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Home My WebLink AboutWQ0028693_Monitoring - 07-2022_20220831Monitoring Report Submittal Permit Number #* WQ0028693 Name of Facility:* Mountain Top Golf & Lake Club Month: * July Year: * 2022 Report Information Type* Upload Document* GW-59 Mountain Top (WQ0028693) 2.09MB GW59 with lab results 8-31- 22.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address:* kreese@rpbsystems.com Name of Submitter: * Kimber Reese Signature: Date of submittal: 8/31/2022 This will be filled in automatically Initial Review Reviewer: Gerald, Wanda Is the project number correct?* WQ0028693 Is the monitoring report accepted?* Yes NO Regional Office* Asheville Reviewer: _anonymous Review Date: 9/26/2022 G\V-69A COMPLIANC.T REPC)RTFORM Pernkit # WO O(D 2- 8 6) q 0 n bneir en? e each In w I ito in ep lod ulu �fth 6P P �-5 9 fin -Ins') I Enter date monitoring results were due. ( Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is " Yes ", contact the Regional Oflicefor-guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is 'WO" skip to section 6. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentrations) exceeding standards in the space provided below: 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is 'WO", skip to section 8. If the answer to question 5 is "YES"'list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years), VVI 1 1-4 PV1 6 Are the monitoring'wells listed in section 5 located at or beyond the review boundary? YES 110 If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is"NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "'YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Re Tonal Office within 90 days; an evaluation may be re wired to determine the impact the waste disposal sntem is having at the review and compliance boundaries, surrounding this facility, Failure to do so may subLect the permittee to a Notice of Violation, fines, andlor Penalties. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to, the address provided at the top of the current GW-59 form, I hereby acknowledge that the above information was evaluatecland the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. -31-2L Signature of Permittee (or Authorized Agent) Date ( Ovk -59A 12/8/2003 SUBMIT FORM ON YELLOW PAPER ONLY s DEPARTMENT OF €NVIR014M€NTAL OUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: IN ORMTION PROCESSINGUNIT COMPLIANCE REPORT FORM a • • 1617 MAILS€RVIC€ CENTER,RAI GH,NC276994617 FACILITY INFORMATION Please Print Cteady or Type PERMIT Number: Expiration Bate: 4l30t2025 Facility Name: Mountaintop Golf & Lake Club Non -Discharge WQ0028693 UIC Permit Name (if different): Mountaintop Community Association Inc NPDES Other Facility Address: P.G. Box 1460 TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Cashiers NC 28717 County Jackson K Spray Field ❑ Remediation: Contact Person: Bob Barr Telephone#: (828) 251-1900 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: MW-01 R No. of wells to be sampled: 3 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-01R Date sample collected: 7121/2022 FIELD ANALYSES: WAS Well Depth: 26.6 ft. Well Diameter: 2 in. pH 00400: 5.65 units Temp, 000lo 15.3 °C DRY at Depth to Water Level 82546: 12.65 ft. below measuring point Screened Interval: 15.6 ft. to 25.6 ft. Spec. Cond. 00094: 56.9 µMhos time of sampling, Measuring Point is 0 ft. above land surface Relative M.P. Elevation: ft. Odor doom: None check Volume of water pumped/bailed before sampling: gallons Appearance Turbid here: El Samples for metals were collected unfiltered: K YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed:8/312022 Laboratory Name: Pace Analytical Certification No. 40 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mgiL Nitrite (NO2) as N oo615 mg1L Pb - Lead o1o51 ug#L Coliform: MF Fecal 316% <1 /100ml- Nitrate (NO3) as N 010620 0.13 mg1L Zn - Zinc 01092 mgiL Coliform: M'F Total 31504 1100ml- Phosphorus: Total as P 00665 0.84 mgiL (Note. Use MPN method for high6y turbid samples) Orthophosphate 70507 mg#L Other (Specify Compounds and Concentration Units): issolved Sclids:Total 70300 54.0 mgiL Al - Aluminum ollo5 mgiL pH (Lab) 00403 units Ba - Barium 01007 ug#L TOG omm 2.7 mgiL Ca - Calcium oog18 mg/L Chloride 00940 4.0 mg/L Cd - Cadmium 01027 ug#L Arsenic 01002 ug/L Chromium: Total 01034 ug#L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg1L Hg - Mercury 71900 ug/L Late Report Attached? ❑ Yes (1) 9 No (0) Specific Conductance oo095 pMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia ooslo 0.14 mg#L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen. NH, as N. Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L method # TKN as N 00625 mg#L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mgiL VOC Removal% Robert P. Barr t Authorized Agent Permittee (o€ Authorized Agent) Name and Title - Please print or type Signature of Perm€ttee (or Authorized Agent# Tr 31_Z ( Date) GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DtV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: . # INFORMATION PROCESSINGUNIT COMPLIANCE REPORT FORM * � 1617MAIL SERVICE CENTER, RAL IGH, NG 27699-181 FACILITY INFORMATION Phase Print Clearly or Type PERMIT Number: Expiration Date: 4/3012025 Facility Name: Mountaintop Golf & Lake. Grub Non -Discharge WQ0028693 UIC Permit Name (if different) Mountaintop Community Association Inc NP'DES Other Facility Address: P.O. Box 1460 TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon [] Remediation: Infiltration Gallery Cashiers NC 23717 County Jackson K Spray Field ❑ Remediation: Contact Person: Bob Barr Telephone#: (828) 251-1900 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: MW-2 No. of wells to be sampled: 3 ❑ Water Source Heat Pump ❑ Other: (from Permit) -_---- SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 712112022 FIELD ANALYSES: WAS Well Depth: 42 ft. Well Diameter: 2 in. pH 00400: 5.82 units Temp. co01a: 13.9 °C DRY at Depth to Water Level s25as: 12.34 ft. below measuring point Screened Interval' 42 ft. to g p 32 ft. S. . ' 151.1 µMhos Spec. Cond00094 time of -_ -- sampling, Measuring Point is 0 ft, above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 813/2022 Laboratory Name: Pace Analytical Certification No, 40 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as IN oo615 mg/L Pb - Lead o1o51 ug/L Goliform: MF Fecal 31616 <1 /100ml- Nitrate (NO3) as N 00620 1.7 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P oo665 <0,50 mg/L (Note. use MPN method for highly turbid samples? Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 106 mg1L Al - Aluminum o11o5 - mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC ao6e0 1-2 mg1L Ca - Calcium oo916 mg/L Chloride 00940 2-7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 g/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 usg/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) A No (0) Specific Conductance 000ss µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.10 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen NH, as N, Ammonia Nrtrogen, Total) Mn - Manganese 01055 ug/L method TKN as N 00625 mg/L Ni - Nickel o1067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Permittee (or Authorized Agent) Name and Title- Please prim or type Signature of Permlttee (or Authorized Agent) (pate) G-59 Rev.06-07-2018 SUBMIT FORMON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clean Facility Name: Mountaintop Golf & Lake Club Permit Name (if different): Mountaintop Community Association Inc Facility Address: P.O. Box 1460 Cashiers NC Contact Person: Bob Barr Well Location/Site Name: MW-3 28717 or County Jackson Telephone#: (828) 251-1900 No, of wells to be sampled: 3 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1817 MAIL SERVICE CENTER, RAL IGH, NC 27999-1617 PERMIT Number: Expiration Date: 413012025 Non -Discharge WQ0028693 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon ❑ Remediation: infiltration Gallery Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-3 Date sample collected: 7121/2022 FIELD ANALYSES: WAS Well Depth: 16() ft. Well Diameter: 4 in. pH 00400: 5.99 units Temp. 00010 118.2 °C DRY at Depth to Water Level 82646: 13.77 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: 82,4 FrMhos time ofsampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: gallons Appearance Clear here: Samples for metals were collected unfiltered: ❑■ YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 813/2022 Laboratory Name: Pace Analytical Certification No, 43 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mgiL Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 