg/L. —Time- Specific Cond. (uS�: JG Time l_lp o l7 Res. CI (mg/Lu(Rg/L). SamplepH(s.u•): Time:'Odor ._. IU-b-nP Time: t(600 ReDox (ntV): Time: Appearance: ►wwrK Time: 1(0 0 O ReDox (EH value):YSI ProPlus +200mV Other: Time: General/WeatherObservations:Vh W- 5 suns cloudy/rainy) Temp.- (CF) Wmd 5�b1o(mph) AS Sampler Signature Stabilization Tao .70r, Time Purged Temp. (°C) Disc Oxy. ' (mg/L) Spec Cond.( PH (s.u.) ReDox m (� o ume Turbidity r - ved ntu ( ) ( o Water level (ft) Other JA �- U—Wk aceAnalytical www.pacelabs.com i ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Sprayfield Well Pace Project No.: 92615936 Sample: MW-5 Lab ID: 92615936003 Collected: 07/20/22 16:00 Received: 07/20/22 18:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by PACE 1 08/01/22 09:38 Collected By JJQ 1 08/01/22 09:38 Collected Date 07/20/22 1 08/01/22 09:38 Collected Time 16:00 1 08/01/22 09:38 pH 6.7 Std. Units 1 08/01/22 09:38 Temperature 18.6 deg C 1 08/01/22 09:38 Static Water Level 10.64 feet 1 08/01/22 09:38 Specific Conductance 2275 umhos/cm 1 08/01/22 09:38 Total Well Depth 29.63 feet 1 08/01/22 09:38 Odor None 1 08/01/22 09:38 Appearance Murky 1 08/01/22 09:38 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 1.0 CFU/100 mL 1.0 1 07/20/22 18:49 07/21/22 17:00 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids 1310 mg/L 50.0 1 07/25/22 12:02 4500H+ pH, Electrometric Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville pH at 25 Degrees C 7.0 Std. Units 0.10 1 07/22/22 15:20 H3 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville Sulfate 28.8 mg/L 1.0 1 07/22/2214:16 14808-79-8 360.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia NO mg/L 0.10 1 07/26/22 13:06 7664-41-7 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Nitrate 0.041 mg/L 0.040 1 07/20/22 23:46 14797-55-8 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus 0.11 mg/L 0.050 1 07/25/22 17:46 07/25/22 21:23 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville Chloride 340 mg/L 20.0 20 07/22/2215:39 16887-00-6 Date: 08/02/2022 05:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 25 1�?(ceAna'lyfical@ / www.pacelabs.com i ANALYTICAL RESULTS Project: Sprayfield Well Pace Project No.: 92615936 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-5 Lab ID: 92615936003 Collected: 07/20/22 16:00 Received: 07/20/22 18:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310E TOC Analytical Method: SM 531OB-2014 Pace Analytical Services - Asheville Total Organic Carbon 1.8 mg/L 1.0 1 07/21/22 22:25 7440-44-0 Date: 08/02/2022 05:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 25 C6Afi!l44ca'f� Document Name: Field data Sheet Document Number. F-CAR-FLD-001-rev.03 yr r Feld Data Clii�nE Y h il!u'—P1a v Locaawn: r Namrs and Affiliation (SamPler(s):`— Name and Affiliation (Inspector}:_. a�� WellIni=ormatien W/" ell lD: ► k-W:-kO Well Diameter: t( -- Total Well Depth: !szsL _ft Static Water Level: Height of Water Column: S2 Lft Date Issued Math 8, 2019 Pant: 1 of Data Sheet Review: Dabs WV �� -7.z_q_7--4- Well Locked: `( ' / NO / Fluslunount ) Construction Steel/Stainless Steel) Multi Factor'`: o + C�3 ['(Radius/12)2 x 3.14 ii 7A). Casing Volume: _ _- gallons. Cal. 3 Volumes: 17. 1 gallons Office . . V-y� By, 444; Ls Pump Intake: Intake:_ Purge Iltformati'on Date Purged: O. / _/ 2� Start :-1-� 1 Fuush: Puge Rate: it q��l Purging Method: -04" vTot21 Volume'Purged: g � . (onon/mjs/p Sampling Information Date Collected:. I - ff Time Collected:�b (am ` ' Sampling Equipment Used: a k-L, Instrument ID:_�� = �� Bottle Type Preservati6n Analysis Required aetvationsIP1411i, Sample Teulp (°C): �_TyII1Q; l Turbidity (ntu): Timer Digs Oxy (>n$/L): Time: Fe 2+mb/L: Time: Specific Cond. (US): a O Time: j4A6—Res. Cl (mg/LU(µg/L)--Time: . Sample pH (s-u.): Tune: ' 14.416 Odor. ... 