WQ0033677_Monitoring - 07-2022_20220823

FORM: NDMR 08-11 NON -DISCHARGE MONITORING REPORT (NDMR) Page L of
Permit No.: 'WQ0033677
Facility Name: CASE FARMS HATCHERY
County: Burke
Month: July
Year: 2022
PPI: 001
Flow Measuring Point: El Influent ❑ Effluent ❑ No flow generated
Parameter Monitoring Point: ❑ influent ❑ Effluent ❑ Groundwater Lowering El Surface Water
Parameter Code -►
"
""LL
00400 00310
0060
31616
00940
00y094
70300
55)050
0rY06=25 0066
p
2
U Hm
~c
10
=
G
m
o
E
�
(n n
LL O
?
Nf
Z
1
rE
Ho.
N
1 F_
1
24-hr
4:00
hrs
12
GPD
t 7,700. .V
su mg/L
mg/L
mg/L
#1100 mL
mg/L
po
mg/L
„, ,g/L
mg/L mg/L
2
7,500;
7,52Mj
3
7:00
5
4
5:00
10
7
5
5:00
13
6
4:00
4
13
7,500<;
7
5:00
8
5:00
13
7,50044
7
9
7,500 `
10
4:00
6
1 7,500
t`
11
5:00
12
7,5001V
7.1
12
5:00
11
7,500 ;
13
5:00
5.5
7,5004 1249
31.26
1080
>1360
84
1529
344
39 2,' 5.84
14
5:00
10.5
7,500-
15
5:00
10.5
7,5Q;
16
7k
17
5:00
6
11.5
7,5
7,500.. 6.8
e
18
5:00
19
5:00
10
7,5001,,
20
6:00
7
? 7,500
21
5:00
10.5
7,500<'
22
5:00
9.5
7.500 ,
_
23
7,500
,
24
5:00
5
7,500
1a-
25
5:00
12
11.5
7,500:: `
7.3
26
5:00
7,500--1
27
6:00
9.5
7,500
28
5:00
10.5
7,500
29
5:00
11
7,500
-
30
7,500
31
7,500
Average::'
7,506
1,249.00
31.
1,080.00
84.00
1,529.00
344.00
3.22
39.00
42.22 "`
5.84
Daily Maximum:
'' 7,700
7.30 1,249.00
31.2M
1,080.00
84.00
1,529.00
344.00
3.22
39.00
42.22,
5.84
Daily Minimum:
7,500
6.80 1,249.00
31.26
1,080.00
8400
1,529.00
344.00
3.22
39.00
4Z221,15.84
Sampling Type:
,.
Monthly Limit:
7z
8000
Daily Limit:
+`
Sample Frequency:

FORM: NDMR 08-11 NON -DISCHARGE MONITORING REPORT (NDMR) Page a of A
Sampling Person(s)
Name: James Edwards
Name: Cindy McGinnis
Name: Water Tech Labs Inc
Name:
Certified Laboratories
Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? ❑ Compliant ❑ Non -compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification
Permittee Certification
ORC: Cindy McGinnis
Permittee: Case Farms Hatchery
Certification No.: 992943
Signing Official: Cindy McGinnis
Grade: SI Phone Number: 808-438-6900
Signing Officials Title: Hatchery Supervisor
Has the ORC changed since the previous NDMR? ❑ yes 0 No
Phone Number: 828-438-6900 Permit Expiration: 12/31/2021
Signature Date
Z
Signature Date
signature, I certify that this report is accurrate and complete to the best of my knowledge.
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
Mail Original and Two Copies to:
Division of Water Quality
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page-tof
Permit No.: WQ0033677
Facility Name: Case Farms Hatchery
County: Burke
Month: July
Year: 2022
Field Name:
1
Field Name:
2
Field Name:
3 ^
Field Name:
4
Did irrigation occur
at this facility?
❑� YES ❑ NO
Area (acres):
1
Area (acres):
1.13
Area (acres):
1.12 '
Area (acres):
0.96
Cover Crop:
FESCUE
Cover Crop:
FESCUE
Cover Crop:
FESCUE
Cover Crop:
FESCUE
' Hourly Rate (in):
0.23
Hourly Rate (in):
0.27
Hourly Rate (in):
0.24
Hourly Rate (in):
0.2
Annual Rate (in):
29,18 j Annual Rate (in):
29.18
Annual Rate (in):
29.18 4,
Annual Rate (in):
29.18
Weather
Freeboard
Field Irrigated?
YES NO} Field Irrigated?
❑ YES ❑ NO
Field Irrigated?
_ YES NO
Field Irrigated?
❑ YES ❑ NO
m
❑>
$`y
M
O.
E
•
7 W.E
d
Q
E
E d
M
_
pa
E
'
Q
-
J
E
>U
E
cc
ca =oG
E
EE
0 °
J_
E T rncl
oc
= J
°F
in
ft
ft
gal
min
in
in gal
min
in
in
gal
min
in
in _,
gal
i min
in
in
1
C 1
80
2,100
22
008
0.08 2,500
26
0.08
0.08
2,500
26
0.08
0.08 '
2,100
31
0.08
0.08
2
C
82
2,100
22
0.08
0.08i 2,500
26
0.08
0.08
2,500
26
0.08
0.08
3
R
82
0.75
4
R
83
1.5
5
PC
85
2,100
22
0.08
0.08 2,500
26
0.08
0.08
2,500
26
0.08
0.,
2,100
31
0.08
0.08
6
R
83
0.25
i
7
C
86
11.5
2,100
22
0.08
0.08 2,500
26
0.08
0.08
42,500
26
0.08
0.08
2,100
31
0.08
0.08
8
C
85
2,100
22
0.08
0.08 2.500
26
0.08
0.08
2,500
26
0.08
0.08 ;,
2,100
31
0.08
0.08
9
C
84
`2,100
22
0,08
0.08'' 2,500
26
0.08
0.08
2,500
26
0.08
0,08';',
2,100
31
0.08
0.08
10
R
73
1.1
11
CL
80
2,100
22
0,08
0.08 2,500
26
0.08
0.08
2,500
26
0.08
0.08
2,100
31
0.08
0.08
12
C
83
2,100
22
0.08
0.08 2,500
26
0.08
0.08
.2,500
26
0.08
0.08I,
2,100
31
0.08
0.08
13
C
85
2,100
22
0.08
0.08; 2,500
26
0.08
0.08
2,500
26
0.08
0.08 `'
2,100
31
0.08
0.08
14
C
85
13
2,100
22
0.08
0.08 2,500
26
0.08
0.08
2,500
26
0.08
2,100
31
0.08
0.08
15
C
82
2,100
22
0.08
0,08 2,500
26
0.08
0.08
2,500
26
0.08 '`
2,100
31
0.08
0.08
16
C
84
2.100
22
0.08
0.08 2,500
26
0.08
0.08
2.500
26
0.08
0,08`,,,
2,100
31
0.08
0.08
17
C
82
2,100
22
0.08
0.08 2,500
26
0.08
0.08
2,500
26
0.08
0.08',
2,100
31
0.08
0.08
18
R
84
0.25
19
C
85
2,100
22
008
0.08
2,500
26
0.08
0.08
2,500
26
0.08
0.08
2,100
31
0.08
0.08
20
R
82
0.25
21
PC
84
14
2,100
22
0,08
0.08
2,500
26
0.08
0.08
2,500
26
0.08
0.08 ""
2,100
31
0.08
0.08
22
PC
84
2,100
22
0.08
0.0 '
2.500
26
0.08
0.08
2,500
26
0.08
0.08'.
2,100
31
0.08
0.08
23
R
85
2
24
C
87
25
PC
82
771,100
22
0,08
0.08
2,500
26
0.08
0.08
2,500
26
0.08
0,08 ;
2,100
31
0.08
0.08
26
R
84
0.6
27
PC
86
2,100
22
0,08
0,08
2,500
26
0.08
0.08
2,500
26
0.08
0,08
2,100
31
0.08
0.08
28
PC
85
15
> 2,100
22
0.08
0.08
2,500
26
0.08
0.08
2.500
26
0.08
0.08
2,100
31
0.08
0.08
29
C
84
2,100
22
0.08
0.06
2,500
26
0.08
0.08
2,500
26
0.08
0,08;
2,100
31
0.08
0.08
30
PC
83
2,100
22
0.08
0.08
2,500
26
0.08
0.08
•2,500
26
0.08
0.08?
2,100
31
0.08
0.08
31
C
85
2,100
22
0.Q8__
:,:Q.0,
2,500
26
0.08
0.08
?2,500
26
0.08
0,08`',
2,000
31
0.08
0.08
Monthly Loading:
46,200
,, ,
1
55,000
1.79
""
,// '
55,000
1.81
44.COc
-:
1.69
12 Month Floating Total (in):
�,
16.
..
�, �!,
17.63
16.47�1
19.48

FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of 41
Did the application rates exceed the limits in Attachment B of your permit?
El Compliant ❑ Non -Compliant
Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Q Compliant ❑ Non -Compliant
Was a suitable vegetative cover maintained on all sites as specified in your permit? ❑� Compliant ❑ Non -Compliant
Were all setbacks listed in your permit maintained for every application to each permitted site? El Compliant ❑ Non -Compliant
Were all freeboards maintained in accordance with the specified freeboard heights in your permit? 2 Compliant ❑ Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification
Permittee Certification
ORC: Cindy McGinnis
Permittee:
Case Farms Hatchery
Certification No.: 992943
Signing Official: Cindy McGinnis
Grade: SI Phone Number: 828-438-6900
Signing Officials Title: Hatchey Supervisor
Has the ORC changed since the previous NDAR-1? ❑ Yes P] No
Phone Number: 828-438-6900 Permit Exp.: 12/31/21
Signature Date
Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge.
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Mail Original and Two Copies to:
Division of Water Quality
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

I
mivrmirrCH Lfifffflnc,
POST OFFICE 130; 1056 , #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH OAROLINA 28630
[phone]
SAMPLE: Case Farms -Hatchery COLLECTION DATE:
7/13/2022
PERMIT#: COLLECTION TIME.,
14:30
ADDRESS: Case Farms Hatchery RECEIVED DATE:
7/13/2022
RECEIVED TIME.
14:30
REPORTED.'
8/4/2022
/S
ANALY SJJ
ANALYSIS
EFFLUENT
UNITS''
------ --- - ------ -
DATE
IANALYST
BOD
1,249
mg/L
7/14/22
jdg
TSS
1,080
mg/L
7116/22
j rg
NH3
31.26
mg/1-
7/15/22
jrg
Fecal Collform
>1360
/100rnL
7/13122
Th
Conductivity
1,529
umhos/cm
7/18/22
Th
NO3-N
3.22
rnglL
7/19/22
jsg
TKN
39.00
mg/L
7/18/22
jdg
T. Nitrogen
42.22
mg/L
7119/22
jdg
T. Phosphorus
5.64
mg/L
7/21122
jdg
Chloride
pace
TDS
pace
7. 71,wi7'
-7
LOG ID: 2207-161 REPORTED BY: NC CERTIFIED LAB # 50

Pace Analytical Services, LLC
1377 South Park Drive
,�aceAnalj4ical Kerners ille,South
Park
Drive
7284
www.pace]abs.com
[phone]-
ANALYTICAL RESULTS
Project CASE FARMS
Pace Project No.: 92614958
Sample: CASE FARMS EFFLUENT Lab ID: 92614958004 Collected: 07/13/22 14.30 Received: 07/14/22 10:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
Total Dissolved Solids 344 mg/L 100 1 07/17/22 14:14
4500 Chloride Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride 84.0 mg/L 3.0 3 07/22/2214:37 16887-00-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/29/2022 04:56 PM without the written consent of Pace Analytical Services, LLC Page 7 of 28
i