e1 /100ml- Nitrate (NO.) as N 00520 0,40 mgiL Zn - Zinc o1o82 mg/L Coliform: MF Total 31504 /100mlL Phosphorus: Total as P 00665 <8.50 mg/L (Note: use.MPN method rorh,ghty turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 50.0 mg/L Al - Aluminum o11o5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC omso <1.8 mg/L Ca - Calcium 00916 mg/L Chloride 00040 3.2 g/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ugiL Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ugiL (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mgiL Hg - Mercury 71900 ug/L Lab Report Attached'? ❑ Yes (1) 1111111 No (0) pecific Conductance 00005 i:Mhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia ooslo <0.10 mg/L Mg - Magnesium 00927 mg/L method (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen. Total) Mn - Manganese olo55 ug/L , method # TKIN as N 00525 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mg/L Effluent Total VOCs: mgiL VOC Removal% Robert P. Barr /Authorized Agent A Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Gate) GVV-59 Rev.06-07-2018 aceAnalytical wurmpacallabs.cmim Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Mountain Top MW 7/21 Pace Project No.: 92616213 Sample: MW-01R Lab ID: 92616213001 Collected: 07/21/22 13:00 Received: 07/21/22 16:22 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by Pace 1 08/02/22 16:48 Collected By M.Swann 1 08/02/22 16:48 Collected Date 7/21/22 1 08/02/22 16:48 Collected Time 13:00 1 08/02/22 16:48 pH 5.65 Std. Units 1 08/02/22 16:48 Temperature 15.3 deg C 1 08/02/22 16:48 Static Water Level 12.65 feet 1 08/02/22 16:48 Specific Conductance 59.9 umhos/cm 1 08/02/22 16:48 Oxygen, Dissolved 4.88 mg/L 1 08/02/22 16:48 7782-44-7 Total Well Depth 25.6 feet 1 08/02/22 16:48 REDOX -161.6 my 1 08/02/22 16:48 Turbidity 496 NTU 1 08/02/22 16:48 Odor None 1 08/02/22 16:48 Appearance Turbid 1 08/02/22 16:48 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Asheville Total Dissolved Solids 54.0 mg/L 25.0 1 07/26/22 10:53 MBIO 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Asheville Fecal Coliforms ND CFU/100 mL 2.0 2 07/21/22 17:02 07/22/22 15:50 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Ammonia 0.14 mg/L 0.10 1 08/03/22 11:23 7664-41-7 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Nitrate ND mg/L 0.040 1 07/22/22 01:33 14797-55-8 Nitrogen, Nitrite 0.096 mg/L 0.040 1 07/22/22 01:33 14797-65-0 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus 0.84 mg/L 0.050 1 08/01/22 17:51 08/01/22 20:05 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville Chloride 4.0 mg/L 1.0 1 07/29/2213:53 16887-00-6 5310E TOC Analytical Method: SM 531OB-2014 Pace Analytical Services - Asheville Total Organic Carbon 2.7 mg/L 1.0 1 07/26/22 15:55 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:13 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 18 aceAnalytical wurmpacallabs.cmim Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Mountain Top MW 7/21 Pace Project No.: 92616213 Sample: MW-2 Lab ID: 92616213002 Collected: 07/21/22 12:35 Received: 07/21/22 16:22 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by Pace 1 08/02/22 16:49 Collected By M.Swann 1 08/02/22 16:49 Collected Date 7/21/22 1 08/02/22 16:49 Collected Time 12:35 1 08/02/22 16:49 pH 5.82 Std. Units 1 08/02/22 16:49 Temperature 13.9 deg C 1 08/02/22 16:49 Static Water Level 12.34 feet 1 08/02/22 16:49 Specific Conductance 151.1 umhos/cm 1 08/02/22 16:49 Oxygen, Dissolved 5.11 mg/L 1 08/02/22 16:49 7782-44-7 Total Well Depth 160.0 feet 1 08/02/22 16:49 REDOX -172.3 my 1 08/02/22 16:49 Turbidity 0.52 NTU 1 08/02/22 16:49 Odor None 1 08/02/22 16:49 Appearance Clear 1 08/02/22 16:49 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Asheville Total Dissolved Solids 106 mg/L 25.0 1 07/26/22 10:53 MBIO 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Asheville Fecal Coliforms ND CFU/100 mL 1.0 1 07/21/22 17:02 07/22/22 15:50 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Ammonia ND mg/L 0.10 1 08/03/22 11:24 7664-41-7 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Nitrate 1.7 mg/L 0.040 1 07/22/22 01:31 14797-55-8 Nitrogen, Nitrite ND mg/L 0.040 1 07/22/22 01:31 14797-65-0 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus ND mg/L 0.050 1 08/01/22 17:51 08/01/22 20:08 