WQ0004797_Monitoring (Report)_20091214

Y -
1
r .r ..
r 1
12-14-09
Division of Water Quality
1617 Mail Service Center
Attn: Information Processing Unit
Raleigh, NC 27699-1617
RE: Permit Number WQ0004797
GW-59 & GW-59A Reports
U`uL�C2O V IF ID
JAN 0 5 2C o3
Asheville regional Of -ice
9'Aqui. er protection
Attached please find 2 copies (each) of Clement Pappas GW-59 & GW-59A Compliance
Report Forms, for the month of November 2009.
Thank You,
Blake Kehoe
cc: Dale Wolfe
pEC � y 2009
Psroces9 A
��form
125 Industrial Park Rd Hendersonville, NC 28792
828-693-0711

GW-59A COMPLIANCE REPORT FORM
Permit # WQ0004797
(Submit one each monitoring period with GW-59 forms.)
1
Enter date monitoring results were due. (12/31/2009 ) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
G)
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
•
explain the problems encountered in obtaining the required information.
I
3
Are any of the monitor wells in'need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Officefor guidance.
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below.•
Total Organic Carbon Qlmit = 10 mg/L) - MW-2R = 13.5 mg/L, MW4 = 31.0 mg/L. MW-8 = 10.8 mgfL
Fecal Coliform (limit =11100 mL) - MW-5 = 2.01100 mL, MW-6 = 30/100 ml-, MW-7 = 2.01100 mL, MW-e = 501100 L.
Tetrachloroethem(limit =0.7 pg/L)- MW-5=872 pg/L
TntUmoethene (limit = 0.7 pg/L) - MW-5 =106 pg/L
cis-1,2-dichlomethene (limit = 0.7 pg/L) - MW-5 = 125 pg/L
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituents) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
Total Organic Carbon (limit = 10 mg/L) - 5128/09: MW-2R = 14A mg/L. MW-5 = 16.1 mg/L. MW-7 = 23A mgfL,
11118108: MW4 = 20.5 mg/L, MW-5 - 25.9 mg/L, MW-e - 14.4 mg/L
5/27/08: MW-2R = 102 mgfL, MW-6 = 10.9 mg/L. MW-8 =12.4 gIL;
11/13/07: MW416.7 mg/l
Fecal Coli(orm (limit = 11100 ml-) - 528169: MW-5 = 4.01100 mI- MW-6 = 2761100 mt_ MW-8 = 240/100 mL1 11118/08: MW-6 = 2.2/10D mL; 11/13107, MW-6 = 3.61100 L.
Tebachtorcethene (limit= 0.7 pg/L) - 11/18108: MW-5 = 2,680 pg/L, M W-6 = 3.0 pg/L, MW-7 = 0.79 pg/L: 11/13/07: MW-5 =1,150 pg/L
'
Tnctdoroethene (8mit = 0.7 pg/L) - 11118/08: MW-5 = 534 pg/L, 11113107: MW-5 = 217 pg/L
cis-1,2-dichloroethene (limit = 0.7 pg/L) - 11118108: MW-5 = 293 pgn- 11113107: MW-5 = 209 pg/L
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
if the answer is "YES'", a groundwater quality problem maybe occurring, CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE If the answer is "NO", monitoring, wells maybe improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by th Nihibn involving this
YES
NO
groundwater quality problem? (', . L%P
If the answer to question 7 is "YES", describe those actions in the spac pro e ow
if the answer to question 7 is "NO", contact the Re Tonal Office with a s tt. airon ma be
required to determine the impact the waste disposal system is having at the and compliance
boundaries surroundin this facili . Failure to do so ma sub •ect the a to a Notice of Violation
fines, and/or penalties.
Total Organic Carbon, VOC, and SVOC analyses were completed for all samples during the May 2007 groundwater sampling event. The TOC is
not attributable to VOCs or SVOCs. Possibly natural occurring. The November 2009 groundwater samples were analyzed according to an
attemative fecal coliforrn method. Fecal colifonn was still detected in the above monitoring wells but contained concentrations below the May 2009
results. Fecal colifonn results will be reviewed following the May 2010 monitoring event to verify that they continue to decrease.
g
The person completing this portion (GW--59A) of the monitoring report should sign below and submit this
form with G W-59 forms for required wells to the address provided at the top of the current G W-59 form.
1 hereby acknowledge thatythe above mformatton was evaluated and the rnformat�on submlttec]in thts Y:
report (Colrnpir ce Report.GW-59A) is true and completeao the best of (my knowledge' ,
_
tuna We f Permittee (or Authorized Agent) Date
GW-59A 12/8/2003

SUBMIT FORM ON YELLOW PAPER ONLY
QUALITY MONITORING:
b i�YA§ffl,�, N ,gg,GROUNDWATER
""vi 0
COMPLIANCE REPORT FORM
sc e, z;'
FACILITY INFORMATION Please Pnnt Clearly or Type
PERMIT Number: Expiration Date: 11/30/2011
Facility Name: Clement Pappas
Non -Discharge WQ0004797 UIC
Permit Name (if different):
NPDES Other
Facility Address: 125 Industrial Park
TYPE OF PERMITTED OPERATION BEING MONITORED
Mountain Home, (street) NC 28758
County Henderson
❑ Lagoon ❑ Remediation: Infiltration Gallery
(city) (state) (zip)
x❑ Spray Field ❑ Remediation:
Contact Person: Mr. Blake Kehoe
Telephonet [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Irrigation Area
No. -of wells to be sampled: 6
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW 2R
Date sample collected: 11/5/2009
FIELD ANALYSES:
WAS
Well Depth: 14.90 ft. relative to top of casing
Well Diameter: 2 in.
pH 5.62 uni Temp. 16.66 eC
DRY at
Depth to Water Level: 6.72 ft. below measuring point
Screened Interval: 6 ft. to
11
ft." Spec. Gawd 67 µMhos
time of
sampling,
Measuring Point is 3.77 ft. above land surface
Relative M.P. Elevation: 2063.0 ft.
Odor None
check
Volume of water pumped/bailed before sampling: 1.50 gallons "'screened Interval is relative to land surface Appearance
here: ❑
Samples for metals were collected unfiltered: DYES ❑ NO
and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: varies; see analytical report
Laboratory Name: Pace Analytical Services, Inc. Certification -No. 37712
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD mg/I
Nitrite (NO2) as N
mg/1
Pb - Lead mg/l
Coliform: MF Fecal < 2.0 /100ml
Nitrate (NO3) as N 0.31
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100mi Phosphorus: Total as P
mg/l
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 80.0 mg/l
Al - Aluminum
mg/l
pH (when analyzed) __ �U(lits
Ba - Barium
mg/I
TOC � 13.5 n
_
Ca - Calcium
mg/I
P-
Chloride _ /l
Cd - Cadmium
mg/I
Arsenic mgms
Grease and Oils pE`, d
Chromium: Total
Cu - Copper
mg/I
mg1l
ORGANICS: (by GC, GC/MS, HPLC)
g/l %OtA
�G"
Phenol mg& t�906t
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate I ��`�A`gh
Hg - Mercury
mg/I
Report Attached? ❑, Yes (1) ❑ No (0)
Specific Conductance �n ° µMhos
K - Potassium
mg/I
VOCs method # 6200B
Total Ammonia < 0.10 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total)
Mn -Manganese
mg/l
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%o
-tf_C)q
iittee (or Authorized Agent) Name and Title - Please print or type Signature`bT PErmi fee (oleAuthorized Agent)
GW-59 Rev.1/2007
`y` 1�

SUBMIT FORM ON YELLQVL PAPER ONLY
ROUNDWATER QUALITY MONITORING: IuiiiN nAWE
OMPLIANCE REPORT FORM s nc .EA. ra ,� 699.�y M001m;
\CILITY INFORMATION Please PrintCteadyorType PERMIT Number: Expiration Date: 11/30/2011
tcility Name: Clement Pappas Non -Discharge .WQ0004797 UIC
armit Name (if different): NPDES Other
icility Address: 125 Industrial Park TYPE OF PERMITTED OPERATION BEING MONITORED
Mountain Home (street) NC 28758 County Henderson ❑ Lagoon ❑ Remediation: Infiltration Gallery
(City) (state) tzp> M Spray Field . ❑ Remediation:
)ntact Person: Mr. Blake Kehoe Telephonem [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
ell Location/Site Name: Irrigation Area No, of wells to be sampled: 6 ❑ Water Source Heat Pump ❑ Other.
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-4
Date sample collected: 11/5/2009
FIELD ANALYSI=SS:
WAS
Well Depth: 18.60 ft. relative to top of casing
Well Diameter: 2 in.
pH 5,8duni s Temp. 16.37 eC
DRY at
Depth to Water Level: .8.53 ft. below measuring point
Screened Interval: 8 ft.* to 16.1 V
Spec. Con120 µMhos
d.
time
sampling,
Measuring Point is 2.43 ft. above land surface
Relative M.P. Elevation: 2064.6 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
5.25gallons *screened Interval Is relative to land surface
Appearance
here:
Samples for metals were collected unfiltered: OYES
❑ NO and field acidified. ❑ YES ❑ NO
sample analyzed: varies; see analytical report Laboratory Name: Pace Analytical Services, Inc. Certification No. 37712
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I
Coliform: MF Fecal < 2.0 2100ml Nitrate (NO3) as N < 0.10 mg/I Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
120 mg/I
Al - Aluminum
mg/I
pH (when analyzed)
Ba - Barium
mg/I
TOC _
_units
31.0m /
Ca - Calcium
mg/I
Chloride
13.6 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
30.7 mg/I
Hg - Mercury
mg/I
Report Attached? M Yes (1) ❑ No (0)
Specific Conductance
µMhos
K- Potassium
mg/I
VOCs method# 6200B
Total Ammonia
< 0.10 mg/I
Mg - Magnesium
mg/1
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/1
method #
TKN as N
mg/I
Ni - Nickel
mg/1
method #
GW-59 Rev.112007

SUBMIT FORM ON YELLOW PAPER ONLY
UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
Name: Clement Pappas
Name (if different):
Address: 125 Industrial Park
writain Home' (Street) NC 28758 County Henderson
act Person; Mr. Blake Kehoe Telephonem [phone]
Location/Site Name: Irrigation Area No. of wells to be sampled: 6
Number: Expiration Date:
;harge WQ0004797 UIC
Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
El Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
:LL ID NUMBER (from Permit): MW 5
Date sample collected: 11/5/2009
FIELD ANALYSES:
WAS
II Depth: 18.60 ft. relative to top of casing
Well Diameter: • 2 in.
pH 5.55 units Temp. 16.40 eC
DRY at
3th to Water Level: 8.63 ft. below measuring point
Screened Interval: 9 ft.* to 19 ft.*
Spec. Cond. 115 µMhos
time of
sampling,check
asuring Point is 3.00 ft, above land surface
Relative M.P. Elevation: 2086.4 ft:
Odor None
ume of water pumped/bailed before sampling:
5.25gallons *screened interval based on well construction record
Appearance
here:
ni3les for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
❑
sample analyzed: varies; see analytical report
Laboratory Name: Pace Analytical Services, Inc.
Certification No: 37712
%METERS NOTE: Values should reflect dissolved and
colloidal concentrations.
COD �, mg/'
Nitrite (NO2) as N
mg/1
Pb - Lead mg/I
Coliform: MF Fecal 2.0 j_j 00ml
Nitrate (NO3) as N
0.15 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note; Use MPN method for highly turbid samples)
Ortho h h t
/1
Oth S • C d C U
Dissolved Solids: Total
112 mg/I
pH (when analyzed)
units
TOC
4.7 mg/I
Chloride
39.1 mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
< 5.0 mg/I
Specific Conductance
µMhos
Total Ammonia
< 0.10 mg/I
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
TKN as N mg/I
p osp a e
mg
All -Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K- Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Ni - Nickel
mg/I
es ( peclfy ompoun s and oncentration nits).
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? E Yes (1) ❑ No (0)
VOCs , method # 6200B
, method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
X
ittee (or A4thorized Agent) Name and Title - Please print or
GW-59 Rev.112007
/02" 1 (f- -6
(Date)

