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HomeMy WebLinkAboutWQ0036881_Corrective Action Monitoring Report Appendices_20160111Corrective Action Monitoring Report October 2015 Semi -Annual Event Appendix A (CD Format Only) TestAmerica ° THE LEADER IN ENVIRONMENTAL TESTING ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 TestAmerica Job ID: 680-118193-1 Client Project/Site: Murphy NC - IZ For: GHD Services Inc. 2055 Niagara Falls Blvd., Suite 3 Niagara Falls, New York 14304 Attn: Ms. Sue Scrocchi 64(��&Ay Authorized for release by. 111512015 9:39:23 AM Lisa Harvey, Project Manager II (912)354-7858 e.3221 lisa.harvey@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Client: GHD Services Inc. Project/Site: Murphy NC - IZ Table of Contents TestAmerica Job ID: 680-118193-1 Cover Page .............................................. 1 Table of Contents ......................................... 2 Case Narrative ........................................... 3 Sample Summary ......................................... 5 Method Summary ......................................... 6 Definitions ............................................... 7 Detection Summary ........................................ 8 Client Sample Results ...................................... 13 Surrogate Summary ....................................... 75 QC Sample Results ........................................ 76 Chronicle................................................ 89 Chain of Custody .......................................... 95 Certification Summary ...................................... 98 Page 2 of 98 TestAmerica Savannah 11 /5/2015 Case Narrative Client: GHD Services Inc. Project/Site: Murphy NC - IZ Job ID: 680-118193-1 Laboratory: TestAmerica Savannah Narrative CASE NARRATIVE Client: GHD Services Inc. Project: Murphy NC - IZ Report Number: 680-118193-1 TestAmerica Job ID: 680-118193-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required. RFCFIPT The samples were received on 10/23/2015 9:44 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 5.80 C. VOLATILE ORGANIC COMPOUNDS (GC -MS) Samples J1155-MW-10-101915 (680-118193-1), J1155-MW-11-101915 (680-118193-2), J1155-MW-12-102115 (680-118193-3), J1155-MW-13-102115 (680-118193-4), J1155-MW-17-101915 (680-118193-5), J1155-MW-20-101915 (680-118193-6), J1155-MW-28-102115 (680-118193-7), J1155-MW-32-101915 (680-118193-8), J1155-MW-35-101915 (680-118193-9), J1155-MW-36-102115 (680-118193-10), J1155-MW-37-102115 (680-118193-11), J1155-MW-45-101915 (680-118193-12), J1155-SP-26-102215 (680-118193-13), J1155-CMP-1-102115 (680-118193-14), J1155-CMP-3-102115 (680-118193-15), J1155-SW-3-102215 (680-118193-16), J1155-SW-6-102215 (680-118193-17), J1 155-SW-1 0-102215 (680-118193-18), J1155-RW-2-102215 (680-118193-19), J1155-RW-3-102215 (680-118193-20), J1155-RW-4-102215 (680-118193-21), J1155-RW-5-102215 (680-118193-22), J1155-DUP-1-101915 (680-118193-23), J1155-DUP-2-101915 (680-118193-24), J1155-DUP-3-102115 (680-118193-25), J1155-DUP-4-102115 (680-118193-26), J1155-EB-01-101915 (680-118193-27), J1155-EB-02-102015 (680-118193-28), J1155-EB-03-102115 (680-118193-29), J1155-EB-04-102215 (680-118193-30) and J1155-TB-01-101915 (680-118193-31) were analyzed for Volatile Organic Compounds (GC -MS) in accordance with EPA SW-846 Method 8260B. The samples were analyzed on 10/28/2015, 10/29/2015 and 10/30/2015. Method(s) 8260B: The laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for analytical batch 680-407738 recovered outside control limits for Carbon tetrachloride. The analyte was biased high in the LCS and was not detected in the associated samples; therefore, the data have been reported. Method(s) 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch 680-407734. Method(s) 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch 680-407738. Method(s) 8260B: Manual integration was performed on the following sample(s): CCVIS, LCS and LCSD. Method(s) 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch 680-407734. Method(s) 8260B: Manual integration was performed on the following samples: (CCVIS 680-407966/3), (LCS 680-407966/4) and (LCSD 680-407966/5). Method(s) 8260B: Manual integration was performed on the following samples: (CCVIS 680-408184/3), (LCS 680-408184/4) and (LCSD 680-408184/5). Samples J1155-MW-11-101915 (680-118193-2)[2X], J1155-MW-12-102115 (680-118193-3)[20X], J1155-MW-13-102115 (680-118193-4) [5X], J1155-MW-28-102115 (680-118193-7)[5X], J1155-MW-36-102115 (680-118193-10)[2X], J1155-MW-37-102115 (680-118193-11) [100X], J1155-RW-4-102215 (680-118193-21)[10X], J1155-RW-5-102215 (680-118193-22)[20X], J1155-RW-5-102215 (680-118193-22) [5X], J1155-DUP-4-102115 (680-118193-26)[20X] and J1155-DUP-4-102115 (680-118193-26)[200X] required dilution prior to analysis. TestAmerica Savannah Page 3 of 98 11 /5/2015 Case Narrative Client: GHD Services Inc. Project/Site: Murphy NC - IZ Job ID: 680-118193-1 (Continued) Laboratory: TestAmerica Savannah (Continued) The reporting limits have been adjusted accordingly. TestAmerica Job ID: 680-118193-1 No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. TestAmerica Savannah Page 4 of 98 11 /5/2015 Sample Summary Client: GHD Services Inc. TestAmerica Job ID: 680-118193-1 Project/Site: Murphy NC - IZ Lab Sample ID Client Sample ID Matrix Collected Received 680-118193-1 A 155-MW-10-101915 Water 10/19/15 11:36 10/23/15 09:44 680-118193-2 A 155-MW-11-101915 Water 10/19/15 10:54 10/23/15 09:44 680-118193-3 J1155-MW-12-102115 Water 10/21/15 14:25 10/23/15 09:44 680-118193-4 J1155-MW-13-102115 Water 10/21/15 13:27 10/23/15 09:44 680-118193-5 J1155-MW-17-101915 Water 10/19/15 13:16 10/23/15 09:44 680-118193-6 J1155-MW-20-101915 Water 10/19/15 12:01 10/23/15 09:44 680-118193-7 J1155-MW-28-102115 Water 10/21/15 12:34 10/23/15 09:44 680-118193-8 J1155-MW-32-101915 Water 10/19/15 12:34 10/23/15 09:44 680-118193-9 A 155-MW-35-101915 Water 10/19/15 14:39 10/23/15 09:44 680-118193-10 J1155-MW-36-102115 Water 10/21/15 12:53 10/23/15 09:44 680-118193-11 J1155-MW-37-102115 Water 10/21/15 14:00 10/23/15 09:44 680-118193-12 J1155-MW-45-101915 Water 10/19/15 13:53 10/23/15 09:44 680-118193-13 A 155-SP-26-102215 Water 10/22/15 09:45 10/23/15 09:44 680-118193-14 A 155-CMP-1-102115 Water 10/21/15 11:10 10/23/15 09:44 680-118193-15 A 155-CMP-3-102115 Water 10/21/15 11:21 10/23/15 09:44 680-118193-16 J 1 155-SW-3-102215 Water 10/22/15 10:16 10/23/15 09:44 680-118193-17 J 1 155-SW-6-102215 Water 10/22/15 09:55 10/23/15 09:44 680-118193-18 A 155-SW-10-102215 Water 10/22/15 10:03 10/23/15 09:44 680-118193-19 J 1 155-RW-2-102215 Water 10/22/15 09:28 10/23/15 09:44 680-118193-20 J 1 155-RW-3-102215 Water 10/22/15 09:34 10/23/15 09:44 680-118193-21 J 1 155-RW-4-102215 Water 10/22/15 09:15 10/23/15 09:44 680-118193-22 J 1 155-RW-5-102215 Water 10/22/15 09:22 10/23/15 09:44 680-118193-23 A 155-DUP-1-101915 Water 10/19/15 16:00 10/23/15 09:44 680-118193-24 A 155-DUP-2-101915 Water 10/19/15 16:00 10/23/15 09:44 680-118193-25 J1155-DUP-3-102115 Water 10/21/15 16:00 10/23/15 09:44 680-118193-26 J1155-DUP-4-102115 Water 10/21/15 16:00 10/23/15 09:44 680-118193-27 A 155-EB-01-101915 Water 10/19/15 17:03 10/23/15 09:44 680-118193-28 A 155-EB-02-102015 Water 10/20/15 16:32 10/23/15 09:44 680-118193-29 A 155-EB-03-102115 Water 10/21/15 15:02 10/23/15 09:44 680-118193-30 A 155-EB-04-102215 Water 10/22/15 09:58 10/23/15 09:44 680-118193-31 A 155-TB-01-101915 Water 10/19/15 08:30 10/23/15 09:44 TestAmerica Savannah Page 5 of 98 11 /5/2015 Method Summary Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Method Method Description Protocol Laboratory 8260B Volatile Organic Compounds (GC/MS) SW846 TAL SAV Protocol References: SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 TestAmerica Savannah Page 6 of 98 11 /5/2015 Definitions/Glossary Client: GHD Services Inc. Project/Site: Murphy NC - IZ Qualifiers GC/MS VOA Qualifier Qualifier Description * LCS or LCSD is outside acceptance limits. Glossary Abbreviation tt %R CFL CNF DER Dil Fac DL, RA, RE, IN DLC M DA EDL MDC MDL ML NC ND PQL QC RER RL RPD TEF TEQ TestAmerica Job ID: 680-118193-1 These commonly used abbreviations may or may not be present in this report. Listed under the "D" column to designate that the result is reported on a dry weight basis Percent Recovery Contains Free Liquid Contains no Free Liquid Duplicate error ratio (normalized absolute difference) Dilution Factor Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample Decision level concentration Minimum detectable activity Estimated Detection Limit Minimum detectable concentration Method Detection Limit Minimum Level (Dioxin) Not Calculated Not detected at the reporting limit (or MDL or EDL if shown) Practical Quantitation Limit Quality Control Relative error ratio Reporting Limit or Requested Limit (Radiochemistry) Relative Percent Difference, a measure of the relative difference between two points Toxicity Equivalent Factor (Dioxin) Toxicity Equivalent Quotient (Dioxin) 0 TestAmerica Savannah Page 7 of 98 11 /5/2015 Detection Summary Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: A 155-MW-10-101915 Lab Sample ID: 680-118193-1 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Chloroform 15 1.0 ug/L 1 8260B Total/NA cis-1,2-Dichloroethene 1.5 1.0 ug/L 1 8260B Total/NA 1,1-Dichloroethane 1.1 1.0 ug/L 1 8260B Total/NA Tetrachloroethene 2.0 1.0 ug/L 1 8260B Total/NA 1, 1, 1 -Trichloroethane 1.3 1.0 ug/L 1 8260B Total/NA Trichloroethene 41 1.0 ug/L 1 8260B Total/NA Client Sample ID: A 155-MW-11-101915 Lab Sample ID: 680-118193-2 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type cis- 1,2-Dichloroethene 80 2.0 ug/L 2 8260B Total/NA 1,1-Dichloroethane 4.8 2.0 ug/L 2 8260B Total/NA 1,1-Dichloroethene 12 2.0 ug/L 2 8260B Total/NA Tetrachloroethene 7.7 2.0 ug/L 2 8260B Total/NA Trichloroethene 170 2.0 ug/L 2 8260B Total/NA Client Sample ID: A 155-MW-12-102115 Lab Sample ID: 680-118193-3 Is Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type cis- 1,2-Dichloroethene 360 20 ug/L 20 8260E Total/NA Dichlorodifluoromethane 45 20 ug/L 20 8260B Total/NA 1,1-Dichloroethane 77 20 ug/L 20 8260B Total/NA 1,1-Dichloroethene 130 20 ug/L 20 8260B Total/NA Tetrachloroethene 96 20 ug/L 20 8260B Total/NA 1,1,1-Trichloroethane 22 20 ug/L 20 8260B Total/NA Trichloroethene 2200 20 ug/L 20 8260E Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 380 20 ug/L 20 8260E Total/NA Client Sample ID: A 155-MW-13-102115 Lab Sample ID: 680-118193-4 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type cis- 1,2-Dichloroethene 14 5.0 ug/L 5 8260B Total/NA 1,1-Dichloroethene 8.2 5.0 ug/L 5 8260B Total/NA Tetrachloroethene 6.2 5.0 ug/L 5 8260B Total/NA 1,1,1-Trichloroethane 7.8 5.0 ug/L 5 8260B Total/NA Trichloroethene 420 5.0 ug/L 5 8260B Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 8.7 5.0 ug/L 5 8260B Total/NA Client Sample ID: A 155-MW-17-101915 Lab Sample ID: 680-118193-5 FNo Detections. Client Sample ID: A 155-MW-20-101915 Lab Sample ID: 680-118193-6 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type cis-1,2-Dichloroethene 2.9 1.0 ug/L 1 8260B Total/NA Client Sample ID: A 155-MW-28-102115 Lab Sample ID: 680-118193-7 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type cis-1,2-Dichloroethene 41 5.0 ug/L 5 8260B Total/NA This Detection Summary does not include radiochemical test results. TestAmerica Savannah Page 8 of 98 11 /5/2015 Detection Summary Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: A 155-MW-28-102115 (Continued) Lab Sample ID: 680-118193-7 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,1-Dichloroethane 27 5.0 ug/L 5 8260B Total/NA 1,1-Dichloroethene 35 5.0 ug/L 5 8260B Total/NA Tetrachloroethene 27 5.0 ug/L 5 8260B Total/NA 1,1,1-Trichloroethane 11 5.0 ug/L 5 8260B Total/NA Trichloroethene 370 5.0 ug/L 5 8260B Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 13 5.0 ug/L 5 8260B Total/NA Client Sample ID: A 155-MW-32-101915 Lab Sample ID: 680-118193-8 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type cis-1,2-Dichloroethene 3.8 1.0 ug/L 1 8260B Total/NA 1,1-Dichloroethene 1.7 1.0 ug/L 1 8260B Total/NA Tetrachloroethene 2.8 1.0 ug/L 1 8260B Total/NA 1,1,1-Trichloroethane 1.1 1.0 ug/L 1 8260B Total/NA Trichloroethene 30 1.0 ug/L 1 8260B Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 1.6 1.0 ug/L 1 8260B Total/NA Client Sample ID: A 155-MW-35-101915 Lab Sample ID: 680-118193-9 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type cis-1,2-Dichloroethene 7.4 1.0 ug/L 1 8260B Total/NA Trichloroethene 4.3 1.0 ug/L 1 8260B Total/NA Client Sample ID: A 155-MW-36-102115 Lab Sample ID: 680-118193-10 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type cis-1,2-Dichloroethene 29 2.0 ug/L 2 8260B Total/NA 1,1-Dichloroethane 11 2.0 ug/L 2 8260B Total/NA 1,1-Dichloroethene 15 2.0 ug/L 2 8260B Total/NA Tetrachloroethene 14 2.0 ug/L 2 8260B Total/NA Trichloroethene 210 2.0 ug/L 2 8260B Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 2.4 2.0 ug/L 2 8260B Total/NA Client Sample ID: J1155-MW-37-102115 Analyte Result Qualifier cis- 1,2-Dichloroethene 1100 1,1-Dichloroethane 250 Tetrachloroethene 220 Trichloroethene 15000 Lab Sample ID: 680-118193-11 RL MDL Unit Dil Fac D Method Prep Type 100 ug/L 100 8260E Total/NA 100 ug/L 100 8260E Total/NA 100 ug/L 100 8260E Total/NA 100 ug/L 100 8260E Total/NA Client Sample ID: A 155-MW-45-101915 Lab Sample ID: 680-118193-12 FNo Detections. Client Sample ID: A 155-SP-26-102215 Analyte Result Qualifier Trichloroethene 1.7 1,1,2-Trichloro-1,2,2-trifluoroethane 1.3 This Detection Summary does not include radiochemical test results. Lab Sample ID: 680-118193-13 RL MDL Unit Dil Fac D Method Prep Type 1.0 ug/L 1 8260B Total/NA 1.0 ug/L 1 8260B Total/NA Page 9 of 98 TestAmerica Savannah 11 /5/2015 Detection Summary Client: GHD Services Inc. Project/Site: Murphy NC - IZ Client Sample ID: A 155-CMP-1-102115 INo Detections. Client Sample ID: A 155-CMP-3-102115 INo Detections. TestAmerica Job ID: 680-118193-1 Lab Sample ID: 680-118193-14 Lab Sample ID: 680-118193-15 n Client Sample ID: A 155-SW-3-102215 Lab Sample ID: 680-118193-16 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Trichloroethene 1.2 1.0 ug/L 1 8260B Total/NA Client Sample ID: A 155-SW-6-102215 Lab Sample ID: 680-118193-17 1 No Detections. Client Sample ID: J1155-SW-10-102215 Lab Sample ID: 680-118193-18 FNo Detections. Client Sample ID: A 155-RW-2-102215 Lab Sample ID: 680-118193-19 Result Qualifier RL MDL Unit Dil Fac D Method Prep Type [Analyte Trichloroethene 4.1 1.0 ug/L 1 8260B Total/NA Client Sample ID: A 155-RW-3-102215 Lab Sample ID: 680-118193-20 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Carbon tetrachloride 3.4 1.0 ug/L 1 8260B Total/NA Chloroform 1.1 1.0 ug/L 1 8260B Total/NA cis- 1,2-Dichloroethene 3.2 1.0 ug/L 1 8260B Total/NA 1,1-Dichloroethane 1.3 1.0 ug/L 1 8260B Total/NA 1,1-Dichloroethene 10 1.0 ug/L 1 8260B Total/NA Tetrachloroethene 7.5 1.0 ug/L 1 8260B Total/NA 1,1,1-Trichloroethane 21 1.0 ug/L 1 8260B Total/NA Trichloroethene 58 1.0 ug/L 1 8260B Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 15 1.0 ug/L 1 8260B Total/NA Client Sample ID: A 155-RW-4-102215 Lab Sample ID: 680-118193-21 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type cis- 1,2-Dichloroethene 31 10 ug/L 10 8260B Total/NA 1,1-Dichloroethene 31 10 ug/L 10 8260B Total/NA Tetrachloroethene 27 10 ug/L 10 8260B Total/NA 1,1,1-Trichloroethane 18 10 ug/L 10 8260B Total/NA Trichloroethene 880 10 ug/L 10 8260B Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 280 10 ug/L 10 8260B Total/NA Client Sample ID: A 155-RW-5-102215 Lab Sample ID: 680-118193-22 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type cis-1,2-Dichloroethene 190 5.0 ug/L 5 8260E Total/NA 1,1-Dichloroethane 200 5.0 ug/L 5 8260B Total/NA This Detection Summary does not include radiochemical test results. TestAmerica Savannah Page 10 of 98 11/5/2015 Detection Summary Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: A 155-RW-5-102215 (Continued) Lab Sample ID: 680-118193-22 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,1-Dichloroethene 78 5.0 ug/L 5 8260B Total/NA Tetrachloroethene 94 5.0 ug/L 5 8260B Total/NA 1, 1, 1 -Trichloroethane 98 5.0 ug/L 5 8260B Total/NA Trichloroethene 3400 20 ug/L 20 8260E Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 9.1 5.0 ug/L 5 8260B Total/NA Client Sample ID: A 155-DUP-1-101915 Lab Sample ID: 680-118193-23 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type cis- 1,2-Dichloroethene 6.2 1.0 ug/L 1 8260B Total/NA 1,1-Dichloroethane 1.5 1.0 ug/L 1 8260B Total/NA 1,1-Dichloroethene 2.2 1.0 ug/L 1 8260B Total/NA Tetrachloroethene 3.4 1.0 ug/L 1 8260B Total/NA 1, 1, 1 -Trichloroethane 1.7 1.0 ug/L 1 8260B Total/NA Trichloroethene 39 1.0 ug/L 1 8260B Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 2.2 1.0 ug/L 1 8260B Total/NA Client Sample ID: A 155-DUP-2-101915 Lab Sample ID: 680-118193-24 ENo Detections. Client Sample ID: A 155-DUP-3-102115 Lab Sample ID: 680-118193-25 ENo Detections. Client Sample ID: A 155-DUP-4-102115 Lab Sample ID: 680-118193-26 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type cis- 1,2-Dichloroethene 980 20 ug/L 20 8260E Total/NA 1,1-Dichloroethane 210 20 ug/L 20 8260B Total/NA 1,1-Dichloroethene 68 20 ug/L 20 8260B Total/NA Tetrachloroethene 190 20 ug/L 20 8260B Total/NA Trichloroethene 12000 200 ug/L 200 8260B Total/NA Client Sample ID: J1155-EB-01-101915 Lab Sample ID: 680-118193-27 ENo Detections. Client Sample ID: A 155-EB-02-102015 Lab Sample ID: 680-118193-28 ENo Detections. Client Sample ID: A 155-EB-03-102115 Lab Sample ID: 680-118193-29 ENo Detections. Client Sample ID: A 155-EB-04-102215 Lab Sample ID: 680-118193-30 INo Detections This Detection Summary does not include radiochemical test results. TestAmerica Savannah Page 11 of 98 11/5/2015 Detection Summary Client: GHD Services Inc. Project/Site: Murphy NC - IZ Client Sample ID: A 155-TB-01-101915 INo Detections. This Detection Summary does not include radiochemical test results. TestAmerica Job ID: 680-118193-1 Lab Sample ID: 680-118193-31 TestAmerica Savannah Page 12 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-10-101915 Lab Sample ID: 680-118193-1 Date Collected: 10/19/15 11:36 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform 15 Chloromethane ND cis-1,2-Dichloroethene 1.5 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane 1.1 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 2.0 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane 1.3 1,1,2-Trichloroethane ND Trichloroethene 41 Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 5.0 ug/L 10/28/1513:33 1 10 ug/L 10/28/1513:33 1 2.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 5.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 5.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 10 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 5.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 5.0 ug/L 10/28/1513:33 1 10 ug/L 10/28/1513:33 1 10 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 10 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 5.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 1.0 ug/L 10/28/1513:33 1 TestAmerica Savannah Page 13 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-10-101915 Lab Sample ID: 680-118193-1 Date Collected: 10/19/15 11:36 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 99 70 - 130 10128115 13:33 1 Dibromofluoromethane (Surr) 109 70 - 130 10128115 13:33 1 1,2-Dichloroethane-d4 (Surr) 106 70- 130 10128115 13:33 1 Toluene-d8 (Surr) 101 70 - 130 10128115 13:33 1 0 TestAmerica Savannah Page 14 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: A155-MW-11-101915 Lab Sample ID: 680-118193-2 Date Collected: 10/19/15 10:54 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 80 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane 4.8 1,2-Dichloroethane ND 1,1-Dichloroethene 12 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 7.7 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 170 Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 20 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 10 ug/L 10/28/1516:03 2 20 ug/L 10/28/1516:03 2 4.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 10 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 10 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 20 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 10 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 10 ug/L 10/28/1516:03 2 20 ug/L 10/28/1516:03 2 20 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 20 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 10 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 2.0 ug/L 10/28/1516:03 2 TestAmerica Savannah Page 15 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: A155-MW-11-101915 Lab Sample ID: 680-118193-2 Date Collected: 10/19/15 10:54 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 99 70 - 130 10128115 16:03 2 Dibromofluoromethane (Surr) 120 70 - 130 10128115 16:03 2 1,2-Dichloroethane-d4 (Surr) 127 70- 130 10128115 16:03 2 Toluene-d8 (Surr) 97 70 - 130 10128115 16:03 2 0 TestAmerica Savannah Page 16 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. TestAmerica Job ID: 680-118193-1 Project/Site: Murphy NC - IZ Client Sample ID: J1155-MW-12-102115 Lab Sample ID: 680-118193-3 Date Collected: 10/21/15 14:25 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 200 ug/L 10/29/15 11:07 20 Benzene ND 20 ug/L 10/29/15 11:07 20 Bromodichloromethane ND 20 ug/L 10/29/15 11:07 20 Bromoform ND 20 ug/L 10/29/15 11:07 20 Bromomethane ND 100 ug/L 10/29/15 11:07 20 2-Butanone ND 200 ug/L 10/29/15 11:07 20 Carbon disulfide ND 40 ug/L 10/29/15 11:07 20 Carbon tetrachloride ND 20 ug/L 10/29/15 11:07 20 Chlorobenzene ND 20 ug/L 10/29/15 11:07 20 Chloroethane ND 100 ug/L 10/29/15 11:07 20 Chloroform ND 20 ug/L 10/29/15 11:07 20 Chloromethane ND 20 ug/L 10/29/15 11:07 20 cis-1,2-Dichloroethene 360 20 ug/L 10/29/15 11:07 20 cis-1,3-Dichloropropene ND 20 ug/L 10/29/15 11:07 20 Cyclohexane ND 20 ug/L 10/29/15 11:07 20 Dibromochloromethane ND 20 ug/L 10/29/15 11:07 20 1,2-Dibromo-3-Chloropropane ND 100 ug/L 10/29/15 11:07 20 1,2-Dibromoethane ND 20 ug/L 10/29/15 11:07 20 1,2-Dichlorobenzene ND 20 ug/L 10/29/15 11:07 20 1,3-Dichlorobenzene ND 20 ug/L 10/29/15 11:07 20 1,4-Dichlorobenzene ND 20 ug/L 10/29/15 11:07 20 Dichlorodifluoromethane 45 20 ug/L 10/29/15 11:07 20 1,1-Dichloroethane 77 20 ug/L 10/29/15 11:07 20 1,2-Dichloroethane ND 20 ug/L 10/29/15 11:07 20 1,1-Dichloroethene 130 20 ug/L 10/29/15 11:07 20 1,2-Dichloropropane ND 20 ug/L 10/29/15 11:07 20 Ethylbenzene ND 20 ug/L 10/29/15 11:07 20 2-Hexanone ND 200 ug/L 10/29/15 11:07 20 Isopropylbenzene ND 20 ug/L 10/29/15 11:07 20 Methyl acetate ND 100 ug/L 10/29/15 11:07 20 Methylcyclohexane ND 20 ug/L 10/29/15 11:07 20 Methylene Chloride ND 100 ug/L 10/29/15 11:07 20 4-Methyl-2-pentanone ND 200 ug/L 10/29/15 11:07 20 Methyl tert-butyl ether ND 200 ug/L 10/29/15 11:07 20 Styrene ND 20 ug/L 10/29/15 11:07 20 1,1,2,2-Tetrachloroethane ND 20 ug/L 10/29/15 11:07 20 Tetrachloroethene 96 20 ug/L 10/29/15 11:07 20 Tetrahydrofuran ND 200 ug/L 10/29/15 11:07 20 Toluene ND 20 ug/L 10/29/15 11:07 20 trans-1,2-Dichloroethene ND 20 ug/L 10/29/15 11:07 20 trans-1,3-Dichloropropene ND 20 ug/L 10/29/15 11:07 20 1,2,4-Trichlorobenzene ND 100 ug/L 10/29/15 11:07 20 1,1,1-Trichloroethane 22 20 ug/L 10/29/15 11:07 20 1,1,2-Trichloroethane ND 20 ug/L 10/29/15 11:07 20 Trichloroethene 2200 20 ug/L 10/29/15 11:07 20 Trichlorofluoromethane ND 20 ug/L 10/29/15 11:07 20 1,1,2-Trichloro-1,2,2-trifluoroetha 380 20 ug/L 10/29/15 11:07 20 ne Vinyl chloride ND 20 ug/L 10/29/15 11:07 20 TestAmerica Savannah Page 17 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-12-102115 Lab Sample ID: 680-118193-3 Date Collected: 10/21/15 14:25 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 20 ug/L 10/29/15 11:07 20 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 91 70 - 130 10/29/15 11:07 20 Dibromofluoromethane (Surr) 99 70 - 130 10/29/15 11:07 20 1,2-Dichloroethane-d4 (Surr) 96 70- 130 10/29/15 11:07 20 Toluene-d8 (Surr) 94 70 - 130 10129115 11:07 20 ' TestAmerica Savannah Page 18 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: A 155-MW-13-102115 Lab Sample ID: 680-118193-4 Date Collected: 10/21/15 13:27 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 14 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene 8.2 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 6.2 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane 7.8 1,1,2-Trichloroethane ND Trichloroethene 420 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 8.7 ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 50 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 25 ug/L 10/29/1511:28 5 50 ug/L 10/29/1511:28 5 10 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 25 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 25 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 50 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 25 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 25 ug/L 10/29/1511:28 5 50 ug/L 10/29/1511:28 5 50 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 50 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 25 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 5.0 ug/L 10/29/1511:28 5 TestAmerica Savannah Page 19 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. TestAmerica Job ID: 680-118193-1 Project/Site: Murphy NC - IZ Client Sample ID: A 155-MW-13-102115 Lab Sample ID: 680-118193-4 Date Collected: 10/21/15 13:27 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 5.0 ug/L 10/29/15 11:28 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 91 70 - 130 10/29/15 11:28 5 Dibromofluoromethane (Surr) 97 70 - 130 10/29/15 11:28 5 1,2-Dichloroethane-d4 (Surr) 95 70- 130 10/29/15 11:28 5 Toluene-d8 (Surr) 96 70 - 130 10129115 11:28 5 ' TestAmerica Savannah Page 20 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: A 155-MW-17-101915 Lab Sample ID: 680-118193-5 Date Collected: 10/19/15 13:16 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 5.0 ug/L 10/28/1513:54 1 10 ug/L 10/28/1513:54 1 2.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 5.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 5.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 10 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 5.