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville Chloride 2.7 mg/L 1.0 1 07/29/2213:56 16887-00-6 5310E TOC Analytical Method: SM 531OB-2014 Pace Analytical Services - Asheville Total Organic Carbon 1.2 mg/L 1.0 1 07/26/22 16:13 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:13 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 aceAnalytical wurmpacallabs.cmim Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Mountain Top MW 7/21 Pace Project No.: 92616213 Sample: MW-3 Lab ID: 92616213003 Collected: 07/21/22 11:35 Received: 07/21/22 16:22 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by Pace 1 08/02/22 16:51 Collected By M.Swann 1 08/02/22 16:51 Collected Date 7/21/22 1 08/02/22 16:51 Collected Time 11:35 1 08/02/22 16:51 pH 5.99 Std. Units 1 08/02/22 16:51 Temperature 18.2 deg C 1 08/02/22 16:51 Static Water Level 13.77 feet 1 08/02/22 16:51 Specific Conductance 82.4 umhos/cm 1 08/02/22 16:51 Oxygen, Dissolved 5.84 mg/L 1 08/02/22 16:51 7782-44-7 Total Well Depth 33.77 feet 1 08/02/22 16:51 REDOX -128.6 my 1 08/02/22 16:51 Turbidity 4.76 NTU 1 08/02/22 16:51 Odor None 1 08/02/22 16:51 Appearance Clear 1 08/02/22 16:51 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Asheville Total Dissolved Solids 50.0 mg/L 25.0 1 07/26/22 10:53 MBIO 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Asheville Fecal Coliforms ND CFU/100 mL 1.0 1 07/21/22 17:02 07/22/22 15:50 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Ammonia ND mg/L 0.10 1 08/03/22 11:25 7664-41-7 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Nitrate 0.40 mg/L 0.040 1 07/22/22 01:27 14797-55-8 Nitrogen, Nitrite ND mg/L 0.040 1 07/22/22 01:27 14797-65-0 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus ND mg/L 0.050 1 08/01/22 17:51 08/01/22 20:08 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville Chloride 3.2 mg/L 1.0 1 07/29/2213:56 16887-00-6 5310E TOC Analytical Method: SM 531OB-2014 Pace Analytical Services - Asheville Total Organic Carbon ND mg/L 1.0 1 07/26/22 16:32 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:13 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 I eAnalytical www.pacallabsxom Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALIFIERS Project: Mountain Top MW 7/21 Pace Project No.: 92616213 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2022 04:13 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 �a7 ce CHAIN -OF -CUSTODY / Analytical Request Document al The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Submitting a sample via this chain of custody constitutes acknowledgment and acceptance of the Pace Terms and Conditions found at https://info.pac-elabs.com/hubfs/pas-standard-terms.pdf. Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: LPage: 1 Of _FePOrT Company: RPB Systems Inc TO: Robert Barr Attention, Address: P 0. Box 1325 Copy To: Company Name. Asheville, NC 28a02 Address, RMulatory Alilena Email: rbarr@rpbsystems.com Purchase Order # Pace Quote Phone: (828)251-1900 Fax Project Name: Mountain Top MWs Pace Project Manager: lorri patton@pacelabs.com, State I Location ,Requested Due Date: Project Pace Profile #: mws Requested Analysis Filtered I YtAt MATRIX CODE COLLECTED z Preservatives D'1-al W1, 3VV W.!. 0 etc Water P SAMPLE ID SLVJ 6 U Ck OL START END 12 One Character per box. W'P. WP w w -6 L) Sample Ids must be unique T TS K LH uf 0 0 UJ < < —DATE TIME < 0 M C) Z ZE < 0 0 Er (3 I mw-12 I �L__ WT X X X X X 06 2 mw-11r Wr 'r-7- X X X X 3 MW4 WT -41 --'LL X _x X X X 4 7 8 10 11 12 ADDITIONAL COMMENTS RELINQUISHED By tAFFILUli9t id DATE -TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITiONS 131, AVI- 'A :21A I SAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: (L uJ E SIGNATURE of SAMPLER: DATE Signed: L) 0 Cn I eAnalytical wurmpacallaba.caim Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 August 03, 2022 Kimber Reese RPB Systems Inc. P.O. Box 1325 Asheville, NC 28802 RE: Project: Mountain Top MW 7/21 Pace Project No.: 92616213 Dear Kimber Reese: Enclosed are the analytical results for sample(s) received by the laboratory on July 21, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton lorri.patton@pacelabs.com 1(828)254-7176 Project Manager Enclosures cc: Mr. Robert Barr, RPB Systems Inc. Ms. Liz Barr, RPB Systems Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18