JUbMI I 'I-UKM UN Yr_L i UVV t'HrtK UNLY
UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
TY INFORMATION. Please Print Clearly or Type
Name: Clement Pappas
Name (if different):
Address: 125 Industrial Park
Iuntain Home." (street) NC 28758 County Henderson
act Person: Mr. Blake Kehoe Telephone#: [phone]
Location/Site Name: Irrigation Area No. of wells to be sampled: 6
Number: Expiration Date:
;harge WQ0004797 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
rx`l Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
L ID NUMBER (from Permit): MW-6 Date sample collected: 11/5/2009
Depth: 11.54 ft. relative to top of casing Well Diameter. •2 in.
h to Water Level: 5.74 ft, below measuring point Screened Interval: 5 ft." to 10 V
wring Point is 3.00 ft. above land surface Relative M.P. Elevation: 2061.9 ft.
Tie of water pumped/bailed before sampling: 3.0 gallons "screened Interval based on well construction record
niles for metals were collected unfiltered: [DYES ❑ NO and field acidified: ❑ YES ❑ NO
FIELD �ANALYSES:
PH ( 5.30 unit
Spec. Coonnd.
Odor None
Appearance
WELL
Temp. 15.37 oC IDRY at
41 µMhos Itime of
sample analyzed: varies: see analytical report
Laboratory Name: Pace Analytical Services, Inc.
Certification No. 37712
%METERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD — mg/1
Nitrite (NO2) as N
mg/I
Pb - Lead mg/l
Coliform: MF Fecal 30 %)I00mi
Nitrate (NO3) as N
0.10 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/l
(Note; use MPN method for highly turbid samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
52.6 mg/I
PH (when analyzed)
units
TOC
6.4 mg/I
Chloride
< 5•0 mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
9.3 mg/I
Specific Conductance
µMhos
Total Ammonia
< 0.10 mg/I
(Ammonia Nitrogen; N1,13as N; Ammonia Nitrogen, Total)
TKN as N mg/1
GW-59 Rev.1/2007
Al Aluminum
mg/I
Ba - Barium
mg/l
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe -Iron
mg/I
Hg - Mercury
mg/1
K- Potassium
mg/1
Mg - Magnesium
mg/I
Mn - Manganese
mg/1
Ni - Nickel
mg/I
ORGANICS: (by GC, GC/MS HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? El Yes (1) ❑ No (0)
VOCs method # 6200B
method #
method #
method #

SUBMI i FUKM UN Y It I (nnr I'ANtK UNLY
(GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
TY INFORMATION Niease Ynnr weary or type
Name: Clement Pappas
Name (if different):
Address: 125 Industrial Park
wntain Home' (Stree`) NC 28758 County Henderson
act Person: Mr. Blake Kehoe Telephone#: [phone]
Location/Site Name: Irrigation Area No. of wells to be sampled: 6
IRMIT Number: Expiration Date: 11/30/2011
n-Discharge WQ0004797 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
0 Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other.
If WELL
.L ID NUMBER (from Permit): MW-7
Date sample collected: 11/5/2009
FIELD ANALYSES:
WAS
Depth: 16.72 ft. relative to top of casing
Well Diameter: 2 in.
pH 5.39 units
Temp. 15.82 eC
DRY at
th to Water Level: 9:89 ft. below measuring point
Screened Interval: 5 V to 15 ft.*
Spec. Co
78 µMhos
f.
time sampling,
suring Point is 3.00 ft. above land surface
Relative M.P. Elevation: 2062.7 ft.
Odor None
check
me of water pumped/balled before sampling: 3.5 gallons "screened Interval based on well construction record
Appearance
here: ❑
t les for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
;ORATORY INFORMATION
l sample analyzed: varies; see analytical report
Laboratory Name: Pace Analytical Services, Inc.
Certification No. 37712
;AMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD g/I
Nitrite (NO2) as N mg/1
Pb - Lead
mg/I
Coliform: MF Fecal 2.0 /10 r ml
Nitrate (NO3) as N 2.3 mg/I
Zn - Zinc
mg/1
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
70.0 mg/I
Al - Aluminum
mg/I
pH (when analyzed)
units
Ba - Barium
mg/I
TOC
5.3 mg/l
Ca - Calcium
mgA
Chloride
10.7 mg/I
Cd - Cadmium
mgA
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/l
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
11.2 mg/I
Hg - Mercury
mg/l
Report Attached? x❑ Yes (1) ❑ No (0)
Specific Conductance
µMhos
K - Potassium
mg/1
VOCs method # 6200B
Total Ammonia
< 0.10 mg/l
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen,
Total)
Mn - Manganese'
mg/I
method #
TKN as N
mg/l
N1- Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
/P r 14-6 1
ittee (or Authorized Agent) Name and Tftle -Please print or type Signature of
GW-59 Rev.112007 -

SUBMIT FORM ON YELLOW PAPER ONLY
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
L nn 1 r IkMr ltg • r1nu Please PAflt CleaHy or
Facility Name: Clement Pappas
Permit Name (if different):
Facility Address: 125 Industrial Park
Mountain Home" (Street) NC 28758 County Henderson
act Person: Mr. Blake Kehoe Telephone#: [phone]
Location/Site Name: Irrigation Area No. of wells to be sampled: 6
RMIT Number: Expiration Date: 11/30/2011
n-Discharge WQ0004797 UIC
'DES Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
0 Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
L ID NUMBER (from Permit): MW-8
Date sample collected: 11/5/2009
FIELD ANALYSE
WAS
Depth: 13.90 ft. relative to top of casing
Well Diameter: 2 in.
pH 5.97 uni
Temp. 15.82 eC
DRY at
:h to Water Level: 9.22 ft, below measuring point
Screened Interval: 3 ft.* to 13 ft *
—
Spec.
124 µMhos
time of
sampling,
suring Point is 3.00 ft. above land surface
Relative M.P. Elevation: 2061.4 ft.
Odor None
check
me of water pumped/bailed before sampling: 2.5
gallons *screened interval based on well construction record
Appearance
here: ❑
pies for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
ORATORY INFORMATION
sample analyzed: • varies; see analytical report
LaboratoryName: Pace Analytical Services, Inc.
Certification No. 37712
AMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/1—
Nitrite (NO2) as N mg/I
Pb - Lead
mg/I
Coliform: MF Fecal ,'� 50 /100m!)
Nitrate (NO3) as N 0.54 mg/I
Zn - Zinc
mg/I
Coliform: MF Total
I ! 0ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
114 mg/I
All - Aluminum
mg/I
,pH (when analyzed)
_ — ---=unit
Ba - Barium
mg/l
TOC
'-,10.8 mg/1
Ca - Calcium
mg/I
Chloride
15.4 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/1
Grease and Oils
mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
18.4 mg/I
Hg - Mercury
mg/I
Report Attached? Yes (1) ❑ No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOCs method # 6200B
Total Ammonia
< 0.10 mg/l
Mg - Magnesium
mg/l
method #
(Ammonia Nitrogen: NH3as N; Ammonia Nitrogen, Total)
-Mn - Manganese
mg/1
method #
TKN as N
mg/l
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.1/2007

�M1
N G 1 N E E R I N G $C H Y c> R O G E O L. O G.Y
2 3 1 H A Y W O O O STREET , A S H E V 1 L L E. N C 2 a B O 1
WWW.q LTA MO NTENV•RONM ENTA L.cOM
Well SaulDling Log
o a
FACILITY NAME: Clement Pappas DATE:
LOCATION: Henderson County, North Carolina SAMPLING TIME: j1 sa
SAMPLING PERSONNEL: E. Yurkovich WEATHER: C1aQW, Su^nry
WELL NUMBER: N w- :z WELL DEPTH IN FEET (WD): ) • YD START TIME: 3
WELL DIAMETER: 2" WATER LEVEL IN FEET (WL):- tQ ��-
TYPE OF CASING: ? Vc— LENGTH OF_ WATER COLUMN: FEET
MEASURING POINT: , dG (WD) - (WL) = (LWC)
FLUSH MOUNT C�K-UP ONE CASING VOLUME: 1, 3q GALLONS
COMMENTS: nc� (ttJ�© (LWC) x (WCV)
THREE CASING VOLUMES: q` GALLONS
ACTUAL VOLUME PURGED: % 5 b GALLONS
�IPI'=�0.04IGal&t" = 0.17 Gal&t�T'=0.38Gal/Ft
WELL CASING VOLUMES (WCV)
4" = 0.66 Gal/Ft 6" =1.5 GaVFt 8" = 2.6 Gal/Ft 12" = 5.8 Gal/Ft
PURGE METHOD: f4E - . BAILER-TEFLON DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER:
SAMPLE METHOD: VjZ0I!ZDRP.
BAILER-TEFLON DEDICATED
PUMP WHALE PUMP GRUNDFOS OTHER:
READING
TIME
GALLONS
PURGED
TEMP
(CO)
SPECIFIC
COND.
(µs)
DISSOLVED
OXYGEN
(mg/L)
pH
(S.U.)
OXIDATION
REDUCTION
POTENTIAL
mV
TURBIDITY
(NTU)
COMMENTS
S*D
slj:
` S. —
2
+ ��
i , �
��•tQ�
c � �
c� . a �
, Ce a-
-71100
3
4
5
6
8
9
SAMPLING
CONTAINER
NUMBER OF CONTAINERS
REQUESTED ANALYSIS
40 ml GLASS
5.
TOC, VOC's by 6200B
125 ml PLASTIC
3
Nitrate, Ammonia
250 ml PLASTIC
1
Fecal Coliform
500 ml PLASTIC
1
Chloride, Sulfate, TDS
PROTECTIVE CASING:_ d�- PAD: (AL
LOCK: 1� VEGETATION: CIL ACCESS: Gt9�
Sampling Personnel Signature:
Date:
Notes: µS = micro-Siemen
C° = degrees Celsius
mg/L = milligrams per liter
mV = millivolt
S.U. = Standard Units
NTU = nephelometric turbidity units
P:1TemplateslGW Drilling Forms1We11 Sampling Log.xls Page 1 of 1

Z 3 1 H A Y W O O O STREET, A S H E V I L LE. N C 2 8 8 0 7
FAG
W W W.A LTA MONTEN V I RONM ENTA L.CO M
Well SamDling Log
FACILITY NAME: Clement Pappas
DATE: 0q
LOCATION: Henderson County, North Carolina SAMPLING TIME: 19a S
SAMPLING PERSONNEL: E. Yurkovich
WEATHER: (:4ea xl Self,
. <�,a [
WELL NUMBER:
WELL DEPTH IN FEET (WD):
START TIME-
WELL DIAMETER: ii
WATER LEVEL IN FEET (WL):�
TYPE OF CASING: . we
LENGTH OF WATER COLUMN: i0 e 04
FEET
MEASURING POINT:
(WD) - (WL) _ (LWC)
FLUSH MOUNT IC -UP
ONE CASING VOLUME:_ t + GALLONS
COMMENTS:
(LWC) x (WCV)
THREE CASING VOLUMES: .� , 1 9
5,19
GALLONS
ACTUAL VOLUME PURGED: Jam^
GALLONS
WELL CASING VOLUMES (WCV)
1" = 0.041.Ga1/Ft 2" = 0.17 Gal/Ft
3" = 0.38 Gal/Ft 4" = 0.66 Gal/Ft 6" =1.5 Gal/Ft 8" = 2.6
Gal/Ft 1211= 5.8 Gal/Ft
PURGE METHOD: -
SP AILER-TEFLON DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER:
SAMPLE METHOD:
. BAILER-TEFLON DEDICATED
PUMP WHALE PUMP GRUNDFOS OTHER:
READING
TIME
GALLONS
TEMP
SPECIFIC
DISSOLVED
pH
OXIDATION
TURBIDITY
COMMENTS
PURGED
(CO)
COND.
OXYGEN
(S.U.)
REDUCTION
(NTU)
(µS)
(mg/L)
POTENTIAL
mV
3
-SI5'o
JU71,5
fIa-
.-4(
�
_<)
4
Ya113
1,
4/(r,4
►v.�
5
6
7
8
9
SAMPLING CONTAINER
NUMBER OF. CONTAINERS
REQUESTED ANALYSIS
0 ml GLASS
5
TOC, VOC's by 6200B
125 ml PLASTIC
3
Nitrate, Ammonia
250 ml PLASTIC
I
Fecal Coliform
500 ml PLASTIC
1 ICWoride,
Sulfate, TDS
PROTECTIVE CASING: PAD: 01C
LOCK: New VEGETATION: of ACCESS: (50e> 3
Sampling Personnel Signature:
Date: i 1/ '541
Notes:
µS =micro-Siemen
C" = degrees Celsius
mg/L = milligrams per liter
mV = millivolt
S.U. = Standard Units
NTU = nephelometric turbidity units
P:\Templates\GW Drilling Forms\Well Sampling Log.xls Page 1 of 1