Method SM 20 Ed 4500-H-2011
PH WORKSHEET
Analysis
Date Time
Collection
Sam le ID Date Time
Results SU's
Analyst
Z
Buffer 4.00 *****
*****
Buffer 10.00
t
S
Buffer 7.00 QC *****
*****
� Ob
*****
Slope Efficiency *****
*****
1.3 05—
uJ 3
c-
H WLP
v
K W
l La
c? J
P
. rs-
C
7. p
BUFFERS:
4.00 LOT # 8111363
7.00 LOT # 8110554
10.00 LOT # 8109645
* NON REPORTABLE
FOR NPDES
EXP NOV 2023
EXP NOV 2023
EXP OCT 2023
Water Tech Labs
PO Box 1056
-5 Pinewood Pie= Dave
Granite Fallh, NC 28630

firm recH t085,Inc.
POST OFFICE 80; 1056 - #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE., Case Farms-Hatchery-MW#3 COLLECTION DATE: 7/13/2022
PERMIT #: COLLECTION TIME: 13:00
ADDRESS: Case Farms Hatchery RECEIVED DATE: 7/13/2022
RECEIVED TIME: 14:30
REPORTED: 8/4/2022
ANALYSIS
- -
-
ANALYSIS
RESULTS
UNITS _
DATE
ANALYST
TDS
pace
NH3
<1.0
mg/L
7/15/22
jrg
Fecal Coliform
<1
/100ml-
7/13/22
Th
Metals
pace
NO3-N
3.00
mg/L
7/19/22
jsg
TKN
<1.0
mg/L
7/18/22
jdg
T. Nitrogen
3.00
mg/L
7/19/22
jdg
T. Phosphorus
0.19
mg/L
7/21/22
jdg
Chloride
pace
i...
:?.1 T
F
..; :. ..
.. .. .
LOG ID: 2207-162 REPORTED BY: NC CERTIFIED LAB # 50

,�aceAnalvfical
www.pacelabs.com
ANALYTICAL RESULTS
Project. CASE FARMS
Pace Project No : 92614958
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Sample: CASE FARMS MW3
Parameters
Lab ID: 92614958001 Collected: 07/13122 13:00
Results Units Report Limit OF
Received: 07/14/22 10:45 Matrix: Water
Prepared Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method. EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Arsenic
NO mg/L
0.010
1
07/19/22 11:24
07/20/22 21:46
7440-38-2
Barium
0.055 mg/L
0.0050
1
07/19/2211:24
07/20/2217:31
7440-39-3
Copper
NO mg/L
0.0050
1
07/19/2211:24
07/20/2217:31
7440-50-8
Iron
NO mg/L
0.050
1
07/19/2211:24
07/20/2217.31
7439-89-6
Manganese
NO mg/L
0.0050
1
07/19/2211:24
07/20/2217:31
7439-96-5
Potassium
NO mg/L
5.0
1
07/19/2211:24
07/20/2217:31
7440-09-7
Sodium
7.6 mg/L
5.0
1
07/19/2211:24
07/20/2217:31
7440-23-5
Zinc
NO mg/L
0.010
1
07/1912211:24
07/20/2217:31
7440-66-6
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
90.0 mg/L
25.0
1
07/17/22 14:14
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
15.1 mg/L
1.0
1
07118/2212:21
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services - Asheville
Total Organic Carbon NO mg/L 1 0 1 07/19/22 19:12 7440-44-0
Date: 07/29/2022 04:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 28
'r-

erit ch, 111Cm
Eovironmerital Laboratory
Laboratory Certiflcatkon No.165
Contact;: Gathy:Grag�
Client 'Water Tech Labs, Ine RPPQrt Date: 7/25/2022
5` P166*60- d Plaza -Drive
Gra4 to Fafj$, NC 28630 Date Sample 4Ov
/4gQ�2.
Mert%ch`Work. :ter# (3l2¢ :Satktpe,..:e.anms-114W#3+rab -
7/13/22
1'ar'amet
#nakysisb—at P Renorting`Lim`it
WAS (as LAS 340) -�:O # Ing/L U;1:o ng/h $Mt54Ii.0
Merifech'Wotk.order.# 07142207 Sample: ase
�� 3f22
a a"ete s
Rauh �t�aIv§isDa�P ,�e,.porting'Limit
�tsAs (as 1AS 40) <020 mg/L-/1412z OAP mWL s�<
MOdt*6 Work,Offer # .07142208 Sariigle; base l: r s - Wilt b 7/
�� Z3 2z
Ntaffide Iffadt is:Date
n --
IV(M (as IAS 340) <0:10 CL 7/14/22. 0.10 *g/L SM 5540;C.
I hereby certify that 1 have reviewed and approve these data. 4�� /4 Z��
La OratOryRepresents ve
642 TaMco Road, Reidsville, North Carolina 2732.0
tel,[phone] tax.[phone]