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 5.0 ug/L 10/28/1513:54 1 10 ug/L 10/28/1513:54 1 10 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 10 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 5.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 1.0 ug/L 10/28/1513:54 1 TestAmerica Savannah Page 21 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: A 155-MW-17-101915 Lab Sample ID: 680-118193-5 Date Collected: 10/19/15 13:16 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 98 70 - 130 10128115 13:54 1 Dibromofluoromethane (Surr) 110 70 - 130 10128115 13:54 1 1,2-Dichloroethane-d4 (Surr) 107 70- 130 10128115 13:54 1 Toluene-d8 (Surr) 101 70 - 130 10128115 13:54 1 0 TestAmerica Savannah Page 22 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-20-101915 Lab Sample ID: 680-118193-6 Date Collected: 10/19/15 12:01 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 2.9 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 5.0 ug/L 10/28/1514:16 1 10 ug/L 10/28/1514:16 1 2.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 5.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 5.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 10 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 5.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 5.0 ug/L 10/28/1514:16 1 10 ug/L 10/28/1514:16 1 10 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 10 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 5.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 1.0 ug/L 10/28/1514:16 1 TestAmerica Savannah Page 23 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-20-101915 Lab Sample ID: 680-118193-6 Date Collected: 10/19/15 12:01 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 99 70 - 130 10128115 14:16 1 Dibromofluoromethane (Surr) 111 70 - 130 10128115 14:16 1 1,2-Dichloroethane-d4 (Surr) 107 70- 130 10128115 14:16 1 Toluene-d8 (Surr) 101 70 - 130 10128115 14:16 1 0 TestAmerica Savannah Page 24 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-28-102115 Lab Sample ID: 680-118193-7 Date Collected: 10/21/15 12:34 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 41 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane 27 1,2-Dichloroethane ND 1,1-Dichloroethene 35 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 27 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane 11 1,1,2-Trichloroethane ND Trichloroethene 370 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 13 ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 50 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 25 ug/L 10/28/1517:08 5 50 ug/L 10/28/1517:08 5 10 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 25 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 25 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 50 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 25 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 25 ug/L 10/28/1517:08 5 50 ug/L 10/28/1517:08 5 50 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 50 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 25 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 5.0 ug/L 10/28/1517:08 5 TestAmerica Savannah Page 25 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. TestAmerica Job ID: 680-118193-1 Project/Site: Murphy NC - IZ Client Sample ID: J1155-MW-28-102115 Lab Sample ID: 680-118193-7 Date Collected: 10/21/15 12:34 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 5.0 ug/L 10/28/15 17:08 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 99 70 - 130 10128115 17:08 5 Dibromofluoromethane (Surr) 120 70 - 130 10128115 17:08 5 1,2-Dichloroethane-d4 (Surr) 124 70- 130 10/28/15 17:08 5 Toluene-d8 (Surr) 94 70 - 130 10128115 17:08 5 ' TestAmerica Savannah Page 26 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-32-101915 Lab Sample ID: 680-118193-8 Date Collected: 10/19/15 12:34 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 3.8 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene 1.7 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 2.8 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane 1.1 1,1,2-Trichloroethane ND Trichloroethene 30 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 1.6 ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 5.0 ug/L 10/29/1510:25 1 10 ug/L 10/29/1510:25 1 2.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 5.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 5.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 10 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 5.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 5.0 ug/L 10/29/1510:25 1 10 ug/L 10/29/1510:25 1 10 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 10 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 5.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 1.0 ug/L 10/29/1510:25 1 TestAmerica Savannah Page 27 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. TestAmerica Job ID: 680-118193-1 Project/Site: Murphy NC - IZ Client Sample ID: J1155-MW-32-101915 Lab Sample ID: 680-118193-8 Date Collected: 10/19/15 12:34 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 1.0 ug/L 10/29/15 10:25 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 95 70 - 130 10129115 10:25 1 Dibromofluoromethane (Surr) 96 70 - 130 10129115 10:25 1 1,2-Dichloroethane-d4 (Surr) 87 70- 130 10/29/15 10:25 1 Toluene-d8 (Surr) 99 70 - 130 10129115 10:25 1 ' TestAmerica Savannah Page 28 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-35-101915 Lab Sample ID: 680-118193-9 Date Collected: 10/19/15 14:39 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 7.4 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 4.3 Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 5.0 ug/L 10/28/1514:37 1 10 ug/L 10/28/1514:37 1 2.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 5.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 5.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 10 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 5.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 5.0 ug/L 10/28/1514:37 1 10 ug/L 10/28/1514:37 1 10 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 10 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 5.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 1.0 ug/L 10/28/1514:37 1 TestAmerica Savannah Page 29 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-35-101915 Lab Sample ID: 680-118193-9 Date Collected: 10/19/15 14:39 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 70 - 130 10128115 14:37 1 Dibromofluoromethane (Surr) 110 70 - 130 10128115 14:37 1 1,2-Dichloroethane-d4 (Surr) 107 70- 130 10128115 14:37 1 Toluene-d8 (Surr) 102 70 - 130 10128115 14:37 1 0 TestAmerica Savannah Page 30 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-36-102115 Lab Sample ID: 680-118193-10 Date Collected: 10/21/15 12:53 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 29 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane 11 1,2-Dichloroethane ND 1,1-Dichloroethene 15 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 14 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 210 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 2.4 ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 20 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 10 ug/L 10/29/1511:49 2 20 ug/L 10/29/1511:49 2 4.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 10 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 10 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 20 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 10 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 10 ug/L 10/29/1511:49 2 20 ug/L 10/29/1511:49 2 20 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 20 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 10 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 2.0 ug/L 10/29/1511:49 2 TestAmerica Savannah Page 31 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-36-102115 Lab Sample ID: 680-118193-10 Date Collected: 10/21/15 12:53 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 2.0 ug/L 10/29/15 11:49 2 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 92 70 - 130 10/29/15 11:49 2 Dibromofluoromethane (Surr) 106 70 - 130 10/29/15 11:49 2 1,2-Dichloroethane-d4 (Surr) 112 70- 130 10/29/15 11:49 2 Toluene-d8 (Surr) 91 70 - 130 10129115 11:49 2 ' TestAmerica Savannah Page 32 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-37-102115 Lab Sample ID: 680-118193-11 Date Collected: 10/21/15 14:00 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 1100 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane 250 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 220 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 15000 Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 1000 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 500 ug/L 10/28/1518:12 100 1000 ug/L 10/28/1518:12 100 200 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 500 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 500 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 1000 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 500 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 500 ug/L 10/28/1518:12 100 1000 ug/L 10/28/1518:12 100 1000 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 1000 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 500 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 100 ug/L 10/28/1518:12 100 TestAmerica Savannah Page 33 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-37-102115 Lab Sample ID: 680-118193-11 Date Collected: 10/21/15 14:00 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 96 70 - 130 10128115 18:12 100 Dibromofluoromethane (Surr) 115 70 - 130 10128115 18:12 100 1,2-Dichloroethane-d4 (Surr) 116 70- 130 10128115 18:12 100 Toluene-d8 (Surr) 100 70 - 130 10128115 18:12 100 0 TestAmerica Savannah Page 34 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-45-101915 Lab Sample ID: 680-118193-12 Date Collected: 10/19/15 13:53 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 5.0 ug/L 10/28/1514:58 1 10 ug/L 10/28/1514:58 1 2.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 5.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 5.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 10 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 5.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 5.0 ug/L 10/28/1514:58 1 10 ug/L 10/28/1514:58 1 10 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 10 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 5.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 1.0 ug/L 10/28/1514:58 1 TestAmerica Savannah Page 35 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-MW-45-101915 Lab Sample ID: 680-118193-12 Date Collected: 10/19/15 13:53 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 99 70 - 130 10128115 14:58 1 Dibromofluoromethane (Surr) 108 70 - 130 10128115 14:58 1 1,2-Dichloroethane-d4 (Surr) 105 70- 130 10128115 14:58 1 Toluene-d8 (Surr) 104 70 - 130 10128115 14:58 1 0 TestAmerica Savannah Page 36 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-SP-26-102215 Lab Sample ID: 680-118193-13 Date Collected: 10/22/15 09:45 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 1.7 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 1.3 ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 5.0 ug/L 10/28/1512:06 1 10 ug/L 10/28/1512:06 1 2.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 5.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 5.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 10 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 5.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 5.0 ug/L 10/28/1512:06 1 10 ug/L 10/28/1512:06 1 10 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 10 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 5.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 TestAmerica Savannah Page 37 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-SP-26-102215 Lab Sample ID: 680-118193-13 Date Collected: 10/22/15 09:45 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Xylenes, Total ND 1.0 ug/L Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 103 70 - 130 Dibromofluoromethane (Surr) 98 70 - 130 1,2-Dichloroethane-d4 (Surr) 93 70- 130 Toluene-d8 (Surr) 100 70 - 130 Prepared Analyzed Dil Fac 10/28/15 12:06 1 Prepared Analyzed Dil Fac 10/28/15 12:06 1 10/28/15 12:06 1 10/28/15 12:06 1 10128115 12:06 1 ' TestAmerica Savannah Page 38 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-CMP-1-102115 Lab Sample ID: 680-118193-14 Date Collected: 10/21/15 11:10 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 5.0 ug/L 10/28/1512:29 1 10 ug/L 10/28/1512:29 1 2.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 5.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 5.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 10 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 5.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 5.0 ug/L 10/28/1512:29 1 10 ug/L 10/28/1512:29 1 10 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 10 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 5.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 1.0 ug/L 10/28/1512:29 1 TestAmerica Savannah Page 39 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-CMP-1-102115 Lab Sample ID: 680-118193-14 Date Collected: 10/21/15 11:10 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 103 70 - 130 10128115 12:29 1 Dibromofluoromethane (Surr) 101 70 - 130 10128115 12:29 1 1,2-Dichloroethane-d4 (Surr) 92 70- 130 10128115 12:29 1 Toluene-d8 (Surr) 100 70 - 130 10128115 12:29 1 0 TestAmerica Savannah Page 40 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-CMP-3-102115 Lab Sample ID: 680-118193-15 Date Collected: 10/21/15 11:21 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 5.0 ug/L 10/28/1512:52 1 10 ug/L 10/28/1512:52 1 2.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 5.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 5.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 10 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 5.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 5.0 ug/L 10/28/1512:52 1 10 ug/L 10/28/1512:52 1 10 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 10 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 5.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 1.0 ug/L 10/28/1512:52 1 TestAmerica Savannah Page 41 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-CMP-3-102115 Lab Sample ID: 680-118193-15 Date Collected: 10/21/15 11:21 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 105 70 - 130 10128115 12:52 1 Dibromofluoromethane (Surr) 99 70 - 130 10128115 12:52 1 1,2-Dichloroethane-d4 (Surr) 95 70- 130 10128115 12:52 1 Toluene-d8 (Surr) 99 70 - 130 10128115 12:52 1 0 TestAmerica Savannah Page 42 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-SW-3-102215 Lab Sample ID: 680-118193-16 Date Collected: 10/22/15 10:16 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 1.2 Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 5.0 ug/L 10/28/1513:15 1 10 ug/L 10/28/1513:15 1 2.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 5.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 5.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 10 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 5.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 5.0 ug/L 10/28/1513:15 1 10 ug/L 10/28/1513:15 1 10 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 10 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 5.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 1.0 ug/L 10/28/1513:15 1 TestAmerica Savannah Page 43 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-SW-3-102215 Lab Sample ID: 680-118193-16 Date Collected: 10/22/15 10:16 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 104 70 - 130 10128115 13:15 1 Dibromofluoromethane (Surr) 101 70 - 130 10128115 13:15 1 1,2-Dichloroethane-d4 (Surr) 95 70- 130 10128115 13:15 1 Toluene-d8 (Surr) 100 70 - 130 10128115 13:15 1 0 TestAmerica Savannah Page 44 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-SW-6-102215 Lab Sample ID: 680-118193-17 Date Collected: 10/22/15 09:55 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 5.0 ug/L 10/28/1513:38 1 10 ug/L 10/28/1513:38 1 2.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 5.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 5.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 10 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 5.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 5.0 ug/L 10/28/1513:38 1 10 ug/L 10/28/1513:38 1 10 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 10 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 5.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 1.0 ug/L 10/28/1513:38 1 TestAmerica Savannah Page 45 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-SW-6-102215 Lab Sample ID: 680-118193-17 Date Collected: 10/22/15 09:55 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 102 70 - 130 10128115 13:38 1 Dibromofluoromethane (Surr) 99 70 - 130 10128115 13:38 1 1,2-Dichloroethane-d4 (Surr) 95 70- 130 10128115 13:38 1 Toluene-d8 (Surr) 99 70 - 130 10128115 13:38 1 0 TestAmerica Savannah Page 46 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-SW-10-102215 Lab Sample ID: 680-118193-18 Date Collected: 10/22/15 10:03 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 5.0 ug/L 10/28/1514:01 1 10 ug/L 10/28/1514:01 1 2.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 5.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 5.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 10 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 5.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 5.0 ug/L 10/28/1514:01 1 10 ug/L 10/28/1514:01 1 10 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 10 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 5.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 1.0 ug/L 10/28/1514:01 1 TestAmerica Savannah Page 47 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-SW-10-102215 Lab Sample ID: 680-118193-18 Date Collected: 10/22/15 10:03 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 103 70 - 130 10128115 14:01 1 Dibromofluoromethane (Surr) 101 70 - 130 10128115 14:01 1 1,2-Dichloroethane-d4 (Surr) 95 70- 130 10128115 14:01 1 Toluene-d8 (Surr) 99 70 - 130 10128115 14:01 1 0 TestAmerica Savannah Page 48 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-RW-2-102215 Lab Sample ID: 680-118193-19 Date Collected: 10/22/15 09:28 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 4.1 Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 5.0 ug/L 10/28/1514:24 1 10 ug/L 10/28/1514:24 1 2.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 5.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 5.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 10 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 5.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 5.0 ug/L 10/28/1514:24 1 10 ug/L 10/28/1514:24 1 10 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 10 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 5.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 1.0 ug/L 10/28/1514:24 1 TestAmerica Savannah Page 49 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-RW-2-102215 Lab Sample ID: 680-118193-19 Date Collected: 10/22/15 09:28 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 105 70 - 130 10128115 14:24 1 Dibromofluoromethane (Surr) 100 70 - 130 10128115 14:24 1 1,2-Dichloroethane-d4 (Surr) 96 70- 130 10128115 14:24 1 Toluene-d8 (Surr) 101 70 - 130 10128115 14:24 1 0 TestAmerica Savannah Page 50 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-RW-3-102215 Lab Sample ID: 680-118193-20 Date Collected: 10/22/15 09:34 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride 3.4 Chlorobenzene ND Chloroethane ND Chloroform 1.1 Chloromethane ND cis-1,2-Dichloroethene 3.2 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane 1.3 1,2-Dichloroethane ND 1,1-Dichloroethene 10 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 7.5 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane 21 1,1,2-Trichloroethane ND Trichloroethene 58 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 15 ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 5.0 ug/L 10/30/1513:56 1 10 ug/L 10/30/1513:56 1 2.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 5.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 5.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 10 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 5.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 5.0 ug/L 10/30/1513:56 1 10 ug/L 10/30/1513:56 1 10 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 10 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 5.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 1.0 ug/L 10/30/1513:56 1 TestAmerica Savannah Page 51 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-RW-3-102215 Lab Sample ID: 680-118193-20 Date Collected: 10/22/15 09:34 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Xylenes, Total ND 1.0 ug/L Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 104 70 - 130 Dibromofluoromethane (Surr) 105 70 - 130 1,2-Dichloroethane-d4 (Surr) 110 70- 130 Toluene-d8 (Surr) 83 70 - 130 Prepared Analyzed Dil Fac 10/30/15 13:56 1 Prepared Analyzed Dil Fac 10130115 13:56 1 10130115 13:56 1 10130115 13:56 1 10130115 13:56 1 ' TestAmerica Savannah Page 52 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-RW-4-102215 Lab Sample ID: 680-118193-21 Date Collected: 10/22/15 09:15 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 31 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene 31 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 27 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane 18 1,1,2-Trichloroethane ND Trichloroethene 880 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 280 ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 100 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 50 ug/L 10/28/1517:52 10 100 ug/L 10/28/1517:52 10 20 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 50 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 50 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 100 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 50 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 50 ug/L 10/28/1517:52 10 100 ug/L 10/28/1517:52 10 100 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 100 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 50 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 10 ug/L 10/28/1517:52 10 TestAmerica Savannah Page 53 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-RW-4-102215 Lab Sample ID: 680-118193-21 Date Collected: 10/22/15 09:15 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 10 ug/L 10/28/15 17:52 10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 102 70 - 130 10128115 17:52 10 Dibromofluoromethane (Surr) 107 70 - 130 10128115 17:52 10 1,2-Dichloroethane-d4 (Surr) 108 70- 130 10/28/15 17:52 10 Toluene-d8 (Surr) 100 70 - 130 10/28/15 17:52 10 ' TestAmerica Savannah Page 54 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-RW-5-102215 Lab Sample ID: 680-118193-22 Date Collected: 10/22/15 09:22 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 190 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane 200 1,2-Dichloroethane ND 1,1-Dichloroethene 78 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 94 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane 98 1,1,2-Trichloroethane ND Trichloroethene 3400 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 9.1 ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 50 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 25 ug/L 10/29/1512:32 5 50 ug/L 10/29/1512:32 5 10 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 25 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 25 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 50 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 25 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 25 ug/L 10/29/1512:32 5 50 ug/L 10/29/1512:32 5 50 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 50 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 25 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 20 ug/L 10/28/1518:15 20 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 5.0 ug/L 10/29/1512:32 5 TestAmerica Savannah Page 55 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. TestAmerica Job ID: 680-118193-1 Project/Site: Murphy NC - IZ Client Sample ID: J1155-RW-5-102215 Lab Sample ID: 680-118193-22 Date Collected: 10/22/15 09:22 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 5.0 ug/L 10/29/15 12:32 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 103 70 - 130 10/28/15 18:15 20 4-Bromofluorobenzene (Surr) 93 70 - 130 10/29/15 12:32 5 Dibromofluoromethane (Surr) 103 70 - 130 10/28/15 18:15 20 Dibromofluoromethane (Surr) 101 70 - 130 10129115 12:32 5 ' 1,2-Dichloroethane-d4 (Surr) 100 70- 130 10128115 18:15 20 1,2-Dichloroethane-d4 (Surr) 101 70- 130 10129115 12:32 5 Toluene-d8 (Surr) 100 70 - 130 10128115 18:15 20 Toluene-d8 (Surr) 94 70 - 130 10129115 12:32 5 TestAmerica Savannah Page 56 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-DUP-1-101915 Lab Sample ID: 680-118193-23 Date Collected: 10/19/15 16:00 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 6.2 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane 1.5 1,2-Dichloroethane ND 1,1-Dichloroethene 2.2 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 3.4 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane 1.7 1,1,2-Trichloroethane ND Trichloroethene 39 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 2.2 ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 5.0 ug/L 10/28/1515:20 1 10 ug/L 10/28/1515:20 1 2.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 5.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 5.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 10 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 5.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 5.0 ug/L 10/28/1515:20 1 10 ug/L 10/28/1515:20 1 10 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 10 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 5.