11%D NET iteDox (mV): Time: Appearance: Time: ,{ ReDox (EH value):YSI FroPlus +200mV Other �! Time: General/Weather Observations:. (sunn clou /rainy) Temp.('F) Wind5iblo (mph) Sampler Signature: Date: -VA '&A JIPI ' Stabilization Test D. . . d► MMA I: M aceAnalyticale / www.pacelabs.com I ANALYTICAL RESULTS Project: SPRAYFIELD WELL Pace Project No.: 92616227 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-6 Lab ID: 92616227002 Collected: 07/21/22 14:45 Received: 07/21/22 17:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Performed by Collected By Collected Date Collected Time pH Temperature Static Water Level Specific Conductance Total Well Depth Odor Appearance MBIO 9222D Fecal Coliform CHT Fecal Coliforms 2540C Total Dissolved Solids Total Dissolved Solids 4500H+ pH, Electrometric pH at 25 Degrees C Total Nitrogen Calculation Total Nitrogen 300.0 IC Anions 28 Days Sulfate 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate Date: 08/01/2022 05:42 PM Analytical Method: Pace Analytical Services - Charlotte PACE 1 08/01/22 09:42 JQ 1 08/01/22 09:42 07/21/22 1 08/01/22 09:42 14:45 1 08/01/22 09:42 6.6 Std. Units 1 08/01/22 09:42 18.3 deg C 1 08/01/22 09:42 9.81 feet 1 08/01/22 09:42 200 umhos/cm 1 08/01/22 09:42 45.02 feet 1 08/01/22 09:42 None 1 08/01/22 09:42 Murky 1 08/01/22 09:42 Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte 4.0 CFU/100 mL 1.0 1 07/21/22 18:05 07/22/22 17:41 Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville 147 mg/L 25.0 1 07/26/2210:53 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services -Asheville 7.4 Std. Units 0.10 1 07/28/22 13:35 H3 Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville ND mg/L 0.040 1 07130/2217:18 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville 9.0 mg/L 1.0 1 07/23/2217:13 14808-79-8 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville NO mg/L 0.10 1 07/26/2214:16 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville ND mg/L 0.50 1 07/26/22 16:09 07/27/22 02:50 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville ND mg/L 0.040 1 07/22/22 01:34 14797-55-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 34 aceAnalytical J www.pacolabs.com I( ANALYTICAL RESULTS Project: SPRAYFIELD WELL Pace Project No.: 92616227 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-6 Parameters Lab ID: 92616227002 Collected: 07/21/22 14:45 Results Units Report Limit DF Received: 07/21/22 17:35 Matrix: Water Prepared Analyzed CAS No. Qual 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 0.34 mg/L 0.050 1 07/26/2217:38 07/27/2218:20 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville Chloride 17.0 mg/L 1.0 1 07/29/2213:26 16887-00-6 5310E TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services - Asheville Total Organic Carbon ND mg/L 1.0 1 07/25/22 18:16 7440-44-0 Date: 08/01/2022 05:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 34 Document Name; Field data Sheet Dafa [sewed Man h 8, 2019 �eft/k9f}l;l' Pa : 1 of Document hlwmber. F-CAtt-Fi D oOi-rev.03g Authority Pace HuntersvLle Quality. -- Office . t Name acid Amlii;tion (Sampler(s): T Name -and Affiliation (Inspector): . N IN - Well Inforrnation Well ID: M Well Diameter: o� Total Well Depth: 3 f-i� ft Static Water Level:ft Height of Water Colunuu:3,,?4.Et Well Locked: As L Field Data Sheet Review: ' Date: 7 Br G-Z G- NO / Flushmount ) Consttuctiion: ?Steel/Stainless Steel) Multi Faotor': Q-1 a r(Radius/12)2 x 3.14 i 7.48). Casing Volume:, . 2 gallons. CaL 3 Volumes: S ganons Pump Intake: PurLre Inforinati'on Date Purged:�/_ a Start jgff Finish �T t Purge Rate: ^ .'1. gyp r✓1 . Purging Method:----*Q�q�(Nifln� Total Volume Purged: I 1 O allo" mis/L) cf . Sampling Infkmation rrJ Date Collected:.b Time Collected:.., Sampling Equipment Used-' 15aA 4m- - Instrument i -361(,p Bottle Type Preservation Analysis Required 3-1/0 h,L'. J'o a At S?XJti►.t$- I -LSD �.