t N G I N E E R I N G $C FI Y m R O G E O L O G Y '
2 3 1 H A Y W 0 0 0 S T R E E T. A S H E V i L L E. N G 2 6 B 0 1
T E L. B 2 8. 2 6 I. as 50 F A c. 8 2 6. 2 B 1. 3 3 5 1
WW W.ALTAMONTENVIRONM EN TA L.coM
Well Sampling Log
FACILITY NAME: Clement Pappas
DATE: 11 1,6/oq
LOCATION: Henderson County, North Carolina
SAMPLING TIME:
SAMPLING PERSONNEL: E. Yurkovich
WEATHER: Cleof, 3Lmn
Cott "
WELL NUMBER: M W-5
WELL DEPTH IN FEET (WD):
START TIME: 16
WELL DIAMETER: i�
WATER LEVEL IN FEET (WL): �a .
TYPE OF CASING:
LENGTH OF WATER COLUMN: CP17+
FEET
MEASURING POINT: 1 be
(WD) - (WL) _ (LWC)
FLUSH MOUNT / ICI -
ONE CASING VOLUME: (91
GALLONS
COMMENTS:
(LWC) x (WCV)
THREE CASING VOLUMES: •®c�
GALLONS
ACTUAL VOLUME PURGED: . a
GALLONS
WELL CASING VOLUMES (WCV)
1" = 0.041 Gal/Ft 2" = 0.17 Gal/Ft
3" = 0.38 Gal/Ft 4" = 0.66 Gal/Ft 6" =1.5 Gal/Ft 8" = 2.6
Gal/Ft 12" = 5.8 GaM
PURGE METHOD: B - IS BAILER-TEFLON DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER:
SAMPLE METHOD:
BAILER-TEFLON DEDICATED
PUMP WHALE PUMP GRUNDFOS OTHER:
READING
TIME
GALLONS
TEMP
SPECIFIC
DISSOLVED
pH
OXIDATION
TURBIDITY
COMMENTS
PURGED
(CO)
COND.
OXYGEN
(S.U.)
REDUCTION
(NTU)
(µS)
(mg/L)
POTENTIAL
mV
1
11
IVA-aR
-F
cDA
S•��
0:74•C0
So i
2
y��
i.75'
1(QI`3(p
PIT
SS?
6.63
ciq�13
-127.6
3
i i o
& 56
qa•
3a-y,4o
02i41
AG40
H
S s 1-+
3,-z`.1-q
151? 7
5
6
7
8
9
SAMPLING CONTAINER
NUMBER OF CONTAINERS
REQUESTED ANALYSIS
40 ml GLASS
5
TOC, VOC's by 6200B
125 ml PLASTIC
3
Nitrate, Ammonia
250 ml PLASTIC
1 IFecal
Coliform
500 ml PLASTIC
1 I
Chloride, Sulfate, TDS
PROTECTIVE CASING: OL PAD: 43f`
LOCK: eli
VEGETATION: ©�— ACCESS: Cx�C
Sampling Personnel Signature:
Date: t l/,qo
Notes: µS = micro-Siemen
C° = degrees Celsius
mg/L = milligrams per liter
mV = millivolt
S.U. = Standard Units
NTU = nephelometric turbidity units
P.\Templates\GW Drilling Forms\Well Sampling Log.xls Page 1 of 1

ir!
E N G I N E E R 1 N G $c H Y M R O G M O L. O G Y I
2 3 1 H A Y W O O O STREET , A S H E V I L L E. NC 2 6 6 O 1
WWW.ALTAMONTENYIRONMENTAt..cOM
Well Sampling Log
FACILITY NAME: Clement Pappas DATE: 0 5-&q
LOCATION: Henderson County, North Carolina SAMPLING TIME: (�
SAMPLING PERSONNEL: E. Yurkovich WEATHER: deka r a,,Y)
WELL NUMBER: /'\�� (f!
WELLDIAMETER:
TYPE OF CASING:
MEASURING POINT. OG
FLUSH MOUNT -
COMMENTS:
WELL DEPTH IN FEET (WD): I - S q START TIME: ITs i
WATER LEVEL IN FEET (WL): 5 •'-T4
LENGTH OF WATER COLUMN: 6 26 FEET
(WD) - (WL) _ (LWC)
ONE CASING VOLUME: L�+� GALLONS
(LWC) x (WCV)
THREE CASING VOLUMES: GALLONS
ACTUAL VOLUME PURGED: S "0 0 GALLONS
1" = 0.041 Gal/Ft 2" = 0.17 Gal/Ft
WELL CASING VOLUMES (WCV)
3" = 0.38 Gal/Ft 4" = 0.66 GaVFt 6" =1.5 Gal/Ft 8" = 2.6 GaVFt 12" = 5.8 Gal/Ft
PURGE METHOD: B zDI
BAILER-TEFLON DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER:
SAMPLE METHOD: -
. BAILER-TEFLON DEDICATED
PUMP WHALE PUMP GRUNDFOS OTHER:
READING
TIME
GALLONS
PURGED
TEMP
(CO)
SPECIFIC
COND.
(µS)
DISSOLVED
OXYGEN
(mg/L)
pH
(S.U.)
OXIDATION
REDUCTION
POTENTIAL
mV
TURBIDITY
(NTU)
COMMENTS
3
r aii
(. _ 1 )
V
4
0,a
Sa i
5
6
7
8
9
SAMPLING CONTAINER
NUMBER OF CONTAINERS
REQUESTED ANALYSIS
40 ml GLASS
5
TOC, VOC's by 6200B
125 ml PLASTIC
3
Nitrate, Ammonia
250 ml PLASTIC
1
Fecal Coliform
500 ml PLASTIC
1
Chloride; Sulfate, TDS
PROTECTIVE CASING: 69- PAD: 6C
LOCK: Mew VEGETATION: 6e-c� ACCESS:
Sampling Personnel Signature:
Date: Ct 5%
^
Notes: µS = micro-Siemen
C° = degrees Celsius
mg/L = milligrams per liter
mV = millivolt
S.U. = Standard Units
NTU = nephelometric turbidity units
P:\Templates\GW Drilling Forms\Well Sampling Log xls Page 1 of 1

N G I N* E E R I N G 8C H Y R O G E O L O G Y
2 3 1 H A Y W O O O S T R E E T. A S H
PAC
WW W.A LTAMONTENYIRONMEN TA L.coM
Well Sampling Log
FACILITY NAME: Clement Pappas
DATE: ' ,r>70q
LOCATION: Henderson County, North Carolina
SAMPLING TIME: i
SAMPLING PERSONNEL: E. Yurkovich
WEATHER: de r•, !&m
, Q�j
WELL NUMBER: 14 ire✓—V
WELL DEPTH IN FEET (WD): 16, -7Q
START TIME: `-(,2
WELL DIAMETER: Q IN
WATER LEVEL IN FEET (WL): "-:?9 ?Q
TYPE OF CASING: j�WC.
LENGTH OF WATER COLUMN: (,
FEET
MEASURING POINT: "�C7C.
(WD) - (WL) _ (LWC)
FLUSH MOUNq: . -U
ONE CASING VOLUME: 1. j (7
GALLONS
COMMENTS:
(LWC) x (WCV)
THREE CASING VOLUMES:
GALLONS
ACTUAL VOLUME PURGED: 0-5,
GALLONS
WELL CASING VOLUMES (WCV)
1" = 0.041 Gal/Ft 2" = 0.17 Gal/Ft
3" = 0.38 Gal/Ft 4" = 0.66 Gal/Ft 6" =1.5 Gal/Ft 8" = 2.6
Gal/Ft 12" = 5.8 Gal/Ft
PURGE METHOD: B -
ISP. BAILER-TEFLON DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER:
SAMPLE METHOD: -
BAILER-TEFLON DEDICATED
PUMP WHALE PUMP GRUNDFOS OTHER:
READING
UME
GALLONS
TEMP
SPECIFIC
DISSOLVED
pH
OXIDATION
TURBIDITY
COMMENTS
PURGED
(CO)
COND.
OXYGEN
(S.U.)
REDUCTION
(NTU)
(µs)
(mg/L)
POTENTIAL
m
1
9v1'
,p
156
ILIA
��
--
53U 0
r y
`J • l0 ii
1),39
2
113
1 t-i-i-4-
T7
400
5M
3W A
3
D- 60
IOD i
i 5-$5
:T(p
6.43
31z' ?
0fiw,-,3L-
4
1,0
.-q3
`31Z?
i�
5
6
7
8
9
SAMPLING
CONTAINER
NUMBER OF CONTAINERS
REQUESTED ANALYSIS
40 ml GLASS
5
TOC, VOC's by 6200B
125 nil PLASTIC
3
Nitrate, Ammonia
250 nil PLASTIC
1
Fecal Coliform
500 ml PLASTIC
I
Chloride, Sulfate, TDS
PROTECTIVE CASING: CAL' PAD: oi:
LO fI of
VEGETATION: 43 r— ACCESS: Cc�ar3
Sampling Personnel Signature:
Date: i
Notes:
µS =micro-Siemen
C° = degrees Celsius
mg/L = milligrams per liter
mV = millivolt
S.U. = Standard Units
NTU = nephelometric turbidity units
P:\Templafes\GW Drilling Forms\Well Sampling Log.xls Page 1 of 1

E N G I N E E'R I ' N G SC - H Y O R O G E O L O G Y
231 H AVWNO 0 S T R E E T, AS H E V I LLE, N C 26 g 0 1
WWW.gt„Tq MONTENV(RONMENTq L.cOM
FACILITY NAME: Clement Pappas
LOCATION: Henderson County, North Carolina
SAMPLING PERSONNEL: E. Yurkovich
WELL, NUMBER: i 1w-
WELL DIAMETER: Da
TYPE OF CASING: F�
MEASURING POINT: I
FLUSH MO TICK -
COMMENTS:
Well Sampling Log
DATE: I j
SAMPLING TIME:
WEATHER: 4*4t r', Jtmw
WELL DEPTH IN FEET (WD):
1 0 START
WATER LEVEL IN FEET (WL):
LENGTH OF WATER COLUMN:
•C. FEET
(WD) - (WL) = (LWC)
ONE CASING VOLUME:
0196 GALLONS
(LWC) x (WCV)
THREE CASING VOLUMES:
0.31 GALLONS
ACTUAL VOLUME PURGED:
Q, 5'0 GALLONS
WELL CASING VOLUMES (WCV)
1" = 0.041 Gal/Ft 2" = 0.17 GaUFt 3" = 0.38 Gal/Ft 4" = 0.66 Gal/Ft 6" =1.5 Gal/Ft 811= 2.6 Gal/Ft 12" = 5.8 Gal/Ft
PURGE METHOD: R-D BAILER-TEFLON DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER:
SAMPLE METHOD: �D�IS'PBAILER-TEFLON DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER:
READING TIME GALLONS TEMP SPECIFIC DISSOLVED pH OXIDATION TURBIDITY COMMENTS
PURGED (C°) COND. OXYGEN (S.U.) REDUCTION (NTU)
(µS) (mg/L) POTENTIAL
1
%Ihb-C-Q
f 10 P
HIT?
GRO
(, (a 1_
5--
p(01
1�1C�,
3
q
I..
�.
�;l- cae
? i (4 c
5
6
7
8
9
SAMPLING
CONTAINER
NUMBER OF CONTAINERS
REQUESTED ANALYSIS
40 ml GLASS
5
TOC, VOC's by 6200B
125 ml PLASTIC
3
Nitrate, Ammonia
250 ml PLASTIC
1
Fecal Coliform
500 ml PLASTIC
1 lChloride,
Sulfate, TDS
PROTECTIVE CASING: t3k PAD: LOCK: ate.' VEGETATION: .Ok- ACCESS:
Sampling Personnel Signature: Date:
Notes: µS = micro-Siemen
C° = degrees Celsius
mg/L = milligrams per liter
mV = millivolt
S.U. = Standard Units
NTU = nephelometric turbidity units
P:\Templates\GW Drilling Forms\Well Sampling Log.xls . Page 1 of 1

ALTAMONT ENVIRONMENTAL, INC.
Engineering & Hydrogeology
231 HAYWOOD STREET, ASHEVILLE, NC 28801
TEL.[phone] FAC.828.281.3351
m" altamontenvironmental com
Equipment Documentation & Instrument Calibration Data Sheet
Proi ect Name: Clement Pannas
Project Number: 2081.01 Calibration Documentation
Project Location: Mountain Home, North Carolina Person Conducting Calibration: �. L'� fGt.Wr1
Date of Calibration: 1116101
Equipment Documentation Date of Field Measurements:
,
Equipment or meters used to take measurements (e.g. water level meters sury equipment, etc.):
Equipment Type Serial Number Brand Date of Use
150-ft Water Level 26154 Solinist
150-ft Water Level 22754 Solinist
150-ft Water Level 150 Testwell
150-ft Drawdown MP30-1527 QED
Micro TPW Turbiditv Meter
Calibration Time
Micro TPW Turbiditv Meter
Calibration Time
��t br q ion
Instrument
Instrument Reading
1000 NTU
10.0 NTU
0.02 NTU
9�
`� i sb
200601045
Initial: s `r°l;•T
Cal: 020
Initial: `2� �o
Cal: (S a ,6
Initial: d too
Cal: -0.
YSI 556 Multlparameter Meter
Instrument Serial
Instrument Readings
Number
Dissolved
PH 7 S.U.
pH 4 S.U.
pH 10 S.U.
QC*
Spec. Cond.
QC*
ORP
Oxygen
ygen
pH 7 S.U.
447/84/23 µS
84 µS
200 mV
Time: 4 4
Time: '454
Time: C60
Time: V 4
Time: 8 if
Time: �
Time: 31�
Time: �;
mmHg: -Tl l�
Initial: 7. & S
Initial: 14`3�
Initial: i ei` �
Meas: ",�.�;'�
Initial: ��-Cf
Meas: ��
Initial: 0�`[- `7'
4
initial:
Cal: q.aU
Cal: 1mPo12
Time:
Cal: 44+
Time:
Cal: 9W,0
07D I O0979
Cal:
Check:
Check:
Time:
Time:
Check:
Check:
Calibration
Date
NA
-
ru'C 1tZo
�jg¢C
�
ial`
,Y-7
�E�VExpiration Oleo
0
Comments:
Signature and Date: 11415/cn
Notes:
1. Electronic equipment calibrated according to the manufacturer's operation manual.
2. Specific Conductivity should be calibrated according to values representative of historic range.
3.Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, ORP, QC checks.
4. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If readings are out of these ranges, meter needs to be recalibrated.
5. * indicates that a QC check must be performed in the morning, afternoon, and the end of the day.
P:\Templates\GW-Drilling Forms\Calibration Data Sheet YSI 556 Paoe r of 1