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 1.0 ug/L 10/28/1515:20 1 TestAmerica Savannah Page 57 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-DUP-1-101915 Lab Sample ID: 680-118193-23 Date Collected: 10/19/15 16:00 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Xylenes, Total ND 1.0 ug/L Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 98 70 - 130 Dibromofluoromethane (Surr) 112 70 - 130 1,2-Dichloroethane-d4 (Surr) 108 70- 130 Toluene-d8 (Surr) 101 70 - 130 Prepared Analyzed Dil Fac 10/28/15 15:20 1 Prepared Analyzed Dil Fac 10/28/15 15:20 1 10/28/15 15:20 1 10128115 15:20 1 10128115 15:20 1 ' TestAmerica Savannah Page 58 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-DUP-2-101915 Lab Sample ID: 680-118193-24 Date Collected: 10/19/15 16:00 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 5.0 ug/L 10/28/1515:42 1 10 ug/L 10/28/1515:42 1 2.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 5.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 5.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 10 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 5.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 5.0 ug/L 10/28/1515:42 1 10 ug/L 10/28/1515:42 1 10 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 10 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 5.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 1.0 ug/L 10/28/1515:42 1 TestAmerica Savannah Page 59 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-DUP-2-101915 Lab Sample ID: 680-118193-24 Date Collected: 10/19/15 16:00 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 70 - 130 10128115 15:42 1 Dibromofluoromethane (Surr) 110 70 - 130 10128115 15:42 1 1,2-Dichloroethane-d4 (Surr) 107 70- 130 10128115 15:42 1 Toluene-d8 (Surr) 103 70 - 130 10128115 15:42 1 0 TestAmerica Savannah Page 60 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-DUP-3-102115 Lab Sample ID: 680-118193-25 Date Collected: 10/21/15 16:00 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 5.0 ug/L 10/28/1514:48 1 10 ug/L 10/28/1514:48 1 2.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 5.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 5.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 10 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 5.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 5.0 ug/L 10/28/1514:48 1 10 ug/L 10/28/1514:48 1 10 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 10 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 5.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 1.0 ug/L 10/28/1514:48 1 TestAmerica Savannah Page 61 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-DUP-3-102115 Lab Sample ID: 680-118193-25 Date Collected: 10/21/15 16:00 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 103 70 - 130 10128115 14:48 1 Dibromofluoromethane (Surr) 101 70 - 130 10128115 14:48 1 1,2-Dichloroethane-d4 (Surr) 93 70- 130 10128115 14:48 1 Toluene-d8 (Surr) 101 70 - 130 10128115 14:48 1 0 TestAmerica Savannah Page 62 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-DUP-4-102115 Lab Sample ID: 680-118193-26 Date Collected: 10/21/15 16:00 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 980 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane 210 1,2-Dichloroethane ND 1,1-Dichloroethene 68 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 190 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 12000 Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 200 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 100 ug/L 10/28/1518:39 20 200 ug/L 10/28/1518:39 20 40 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 100 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 100 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 200 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 100 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 100 ug/L 10/28/1518:39 20 200 ug/L 10/28/1518:39 20 200 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 200 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 100 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 200 ug/L 10/29/1512:11 200 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 20 ug/L 10/28/1518:39 20 TestAmerica Savannah Page 63 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-DUP-4-102115 Lab Sample ID: 680-118193-26 Date Collected: 10/21/15 16:00 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 103 70 - 130 10128115 18:39 20 4-Bromofluorobenzene (Surr) 94 70 - 130 10129115 12:11 200 Dibromofluoromethane (Surr) 104 70 - 130 10128115 18:39 20 Dibromofluoromethane (Surr) 99 70 - 130 10129115 12:11 200 1,2-Dichloroethane-d4 (Surr) 104 70- 130 10128115 18:39 20 1,2-Dichloroethane-d4 (Surr) 96 70- 130 10129115 12:11 200 Toluene-d8 (Surr) 101 70 - 130 10/28/15 18:39 20 Toluene-d8 (Surr) 95 70 - 130 10/29/15 12:11 200 TestAmerica Savannah Page 64 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-EB-01-101915 Lab Sample ID: 680-118193-27 Date Collected: 10/19/15 17:03 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 5.0 ug/L 10/28/1512:06 1 10 ug/L 10/28/1512:06 1 2.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 5.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 5.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 10 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 5.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 5.0 ug/L 10/28/1512:06 1 10 ug/L 10/28/1512:06 1 10 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 10 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 5.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 1.0 ug/L 10/28/1512:06 1 TestAmerica Savannah Page 65 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-EB-01-101915 Lab Sample ID: 680-118193-27 Date Collected: 10/19/15 17:03 Matrix: Water Date Received: 10/23/15 09:44 I Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 70 - 130 10128115 12:06 1 Dibromofluoromethane (Surr) 108 70 - 130 10128115 12:06 1 1,2-Dichloroethane-d4 (Surr) 104 70- 130 10128115 12:06 1 Toluene-d8 (Surr) 103 70 - 130 10128115 12:06 1 0 TestAmerica Savannah Page 66 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-EB-02-102015 Lab Sample ID: 680-118193-28 Date Collected: 10/20/15 16:32 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 5.0 ug/L 10/28/1512:28 1 10 ug/L 10/28/1512:28 1 2.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 5.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 5.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 10 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 5.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 5.0 ug/L 10/28/1512:28 1 10 ug/L 10/28/1512:28 1 10 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 10 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 5.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 1.0 ug/L 10/28/1512:28 1 TestAmerica Savannah Page 67 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-EB-02-102015 Lab Sample ID: 680-118193-28 Date Collected: 10/20/15 16:32 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 98 70 - 130 10128115 12:28 1 Dibromofluoromethane (Surr) 110 70 - 130 10128115 12:28 1 1,2-Dichloroethane-d4 (Surr) 107 70- 130 10128115 12:28 1 Toluene-d8 (Surr) 103 70 - 130 10128115 12:28 1 0 TestAmerica Savannah Page 68 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-EB-03-102115 Lab Sample ID: 680-118193-29 Date Collected: 10/21/15 15:02 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 5.0 ug/L 10/28/1515:11 1 10 ug/L 10/28/1515:11 1 2.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 5.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 5.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 10 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 5.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 5.0 ug/L 10/28/1515:11 1 10 ug/L 10/28/1515:11 1 10 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 10 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 5.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 1.0 ug/L 10/28/1515:11 1 TestAmerica Savannah Page 69 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-EB-03-102115 Lab Sample ID: 680-118193-29 Date Collected: 10/21/15 15:02 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 104 70 - 130 10128115 15:11 1 Dibromofluoromethane (Surr) 98 70 - 130 10128115 15:11 1 1,2-Dichloroethane-d4 (Surr) 94 70- 130 10128115 15:11 1 Toluene-d8 (Surr) 100 70 - 130 10128115 15:11 1 0 TestAmerica Savannah Page 70 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-EB-04-102215 Lab Sample ID: 680-118193-30 Date Collected: 10/22/15 09:58 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 5.0 ug/L 10/28/1515:34 1 10 ug/L 10/28/1515:34 1 2.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 5.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 5.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 10 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 5.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 5.0 ug/L 10/28/1515:34 1 10 ug/L 10/28/1515:34 1 10 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 10 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 5.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 1.0 ug/L 10/28/1515:34 1 TestAmerica Savannah Page 71 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-EB-04-102215 Lab Sample ID: 680-118193-30 Date Collected: 10/22/15 09:58 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 102 70 - 130 10128115 15:34 1 Dibromofluoromethane (Surr) 100 70 - 130 10128115 15:34 1 1,2-Dichloroethane-d4 (Surr) 96 70- 130 10128115 15:34 1 Toluene-d8 (Surr) 100 70 - 130 10128115 15:34 1 0 TestAmerica Savannah Page 72 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-TB-01-101915 Lab Sample ID: 680-118193-31 Date Collected: 10/19/15 08:30 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 10 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 5.0 ug/L 10/28/1511:23 1 10 ug/L 10/28/1511:23 1 2.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 5.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 5.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 10 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 5.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 5.0 ug/L 10/28/1511:23 1 10 ug/L 10/28/1511:23 1 10 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 10 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 5.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 1.0 ug/L 10/28/1511:23 1 TestAmerica Savannah Page 73 of 98 11/5/2015 Client Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: J1155-TB-01-101915 Lab Sample ID: 680-118193-31 Date Collected: 10/19/15 08:30 Matrix: Water Date Received: 10/23/15 09:44 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 70 - 130 10128115 11:23 1 Dibromofluoromethane (Surr) 106 70 - 130 10128115 11:23 1 1,2-Dichloroethane-d4 (Surr) 103 70- 130 10128115 11:23 1 Toluene-d8 (Surr) 103 70 - 130 10128115 11:23 1 0 TestAmerica Savannah Page 74 of 98 11/5/2015 Surrogate Summary Client: GHD Services Inc. Project/Site: Murphy NC - IZ Method: 8260B - Volatile Organic Compounds (GC/MS) Matrix: Water TestAmerica Job ID: 680-118193-1 Prep Type: Total/NA Percent Surrogate Recovery (Acceptance Limits) Lab Sample ID Client Sample ID BFB (70-130) DBFM (70-130) 12DCE (70-130) TOL (70-130) 680-118193-1 J1155-MW-10-101915 99 109 106 101 680-118193-2 J1155-MW-11-101915 99 120 127 97 680-118193-3 J1155-MW-12-102115 91 99 96 94 680-118193-4 J1155-MW-13-102115 91 97 95 96 680-118193-5 J1155-MW-17-101915 98 110 107 101 680-118193-6 J1155-MW-20-101915 99 111 107 101 680-118193-7 J1155-MW-28-102115 99 120 124 94 680-118193-8 J1155-MW-32-101915 95 96 87 99 680-118193-9 J1155-MW-35-101915 101 110 107 102 680-118193-10 J1155-MW-36-102115 92 106 112 91 680-118193-11 J1155-MW-37-102115 96 115 116 100 680-118193-12 J1155-MW-45-101915 99 108 105 104 680-118193-13 J1155-SP-26-102215 103 98 93 100 680-118193-14 J1155-CMP-1-102115 103 101 92 100 680-118193-15 J1155-CMP-3-102115 105 99 95 99 680-118193-16 J 1 155-SW-3-102215 104 101 95 100 680-118193-17 J 1 155-SW-6-102215 102 99 95 99 680-118193-18 J1155-SW-10-102215 103 101 95 99 680-118193-19 J1155-RW-2-102215 105 100 96 101 680-118193-20 J1155-RW-3-102215 104 105 110 83 680-118193-21 J1155-RW-4-102215 102 107 108 100 680-118193-22 J1155-RW-5-102215 103 103 100 100 680-118193-22 J1155-RW-5-102215 93 101 101 94 680-118193-23 J1155-DUP-1-101915 98 112 108 101 680-118193-24 J1155-DUP-2-101915 100 110 107 103 680-118193-25 J1155-DUP-3-102115 103 101 93 101 680-118193-26 J1155-DUP-4-102115 103 104 104 101 680-118193-26 J1155-DUP-4-102115 94 99 96 95 680-118193-27 J1155-EB-01-101915 100 108 104 103 680-118193-28 J1155-EB-02-102015 98 110 107 103 680-118193-29 J1155-EB-03-102115 104 98 94 100 680-118193-30 J1155-EB-04-102215 102 100 96 100 680-118193-31 J1155-TB-01-101915 101 106 103 103 LCS 680-407738/4 Lab Control Sample 103 112 109 101 LCS 680-407966/4 Lab Control Sample 97 100 96 99 LCS 680-408184/4 Lab Control Sample 103 109 109 93 LCSD 680-407738/5 Lab Control Sample Dup 104 114 107 103 LCSD 680-407966/5 Lab Control Sample Dup 96 101 96 100 LCSD 680-408184/5 Lab Control Sample Dup 106 105 111 93 MB 680-407734/9 Method Blank 104 99 93 100 MB 680-407738/9 Method Blank 101 109 105 105 MB 680-407966/9 Method Blank 95 94 90 100 MB 680-408184/9 Method Blank 102 99 101 92 Surrogate Legend BFB = 4-Bromofluorobenzene (Surr) DBFM = Dibromofluoromethane (Surr) 12DCE = 1,2-Dichloroethane-d4 (Surr) TOL = Toluene-d8 (Surr) 0 TestAmerica Savannah Page 75 of 98 11/5/2015 QC Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Method: 8260B - Volatile Organic Compounds (GC/MS) Lab Sample ID: MB 680-407734/9 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 407734 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 10 ug/L 10/28/15 11:1 B 1 z endene ND 1.0 ug/L 10/28/15 11:1 B 1 zromofichloromethane ND 1.0 ug/L 10/28/15 11:1 B 1 z romo*orm ND 1.0 ug/L 10/28/15 11:1 B 1 z romomethane ND 5.0 ug/L 10/28/15 11:1 B 1 2-z utanone ND 10 ug/L 10/28/15 11:1 B 1 Carbon f isul if e ND 2.0 ug/L 10/28/15 11:1 B 1 Carbon tetrachlorif a ND 1.0 ug/L 10/28/15 11:1 B 1 Chlorobendene ND 1.0 ug/L 10/28/15 11:1 B 1 Chloroethane ND 5.0 ug/L 10/28/15 11:1 B 1 Chloro'orm ND 1.0 ug/L 10/28/15 11:1 B 1 Chloromethane ND 1.0 ug/L 10/28/15 11:1 B 1 cis-1,2-Dichloroethene ND 1.0 ug/L 10/28/15 11:1 B 1 cis-1,3-Dichloropropene ND 1.0 ug/L 10/28/15 11:1 B 1 Cyclohexane ND 1.0 ug/L 10/28/15 11:1 B 1 Dibromochloromethane ND 1.0 ug/L 10/28/15 11:1 B 1 1,2-Dibromo-3-Chloropropane ND 5.0 ug/L 10/28/15 11:1 B 1 1,2-Dibromoethane ND 1.0 ug/L 10/28/15 11:1 B 1 1,2-Dichlorobendene ND 1.0 ug/L 10/28/15 11:1 B 1 1,3-Dichlorobendene ND 1.0 ug/L 10/28/15 11:1 B 1 1,4-Dichlorobendene ND 1.0 ug/L 10/28/15 11:1 B 1 Dichlorof iluoromethane ND 1.0 ug/L 10/28/15 11:113 1 1,1-Dichloroethane ND 1.0 ug/L 10/28/15 11:1 B 1 1,2-Dichloroethane ND 1.0 ug/L 10/28/15 11:1 B 1 1,1-Dichloroethene ND 1.0 ug/L 10/28/15 11:1 B 1 1,2-Dichloropropane ND 1.0 ug/L 10/28/15 11:1 B 1 Ethylbendene ND 1.0 ug/L 10/28/15 11:1 B 1 2-Hexanone ND 10 ug/L 10/28/15 11:1 B 1 Isopropylbendene ND 1.0 ug/L 10/28/15 11:1 B 1 Methyl acetate ND 5.0 ug/L 10/28/15 11:1B 1 Methylcyclohexane ND 1.0 ug/L 10/28/15 11:1 B 1 Methylene Chlorif e ND 5.0 ug/L 10/28/15 11:1 B 1 4-Methyl-2-pentanone ND 10 ug/L 10/28/15 11:1 B 1 Methyl tert-butyl ether ND 10 ug/L 10/28/15 11:113 1 Styrene ND 1.0 ug/L 10/28/15 11:1 B 1 1,1,2,2-Tetrachloroethane ND 1.0 ug/L 10/28/1511:113 1 Tetrachloroethene ND 1.0 ug/L 10/28/1511:113 1 Tetrahyf ro"uran ND 10 ug/L 10/28/15 11:113 1 Toluene ND 1.0 ug/L 10/28/15 11:1 B 1 trans-1,2-Dichloroethene ND 1.0 ug/L 10/28/1511:113 1 trans-1,3-Dichloropropene ND 1.0 ug/L 10/28/1511:113 1 1,2,4-Trichlorobendene ND 5.0 ug/L 10/28/15 11:1 B 1 1,1,1-Trichloroethane ND 1.0 ug/L 10/28/1511:113 1 1,1,2-Trichloroethane ND 1.0 ug/L 10/28/1511:113 1 Trichloroethene ND 1.0 ug/L 10/28/1511:113 1 Trichloroluoromethane ND 1.0 ug/L 10/28/1511:113 1 1,1,2-Trichloro-1,2,2-triluoroethane ND 1.0 ug/L 10/28/1511:113 1 Vinyl chlorif a ND 1.0 ug/L 10/28/15 11:1B 1 TestAmerica Savannah Page 76 of 98 11/5/2015 QC Sample Results Client: GHD Services Inc. TestAmerica Job ID: 680-118193-1 Project/Site: Murphy NC - IZ Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 680-407734/9 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 407734 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 1.0 ug/L 10/28/15 11:1B 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 974 07 - 917 973 218 99530 9 Dibromofluoromethane (Surr) 07 - 917 973 218 99530 9 9,/ -Dichloroethane-d4 (Surr) :1 07 - 917 973 218 99530 9 6oluene-d2 (Surr) 977 07-917 973218 99TO 9 Lab Sample ID: MB 680-407738/9 Client Sample ID: Method Blank m Matrix: Water Prep Type: Total/NA Analysis Batch: 407738 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 10 ug/L 10/28/15 11:02 1 zendene ND 1.0 ug/L 10/28/15 11:02 1 zromofichloromethane ND 1.0 ug/L 10/28/15 11:02 1 zromo'orm ND 1.0 ug/L 10/28/15 11:02 1 zromomethane ND 5.0 ug/L 10/28/15 11:02 1 2-zutanone ND 10 ug/L 10/28/15 11:02 1 Carbon f isul if e ND 2.0 ug/L 10/28/15 11:02 1 Carbon tetrachlorif a ND 1.0 ug/L 10/28/15 11:02 1 Chlorobendene ND 1.0 ug/L 10/28/15 11:02 1 Chloroethane ND 5.0 ug/L 10/28/15 11:02 1 Chloro*orm ND 1.0 ug/L 10/28/15 11:02 1 Chloromethane ND 1.0 ug/L 10/28/15 11:02 1 cis-1,2-Dichloroethene ND 1.0 ug/L 10/28/15 11:02 1 cis-1,3-Dichloropropene ND 1.0 ug/L 10/28/15 11:02 1 Cyclohexane ND 1.0 ug/L 10/28/15 11:02 1 Dibromochloromethane ND 1.0 ug/L 10/28/15 11:02 1 1,2-Dibromo-3-Chloropropane ND 5.0 ug/L 10/28/15 11:02 1 1,2-Dibromoethane ND 1.0 ug/L 10/28/15 11:02 1 1,2-Dichlorobendene ND 1.0 ug/L 10/28/15 11:02 1 1,3-Dichlorobendene ND 1.0 ug/L 10/28/15 11:02 1 1,4-Dichlorobendene ND 1.0 ug/L 10/28/15 11:02 1 Dichlorof iluoromethane ND 1.0 ug/L 10/28/15 11:02 1 1,1-Dichloroethane ND 1.0 ug/L 10/28/15 11:02 1 1,2-Dichloroethane ND 1.0 ug/L 10/28/15 11:02 1 1,1-Dichloroethene ND 1.0 ug/L 10/28/15 11:02 1 1,2-Dichloropropane ND 1.0 ug/L 10/28/15 11:02 1 Ethylbendene ND 1.0 ug/L 10/28/15 11:02 1 2-Hexanone ND 10 ug/L 10/28/15 11:02 1 Isopropylbendene ND 1.0 ug/L 10/28/15 11:02 1 Methyl acetate ND 5.0 ug/L 10/28/15 11:02 1 Methylcyclohexane ND 1.0 ug/L 10/28/15 11:02 1 Methylene Chlorif e ND 5.0 ug/L 10/28/15 11:02 1 4-Methyl-2-pentanone ND 10 ug/L 10/28/15 11:02 1 Methyl tert-butyl ether ND 10 ug/L 10/28/15 11:02 1 Styrene ND 1.0 ug/L 10/28/15 11:02 1 TestAmerica Savannah Page 77 of 98 11/5/2015 QC Sample Results Client: GHD Services Inc. TestAmerica Job ID: 680-118193-1 Project/Site: Murphy NC - IZ Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 680-407738/9 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 407738 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,2,2-Tetrachloroethane ND 1.0 ug/L 10/28/15 11:02 1 Tetrachloroethene ND 1.0 ug/L 10/28/15 11:02 1 Tetrahyf ro*uran ND 10 ug/L 10/28/15 11:02 1 Toluene ND 1.0 ug/L 10/28/15 11:02 1 trans-1,2-Dichloroethene ND 1.0 ug/L 10/28/15 11:02 1 trans-1,3-Dichloropropene ND 1.0 ug/L 10/28/15 11:02 1 1,2,4-Trichlorobendene ND 5.0 ug/L 10/28/15 11:02 1 1,1,1-Trichloroethane ND 1.0 ug/L 10/28/15 11:02 1 1,1,2-Trichloroethane ND 1.0 ug/L 10/28/15 11:02 1 m Trichloroethene ND 1.0 ug/L 10/28/15 11:02 1 Trichloroluoromethane ND 1.0 ug/L 10/28/15 11:02 1 1,1,2-Trichloro-1,2,2-triluoroethane ND 1.0 ug/L 10/28/15 11:02 1 Vinyl chlorif e ND 1.0 ug/L 10/28/15 11:02 1 Xylenes, Total ND 1.0 ug/L 10/28/15 11:02 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 979 07 - 917 97,7218 999/ 9 Dibromofluoromethane (Surr) 97: 07 - 917 97,7218 999/ 9 9,/-Dichloroethane-d4 (Surr) 978 07 - 917 97,7218 999/ 9 6oluene-d2 (Surr) 978 07 - 917 9732189991 9 Lab Sample ID: LCS 680-407738/4 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 407738 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Acetone 250 188 ug/L B5 60-154 z endene 50.0 49.3 ug/L 99 133 -131 z romof ichloromethane 50.0 58.1 ug/L 116 BB-129 z romo*orm 50.0 58.0 ug/L 116 69 -135 z romomethane 50.0 56.5 ug/L 113 20 -180 2-z utanone 250 204 ug/L 82 135 -133 Carbon f isul if e 50.0 50.3 ug/L 101 B3 -12B Carbon tetrachlorif e 50.0 68.0 7 ug/L 136 135 -130 Chlorobendene 50.0 50.2 ug/L 100 80 -120 Chloroethane 50.0 55.5 ug/L ill 50 -151 Chloro*orm 50.0 54.6 ug/L 109 139 -122 Chloromethane 50.0 55.8 ug/L 112 63 -126 cis-1,2-Dichloroethene 50.0 55.5 ug/L 111 80 -122 cis-1,3-Dichloropropene 50.0 55.5 ug/L 111 80 -133 Cyclohexane 50.0 49.4 ug/L 99 69 -130 Dibromochloromethane 50.0 60.0 ug/L 120 B1 -136 1,2-Dibromo-3-Chloropropane 50.0 45.6 ug/L 91 59 -141 1,2-Dibromoethane 50.0 413.9 ug/L 96 BB-131 1,2-Dichlorobendene 50.0 51.0 ug/L 102 80 -120 1,3-Dichlorobendene 50.0 50.8 ug/L 102 80 -120 1,4-Dichlorobendene 50.0 48.6 ug/L 96 80 -120 Dichlorof iluoromethane 50.0 55.5 ug/L ill 51 -140 TestAmerica Savannah Page 78 of 98 11/5/2015 QC Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 680-407738/4 Matrix: Water Analysis Batch: 407738 Analyte 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene 1,2-Dichloropropane Ethylbendene 2-Hexanone Isopropylbendene Methyl acetate Methylcyclohexane Methylene Chlorif e 4-M ethyl-2-pentan one Methyl tert-butyl ether Styrene 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahyf ro"uran Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene 1,2,4-Trichlorobendene 1,1,1-Trich loroethane 1,1,2-Trich loroethane Trichloroethene Trichloro"luoromethane 1,1,2-Trich loro-1,2,2-tri"luoroetha ne Vinyl chlorif e Xylenes, Total Surrogate 4-Bromofluorobenzene (Surr) Dibromofluoromethane (Surr) 9,/-Dichloroethane-d4 (Surr) 6oluene-d2 (Surr) LCS LCS %Recovery Qualifier 971 991 97: 979 Lab Sample ID: LCSD 680-40773815 Matrix: Water Analysis Batch: 407738 Analyte Acetone z endene z romof ichloromethane z romo*orm z romomethane 2-z utanone Carbon f isul f e Carbon tetrachlorif e TestAmerica Job ID: 680-118193-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 50.0 53.4 ug/L 10B 80 -120 50.0 54.6 ug/L 109 B5 -130 50.0 51.5 ug/L 103 134-125 50.0 51.3 ug/L 103 80 -123 50.0 49.3 ug/L 99 80 -120 250 209 ug/L 84 130-141 50.0 50.5 ug/L 101 80-120 250 212 ug/L 85 66-134 50.0 48.6 ug/L 96 B5 -12B 50.0 51.5 ug/L 103 B6-129 250 212 ug/L 85 B5-135 50.0 48.6 ug/L 913 B4 -135 50.0 50.1 ug/L 100 80 -122 50.0 40.9 ug/L 82 B2 -128 50.0 52.4 ug/L 105 1313-123 100 BB.B ug/L B9 69 -129 50.0 50.4 ug/L 101 80 -122 50.0 50.1 ug/L 100 138 -123 50.0 58.13 ug/L 11 B 134 -140 50.0 52.9 ug/L 106 1313-131 50.0 61.5 ug/L 123 B4-128 50.0 413.1 ug/L 94 139 -125 50.0 53.3 ug/L 10B 80 -123 50.0 60.2 ug/L 120 58 -145 50.0 54.3 ug/L 109 65 -131 50.0 54.3 ug/L 109 68 -132 100 102 ug/L 102 80 -120 Limits 07-917 07 - 917 07 - 917 07-917 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike LCSD LCSD %Rec. RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 250 185 ug/L 134 60-154 2 40 50.0 49.13 ug/L 99 133-131 1 30 50.0 59.0 ug/L 118 1313-129 1 20 50.0 513.9 ug/L 116 69 -135 0 20 50.0 55.6 ug/L 111 20 -180 2 40 250 193 ug/L BB B5-133 6 30 50.0 49.9 ug/L 100 133 -12B 1 20 50.0 613.5 7 ug/L 135 135 -130 1 20 TestAmerica Savannah Page 79 of 98 11/5/2015 QC Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 680-407738/5 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 407738 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Chlorobendene 50.0 50.6 ug/L 101 80-120 1 20 Chloroethane 50.0 56.1 ug/L 112 50 -151 1 30 Chloro'orm 50.0 54.9 ug/L 110 B9 -122 1 20 Chloromethane 50.0 55.6 ug/L ill 63 -126 0 30 cis-1,2-Dichloroethene 50.0 55.4 ug/L ill 80 -122 0 20 cis-1,3-Dichloropropene 50.0 55.5 ug/L ill 80 -133 0 20 Cyclohexane 50.0 48.6 ug/L 913 69 -130 2 30 Dibromochloromethane 50.0 60.2 ug/L 120 B1 -136 0 20 1,2-Dibromo-3-Chloropropane 50.0 46.3 ug/L 93 59 -141 2 30 m 1,2-Dibromoethane 50.0 413.0 ug/L 94 1313-131 2 30 1,2-Dichlorobendene 50.0 51.1 ug/L 102 80 -120 0 20 1,3-Dichlorobendene 50.0 50.13 ug/L 101 80 -120 0 20 1,4-Dichlorobendene 50.0 49.4 ug/L 99 80 -120 2 20 Dichlorof i"luoromethane 50.0 52.3 ug/L 105 51 -140 6 40 1,1-Dichloroethane 50.0 53.8 ug/L 108 80-120 1 20 1,2-Dichloroethane 50.0 53.6 ug/L 10B B5 -130 2 20 1,1-Dichloroethene 50.0 51.0 ug/L 102 134-125 1 20 1,2-Dichloropropane 50.0 51.13 ug/L 103 80 -123 1 20 Ethylbendene 50.0 49.6 ug/L 99 80 -120 1 20 2-Hexanone 250 205 ug/L 82 BO-141 2 40 Isopropylbendene 50.0 50.6 ug/L 101 80 -120 0 20 Methyl acetate 250 208 ug/L 83 66 -134 2 30 Methylcyclohexane 50.0 413.6 ug/L 95 135 -126 2 30 Methylene Chlorif e 50.0 51.8 ug/L 104 136 -129 1 20 4-Methyl-2-pentanone 250 209 ug/L 84 135 -135 1 30 Methyl tert-butyl ether 50.0 413.9 ug/L 96 134 -135 2 20 Styrene 50.0 50.2 ug/L 100 80 -122 0 20 1,1,2,2-Tetrachloroethane 50.0 40.9 ug/L 82 132-128 0 20 Tetrachloroethene 50.0 52.1 ug/L 104 BB-123 1 20 Tetrahyf ro"uran 100 1313.1 ug/L BB 69 -129 2 30 Toluene 50.0 50.0 ug/L 100 80 -122 1 20 trans-1,2-Dichloroethene 50.0 50.8 ug/L 102 138 -123 1 20 trans-1,3-Dichloropropene 50.0 513.8 ug/L 116 134 -140 1 20 1,2,4-Trichlorobendene 50.0 54.0 ug/L 108 BB-131 2 20 1,1,1-Trichloroethane 50.0 59.9 ug/L 120 134-128 3 20 1,1,2-Trichloroethane 50.0 413.1 ug/L 94 139-125 0 20 Trichloroethene 50.0 53.6 ug/L 10B 80 -123 1 20 Trichloro"luoromethane 50.0 513.1 ug/L 114 58 -145 5 30 1,1,2-Trichloro-1,2,2-tri1uoroetha 50.0 52.4 ug/L 105 65-131 4 30 ne Vinyl chlorif e 50.0 54.0 ug/L 108 68 -132 0 30 Xylenes, Total 100 103 ug/L 103 80 -120 1 20 LCSD LCSD Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 974 07-917 Dibromofluoromethane (Surr) 994 07-917 9,/ -Dichloroethane-d4 (Surr) 970 07 - 917 6oluene-d2 (Surr) 971 07-917 TestAmerica Savannah Page 80 of 98 11/5/2015 QC Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 680-407966/9 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 407966 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 10 ug/L 10/29/15 09:58 1 z endene ND 1.0 ug/L 10/29/15 09:58 1 z romof ichloromethane ND 1.0 ug/L 10/29/15 09:58 1 z romo*orm ND 1.0 ug/L 10/29/15 09:58 1 z romomethane ND 5.0 ug/L 10/29/15 09:58 1 2-z utanone ND 10 ug/L 10/29/15 09:58 1 Carbon f isul if e ND 2.0 ug/L 10/29/15 09:58 1 Carbon tetrachlorif a ND 1.0 ug/L 10/29/15 09:58 1 Chlorobendene ND 1.0 ug/L 10/29/15 09:58 1 Chloroethane ND 5.0 ug/L 10/29/15 09:58 1 Chloro'orm ND 1.0 ug/L 10/29/15 09:58 1 Chloromethane ND 1.0 ug/L 10/29/15 09:58 1 cis-1,2-Dichloroethene