-Js+� mil. ddoa/E � CL 1 /�'T'`� Sartuple I stop (°C): _- Time: 15i . Turbidity (ntu): -- me:: �--- Dios Oxy (mg/L): Time: Fe 2+m L: 2 / 'Time': Specific Cond. (u6): Time: --��5�-ell Res. CI (mg/L)/(Ag/L): Time:. Sample pH (s.u.):-. Time: ti Odor Nb of, Time: ReDoz (mV): Time: Appearance: _ YYt k, k 4 Time:_ I S) rJ ReDox (EH value):YSI ProPlus +200mV Other: Time: General/Weather Observations:�- (sunny/ oud rainy) Temp.-'jQ(f) Wind—Q(mph) Sampler Signature: Date: Stabilizdtion'Test Time Purged Temp. (°C) Diss Oxy, (mg/L) Spec' Cond. (US) Hsu P ( ) © o rune ReDox Turbidity reatoved (m� (n) (m)s/ Water Other level (ft) V 5 aceAnalXical / www.pacelabs.com i ANALYTICAL RESULTS Project: SPRAYFIELD WELL Pace Project No.: 92616227 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-7 Lab lD: 92616227003 Collected: 07/21/22 15:15 Received: 07/21/22 17:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by PACE 1 08/01/22 09:43 Collected By JQ 1 08/01/22 09:43 Collected Date 07/21/22 1 08/01/22 09:43 Collected Time 16:15 1 08/01/22 09:43 pH 7.2 Std. Units 1 08/01/22 09:43 Temperature 18.5 deg C 1 08/01/22 09:43 Static Water Level 21.33 feet 1 08/01/22 09:43 Specific Conductance 543 umhos/cm 1 08/01/22 09:43 Total Well Depth 53.42 feet 1 08/01/22 09:43 Odor None 1 08/01/22 09:43 Appearance Murky 1 08/01/22 09:43 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 4.0 CFU/100 mL 1.0 1 07/21/22 18:14 07/22/22 17:46 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Asheville Total Dissolved Solids 314 mg/L 25.0 1 07/26/22 10:53 4500H+ pH, Electrometric Analytical Method: SM 4500-H+B-2011 Pace Analytical Services -Asheville pH at 25 Degrees C 7.5 Std. Units 0.10 1 07/28/22 13:43 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 0.27 mg/L 0.040 1 07/30/22 17:18 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 6.5 mg/L 1.0 1 07/23/2217:32 14808-79-8 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Ammonia ND mg/L 0.10 1 07/26/22 14:20 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total ND mg/L 0.50 1 07/26/22 16:09 07/27/22 02:51 7727-37-9 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Nitrate 0.27 mg/L 0.040 1 07/22/22 01:37 14797-55-8 Date: 08/01/2022 05:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. D6 H3 Page 9 of 34 1�;a'ce Analy'fical www.pacelabs.com i ANALYTICAL RESULTS Project: SPRAYFIELD WELL Pace Project No.: 92616227 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-7 Lab ID: 92616227003 Collected: 07/21/22 15:15 Received: 07/21/22 17:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus ND mg/L 0.050 1 07/26/2217:38 07/27/2218:20 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 33.8 mg/L 1.0 1 07/29/2213:29 16887-00-6 5310B TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 07/25/22 19:04 7440-44-0 Date: 08/01/2022 05:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 34 Document Name: Field data Sheet ce.�/kil{eS%' Document Number.. XCAR-FLD-001-rev.03 lr ata Client V ��VV9 Location:' h Name arid Aff tion (Sar pler(s): Name and Affiliation {Inspector): . wA - Well Information Well tD: . h�WJ g Well Diameter: . 