Analytical Environmental Services, Inc
Date: 21-Jul-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
CASE FARMS MW3
Project Name:
92614958
Collection Date:
7/13/2022 1:00:00 PM
Lab ID:
2207F49-001
Matrix:
Aqueous
Analyses xepornng Dilution
Y Result Qua] Units BatchID Date Analyzed Analyst
Limit
Factor
Formaldehyde by SW8315A
Formaldehyde BRL 50 ug/L 339642 1 07/18/202212:35 CM
Qualifiers: r Value exceeds maximum contaminant level
B Estimated (value above quamitation range)
BRL Below reporting limit
S Spike Recovery outside limits due to matrix
H Holding times for preparation or analysis exceeded
Narr See case nornrtive
N Analyre not NBLAC certified
F Analyzed in the lob which Is s deviation @tan the method
B Analyte detected in the associated method blank
< Less than Result value
> Greater than Result value
I Bstimated value detected below Reporting Litnil
n..,.,, n -V t t

WfirrRilrECH LH85,Inc,
s
POST OFFICE 80X 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE: Case Farms-Hatchery-MW#4 COLLECTION DATE: 7/13/2022
PERMIT #: COLLECTION TIME: 14:00
ADDRESS: Case Farms Hatchery RECEIVED DATE: 7/13/2022
RECEIVED TIME: 14:30
REPORTED: 8/4/2022
ANALYSIS
ANALYSIS
RESULTS
UNITS
DATE
ANALYST j
TDS
pace
NH3
<1.0
mg/L
7115/22
jrg
Fecal Coliform
<1
1100ml-
7/13/22
Th
Metals
pace
NO3-N
4.53
mg/L
7/19/22
jsg
TKN
<1.0
mg/L
7118/22
jdg
T. Nitrogen
4.53
mg1L
7119122
jdg
T. Phosphorus
<0.16
mg/L
7/21122
jdg
Chloride
pace
-'•r;-§--•-+'i"7:t, �^�^--
•'�-'r.:--,'--�'..- -�.nv,-,*.,:,+r:;� - --ma's ---•;_..
t: '
- �--:'*':—• - -
LOG ID: 2207-163 REPORTED BY: NC CERTIFIED LAB # 50

Pace Analytical Services, LLC
1377 South Park Drive
��aeAnalytical www.pacelahs.com Kernersvilie, NC 27284
[phone] -
ANALYTICAL RESULTS
Project: CASE FARMS
Pace Project No. 92614958
Sample: CASE FARMS MW4
Lab ID: 92614958002 Collected.
07/13/22 14:00
Received: 07/14/22 10:45 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method. EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Arsenic
ND mg/L
0.010
1
07/19/22 11:24
07/20/22 21:51
7440-38-2
Barium
0.084 mg/L
0.0050
1
07/19/2211:24
07/2012217:34
7440-39-3
Copper
ND mg/L
0,0050
1
07/19/2211:24
07/20/2217:34
7440-50-8
Iron
0.16 mg/L
0.050
1
07/19/2211:24
07120/2217:34
7439-89-6
Manganese
0.016 mg/L
0.0050
1
07/19/2211:24
07/20/2217:34
7439-96-5
Potassium
ND mg/L
5.0
1
07/19/2211:24
07/20/2217:34
7440-09-7
Sodium
8.8 mg/L
5.0
1
07/19/2211:24
07/20/2217:34
7440-23-5
Zinc
ND mg/L
0,010
1
07/1912211:24
07/20/2217:34
7440-66-6
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
Total Dissolved Solids
106 mg/L
25.0
1
07/17/22 14:14
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
18.2 mg/L
1.0
1
07/18/2212:22
16887-00-6
5310E TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services - Asheville
Total Organic Carbon
ND mg/L
1.0
1
07/19/22 19:31
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/29/2022 04.56 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 28