ND 1.0 ug/L 10/29/15 09:58 1 cis-1,3-Dichloropropene ND 1.0 ug/L 10/29/15 09:58 1 Cyclohexane ND 1.0 ug/L 10/29/15 09:58 1 Dibromochloromethane ND 1.0 ug/L 10/29/15 09:58 1 1,2-Dibromo-3-Chloropropane ND 5.0 ug/L 10/29/15 09:58 1 1,2-Dibromoethane ND 1.0 ug/L 10/29/15 09:58 1 1,2-Dichlorobendene ND 1.0 ug/L 10/29/15 09:58 1 1,3-Dichlorobendene ND 1.0 ug/L 10/29/15 09:58 1 1,4-Dichlorobendene ND 1.0 ug/L 10/29/15 09:58 1 Dichlorof iluoromethane ND 1.0 ug/L 10/29/15 09:58 1 1,1-Dichloroethane ND 1.0 ug/L 10/29/15 09:58 1 1,2-Dichloroethane ND 1.0 ug/L 10/29/15 09:58 1 1,1-Dichloroethene ND 1.0 ug/L 10/29/15 09:58 1 1,2-Dichloropropane ND 1.0 ug/L 10/29/15 09:58 1 Ethylbendene ND 1.0 ug/L 10/29/15 09:58 1 2-Hexanone ND 10 ug/L 10/29/15 09:58 1 Isopropylbendene ND 1.0 ug/L 10/29/15 09:58 1 Methyl acetate ND 5.0 ug/L 10/29/15 09:58 1 Methylcyclohexane ND 1.0 ug/L 10/29/15 09:58 1 Methylene Chlorif e ND 5.0 ug/L 10/29/15 09:58 1 4-Methyl-2-pentanone ND 10 ug/L 10/29/15 09:58 1 Methyl tert-butyl ether ND 10 ug/L 10/29/15 09:58 1 Styrene ND 1.0 ug/L 10/29/15 09:58 1 1,1,2,2-Tetrachloroethane ND 1.0 ug/L 10/29/15 09:58 1 Tetrachloroethene ND 1.0 ug/L 10/29/15 09:58 1 Tetrahyf ro"uran ND 10 ug/L 10/29/15 09:58 1 Toluene ND 1.0 ug/L 10/29/15 09:58 1 trans-1,2-Dichloroethene ND 1.0 ug/L 10/29/15 09:58 1 trans-1,3-Dichloropropene ND 1.0 ug/L 10/29/15 09:58 1 1,2,4-Trichlorobendene ND 5.0 ug/L 10/29/15 09:58 1 1,1,1-Trichloroethane ND 1.0 ug/L 10/29/15 09:58 1 1,1,2-Trichloroethane ND 1.0 ug/L 10/29/15 09:58 1 Trichloroethene ND 1.0 ug/L 10/29/15 09:58 1 Trichloroluoromethane ND 1.0 ug/L 10/29/15 09:58 1 1,1,2-Trichloro-1,2,2-triluoroethane ND 1.0 ug/L 10/29/15 09:58 1 Vinyl chlorif a ND 1.0 ug/L 10/29/15 09:58 1 TestAmerica Savannah Page 81 of 98 11/5/2015 QC Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 680-407966/9 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 407966 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 1.0 ug/L 10/29/15 09:58 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) : 8 07 - 917 973: 18 7: 532 9 Dibromofluoromethane (Surr) : 4 07-917 973: 18 7: 532 9 9,/ -Dichloroethane-d4 (Surr) :7 07 - 917 973: 18 7: 532 9 6oluene-d2 (Surr) 977 07-917 973: 18 7: 532 9 Lab Sample ID: LCS 680-407966/4 Matrix: Water Analysis Batch: 407966 Analyte Acetone z endene z romof ichloromethane z romo'orm z romomethane 2-z utanone Carbon f isullf e Carbon tetrachlorif e Chlorobendene Chloroethane Chloro*orm Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Cyclohexane Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane 1,2-Dichlorobendene 1,3-Dichlorobendene 1,4-Dichlorobendene Dichlorof iluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene 1,2-Dichloropropane Ethylbendene 2-Hexanone Isopropylbendene Methyl acetate Methylcyclohexane Methylene Chlorif e 4-M ethyl-2-pentan one Methyl tert-butyl ether Styrene Client Sample ID: Lab Control Sample m Prep Type: Total/NA Spike Added LCS LCS Result Qualifier Unit D %Rec %Rec. Limits 250 238 ug/L 95 60-154 50.0 413.3 ug/L 95 B3 -131 50.0 49.4 ug/L 99 1313-129 50.0 51.5 ug/L 103 69 -135 50.0 66.4 ug/L 133 20 -180 250 246 ug/L 98 B5-133 50.0 46.1 ug/L 92 B3 -12B 50.0 49.1 ug/L 98 B5 -130 50.0 49.6 ug/L 99 80 -120 50.0 48.4 ug/L 96 50 -151 50.0 413.8 ug/L 96 B9 -122 50.0 45.2 ug/L 90 63 -126 50.0 45.5 ug/L 91 80-122 50.0 48.8 ug/L 98 80-133 50.0 49.13 ug/L 99 69 -130 50.0 51.5 ug/L 103 B1 -136 50.0 48.5 ug/L 9B 59 -141 50.0 51.6 ug/L 103 1313-131 50.0 48.5 ug/L 913 80 -120 50.0 48.6 ug/L 913 80 -120 50.0 413.8 ug/L 96 80 -120 50.0 40.3 ug/L 81 51-140 50.0 46.0 ug/L 92 80-120 50.0 46.8 ug/L 94 B5-130 50.0 46.2 ug/L 92 134 -125 50.0 46.3 ug/L 93 80-123 50.0 49.3 ug/L 99 80-120 250 22B ug/L 91 BO -141 50.0 51.3 ug/L 103 80-120 250 219 ug/L 88 66-134 50.0 50.13 ug/L 101 B5 -12B 50.0 50.5 ug/L 101 B6-129 250 221 ug/L 89 B5-135 50.0 49.1 ug/L 98 B4 -135 50.0 50.3 ug/L 101 80-122 Page 82 of 98 TestAmerica Savannah 11 /5/2015 QC Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 680-407966/4 Matrix: Water Analysis Batch: 407966 TestAmerica Job ID: 680-118193-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits 1,1,2,2-Tetrachloroethane 50.0 48.0 ug/L 96 B2-128 Tetrachloroethene 50.0 49.4 ug/L 99 1313-123 Tetrahyf ro*uran 100 91.4 ug/L 91 69 -129 Toluene 50.0 49.2 ug/L 98 80 -122 trans-1,2-Dichloroethene 50.0 48.4 ug/L 913 138 -123 trans-1,3-Dichloropropene 50.0 50.6 ug/L 101 134 -140 1,2,4-Trichlorobendene 50.0 46.1 ug/L 92 1313-131 1,1,1-Trichloroethane 50.0 413.6 ug/L 95 B4-128 1,1,2-Trichloroethane 50.0 49.2 ug/L 98 B9-125 Trichloroethene 50.0 49.4 ug/L 99 80 -123 Trichloro"luoromethane 50.0 48.5 ug/L 913 58 -145 1,1,2-Trichloro-1,2,2-tri"luoroetha 50.0 413.4 ug/L 95 65-131 ne Vinyl chlorif e 50.0 49.9 ug/L 100 68 -132 Xylenes, Total 100 99.5 ug/L 100 80 -120 LCS LCS Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) : 0 07 - 917 Dibromofluoromethane (Surr) 977 07-917 9,/-Dichloroethane-d4 (Surr) : T 07-917 6oluene-d2 (Surr) 07 - 917 Lab Sample ID: LCSD 680-407966/5 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 407966 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Acetone 250 239 u -g/ L 96 60-154 0 40 z endene 50.0 48.4 ug/L 96 B3 -131 2 30 z romof ichloromethane 50.0 49.8 ug/L 100 1313-129 1 20 z romo"orm 50.0 51.9 ug/L 104 69 -135 1 20 z romomethane 50.0 64.8 ug/L 130 20 -180 3 40 2-z utanone 250 245 ug/L 98 B5 -133 0 30 Carbon f isul if e 50.0 46.6 ug/L 93 B3 -12B 1 20 Carbon tetrachlorif e 50.0 49.0 ug/L 98 B5 -130 0 20 Chlorobendene 50.0 50.3 ug/L 101 80-120 1 20 Chloroethane 50.0 44.4 ug/L 89 50 -151 9 30 Chloro'orm 50.0 48.6 ug/L 913 139 -122 2 20 Chloromethane 50.0 41.2 ug/L 82 63 -126 9 30 cis-1,2-Dichloroethene 50.0 45.13 ug/L 91 80 -122 0 20 cis-1,3-Dichloropropene 50.0 49.6 ug/L 99 80 -133 2 20 Cyclohexane 50.0 48.9 ug/L 98 69 -130 2 30 Dibromochloromethane 50.0 50.9 ug/L 102 131 -136 1 20 1,2-Dibromo-3-Chloropropane 50.0 49.5 ug/L 99 59 -141 2 30 1,2-Dibromoethane 50.0 51.4 ug/L 103 1313-131 0 30 1,2-Dichlorobendene 50.0 50.1 ug/L 100 80 -120 3 20 1,3-Dichlorobendene 50.0 49.6 ug/L 99 80 -120 2 20 1,4-Dichlorobendene 50.0 48.6 ug/L 913 80 -120 2 20 TestAmerica Savannah Page 83 of 98 11/5/2015 QC Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 680-407966/5 Matrix: Water Analysis Batch: 407966 TestAmerica Job ID: 680-118193-1 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Dichlorof iluoromethane 50.0 39.5 ug/L B9 51 -140 2 40 1,1-Dichloroethane 50.0 46.4 ug/L 93 80-120 1 20 1,2-Dichloroethane 50.0 413.4 ug/L 95 B5 -130 1 20 1,1-Dichloroethene 50.0 42.5 ug/L 85 B4-125 8 20 1,2-Dichloropropane 50.0 413.3 ug/L 95 80 -123 2 20 Ethylbendene 50.0 49.13 ug/L 99 80 -120 1 20 2-Hexanone 250 22B ug/L 91 BO-141 0 40 Isopropylbendene 50.0 51.8 ug/L 104 80 -120 1 20 Methyl acetate 250 218 ug/L 86 66 -134 0 30 m Methylcyclohexane 50.0 50.2 ug/L 100 135 -12B 1 30 Methylene Chlorif e 50.0 51.4 ug/L 103 136 -129 2 20 4-Methyl-2-pentanone 250 223 ug/L 89 135 -135 1 30 Methyl tert-butyl ether 50.0 49.0 ug/L 98 134 -135 0 20 Styrene 50.0 51.1 ug/L 102 80 -122 2 20 1,1,2,2-Tetrachloroethane 50.0 48.6 ug/L 96 132-128 2 20 Tetrachloroethene 50.0 50.1 ug/L 100 BB-123 1 20 Tetrahyf ro*uran 100 93.9 ug/L 94 69 -129 3 30 Toluene 50.0 49.4 ug/L 99 80 -122 0 20 trans-1,2-Dichloroethene 50.0 48.9 ug/L 98 138 -123 1 20 trans-1,3-Dichloropropene 50.0 50.6 ug/L 101 134 -140 0 20 1,2,4-Trichlorobendene 50.0 413.1 ug/L 94 BB-131 2 20 1,1,1-Trichloroethane 50.0 48.4 ug/L 96 134-128 2 20 1,1,2-Trichloroethane 50.0 49.0 ug/L 98 139-125 1 20 Trichloroethene 50.0 50.2 ug/L 100 80 -123 2 20 Trichloroluoromethane 50.0 42.9 ug/L 86 58 -145 12 30 1,1,2-Trichloro-1,2,2-triluoroetha 50.0 46.3 ug/L 93 65-131 2 30 ne Vinyl chlorif e 50.0 49.1 ug/L 98 68 -132 2 30 Xylenes, Total 100 101 ug/L 101 80 -120 1 20 LCSD LCSD Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) : T 07 - 917 Dibromofluoromethane (Surr) 979 07-917 9,/-Dichloroethane-d4 (Surr) : T 07-917 6oluene-d2 (Surr) 977 07 - 917 Lab Sample ID: MB 680-408184/9 Matrix: Water Analysis Batch: 408184 Analyte MB MB Result Qualifier Acetone ND zendene ND z romof ichloromethane ND z romo*orm ND z romomethane ND 2-z utanone ND Carbon f isullf e ND RL MDL Unit D 10 ug/L 1.0 ug/L 1.0 ug/L 1.0 ug/L 5.0 ug/L 10 ug/L 2.0 ug/L Client Sample ID: Method Blank Prep Type: Total/NA Prepared Analyzed Dil Fac 10/30/15 08:213 1 10/30/15 08:213 1 10/30/15 08:213 1 10/30/15 08:213 1 10/30/15 08:213 1 10/30/15 08:213 1 10/30/15 08:213 1 Page 84 of 98 TestAmerica Savannah 11 /5/2015 QC Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 680-408184/9 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 408184 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Carbon tetrachlorif a ND 1.0 ug/L 10/30/15 08:213 1 Chlorobendene ND 1.0 ug/L 10/30/15 08:213 1 Chloroethane ND 5.0 ug/L 10/30/15 08:213 1 Chloro'orm ND 1.0 ug/L 10/30/15 08:213 1 Chloromethane ND 1.0 ug/L 10/30/15 08:213 1 cis-1,2-Dichloroethene ND 1.0 ug/L 10/30/15 08:213 1 cis-1,3-Dichloropropene ND 1.0 ug/L 10/30/15 08:213 1 Cyclohexane ND 1.0 ug/L 10/30/15 08:213 1 Dibromochloromethane ND 1.0 ug/L 10/30/15 08:213 1 1,2-Dibromo-3-Chloropropane ND 5.0 ug/L 10/30/1508:213 1 1,2-Dibromoethane ND 1.0 ug/L 10/30/1508:213 1 1,2-Dichlorobendene ND 1.0 ug/L 10/30/1508:213 1 1,3-Dichlorobendene ND 1.0 ug/L 10/30/1508:213 1 1,4-Dichlorobendene ND 1.0 ug/L 10/30/1508:213 1 Dichlorof i"luoromethane ND 1.0 ug/L 10/30/15 08:213 1 1,1-Dichloroethane ND 1.0 ug/L 10/30/1508:213 1 1,2-Dichloroethane ND 1.0 ug/L 10/30/1508:213 1 1,1-Dichloroethene ND 1.0 ug/L 10/30/1508:213 1 1,2-Dichloropropane ND 1.0 ug/L 10/30/1508:213 1 Ethylbendene ND 1.0 ug/L 10/30/15 08:213 1 2-Hexanone ND 10 ug/L 10/30/15 08:213 1 Isopropylbendene ND 1.0 ug/L 10/30/15 08:213 1 Methyl acetate ND 5.0 ug/L 10/30/15 08:213 1 Methylcyclohexane ND 1.0 ug/L 10/30/15 08:213 1 Methylene Chlorif e ND 5.0 ug/L 10/30/15 08:213 1 4-Methyl-2-pentanone ND 10 ug/L 10/30/15 08:213 1 Methyl tert-butyl ether ND 10 ug/L 10/30/15 08:213 1 Styrene ND 1.0 ug/L 10/30/15 08:213 1 1,1,2,2-Tetrachloroethane ND 1.0 ug/L 10/30/1508:213 1 Tetrachloroethene ND 1.0 ug/L 10/30/15 08:213 1 Tetrahyf ro"uran ND 10 ug/L 10/30/15 08:213 1 Toluene ND 1.0 ug/L 10/30/15 08:213 1 trans-1,2-Dichloroethene ND 1.0 ug/L 10/30/1508:213 1 trans-1,3-Dichloropropene ND 1.0 ug/L 10/30/1508:213 1 1,2,4-Trichlorobendene ND 5.0 ug/L 10/30/1508:213 1 1,1,1-Trichloroethane ND 1.0 ug/L 10/30/1508:213 1 1,1,2-Trichloroethane ND 1.0 ug/L 10/30/1508:213 1 Trichloroethene ND 1.0 ug/L 10/30/15 08:213 1 Trichloro'luoromethane ND 1.0 ug/L 10/30/15 08:213 1 1,1,2-Trichloro-1,2,2-tri"luoroethane ND 1.0 ug/L 10/30/1508:213 1 Vinyl chlorif a ND 1.0 ug/L 10/30/15 08:213 1 Xylenes, Total ND 1.0 ug/L 10/30/15 08:213 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 97/ 07 - 917 97317W 729 0 9 Dibromofluoromethane (Surr) 07 - 917 97317W 729 0 9 9,/-Dichloroethane-d4 (Surr) 979 07-917 97317W 7250 9 6oluene-d2 (Surr) : / 07-917 9731718 7290 9 TestAmerica Savannah Page 85 of 98 11/5/2015 QC Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 680-408184/4 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 408184 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Acetone 250 244 ug/L 98 60-154 z endene 50.0 49.6 ug/L 99 B3 -131 z romof ichloromethane 50.0 54.13 ug/L 109 1313-129 z romo*orm 50.0 54.0 ug/L 108 69 -135 z romomethane 50.0 80.9 ug/L 162 20 -180 2-z utanone 250 304 ug/L 122 B5 -133 Carbon f isul if e 50.0 45.3 ug/L 91 B3 -12B Carbon tetrachlorif e 50.0 56.9 ug/L 114 B5 -130 Chlorobendene 50.0 48.1 ug/L 96 80 -120 Chloroethane 50.0 51.0 ug/L 102 50 -151 Chloro'orm 50.0 55.6 ug/L 111 B9 -122 Chloromethane 50.0 53.8 ug/L 108 63 -126 cis-1,2-Dichloroethene 50.0 58.5 ug/L 11 B 80 -122 cis-1,3-Dichloropropene 50.0 54.8 ug/L 110 80 -133 Cyclohexane 50.0 56.0 ug/L 112 69 -130 Dibromochloromethane 50.0 50.1 ug/L 100 B1 -136 1,2-Dibromo-3-Chloropropane 50.0 52.1 ug/L 104 59 -141 1,2-Dibromoethane 50.0 48.4 ug/L 913 1313-131 1,2-Dichlorobendene 50.0 49.9 ug/L 100 80 -120 1,3-Dichlorobendene 50.0 50.3 ug/L 101 80 -120 1,4-Dichlorobendene 50.0 413.9 ug/L 96 80 -120 Dichlorof iluoromethane 50.0 46.3 ug/L 93 51 -140 1,1-Dichloroethane 50.0 54.9 ug/L 110 80-120 1,2-Dichloroethane 50.0 53.8 ug/L 108 B5 -130 1,1-Dichloroethene 50.0 49.6 ug/L 99 B4-125 1,2-Dichloropropane 50.0 52.0 ug/L 104 80 -123 Ethylbendene 50.0 51.5 ug/L 103 80 -120 2-Hexanone 250 236 ug/L 94 BO-141 Isopropylbendene 50.0 52.5 ug/L 105 80 -120 Methyl acetate 250 238 ug/L 95 66 -134 Methylcyclohexane 50.0 50.0 ug/L 100 135 -12B Methylene Chlorif e 50.0 413.5 ug/L 95 136 -129 4-Methyl-2-pentanone 250 252 ug/L 101 135 -135 Methyl tert-butyl ether 50.0 54.9 ug/L 110 134 -135 Styrene 50.0 51.5 ug/L 103 80 -122 1,1,2,2-Tetrachloroethane 50.0 51.3 ug/L 103 132-128 Tetrachloroethene 50.0 49.0 ug/L 98 BB-123 Tetrahyf ro"uran 100 11 B ug/L 11 B 69 -129 Toluene 50.0 45.9 ug/L 92 80 -122 trans-1,2-Dichloroethene 50.0 52.9 ug/L 106 B8 -123 trans-1,3-Dichloropropene 50.0 52.5 ug/L 105 134 -140 1,2,4-Trichlorobendene 50.0 55.8 ug/L 112 BB-131 1,1,1-Trichloroethane 50.0 55.4 ug/L 111 134-128 1,1,2-Trichloroethane 50.0 49.0 ug/L 98 139-125 Trichloroethene 50.0 50.0 ug/L 100 80 -123 Trichloroluoromethane 50.0 59.3 ug/L 119 58 -145 1,1,2-Trichloro-1,2,2-triluoroetha 50.0 54.0 ug/L 108 65-131 ne TestAmerica Savannah Page 86 of 98 11/5/2015 QC Sample Results Client: GHD Services Inc. TestAmerica Job ID: 680-118193-1 Project/Site: Murphy NC - IZ Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 680-408184/4 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 408184 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Vinyl chlorif e 50.0 49.9 ug/L 100 68 -132 Xylenes, Total 100 101 ug/L 101 80 -120 LCS LCS Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 971 07 - 917 Dibromofluoromethane (Surr) 97: 07 - 917 9,/ -Dichloroethane-d4 (Surr) 97: 07 - 917 6oluene-d2 (Surr) : 1 07-917 Lab Sample ID: LCSD 680-408184/5 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 408184 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Acetone 250 24B ug/L 99 60 -154 1 40 z endene 50.0 49.1 ug/L 98 B3 -131 1 30 z romof ichloromethane 50.0 54.0 ug/L 108 1313-129 1 20 z romo'orm 50.0 54.3 ug/L 109 69 -135 1 20 z romomethane 50.0 80.0 ug/L 160 20 -180 1 40 2-z utanone 250 298 ug/L 119 135 -133 2 30 Carbon f isul if e 50.0 44.6 ug/L 89 133 -12B 2 20 Carbon tetrachlorif e 50.0 54.3 ug/L 109 B5 -130 5 20 Chlorobendene 50.0 48.3 ug/L 913 80 -120 0 20 Chloroethane 50.0 51.2 ug/L 102 50 -151 0 30 Chloro*orm 50.0 53.0 ug/L 106 B9 -122 5 20 Chloromethane 50.0 51.9 ug/L 104 63 -126 4 30 cis-1,2-Dichloroethene 50.0 55.3 ug/L 111 80 -122 6 20 cis-1,3-Dichloropropene 50.0 54.1 ug/L 108 80 -133 1 20 Cyclohexane 50.0 53.2 ug/L 106 69 -130 5 30 Dibromochloromethane 50.0 50.1 ug/L 100 B1 -136 0 20 1,2-Dibromo-3-Chloropropane 50.0 55.9 ug/L 112 59 -141 B 30 1,2-Dibromoethane 50.0 49.2 ug/L 98 1313-131 2 30 1,2-Dichlorobendene 50.0 52.0 ug/L 104 80 -120 4 20 1,3-Dichlorobendene 50.0 51.0 ug/L 102 80 -120 1 20 1,4-Dichlorobendene 50.0 49.2 ug/L 98 80 -120 3 20 Dichlorof iluoromethane 50.0 46.0 ug/L 92 51 -140 1 40 1,1-Dichloroethane 50.0 55.8 ug/L 112 80-120 2 20 1,2-Dichloroethane 50.0 54.9 ug/L 110 B5 -130 2 20 1,1-Dichloroethene 50.0 413.8 ug/L 96 134-125 4 20 1,2-Dichloropropane 50.0 51.6 ug/L 103 80 -123 1 20 Ethylbendene 50.0 51.0 ug/L 102 80 -120 1 20 2-Hexanone 250 241 ug/L 96 BO-141 2 40 Isopropylbendene 50.0 51.3 ug/L 103 80 -120 2 20 Methyl acetate 250 244 ug/L 98 66 -134 2 30 Methylcyclohexane 50.0 49.6 ug/L 99 135 -126 1 30 Methylene Chlorif e 50.0 413.1 ug/L 94 136 -129 1 20 4-Methyl-2-pentanone 250 258 ug/L 103 135 -135 2 30 Methyl tert-butyl ether 50.0 56.6 ug/L 113 134 -135 3 20 TestAmerica Savannah Page 87 of 98 11/5/2015 QC Sample Results Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 680-408184/5 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 408184 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Styrene 50.0 51.2 ug/L 102 80 -122 1 20 1,1,2,2-Tetrachloroethane 50.0 51.6 ug/L 103 B2-128 0 20 Tetrachloroethene 50.0 48.2 ug/L 96 1313-123 2 20 Tetrahyf ro*uran 100 110 ug/L 110 69 -129 B 30 Toluene 50.0 46.4 ug/L 93 80 -122 1 20 trans-1,2-Dichloroethene 50.0 53.0 ug/L 106 B8 -123 0 20 trans-1,3-Dichloropropene 50.0 53.1 ug/L 106 B4 -140 1 20 1,2,4-Trichlorobendene 50.0 56.8 ug/L 114 1313-131 2 20 1,1,1-Trichloroethane 50.0 52.4 ug/L 105 B4-128 5 20 m 1,1,2-Trichloroethane 50.0 49.5 ug/L 99 B9-125 1 20 Trichloroethene 50.0 49.8 ug/L 100 80 -123 0 20 Trichloro"luoromethane 50.0 513.2 ug/L 114 58 -145 4 30 1,1,2-Trichloro-1,2,2-tri"luoroetha 50.0 53.6 ug/L 10B 65-131 1 30 ne Vinyl chlorif e 50.0 49.4 ug/L 99 68 -132 1 30 Xylenes, Total 100 100 ug/L 100 80 -120 0 20 LCSD LCSD Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 97T 07 - 917 Dibromofluoromethane (Surr) 978 07-917 9,/-Dichloroethane-d4 (Surr) 999 07-917 6oluene-d2 (Surr) :1 07 - 917 TestAmerica Savannah Page 88 of 98 11/5/2015 Lab Chronicle Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: A 155-MW-10-101915 Lab Sample ID: 680-118193-1 Date Collected: 10/19/15 11:36 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407738 10/28/15 13:33 - CEJ TAL SAT Client Sample ID: J1155-MW-11-101915 Lab Sample ID: 680-118193-2 Date Collected: 10/19/15 10:54 Matrix: Water Date Received: 10/23/15 09:44 F Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 2 407738 10/28/15 16:03 CEJ TAL SAV Client Sample ID: J1155-MW-12-102115 Lab Sample ID: 680-118193-3 m Date Collected: 10/21/15 14:25 Matrix: Water Date Received: 10/23/15 09:44 F Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 20 407966 10/29/15 11:07 - CEJ TAL SAT Client Sample ID: A 155-MW-13-102115 Lab Sample ID: 680-118193-4 Date Collected: 10/21/15 13:27 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 5 407966 10/29/15 11:28 CEJ TAL SAV Client Sample ID: A 155-MW-17-101915 Lab Sample ID: 680-118193-5 Date Collected: 10/19/15 13:16 Matrix: Water Date Received: 10/23/15 09:44 F Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 407738 10/28/15 13:54 CEJ TAL SAV Client Sample ID: A 155-MW-20-101915 Lab Sample ID: 680-118193-6 Date Collected: 10/19/15 12:01 Matrix: Water Date Received: 10/23/15 09:44 F Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407738 10/28/15 14:16 CEJ TAL SAV TestAmerica Savannah Page 89 of 98 11/5/2015 Lab Chronicle Client: GHD Services Inc. TestAmerica Job ID: 680-118193-1 Project/Site: Murphy NC - IZ Client Sample ID: A 155-MW-28-102115 Lab Sample ID: 680-118193-7 Date Collected: 10/21/15 12:34 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260E 5 407738 10/28/15 17:08 CEJ TAL SAV Client Sample ID: J1155-MW-32-101915 Lab Sample ID: 680-118193-8 Date Collected: 10/19/15 12:34 Matrix: Water Date Received: 10/23/15 09:44 F Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 407966 10/29/15 10:25 CEJ TAL SAV Client Sample ID: J1155-MW-35-101915 Date Collected: 10/19/15 14:39 Date Received: 10/23/15 09:44 Batch Batch Dilution Prep Type Type Method Run Factor Total/NA Analysis 8260B 1 Lab Sample ID: 680-118193-9 m Matrix: Water Batch Prepared Number or Analyzed Analyst Lab 407738 10/28/15 14:37 CEJ TAL SAV Client Sample ID: J1155-MW-36-102115 Lab Sample ID: 680-118193-10 Date Collected: 10/21/15 12:53 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260E 2 407966 10/29/15 11:49 CEJ TAL SAV Client Sample ID: J1155-MW-37-102115 Lab Sample ID: 680-118193-11 Date Collected: 10/21/15 14:00 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 100 407738 10/28/15 18:12 CEJ TAL SAV Client Sample ID: J1155-MW-45-101915 Lab Sample ID: 680-118193-12 Date Collected: 10/19/15 13:53 Matrix: Water Date Received: 10/23/15 09:44 F Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407738 10/28/15 14:58 CEJ TAL SAV TestAmerica Savannah Page 90 of 98 11/5/2015 Lab Chronicle Client: GHD Services Inc. Project/Site: Murphy NC - IZ Client Sample ID: A 155-SP-26-102215 Date Collected: 10/22/15 09:45 Date Received: 10/23/15 09:44 Batch Prep Type Type Total/NA Analysis Batch Method Run 8260E TestAmerica Job ID: 680-118193-1 Lab Sample ID: 680-118193-13 Matrix: Water Dilution Batch Prepared Factor Number or Analyzed Analyst Lab 1 407734 10/28/15 12:06 CEJ TAL SAV Client Sample ID: A 155-CMP-1-102115 Lab Sample ID: 680-118193-14 Date Collected: 10/21/15 11:10 Matrix: Water Date Received: 10/23/15 09:44 F Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 407734 10/28/15 12:29 CEJ TAL SAV Client Sample ID: J1155-CMP-3-102115 Date Collected: 10/21/15 11:21 Date Received: 10/23/15 09:44 Batch Batch Dilution Prep Type Type Method Run Factor Total/NA Analysis 8260B 1 Lab Sample ID: 680-118193-15 m Matrix: Water Batch Prepared Number or Analyzed Analyst Lab 407734 10/28/15 12:52 CEJ TAL SAV Client Sample ID: J1155-SW-3-102215 Lab Sample ID: 680-118193-16 Date Collected: 10/22/15 10:16 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 407734 10/28/15 13:15 CEJ TAL SAV Client Sample ID: J1155-SW-6-102215 Lab Sample ID: 680-118193-17 Date Collected: 10/22/15 09:55 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407734 10/28/15 13:38 CEJ TAL SAV Client Sample ID: J1155-SW-10-102215 Lab Sample ID: 680-118193-18 Date Collected: 10/22/15 10:03 Matrix: Water Date Received: 10/23/15 09:44 F Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407734 10/28/15 14:01 CEJ TAL SAV Page 91 of 98 TestAmerica Savannah 11 /5/2015 Lab Chronicle Client: GHD Services Inc. TestAmerica Job ID: 680-118193-1 Project/Site: Murphy NC - IZ Client Sample ID: A 155-RW-2-102215 Lab Sample ID: 680-118193-19 Date Collected: 10/22/15 09:28 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 407734 10/28/15 14:24 CEJ TAL SAV Client Sample ID: A 155-RW-3-102215 Lab Sample ID: 680-118193-20 Date Collected: 10/22/15 09:34 Matrix: Water Date Received: 10/23/15 09:44 F Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 408184 10/30/15 13:56 CEJ TAL SAV Client Sample ID: A 155-RW-4-102215 Date Collected: 10/22/15 09:15 Date Received: 10/23/15 09:44 F Batch Batch Dilution Prep Type Type Method Run Factor Total/NA Analysis 8260B 10 Lab Sample ID: 680-118193-21 Matrix: Water m Batch Prepared Number or Analyzed Analyst Lab 407734 10/28/15 17:52 CEJ TAL SAV Client Sample ID: J1155-RW-5-102215 Lab Sample ID: 680-118193-22 Date Collected: 10/22/15 09:22 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 82606 20 407734 10/28/15 18:15 CEJ TAL SAT- Total/NA Analysis 8260E 5 407966 10/29/15 12:32 CEJ TAL SAV Client Sample ID: A155-DUP-1-101915 Lab Sample ID: 680-118193-23 Date Collected: 10/19/15 16:00 Matrix: Water Date Received: 10/23/15 09:44 1 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407738 10/28/15 15:20 CEJ TAL SAV Client Sample ID: A 155-DUP-2-101915 Lab Sample ID: 680-118193-24 Date Collected: 10/19/15 16:00 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407738 10/28/15 15:42 CEJ TAL SAV TestAmerica Savannah Page 92 of 98 11/5/2015 Lab Chronicle Client: GHD Services Inc. Project/Site: Murphy NC - IZ TestAmerica Job ID: 680-118193-1 Client Sample ID: A 155-DUP-3-102115 Lab Sample ID: 680-118193-25 Date Collected: 10/21/15 16:00 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 407734 10/28/15 14:48 CEJ TAL SAV Client Sample ID: A 155-DUP-4-102115 Lab Sample ID: 680-118193-26 Date Collected: 10/21/15 16:00 Matrix: Water Date Received: 10/23/15 09:44 F Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 20 407734 10/28/15 18:39 CEJ TAL SAV Total/NA Analysis 8260B 200 407966 10/29/15 12:11 CEJ TAL SAV Client Sample ID: A 155-EB-01-101915 Lab Sample ID: 680-118193-27 m Date Collected: 10/19/15 17:03 Matrix: Water W �� Date Received: 10/23/15 09:44 ■� Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407738 10/28/15 12:06 CEJ TAL SAV Client Sample ID: A 155-EB-02-102015 Lab Sample ID: 680-118193-28 Date Collected: 10/20/15 16:32 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 407738 10/28/15 12:28 CEJ TAL SAV Client Sample ID: A 155-EB-03-102115 Lab Sample ID: 680-118193-29 Date Collected: 10/21/15 15:02 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407734 10/28/15 15:11 CEJ TAL SAV Client Sample ID: A 155-EB-04-102215 Lab Sample ID: 680-118193-30 Date Collected: 10/22/15 09:58 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407734 10/28/15 15:34 CEJ TAL SAV TestAmerica Savannah Page 93 of 98 11/5/2015 Lab Chronicle Client: GHD Services Inc. Project/Site: Murphy NC - IZ Client Sample ID: J1155-TB-01-101915 Date Collected: 10/19/15 08:30 Date Received: 10/23/15 09:44 TestAmerica Job ID: 680-118193-1 Lab Sample ID: 680-118193-31 Matrix: Water Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407738 10/28/15 11:23 CEJ TAL SAV Laboratory References: TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 TestAmerica Savannah Page 94 of 98 11/5/2015 dpOasn � ;a uieu� g6 i8 b 1-(799 t z o c O pl O m� `m uu� L TZ E EE U n V LO o� r C Jo¢bza N o v 7k .. 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UX wO `�� y�q? N rn �� YlL 'C❑�, fl. iq T Ll N 4 71 U d �� aE c 9 ¢ 02 m N mC9 of ar w n �� 7 �� N y O� 4 Q1 C] E w a V Page 97 of 98 11 /5/2015 Certification Summary Client: GHD Services Inc. Project/Site: Murphy NC - IZ Laboratory: TestAmerica Savannah The certifications listed below are applicable to this report. TestAmerica Job ID: 680-118193-1 Authority Program EPA Region Certification ID Expiration Date North Carolina (DW) State Program 4 13701 07-31-16 TestAmerica Savannah Page 98 of 98 11/5/2015 TestAmerica ° THE LEADER IN ENVIRONMENTAL TESTING ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Nashville 2960 Foster Creighton Drive Nashville, TN 37204 Tel: (615)726-0177 TestAmerica Job ID: 490-90373-1 TestAmerica Sample Delivery Group: 55912-J1155 Client Project/Site: Murphy, NC Revision: 1 For: Dextra Group 1205 Johnson Ferry Road Suite 136-446 Marietta, Georgia 30068 Attn: Kurt Batsel Rj "j Q.hI L- 6a*i/' rVIS Authorized for release by. 111612015 2:18:04 PM Roxanne Cisneros, Senior Project Manager (615)301-5761 rxanne.cisneros@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 S DG: 55912-J 1155 Table of Contents Cover Page .............................................. 1 Table of Contents ......................................... 2 Sample Summary ......................................... 3 Case Narrative ........................................... 