acoAnaIXical
www.pacelabs.com
November 23, 2009
Mr. Chris Gilbert
Altamont Environmental
231 Haywood Street
Asheville, NC 28801
RE: Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Dear Mr. Gilbert:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 05, 2009.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lord Patton
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc._
C N NCCOq
c3-\e
Page 9 of 29

aceAnaljdical
www.pacelabs.rom
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Charlotte Certification IDs
Connecticut Certificafion #: PH-0104
Pennsylvania Certification #: 68-00784
Florida/NELAP Certification #: E87627
North Carolina Wastewater Certification * 12
9800 Kincey Ave. - Ste 100 Huntersville, NC 28078
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Drinking Water Certification #: 37706
Virginia Certification #: 00213
New Jersey Certification #: NC012
Tennessee Certification * 04010
Louisiana/LELAP Certification #: 04034
South Carolina Drinking Water Cert. #: 990060003
Kentucky UST Certification #. 84
South Carolina Certification #: 990060001
Asheville Certification IDs
Connecticut Certification #: PH-0106
North Carolina Drinking Water Certification #: 37712
2225 Riverside Dr. Asheville, NC 28804
North Carolina Bioassay Certification #: 9
Virginia Certification #: 00072
New Jersey Certification #: NC011
Tennessee Certification #: 2980
Massachusetts Certification #: M-NC030
South Carolina Certification #: 99030001
Louisiana/LELAP Certification #: 03095
South Carolina Bioassay Certification #: 9903b002
Florida/NELAP Certification #: E87648
Pennsylvania Certification* 68-03578
West Virginia Certification #: 356
North Carolina Wastewater Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
a`�
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 29

s F
aceAnalytical
www.pacelabs.com
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-2R Lab ID: 9256937001 Collected: 11/05/09 11:45 Received: 11/05/09 13:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
92210E Fecal Coliform, MPN
Analytical Method: SM 9221C/E
Fecal Coliforms, MPN
<2 MPN/100ml-
1.0
1
6200B MSV
Analytical Method: SM 62006
Benzene
ND ug/L
0.50
1
Bromobenzene
ND ug/L
0.50
1
Bromochloromethane
ND ug/L
0.50
1
Bromodichloromethane
ND ug/L
0.50
1
Bromoform
ND ug/L
0.50
1
Bromomethane
ND ug/L
1.0
1
n-Butylbenzene
ND ug/L
0.50
1
sec-Butylbenzene
ND ug/L
0.50
1
tert-Butylbenzene
ND ug/L
0.50
1
Carbon tetrachloride
ND ug/L
0.50
1
Chlorobenzene
ND ug/L
0.50
1
Chloroethane
ND ug/L
1.0
1
Chloroform
ND ug/L
0.50
1
Chloromethane
ND ug/L
1.0
1
2-Chlorotoluene
ND ug/L
0.50
1
4-Chlorotoluene
ND ug/L
0.50
1
1,2-Dibromo-3-chloropropane
ND ug/L
1.0
1
Dibromochloromethane
ND ug/L
0.50
1
1,2-Dibromoethane (EDB)
ND ug/L
0.50
1
Dibromomethane
ND ug/L
0.50
1
1,2-Dichlorobenzene
ND ug/L
0.50
1
1,3-Dichlorobenzene
ND ug/L
0.50
1
1,4-Dichlorobenzene
ND ug/L
0.50
1
Dichlorodifluoromethane
ND ug/L
0.50
1
1,1-Dichloroethane
ND ug/L
0.50
1
1,2-Dichloroethane
ND ug/L
0.50
1
M-Dichloroethene
ND ug/L
0.50
1
cis-1,2-Dichloroethene
ND ug/L
0.50
1
trans-1,2-Dichloroethene
ND ug/L
0.50
1
1,2-Dichloropropane
ND ug/L
0.50
1
1,3-Dichloropropane
ND ug/L
0.50
1
2,2-Dichloropropane
ND ug/L
0.50
1
1,1-Dichloropropene
ND ug/L
0.50
1
cis-1,3-Dichloropropene
ND ug/L
0.50
1
trans-1,3-Dichloropropene
ND ug/L
0.50
1
Diisopropyl ether
ND ug/L
0.50
1
Ethylbenzene
ND ug/L
0.50
1
Hexachloro-1,3-butadiene
ND ug/L
2.0
1
Isopropylbenzene (Cumene)
ND ug/L
0.50
1
Methylene Chloride
ND ug/L
2.0
1
Methyl-tert-butyl ether
ND ug/L
0.50
1
Naphthalene
ND ug/L
2.0
1
n-Propylbenzene
ND ug/L
0.50
1
Styrene
ND ug/L
0.50
1
Date: 11/23/2009 01:16 PM
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
`�I_6-.1LLL1
11/05/09 16:50
11/11/09 04:35 71-43-2
11/11/09 04:35 108-86-1
11/11/09 04:35 74-97-5
11/11/09 04:35 75-27-4
11/11/09 04:35 75-25-2
11/11/09 04:35 74-83-9
11/11/09 04:35 104-51-8
11/11/09 04:35 135-98-8
11/11/09 04:35 98-06-6
11/11/09 04:35 56-23-5
11/11/09 04:35 108-90-7
11/11/09 04:35 75-00-3
11/11/09 04:35 67-68-3
11/11/09 04:35 74-87-3
11/11/09 04:35 95-49-8
11/11/09 04:35 106-43-4
11/11/09 04:35 96-12-8
11/11/09 04:35 124-48-1
11/11/09 04:35 106-93-4
11/11/09 04:35 74-95-3
11/11/09 04:35 95-50-1
11/11/09 04:35 541-73-1
11/11/09 04:35 106-46-7
11/11/09 04:35 75-71-8
11/11/09 04:35 75-34-3
11/11/09 04:35 107-06-2
11/11/09 04:35 75-35-4
11/11/09 04:35 156-59-2
11/11/09 04:35 156-60-5
11111 /09 04:35 78-87-5
11/11/09 04:35 142-28-9
11/11/09 04:35 594-20-7
11/11/09 04:35 563-58-6
11/11/09 04:35 10061-01-5
11/11/09 04:35 10061-02-6
11/11/09 04:35 108-20-3
11/11/09 04:35 100-41-4
11/11/09 04:35 87-68-3
11/11/09 04:35 98-82-8
11/11/09 04:35 75-09-2
11/11/09 04:35 1634-04-4
11/11/09 04:35 91-20-3
11/11/09 04:35 103-65-1
11/11/09 04:35 100-42-5
Page 3 of 29

QD
aceAnalj&al
( www.pacelabs.com
1
Project: CLEMENT PAPPAS 11 /05
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr -
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-2R
Lab ID: 9256937001 Collected:
11/05/0911:45
Received: 11/0510913:32 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
6200E MSV
Analytical Method: SM 6200B
1,1,1,2-Tetrachloroethane
ND ug/L
0.50
1
11/11/09 04:35
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
0.50
1
11/11/09 04:35
79-34-5
Tetrachloroethene
ND ug/L
0.50
1
11/11/09 04:35
127-18-4
Toluene
ND ug/L
0.50
1
11/11/09 04:35
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
2.0
1
11/11/09 04:35
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
2.0
1
11/11/09 04:35
120-82-1
1,1,1-Trichloroethane
ND ug/L
0.50
1
11/11/09 04:35
71-55-6
1,1,2-Trichloroethane
ND ug/L
0.50
1
11111/0904:35
79-00-5
Trichloroethene
ND ug/L
0.50
1
11/11/09 04:35
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
11/11/09 04:35
75-69-4
1,2,3-Trichloropropane
ND ug/L
0.50
1
11/11/09 04:35
96-18-4
1,2,4-Trimethylbenzene
ND ug/L
0.50
1
11/11/09 04:35
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
0.50
1
11/11/09 04:35
108-67-8
Vinyl chloride
ND ug/L
1.0
1
11/11/09 04:35
75-01-4
m&p-Xylene
ND ug/L
1.0
1
11/11/09 04:35
1330-20-7
o-Xylene
ND ug/L
0-50
1
11/11/09 04:35
95-47-6
1,2-Dichloroethane-d4 (S)
102 %
70-130
1
11/11/09 04:35
17060-07-0
Dibromofluoromethane (S)
101 %
70-130
1
11/11/09 04:35
1868-53-7
4-Bromofluorobenzene (S)
96 %
70-130
1
11/11/09 04:35
460-00-4
Toluene-d8 (S)
99 %
70-130
1
11/11/09 04:35
2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 2540C
Total Dissolved Solids
80.0 mg/L
20.0
1
11/10/0915:03
-
350.1 Ammonia
Analytical Method: EPA350.1
Nitrogen, Ammonia
ND mg/L
0.10
1
11/17/09 23:57
766441-7
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
0.31 mg/L
0.10
1
11 /06/09 21:05
4500 Chloride
Analytical Method: SM 4500-CI-E
Chloride
5.9 mg/L
5.0
1
11/1310916:29
16887-00-6
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
13.5 mg/L
1.0
1
11/10/09 18:05
7440-44-0
ASTM D516-90 Sulfate Water
Analytical Method: ASTM D516-90
Sulfate
23.5 mg/L
5.0
1
11/12/0916:17
14808-79-8
Date: 11/23/2009 01:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
4I �ge
_�o,N\
Page 4 of 29

.e
aceAnalytical
www.pacelab&cam
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-4 Lab ID: 9256937002 Collected: 11/05/09 12:23 Received: 11/05/09 13:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
92210E Fecal Coliform, MPN
Fecal Coliforms, MPN
6200B MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-b utad iene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
Date: 11/23/2009 01:16 PM
Analytical Method: SM 9221C/E
<2 MPN/100ml- 1.0 1
Analytical Method: SM 6200B
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
2.0
1
ND ug/L
0.50
1
ND ug/L
2.0
1
ND ug/L
0.50
1
ND ug/L
2.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
REPORT
OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Analytical Services, Inc..
�Paccee
11105/0916:50
11/11/09 04:59 71-43-2
11/11/09 04:59 108-86-1
11/11/09 04:59 74-97-5
11/11/09 04:59 75-27-4
11/11/09 04:59 75-25-2
11/11/09 04:59 74-83-9
11/11/09 04:59 104-51-8
11/11/09 04:59 135-98-8
11/11/09 04:59 98-06-6
11/11/09 04:59 56-23-5
11/11/09 04:59 108-90-7
11111 /09 04:59 75-00-3
11/11/09 04:59 67-66-3
11111 /09 04:59 74-87-3
11/11/09 04:59 95-49-8
11/11/09 04:59 106-43-4
11/11/09 04:59 96-12-8
11/11/09 04:59 124-48-1
11/11/09 04:59 106-93-4
11/11/09 04:59 74-95-3
11111 /09 04:59 95-50-1
11/11/09 04:59 541-73-1
11/11/09 04:59 106-46-7
11/11/09 04:59 75-71-8
11/11/09 04:59 75-34-3
11/11/09 04:59 107-06-2
11/11/09 04:59 75-35-4
11/11/09 04:59 156-59-2
11/11/09 04:59 156-60-5
11111 /09 04:59 78-87-5
11/11/09 04:59 142-28-9
11/11/09 04:59 594-20-7
11111 /09 04:59 563-58-6
11/11/09 04:59 10061-01-5
11/11/09 04:59 10061-02-6
11/11/09 04:59 108-20-3
11111 /09 04:59 100-41-4
11/11/09 04:59 87-68-3
11/11/09 04:59 98-82-8
11/11/09 04:59 75-09-2
11/11/09 04:59 1634-04-4
11/11/09 04:59 91-20-3
11/11/09 04:59 103-65-1
11/11/09 04:59 100-42-5
Page 5 of 29

aceAnalj&al
www.pacelabscom
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-4 Lab ID: 9256937002 Collected: 11/05/0912:23 Received: 11/05/09 13:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200E MSV
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1, 1 -Trichloroethane
1, 1, 2-Trichloroethane
Trchloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
1,2-Dichloroethane-d4 (S)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
350.1 Ammonia
Nitrogen, Ammonia
363.2 Nitrogen, N021NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
5310B TOC
Total Organic Carbon
ASTM D516-90 Sulfate Water
Sulfate
Date: 11/23/2009 01:16 PM
Analytical Method: SM 6200B
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
104 %
103 %
99 %
99 %
Analytical Method: SM 2540C
120 mg/L
Analytical Method: EPA 350.1
ND mg/L
Analytical Method: EPA 353.2
ND mg/L
Analytical Method: SM 4500-CI-E
13.6 mg/L
Analytical Method: SM 5310B
31.0 mg/L
Analytical Method: ASTM D516-90
30.7 mg/L
0.50
0.50
0.50
0.50
2.0
2.0
0.50
0.50
0.50
1.0
0.50
0.50
0.50
1.0
1.0
0.50
70-130
70-130
70-130
70-130
20.0 1
0.10 1
0.10 1
5.0 1
1.0 1
5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
11/11/09 04:59
630-20-6
11/11/09 04:59
79-34-5
11/11/09 04:59
127-18-4
11/11/09 04:59
108-88-3
11/11/09 04:59
87-61-6
11/11/09 04:59
120-82-1
11/11/09 04:59
71-55-6
11/11/09 04:59
79-00-5
11/11/09 04:59
79-01-6
11/11/09 04:59
75-69-4
11/11/09 04:59
96-18-4
11/11/09 04:59
95-63-6
11/11/09 04:59
108-67-8
11/11/09 04:59
75-01-4
11/11/09 04:59
1330-20-7
11/11/09 04:59
95-47-6
11/11/09 04:59
17060-07-0
11/11/09 04:59
1868-53-7
11/11/09 04:59
460-00-4
11/11/09 04:59
2037-26-5
11 /10/09 15:03
11 /17/09 23:58 7664-41-7
11/06/09 21:06
11 /13/09 16:29 16887-00-6
11 /10/09 18:21 7440-44-0
11 / 12/09 16:17 14808-79-8
Page 6 of 29

• ® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnaljd cal 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pace/abu.00m Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Sample: MW 5 Lab ID: 9256937003 Collected: 11/05/09 11:11 Received: 11/05/09 13:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
92210E Fecal Coliform, MPN
Analytical Method: SM 9221C/E
Fecal Coliforms, MPN
2 MPN/100ml-
1.0
1
11/05/09 16:50
6200B MSV
Analytical Method: SM 6200B
Benzene
ND ug/L
0.50
1
11/11/09 05:22
71-43-2
Bromobenzene
ND ug/L
0.50
1
11/11/09 05:22
108-86-1
Bromochloromethane
ND ug/L
0.50
1
11/11/09 05:22
74-97-5
Bromodichloromethane
ND ug/L
0.50
1
11/11/09 05:22
75-27-4
Bromoform
ND ug/L
0.50
1
11/11/09 05:22
75-25-2
Bromomethane
ND ug/L
1.0
1
11/11/09 05:22
74-83-9
n-Butylbenzene
ND ug/L
0.50
1
11/11/09 05:22
104-51-8
sec-Butylbenzene
ND ug/L
0.50
1
11/11/09 05:22
135-98-8
tert-Butylbenzene
ND ug/L
0.50
1
11/11/09 05:22
98-06-6
Carbon tetrachloride
ND ug/L
0.50
1
11/11/09 05:22
56-23-5
Chlorobenzene
ND ug/L
0.50
1
11/11/09 05:22
108-90-7
Chloroethane
ND ug/L
1.0
1
11/11/09 05:22
75-00-3
Chloroform
ND ug/L
0.50
1
11/11/09 05:22
67-66-3
Chloromethane
ND ug/L
1.0
1
11/11/09 05:22
74-87-3
2-Chlorotoluene
ND ug/L
0.50
1
11/11/09 05:22
95-49-8
4-Chlorotoluene
ND ug/L
0.50
1
11/11/09 05:22
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
1.0
1
11/11/09 05:22
96-12-8
Dibromochloromethane
ND ug/L
0.50
1
11/11/09 05:22
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
0.50
1
11/11/09 05:22
106-93-4
Dibromomethane
ND ug/L
0.50
1
11/11/09 05:22
74-95-3
1,2-Dichlorobenzene
ND ug/L
0.50
1
11/11/09 05:22
95-50-1
1,3-Dichlorobenzene
ND ug/L
0.50
1
11/11/09 05:22
541-73-1
1,4-Dichlorobenzene
ND ug/L
0.50
1
11/11/09 05:22
106-46-7
Dichlorodifluoromethane
ND ug/L
0.50
1
11/11/09 05:22
75-71-8
1,1-Dichloroethane
ND ug/L
0.50
1
11/11/09 05:22
75-34-3
1,2-Dichloroethane
ND ug/L
0.50
1
11/11/09 05:22
107-06-2
1,1-Dichloroethene
D_ug/L \
0.50
1
11/11/09 05:22
75-35-4
cis-1,2-Dichloroethene
125 ug%L J
0.50
1
11/11/09 05:22
156-59-2
trans-1,2-Dichloroethene
S2-ug/lf
0.50
1
11 /11109 05:22
156-60-5
1,2-Dichloropropane
ND ug/L
0.50
1
11/11/09 05:22
78-87-5
1,3-Dichloropropane
ND ug/L
0.50
1
11/11/09 05:22
142-28-9
2,2-Dichloropropane
ND ug/L
0.50
1
11/11/09 05:22
594-20-7
1,1-Dichloropropene
ND ug/L
0.50
1
11/11/09 05:22
563-58-6
cis-1,3-Dichloropropene
ND ug/L
0.50
1
11/11/09 05:22
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
0.50
1
11/11/09 05:22
10061-02-6
Diisopropyl ether
ND ug/L
0.50
1
11/11/09 05:22
108-20-3
Ethylbenzene
ND ug/L
0.50
1
11/11/09 05:22
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
2.0
1
11/11/09 05:22
87-68-3
Isopropylbenzene (Cumene)
ND ug/L
0.50
1
11/11/09 05:22
98-82-8
Methylene Chloride
ND ug/L
2.0
1
11/11/09 05:22
75-09-2
Methyl-tert-butyl ether
ND ug/L
0.50
1
11/11/09 05:22
1634-04-4
Naphthalene
ND ug/L
2.0
1
11/11/09 05:22
91-20-3
n-Propylbenzene
ND ug/L
0.50
1
11/11/09 05:22
103-65-1
Styrene
ND ug/L
0.60
1
11/11/09 05:22
100-42-5
Date: 11/23/2009 01:16 PM
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
without the written consent
of Pace Analytical Services, Inc..
r
Page 7 of 29

aceAnalj&al
xwx:paceiabs.com
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-5 Lab ID: 9256937003 Collected: 11/05/09 11:11 Received: 1110510913:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3 Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Tdchloroethane
Trichioroethene
Trichlorofluoromethane
1,2, 3-Trichloropropane
1,2,4-Trimethylbenzene
1,3, 5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
1,2-Dichloroethane-d4 (S)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4600 Chloride
Chloride
5310E TOC
Total Organic Carbon
ASTM D516-90 Sulfate Water
Sulfate
f
Date: 11/23/2009 01:16 PM
Analytical Method: SM 6200B
ND ug/L
�D g
872 ug/
�6 ug
ND ug/L
ND ug/L
.ND ug/L
ND ug/L
106 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
101 %
103 %
100 %
98 %
Analytical Method: SM 2540C
112 mg/L
Analytical Method: EPA 350.1
ND mg/L
Analytical Method: EPA 353.2
0.15 mg/L
Analytical Method: SM 4500-CI-E
39.1 mg/L
Analytical Method: SM 5310B
4.7 mg/L
Analytical Method: ASTM D516-90
ND mg/L
0.50
1
11/11/09 05:22
630-20-6
0.50
1
11/11/09 05:22
79-34-5
5.0
10
11/11/09 23:51
127-18-4
0.50
1
11/11/09 05:22
108-88-3
2.0
1
11/11/09 05:22
87-61-6
2.0
1
11/11/09 05:22
120-82-1
0.50
1
11/11/09 05:22
71-55-6
0.50
1
11/11/09 05:22
79-00-5
0.50
1
11/11/09 05:22
79-01-6
1.0
1
11/11/09 05:22
75-69-4
0.50
1
11/11/09 05:22
96-18-4
0.50
1
11/11/09 05:22
95-63-6
0.50
1
11/11/09 05:22
108-67-8
1.0
1
11/11/09 05:22
75-01-4
1.0
1
11/11/09 05:22
1330-20-7
0.50
1
11/11/09 05:22
95-47-6
70-130
1
11/11/09 05:22
17060-07-0
70-130
1
11/11/09 05:22
1868-53-7
70-130
1
11/11/09 05:22
460-00-4
70-130
1
11/11/09 05:22
2037-26-5
20.0
1
11 /10/0915:03
0.10
1
11/17/09 23:58
7664-41-7
0.10
1
11 /06/09 21:00
10.0
2
11/13/0916:38
16887-00-6
1.0
1
11/10/09 18:34
7440-44-0
5.0
1
11 /12/09 16:19
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 29

axAnalytical
www.pacelabs.com
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-6 Lab ID: 9256937004 Collected: 11/05/0910:33 Received: 11105/0913:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
92210E Fecal Coliform, MPN
Fecal Coliforms, MPN
6200E MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1, 2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloroprop ene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
Date: 11/23/2009 01:16 PM
Analytical Method: SM 9221 C/E
30 MPN/100mL
1.0
1
Analytical Method: SM 6200B
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
1.0
1 .
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
.1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
2.0
1
ND ug/L
0.50
1
ND ug/L
2.0
1
ND ug/L
0.50
1
ND ug/L
2.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
REPORT OF
LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
11 /05/09 16:00
11/11/09 11:44 71-43-2
11/11/09 11:44 108-86-1
11/11/09 11:44 74-97-5
11/11/09 11:44 75-27-4
1111110911:44 75-25-2
11/11/09 11:44 74-83-9
11/11/09 11:44 104-51-8
11/11/09 11:44 135-98-8
11111/0911:44 98-06-6
11/11/09 11:44 56-23-5
11 /11109 11:44 108-90-7
11/11/09 11:44 75-00-3
11/11/09 11:44 67-66-3
11/11/09 11:44 74-87-3
11/1110911:44 95-49-8
11/11/09 11:44 106-43-4
11/11/09 11:44 96-12-8
11111 /09 11:44 124-48-1
11/11/09 11:44 106-93-4
11/11/09 11:44 74-95-3
11/11/09 11:44 95-50-1
11/11/09 11:44 541-73-1
11/11/09 11:44 106-46-7
11/11/09 11:44 75-71-8
11/11/09 11:44 75-34-3
11/11/09 11:44 107-06-2
11/11/09 11:44 75-35-4
11/11/09 11:44 156-59-2
11/11/09 11:44 156-60-5
11/11/09 11:44 78-87-5
11/11/09 11:44 142-28-9
11111 /09 11:44 594-20-7
11/11/09 11:44 563-58-6
11/11/09 11:44 10061-01-5
11/11/09 11:44 10061-02-6
11/11/09 11:44 108-20-3
11/11/09 11:44 100-41-4
11/11/09 11:44 87-68-3
11/11/09 11:44 98-82-8
11/1110911:44 75-09-2
11/11/09 11:44 1634-04-4
11 /11109 11:44 91-20-3
11111 /09 11:44 103-65-1
11/11/09 11:44 100-42-5
Page 9 of 29

y
r
aceAnalyt'
www.pawlabs.com
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-6 Lab ID: 9256937004 Collected: 11/05/09 10:33 Received: 11/05/09 13:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
6200E MSV
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Tdchloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
1,2-Dichloroethane-d4 (S)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
360.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
5310B TOC
Total Organic Carbon
ASTM D516-90 Sulfate Water
Sulfate
Date: 11/23/2009 01:16 PM
Analytical Method: SM 62008
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
103 %
102 %
94 %
96 %
Analytical Method: SM 2540C
52.0 mg/L
Analytical Method: EPA 350.1
ND mg/L
Analytical Method: EPA 353.2
0.10 mg/L
Analytical Method: SM 4500-CI-E
ND mg/L
Analytical Method: SM 5310B
6.4 mg/L
Analytical Method: ASTM D516-90
9.3 mg/L
0.50
1
11111/0911:44
630-20-6
0.50
1
11/11/09 11:44
79-34-5
0.50
1
11/11/09 11:44
127-18-4
0.50
1
11 /11109 11:44
108-88-3
2.0
1
11/11/09 11:44
87-61-6
2.0
1
11/11/09 11:44
120-82-1
0.50
1
11/11/09 11:44
71-55-6
0.50
1
11111 /09 11:44
79-00-5
0.50
1
11/11/09 11:44
79-01-6
1.0
1
11/11/09 11:44
75-69-4
0.50
1
11/11/09 11:44
96-18-4
0.50
1
11/11/09 11:44
95-63-6
0.50
1
11/11/09 11:44
108-67-8
1.0
1
11/11/09 11:44
75-01-4
1.0
1
11111 /09 11:44
1330-20-7
0.50
1
11/11/09 11:44
95-47-6
70-130
1
11 /11109 11:44
17060-07-0
70-130
1
11/11/09 11:44
1868-53-7
70-130
1
11/11/09 11:44
460-00-4
70-130
1
11/11/09 11:44
2037-26-5
20.0
1
11/10/09 15:04
0.10
1
11 /18/09 00:00
7664-41-7
0.10
1
11/06/09 20:59
5.0
1
11 /13109 16:29
16887-00-6
1.0
1
11/10/0918:44
7440-44-0
5.0
1
11 /12/09 16:19
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc._
4 ' \
N.
Page 10 of 29