9 it -- Total Well Depth: a ft Static Water Level:_ r �?JF ft Height of Water Column:a�(t Well Locked: Office . Field Data Sheet Review: ' Date: ��q,�-2. P// NO / Flushraount ) Construction MO/Steel/Stainless Steel) Multi Factor*: o -.1 W (+(Fadius/12)2 x 3.14 i7"j. Casing Volume: 3 • �� gallons Cal. 3 Voluines: '= (� - gallons Pump Intake: A CA ft Purge I'nfoxination Date Purpd:--P-T-/'10. ./ � . Start 1 ;Finish /5.30 Purge Rate: Purging Method: Tota1 Volume'Purged: anon /mis/L) SaaialingInformation Drys Date Collected:_ Time Collected:-P�_ ( / Sampling Equipment Used:-__ L \` 1 to Ins moment ID: Y6T- *3St b Bottle Type he:servatipn -v►.L V 6A. Analysis Required 40 - _ 1 w\ D /_-�L� L ! ,�5a► T�-i�b�,.Q. /VbN13 CL-- SO Sample Temp (°C): aU Time:lalD -Turbidity (ntu): Time —� Digs OxY (mg/L)- Time: Fe 2+ mg/L: Time: Specific Cond. (u6): Time:, 1 �40 . Res. C1(mg/L)I(µg/4"-' T=e:. Sample pH (s.u.): %r • Time: Odor: _ j� ' Time; ReDox m: '�' pp K Time:_ 1 a Q _ ( Time: A earance: stir ReDox (FH value):YSI ProPlus +200mV Other: Time: General/Weather Observations:. m ji , satin cloudy/rainy) Temp.CF) Wmd...%ZQ(mplt) Sampler Signature Stabilization Test Time I' urged( Temp. ) Digs Oxy, (mg/L) Spec. Cond.pH (US) (s.u.) ReDox (mV) ume Turbidity removed (nm) ,/MIS/ Water level (R) Other JA :. .. _ 1. y aceAnaiytical 1,' www.pacslabs.com i ANALYTICAL RESULTS Project: SPRAYFIELD WELL Pace Project No.: 92616227 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-8 Lab ID: 92616227004 Collected: 07/21/22 12:40 Received: 07/21/22 17:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Performed by Collected By Collected Date Collected Time pH Temperature Static Water Level Specific Conductance Total Well Depth Odor Appearance MBIO 9222D Fecal Coliform CHT Fecal Coliforms 2640C Total Dissolved Solids Total Dissolved Solids 4500H+ pH, Electrometric pH at 25 Degrees C Total Nitrogen Calculation Total Nitrogen 300.0 IC Anions 28 Days Sulfate 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate Date: 08/01/2022 05:42 PM Analytical Method: Pace Analytical Services - Charlotte PACE 1 08/01/22 09:44 JQ 1 08/01/22 09:44 07/21/22 1 08/01/22 09:44 12:40 1 08/01/22 09:44 6.8 Std. Units 1 08/01/22 09:44 20.7 deg C 1 08/01/22 09:44 5.65 feet 1 08/01/22 09:44 634 umhos/cm 1 08/01/22 09:44 29.60 feet 1 08/01/22 09:44 None 1 08/01/22 09:44 Murky 1 08/01/22 09:44 Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte ND CFU/100 mL 1.0 1 07/21/22 18:05 07/22/22 17:41 Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville 430 mg/L 25.0 1 07/26/2210:53 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 7.2 Std. Units 0.10 1 07/28/22 13:31 H3 Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville ND mg/L 0.040 1 07/30/2217:18 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville 9.5 mg/L 1.0 1 07/23/2217:51 14808-79-8 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville ND mg/L 0.10 1 07/26/2214:22 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville ND mg/L 0.50 1 07/26/22 16:09 07/27/22 02:52 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville ND mg/L 0.040 1 07/22/22 01:32 14797-55-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 34 aceAnalyiical j www.pacolabs.com i ANALYTICAL RESULTS Project: SPRAYFIELD WELL Pace Project No.: 92616227 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-8 Lab ID: 92616227004 Collected: 07/21/22 12:40 Received: 07/21/22 17:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 0.070 mg/L 0.050 1 07/26/2217:38 07/27/2218:23 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville Chloride 104 mg/L 5.0 5 07/29/2213:30 16887-00-6 5310E TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 07/25/22 19:24 7440-44-0 "Date: 08/01/2022 05:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 34 Document Name: Field date Street Dare Issued: March a, 2019 1. CBRRlfll�i4tE$l� Pap. 1 of ! Document (Number. ILCAR-PLD-001-rev.o3 Ewing Authority: Pace Huntemvilk — -. Office . Pf, r (" Name emd AfSliation (Sampler(s): — Name and Affiliation (Inspector): Well Information WeU ID: . VA W— � Well Locked: Well Diameter: - _ -. a 4 Total Well Depth: Q ft Static Water Level: i. t% ' ft Height of Water Column:/ dd Data Sheet Review: Date: ?