4 Definitions ............................................... 5 Client Sample Results ...................................... 6 QC Sample Results ........................................ 40 QC Association ........................................... 47 Chronicle................................................ 48 Method Summary ......................................... 51 Certification Summary ...................................... 52 Chain of Custody .......................................... 53 Receipt Checklists ......................................... 56 Field Data Sheets ......................................... 57 12 13 14 TestAmerica Nashville Page 2 of 79 11 /6/2015 Sample Summary Client: Dextra Group TestAmerica Job ID: 490-90373-1 Project/Site: Murphy, NC SDG: 55912-J1155 Lab Sample ID Client Sample ID Matrix Collected Received 490-90373-1 J1155-MW-23-102115 Water 10/21/15 09:56 10/23/15 10:00 490-90373-2 J1155-MW-25-102115 Water 10/21/15 09:33 10/23/15 10:00 490-90373-3 J 1 155-MW-33-102015 Water 10/20/15 13:06 10/23/15 10:00 490-90373-4 J 1 155-MW-34-102015 Water 10/20/15 11:39 10/23/15 10:00 490-90373-5 J 1 155-MW-40-102015 Water 10/20/15 13:44 10/23/15 10:00 490-90373-6 J 1 155-MW-41-102015 Water 10/20/15 11:09 10/23/15 10:00 490-90373-7 J 1 155-MW-44-102015 Water 10/20/15 12:27 10/23/15 10:00 490-90373-8 J 1 155-MW-46-102015 Water 10/20/15 10:13 10/23/15 10:00 490-90373-9 J 1 155-MW-47-102015 Water 10/20/15 09:55 10/23/15 10:00 490-90373-10 J 1 155-MW-60-102015 Water 10/20/1514:43 10/23/15 10:00 490-90373-11 J 1 155-MW-61-102015 Water 10/20/15 15:23 10/23/15 10:00 490-90373-12 J1155-MW-62-102115 Water 10/21/1510:53 10/23/15 10:00 490-90373-13 J1155-MW-63-102115 Water 10/21/1510:22 10/23/15 10:00 490-90373-14 J 1 155-MW-64-102015 Water 10/20/1514:15 10/23/15 10:00 490-90373-15 J1155-PW-9-102115 Water 10/21/1511:59 10/23/15 10:00 490-90373-16 A155-CMP-4-102115 Water 10/21/1511:29 10/23/15 10:00 490-90373-17 A 155-Trip Blank-101915 Water 10/19/15 08:30 10/23/15 10:00 12 13 14 TestAmerica Nashville Page 3 of 79 11 /6/2015 Case Narrative Client: Dextra Group Project/Site: Murphy, NC Job ID: 490-90373-1 Laboratory: TestAmerica Nashville Narrative TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 F47 Job Narrative 490-90373-1 Comments Revised Report to include field data sheets Receipt The samples were received on 10/23/2015 10:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 4.41 C. GC/MS VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. 12 13 14 TestAmerica Nashville Page 4 of 79 11 /6/2015 Definitions/Glossary Client: Dextra Group TestAmerica Job ID: 490-90373-1 Project/Site: Murphy, NC SDG: 55912-J1155 Qualifiers GC/MS VOA Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. tt Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit Is ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit M QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Nashville Page 5 of 79 11 /6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-23-102115 Lab Sample ID: 490-90373-1 Date Collected: 10/21/15 09:56 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 0.898 Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/30/15 20:16 1 0.500 0.200 ug/L 10/30/15 20:16 1 0.500 0.170 ug/L 10/30/15 20:16 1 0.500 0.290 ug/L 10/30/15 20:16 1 0.500 0.350 ug/L 10/30/15 20:16 1 50.0 2.64 ug/L 10/30/15 20:16 1 0.500 0.220 ug/L 10/30/15 20:16 1 0.500 0.180 ug/L 10/30/15 20:16 1 0.500 0.180 ug/L 10/30/15 20:16 1 0.500 0.360 ug/L 10/30/15 20:16 1 0.500 0.230 ug/L 10/30/15 20:16 1 0.500 0.360 ug/L 10/30/15 20:16 1 0.500 0.210 ug/L 10/30/15 20:16 1 0.500 0.170 ug/L 10/30/15 20:16 1 1.00 0.130 ug/L 10/30/15 20:16 1 0.500 0.250 ug/L 10/30/15 20:16 1 5.00 0.940 ug/L 10/30/15 20:16 1 0.500 0.210 ug/L 10/30/15 20:16 1 0.500 0.190 ug/L 10/30/15 20:16 1 0.500 0.180 ug/L 10/30/15 20:16 1 0.500 0.170 ug/L 10/30/15 20:16 1 0.500 0.170 ug/L 10/30/15 20:16 1 0.500 0.240 ug/L 10/30/15 20:16 1 0.500 0.200 ug/L 10/30/15 20:16 1 0.500 0.250 ug/L 10/30/15 20:16 1 0.500 0.250 ug/L 10/30/15 20:16 1 0.500 0.190 ug/L 10/30/15 20:16 1 5.00 1.28 ug/L 10/30/15 20:16 1 1.00 0.330 ug/L 10/30/15 20:16 1 10.0 0.580 ug/L 10/30/15 20:16 1 0.500 0.0900 ug/L 10/30/15 20:16 1 5.00 0.220 ug/L 10/30/15 20:16 1 5.00 0.810 ug/L 10/30/15 20:16 1 0.500 0.170 ug/L 10/30/15 20:16 1 0.500 0.280 ug/L 10/30/15 20:16 1 0.500 0.190 ug/L 10/30/15 20:16 1 0.500 0.140 ug/L 10/30/15 20:16 1 5.00 0.820 ug/L 10/30/15 20:16 1 0.500 0.170 ug/L 10/30/15 20:16 1 0.500 0.230 ug/L 10/30/15 20:16 1 0.500 0.170 ug/L 10/30/15 20:16 1 0.500 0.200 ug/L 10/30/15 20:16 1 0.500 0.190 ug/L 10/30/15 20:16 1 0.500 0.190 ug/L 10/30/15 20:16 1 0.500 0.200 ug/L 10/30/15 20:16 1 0.500 0.210 ug/L 10/30/15 20:16 1 1.00 0.150 ug/L 10/30/15 20:16 1 0.500 0.180 ug/L 10/30/15 20:16 1 1.00 0.580 ug/L 10/30/15 20:16 1 Page 6 of 79 TestAmerica Nashville 11 /6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J1155 Client Sample ID: J1155-MW-23-102115 Lab Sample ID: 490-90373-1 Date Collected: 10/21/15 09:56 Matrix: Water Date Received: 10/23/15 10:00 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 99 70 - 130 10130112 8051: 1 Dibromofluoromethane (Surr) 99 70 - 130 10130112 8051: 1 1,8-Dichloroethane-d4 (Surr) 99 70- 130 10130112 8051: 1 6oluene-dT (Surr) 100 70 - 130 10130112 8051: 1 12 13 14 TestAmerica Nashville Page 7 of 79 11 /6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-25-102115 Lab Sample ID: 490-90373-2 Date Collected: 10/21/15 09:33 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 1.16 Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/30/15 20:45 1 0.500 0.200 ug/L 10/30/15 20:45 1 0.500 0.170 ug/L 10/30/15 20:45 1 0.500 0.290 ug/L 10/30/15 20:45 1 0.500 0.350 ug/L 10/30/15 20:45 1 50.0 2.64 ug/L 10/30/15 20:45 1 0.500 0.220 ug/L 10/30/15 20:45 1 0.500 0.180 ug/L 10/30/15 20:45 1 0.500 0.180 ug/L 10/30/15 20:45 1 0.500 0.360 ug/L 10/30/15 20:45 1 0.500 0.230 ug/L 10/30/15 20:45 1 0.500 0.360 ug/L 10/30/15 20:45 1 0.500 0.210 ug/L 10/30/15 20:45 1 0.500 0.170 ug/L 10/30/15 20:45 1 1.00 0.130 ug/L 10/30/15 20:45 1 0.500 0.250 ug/L 10/30/15 20:45 1 5.00 0.940 ug/L 10/30/15 20:45 1 0.500 0.210 ug/L 10/30/15 20:45 1 0.500 0.190 ug/L 10/30/15 20:45 1 0.500 0.180 ug/L 10/30/15 20:45 1 0.500 0.170 ug/L 10/30/15 20:45 1 0.500 0.170 ug/L 10/30/15 20:45 1 0.500 0.240 ug/L 10/30/15 20:45 1 0.500 0.200 ug/L 10/30/15 20:45 1 0.500 0.250 ug/L 10/30/15 20:45 1 0.500 0.250 ug/L 10/30/15 20:45 1 0.500 0.190 ug/L 10/30/15 20:45 1 5.00 1.28 ug/L 10/30/15 20:45 1 1.00 0.330 ug/L 10/30/15 20:45 1 10.0 0.580 ug/L 10/30/15 20:45 1 0.500 0.0900 ug/L 10/30/15 20:45 1 5.00 0.220 ug/L 10/30/15 20:45 1 5.00 0.810 ug/L 10/30/15 20:45 1 0.500 0.170 ug/L 10/30/15 20:45 1 0.500 0.280 ug/L 10/30/15 20:45 1 0.500 0.190 ug/L 10/30/15 20:45 1 0.500 0.140 ug/L 10/30/15 20:45 1 5.00 0.820 ug/L 10/30/15 20:45 1 0.500 0.170 ug/L 10/30/15 20:45 1 0.500 0.230 ug/L 10/30/15 20:45 1 0.500 0.170 ug/L 10/30/15 20:45 1 0.500 0.200 ug/L 10/30/15 20:45 1 0.500 0.190 ug/L 10/30/15 20:45 1 0.500 0.190 ug/L 10/30/15 20:45 1 0.500 0.200 ug/L 10/30/15 20:45 1 0.500 0.210 ug/L 10/30/15 20:45 1 1.00 0.150 ug/L 10/30/15 20:45 1 0.500 0.180 ug/L 10/30/15 20:45 1 1.00 0.580 ug/L 10/30/15 20:45 1 Page 8 of 79 TestAmerica Nashville 11 /6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J1155 Client Sample ID: J1155-MW-25-102115 Lab Sample ID: 490-90373-2 Date Collected: 10/21/15 09:33 Matrix: Water Date Received: 10/23/15 10:00 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 108 70 - 130 10130112 80512 1 Dibromofluoromethane (Surr) 99 70 - 130 10130112 8002 1 1,8-Dichloroethane-d4 (Surr) 97 70- 130 10130112 8002 1 6oluene-dT (Surr) 101 70 - 130 10130112 80512 1 12 13 14 TestAmerica Nashville Page 9 of 79 11 /6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-33-102015 Lab Sample ID: 490-90373-3 Date Collected: 10/20/15 13:06 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 0.503 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 0.146 J Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 8.05 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 0.334 J ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/30/15 21:13 1 0.500 0.200 ug/L 10/30/15 21:13 1 0.500 0.170 ug/L 10/30/15 21:13 1 0.500 0.290 ug/L 10/30/15 21:13 1 0.500 0.350 ug/L 10/30/15 21:13 1 50.0 2.64 ug/L 10/30/15 21:13 1 0.500 0.220 ug/L 10/30/15 21:13 1 0.500 0.180 ug/L 10/30/15 21:13 1 0.500 0.180 ug/L 10/30/15 21:13 1 0.500 0.360 ug/L 10/30/15 21:13 1 0.500 0.230 ug/L 10/30/15 21:13 1 0.500 0.360 ug/L 10/30/15 21:13 1 0.500 0.210 ug/L 10/30/15 21:13 1 0.500 0.170 ug/L 10/30/15 21:13 1 1.00 0.130 ug/L 10/30/15 21:13 1 0.500 0.250 ug/L 10/30/15 21:13 1 5.00 0.940 ug/L 10/30/15 21:13 1 0.500 0.210 ug/L 10/30/15 21:13 1 0.500 0.190 ug/L 10/30/15 21:13 1 0.500 0.180 ug/L 10/30/15 21:13 1 0.500 0.170 ug/L 10/30/15 21:13 1 0.500 0.170 ug/L 10/30/15 21:13 1 0.500 0.240 ug/L 10/30/15 21:13 1 0.500 0.200 ug/L 10/30/15 21:13 1 0.500 0.250 ug/L 10/30/15 21:13 1 0.500 0.250 ug/L 10/30/15 21:13 1 0.500 0.190 ug/L 10/30/15 21:13 1 5.00 1.28 ug/L 10/30/15 21:13 1 1.00 0.330 ug/L 10/30/15 21:13 1 10.0 0.580 ug/L 10/30/15 21:13 1 0.500 0.0900 ug/L 10/30/15 21:13 1 5.00 0.220 ug/L 10/30/15 21:13 1 5.00 0.810 ug/L 10/30/15 21:13 1 0.500 0.170 ug/L 10/30/15 21:13 1 0.500 0.280 ug/L 10/30/15 21:13 1 0.500 0.190 ug/L 10/30/15 21:13 1 0.500 0.140 ug/L 10/30/15 21:13 1 5.00 0.820 ug/L 10/30/15 21:13 1 0.500 0.170 ug/L 10/30/15 21:13 1 0.500 0.230 ug/L 10/30/15 21:13 1 0.500 0.170 ug/L 10/30/15 21:13 1 0.500 0.200 ug/L 10/30/15 21:13 1 0.500 0.190 ug/L 10/30/15 21:13 1 0.500 0.190 ug/L 10/30/15 21:13 1 0.500 0.200 ug/L 10/30/15 21:13 1 0.500 0.210 ug/L 10/30/15 21:13 1 1.00 0.150 ug/L 10/30/15 21:13 1 0.500 0.180 ug/L 10/30/15 21:13 1 TestAmerica Nashville Page 10 of 79 11/6/2015 Client Sample Results Client: Dextra Group TestAmerica Job ID: 490-90373-1 Project/Site: Murphy, NC SDG: 55912-J1155 Client Sample ID: J1155-MW-33-102015 Lab Sample ID: 490-90373-3 Date Collected: 10/20/15 13:06 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 1.00 0.580 ug/L 10/30/15 21:13 1 Surrogate %Recovery Qualifier Limits • Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 70 - 130 10130112 81513 1 Dibromofluoromethane (Surr) 108 70 - 130 10130112 81513 1 1,8-Dichloroethane-d4 (Surr) 9: 70- 130 10130112 81513 1 6oluene-dT (Surr) 9T 70 - 130 10130112 81513 1 12 13 14 TestAmerica Nashville Page 11 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-34-102015 Lab Sample ID: 490-90373-4 Date Collected: 10/20/15 11:39 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 0.597 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 0.188 J Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 8.97 Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/30/15 21:42 1 0.500 0.200 ug/L 10/30/15 21:42 1 0.500 0.170 ug/L 10/30/15 21:42 1 0.500 0.290 ug/L 10/30/15 21:42 1 0.500 0.350 ug/L 10/30/15 21:42 1 50.0 2.64 ug/L 10/30/15 21:42 1 0.500 0.220 ug/L 10/30/15 21:42 1 0.500 0.180 ug/L 10/30/15 21:42 1 0.500 0.180 ug/L 10/30/15 21:42 1 0.500 0.360 ug/L 10/30/15 21:42 1 0.500 0.230 ug/L 10/30/15 21:42 1 0.500 0.360 ug/L 10/30/15 21:42 1 0.500 0.210 ug/L 10/30/15 21:42 1 0.500 0.170 ug/L 10/30/15 21:42 1 1.00 0.130 ug/L 10/30/15 21:42 1 0.500 0.250 ug/L 10/30/15 21:42 1 5.00 0.940 ug/L 10/30/15 21:42 1 0.500 0.210 ug/L 10/30/15 21:42 1 0.500 0.190 ug/L 10/30/15 21:42 1 0.500 0.180 ug/L 10/30/15 21:42 1 0.500 0.170 ug/L 10/30/15 21:42 1 0.500 0.170 ug/L 10/30/15 21:42 1 0.500 0.240 ug/L 10/30/15 21:42 1 0.500 0.200 ug/L 10/30/15 21:42 1 0.500 0.250 ug/L 10/30/15 21:42 1 0.500 0.250 ug/L 10/30/15 21:42 1 0.500 0.190 ug/L 10/30/15 21:42 1 5.00 1.28 ug/L 10/30/15 21:42 1 1.00 0.330 ug/L 10/30/15 21:42 1 10.0 0.580 ug/L 10/30/15 21:42 1 0.500 0.0900 ug/L 10/30/15 21:42 1 5.00 0.220 ug/L 10/30/15 21:42 1 5.00 0.810 ug/L 10/30/15 21:42 1 0.500 0.170 ug/L 10/30/15 21:42 1 0.500 0.280 ug/L 10/30/15 21:42 1 0.500 0.190 ug/L 10/30/15 21:42 1 0.500 0.140 ug/L 10/30/15 21:42 1 5.00 0.820 ug/L 10/30/15 21:42 1 0.500 0.170 ug/L 10/30/15 21:42 1 0.500 0.230 ug/L 10/30/15 21:42 1 0.500 0.170 ug/L 10/30/15 21:42 1 0.500 0.200 ug/L 10/30/15 21:42 1 0.500 0.190 ug/L 10/30/15 21:42 1 0.500 0.190 ug/L 10/30/15 21:42 1 0.500 0.200 ug/L 10/30/15 21:42 1 0.500 0.210 ug/L 10/30/15 21:42 1 1.00 0.150 ug/L 10/30/15 21:42 1 0.500 0.180 ug/L 10/30/15 21:42 1 1.00 0.580 ug/L 10/30/15 21:42 1 TestAmerica Nashville Page 12 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J1155 Client Sample ID: J1155-MW-34-102015 Lab Sample ID: 490-90373-4 Date Collected: 10/20/15 11:39 Matrix: Water Date Received: 10/23/15 10:00 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 70 - 130 10130112 8108 1 Dibromofluoromethane (Surr) 100 70 - 130 10130112 8108 1 1,8-Dichloroethane-d4 (Surr) 99 70- 130 10130112 8108 1 6oluene-dT (Surr) 99 70 - 130 10130112 81518 1 12 13 14 TestAmerica Nashville Page 13 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-40-102015 Lab Sample ID: 490-90373-5 Date Collected: 10/20/15 13:44 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide 0.641 Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 0.243 J Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/30/15 22:10 1 0.500 0.200 ug/L 10/30/15 22:10 1 0.500 0.170 ug/L 10/30/15 22:10 1 0.500 0.290 ug/L 10/30/15 22:10 1 0.500 0.350 ug/L 10/30/15 22:10 1 50.0 2.64 ug/L 10/30/15 22:10 1 0.500 0.220 ug/L 10/30/15 22:10 1 0.500 0.180 ug/L 10/30/15 22:10 1 0.500 0.180 ug/L 10/30/15 22:10 1 0.500 0.360 ug/L 10/30/15 22:10 1 0.500 0.230 ug/L 10/30/15 22:10 1 0.500 0.360 ug/L 10/30/15 22:10 1 0.500 0.210 ug/L 10/30/15 22:10 1 0.500 0.170 ug/L 10/30/15 22:10 1 1.00 0.130 ug/L 10/30/15 22:10 1 0.500 0.250 ug/L 10/30/15 22:10 1 5.00 0.940 ug/L 10/30/15 22:10 1 0.500 0.210 ug/L 10/30/15 22:10 1 0.500 0.190 ug/L 10/30/15 22:10 1 0.500 0.180 ug/L 10/30/15 22:10 1 0.500 0.170 ug/L 10/30/15 22:10 1 0.500 0.170 ug/L 10/30/15 22:10 1 0.500 0.240 ug/L 10/30/15 22:10 1 0.500 0.200 ug/L 10/30/15 22:10 1 0.500 0.250 ug/L 10/30/15 22:10 1 0.500 0.250 ug/L 10/30/15 22:10 1 0.500 0.190 ug/L 10/30/15 22:10 1 5.00 1.28 ug/L 10/30/15 22:10 1 1.00 0.330 ug/L 10/30/15 22:10 1 10.0 0.580 ug/L 10/30/15 22:10 1 0.500 0.0900 ug/L 10/30/15 22:10 1 5.00 0.220 ug/L 10/30/15 22:10 1 5.00 0.810 ug/L 10/30/15 22:10 1 0.500 0.170 ug/L 10/30/15 22:10 1 0.500 0.280 ug/L 10/30/15 22:10 1 0.500 0.190 ug/L 10/30/15 22:10 1 0.500 0.140 ug/L 10/30/15 22:10 1 5.00 0.820 ug/L 10/30/15 22:10 1 0.500 0.170 ug/L 10/30/15 22:10 1 0.500 0.230 ug/L 10/30/15 22:10 1 0.500 0.170 ug/L 10/30/15 22:10 1 0.500 0.200 ug/L 10/30/15 22:10 1 0.500 0.190 ug/L 10/30/15 22:10 1 0.500 0.190 ug/L 10/30/15 22:10 1 0.500 0.200 ug/L 10/30/15 22:10 1 0.500 0.210 ug/L 10/30/15 22:10 1 1.00 0.150 ug/L 10/30/15 22:10 1 0.500 0.180 ug/L 10/30/15 22:10 1 1.00 0.580 ug/L 10/30/15 22:10 1 TestAmerica Nashville Page 14 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J1155 Client Sample ID: J1155-MW-40-102015 Lab Sample ID: 490-90373-5 Date Collected: 10/20/15 13:44 Matrix: Water Date Received: 10/23/15 10:00 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 108 70 - 130 10130112 88510 1 Dibromofluoromethane (Surr) 100 70 - 130 10130112 88510 1 1,8-Dichloroethane-d4 (Surr) 9T 70- 130 10130112 88510 1 6oluene-dT (Surr) 99 70 - 130 10130112 88510 1 12 13 14 TestAmerica Nashville Page 15 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-41-102015 Lab Sample ID: 490-90373-6 Date Collected: 10/20/15 11:09 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) 31.4 J Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 227 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane 0.889 1,1-Dichloroethane 17.4 1,2-Dichloroethane ND 1,1-Dichloroethene 10.8 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 17.9 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene 0.328 J trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 951 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 0.670 J ne Vinyl chloride 12.1 RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/31/15 03:22 1 0.500 0.200 ug/L 10/31/15 03:22 1 0.500 0.170 ug/L 10/31/15 03:22 1 0.500 0.290 ug/L 10/31/15 03:22 1 0.500 0.350 ug/L 10/31/15 03:22 1 50.0 2.64 ug/L 10/31/15 03:22 1 0.500 0.220 ug/L 10/31/15 03:22 1 0.500 0.180 ug/L 10/31/15 03:22 1 0.500 0.180 ug/L 10/31/15 03:22 1 0.500 0.360 ug/L 10/31/15 03:22 1 0.500 0.230 ug/L 10/31/15 03:22 1 0.500 0.360 ug/L 10/31/15 03:22 1 0.500 0.210 ug/L 10/31/15 03:22 1 0.500 0.170 ug/L 10/31/15 03:22 1 1.00 0.130 ug/L 10/31/15 03:22 1 0.500 0.250 ug/L 10/31/15 03:22 1 5.00 0.940 ug/L 10/31/15 03:22 1 0.500 0.210 ug/L 10/31/15 03:22 1 0.500 0.190 ug/L 10/31/15 03:22 1 0.500 0.180 ug/L 10/31/15 03:22 1 0.500 0.170 ug/L 10/31/15 03:22 1 0.500 0.170 ug/L 10/31/15 03:22 1 0.500 0.240 ug/L 10/31/15 03:22 1 0.500 0.200 ug/L 10/31/15 03:22 1 0.500 0.250 ug/L 10/31/15 03:22 1 0.500 0.250 ug/L 10/31/15 03:22 1 0.500 0.190 ug/L 10/31/15 03:22 1 5.00 1.28 ug/L 10/31/15 03:22 1 1.00 0.330 ug/L 10/31/15 03:22 1 10.0 0.580 ug/L 10/31/15 03:22 1 0.500 0.0900 ug/L 10/31/15 03:22 1 5.00 0.220 ug/L 10/31/15 03:22 1 5.00 0.810 ug/L 10/31/15 03:22 1 0.500 0.170 ug/L 10/31/15 03:22 1 0.500 0.280 ug/L 10/31/15 03:22 1 0.500 0.190 ug/L 10/31/15 03:22 1 0.500 0.140 ug/L 10/31/15 03:22 1 5.00 0.820 ug/L 10/31/15 03:22 1 0.500 0.170 ug/L 10/31/15 03:22 1 0.500 0.230 ug/L 10/31/15 03:22 1 0.500 0.170 ug/L 10/31/15 03:22 1 0.500 0.200 ug/L 10/31/15 03:22 1 0.500 0.190 ug/L 10/31/15 03:22 1 0.500 0.190 ug/L 10/31/15 03:22 1 5.00 2.00 ug/L 10/31/15 03:51 10 0.500 0.210 ug/L 10/31/15 03:22 1 1.00 0.150 ug/L 10/31/15 03:22 1 0.500 0.180 ug/L 10/31/15 03:22 1 TestAmerica Nashville Page 16 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-41-102015 Lab Sample ID: 490-90373-6 Date Collected: 10/20/15 11:09 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Xylenes, Total ND 1.00 0.580 ug/L Surrogate %Recovery Qualifier 4-Bromofluorobenzene (Surr) 108 4-Bromofluorobenzene (Surr) 108 Dibromofluoromethane (Surr) 9T Dibromofluoromethane (Surr) 100 1,8-Dichloroethane-d4 (Surr) 92 1,8-Dichloroethane-d4 (Surr) 9: 6oluene-dT (Surr) 100 6oluene-dT (Surr) 100 Limits 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 Prepared Analyzed Dil Fac 10/31/15 03:22 1 Analyzed Dil Fac 10131112 03838 1 10131112 0321 10 10131112 03838 1 10131112 03T 1 10 10131112 03538 1 10131112 03T 1 10 10131112 03,T8 1 10131112 0321 10 Page 17 of 79 TestAmerica Nashville 11 /6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-44-102015 Lab Sample ID: 490-90373-7 Date Collected: 10/20/15 12:27 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride 0.491 J Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/30/15 22:38 1 0.500 0.200 ug/L 10/30/15 22:38 1 0.500 0.170 ug/L 10/30/15 22:38 1 0.500 0.290 ug/L 10/30/15 22:38 1 0.500 0.350 ug/L 10/30/15 22:38 1 50.0 2.64 ug/L 10/30/15 22:38 1 0.500 0.220 ug/L 10/30/15 22:38 1 0.500 0.180 ug/L 10/30/15 22:38 1 0.500 0.180 ug/L 10/30/15 22:38 1 0.500 0.360 ug/L 10/30/15 22:38 1 0.500 0.230 ug/L 10/30/15 22:38 1 0.500 0.360 ug/L 10/30/15 22:38 1 0.500 0.210 ug/L 10/30/15 22:38 1 0.500 0.170 ug/L 10/30/15 22:38 1 1.00 0.130 ug/L 10/30/15 22:38 1 0.500 0.250 ug/L 10/30/15 22:38 1 5.00 0.940 ug/L 10/30/15 22:38 1 0.500 0.210 ug/L 10/30/15 22:38 1 0.500 0.190 ug/L 10/30/15 22:38 1 0.500 0.180 ug/L 10/30/15 22:38 1 0.500 0.170 ug/L 10/30/15 22:38 1 0.500 0.170 ug/L 10/30/15 22:38 1 0.500 0.240 ug/L 10/30/15 22:38 1 0.500 0.200 ug/L 10/30/15 22:38 1 0.500 0.250 ug/L 10/30/15 22:38 1 0.500 0.250 ug/L 10/30/15 22:38 1 0.500 0.190 ug/L 10/30/15 22:38 1 5.00 1.28 ug/L 10/30/15 22:38 1 1.00 0.330 ug/L 10/30/15 22:38 1 10.0 0.580 ug/L 10/30/15 22:38 1 0.500 0.0900 ug/L 10/30/15 22:38 1 5.00 0.220 ug/L 10/30/15 22:38 1 5.00 0.810 ug/L 10/30/15 22:38 1 0.500 0.170 ug/L 10/30/15 22:38 1 0.500 0.280 ug/L 10/30/15 22:38 1 0.500 0.190 ug/L 10/30/15 22:38 1 0.500 0.140 ug/L 10/30/15 22:38 1 5.00 0.820 ug/L 10/30/15 22:38 1 0.500 0.170 ug/L 10/30/15 22:38 1 0.500 0.230 ug/L 10/30/15 22:38 1 0.500 0.170 ug/L 10/30/15 22:38 1 0.500 0.200 ug/L 10/30/15 22:38 1 0.500 0.190 ug/L 10/30/15 22:38 1 0.500 0.190 ug/L 10/30/15 22:38 1 0.500 0.200 ug/L 10/30/15 22:38 1 0.500 0.210 ug/L 10/30/15 22:38 1 1.00 0.150 ug/L 10/30/15 22:38 1 0.500 0.180 ug/L 10/30/15 22:38 1 1.00 0.580 ug/L 10/30/15 22:38 1 TestAmerica Nashville Page 18 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J1155 Client Sample ID: J1155-MW-44-102015 Lab Sample ID: 490-90373-7 Date Collected: 10/20/15 12:27 Matrix: Water Date Received: 10/23/15 10:00 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 108 70- 130 10130112 8853T 1 Dibromofluoromethane (Surr) 100 70- 130 10130112 8853T 1 1,8-Dichloroethane-d4 (Surr) 99 70- 130 10130112 8853T 1 6oluene-dT (Surr) 100 70 - 130 10130112 8853T 1 12 13 14 TestAmerica Nashville Page 19 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-46-102015 Lab Sample ID: 490-90373-8 Date Collected: 10/20/15 10:13 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/30/15 23:07 1 0.500 0.200 ug/L 10/30/15 23:07 1 0.500 0.170 ug/L 10/30/15 23:07 1 0.500 0.290 ug/L 10/30/15 23:07 1 0.500 0.350 ug/L 10/30/15 23:07 1 50.0 2.64 ug/L 10/30/15 23:07 1 0.500 0.220 ug/L 10/30/15 23:07 1 0.500 0.180 ug/L 10/30/15 23:07 1 0.500 0.180 ug/L 10/30/15 23:07 1 0.500 0.360 ug/L 10/30/15 23:07 1 0.500 0.230 ug/L 10/30/15 23:07 1 0.500 0.360 ug/L 10/30/15 23:07 1 0.500 0.210 ug/L 10/30/15 23:07 1 0.500 0.170 ug/L 10/30/15 23:07 1 1.00 0.130 ug/L 10/30/15 23:07 1 0.500 0.250 ug/L 10/30/15 23:07 1 5.00 0.940 ug/L 10/30/15 23:07 1 0.500 0.210 ug/L 10/30/15 23:07 1 0.500 0.190 ug/L 10/30/15 23:07 1 0.500 0.180 ug/L 10/30/15 23:07 1 0.500 0.170 ug/L 10/30/15 23:07 1 0.500 0.170 ug/L 10/30/15 23:07 1 0.500 0.240 ug/L 10/30/15 23:07 1 0.500 0.200 ug/L 10/30/15 23:07 1 0.500 0.250 ug/L 10/30/15 23:07 1 0.500 0.250 ug/L 10/30/15 23:07 1 0.500 0.190 ug/L 10/30/15 23:07 1 5.00 1.28 ug/L 10/30/15 23:07 1 1.00 0.330 ug/L 10/30/15 23:07 1 10.0 0.580 ug/L 10/30/15 23:07 1 0.500 0.0900 ug/L 10/30/15 23:07 1 5.00 0.220 ug/L 10/30/15 23:07 1 5.00 0.810 ug/L 10/30/15 23:07 1 0.500 0.170 ug/L 10/30/15 23:07 1 0.500 0.280 ug/L 10/30/15 23:07 1 0.500 0.190 ug/L 10/30/15 23:07 1 0.500 0.140 ug/L 10/30/15 23:07 1 5.00 0.820 ug/L 10/30/15 23:07 1 0.500 0.170 ug/L 10/30/15 23:07 1 0.500 0.230 ug/L 10/30/15 23:07 1 0.500 0.170 ug/L 10/30/15 23:07 1 0.500 0.200 ug/L 10/30/15 23:07 1 0.500 0.190 ug/L 10/30/15 23:07 1 0.500 0.190 ug/L 10/30/15 23:07 1 0.500 0.200 ug/L 10/30/15 23:07 1 0.500 0.210 ug/L 10/30/15 23:07 1 1.00 0.150 ug/L 10/30/15 23:07 1 0.500 0.180 ug/L 10/30/15 23:07 1 1.00 0.580 ug/L 10/30/15 23:07 1 TestAmerica Nashville Page 20 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J1155 Client Sample ID: J1155-MW-46-102015 Lab Sample ID: 490-90373-8 Date Collected: 10/20/15 10:13 Matrix: Water Date Received: 10/23/15 10:00 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 70- 130 10130112 833)7 1 Dibromofluoromethane (Surr) 108 70- 130 10130112 833)7 1 1,8-Dichloroethane-d4 (Surr) 99 70- 130 10130112 835)7 1 6oluene-dT (Surr) 101 70 - 130 10130112 83T7 1 12 13 14 TestAmerica Nashville Page 21 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-47-102015 Lab Sample ID: 490-90373-9 Date Collected: 10/20/15 09:55 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/30/15 23:35 1 0.500 0.200 ug/L 10/30/15 23:35 1 0.500 0.170 ug/L 10/30/15 23:35 1 0.500 0.290 ug/L 10/30/15 23:35 1 0.500 0.350 ug/L 10/30/15 23:35 1 50.0 2.64 ug/L 10/30/15 23:35 1 0.500 0.220 ug/L 10/30/15 23:35 1 0.500 0.180 ug/L 10/30/15 23:35 1 0.500 0.180 ug/L 10/30/15 23:35 1 0.500 0.360 ug/L 10/30/15 23:35 1 0.500 0.230 ug/L 10/30/15 23:35 1 0.500 0.360 ug/L 10/30/15 23:35 1 0.500 0.210 ug/L 10/30/15 23:35 1 0.500 0.170 ug/L 10/30/15 23:35 1 1.00 0.130 ug/L 10/30/15 23:35 1 0.500 0.250 ug/L 10/30/15 23:35 1 5.00 0.940 ug/L 10/30/15 23:35 1 0.500 0.210 ug/L 10/30/15 23:35 1 0.500 0.190 ug/L 10/30/15 23:35 1 0.500 0.180 ug/L 10/30/15 23:35 1 0.500 0.170 ug/L 10/30/15 23:35 1 0.500 0.170 ug/L 10/30/15 23:35 1 0.500 0.240 ug/L 10/30/15 23:35 1 0.500 0.200 ug/L 10/30/15 23:35 1 0.500 0.250 ug/L 10/30/15 23:35 1 0.500 0.250 ug/L 10/30/15 23:35 1 0.500 0.190 ug/L 10/30/15 23:35 1 5.00 1.28 ug/L 10/30/15 23:35 1 1.00 0.330 ug/L 10/30/15 23:35 1 10.0 0.580 ug/L 10/30/15 23:35 1 0.500 0.0900 ug/L 10/30/15 23:35 1 5.00 0.220 ug/L 10/30/15 23:35 1 5.00 0.810 ug/L 10/30/15 23:35 1 0.500 0.170 ug/L 10/30/15 23:35 1 0.500 0.280 ug/L 10/30/15 23:35 1 0.500 0.190 ug/L 10/30/15 23:35 1 0.500 0.140 ug/L 10/30/15 23:35 1 5.00 0.820 ug/L 10/30/15 23:35 1 0.500 0.170 ug/L 10/30/15 23:35 1 0.500 0.230 ug/L 10/30/15 23:35 1 0.500 0.170 ug/L 10/30/15 23:35 1 0.500 0.200 ug/L 10/30/15 23:35 1 0.500 0.190 ug/L 10/30/15 23:35 1 0.500 0.190 ug/L 10/30/15 23:35 1 0.500 0.200 ug/L 10/30/15 23:35 1 0.500 0.210 ug/L 10/30/15 23:35 1 1.00 0.150 ug/L 10/30/15 23:35 1 0.500 0.180 ug/L 10/30/15 23:35 1 1.00 0.580 ug/L 10/30/15 23:35 1 TestAmerica Nashville Page 22 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J1155 Client Sample ID: J1155-MW-47-102015 Lab Sample ID: 490-90373-9 Date Collected: 10/20/15 09:55 Matrix: Water Date Received: 10/23/15 10:00 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 70 - 130 10130112 83532 1 Dibromofluoromethane (Surr) 100 70 - 130 10130112 83532 1 1,8-Dichloroethane-d4 (Surr) 9T 70- 130 10130112 83532 1 6oluene-dT (Surr) 99 70 - 130 10130112 83532 1 12 13 14 TestAmerica Nashville Page 23 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-60-102015 Lab Sample ID: 490-90373-10 Date Collected: 10/20/15 14:43 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 1.09 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 0.336 J Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 17.5 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 0.763 J ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/31/15 00:03 1 0.500 0.200 ug/L 10/31/15 00:03 1 0.500 0.170 ug/L 10/31/15 00:03 1 0.500 0.290 ug/L 10/31/15 00:03 1 0.500 0.350 ug/L 10/31/15 00:03 1 50.0 2.64 ug/L 10/31/15 00:03 1 0.500 0.220 ug/L 10/31/15 00:03 1 0.500 0.180 ug/L 10/31/15 00:03 1 0.500 0.180 ug/L 10/31/15 00:03 1 0.500 0.360 ug/L 10/31/15 00:03 1 0.500 0.230 ug/L 10/31/15 00:03 1 0.500 0.360 ug/L 10/31/15 00:03 1 0.500 0.210 ug/L 10/31/15 00:03 1 0.500 0.170 ug/L 10/31/15 00:03 1 1.00 0.130 ug/L 10/31/15 00:03 1 0.500 0.250 ug/L 10/31/15 00:03 1 5.00 0.940 