r
® Pace Analytical Services, Inc.
aceAnalytical 2225 Riverside Dr.
wmpacelabs.com As NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite100
Huntersville, NC 28078
[phone]
Project: CLEMENT PAPPAS 11105
Pace Project No.: 9256937
Sample: MW 7 Lab ID: 9266937005 Collected: 11/05/09 10:05 Received: 11/05/09 13:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
92210E Fecal Coliform, MPN
Fecal Coliforms, MPN
6200B MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibro mo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
Analytical Method: SM 9221C/E
2 MPN/100mL 1.0 1
Analytical Method: SM 6200B
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
2.0
1
ND ug/L
0.50
1
ND ug/L
2.0
1
ND ug/L
0.50
1
ND ug/L
2.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
11/05/09 16:00
11/11/09 06:10 71-43-2
11/11/09 06:10 108-86-1
11/11/09 06:10 74-97-5
11/11/09 06:10 75-27-4
11111 /09 06:10 75-25-2
11/11/09 06:10 74-83-9
11/11/09 06:10 104-51-8
11111 /09 06:10 135-98-8
11/11/09 06:10 98-06-6
11/11/09 06:10 56-23-5
11/11/09 06:10 108-90-7
11/11/09 06:10 75-00-3
11/11/09 06:10 67-66-3
11/11/09 06:10 74-87-3
11/11/09 06:10 95-49-8
11/11/09 06:10 106-43-4
11/11/09 06:10 96-12-8
11/11/09 06:10 124-48-1
11/11/09 06:10 106-93-4
11/11/09 06:10 74-95-3
11/11/09 06:10 95-50-1
11/11/09 06:10 541-73-1
11/11/09 06:10 106-46-7
11/11/09 06:10 75-71-8
11 %11 /09 06:10 75-34-3
11/11/09 06:10 107-06-2
11/11/09 06:10 75-35-4
11/11/09 06:10 156-59-2
11/11/09 06:10 156-60-5
11/11/09 06:10 78-87-5
11/11/09 06:10 142-28-9
11/11/09 06:10 594-20-7
11/11/09 06:10 563-58-6
11/11/09 06:10 10061-01-5
11/11/09 06:10 10061-02-6
11 /11109 06:10 108-20-3
11 /11109 06:10 100-41-4
11/11/09 06:10 87-68-3
11/11/09 06:10 98-82-8
11 /11109 06:10 75-09-2
11/11/09 06:10 1634-04-4
11/11/09 06:10 91-20-3
11/11/09 06:10 103-65-1
11/11/09 06:10 100-42-5
Date: 11/23/2009 01:16 PM REPORT OF LABORATORY ANALYSIS Page 11 of 29
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
x

C
aceAnalj6cal
www.pacefabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: CLEMENT PAPPAS 11105
Pace Project No.: 9256937
Sample: MW-7 Lab ID: 9266937006 Collected: 11/05/09 10:05 Received: 11/05/09 13:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2, 3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2, 3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
1,2-Dichloroethane-d4 (S)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
5310E TOC
Total Organic Carbon
ASTM D616-90 Sulfate Water
Sulfate
Date: 11/23/2009 01:16 PM
Analytical Method: SM 6200B
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
103 %
102 %
97 %
100 %
Analytical Method: SM 2540C
70.0 mg/L
Analytical Method: EPA 350.1
ND mg/L
Analytical Method: EPA 353.2
2.3 mg/L
Analytical Method: SM 4500-CI-E
10.7 mg/L
Analytical Method: SM 5310B
5.3 mg/L
Analytical Method: ASTM D516-90
11.2 mg/L
0.50
0.50
0.50
0.50
2.0
2.0
0.50
0.50
0.50
1.0
0.50
0.50
0.50
1.0
1.0
0.50
70-130
70-130
70-130
70-130
1
1
1
1
1
20.0 1
0.10 1
0.10 1
5.0 1
1.0 1
5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
11/11/09 06:10 630-20-6
11/11/09 06:10 79-34-5
11/11/09 06:10 127-18-4
11/11/09 06:10 108-88-3
11/11/09 06:10 87-61-6
11/11/09 06:10 120-82-1
11/11/09 06:10 71-55-6
11/11/09 06:10 79-00-5
11/11/09 06:10 79-01-6
11/11/09 06:10 75-69-4
11/11/09 06:10 96-18-4
11/11/09 06:10 95-63-6
11/11/09 06:10 108-67-8
11/11/09 06:10 75-01-4
11/11/09 06:10 1330-20-7
11/11/09 06:10 95-47-6
11111 /09 06:10 17060-07-0
11/11/09 06:10 1868-53-7
11/11/09 06:10 460-00-4
11/11/09 06:10 2037-26-5
11/10/09 15:04
11/18/09 00:00 7664-41-7
11/06/09 20:56
11/13/09 16:29 16887-00-6
11/10/0918:55 7440-44-0
11 /12/09 16:20 14808-79-8
Page 12 of 29

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acmnalyiical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
mvw.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Sample: MW78
LabID: 9256937006
Collected: 11/05/09 09:35 Received:
11105/0913:32 Matrix: Water
Parameters
Results Units
Report Limit
DF Prepared
Analyzed
CAS No. Quaff
92210E Fecal Coliforrn, MPN
Analytical Method: SM 9221C/E
Fecal Coliforms, MPN
50 MPN/100ml-
1.0
1
11/05/0915:30
6200E MSV
Analytical Method: SM 6200B
Benzene
ND ug/L
0.50
1
11/11/09 06:33
71-43-2
Bromobenzene
ND ug/L
0.50
1
11/11/09 06:33
108-86-1
Bromochloromethane
ND ug/L
0.50
1
11/11/09 06:33
74-97-5
Bromodichloromethane
ND ug/L
0.50
1
11/11/09 06:33
75-27-4
Bromoform
ND ug/L
0.50
1
11/11/09 06:33
75-25-2
Bromomethane
ND ug/L
1.0
1
11/11/09 06:33
74-83-9
n-Butylbenzene
ND ug/L
0.50
1
11/11/09 06:33
104-51-8
sec-Butylbenzene,
ND ug/L
0.50
1
11/11/09 06:33
135-98-8
tert-Butylbenzene
ND ug/L
0.50
1
11/11/09 06:33
98-06-6
Carbon tetrachloride
ND ug/L
0.50
1
11/11/09 06:33
56-23-5
Chlorobenzene
ND ug/L
0.50
1
11/11/09 06:33
108-90-7
Chloroethane
ND ug/L
1.0
1
11/11/09 06:33
75-00-3
Chloroform
ND ug/L
0.50
1
11/11/09 06:33
67-66-3
Chloromethane
ND ug/L
1.0
1
11/11/09 06:33
74-87-3
2-Chlorotoluene
ND ug/L
0.50
1
11/11/09 06:33
95-49-8
4-Chlorotoluene
ND ug/L
0.50
1
11/11/09 06:33
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
1.0
1
11/11/09 06:33
96-12-8
Dibromochioromethane
ND ug/L
0.50
1
11/11/09 06:33
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
0.50
1
11/11/09 06:33
106-93-4
Dibromomethane
ND ug/L
0.50
1
11/11/09 06:33
74-95-3
1,2-Dichlorobenzene
ND ug/L
0.50
1
11/11/09 06:33
95-50-1
1,3-Dichlorobenzene
ND ug/L
0.50
1
11/11/09 06:33
541-73-1
1,4-Dichlorobenzene
ND ug/L
0.50
1
11/11/09 06:33
106-46-7
Dichlorodifluoromethane
ND ug/L
0.50
1
11/11/09 06:33
75-71-8
1,1-Dichloroethane
ND_ ug/L
0.50
1
11/11/09 06:33
75-34-3
1,2-Dichloroethane
ND ug/L
0.50
1
11/11/09 06:33
107-06-2
1,1-Dichloroethene
ND ug/L
0.50
1
11/11/09 06:33
75-35-4
c7ts-1,2-Dichloroethene
ND ug/L
0.50
1
11/11/09 06:33
156-59-2
trans-1,2-Dichloroethene
ND ug/L
0.50
1
11/11/09 06:33
156-60-5
1,2-Dichloropropane
ND ug/L
0.50
1
11/11/09 06:33
78-87-5
1,3-Dichloropropane
ND ug/L
0.50
1
11/11/09 06:33
142-28-9
2,2-Dichloropropane
ND ug/L
0.50
1
11/11/09 06:33
594-20-7
1,1-Dichloropropene
ND ug/L
0.50
1
11/11/09 06:33
563-58-6
cis-1,3-Dichloropropene
ND ug/L
0.50
1
11/11/09 06:33
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
0.50
1
11/11/09 06:33
10061-02-6
Diisopropyl ether
ND ug/L
0.50
1
11/11/09 06:33
108-20-3
Ethylbenzene
ND ug/L
0.50
1
11/11/09 06:33
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
2.0
1
11/11/09 06:33
87-68-3
Isopropylbenzene (Cumene)
ND ug/L
0.50
1
11/11/09 06:33
98-82-8
Methylene Chloride
ND ug/L
2.0
1
11/11/09 06:33
75-09-2
Methyl-tert-butyl ether
ND ug/L
0.50
1
11/11/09 06:33
1634-04-4
Naphthalene
ND ug/L
2.0
1
11/11/09 06:33
91-20-3
n-Propyibenzene
ND ug/L
0.50
1
11/11/09 06:33
103-65-1
Styrene
ND ug/L
0.50
1
11/11/09 06:33
100-42-5
Date: 11/23/2009 01:16 PM
REPORT OF LABORATORY ANALYSIS
Page 13 of 29
This report shall
not be reproduced,
except in full,
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
,1�laoeAnalXicajo 2225 Riverside Dr. 9800 KinceyAve. Suite 100
wwwPacelebs.eotrr Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Sample: MW-8 Lab ID: 9256937006 Collected: 11/05/09 09:35 Received: 11/05/09 13:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200E MSV
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2 Trichloroethane
Trchloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5 Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
1,2-Dichloroethane-d4 (S)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
5310B TOC
Total Organic Carbon
ASTM D516-90 Sulfate Water
Sulfate
Date: 11/23/2009 01:16 PM
Analytical Method: SM 6200B
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
102 %
104 %
97 %
97 %
Analytical Method: SM 2540C
114 mg/L
Analytical Method: EPA 350.1
ND mg/L
Analytical Method: EPA353.2
0.54 mg/L
Analytical Method: SM 4500-CI-E
15.4 mg/L
Analytical Method: SM 5310B
10.8 mg/L
Analytical Method: ASTM D516-90
18.4 mg/L
0.50
1
11/11/09 06:33
630-20-6
0.50
1
11/11/09 06:33
79-34-5
0.50
1
11/11/09 06:33
127-18-4
0.50
1
11/11/09 06:33
108-88-3
2.0
1
11/11/09 06:33
87-61-6
2.0
1
11/11/09 06:33
120-82-1
0.50
1
11/11/09 06:33
71-55-6
0.50
1
11/11/09 06:33
79-00-5
0.50
1
11/11/09 06:33
79-01-6
1.0
1
11/11/09 06:33
75-69-4
0.50
1
11/11/09 06:33
96-18-4
0.50
1
11/11/09 06:33
95-63-6
0.50
1
11/11/09 06:33
108-67-8
1.0
1
11/11/09 06:33
75-01-4
1.0
1
11/11/09 06:33
1330-20-7
0.50
1
11/11/09 06:33
95-47-6
70-130
1
11/11/09 06:33
17060-07-0
70-130
1
11/11/09 06:33
1868-53-7
70-130
1
11 /11109 06:33
460-00-4
70-130
1
11/11/09 06:33
2037-26-5
20.0
1
11 /10/09 15:05
0.10
1
11/18/09 00:02
7664-41-7
0.10
1
11/06/09 20:53
5.0
1
11 /13/09 16:29
16887-00-6
1.0
1
11/10/0919:05
7440-44-0
5.0
1
11 /12/09 16:20
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
.Wogk
w
Page 14 of 29