(Onbitt;,- Cathy rragg
Climb Water.T.ech LOk, We
5- NOW66d Plaza -Drive
Granite VOW, NC 28630
Meritech, Inc.
Environmental Laboratory
Laboratory Cert
ification No. 165
Repq.t 5/2022
. t pgtt.e 7/2-
Date Sam,Je Rpq
M'e1Itech.'WQrk'O,rOOr# 070446 :Sample:: O ;C. se #arms .-Mw#3 Crab 7/13122
Analysis Date
.MBAS -(as LAS 340) 4.1-4 mg/L .5 4-0: C_
Wfite6hWork-Orderg -07142207 SWAPII:
Parameters g6gh te "k wig M X lingLimi
Mobod
M BAS [as'LAS 340) .<0.10 mg./A 7/14/2 2 0.10 m
MOdte&-WOrk,OtA0Y # 0714220(8 Sample. 'CUdF4rffi§_MW Grab 7/13/2.2
Parametersllesiilt Analysis Date Amotting Limit Akthod
WAS (4s LAS $46) <Q 1Q MOA 0.1() ing/L SM 5540C
I hereby certify that I have reviewed and approve these data,
i alWe-
La 6 atoj
642 Tamdb Road, Reidsville, 'North Camliha 27320
tel-[phone] fax[phone],2

Analytical Environmental Services, Inc
Date: 21-Jul-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
CASE FARMS MW4
Project Name:
92614958
Collection Date:
7/13/2022 2:00:00 PM
Lab ID:
22071749-002
Marti:
Aqueous
Analyses meporting y Result Limit B Qua[ Units BatchID Factor
Date Analyzed Analyst
Formaldehyde by SW8315A
Formaldehyde BRL 50 UA 339759 1 07/15/202219:17 CM
Qualifiers: • Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above qua citation range)
S Spike Recovery outside limits duce to matrix
Narr See case narrative
F Analyzed In 010 lab which is n deviation ftmn the method
< Lem than Result value
I Estimated value detected below Rapartiuug I imd q. y

14RrffR r`rCff L.RRS.In..
POST OFFICE BOX 1056 - #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE: Case Farms-Hatchery-MW#5 COLLECTION DATE:
7/13/2022
PERMIT A- COLLECTION TIME.
13:30
ADDRESS: Case Farms Hatchery RECEIVED DATE:
7/13/2022
RECEIVED TIME:
14:30
REPORTED:
8/4/2022
-- X
ANALYSIS
ANALYSIS
RLSULTS
UNITS:
DATE
ANALYST
TDS
pace
NH3
<1.0
mg/L
7115/22
jrg
Fecal Coliform
<1
/100mL
7/13/22
Th
Metals
pace
NO3-N
2.77
mg/L
7119122
jsg
TKN
<1.0
mg/L
7/18/22
jdg
T. Nitrogen
2.77
mg/L
7/19/22
jdg
T. Phosphorus
0.20
mg/L
7/21/22
jdg
Chloride
pace
,_...G--.,.r,-._ - -
J
LOG ID: 2207-164 REPORTED BY: NC CEERQTIFIED LAB # 50
T111 P �

aceAnalytical v
www.pacelabs com
/
I
ANALYTICAL RESULTS
Project: CASE FARMS
Pace Project No.: 92614958
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Sample: CASE FARMS MW5
Parameters
Lab ID: 92614958003 Collected: 07/13/22 13:30
Results Units Report Limit DF
Received: 07/14/22 10:45 Matrix: Water
Prepared Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Arsenic
ND mg/L
0.010
1
07/19/22 11:24
07/20/22 22:09
7440-38-2
Barium
0.062 mg/L
0.0050
1
07/19/22 11:24
07/20/2217:37
7440-39-3
Copper
ND mg/L
0.0050
1
07/1912211:24
07/20/2217:37
7440-50-8
Iron
0.073 mg/L
0.050
1
07/19/22 11:24
07/20/2217:37
7439-89-6
Manganese
0.0056 mg/L
0.0050
1
07/19/22 11:24
07/20/2217:37
7439-96-5
Potassium
ND mg/L
5.0
1
07/19/22 11:24
07120/2217:37
7440-09-7
Sodium
8.5 mg/L
5.0
1
07/19/22 11:24
07/20/22 22:09
7440-23-5
Zinc
ND mg/L
0.010
1
07/19/22 11:24
07/2012217:37
7440-66-6
2540C Total Dissolved Solids
Analytical Method SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
120 mg/L
25.0
1
07/17/22 14:14
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
15.5 mg/L
1.0
1
07/18/221Z23
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services - Asheville
Total Organic Carbon
ND mg/L
1.0
1
07/19/22 19A8
7440-44-0
Date. 07/29/2022 04.56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 28
f