ug/L 10/31/15 00:03 1 0.500 0.210 ug/L 10/31/15 00:03 1 0.500 0.190 ug/L 10/31/15 00:03 1 0.500 0.180 ug/L 10/31/15 00:03 1 0.500 0.170 ug/L 10/31/15 00:03 1 0.500 0.170 ug/L 10/31/15 00:03 1 0.500 0.240 ug/L 10/31/15 00:03 1 0.500 0.200 ug/L 10/31/15 00:03 1 0.500 0.250 ug/L 10/31/15 00:03 1 0.500 0.250 ug/L 10/31/15 00:03 1 0.500 0.190 ug/L 10/31/15 00:03 1 5.00 1.28 ug/L 10/31/15 00:03 1 1.00 0.330 ug/L 10/31/15 00:03 1 10.0 0.580 ug/L 10/31/15 00:03 1 0.500 0.0900 ug/L 10/31/15 00:03 1 5.00 0.220 ug/L 10/31/15 00:03 1 5.00 0.810 ug/L 10/31/15 00:03 1 0.500 0.170 ug/L 10/31/15 00:03 1 0.500 0.280 ug/L 10/31/15 00:03 1 0.500 0.190 ug/L 10/31/15 00:03 1 0.500 0.140 ug/L 10/31/15 00:03 1 5.00 0.820 ug/L 10/31/15 00:03 1 0.500 0.170 ug/L 10/31/15 00:03 1 0.500 0.230 ug/L 10/31/15 00:03 1 0.500 0.170 ug/L 10/31/15 00:03 1 0.500 0.200 ug/L 10/31/15 00:03 1 0.500 0.190 ug/L 10/31/15 00:03 1 0.500 0.190 ug/L 10/31/15 00:03 1 0.500 0.200 ug/L 10/31/15 00:03 1 0.500 0.210 ug/L 10/31/15 00:03 1 1.00 0.150 ug/L 10/31/15 00:03 1 0.500 0.180 ug/L 10/31/15 00:03 1 TestAmerica Nashville Page 24 of 79 11/6/2015 Client Sample Results Client: Dextra Group TestAmerica Job ID: 490-90373-1 Project/Site: Murphy, NC SDG: 55912-J1155 Client Sample ID: J1155-MW-60-102015 Lab Sample ID: 490-90373-10 Date Collected: 10/20/15 14:43 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 1.00 0.580 ug/L 10/31/15 00:03 1 Surrogate %Recovery Qualifier Limits • Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 70 - 130 10131112 00313 1 Dibromofluoromethane (Surr) 100 70 - 130 10131112 00313 1 1,8-Dichloroethane-d4 (Surr) 100 70- 130 10131112 00313 1 6oluene-dT (Surr) 99 70 - 130 10131112 00T3 1 12 13 14 TestAmerica Nashville Page 25 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-61-102015 Lab Sample ID: 490-90373-11 Date Collected: 10/20/15 15:23 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone 2.90 J Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 0.976 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 0.233 J Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 12.4 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 0.358 J ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/31/15 00:32 1 0.500 0.200 ug/L 10/31/15 00:32 1 0.500 0.170 ug/L 10/31/15 00:32 1 0.500 0.290 ug/L 10/31/15 00:32 1 0.500 0.350 ug/L 10/31/15 00:32 1 50.0 2.64 ug/L 10/31/15 00:32 1 0.500 0.220 ug/L 10/31/15 00:32 1 0.500 0.180 ug/L 10/31/15 00:32 1 0.500 0.180 ug/L 10/31/15 00:32 1 0.500 0.360 ug/L 10/31/15 00:32 1 0.500 0.230 ug/L 10/31/15 00:32 1 0.500 0.360 ug/L 10/31/15 00:32 1 0.500 0.210 ug/L 10/31/15 00:32 1 0.500 0.170 ug/L 10/31/15 00:32 1 1.00 0.130 ug/L 10/31/15 00:32 1 0.500 0.250 ug/L 10/31/15 00:32 1 5.00 0.940 ug/L 10/31/15 00:32 1 0.500 0.210 ug/L 10/31/15 00:32 1 0.500 0.190 ug/L 10/31/15 00:32 1 0.500 0.180 ug/L 10/31/15 00:32 1 0.500 0.170 ug/L 10/31/15 00:32 1 0.500 0.170 ug/L 10/31/15 00:32 1 0.500 0.240 ug/L 10/31/15 00:32 1 0.500 0.200 ug/L 10/31/15 00:32 1 0.500 0.250 ug/L 10/31/15 00:32 1 0.500 0.250 ug/L 10/31/15 00:32 1 0.500 0.190 ug/L 10/31/15 00:32 1 5.00 1.28 ug/L 10/31/15 00:32 1 1.00 0.330 ug/L 10/31/15 00:32 1 10.0 0.580 ug/L 10/31/15 00:32 1 0.500 0.0900 ug/L 10/31/15 00:32 1 5.00 0.220 ug/L 10/31/15 00:32 1 5.00 0.810 ug/L 10/31/15 00:32 1 0.500 0.170 ug/L 10/31/15 00:32 1 0.500 0.280 ug/L 10/31/15 00:32 1 0.500 0.190 ug/L 10/31/15 00:32 1 0.500 0.140 ug/L 10/31/15 00:32 1 5.00 0.820 ug/L 10/31/15 00:32 1 0.500 0.170 ug/L 10/31/15 00:32 1 0.500 0.230 ug/L 10/31/15 00:32 1 0.500 0.170 ug/L 10/31/15 00:32 1 0.500 0.200 ug/L 10/31/15 00:32 1 0.500 0.190 ug/L 10/31/15 00:32 1 0.500 0.190 ug/L 10/31/15 00:32 1 0.500 0.200 ug/L 10/31/15 00:32 1 0.500 0.210 ug/L 10/31/15 00:32 1 1.00 0.150 ug/L 10/31/15 00:32 1 0.500 0.180 ug/L 10/31/15 00:32 1 TestAmerica Nashville Page 26 of 79 11/6/2015 Client Sample Results Client: Dextra Group TestAmerica Job ID: 490-90373-1 Project/Site: Murphy, NC SDG: 55912-J1155 Client Sample ID: J1155-MW-61-102015 Lab Sample ID: 490-90373-11 Date Collected: 10/20/15 15:23 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 1.00 0.580 ug/L 10/31/15 00:32 1 Surrogate %Recovery Qualifier Limits • Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 70 - 130 10131112 00538 1 Dibromofluoromethane (Surr) 108 70 - 130 10131112 00538 1 1,8-Dichloroethane-d4 (Surr) 100 70- 130 10131112 00538 1 6oluene-dT (Surr) 99 70 - 130 10131112 00538 1 12 13 14 TestAmerica Nashville Page 27 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-62-102115 Lab Sample ID: 490-90373-12 Date Collected: 10/21/15 10:53 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 5.07 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene 0.900 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 1.60 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 18.9 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 1.31 ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/31/15 01:00 1 0.500 0.200 ug/L 10/31/15 01:00 1 0.500 0.170 ug/L 10/31/15 01:00 1 0.500 0.290 ug/L 10/31/15 01:00 1 0.500 0.350 ug/L 10/31/15 01:00 1 50.0 2.64 ug/L 10/31/15 01:00 1 0.500 0.220 ug/L 10/31/15 01:00 1 0.500 0.180 ug/L 10/31/15 01:00 1 0.500 0.180 ug/L 10/31/15 01:00 1 0.500 0.360 ug/L 10/31/15 01:00 1 0.500 0.230 ug/L 10/31/15 01:00 1 0.500 0.360 ug/L 10/31/15 01:00 1 0.500 0.210 ug/L 10/31/15 01:00 1 0.500 0.170 ug/L 10/31/15 01:00 1 1.00 0.130 ug/L 10/31/15 01:00 1 0.500 0.250 ug/L 10/31/15 01:00 1 5.00 0.940 ug/L 10/31/15 01:00 1 0.500 0.210 ug/L 10/31/15 01:00 1 0.500 0.190 ug/L 10/31/15 01:00 1 0.500 0.180 ug/L 10/31/15 01:00 1 0.500 0.170 ug/L 10/31/15 01:00 1 0.500 0.170 ug/L 10/31/15 01:00 1 0.500 0.240 ug/L 10/31/15 01:00 1 0.500 0.200 ug/L 10/31/15 01:00 1 0.500 0.250 ug/L 10/31/15 01:00 1 0.500 0.250 ug/L 10/31/15 01:00 1 0.500 0.190 ug/L 10/31/15 01:00 1 5.00 1.28 ug/L 10/31/15 01:00 1 1.00 0.330 ug/L 10/31/15 01:00 1 10.0 0.580 ug/L 10/31/15 01:00 1 0.500 0.0900 ug/L 10/31/15 01:00 1 5.00 0.220 ug/L 10/31/15 01:00 1 5.00 0.810 ug/L 10/31/15 01:00 1 0.500 0.170 ug/L 10/31/15 01:00 1 0.500 0.280 ug/L 10/31/15 01:00 1 0.500 0.190 ug/L 10/31/15 01:00 1 0.500 0.140 ug/L 10/31/15 01:00 1 5.00 0.820 ug/L 10/31/15 01:00 1 0.500 0.170 ug/L 10/31/15 01:00 1 0.500 0.230 ug/L 10/31/15 01:00 1 0.500 0.170 ug/L 10/31/15 01:00 1 0.500 0.200 ug/L 10/31/15 01:00 1 0.500 0.190 ug/L 10/31/15 01:00 1 0.500 0.190 ug/L 10/31/15 01:00 1 0.500 0.200 ug/L 10/31/15 01:00 1 0.500 0.210 ug/L 10/31/15 01:00 1 1.00 0.150 ug/L 10/31/15 01:00 1 0.500 0.180 ug/L 10/31/15 01:00 1 TestAmerica Nashville Page 28 of 79 11/6/2015 Client Sample Results Client: Dextra Group TestAmerica Job ID: 490-90373-1 Project/Site: Murphy, NC SDG: 55912-J1155 Client Sample ID: J1155-MW-62-102115 Lab Sample ID: 490-90373-12 Date Collected: 10/21/15 10:53 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 1.00 0.580 ug/L 10/31/15 01:00 1 Surrogate %Recovery Qualifier Limits • Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 70- 130 10131112 01TO 1 Dibromofluoromethane (Surr) 108 70- 130 10131112 01TO 1 1,8-Dichloroethane-d4 (Surr) 9T 70- 130 10131112 01TO 1 6oluene-dT (Surr) 100 70- 130 10131112 01TO 1 12 13 14 TestAmerica Nashville Page 29 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-63-102115 Lab Sample ID: 490-90373-13 Date Collected: 10/21/15 10:22 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 11.1 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane 0.551 1,2-Dichloroethane ND 1,1-Dichloroethene 0.294 J 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 7.52 Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/31/15 01:29 1 0.500 0.200 ug/L 10/31/15 01:29 1 0.500 0.170 ug/L 10/31/15 01:29 1 0.500 0.290 ug/L 10/31/15 01:29 1 0.500 0.350 ug/L 10/31/15 01:29 1 50.0 2.64 ug/L 10/31/15 01:29 1 0.500 0.220 ug/L 10/31/15 01:29 1 0.500 0.180 ug/L 10/31/15 01:29 1 0.500 0.180 ug/L 10/31/15 01:29 1 0.500 0.360 ug/L 10/31/15 01:29 1 0.500 0.230 ug/L 10/31/15 01:29 1 0.500 0.360 ug/L 10/31/15 01:29 1 0.500 0.210 ug/L 10/31/15 01:29 1 0.500 0.170 ug/L 10/31/15 01:29 1 1.00 0.130 ug/L 10/31/15 01:29 1 0.500 0.250 ug/L 10/31/15 01:29 1 5.00 0.940 ug/L 10/31/15 01:29 1 0.500 0.210 ug/L 10/31/15 01:29 1 0.500 0.190 ug/L 10/31/15 01:29 1 0.500 0.180 ug/L 10/31/15 01:29 1 0.500 0.170 ug/L 10/31/15 01:29 1 0.500 0.170 ug/L 10/31/15 01:29 1 0.500 0.240 ug/L 10/31/15 01:29 1 0.500 0.200 ug/L 10/31/15 01:29 1 0.500 0.250 ug/L 10/31/15 01:29 1 0.500 0.250 ug/L 10/31/15 01:29 1 0.500 0.190 ug/L 10/31/15 01:29 1 5.00 1.28 ug/L 10/31/15 01:29 1 1.00 0.330 ug/L 10/31/15 01:29 1 10.0 0.580 ug/L 10/31/15 01:29 1 0.500 0.0900 ug/L 10/31/15 01:29 1 5.00 0.220 ug/L 10/31/15 01:29 1 5.00 0.810 ug/L 10/31/15 01:29 1 0.500 0.170 ug/L 10/31/15 01:29 1 0.500 0.280 ug/L 10/31/15 01:29 1 0.500 0.190 ug/L 10/31/15 01:29 1 0.500 0.140 ug/L 10/31/15 01:29 1 5.00 0.820 ug/L 10/31/15 01:29 1 0.500 0.170 ug/L 10/31/15 01:29 1 0.500 0.230 ug/L 10/31/15 01:29 1 0.500 0.170 ug/L 10/31/15 01:29 1 0.500 0.200 ug/L 10/31/15 01:29 1 0.500 0.190 ug/L 10/31/15 01:29 1 0.500 0.190 ug/L 10/31/15 01:29 1 0.500 0.200 ug/L 10/31/15 01:29 1 0.500 0.210 ug/L 10/31/15 01:29 1 1.00 0.150 ug/L 10/31/15 01:29 1 0.500 0.180 ug/L 10/31/15 01:29 1 1.00 0.580 ug/L 10/31/15 01:29 1 TestAmerica Nashville Page 30 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J1155 Client Sample ID: J1155-MW-63-102115 Lab Sample ID: 490-90373-13 Date Collected: 10/21/15 10:22 Matrix: Water Date Received: 10/23/15 10:00 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 70- 130 10131112 01T9 1 Dibromofluoromethane (Surr) 100 70- 130 10131112 01T9 1 1,8-Dichloroethane-d4 (Surr) 100 70- 130 10131112 01T9 1 6oluene-dT (Surr) 100 70 - 130 10131112 01T9 1 12 13 14 TestAmerica Nashville Page 31 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-64-102015 Lab Sample ID: 490-90373-14 Date Collected: 10/20/15 14:15 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene 1.36 cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane 0.486 J 1,2-Dichloroethane ND 1,1-Dichloroethene 0.577 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene 0.667 Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 23.5 Trichlorofluoromethane ND 1 1 2-Trichloro-1 2 2-trifluoroetha 5.42 ne Vinyl chloride ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/31/15 01:57 1 0.500 0.200 ug/L 10/31/15 01:57 1 0.500 0.170 ug/L 10/31/15 01:57 1 0.500 0.290 ug/L 10/31/15 01:57 1 0.500 0.350 ug/L 10/31/15 01:57 1 50.0 2.64 ug/L 10/31/15 01:57 1 0.500 0.220 ug/L 10/31/15 01:57 1 0.500 0.180 ug/L 10/31/15 01:57 1 0.500 0.180 ug/L 10/31/15 01:57 1 0.500 0.360 ug/L 10/31/15 01:57 1 0.500 0.230 ug/L 10/31/15 01:57 1 0.500 0.360 ug/L 10/31/15 01:57 1 0.500 0.210 ug/L 10/31/15 01:57 1 0.500 0.170 ug/L 10/31/15 01:57 1 1.00 0.130 ug/L 10/31/15 01:57 1 0.500 0.250 ug/L 10/31/15 01:57 1 5.00 0.940 ug/L 10/31/15 01:57 1 0.500 0.210 ug/L 10/31/15 01:57 1 0.500 0.190 ug/L 10/31/15 01:57 1 0.500 0.180 ug/L 10/31/15 01:57 1 0.500 0.170 ug/L 10/31/15 01:57 1 0.500 0.170 ug/L 10/31/15 01:57 1 0.500 0.240 ug/L 10/31/15 01:57 1 0.500 0.200 ug/L 10/31/15 01:57 1 0.500 0.250 ug/L 10/31/15 01:57 1 0.500 0.250 ug/L 10/31/15 01:57 1 0.500 0.190 ug/L 10/31/15 01:57 1 5.00 1.28 ug/L 10/31/15 01:57 1 1.00 0.330 ug/L 10/31/15 01:57 1 10.0 0.580 ug/L 10/31/15 01:57 1 0.500 0.0900 ug/L 10/31/15 01:57 1 5.00 0.220 ug/L 10/31/15 01:57 1 5.00 0.810 ug/L 10/31/15 01:57 1 0.500 0.170 ug/L 10/31/15 01:57 1 0.500 0.280 ug/L 10/31/15 01:57 1 0.500 0.190 ug/L 10/31/15 01:57 1 0.500 0.140 ug/L 10/31/15 01:57 1 5.00 0.820 ug/L 10/31/15 01:57 1 0.500 0.170 ug/L 10/31/15 01:57 1 0.500 0.230 ug/L 10/31/15 01:57 1 0.500 0.170 ug/L 10/31/15 01:57 1 0.500 0.200 ug/L 10/31/15 01:57 1 0.500 0.190 ug/L 10/31/15 01:57 1 0.500 0.190 ug/L 10/31/15 01:57 1 0.500 0.200 ug/L 10/31/15 01:57 1 0.500 0.210 ug/L 10/31/15 01:57 1 1.00 0.150 ug/L 10/31/15 01:57 1 0.500 0.180 ug/L 10/31/15 01:57 1 TestAmerica Nashville Page 32 of 79 11/6/2015 Client Sample Results Client: Dextra Group TestAmerica Job ID: 490-90373-1 Project/Site: Murphy, NC SDG: 55912-J1155 Client Sample ID: J1155-MW-64-102015 Lab Sample ID: 490-90373-14 Date Collected: 10/20/15 14:15 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Xylenes, Total ND 1.00 0.580 ug/L 10/31/15 01:57 1 Surrogate %Recovery Qualifier Limits • Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 99 70 - 130 10131112 0127 1 Dibromofluoromethane (Surr) 101 70 - 130 10131112 0127 1 1,8-Dichloroethane-d4 (Surr) 97 70- 130 10131112 0127 1 6oluene-dT (Surr) 99 70- 130 10131112 01T7 1 12 13 14 TestAmerica Nashville Page 33 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-PW-9-102115 Lab Sample ID: 490-90373-15 Date Collected: 10/21/15 11:59 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/31/15 02:26 1 0.500 0.200 ug/L 10/31/15 02:26 1 0.500 0.170 ug/L 10/31/15 02:26 1 0.500 0.290 ug/L 10/31/15 02:26 1 0.500 0.350 ug/L 10/31/15 02:26 1 50.0 2.64 ug/L 10/31/15 02:26 1 0.500 0.220 ug/L 10/31/15 02:26 1 0.500 0.180 ug/L 10/31/15 02:26 1 0.500 0.180 ug/L 10/31/15 02:26 1 0.500 0.360 ug/L 10/31/15 02:26 1 0.500 0.230 ug/L 10/31/15 02:26 1 0.500 0.360 ug/L 10/31/15 02:26 1 0.500 0.210 ug/L 10/31/15 02:26 1 0.500 0.170 ug/L 10/31/15 02:26 1 1.00 0.130 ug/L 10/31/15 02:26 1 0.500 0.250 ug/L 10/31/15 02:26 1 5.00 0.940 ug/L 10/31/15 02:26 1 0.500 0.210 ug/L 10/31/15 02:26 1 0.500 0.190 ug/L 10/31/15 02:26 1 0.500 0.180 ug/L 10/31/15 02:26 1 0.500 0.170 ug/L 10/31/15 02:26 1 0.500 0.170 ug/L 10/31/15 02:26 1 0.500 0.240 ug/L 10/31/15 02:26 1 0.500 0.200 ug/L 10/31/15 02:26 1 0.500 0.250 ug/L 10/31/15 02:26 1 0.500 0.250 ug/L 10/31/15 02:26 1 0.500 0.190 ug/L 10/31/15 02:26 1 5.00 1.28 ug/L 10/31/15 02:26 1 1.00 0.330 ug/L 10/31/15 02:26 1 10.0 0.580 ug/L 10/31/15 02:26 1 0.500 0.0900 ug/L 10/31/15 02:26 1 5.00 0.220 ug/L 10/31/15 02:26 1 5.00 0.810 ug/L 10/31/15 02:26 1 0.500 0.170 ug/L 10/31/15 02:26 1 0.500 0.280 ug/L 10/31/15 02:26 1 0.500 0.190 ug/L 10/31/15 02:26 1 0.500 0.140 ug/L 10/31/15 02:26 1 5.00 0.820 ug/L 10/31/15 02:26 1 0.500 0.170 ug/L 10/31/15 02:26 1 0.500 0.230 ug/L 10/31/15 02:26 1 0.500 0.170 ug/L 10/31/15 02:26 1 0.500 0.200 ug/L 10/31/15 02:26 1 0.500 0.190 ug/L 10/31/15 02:26 1 0.500 0.190 ug/L 10/31/15 02:26 1 0.500 0.200 ug/L 10/31/15 02:26 1 0.500 0.210 ug/L 10/31/15 02:26 1 1.00 0.150 ug/L 10/31/15 02:26 1 0.500 0.180 ug/L 10/31/15 02:26 1 1.00 0.580 ug/L 10/31/15 02:26 1 TestAmerica Nashville Page 34 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J1155 Client Sample ID: J1155-PW-9-102115 Lab Sample ID: 490-90373-15 Date Collected: 10/21/15 11:59 Matrix: Water Date Received: 10/23/15 10:00 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 70 - 130 10131112 08,T: 1 Dibromofluoromethane (Surr) 101 70 - 130 10131112 08,T: 1 1,8-Dichloroethane-d4 (Surr) 99 70- 130 10131112 08,T: 1 6oluene-dT (Surr) 99 70 - 130 10131112 08,T: 1 12 13 14 TestAmerica Nashville Page 35 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-CMP-4-102115 Lab Sample ID: 490-90373-16 Date Collected: 10/21/15 11:29 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene 2.75 Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/31/15 02:54 1 0.500 0.200 ug/L 10/31/15 02:54 1 0.500 0.170 ug/L 10/31/15 02:54 1 0.500 0.290 ug/L 10/31/15 02:54 1 0.500 0.350 ug/L 10/31/15 02:54 1 50.0 2.64 ug/L 10/31/15 02:54 1 0.500 0.220 ug/L 10/31/15 02:54 1 0.500 0.180 ug/L 10/31/15 02:54 1 0.500 0.180 ug/L 10/31/15 02:54 1 0.500 0.360 ug/L 10/31/15 02:54 1 0.500 0.230 ug/L 10/31/15 02:54 1 0.500 0.360 ug/L 10/31/15 02:54 1 0.500 0.210 ug/L 10/31/15 02:54 1 0.500 0.170 ug/L 10/31/15 02:54 1 1.00 0.130 ug/L 10/31/15 02:54 1 0.500 0.250 ug/L 10/31/15 02:54 1 5.00 0.940 ug/L 10/31/15 02:54 1 0.500 0.210 ug/L 10/31/15 02:54 1 0.500 0.190 ug/L 10/31/15 02:54 1 0.500 0.180 ug/L 10/31/15 02:54 1 0.500 0.170 ug/L 10/31/15 02:54 1 0.500 0.170 ug/L 10/31/15 02:54 1 0.500 0.240 ug/L 10/31/15 02:54 1 0.500 0.200 ug/L 10/31/15 02:54 1 0.500 0.250 ug/L 10/31/15 02:54 1 0.500 0.250 ug/L 10/31/15 02:54 1 0.500 0.190 ug/L 10/31/15 02:54 1 5.00 1.28 ug/L 10/31/15 02:54 1 1.00 0.330 ug/L 10/31/15 02:54 1 10.0 0.580 ug/L 10/31/15 02:54 1 0.500 0.0900 ug/L 10/31/15 02:54 1 5.00 0.220 ug/L 10/31/15 02:54 1 5.00 0.810 ug/L 10/31/15 02:54 1 0.500 0.170 ug/L 10/31/15 02:54 1 0.500 0.280 ug/L 10/31/15 02:54 1 0.500 0.190 ug/L 10/31/15 02:54 1 0.500 0.140 ug/L 10/31/15 02:54 1 5.00 0.820 ug/L 10/31/15 02:54 1 0.500 0.170 ug/L 10/31/15 02:54 1 0.500 0.230 ug/L 10/31/15 02:54 1 0.500 0.170 ug/L 10/31/15 02:54 1 0.500 0.200 ug/L 10/31/15 02:54 1 0.500 0.190 ug/L 10/31/15 02:54 1 0.500 0.190 ug/L 10/31/15 02:54 1 0.500 0.200 ug/L 10/31/15 02:54 1 0.500 0.210 ug/L 10/31/15 02:54 1 1.00 0.150 ug/L 10/31/15 02:54 1 0.500 0.180 ug/L 10/31/15 02:54 1 1.00 0.580 ug/L 10/31/15 02:54 1 TestAmerica Nashville Page 36 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J1155 Client Sample ID: J1155-CMP-4-102115 Lab Sample ID: 490-90373-16 Date Collected: 10/21/15 11:29 Matrix: Water Date Received: 10/23/15 10:00 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 70 - 130 10131112 08`24 1 Dibromofluoromethane (Surr) 99 70 - 130 10131112 08`24 1 1,8-Dichloroethane-d4 (Surr) 9T 70- 130 10131112 08T4 1 6oluene-dT (Surr) 100 70 - 130 10131112 08g4 1 12 13 14 TestAmerica Nashville Page 37 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-Trip Blank-101915 Lab Sample ID: 490-90373-17 Date Collected: 10/19/15 08:30 Matrix: Water Date Received: 10/23/15 10:00 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropane ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methylcyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene ND 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans- 1,3-Dichloropropene ND 1,2,4-Trichlorobenzene ND 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,1,2-Trichloro-1,2,2-trifluoroethane ND Vinyl chloride ND Xylenes, Total ND RL MDL Unit D Prepared Analyzed Dil Fac 5.00 2.66 ug/L 10/30/1519:48 1 0.500 0.200 ug/L 10/30/1519:48 1 0.500 0.170 ug/L 10/30/1519:48 1 0.500 0.290 ug/L 10/30/1519:48 1 0.500 0.350 ug/L 10/30/1519:48 1 50.0 2.64 ug/L 10/30/1519:48 1 0.500 0.220 ug/L 10/30/1519:48 1 0.500 0.180 ug/L 10/30/1519:48 1 0.500 0.180 ug/L 10/30/1519:48 1 0.500 0.360 ug/L 10/30/1519:48 1 0.500 0.230 ug/L 10/30/1519:48 1 0.500 0.360 ug/L 10/30/1519:48 1 0.500 0.210 ug/L 10/30/1519:48 1 0.500 0.170 ug/L 10/30/1519:48 1 1.00 0.130 ug/L 10/30/1519:48 1 0.500 0.250 ug/L 10/30/1519:48 1 5.00 0.940 ug/L 10/30/1519:48 1 0.500 0.210 ug/L 10/30/1519:48 1 0.500 0.190 ug/L 10/30/1519:48 1 0.500 0.180 ug/L 10/30/1519:48 1 0.500 0.170 ug/L 10/30/1519:48 1 0.500 0.170 ug/L 10/30/1519:48 1 0.500 0.240 ug/L 10/30/1519:48 1 0.500 0.200 ug/L 10/30/1519:48 1 0.500 0.250 ug/L 10/30/1519:48 1 0.500 0.250 ug/L 10/30/1519:48 1 0.500 0.190 ug/L 10/30/1519:48 1 5.00 1.28 ug/L 10/30/1519:48 1 1.00 0.330 ug/L 10/30/1519:48 1 10.0 0.580 ug/L 10/30/1519:48 1 0.500 0.0900 ug/L 10/30/1519:48 1 5.00 0.220 ug/L 10/30/1519:48 1 5.00 0.810 ug/L 10/30/1519:48 1 0.500 0.170 ug/L 10/30/1519:48 1 0.500 0.280 ug/L 10/30/1519:48 1 0.500 0.190 ug/L 10/30/1519:48 1 0.500 0.140 ug/L 10/30/1519:48 1 5.00 0.820 ug/L 10/30/1519:48 1 0.500 0.170 ug/L 10/30/1519:48 1 0.500 0.230 ug/L 10/30/1519:48 1 0.500 0.170 ug/L 10/30/1519:48 1 0.500 0.200 ug/L 10/30/1519:48 1 0.500 0.190 ug/L 10/30/1519:48 1 0.500 0.190 ug/L 10/30/1519:48 1 0.500 0.200 ug/L 10/30/1519:48 1 0.500 0.210 ug/L 10/30/1519:48 1 1.00 0.150 ug/L 10/30/1519:48 1 0.500 0.180 ug/L 10/30/1519:48 1 1.00 0.580 ug/L 10/30/1519:48 1 TestAmerica Nashville Page 38 of 79 11/6/2015 Client Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J1155 Client Sample ID: J1155-Trip Blank-101915 Lab Sample ID: 490-90373-17 Date Collected: 10/19/15 08:30 Matrix: Water Date Received: 10/23/15 10:00 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 70 - 130 10130112 190T 1 Dibromofluoromethane (Surr) 100 70 - 130 10130112 190T 1 1,8-Dichloroethane-d4 (Surr) 99 70- 130 10130112 190T 1 6oluene-dT (Surr) 9T 70 - 130 10130112 1951T 1 12 13 14 TestAmerica Nashville Page 39 of 79 11/6/2015 QC Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J1155 Method: 8260B - Volatile Organic Compounds (GC/MS) Lab Sample ID: MB 490-294431/7 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 294431 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 5.00 2.66 ug/L 10/30/15 19:19 1 Benzene ND 0.500 0.200 ug/L 10/30/15 19:19 1 Bromodichloromethane ND 0.500 0.170 ug/L 10/30/15 19:19 1 Bromoform ND 0.500 0.290 ug/L 10/30/15 19:19 1 Bromomethane ND 0.500 0.350 ug/L 10/30/15 19:19 1 2-Butanone (MEK) ND 50.0 2.64 ug/L 10/30/15 19:19 1 Carbon disulfide ND 0.500 0.220 ug/L 10/30/15 19:19 1 Carbon tetrachloride ND 0.500 0.180 ug/L 10/30/15 19:19 1 Chlorobenzene ND 0.500 0.180 ug/L 10/30/15 19:19 1 Chloroethane ND 0.500 0.360 ug/L 10/30/15 19:19 1 Chloroform ND 0.500 0.230 ug/L 10/30/15 19:19 1 Chloromethane ND 0.500 0.360 ug/L 10/30/15 19:19 1 cis-1,2-Dichloroethene ND 0.500 0.210 ug/L 10/30/15 19:19 1 cis-1,3-Dichloropropene ND 0.500 0.170 ug/L 10/30/15 19:19 1 Cyclohexane ND 1.00 0.130 ug/L 10/30/15 19:19 1 Dibromochloromethane ND 0.500 0.250 ug/L 10/30/15 19:19 1 1,2-Dibromo-3-Chloropropane ND 5.00 0.940 ug/L 10/30/15 19:19 1 1,2-Dibromoethane (EDB) ND 0.500 0.210 ug/L 10/30/15 19:19 1 1,2-Dichlorobenzene ND 0.500 0.190 ug/L 10/30/15 19:19 1 1,3-Dichlorobenzene ND 0.500 0.180 ug/L 10/30/15 19:19 1 1,4-Dichlorobenzene ND 0.500 0.170 ug/L 10/30/15 19:19 1 Dichlorodifluoromethane ND 0.500 0.170 ug/L 10/30/15 19:19 1 1,1-Dichloroethane ND 0.500 0.240 ug/L 10/30/15 19:19 1 1,2-Dichloroethane ND 0.500 0.200 ug/L 10/30/15 19:19 1 1,1-Dichloroethene ND 0.500 0.250 ug/L 10/30/15 19:19 1 1,2-Dichloropropane ND 0.500 0.250 ug/L 10/30/15 19:19 1 Ethylbenzene ND 0.500 0.190 ug/L 10/30/15 19:19 1 2-Hexanone ND 5.00 1.28 ug/L 10/30/15 19:19 1 Isopropylbenzene ND 1.00 0.330 ug/L 10/30/15 19:19 1 Methyl acetate ND 10.0 0.580 ug/L 10/30/15 19:19 1 Methylcyclohexane ND 0.500 0.0900 ug/L 10/30/15 19:19 1 Methylene Chloride ND 5.00 0.220 ug/L 10/30/15 19:19 1 4-Methyl-2-pentanone (MIBK) ND 5.00 0.810 ug/L 10/30/15 19:19 1 Methyl tert-butyl ether ND 0.500 0.170 ug/L 10/30/15 19:19 1 Styrene ND 0.500 0.280 ug/L 10/30/15 19:19 1 1,1,2,2-Tetrachloroethane ND 0.500 0.190 ug/L 10/30/15 19:19 1 Tetrachloroethene ND 0.500 0.140 ug/L 10/30/15 19:19 1 Tetrahydrofuran ND 5.00 0.820 ug/L 10/30/15 19:19 1 Toluene ND 0.500 0.170 ug/L 10/30/15 19:19 1 trans-1,2-Dichloroethene ND 0.500 0.230 ug/L 10/30/15 19:19 1 trans-1,3-Dichloropropene ND 0.500 0.170 ug/L 10/30/15 19:19 1 1,2,4-Trichlorobenzene ND 0.500 0.200 ug/L 10/30/15 19:19 1 1,1,1-Trichloroethane ND 0.500 0.190 ug/L 10/30/15 19:19 1 1,1,2-Trichloroethane ND 0.500 0.190 ug/L 10/30/15 19:19 1 Trichloroethene ND 0.500 0.200 ug/L 10/30/15 19:19 1 Trichlorofluoromethane ND 0.500 0.210 ug/L 10/30/15 19:19 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 1.00 0.150 ug/L 10/30/15 19:19 1 Vinyl chloride ND 0.500 0.180 ug/L 10/30/15 19:19 1 TestAmerica NashXille Page 40 of 79 11/6/2015 QC Sample Results Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 490-294431/7 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 294431 Analyte v ylenes, Total Surrogate 4-Bromofluorobenzene (Surr) Dibromofluoromethane (Surr) 1,2-Dichloroethane-d4 (Surr) Toluene-d8 (Surr) MB Result MB Qualifier RL MDL Unit D Prepared Analyzed Dil Fac ND 1.00 0.580 ug/L 10/30/1519:19 1 MB MB %Recovery Qualifier Limits Prepared Analyzed Dil Fac 100 70 - 130 10130115 19:19 1 99 70 - 130 10130115 19:19 1 97 70 - 130 10130115 19:19 1 100 70 - 130 10130115 19:19 1 Lab Sample ID: LCS 490-294431/3 Matrix: Water Analysis Batch: 294431 Analyte Acetone Benzene Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Cyclohexane Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene 1,2-Dichloropropane Ethylbenzene 2-Hexanone Isopropylbenzene Methyl acetate Methylcyclohexane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Styrene Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike Added LCS LCS Result Qualifier Unit D %Rec %Rec. Limits 250 211.6 ug/L 85 54-145 50.0 44.87 ug/L 90 80 -121 50.0 46.84 ug/L 94 75 -129 50.0 55.48 ug/L ill 46 -145 50.0 58.21 ug/L 116 41 -150 250 227.3 ug/L 91 62-133 50.0 43.45 ug/L 87 77 -126 50.0 45.89 ug/L 92 64 -147 50.0 44.48 ug/L 89 80 -120 50.0 48.31 ug/L 97 72 -120 50.0 45.21 ug/L 90 73 -129 50.0 44.03 ug/L 88 12 -150 50.0 45.74 ug/L 91 76 -125 50.0 49.42 ug/L 99 74 -140 50.0 44.69 ug/L 89 73 -122 50.0 51.59 ug/L 103 69-133 50.0 47.81 ug/L 96 54 -125 50.0 48.27 ug/L 97 80 -129 50.0 46.80 ug/L 94 80 -121 50.0 46.47 ug/L 93 80 -122 50.0 45.61 ug/L 91 80 -120 50.0 46.42 ug/L 93 37 -127 50.0 43.78 ug/L 88 78 -125 50.0 48.69 ug/L 97 77 -121 50.0 46.35 ug/L 93 79 -124 50.0 45.79 ug/L 92 75 -120 50.0 45.75 ug/L 92 80 -130 250 227.3 ug/L 91 60-142 50.0 45.64 ug/L 91 80 -141 250 231.1 ug/L 92 64-150 50.0 43.37 ug/L 87 71 -129 50.0 46.58 ug/L 93 79-123 250 237.5 ug/L 95 60-137 50.0 47.75 ug/L 96 72-133 50.0 47.14 ug/L 94 80 -127 Page 41 of 79 TestAmerica NashXille 11 /6/2015 QC Sample Results Client: Dextra Group Project/Site: Murphy, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 490-294431/3 Matrix: Water Analysis Batch: 294431 TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits 1,1,2,2-Tetrachloroethane 50.0 49.12 ug/L 98 69-131 Tetrachloroethene 50.0 45.53 ug/L 91 80 -126 Tetrahydrofuran 100 92.88 ug/L 93 51 -124 Toluene 50.0 45.50 ug/L 91 80 -126 trans-1,2-Dichloroethene 50.0 43.85 ug/L 88 79 -126 trans-1,3-Dichloropropene 50.0 50.02 ug/L 100 63 -134 1,2,4-Trichlorobenzene 50.0 40.51 ug/L 81 63 -133 1,1,1-Trichloroethane 50.0 45.45 ug/L 91 78-135 1,1,2-Trichloroethane 50.0 47.38 ug/L 95 80-124 Trichloroethene 50.0 45.37 ug/L 91 80 -123 Trichlorofluoromethane 50.0 47.22 ug/L 94 65 -124 1,1,2-Trichloro-1,2,2-trifluoroetha 50.0 45.49 ug/L 91 77-129 ne Vinyl chloride 50.0 47.28 ug/L 95 68 -120 v ylenes, Total 100 91.11 ug/L 91 80 -132 LCS LCS Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 102 70 - 130 Dibromofluoromethane (Surr) 100 70 - 130 1,2-Dichloroethane-d4 (Surr) 98 70- 130 Toluene-d8 (Surr) 99 70 - 130 Lab Sample ID: LCSD 490-294431/4 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 294431 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Acetone 250 207.3 ug/L 83 54- 445 2 21 Benzene 50.0 45.65 ug/L 91 80-121 2 17 Bromodichloromethane 50.0 46.98 ug/L 94 75 -129 