,y
aceAnalytical
wmpacelabaxom
Project: CLEMENT PAPPAS 11105
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: TB Lab ID: 9256937007 Collected: 11/05/09 00:00 Received: 11/05/09 13:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
6200B MSV Analytical Method: SM 6200B
Benzene
ND ug/L
0.50
1
11/10/09 23:51
71-43-2
Bromobenzene
ND ug/L
0.50
1
11/10/09 23:51
108-86-1
Bromochloromethane
ND ug/L
0.50
1
11/10/09 23:51
74-97-5
Bromodichloromethane
ND ug/L
0.50
1
11/10/09 23:51
75-27-4
Bromoform
ND ug/L
0.50
1
11/10/09 23:51
75-25-2
Bromomethane
ND ug/L
1.0
1
11/10/09 23:51
74-83-9
n-Butylbenzene
ND ug/L
0.50
1
11/10/09 23:51
104-51-8
sec-Butylbenzene
ND ug/L
0.50
1
11/1010923:51
135-98-8
tert-Butylbenzene
ND ug/L
0.50
1
11/10/09 23:51
98-06-6
Carbon tetrachloride
ND ug/L
0.50
1
11/10/09 23:51
56-23-5
Chlorobenzene
ND ug/L
0.50
1
11/1010923:51
108-90-7
Chloroethane
ND ug/L
1.0
1
11/10/09 23:51
75-00-3
Chloroform
ND ug/L
0.50
1
11/10/09 23:51
67-66-3
Chloromethane
ND ug/L
1.0
1
11/10/09 23:51
74-87-3
2-Chlorotoluene
ND ug/L
0.50
1
11/10/09 23:51
95-49-8
4-Chlorotoluene
ND ug/L
0.50
1
11/10/09 23:51
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
1.0
1
11/10/09 23:51
96-12-8
Dibromochloromethane
ND ug/L
0.50
1
11/10/09 23:51
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
0.50
1
11/10/09 23:51
106-93-4
Dibromomethane
ND ug/L
0.50
1
11/10/09 23:51
74-95-3
1,2-Dichlorobenzene
ND ug/L
0.50
1
11/10/09 23:51
95-50-1
1,3-Dichlorobenzene
ND ug/L
0.50
1
11/10/09 23:51
541-73-1
1,4-Dichlorobenzene
ND ug/L
0.50
1
11/10/09 23:51
106-46-7
Dichlorodifluoromethane
ND ug/L
0.50
1
11/10/09 23:51
75-71-8
1,1-Dichloroethane
ND ug/L
0.50
1
11/10/09 23:51
75-34-3
1,2-Dichloroethane
ND ug/L
0.50
1
11/10/09 23:51
107-06-2
1,1-Dichloroethene
ND ug/L
0.50
1
11/10/09 23:51
75-35-4
cis-1,2-Dichloroethene
ND ug/L
0.50
1
11/10/09 23:51
156-59-2
trans-1,2-Dichloroethene
ND ug/L
0.50
1
11/10/09 23:51
156-60-5
1,2-Dichloropropane
ND ug/L
0.50
1
11/10/09 23:51
78-87-5
1,3-Dichloropropane
ND ug/L
0.50
1
11/10/09 23:51
142-28-9
2,2-Dichloropropane
ND ug/L
0.50
1
11/1010923:51
594-20-7
1,1-Dichloropropene
ND ug/L
0.50
1
11/10/09 23:51
563-58-6
cis-1,3-Dichloropropene
ND ug/L
0.50
1
11/10/09 23:51
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
0.50
1
11/10/09 23:51
10061-02-6
Diisopropyl ether
ND ug/L
0.50
1
11/10/09 23:51
108-20-3
Ethylbenzene
ND ug/L
0.50
1
11/1010923:51
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
2.0
1
11/1010923:51
87-68-3
Isopropylbenzene(Cumene)
ND ug/L
0.50
1
11/1010923:51
98-82-8
Methylene Chloride
ND ug/L
2.0
1
11/10/09 23:51
75-09-2
Methyl-tert-butyl ether
ND ug/L
0.50
1
11/10/09 23:51
1634-04-4
Naphthalene
ND ug/L
2.0
1
11/10/09 23:51
91-20-3
n-Propylbenzene
ND ug/L
0.50
1
11/10/09 23:51
103-65-1
Styrene
ND ug/L
0.50
1
11/10/09 23:51
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
0.50
1
11/1010923:51
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
0.50
1
11/10/09 23:51
79-34-5
Tetrachloroethene
ND ug/L
0.50
1
11/10/09 23:51
127-18=4
Qual
Date: 11/23/2009 01:16 PM REPORT OF LABORATORY ANALYSIS Page 15 of 29
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
4I F_�ogeryc�=

aceAnalytical
..pacelabs.com
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: TB
Lab ID: 9266937007 Collected: 11/05/09 00:00
Received: 11/05/09 13:32 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
6200E MSV
Analytical Method: SM 6200B
Toluene
ND ug/L
0.50
1
11/10/09 23:51
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
2.0
1
11/10/09 23:51
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
2.0
1
11/1010923:51
120-82-1
1,1,1-Trichloroethane
ND ug/L
0.50
1
11/10/09 23:51
71-55-6
1,1,2-Trichloroethane
ND ug/L
0.50
1
11/10/09 23:51
79-00-5
Trichioroethene
ND ug/L
0.50
1
11/10/09 23:51
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
11/10/09 23:51
75-69-4
1,2,3-Trichloropropane
ND ug/L
0.50
1
11/10/09 23:51
96-18-4
1,2,4-Trimethylbenzene
ND ug/L
0.50
1
11110/0923:51
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
0.50
1
11/10/09 23:51
108-67-8
Vinyl chloride
ND ug/L
1.0
1
11/10/09 23:51
75-01-4
m&p-Xylene
ND ug/L
1.0
1
11/10/09 23:51
1330-20-7
o-Xylene
ND ug/L
0.50
1
11/10/09 23:51
95-47-6
1,2-Dichloroethane-d4 (S)
102 %
70-130
1
11/10/09 23:51
17060-07-0
Dibromofluoromethane (S)
101 %
70-130
1
11/10/09 23:51
1868-53-7
4-Bromofluorobenzene(S)
98 %
70-130
1
11/10/09 23:51
460-00-4
Toluene-d8 (S)
98 %
70-130
1
11/10/09 23:51
2037-26-5
Date: 11 /23/2009 01:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
JI IG�
Page 16 of 29

,y
® Pace Analytical Services, Inc.
aceAnaljdical 2225 Riverside Dr.
www.pacdabscom Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
QC Batch: WETA/6227 Analysis Method: SM 5310B
QC Batch Method: SM 5310B Analysis Description: 5310B TOC
Associated Lab Samples: 9256937001, 9256937002, 9256937003, 9256937004, 9256937005, 9256937006
METHOD BLANK: 364011 Matrix: Water
Associated Lab Samples: 9256937001, 9256937002, 9256937003, 9256937004, 9256937005, 9256937006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Organic Carbon mg/L ND 1.0 11/10/09 14:57
LABORATORY CONTROL SAMPLE: 364012
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Parameter Units • Conc. Result % Rec Limits Qualifiers
Total Organic Carbon mg/L 25 24.0 96 90-110
MATRIX SPIKE SAMPLE:
364013
9256703008
Spike
MS
MS
Parameter
Units
Result
Conc.
Result
% Rec
Total Organic Carbon
mg/L
ND
25
27.3
108
MATRIX SPIKE SAMPLE:
364015
9256907003
Spike
MS
MS
Parameter
Units
Result
Conc.
Result
% Rec
Total Organic Carbon
mg/L
1.8
25
25.9
97
SAMPLE DUPLICATE: 364014
9256880001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Total Organic Carbon
mg/L
25.7
25.4
1
SAMPLE DUPLICATE: 364016
9256937001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Total Organic Carbon
mg/L
13.5
13.6
0
Date:11123/2009 01:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pa�e Analytical Services, Inc..
-co,
% Rec
Limits Qualifiers
75-125
% Rec
Limits Qualifiers
75-125
Page 17 of 29

aceAnaljftal
www.pacdabs.com
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MBIO/3629 Analysis Method: SM 9221C/E
QC Batch Method: SM 9221C/E Analysis Description: 92210E Fecal Coliform, MPN
Associated Lab Samples: 9256937001, 9256937002, 9256937003, 9256937004, 9256937005, 9256937006
METHOD BLANK: 362803 Matrix: Water
Associated Lab Samples: 9256937001, 9256937002, 9256937003, 9256937004, 9256937005, 9256937006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/100mL negative 1.0 11/05/09 15:30
Date: 11/23/2009 01:16 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite100
Huntersville, NC 28078
[phone]
Page 18 of 29

T
/+ pQ �►n7 I� ,r® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
ao N lalXi/ al 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pate1J aab&com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
QC Batch: WETA/6256 Analysis Method: SM 4500-CI-E
QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride
Associated Lab Samples: 9256937001, 9256937002, 9256937003, 9256937004, 9256937005, 9256937006
METHOD BLANK: 366361 Matrix: Water
Associated Lab Samples: 9256937001, 9256937002, 9256937003, 9256937004, 9256937005, 9256937006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride mg/L ND 5.0 11/13/0916:28
LABORATORY CONTROL SAMPLE: 366362
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chloride mg/L 20 21.4 107 90-110
MATRIX SPIKE SAMPLE:
Parameter
366363
Units
9257185001
Result
Spike MS MS % Rec
Conc. Result % Rec Limits Qualifiers
Chloride
mg/L
5910
1000 5890 -2 75-125 MO
SAMPLE DUPLICATE: 366364
9257186001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Chloride
mg/L
184
189 3
Date: 11/23/2009 01:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 29

C
® Pace Analytical Services, Inc.
aceMaOcal 2225 Riverside Dr.
wwwpacelabscom Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
QC Batch: WET/10415 Analysis Method: SM 2540C
QC Batch Method: SM 2540C Analysis Description: 2540C Total Dissolved Solids
Associated Lab Samples: 9256937001, 9256937002, 9256937003, 9256937004, 9256937005, 9256937006
METHOD BLANK: 364062 Matrix: Water
Associated Lab Samples: 9256937001, 9256937002, 9256937003, 9256937004, 9256937005, 9256937006
Blank . Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Dissolved Solids mg/L ND 20.0 11/10/09 14:56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 364063
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids mg/L 250 264 106 80-120
SAMPLE DUPLICATE: 364064
Parameter
Total Dissolved Solids
Date: 11/23/2009 01:16 PM
9256880001 Dup
Units Result Result
mg/L 102 98.0
RPD Qualifiers
4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 20 of 29

r
aceAnalj fical ®
wwwpaWabs.com
Project: CLEMENT PAPPAS 11105
Pace Project No.: 9256937
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
2225 Riverside Dr.
9800 KinceyAve. Suite 100
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/6277
Analysis Method: EPA 350.1
QC Batch Method: EPA 350.1
Analysis Description: 350.1 Ammonia
Associated Lab Samples: 9256937001, 9256937002, 9256937003, 9256937004, 9256937005, 9256937006
METHOD BLANK: 367953
Matrix: Water
Associated Lab Samples: 9256937001, 9256937002,
9256937003, 9256937004, 9256937005, 9256937006
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Nitrogen, Ammonia
mg/L
ND 0.10 11/18/09 10:29
LABORATORY CONTROL SAMPLE:
367954
Spike LCS LCS % Rec
Parameter
Units
Cone. Result % Rec Limits Qualifiers
Nitrogen, Ammonia
mg/L
5 4.8 97 90-110
MATRIX SPIKE SAMPLE:
367955
9256888004 Spike MS MS
% Rec
Parameter
Units
Result Cone. Result % Rec
Limits Qualifiers
Nitrogen, Ammonia
mg/L
<0.10 5 6.3 127
90-110 MO
MATRIX SPIKE SAMPLE:
367956
9256892001 Spike MS MS
% Rec
Parameter
Units
Result Cone. Result % Rec
Limits Qualifiers
Nitrogen, Ammonia
mg/L
7.2 5 12.3 101
90-110
SAMPLE DUPLICATE: 367957
9256893001 Dup
Parameter
Units
Result Result RPD Qualifiers
Nitrogen, Ammonia
mg/L
1.4 1.5 5
SAMPLE DUPLICATE: 367958
9256647005 Dup
Parameter
Units
Result Result RPD Qualifiers
Nitrogen, Ammonia
mg/L
ND ND
Date: 11 /23/2009 01:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 21 of 29