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contaict, Cathy Gragg
Client: Water Tech Labs; Inc
5 PirteWdbd fl-az A.DrIve
ROPP,rt P406 7/25/2,022
Granite Falls, NC 28.630 Date Sam R
Sample C-V4 7 /14/ZQ22
Merite ch Wopk." rd.or
-am .le; tase f;wms ..MW#3 Grab 7/13/22
AararnetersRes lysis Date lReportim Urrii
MBAS',(as LAS 340) <0110 MgA 7 2.2 -
940 :]MgA V654
.-0. C
MOOtkh 'Work Order 4 -07142207 Sample- C sef .-'M-W#.4-Grab 7/1. g2
.Parameters R-eusul AARK9. bath Reporfing-MMU
-MBAS.(as LAS 340.) -<M10 mg/L 7/14/22 OAU m L
-9/ S-M 5540 C-
MdrJt6Ch*WQ* Ordet # 0714Z20`8Sant 7ew'Qse Fa Mis -:M4
C rab 7/13/22
B=Mkters Rego AugWis,pat& R!w6rungullut -Hfabd
WAS (as .LAS 340). <Oao MOA 7/14/22
0.10 mg/L SM 5540C
I hereby certify thatl have reviewed and approve these data
Ldhorator
y Represents )lVe'
642 Tamco Road, Reldsvlfti, North Cardfta 27320
teQ33: 6,)342-4748 fa*.(M)342-j2.2

Analytical Environmental Services, Inc
Date: 21-Jul-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
CASE FARMS MW5
Project Name:
92614958
Collection Date:
7/13/2022 1:30:00 PM
Lab ID:
22071749-003
Matrix:
Aqueous
Analyses Result reporting Dilution
Limit Qua] Units 13atchlD Date Analyzed Analyst
Factor
Formaldehyde by SW8315A
Formaldehyde
Qualifiers: • Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analytc detected in the associated method blank
> Greater then Result value
BRL 50 ug/L 339642 1 07/18/202212:46 CM
E Estimated (value above cluanlitalion range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
f Analyzed in the lob which is a deviation from the method
< Less than Result value
Dni... 4 —4' 1 1

W/Al/j''T1111-117 CHLAB5� INS'*;
'r
5 Pinewood Plaza Drive • P.O. Box 1056
Granite Falls, NC 28630
Phone [phone]
CHAIN OF CUSTODY
CLIENT: Case Farms Hatchery PERMIT #:
TYPE SAMPLE:
SAMPLER NAME:-nS� C, Bvu ck
PHONE #: [phone]
Sample Collection Information
TYPE
CONTAINERS
Sample Location DATE TIME TEMP. °C Grab/
Facility Name
No Plastic/
ANALYSIS REQUIRED
Composite
Glass
Effluent
f f 31 I ; 3� aq
Grab
8 P
SOD, TSS, TDS, Fecal
Cond, Cl, NO3, NH3, TKN
M. Well #3
J l ; Q a�
Grab
12 PIG
TDS, CI, MBAS, Formelde
As, Cu,K,Zn,Na,Ba,Fe,Mn
NH3, NO3, T.P, Fecal, TOC
VOC (Annual Nov.)
M Well #4
1 l ; (�
Grab
12 PIG
Same as #3
M. Well #5
1 I (3 : 3Q T
Grab
12 PIG
Same as #3
Relin uishe By:
Date: Time:
i r3aa (11 S.OJ
Re eiv d By:
Date Time:
7 �3 C.S~
elinquished 8y:
Date: Time:
Rec ed B `
Date: Time:
PRESERVATION.
M Cool 6°C
PC HNO3
X H2SO4
(j Dechlorinating Agent
j NaOH
Other
SAMPLE TEMP. @ LAB
1 - Chlorine ResiduaK�.
rr��
(° _ 3• �l�
mall
NC CERTIFIED
LAB # 50

QKIM
1
0.4