0 18 Bromoform 50.0 55.09 ug/L 110 46 -145 1 16 Bromomethane 50.0 57.57 ug/L 115 41 -150 1 50 2-Butanone (MEK) 250 217.5 ug/L 87 62 -133 4 19 Carbon disulfide 50.0 44.85 ug/L 90 77 -126 3 21 Carbon tetrachloride 50.0 46.86 ug/L 94 64 -147 2 19 Chlorobenzene 50.0 45.68 ug/L 91 80 -120 3 14 Chloroethane 50.0 48.66 ug/L 97 72 -120 1 20 Chloroform 50.0 46.07 ug/L 92 73 -129 2 18 Chloromethane 50.0 44.37 ug/L 89 12 -150 1 31 cis-1,2-Dichloroethene 50.0 46.19 ug/L 92 76 -125 1 17 cis-1,3-Dichloropropene 50.0 50.22 ug/L 100 74 -140 2 15 Cyclohexane 50.0 44.91 ug/L 90 73 -122 0 16 Dibromochloromethane 50.0 52.73 ug/L 105 69 -133 2 15 1,2-Dibromo-3-Chloropropane 50.0 45.78 ug/L 92 54 -125 4 24 1,2-Dibromoethane (EDB) 50.0 48.24 ug/L 96 80 -129 0 15 1,2-Dichlorobenzene 50.0 47.12 ug/L 94 80 -121 1 15 1,3-Dichlorobenzene 50.0 47.61 ug/L 95 80 -122 2 15 1,4-Dichlorobenzene 50.0 46.35 ug/L 93 80 -120 2 15 TestAmerica NashXille Page 42 of 79 11/6/2015 QC Sample Results Client: Dextra Group Project/Site: Murphy, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 490-294431/4 Matrix: Water Analysis Batch: 294431 TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Dichlorodifluoromethane 50.0 46.39 ug/L 93 37 -127 0 18 1,1-Dichloroethane 50.0 44.17 ug/L 88 78-125 1 17 1,2-Dichloroethane 50.0 48.35 ug/L 97 77 -121 1 17 1,1-Dichloroethene 50.0 47.83 ug/L 96 79-124 3 17 1,2-Dichloropropane 50.0 44.61 ug/L 89 75 -120 3 17 Ethylbenzene 50.0 46.52 ug/L 93 80 -130 2 15 2-Hexanone 250 222.0 ug/L 89 60-142 2 15 Isopropylbenzene 50.0 46.89 ug/L 94 80 -141 3 16 Methyl acetate 250 226.8 ug/L 91 64 -150 2 31 Methylcyclohexane 50.0 42.80 ug/L 86 71 -129 1 19 Methylene Chloride 50.0 45.64 ug/L 91 79 -123 2 17 4-Methyl-2-pentanone (MIBK) 250 227.4 ug/L 91 60 -137 4 17 Methyl tert-butyl ether 50.0 46.61 ug/L 93 72 -133 2 16 Styrene 50.0 48.04 ug/L 96 80 -127 2 24 1,1,2,2-Tetrachloroethane 50.0 48.25 ug/L 97 69-131 2 20 Tetrachloroethene 50.0 46.43 ug/L 93 80 -126 2 16 Tetrahydrofuran 100 92.65 ug/L 93 51 -124 0 18 Toluene 50.0 46.58 ug/L 93 80 -126 2 15 trans-1,2-Dichloroethene 50.0 44.37 ug/L 89 79 -126 1 16 trans-1,3-Dichloropropene 50.0 51.19 ug/L 102 63 -134 2 14 1,2,4-Trichlorobenzene 50.0 40.08 ug/L 80 63 -133 1 19 1,1,1-Trichloroethane 50.0 46.83 ug/L 94 78-135 3 17 1,1,2-Trichloroethane 50.0 47.52 ug/L 95 80-124 0 15 Trichloroethene 50.0 46.25 ug/L 92 80 -123 2 17 Trichlorofluoromethane 50.0 48.36 ug/L 97 65 -124 2 18 1,1,2-Trichloro-1,2,2-trifluoroetha 50.0 45.61 ug/L 91 77-129 0 18 ne Vinyl chloride 50.0 44.78 ug/L 90 68 -120 5 17 v ylenes, Total 100 93.57 ug/L 94 80 -132 3 15 LCSD LCSD Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 102 70 - 130 Dibromofluoromethane (Surr) 101 70 - 130 1,2-Dichloroethane-d4 (Surr) 96 70- 130 Toluene-d8 (Surr) 101 70 - 130 Lab Sample ID: 490-90373-7 MS Matrix: Water Analysis Batch: 294431 Analyte Sample Sample Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Spike MS MS Added Result Qualifier 250 168.3 50.0 47.59 50.0 46.11 50.0 48.89 50.0 54.85 250 186.5 50.0 51.95 Client Sample ID: J1155-MW-44-102015 Prep Type: Total/NA Unit D %Rec %Rec. Limits ug/L 67 45 -141 ug/L 95 75 -133 ug/L 92 70 -140 ug/L 98 42 -147 ug/L 110 16 -163 ug/L 75 50 -138 ug/L 104 48-152 Page 43 of 79 TestAmerica NashXille 11 /6/2015 QC Sample Results Client: Dextra Group Project/Site: Murphy, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-90373-7 MS Matrix: Water Analysis Batch: 294431 Analyte Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Cyclohexane Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene 1,2-Dichloropropane Ethylbenzene 2-Hexanone Isopropylbenzene Methyl acetate Methylcyclohexane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Styrene 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene 1,2,4-Trichlorobenzene 1,1,1-Trich loroethane 1,1,2-Trich loroethane Trichloroethene Trichlorofluoromethane 1,1,2-Trich loro-1,2,2-trifluoroetha ne Vinyl chloride v ylenes, Total Surrogate 4-Bromofluorobenzene (Surr) Dibromofluoromethane (Surr) 1,2-Dichloroethane-d4 (Surr) TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-44-102015 Prep Type: Total/NA Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits N D 50.0 52.37 ug/L 105 62 -164 ND 50.0 46.65 ug/L 93 80 -129 ND 50.0 51.25 ug/L 103 58 -137 ND 50.0 46.81 ug/L 94 66 -138 ND 50.0 45.12 ug/L 90 10 -169 ND 50.0 47.82 ug/L 96 68 -138 ND 50.0 49.48 ug/L 99 71 -141 N D 50.0 51.26 ug/L 103 58 -144 ND 50.0 48.65 ug/L 97 66 -140 ND 50.0 38.53 ug/L 77 52 -126 ND 50.0 43.75 ug/L 88 75 -137 ND 50.0 45.23 ug/L 90 79 -128 ND 50.0 47.79 ug/L 96 77 -131 ND 50.0 45.75 ug/L 92 78 -126 ND 50.0 49.03 ug/L 98 40 -127 ND 50.0 46.29 ug/L 93 71 -139 ND 50.0 44.42 ug/L 89 64 -136 ND 50.0 52.48 ug/L 105 70 -142 ND 50.0 45.59 ug/L 91 67 -131 ND 50.0 49.25 ug/L 98 79 -139 N D 250 192.7 ug/L 77 50 -150 N D 50.0 49.54 ug/L 99 80 -153 N D 250 190.9 ug/L 76 30 -165 N D 50.0 48.76 ug/L 98 59 -151 N D 50.0 46.32 ug/L 93 64 -139 ND 250 200.1 ug/L 80 50 -147 ND 50.0 40.65 ug/L 81 66 -141 ND 50.0 48.02 ug/L 96 61 -148 ND 50.0 42.80 ug/L 86 56 -143 ND 50.0 51.30 ug/L 103 72 -145 ND 100 93.70 ug/L 94 34 -133 ND 50.0 49.17 ug/L 98 75 -136 ND 50.0 47.99 ug/L 96 66 -143 ND 50.0 47.77 ug/L 96 59 -135 ND 50.0 37.17 ug/L 74 60 -136 ND 50.0 50.77 ug/L 102 76 -149 ND 50.0 43.78 ug/L 88 74 -134 ND 50.0 49.66 ug/L 99 73 -144 ND 50.0 56.05 ug/L 112 58 -139 ND 50.0 51.41 ug/L 103 72 -148 0.491 J 50.0 52.48 ug/L 104 56 -129 ND 100 97.51 ug/L 98 74 -141 MS MS %Recovery Qualifier 103 99 92 Limits 70 - 130 70 - 130 70 - 130 Page 44 of 79 TestAmerica NashXille 11 /6/2015 QC Sample Results Client: Dextra Group Project/Site: Murphy, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-90373-7 MS Matrix: Water Analysis Batch: 294431 MS MS Surrogate %Recovery Qualifier Toluene-d8 (Surr) 100 Lab Sample ID: 490-90373-7 MSD Matrix: Water Analysis Batch: 294431 Sample Sample Analyte Result Qualifier Acetone ND Benzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND cis-1,2-Dichloroethene ND cis-1,3-Dichloropropene ND Cyclohexane ND Dibromochloromethane ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,3-Dichlorobenzene ND 1,4-Dichlorobenzene ND Dichlorodifluoromethane ND 1,1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND 1,2-Dichloropropene ND Ethylbenzene ND 2-Hexanone ND Isopropylbenzene ND Methyl acetate ND Methyl cyclohexane ND Methylene Chloride ND 4-Methyl-2-pentanone (MIBK) ND Methyl tert-butyl ether ND Styrene N D 1,1,2,2-Tetrachloroethane ND Tetrachloroethene ND Tetrahydrofuran ND Toluene ND trans-1,2-Dichloroethene ND trans-1,3-Dichloropropene ND Limits 70-130 TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Client Sample ID: J1155-MW-44-102015 Prep Type: Total/NA Client Sample ID: J1155-MW-44-102015 Prep Type: Total/NA Spike Added MSD MSD Result Qualifier Unit D %Rec %Rec. Limits RPD RPD Limit 250 172.6 ug/L 69 45 -141 2 21 50.0 49.75 ug/L 99 75 -133 4 17 50.0 48.88 ug/L 98 70 -140 6 18 50.0 53.15 ug/L 106 42 -147 8 16 50.0 61.97 ug/L 124 16 -163 12 50 250 202.3 ug/L 81 50-138 8 19 50.0 52.24 ug/L 104 48 -152 1 21 50.0 53.96 ug/L 108 62 -164 3 19 50.0 48.11 ug/L 96 80 -129 3 14 50.0 52.45 ug/L 105 58 -137 2 20 50.0 48.67 ug/L 97 66 -138 4 18 50.0 47.38 ug/L 95 10 -169 5 31 50.0 48.87 ug/L 98 68 -138 2 17 50.0 50.90 ug/L 102 71 -141 3 15 50.0 52.20 ug/L 104 58 -144 2 16 50.0 52.02 ug/L 104 66 -140 7 15 50.0 43.84 ug/L 88 52 -126 13 24 50.0 47.26 ug/L 95 75 -137 8 15 50.0 47.74 ug/L 95 79 -128 5 15 50.0 49.31 ug/L 99 77 -131 3 15 50.0 47.86 ug/L 96 78 -126 4 15 50.0 50.21 ug/L 100 40 -127 2 18 50.0 47.54 ug/L 95 71 -139 3 17 50.0 48.10 ug/L 96 64 -136 8 17 50.0 54.10 ug/L 108 70 -142 3 17 50.0 48.32 ug/L 97 67 -131 6 17 50.0 50.56 ug/L 101 79 -139 3 15 250 212.1 ug/L 85 50 -150 10 15 50.0 50.93 ug/L 102 80 -153 3 16 250 211.3 ug/L 85 30-165 10 31 50.0 49.96 ug/L 100 59 -151 2 19 50.0 48.15 ug/L 96 64 -139 4 17 250 219.3 ug/L 88 50 -147 9 17 50.0 45.23 ug/L 90 66 -141 11 16 50.0 50.26 ug/L 101 61 -148 5 24 50.0 46.82 ug/L 94 56 -143 9 20 50.0 52.42 ug/L 105 72 -145 2 16 100 82.87 ug/L 83 34 -133 12 18 50.0 50.91 ug/L 102 75 -136 3 15 50.0 49.52 ug/L 99 66 -143 3 16 50.0 51.42 ug/L 103 59 -135 7 14 TestAmerica NashXille Page 45 of 79 11/6/2015 QC Sample Results Client: Dextra Group TestAmerica Job ID: 490-90373-1 Project/Site: Murphy, NC SDG: 55912-J1155 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-90373-7 MSD Client Sample ID: J1155-MW-44-102015 Matrix: Water Prep Type: Total/NA Analysis Batch: 294431 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit 1,2,4-Trichlorobenzene ND 50.0 40.69 ug/L 81 60-136 9 19 1,1,1-Trichloroethane ND 50.0 52.27 ug/L 105 76-149 3 17 1,1,2-Trichloroethane ND 50.0 47.35 ug/L 95 74-134 8 15 Trichloroethene ND 50.0 51.78 ug/L 104 73 -144 4 17 Trichlorofluoromethane ND 50.0 56.84 ug/L 114 58 -139 1 18 1,1,2-Trichloro-1,2,2-trifluoroetha ND 50.0 53.33 ug/L 107 72-148 4 18 ne Vinyl chloride 0.491 J 50.0 53.15 ug/L 105 56 -129 1 17 v ylenes, Total ND 100 100.0 ug/L 100 74 -141 3 15 MSD MSD Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 104 70 - 130 Dibromofluoromethane (Surr) 101 70 - 130 Is 1,2-Dichloroethane-d4 (Surr) 95 70- 130 Toluene-d8 (Surr) 99 70 - 130 M TestAmerica NashXille Page 46 of 79 11/6/2015 QC Association Summary Client: Dextra Group Project/Site: Murphy, NC GC/MS VOA Analysis Batch: 294431 TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Lab Sample ID Client Sample ID Prep Type Matrix Method 490-90373-1 J1155-MW-23-102115 Total/NA Water 8260B 490-90373-2 J1155-MW-25-102115 Total/NA Water 8260B 490-90373-3 J1155-MW-33-102015 Total/NA Water 8260B 490-90373-4 J1155-MW-34-102015 Total/NA Water 8260B 490-90373-5 J1155-MW-40-102015 Total/NA Water 8260B 490-90373-6 J1155-MW-41-102015 Total/NA Water 8260B 490-90373-6 A155-MW-41-102015 Total/NA Water 8260B 490-90373-7 A 155-MW-44-102015 Total/NA Water 8260B 490-90373-7 MS A 155-MW-44-102015 Total/NA Water 8260B 490-90373-7 MSD A 155-MW-44-102015 Total/NA Water 8260B 490-90373-8 A 155-MW-46-102015 Total/NA Water 8260B 490-90373-9 A 155-MW-47-102015 Total/NA Water 8260B 490-90373-10 J1155-MW-60-102015 Total/NA Water 8260B 490-90373-11 J1155-MW-61-102015 Total/NA Water 8260B 490-90373-12 J1155-MW-62-102115 Total/NA Water 8260B 490-90373-13 J1155-MW-63-102115 Total/NA Water 8260B 490-90373-14 J1155-MW-64-102015 Total/NA Water 8260B 490-90373-15 J1155-PW-9-102115 Total/NA Water 8260B 490-90373-16 A 155-CMP-4-102115 Total/NA Water 8260B 490-90373-17 J1155-Trip Blank-101915 Total/NA Water 8260B LCS 490-294431/3 Lab Control Sample Total/NA Water 8260B LCSD 490-294431/4 Lab Control Sample Dup Total/NA Water 8260B MB 490-294431/7 Method Blank Total/NA Water 8260B Prep Batch 0 TestAmerica Nashville Page 47 of 79 11/6/2015 Lab Chronicle Client: Dextra Group Project/Site: Murphy, NC Client Sample ID: A 155-MW-23-102115 Date Collected: 10/21/15 09:56 Date Received: 10/23/15 10:00 TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Lab Sample ID: 490-90373-1 Matrix: Water Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 10 mL 10 mL 294431 10/30/15 20:16 KS TAL NSH Client Sample ID: J1155-MW-25-102115 Date Collected: 10/21/15 09:33 Date Received: 10/23/15 10:00 F Batch Batch Dil Initial Final Batch Prep Type Type Method Run Factor Amount Amount Number Total/NA Analysis 8260B 1 10 mL 10 mL 294431 Client Sample ID: J1155-MW-33-102015 Date Collected: 10/20/15 13:06 Date Received: 10/23/15 10:00 Lab Sample ID: 490-90373-2 Matrix: Water Prepared or Analyzed Analyst Lab 10/30/15 20:45 KS TAL NSH Lab Sample ID: 490-90373-3 Matrix: Water Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 10 mL 10 mL 294431 10/30/15 21:13 KS TAL NSH Client Sample ID: A 155-MW-34-102015 Date Collected: 10/20/15 11:39 Date Received: 10/23/15 10:00 Lab Sample ID: 490-90373-4 Matrix: Water Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 10 mL 10 mL 294431 10/30/15 21:42 KS TAL NSH Client Sample ID: A 155-MW-40-102015 Lab Sample ID: 490-90373-5 Date Collected: 10/20/15 13:44 Matrix: Water Date Received: 10/23/15 10:00 F Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 10 mL 10 mL 294431 10/30/15 22:10 KS TAL NSH Client Sample ID: J1155-MW-41-102015 Date Collected: 10/20/15 11:09 Date Received: 10/23/15 10:00 Lab Sample ID: 490-90373-6 Matrix: Water Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 10 mL 10 mL 294431 10/31/15 03:22 KS TAL NSH Total/NA Analysis 8260B 10 10 mL 10 mL 294431 10/31/15 03:51 KS TAL NSH Page 48 of 79 TestAmerica Nashville 11 /6/2015 Lab Chronicle Client: Dextra Group TestAmerica Job ID: 490-90373-1 Project/Site: Murphy, NC SDG: 55912-J1155 Client Sample ID: A 155-MW-44-102015 Lab Sample ID: 490-90373-7 Date Collected: 10/20/15 12:27 Matrix: Water Date Received: 10/23/15 10:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 10 mL 10 mL 294431 10/30/15 22:38 KS TAL NSH Client Sample ID: A 155-MW-46-102015 Lab Sample ID: 490-90373-8 Date Collected: 10/20/15 10:13 Matrix: Water Date Received: 10/23/15 10:00 F Batch Batch Dil Initial Final Batch Prepared • Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 10 mL 10 mL 294431 10/30/15 23:07 KS TAL NSH Client Sample ID: J1155-MW-47-102015 Lab Sample ID: 490-90373-9 Date Collected: 10/20/15 09:55 Matrix: Water Date Received: 10/23/15 10:00 Batch Batch Dil Initial Final Is Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 10 mL 10 mL 294431 10/30/15 23:35 KS TAL NSH Client Sample ID: J1155-MW-60-102015 Lab Sample ID: 490-90373-10 Date Collected: 10/20/15 14:43 Matrix: Water Date Received: 10/23/15 10:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 10 mL 10 mL 294431 10/31/15 00:03 KS TAL NSH Client Sample ID: A 155-MW-61-102015 Lab Sample ID: 490-90373-11 Date Collected: 10/20/15 15:23 Matrix: Water Date Received: 10/23/15 10:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 10 mL 10 mL 294431 10/31/15 00:32 KS TAL NSH Client Sample ID: J1155-MW-62-102115 Lab Sample ID: 490-90373-12 Date Collected: 10/21/15 10:53 Matrix: Water Date Received: 10/23/15 10:00 F Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 10 mL 10 mL 294431 10/31/15 11:00 KS TAL NSH TestAmerica Nashville Page 49 of 79 11/6/2015 Lab Chronicle Client: Dextra Group TestAmerica Job ID: 490-90373-1 Project/Site: Murphy, NC SDG: 55912-J1155 Client Sample ID: A 155-MW-63-102115 Lab Sample ID: 490-90373-13 Date Collected: 10/21/15 10:22 Matrix: Water Date Received: 10/23/15 10:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 10 mL 10 mL 294431 10/31/15 01:29 KS TAL NSH Client Sample ID: A 155-MW-64-102015 Lab Sample ID: 490-90373-14 Date Collected: 10/20/15 14:15 Matrix: Water Date Received: 10/23/15 10:00 F Batch Batch Dil Initial Final Batch Prepared • Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 10 mL 10 mL 294431 10/31/15 01:57 KS TAL NSH Client Sample ID: J1155-PW-9-102115 Date Collected: 10/21/15 11:59 Date Received: 10/23/15 10:00 Batch Batch Prep Type Type Method Run Total/NA Analysis 8260B Lab Sample ID: 490-90373-15 Matrix: Water Dil Initial Final Batch Factor Amount Amount Number 1 10 mL 10 mL 294431 Is Prepared or Analyzed Analyst Lab 10/31/15 02:26 KS TAL NSH Client Sample ID: J1155-CMP-4-102115 Lab Sample ID: 490-90373-16 Date Collected: 10/21/15 11:29 Matrix: Water Date Received: 10/23/15 10:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 10 mL 10 mL 294431 10/31/15 02:54 KS TAL NSH Client Sample ID: A 155-Trip Blank-101915 Lab Sample ID: 490-90373-17 Date Collected: 10/19/15 08:30 Matrix: Water Date Received: 10/23/15 10:00 F Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 10 mL 10 mL 294431 10/30/15 19:48 KS TAL NSH Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 Page 50 of 79 TestAmerica Nashville 11 /6/2015 Method Summary Client: Dextra Group Project/Site: Murphy, NC TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Method Method Description Protocol Laboratory 8260B Volatile Organic Compounds (GC/MS) SW846 TAL NSH Protocol References: SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 L1O: 12 13 14 TestAmerica Nashville Page 51 of 79 11/6/2015 Certification Summary Client: Dextra Group Project/Site: Murphy, NC Laboratory: TestAmerica Nashville The certifications listed below are applicable to this report. TestAmerica Job ID: 490-90373-1 SDG: 55912-J 1155 Authority Program EPA Region Certification ID Expiration Date North Carolina (WW/SW) State Program 4 387 12-31-15 12 13 14 TestAmerica Nashville Page 52 of 79 11/6/2015 Test medca THE LEADER IN ENVIRONMENTAL TESTING Nashville, TN COOLER RECEIPT FORM Cooler Received/Opened On 10/23/2015 00000 1. Tracking # 2-a 01 (last 4 digits, FedEx) 490-90:373 Chain of Custody Courier: FedEx IR Gun ID 96210146 2. Temperature of rep. sample or temp blank when opened: Degrees Celsius 3. If Item #2 temperature is 0°C or less, was the representative sample or temp blank frozen? YES NO..( 4. Were custody seals on outside of cooler? ES ..NO...NA yy` how T1�'J••'('� If yes, many and where: 1 5. Were the seals intact, signed, and dated correctly? ES ..NO ... NA 6. Were custody papers inside Gooier? ..NO... NA certify that I opened the cooler and answered questions 1-6 (intial) 147 ca 7. Were custody seals on containers: YES NO and Intact YES...NO.. NA Were these signed and dated correctly? YES ... NO. .NA 8. Packing mat'I used? Bubblewrap Plastic bag Peanuts Vermiculite Foam Insert Paper Other None 9. Cooling process: Ice Ice -pack Ice (direct contact) Dry ice Other None 10. Did all containers arrive in good condition (unbroken)? ONO ... NA 11. Were all container labels complete (#, date, signed, pres., etc)? (a..NO... NA 12. Did all container labels and tags agree with custody papers? .N0... NA 13a. Were VOA vials received? ES NO...NA b. Was there any observable headspace present in any VOA vial? YES..NO .NA 14. Was there a Trip Blank in this cooler? ES ..N0...NA If multiple coolers, sequence # , r certify that I unloaded the cooler and answered questions 7-14 (intial) IJ 15a. On pres'd bottles, did pH test strips suggest preservation reached the correct pH level? YES..NO.A b. Did the bottle labels indicate that the correct preservatives were used < ES .NO ... NA 16. Was residual chlorine present? YES ... N0..NA �) 4 I certify that I checked for chlorine and pH as per SOP and answered questions 15-16 (intial) 17. Were custody papers properly filled out (ink, signed, etc)? ES ..NO...NA 18. Did you sign the custody papers in the appropriate place? to . -NO 19. Were correct containers used for the analysis requested? E$)..NO... NA 20. Was sufficient amount of sample sent in each container? YES..NO... NA ] A I certify that I entered this protect into LIMS and answered questions 17-20 (intial) certifv that I attached a label with the uniaue LIMS number to each container (intial) t 1- 21. Were there Non -Conformance issues at login? YES. (2, Was a NCM generated? YES. NO ..#, BIS = Broken in shipment Cooler Receipt Fonn.doc LF-1 End of Fonn Page 53 of 79 Revised 11/28/12 11 /6/2015 cs -0 VO -j ls- k,\ -r- W L -, A m A <° A M 3 q (D � O �y CA d n(n m �-0 c o o-m y 3 0) -0 V o G)N (D01 En d —➢ Na �O,�n 3� m n _ c D N a a a < @ z H 3 'O m =r M. (a' wm W o m 0 N CD CA L m CD �� CO n(D w N d d rt N In a Q ;6 IDZ Z (D"O "D O N d Hf CD D v N_ �• D Z y T o O a r s CD CDK n Q z fU = N O rn CD` 3 CO .. 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O O (� A n n l � ? m D o' " N a a ti a n � O <C -Iw AO m0z� m n O n ' eny o -Z�: > N Z Z Z➢ Z x 1)0��� ]p�NQ AO (nN @ Z m m Ow w N n m m � � o o y V Z n CD Ch V @, O O 03 A O z O m o ID � N Page 54 of 79 11/6/2015 ON(O-)$45 rX -1 ss w ,--e., w A A A rfl N 'O U) N [n n _. �y7 �� ro Q m O U G) (n D m () _ N > D o n —I n 3 T. n O m -c N N `la' ID D N z V CDK 1 m (A) �`D cQ IV N 'o � tU �m O p°�' (D Wn7 N r•n O @ N U) ,Q Q ;U O O N ,•°• M D w S c a Z _ -p = N U) Q j ram+ CD ``JJn N >y p- �- > > CD O = Cr —_ _ lj N ry lb N N Ci Uhl -V (�31 (NI1 (Ch O = O N n' Cn C N —_ � W GG <� < <� G C� G K � (D j N O O N w > (D j (n Ul Ui Vt J O y m m m © Cl w O U1 'jJ -17 i -D-i O m -0 W �3 a a W e c ( , j-3 �.a Y W CD c m 7 Vt != _ 0 fiGCD j (D w "A N (—p o- 'z"S (n ID T Q Gi II -1 m DS G) G) G) G) G) G) CD v o m m 3 m pp \ �. N > > > m m w w m m o e a o m ! z z z z z z X Field Filtered Sample (Yes or No) o o n, m y 3 z z z z z z Perform MS/MSD (Yes or No) r) g A A A w w w w w w D 8260B LL - Site Specific VOC List - 0 < 2 a BCD sm �, m o0 O y h � a Q 3 U) p O m m (D m N X 3 m (D N C n F O H (D (n ?. - 3 y N N rD Q n `C C m cN � Q a m m wm N m ' d w w w w w w Total Number of containers 0 N A '_O O 0 omogm DDT m zN = m � m m Cnn Q Cn ozi 0- Z D D ° 0'0T -n N zo '6 o�i cDi a d = m ¢� O n N N• to 3 — o n D N 3 N a N� <C-I InAOm0 z 3 CD o C7 0 3 3 0 r. ��n'D'rnNmmmyom d m w oCn O m Ayo v0U)(n Ooze 'm nxi 4) �NOAO m N p, W (n N 0 O W 61 N n O h O C. K 0 0 IN CL f s 4 Page 55 of 79 11/6/2015 Client: Dextra Group Login Number: 90373 List Number: 1 Creator: Armstrong, Daniel Question Login Sample Receipt Checklist Answer Comment Radioactivity wasn't checked or is </= background as measured by a True survey meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. N/A The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A 4AC Job Number: 490-90373-1 SDG Number: 55912-J1155 List Source: TestAmerica Nashville TestAmerica Nashville Page 56 of 79 11/6/2015 Corrective Action Monitoring Report October 2015 Semi -Annual Event Appendix B EMServt*ces Environmental Monitoring Services, LLC Phone (770) 516-2081 Fax (678) 445-3276 October 26, 2015 Ms. Lisa Harvey Test America - Savannah 5102 LaRoche Avenue Savannah, GA 31404 RE: Semi -Annual Groundwater Sampling at the Murphy, NC (former Clifton Precision) site Lisa, On October 19t' - 22°d we completed the semi-annual groundwater -sampling event at the Murphy, NC site. The following points were sampled for: MW-10, 11, 12, 13, 17, 20, 32, 33, 34, 35, 36, 37, 40, Permit specific VOC's by EPA 8260B 41, 45, 47, 60, 61, 62, 63, DUP-1 (MW-35), DUP-2 (SW-10), DUP-3 (MW-34), DUP-4 (MW-13), CMP-1, 3, 4, SW-3, 6, 10, SP-26, RW-2, 3, 4, 5 The sampling activities were performed according to EPA Region IV Science and Ecosystem Support Division's Field Branches Quality System and Technical Procedures. Upon arrival at the site, the process of collecting water levels began. The depth to water was measured from a surveyed mark on the top of casing, if present. The process of collecting water levels was completed within a 24-hour period to ensure a representative potentiometric map. The water level indicator was cleaned in between each well using a Liquinox soap solution followed by a water rinse, then a DI water rinse. Upon arrival at each well, notes were taken as to the condition of the area around the well and the condition of the well itself. The samplers then donned new Nitrile gloves. These gloves were changed as often as deemed necessary to prevent contamination of the samples. A new piece of plastic was laid down next to the well to serve as a work area. We calculated the purge volume to three well volumes using a standard formula. Purging continued until at least three well volumes were removed and the field parameters were stable or until the well was purged dry. The purge water was captured in 5-gallon buckets to quantify the purge volumes. We employed a submersible pump for the purging of all wells. The pump used was a Grundfos Redi-Flo 2 model that was attached to dedicated, Teflon tubing at each well. After purging was complete, the pump was washed using a Liquinox soap solution followed by a water rinse and a DI water rinse. Each well was sampled using a dedicated Teflon bailer. The VOC samples were collected immediately following the purging process or upon sufficient recovery for the wells that purged dry. Well RW-2 was sampled with a new disposable Teflon bailer as this well no longer has in -place plumbing. Off -site wells MW-42 and 43 were unable to be located because of recent tilling activities by the landowner. "For all your environmental monitoring needs " 803 Bermuda Run Woodstock, GA 30189 inquiry@emservicesonline.com Pagel oft Off -site well PW-16's pump apparently does not have electricity running to it. The well is unable to be sampled. During the purging process, pH, conductivity, temperature, and turbidity readings were collected at each well volume and recorded in the logbook. These readings were recorded from an YSI 556MPS that was calibrated each morning. Turbidity readings were collected using a Hach DR-820, which is zeroed before each reading. The Hach DR-820 contains a factory calibration that is checked in-house using formazine standards. The samples were collected in containers provided by the laboratory. These containers were of types, sizes and preserved in a manner consistent with EPA Region IV SESD guidance. Upon filling, the containers were placed on ice. The samples were delivered via Federal Express under chain of custody to Test America located in Savannah, GA. We appreciate the opportunity to work with you on this project, and look forward to any feedback you have. Respectfully, Jeff Johnson Attachments: Field Notes NGC-FSK Page 2 of 2 EMServieves Environmental Monitoring Services, LLC Former Clifton Precision Water Lbvels Date: Well ID Time DTW DTB Well ID MW-41 MW-42 MW-43 MW-44 MW-45 MW-46 MW-47 MW-49 MW-50 MW-51 MW-52 MW-53 MW-54 MW-55 MW-56 MW-57 MW-60 MW-61 MW-62 MW-63 MW-64 RW-2 RW-3 RW-4 RW-5 PW-16 Time DTW DTB MW-9 1 9.59 2 S ` 'b"� 157.90 MW-10 JC) % , (q 35.91 27.34 MW-1l D2-C) 9. )a 74.73 82.40 MW-12 I O iS 2 7, I LI 31.87 S -7. 73.43 MW-13 31.12 ``9 J �32 7r 11 76.65 MW-14R 80.51 9q I"Z • -(�- 1 52.90 MW-17 37.20 ( 3 Z- 92.62 MW-18 65.04 10.26 MW-19R 69.30 81.41 MW-20 ` I 2- I n 7 1 13.93 114.30 MW-22 Ii j I 6 7, 7g 52.11 40.61 MW-23 009 211 b 28.38 52.29 MW-25 �Qj 2 Q b 29.64 / [gyp 3 0 i 3 , 13 37.85 MW-27 79.12 f 6 Z (e i LI , S 2 109.51 MW-28 51.04 77.21 MW-29 29.63 91.08 MW-30 Well filled in at 2' BGS 005 A,65' 'n 49.18 MW-31 24.86 , DO6 4(i- t a✓t 84.15 MW-32 Z O 7 , D 31.60 I D [ Z Z. , 9,0 44.55 MW-33 % S 7 �1 �s tav, 74.56 to 2 ° 84.00 MW-34 10 S , 3 6 40.86 D03 3 , O'9 15.03 MW-35 ) U ld 7 :Ps 90.04 39.92 MW-36 69.64 31.83 MW-37 108.22 37.70 MW-38 103.11 117.48 MW-39 167.35 q S 2` S 156.29 MW-40 1 Mw .,35 1 f-1 D-7 7- Z 9 EMServices Environmental Monitoring Services, LLC Former Clifton Precision Water Levels Date: Well ID Time DTW DTB Well ID MW-41 MW-42 MW-43 MW-44 MW-45 MW-46 MW-47 MW-49 Time DTW DTB MW-9 15 76 9.59 157.90 MW-10 35.91 27.34 MW-11 74.73 82.40 MW-12 31.87 73.43 MW-13 10Z ` 6 31.12 76.65 MW-14R 10 S 1 0.44 80.51 52.90 MW-17 f Z�I 7 6 . 