/�•�'"`Z BT.1� NO / Flushmount ) Construction: - /Steel/StEdnIessSteeI) Multi Factor*: Q� 3 [»(gadius/12J2x 3.34 ii 7.48]. Casing Volume:��, /��■y-- gallons. Cal. 3 Volumes: (J Y 1 gallons Pump Intake: tm a Ihfaiinatiun Date Purge'd:�/� . / _ StarE �.. Finish)-purgeRate:� Purging Method: CMG t dl✓ Total Volume'Purged: J gaIlo s/mis/L) Sampling Information Date Collected: D a '2. �--� Time Collected: 06 Sampling Equipment Used.- Ci t L+r Instrument M.(� �p B'I W15 ott a T ype Preservation Analysis Required '�fa trQ Jo q Aq-c A-C l j � -smL AlAnlr S o3`P Sample Ternp (oq- Time: l J� Turbidity (ntu): Time Dins Oxy (Iftg/L): Time: Fe 2+ m L: 8/ Time: Specific Cond. (uS): 9—(Q �2 Time: Res. Q (mS/LU(l,g/L)--Time•. Sautple pH (S-u.): Le Time: [ Od'or: /l/ Q1i,,0 ,Time; ReDox (mV): Time f Appearance: r TIme:_ 1�05 ReDox (EH value):YSI ProPlus +20omV Other: Time: '�� General/4Veather Observations.. m.(� (sunny on /rainy) Sampler Signature Stabilization Test (OF) WindN /Ze(mph) al a �2 Time Purged Temp. ( q Diss Oxy. (mg/L) Spec' C Sd' ( ) PH (s.u.) ReDox m ( V) ume Turbidity moved (nta) mis/ Water level (ft) Other I e7 /� a /L 1 1 • O .� i� .�`� aceAnalXical lwww.paceiabs.com Project: SPRAYFIELD WELL Pace Project No.: 92616227 Sample: MW-9 Parameters Monitoring Well Data Performed by Collected By Collected Date Collected Time pH Temperature Static Water Level Specific Conductance Total Well Depth Odor Appearance MBIO 9222D Fecal Coliform CHT Fecal Coliforms 2540C Total Dissolved Solids Total Dissolved Solids 4500H+ pH, Electrometric pH at 25 Degrees C Total Nitrogen Calculation Total Nitrogen 300.0 IC Anions 28 Days Sulfate 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate 'Date: 08/01/2022 05:42 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Lab ID: 92616227005 Collected: 07/21/22 12:05 Received: 07/21/22 17:35 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: Pace Analytical Services - Charlotte PACE 1 08/01/22 09:45 JQ 1 08/01/22 09:45 07/21/22 1 08/01/22 09:45 12:05 1 08/01/22 09:45 6.8 Std. Units 1 08/01/22 09:45 17.9 deg C 1 08/01/22 09:45 11.70 feet 1 08/01/22 09:45 1866 umhos/cm 1 08/01/22 09:45 29.36 feet 1 08/01/22 09:45 None 1 08/01/22 09:45 Murky 1 08/01/22 09:45 Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte ND CFU/100 mL 1.0 1 07/21/22 18:05 07/22/22 17:41 Analytical Method: SM 2540C-2015 Pace Analytical Services - Asheville 1050 mg/L 50.0 1 07/26/2210:53 Analytical Method: SM 4500-H+6-2011 Pace Analytical Services - Asheville 7.2 Std. Units 0.10 1 07/28/22 13:27 H3 Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville 0.79 mg/L 0.040 1 07/30/2217:18 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 26.6 mg/L 1.0 1 07/23/2218:10 14808-79-8 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville ND mg/L 0.10 1 07/29/22 08:31 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville ND mg/L 0.50 1 07/26/22 13:22 07/27/22 03:45 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville 0.54 mg/L 0.040 1 07/22/22 01:30 14797-55-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 34 �2ce Analytical iwww.pacelabs.com I ANALYTICAL RESULTS Project: SPRAYFIELD WELL Pace Project No.: 92616227 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-9 Lab lD: 92616227005 Collected: 07/21/22 12:05 Received: 07/21/22 17:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus 0.054 mg/L 0.050 1 07/26/2217:38 07/27/2218:23 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville Chloride 501 mg/L 20.0 20 07/29/2213:31 16887-00-6 5310B TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services - Asheville Total Organic Carbon ND mg/L 1.0 1 07/25/22 19:41 7440-44-0 gate: 08/01/2022 05:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 34