3 \ 37.20 92.62 MW-18 q ��,� I 65.04 i I IS3 7 10.26 MW-19R 3�Ivj i3= �� 69.30 MW-50 MW-51 MW-52 MW-53 MW-54 MW-55 MW-56 MW-57 MW-60 M W-61 MW-62 MW-63 MW-64 RW-2 RW-3 RW-4 RW-5 �� �, �L 81.41 MW-20 13.93 �;SS , g 114.30 MW-22 52.11 9� 40.61 MW-23 28.38 52.29 MW-25 29.64 37.85 MW-27 i I / q 79.12 109.51 MW-28 ''j j //�/ V )Z I , '3S 51.04 / ZS b 7r 30 77.21 MW-29 I Z ` � � 29.63 1 Z�3 2-z 3 j 91.08 MW-30 Well filled in at 2' BGS 49.18 M W-31 j Z-z " Li f1 24.86 84.15 MW-32 31.60 44.55 MW-33 74.56 84.00 MW-34 40.86 15.03 MW-35 90.04 39.92 MW-36 ,Z Z qo _ ,I 69.64 1170 31.83 MW-37 01 � Z-Z 3 108.22 �Sc)t �I.5' 37.70 MW-38 014 --►Z 103.11 1 �6 117.48 MW-39 ��5� 2� • 3Z 167.35 PW-16 �jj(�(�, M W-40 156.29 EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-10 1 0_ V) 4 t S Date DTW' 7 { DTBZ 35.91 r q * 1 Well Volume (DTB - DTW) 0.163p b 9 3 Well Volumes 1 WV * 3 = i LI a t)! Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America- Savannah CoC No: J1155S10151 Time Started: �OS� Purge Rate (gallons per minute) Actual Volume (gallons) pH SC ( S/cm) T (°C) Turbidity (NTU Time 1\03 (),So 2.so 7,60 4-1,3S� 110�? 0, SD LI , 7S -If'3 6 9 ZZ i113 O,SO 7,ZS 7, 12 11 V O' S o 9. E O 7 It Z3 0.S0 �z,0C> 61 II Z9 o► SD 1LI, ZS (, q 7 901 l g. Z 3 V 3 O, so 16, 7S 6,90 903 19, I 31 Comments Pump control setting: $ 3 H .y Sam le time: I ` �u Depth to water as measured in feet from top of casing Total well depth measured in feet from top of casing Field Technician: Client Site Well ID Date DTW' DTB2 1 Well Volume 3 Well Volumes Purge Method Sample Method Parameters Laboratory/CoC No. EMServices Environmental Monitoring Services, LLC Field Data Sheet Former Clifton Precision Murphy, NC MW-11 10^`a-1 S'' 74.73 (DTB - DTW) * 0.653 = L13 •S 1WV*3= 13C) SS Submersible Pump / Dedicated Teflon Tubing Dedicated Teflon Bailer Site Specific VOC's (EPA 826013) Test America - Savannah CoC No: J1155S10151 Time Started: 'L Pur]Rate (gal m(gallons) Actual VolumeTime 1.50 72. nO 6 7 2 3 Ins 1 1 Li/-wo 7, 79 t � t I .00R L W i Comments Pump control setting: Sample time: i OP-i 00 ' Depth to water as measured in feet from top of casing 2 Total well depth measured ' feet from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-12 Date ' C jam' DTW' 7, ly DTB2 31.87 * ' �-3 1 Well Volume (DTB - DTW) 0.163 = 3 Well Volumes 1 WV * 3 = i ?- -CY? Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 8260B) Laboratory/CoC No. Test America - Savannah CoC No: J1155S10151 Time Started: Purge Rate (gallons per minute) Actual Volume (gallons) pH SC ( S/cm) T (°C) Turbidity (NTU Time 1y1� c7. Z,ZS -56 i LI IJC, 0.7 S 4 > ZS 7.4 33�7 1-77 j -M � �� 3�' 17,-? .s Comments Pump control setting: J I . / I I N'aCyS- r- C �S Sample time: IC �5 Depth to water as measured in feet from top of casing 2 Total well depth measured in from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Site Well ID Date Former Clifton Precision Murphy, NC MW-13 \O,Z) ` 1s DTW' 3. `9 0 DTB2 31.12 1 Well Volume (DTB - DTW) " 0.163 3 Well Volumes 1WV * 3 = jQ , 63 Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America - Savannah CoC No: Jl 155SIO151 Time Started: Purge Rate (gallons per minute) Actual Volume (gallons) PH SC ( S/cm) T (°C) Turbidity (NTU) Time 13c��i 0,T5 131Z 0. i 11 j 00 7• t Z ZC 2 i cZ, 6 ?lldd 1Y I�i C7.?5 C .00 7. a4 -Z0 i�==. w Tt,oa ) 3) 7 ?, &-k:? -7 , 1) ZG `-1 1 g .� ' ►,o� 1, ►9 o, I5 Z9 1 x, G 41( -- i )-Z a; 7 �z. �u G.��, Zs� Ik' co 33G i'3 c, tj O� -7 IA OC) 00 Comments Pump control setting: IQ 3 HZ Sample time: 3 Z 1 Depth to water as measured in feet from top of casing Z Total well depth measured in feet from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-17 Date ID - ICI' IS DTW Cad - DTB2 37.20 1 Well Volume (DTB - DTW) * 0.163 = `� .(t 3 Well Volumes 1WV * 3 = qs , Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America - Savannah CoC No: J1155SIO151 Time Started: 1' Purge Rate (gallons per minute) Actual Volume (gallons) pH SC (PS/cm) T (°C) Turbidity (NTU) Time �2J3 0.15 3. w 7 j�. 77>4 Y l 0, -)5 Coo -? y-L 3se-I LI oc> 7OZ 3G4 16, 1 13 1�.00 7,OZ 36S I4, 13 1-7 1 1 Comments Pump control setting: <�I ' Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-20 Date 10 ---19 - I S DTW' f� c ( 2 S DTB2 13.93 1 Well Volume (DTB - DTW) * 0.163 = 1 1 b 3 Well Volumes 1 W V* 3='3, q! Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America - Savannah CoC No: J 1155S 10151 11`1i-41Aja. Time Started: �' purge Rate (gallons per Actual Volume (allons) H SC ( S/cm) Turbidity Time 71minute) il`lC (D.3(Z) J.�O �.�3 Z'1S -SS i 14`15 0.30 l,.ZZ� C, 2-23 V 0,30 \ AID C•CI() Z)5 rS `I o •3-0 3.00 C; iy 2�Z ZJ 5 t I�Sv 0,30 -3.G3 Comments Pump control setting: C '7 1-1Z time: 1 7-01 Depth to water as measured in feet from top of casing 2 Total well depth measured in f from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-28 Date ((, " DTW" c� L 35 DTB2 51.04 1 Well Volume (DTB - DTW) " 0.653 = Z`1 3 Well Volumes 1 WV * 3 = b3 , C,3 Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 8260B) Laboratory/CoC No. Test America - Savannah CoC No: J 1155SI O151 Time Started:17,1q I Purge Rate (gallons per minute)(gallons) Actual Volume pH SC (PS/cm) T (°C) Turbidity (NTU) Time �22► LSO iti . 0c) r9 79 ?`Z`3 17 -Z"� G 6 3 !; 17. 9 lq 7 vs Comments Pump control setting: 5 lea ?JCSCJ �� J 2g 0c) c �S Sample time:( Z -3L V ' Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-32 Date t0- tvi-•7l� DTW' 9Y O I DTBZ 31.60 1 Well Volume (DTB - DTW) 0.163 = 3. 5 L� 3 Well Volumes I WV * 3 = i p, Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 8260B) Laboratory/CoC No. Test America - Savannah CoC No: J1155S10151 Time Started: purge Rate (gallons per minute) Actual Volume (ailons) H SC ( Slcm) T (°C) Turbidity (NTU) Time Q 1 2- 121 -C o.SJ I ZICI 0.SJ IZ-�3 0 �.Zp -?� �8C� i7S �-2-z�. o.s� �. Z9 395 ids s 1 0 �> Nz3v 0.SJ lo�1-C) ,Z-? Li CZ 16,0 �15 Comments Pump control setting: -' I Sam le time: I Z 3 ti Depth to water as measured in feet from top of casing Total well depth measured in feet from top of casing Field Technician: Client Site Well ID Date DTW' DTB2 1 Well Volume 3 Well Volumes Purge Method Sample Method Parameters Laboratory/CoC No. EMServices Environmental Monitoring Services, LLC Field Data Sheet Former Clifton Precision Murphy, NC MW-35 iO-t`1- t5 - �.-y 90.04 (DTB - DTW)* 0.163 IWV*3= q(!)"---L SS Submersible Pump / Dedicated Teflon Tubing Dedicated Teflon Bailer Site Specific VOC's (EPA 8260B) Test America - Savannah CoC No: J1155S 10151 Time Started:) Purge Rate (gallons per minute) Actual Volume (gallons) pH SC ( S/cm) Turbidity Time ILAiL j.jJ �.15 f.53 ,36 1G.3 �li0l� w) I,SD 301 iS.S i��z ILi SL' 30 is,s 95Li Lio.--C S .1 C5 t Comments Pump control setting: ) 63 H-, ISamp'le' time: LI 3 -/ Depth to water as measured in feet from top of casing z Total well depth measured ' feet from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-36 Date C 10- Q - (1 DTW' 10' Lly DTB2 69.64 1 Well Volume (DTB - DTW) * 0.163 = 1•� 3 Well Volumes 1 WV * 3 = 14. 2� Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America - Savannah CoC No: J1155S10151 Time Started: I Purge Rate (gallons per minute) Actual Volume (gallons) pH SC ( S/cm T (°C) Turbidity (NTU) Time tZ `k3 (. a D 2':)C) ? .37 FICA )Z . Z:� I v-1 i, O 5, Comments Pump control setting: 1 Y% iq z, Sample time: 12,53 Depth to water as measured in feet from top of casing 2 TotaI well depth measured in feet from top of casing Field Technician.. EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-37 Date DTW ZZ. 33 DTBZ 108.22 * g 1 Well Volume (DTB - DTW) 0.163 = 3 Well Volumes 1 WV * 3= `{ Z, O CI Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America - Savannah CoC No: J1155S10151 13 q Time Started: J Purge Rate (gallons per minute) Actual Volume (gallons) PH SC ( S/cm) T (°C) Turbidity (NTU) Time 7� 3" 1 fyj)o 3W Comments Pump control setting: t_o:3 Sample time: f -I 60 aG Q"`rT O J rr ' Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-42q Date DTW' —' DTB2 27.34 1 Well Volume (DTB - DTW) * 0.I63 = 3 Well Volumes 1 WV * 3 = Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America - Savannah CoC No: J1155SIO152 Time Started: Purge Rate (gallons per minute) Actual Volume (gallons) pH SC (PS/cm) T (°C) Turbidity (NTU) Time Comments Pump control setting: } Sample time: Depth to water as measured in feet from top of casing Total well depth measured in feet from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-43 Date io DTW DTB2 82.40 1 Well Volume (DTB - DTW) * 0.163 = . 3 Well Volumes 1 WV * 3 = Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America - Savannah CoC No: J1155SIO152 Time Started: Purge Rate (gallons per minute) Actual Volume (gallons) pH SC ( S/cm) T (°C) Turbidity (NTU) Time Comments Pump control setting: L),ublc 40 10re,: / bor-iec� Sample time: Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing Field Technicia EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-45 I(D-L9-ts Date DTW� l 1 1 1 DTB2 76.65 s 1 Well Volume (DTB - DTW) 0.163 = 1 �� 3 Well Volumes 1WV M 3 = I Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 8260B) Laboratory/CoC No. Test America - Savannah CoC No: J1155SIO152 Time Started: I�ZS Purge Rate (gallons per minute) Actual Volume (gallons) pH SC (PS/cm) T (°C) Turbidity (NTU) Time j3 1,S0 6,00 7.23S 1333 o IhSO -7 339 1c.0 Zl� 1337 �S© IISO 33, Ic.I Q)4i f-3.0j -7.Lm 33`t 16.0 rtiS Zz.cc `?,SO 339 I6,a t6� �3g 16� z 7S Comments Pump control setting: 04 &IUCH here, God, Sample time: -� S3 Depth to water as measured in feet from top of casing 2 Total well depth measure 'n feet from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Sample Method Direct grab Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No Test America - Savannah CoC No: N/A Turbidity Sample ID Date Time pH SC (µS/cm) T (°C) (NTU) F—Pw- 16 110-11--a t 2,� Field Technician. Client Site Sample Method Parameters Laboratory/CoC No EMServices Environmental Monitoring Services, LLC Field Data Sheet Former Clifton Precision Murphy, NC Dedicated Teflon Bailer Site Specific VOC's (EPA 8260B) Test America - Savannah CoC No: J 1 ] 55 S ] 0142/J 1155 S 1015: Sample ID Date Time H SC (µS/cm) T (°C) Turbidity (NTU) RW-2 `O-z�s 9z t i3 2�s )�� 0-2 3s� RW-4 1�`�Z�IS ! `� v� `� �/ !1I =G �( RW-5 IV`ZZ-�� �ZZ �7Q qo CMP-] '-7 `l CMP-3 ►o - z - 15 --L go gS 11, I a SW-3 to `j 6"� UD SW-6 �d ZL 9SS -7Z-3 28 SW-10 7 tgZ-I 9 S io. `7 �o SP-26 6 �)� g -1� S O 1 1: 1 q 7--J Field Technician: EMServieces Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Sample Method Parameters Laboratory/CoC No. Field Technician: Murphy, NC Direct grab Site Specific VOC's (EPA 8260B) Test America - Savannah CoC No: J l l 55S 10153 Sample ID Date Time EB-I 10- icl — r� 1103 EB-2 10-70-IS IC3Z EB-3 EB-4 10 --�5 EB-5 Comments DI Water from Test America Atlanta Service Center stored at EM Services' office. Equipment Blanks poured at equipment trailer near storage area. EMServt*ces Environmental Monitoring Services, LLC Phone (770) 516-2081 Fax (678) 445-3276 October 26, 2015 Ms. Roxanne Connor Test America — Nashville 2960 Foster Creighton Dr. Nashville, TN 37207 RE: Groundwater and Surface Water Sampling at the Murphy, NC (former Clifton Precision) Site Roxanne, On October 19t' — 2I't we completed the 3' Month (I" Quarter) Groundwater Reinjection Monitoring sampling event at the Murphy, NC site. The following points were sampled for: MW-23, 23, 33, 34, 40, 41, 44, 46, 47, 60, 61, Permit specific VOC's by EPA 8260B LL 62, 63, 64, CMP-4, PW-9 The sampling activities were performed according to EPA Region IV Science and Ecosystem Support Division's Field Branches Quality System and Technical Procedures. Upon arrival at the site, the process of collecting water levels began. The depth to water was measured from a surveyed mark on the top of casing, if present. The process of collecting water levels was completed within a 24-hour period to ensure a representative potentiometric map. The water level indicator was cleaned in between each well using a Liquinox soap solution followed by a water rinse, then a DI water rinse. Upon arrival at each well, notes were taken as to the condition of the area around the well and the condition of the well itself. The samplers then donned new Nitrile gloves. These gloves were changed as often as deemed necessary to prevent contamination of the samples. A new piece of plastic was laid down next to the well to serve as a work area. We calculated the purge volume to three well volumes using a standard formula. Purging continued until at least three well volumes were removed and the field parameters were stable or until the well was purged dry. The purge water was captured in 5-gallon buckets to quantify the purge volumes. We employed a submersible pump for the purging of all wells. The pump used was a Grundfos Redi-Flo 2 model that was attached to dedicated, Teflon tubing at each well. After purging was complete, the pump was washed using a Liquinox soap solution followed by a water rinse and a DI water rinse. Each well was sampled using a dedicated Teflon bailer. The VOC samples were collected immediately following the purging process or upon sufficient recovery for the wells that purged dry. During the purging process, pH, conductivity, temperature, and turbidity readings were collected at each well volume and recorded in the logbook. These readings were recorded from an YSI 556MPS that was calibrated each morning. Turbidity readings were collected using a Hach DR-820, which is zeroed before each reading. The Hach DR-820 contains a factory calibration that is checked in-house using formazine "For all your environmental monitoring needs " 803 Bermuda Run Woodstock, GA 30189 inquiry@emservicesonline.com Pagel oft standards. In addition to these parameters, field tests for carbon dioxide and hydrogen peroxide were conducted and results also recorded in the logbook. The samples were collected in containers provided by the laboratory. These containers were of types, sizes and preserved in a manner consistent with EPA Region IV SESD guidance. Upon filling, the containers were placed on ice. The samples were delivered via Federal Express under chain of custody to Test America located in Nashville, TN. We appreciate the opportunity to work with you on this project, and look forward to any feedback you have. Respectfully, Jeff Johnson Attachments: Field Notes NGC-FSK Page 2 of 2 EMServices Environmental Monitoring Services, LLC Field Data SIz'eet Client Former Clifton Precision Site Murphy, NC Well ID MW-23 Date DTW Z.L� DTB2 28.38 1 Well Volume (DTB - DTW) * 0.163 3 Well Volumes 1WV * 3 = Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 8260B) Laboratory/CoC No. Test America - Nashville CoC No: J 1155NI O151 6 Time Started: a Purge Rate (gallons per minute) Actual Volume (gallons) pH Turbidity Time �.GS Ll L-)q 0 134, 2sZ. i-13 j au L1 Ll{Z iL►, j �zS � LJG ', L7t3 C& -1e; L1 I --I IN: L' ^1'ty 1.00 r,�00 -7.10 03 )il.3 �WZ ,,-1 0 ;. 0v ;1, z5 .ace 1i rz 14 63 �Z2. C)r Li09 ILI,� Comments Pump control setting: P 7 CO2 (mg/L) _ C7 H2O2 (mg/L) _ '3 Sam le time: 1 S To I Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing Field Technician: Client S ite Well 1D ,."Date DTW' DTB2 1 Well Volume 3 Well Volumes Purge Method Sample Method Parameters Laboratory/CoC No. EMServices Environmental Monitoring Services, LLC Field Data Sheet Former Clifton Precision Murphy, NC MW-25 29.64 (DTB - DTW) * 0.106/3 = 1WV*3= SS Submersible Pump / Dedicated Teflon Tubing Dedicated Teflon Bailer Site Specific VOC's (EPA 826013) Test America - Nashville CoC No: J1155N 10151 Time Started: -to Y purge Rate (gallons per minute) Actual Volume (gallons) pH SC (µS/cm) T (°C Turbidity (NTU) Time 91,0 1. Do -za S 5 ,5 LIST 13, Y -21,00 17- i,00 11, b\-D C�-L) Ll'3`L 13.2 "L]s 10 O c .-)cj C,cn- 13 , C 09 `� 17 1,00 A.10 C. 13..E is`? 1 ,100 11. 2 `� 4n. iG, 4Z�;.,';- 1 'ZlO Z__L t. DO i"3,`�� �.a1 117(1" . 13,E 1 I Oo �V, 00 L117 13.6 rZ2 q Lc.+ -17-.2 5 7 . CP) L12.3 13, -7 � L Comments Pump control setting: Ct,5 CO, (mg/L) = qo H2O2 (mg/L) _ Sam le time: Depth to water as measured in feet from top of casing 2 Total well depth meas ed in feet from top of casing Field Technician: `` EMServ"ices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-33 j©-IC2 — i.S Date DTW Aries lt:,h DTB2 74.56 1 Well Volume 0.163 = 2- 4 S (DTB - DTW) *1, 3 Well Volumes 1WV * 3 = 26, `�5 Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America - Nashville CoC No: J1155N10151 Time Started: ����, Purge Rate (gallons per minute) Actual Volume (gallons) pH SC (µS/cm) T (°C) Turbidity (NTU) Time �2 3 0 �,�s -� �� Sao i�, >►��, 17,' 7 [2,, z.s IS, ;f �Z,30 �.►�� 3cb ►5.7 �r�ov t� 55 6,5O zq,So �7-7`3 12 s"I I � SU `7r L 7 :jbO IS, 3 S so "7AS .zi 9 control setting: � -*� ! C'.Z_ (mg/L) = i 5 H202 (mg/L) _ C=O (5 x Ile time: Depth to water as measured in feet from top of casing z Total well depth measured in feet from top of casing Field Technician: Client Site Well ID Date DTW 1 DTB2 1 Well Volume 3 Well Volumes Purge Method Sample Method Parameters Laboratory/CoC No. EMServices Environmental Monitoring Services, LLC Field Data Sheet Former Clifton Precision Murphy, NC MW-34 o-ZC) -5 3 G 40.86 q (nTR - 1)TW) * 0 1 Al 79 1WV*3= SS Submersible Pump / Dedicated Teflon Tubing Dedicated Teflon Bailer Site Specific VOC's (EPA 826013) Test America - Nashville CoC No: J1155NIO151 Time Started:) 1 Purge Rate (gallons per minute) Actual Volume (gallons) H SC ( S/cm) T (-C) Turbidity (NTU) Time 1.1.0 it 00 2 0) :. 1 tZ3 (, 00 6-c)0 25i3 0 r i Z"I Lob iz, i:�D 7 zz W LI 6 11,32 I o0 15, O . 7 , Z9 2i Z 16,3 d5 i 1 '3 S i oo ) *TT Z 3 i 5, Ll Comments 1 control setting: `2t (mg/L) _ .Z`' H202 (mg/L) = S J CJ JC p OI�YiT� a J time: 13 Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-40 Date `-Z. p — 5 DTW DTB2 156.29 1 Well Volume (DTB - DTW) * 0.163 = Z S t 07 3 Well Volumes 1 WV * 3= S i ZQ Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 8260B) Laboratory/CoC,No. Test America - Nashville CoC No: J1155NIO151 Time Started: 1-3ILI purge Rate (gallons per Actual Volume Turbidity (NTU) Time 11 1319 7S �,�� z��� �� s �►� 1323 �� so zs,'zS SO 73'18,00 T T. 4 `21 I �2> C ..5C3 5(0�$:9 `1.161 -'�-)y lql ZS 7,25 `t-7S 17, 3[ 13Lii �,SU -63, ZS '� , S Comments Pump control setting: ZS s�� CO2 (mg/L) = 17S H2O2 (mg/L) = 3 3 Sam le time: ''S Ll L Depth to water as measured in feet from top of casing z Total well depth measured in feet from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-41 Date DTW. �, g DTB2 157.90 1 Well Volume , (DTB - DTW) * 0.163 = 2H , -It 3 Well Volumes 1 WV * 3 =' Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC. No. Test America - Nashville COC No: JI155NI0151 Time Started: j Purge Rate (gallons per minute) Actual Volume (gallons) pH SC ( S/cm) T (°C) Turbidity (NTU) Time Sc)�Z. SO �, �3 Z3 `L.... 1 . Z 3 I,I 1�4C�0 :. i" JO '� .W �j. 39 3-2 ::�� o�jl� t V S ('. . �� ,�� . ��l% fir, .2 alp' 5o , CO 6,03 13 8 IT I S' L� s� u Pump control setting: 21 c1 11 z fb Wit. Dr & W.Co l j J- CO2 (mg/W H2O2 (mg/L) Sample time: Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing M Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-44 Date ip_ 20 ` i5 DTW 7 �3 DTB2 73.43 10 ` '16 Z 1 Well Volume (DTB - DTW) * 0.163 = 3 Well Volumes 1 WV * 3= �32 e Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters w: Site Specific VOC's (EPA 8260B) Laboratory/CoC No. Test America - Nashville CoC No: J 1155N 10151 Time Started. Time Purge Rate (gallons per minute) Actual - Volume (gallons) pH SC (µS/cm) T (°C) Turbidity (NTU) 1zo1 1,C. S.So date`'( 30°1 1G,-i zff's 12-I0 i.SQ t 1 00 `7 ,3G 71,03 1S, L8 1`z 12 ILI I,S� IG .SO T72A Zg_7 1J,( CI -CZ, Go -). O 14-Z A ),SL? 33 .00 ,OLI —L93 1`I1, t 10 Comments Pump control setting: i of H;. (mg/) _ H2O2 (mg/L) _ (Sx- ale time: 2 Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing Field Technician:~- — a" EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-46 Date DTW� DTB2 52.90 1 Well Volume (DTB - DTW) * 0.163 < 5 3 Well Volumes 1 WV * 3 = I q .66 Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America - Nashville CoC No: JI155N10151 Time Started: i �O Z Purge Rate (gallons per minute) Actual Volume (gallons) H SC (µS/cm) T (°C) Turbidity (NTU) Time 100)0 1.00 73 , S D U- `Z xI O � G . G 30 10(7�1 1, 6, ZS 9.G(� 11L1 iC; , C, ,f Comments Pump control setting: ISJ 1-1 Z COZ (mg/L) _ tH202 (mg/L) time: Vo l.'.� Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing Field Technician: �3 EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-47 Date DTW DTB2 92.62 1 Well Volume (DTB - DTW) * 0.163 = 1 Z 3 Well Volumes 1WV * 3 = �' 7 Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 8260B) Laboratory/CoC No.. 'Test America - Nashville CoC No: J1155NIO151 Time Started: ` Purge Rate (gallons per minute) Actual Volume (gallons) pH SC (µS/cm) T (°C) Turbidity (NTU) Time 91.3 S E s S , r � ► kb rz'' 7z� 1 �7 � � S� 13,00 � , y 9 1'77 �Z2 1, s6 1?tSO� YI 167 1q, 9 00 Zv 1, SO Z6,6o 7, 10 rbs 15, O S-q 3 1- S o 32 t S' -� 1-31 ►G/-I "1, c 3c �3S -S0 7300 15,0 61 LIS',S0 ` 9 1G � 15. Z� 9 co 7, SO '1'5 9S 3 NO Qnv Comments p control setting: J H z (mg/L) _ ( D H202 (mg/L) = Z ale time: c. Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-60 Date 10 - Z0 - 1 S DTW f des lay DTB2 49.18 1 Well Volume (DTB - DTW) * 0.163 = -� 3 Well Volumes I WV * 3 = Z C-( r �S Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America - Nashville CoC No: J1155NI0151 Time Started: N Purge Rate (gallons per minute) Actual Volume (gallons) pH SC (PS/cm) T (°C) Turbidity (NTU) Time j , SJ �`ga ^� �/f�>`a� r_% ,� �d Z I 1 C.,1 P `�,216 J,SD 9,03 -D� 15,'Y �7�} �'1 J V-01 J ' j k 3 . so/ r � �1 799 I'Sr .S JCS 1 ►`►37 `30o �S , 2Z 300 15,-Z 33 Comments Pump control setting: CO2 (mg/L) _ �J H20z (mg/L) = Z Sample time: 1443 Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing Field Technician: _7 Client Site Well ID Environmental Monitoring Services, LLC Field Data Sheet Former Clifton Precision Murphy, NC MW-61 Date DTW' DTB2 84.15 * 1 Well Volume (DTB - DTW) 0.163 = 3 Well Volumes 1 WV * 3 = LI ) , 1S Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 8260B) Laboratory/CoC No. Test America - Nashville CoC No: J1155NIO151 Time Started: 1 purge Rate (gallons per minute) Actual Volume (gallons) pH SC (µS/cm) T (°C) Turbidity (NTU) Time SO 7, -2'T-) (� .3 35 IyS9 Sb 11�1►cam Z9� j, "-I q is � �(5o �1,GD © 9 SO 2,5.6D' IS 1 I ' 5c> S � cc `S , C1 CD Comments Pump control setting: t q 3 CO2 (mg/L) _ �V H2O2 (mg/L) _ Sample time: ' Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing Field Technician: EMServices Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-62 Date DTWi DTB2 44.55 1 Well Volume (DTB - DTW) * 0.163 3 Volumes 1 * 3 = Well WV Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America - Nashville CoC No: J 1155N10152 Time Started: C)-Ia Purge Rate (gallons per minute) Actual Volume (gallons) pH SC (µS/cm) T (°C) Turbidity (NTU) Time la y 10© '3, SO `1u16 Lln, IS1 3 b0 1,00 -).•2S LII,-? 1G .l 0 1��11 koa �0,S-D -1.16 M6 iv Ll Ll 1,00 P-1,.00 "1, j Li iS i Jos.) ),00 121,00 "? 407 1 C- 0 Comments Pump control setting: 1?1 1 1, CO2 (mg/L) = 2, C) H2O2 (mg/L) = Li ,Sample time: 10 jS Depth to water as measured in feet from top of casing z Total well depth measured in feet from top of casing _—:V, Field Technician: EM Services Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Well ID MW-63 Date 1c)-11 iS DTW' 2 , 90 DTB2 84.00 1 Well Volume (DTB - DTW) * 0.163 = •3 ° 3 S 3 Well Volumes I WV * 3 = WO °©S Purge Method SS Submersible Pump / Dedicated Teflon Tubing Sample Method Dedicated Teflon Bailer Parameters Site Specific VOC's (EPA 8260B) Laboratory/CoC No. Test America - Nashville CoC No: J1155N10152 Time Started: ��ti�/ Purge Rate (gallons per minute) Actual Volume (gallons) pH SC ( S/cm) T (°C) Turbidity (NTU) Time 101 1,00 iitl.00 -?,3-1 403 ►ram. Z I ® Comments Pump control setting: 715- 1-1-L V,r (3� CA ry � 1 --=v CO, (mg/t;) = i 5 H2O2 (mg/L) _ time: 10 2 Z Depth to water as measured in feet from top of casing 2 Total well depth measured iD,.fqet fromtop of casing Field Technician: Client Site Well ID Date DTW 1 DTB2 1 Well Volume 3 Well Volumes' Purge Method Sample Method Parameters Laboratory/CoC No. EMServices Environmental Monitoring Services, LLC Field Data Sheet Former Clifton Precision Murphy, NC MW-64 to -`2 ) -- is ,.3 "Oa 15.00 (DTB - DTW))e * 0.163 = I � J _I J 1WV*3= ,&2 SS Submersible Pump / Dedicated Teflon Tubing Dedicated Teflon Bailer Site Specific VOC's (EPA 826013) Test America - Nashville CoC No: J1155NIO152 Time Started) I Purge Rate (gallons per minute) Actual Volume (gallons) pH SC (AS/cm) T (°C) Turbidity (NTU) Time V-103 0. 'so i , 0'0 1210-7 0,5J 3,?,0 -7.5o 2!i 6-7.�� -Z t4a O,So I bvvo -7+53 21i 0- p � 1411 0,s-0 5.00 -? ,�cl "LO-) 1-7, -7 C� Comments Pump control setting: 77 f�jZ CO2 (mg/L) = Z S H202 (mg/L) =''— Sam le time: Depth to water as measured in feet from top of casing 2 Total well depth measured in feet from top of casing Field Technician: • EM Services Environmental Monitoring Services, LLC Field Data Sheet Client Former Clifton Precision Site Murphy, NC Date i c7 21 I S Well ID Sample Method Direct grab Parameters Site Specific VOC's (EPA 826013) Laboratory/CoC No. Test America- Nashville CoC No: J1155N10152 Time Started: I I OLI pH SC ( S/cm) T (°C) Turbidity (NTU) Time ►13�t ) ,'3 1 103 11 O S 103 10� u �,�►� ib�► i�, O 1143 i I�r'o G Sc► 6-"3 II S.5 C_.-Yi Iou Field Technician: tg. Comments Purged for 30 minutes, then lowered flow rate and began recording parameters for stabilization. C)2 (mg/L) = V 5 H2O2 (mg/L) _ Client Site Sample Method Parameters Laboratory/CoC No EMServisces Environmental Monitoring Services, LLC Field Data Sheet Former Clifton Precision Murphy, NC Direct Grab l S' fe¢ C oC, VOC's (erA- SIZ60 Q Test America - Nashville CoC No: J1155NI0152 Turbidity Sample ID Date Time pH SC (µS/cm) TP (°C) (NTU) F-CMP-4 FO-21-15 ((Zg )_. (2 99 1P, 3 Field T 00 l 14 I I S Ln Qj 40 6c), Lon On -oN �j