6
® Pace Analytical Services, Inc.
aG'eAI /n all /fi'm' f 2225 Riverside Dr.
wmpacelabs.com Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
QC Batch: WETA/6243 Analysis Method: ASTM D516-90
QC Batch Method: ASTM D516-90 Analysis Description: ASTM D516-90 Sulfate Water
Associated Lab Samples: 9256937001, 9256937002, 9256937003, 9256937004, 9256937005, 9256937006
METHOD BLANK: 365733 Matrix: Water
Associated Lab Samples: 9256937001, 9256937002, 9256937003, 9256937004, 9256937005, 9256937006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfate mg/L ND 5.0 11112/0916:11
LABORATORY CONTROL SAMPLE:
365734
Parameter
Units
Sulfate
mg/L
MATRIX SPIKE SAMPLE:
365735
Parameter
Units
Sulfate
mg/L
MATRIX SPIKE SAMPLE:
365736
Parameter
Units
Sulfate
mg/L
SAMPLE DUPLICATE: 365737
Parameter
Sulfate
SAMPLE DUPLICATE: 365738
Parameter
Sulfate
Date: 11/23/2009 01:16 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
20 20.7 103 90-110
9256813001 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
2240 2000 1880 -18 75-125 MO
9256703006 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 20 23.3 106 75-125
9256703007 Dup
Units Result Result
mg/L ND ND
9256703008 Dup
Units Result Result
mg/L 9.1 9.1
RPD Qualifiers
RPD Qualifiers
0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 22 of 29

r .
aceAnalytical
www.pacelabs.com
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
QUALITY CONTROL DATA
[phone]
QC Batch: MSV18971 Analysis Method: SM 6200B
QC Batch Method: SM 62008 Analysis Description: 6200B MSV
Associated Lab Samples: 9256937001, 9256937002, 9256937003, 9256937004, 9256937005, 9256937006, 9256937007
METHOD BLANK 364070
Matrix: Water
Associated Lab Samples: 9256937001, 9256937002, 9256937003; 9256937004, 9256937005, 9256937006, 9256937007
Blank Reporting
Parameter
Units Result Limit
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
1111010923:28
1,1,1-Trichloroethane
ug/L
ND
0.50
11/10/09 23:28
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
11/10/09 23:28
1,1,2-Trichloroethane
ug/L
ND
0.50
11/10/09 23:28
1,1-Dichloroethane
ug/L
ND
0.50
11/10/09 23:28
1,1-Dichloroethene
ug/L
ND
0.50
11/10/09 23:28
1,1-Dichloropropene
ug/L
ND
0.50
11/10/09 23:28
1,2,3-Trichlorobenzene
ug/L
ND
2.0
11/10/09 23:28
1,2,3-Trichloropropane
ug/L
ND
0.50
11/10/09 23:28
1,2,4-Trichlorobenzene
ug/L
ND
2.0
11/10/09 23:28
1,2,4-Trimethylbenzene
ug/L
NO
0.60
11/10/09 23:28
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
11/10/09 23:28
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
11/10/09 23:28
1,2-Dichlorobenzene
ug/L
ND
0.50
11/10/09 23:28
1,2-Dichloroethane
ug/L
ND
0.50
11110/0923:28
1,2-Dichloropropane
ug/L
ND
0.50
11/10/09 23:28
1,3,5-Trimethylbenzene
ug/L
ND
0.50
11/10/09 23:28
1,3-Dichlorobenzene
ug/L
ND
0.50
11/10/09 23:28
1,3-Dichloropropane
ug/L
ND
0.50
11/10/09 23:28
1,4-Dichlorobenzene
ug/L
NO
0.50
11/10/09 23:28
2,2-Dichloropropane
ug/L
ND
0.50
11/10/09 23:28
2-Chlorotoluene
ug/L
ND
0.50
11/10/09 23:28
4-Chlorotoluene
ug/L
ND
0.50
11/10/09 23:28
Benzene
ug/L
ND
0.50
11/10/09 23:28
Bromobenzene
ug/L
ND
0.50
11/10/09 23:28
Bromochloromethane
ug/L
ND
0.50
11/10/09 23:28
Bromodichloromethane
ug/L
ND
0.50
11/1010923:28
Bromoform
ug/L
ND
0.50
11/10/09 23:28
Bromomethane
ug/L
ND
1.0
11/10/09 23:28
Carbon tetrachloride
ug/L
ND
0.50
11/10/09 23:28
Chlorobenzene
ug/L
ND
0.50
11/10/09 23:28
Chloroethane
ug/L
ND
1.0
11/10/09 23:28
Chloroform
ug/L
ND
0.50
11/10/09 23:28
Chloromethane
ug/L
ND
1.0
11/10/09 23:28
cis-1,2-Dichloroethene
ug/L
ND
0.50
11/10/09 23:28
cis-1,3-Dichloropropene
ug/L
ND
0.50
11/10/09 23:28
Dibromochloromethane
ug/L
ND
0.50
11/10/09 23:28
Dibromomethane
ug/L
ND
0.50
11/10/09 23:28
Dichlorodifluoromethane
ug/L
NO
0.50
11/10/09 23:28
Diisopropyl ether
ug/L
ND
0.50
11/10/09 23:28
Ethylbenzene
ug/L
ND
0.50
11/10/09 23:28
Hexachloro-1,3-butadiene
ug/L
ND
2.0
11/10/09 23:28
Isopropylbenzene (Cumene)
ug/L
ND
0.60
11/10/09 23:28
Date: 11/23/2009 01:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�1�1r o1 µ A�CC�.Spy�
�! 1-lllfiV.Jz
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 29

aceAnaljdical
www.pawlabscorn
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
METHOD BLANK: 364070
Associated Lab Samples:
Parameter
m&p-Xylene
Methyl-tert-butyl ether
Methylene Chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Matrix: Water
9256937001,9256937002,9256937003,9256937004,9256937005,9256937006,9256937007
Blank Reporting
Units Result Limit Analyzed Qualifiers
ug/L
ND
1.0
11/10/09 23:28
ug/L
ND
0.50
11/10/09 23:28
ug/L
ND
2.0
11/10/09 23:28
ug/L
ND
0.50
11/10/09 23:28
ug/L
ND
0.50
11/10/09 23:28
ug/L
ND
2.0
11/10/09 23:28
ug/L
ND
0.50
11/10/09 23:28
ug/L
ND
0.50
11/10/09 23:28
ug/L.
ND
0.50
11/10/09 23:28
ug/L
ND
0.50
11/10/09 23:28
ug/L
ND
0.50
11/10/09 23:28
ug/L
ND
0.50
11/10/09 23:28
ug/L
ND
0.50
11/10/09 23:28
ug/L
ND
0.50
11/10/09 23:28
ug/L
ND
0.50
11/10/09 23:28
ug/L
ND
1.0
11/10/09 23:28
ug/L
ND
1.0
11/10/09 23:28
%
100
70-130
11/10/09 23:28
%
101
70-130
11/10/09 23:28
%
101
70-130
11/10/09 23:28
%
100
70-130
11/10/09 23:28
LABORATORY CONTROL SAMPLE:
Parameter
364071
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
55.1
110
60-140
1,1,1-Trichloroethane
ug/L
50
52.0
104
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
50.8
102
60-140
1,1,2-Trichloroethane
ug/L
50
55.4
111
60-140
1,1-Dichloroethane
ug/L
50
54.7
109
60-140
1,1-Dichloroethene
ug/L
50
58.6
117
60-140
1,1-Dichloropropene
ug/L
50
56.3
113
60-140
1,2,3-Trichlorobenzene
ug/L
50
51.3
103
60-140
1,2,3-Trichloropropane
ug/L
50
49.1
98
60-140
1,24-Trichlorobenzene
ug/L
50
48.6
97
60-140
1,2,4-Trimethylbenzene
ug/L
50
53.0
106
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
49.6
99
60-140
1,2-Dibromoethane (EDB)
ug/L
50
53.3
107
60-140
1,2-Dichlorobenzene
ug/L
50
48.7
97
60-140
1,2-Dichloroethane
ug/L
50
53.9
108
60-140
1,2-Dichloropropane
ug/L
50
57.1
114
60-140
1,3,5 Trimethylbenzene
ug/L
50
51.3
103
60-140
1,3-Dichlorobenzene
ug/L
50
47.0
94
60-140
1,3-Dichloropropane
ug/L
50
53.3
107
60-140
1,4-Dichlorobenzene
ug/L
50
46.5
93
60-140
Date: 11/23/2009 01:16 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
4 f,r�.�goNcf=
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 24 of 29

aceAnal0cal
www.pacefabscom
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
QUALITY CONTROL DATA
[phone]
Pace Analytical Services, Inc.
9800 KinceyAve. Suite too
Huntersville, NC 28078
LABORATORY CONTROL SAMPLE:
Parameter
364071
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,2-Dichloropropane
ug/L
50
50.6
101
60-140
2-Chlorotoluene
ug/L
50
48.8
98
60-140
4-Chlorotoluene
ug/L
50
51.2
102
60-140
Benzene
ug/L
50
53.2
106
60-140
Bromobenzene
ug/L
50
51.2
102
60-140
Bromochloromethane
ug/L
50
54.8
110
60-140
Bromodichloromethane
ug/L
50
54.0
108
60-140
Bromoform
ug/L
50
60.9
122
60-140
Bromomethane
ug/L
50
39.3
79
60-140
Carbon tetrachloride
ug/L
50
55.9
112
60-140
Chlorobenzene
ug/L
50
48.8
98
60-140
Chloroethane
ug/L
50
72.1
.144
60-140 L3
Chloroform
ug/L
50
50.6
101
60-140
Chloromethane
ug/L
50
60.0
120
60-140
cis-1,2-Dichloroethene
ug/L
50
56.5
113
60-140
cis-1,3-Dichloropropene
ug/L
50
60.9
122
60-140
Dibromochloromethane
ug/L
50
53.6
107
60-140
Dibromomethane
ug/L
50
59.2
118
60-140
Dichlorodifluoromethane
ug/L
50
70.1
140
60-140
Diisopropyl ether
ug/L
50
52.8
106
60-140
Ethylbenzene
ug/L
50
51.8
104
60-140
Hexachloro-1,3-butadiene
ug/L
50
54.0
108
60-140
Isopropylbenzene (Cumene)
ug/L
50
54.7
109
60-140
m&p-Xylene
ug/L
100
108
108
60-140
Methyl-tert-butyl ether
ug/L
50
52.7
105
60-140
Methylene Chloride
ug/L
50
42.3
85
60-140
n-Butylbenzene
ug/L
50
50.3
101
60-140
n-Propylbenzene
ug/L
50
51.9
104
60-140
Naphthalene
ug/L
50
53.2
106
60-140
o-Xylene
ug/L
50
55.2
110
60-140
sec-Butylbenzene
ug/L
50
51.8
104
60-140
Styrene
ug/L
50
54.4
109
60-140
tert-Butylbenzene
ug/L
50
53.2
106
60-140
Tetrachloroethene
ug/L
50
52.1
104
60-140
Toluene
ug/L
50
51.9
104
60-140
trans-1,2-Dichloroethene
ug/L
50
51.3
103
60-140
trans-1,3-Dichloropropene
ug/L
50
59.2
118
60-140
Trichloroethene
ug/L
50
55.5
111
60-140
Trichlorofluoromethane
ug/L
50
60.7
121
60-140
Vinyl chloride
ug/L
50
76.3
153
60-140 LO
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
106
70-130
Dibromofluoromethane (S)
%
98
70-130
Toluene-d8(S)
%
101
70-130
[phone]
Date: 11/23/2009 01:16 PM REPORT OF LABORATORY ANALYSIS Page 25 of 29
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceMalXical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wmpacelabs corn Asheville, NC 28804 Huntersville, NC 28078
QUALITY CONTROL DATA
Project: CLEMENT PAPPAS 11105
Pace Project No.: 9256937
[phone] [phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
364314
364315
MS
MSD
9256882004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
20.3
18.9
102
95
60-140
7
1,1,1-Trichloroethane
ug/L
ND
20
20
18.3
18.8
91
94
60-140
2
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.1
17.3
111
87
60-140
24
1,1,2-Trichloroethane
ug/L
ND
20
20
23.3
18.6
117
93
60-140
22
1,1-Dichloroethane
ug/L
ND
20
20
22.2
20.0
111
100
60-140
11
1,1-Dichloroethene
ug/L
ND
20
20
16.0
20.5
80
103
60-140
25
1,1-Dichloropropene
ug/L
ND
20
20
17.7
19.8
88
99
60-140
11
1,2,3-Trichlorobenzene
ug/L
ND
20
20
21.2
18.1
106
91
60-140
16
1,2,3-Trichooropropane
ug/L
ND
20
20
22A
17.3
112
86
60-140
26
1,2,4-Trichlorobenzene
ug/L
ND
20
20
19.4
17.3
97
86
60-140
12
1,2,4-Trimethylbenzene
ug/L
ND
20
20
17.0
15.8
85
79
60-140
7
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
23.4
16.9
117
84
60-140
32 R1
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.6
18.7
113
94
60-140
19
1,2-Dichlorobenzene
ug/L
ND
20
20
18.8
18.0
92
88
60-140
4
1,2-Dichloroethane
ug/L
ND
20
20
23.8
19.0
119
95
60-140
23
1,2-Dichloropropane
ug/L
ND
20
20
23.7
20.4
118
102
60-140
15
1,3,5-Trimethylbenzene
ug/L
ND
20
20
15.1
14.7
76
74
60-140
3
1,3-Dichlorobenzene
ug/L
ND
20
20
17.1
17.1
86
86
60-140
0
1,3-Dichloropropane
ug/L
ND
20
20
23.2
18.5
116
92
60-140
23
1,4-Dichlorobenzene
ug/L
1.1
20
20
18.1
18.4
85
86
60-140
2
2,2-Dichloropropane
ug/L
ND
20
20
18.6
14.4
93
72
60-140
26
2-Chlorotoluene
ug/L
ND
20
20
17.0
16.9
85
84
60-140
1
4-Chlorotoluene
ug/L
ND
20
20
18.0
18.2
90
91
60-140
1
Benzene
ug/L
0.91
20
20
21.4
20.1
103
96
60-140
6
Bromobenzene
ug/L
ND
20
20
19.8
18.2
99
91
60-140
9
Bromochloromethane
ug/L
ND
20
20
17.4
19.3
87
96
60-140
10
Bromodichloromethane
ug/L
ND
20
20
21.0
18.1
105
90
60-140
15
Bromoform
ug/L
ND
20
20
22.0
18.1
110
91
60-140
19
Bromomethane
ug/L
ND
20
20
22.8
21.6
114
108
60-140
6
Carbon tetrachloride
ug/L
ND
20
20
17.7
20.2
88
101
60-140
13
Chlorobenzene
ug/L
8.7
20
20
24.3
26.4
78
88
60-140
8
Chloroethane
ug/L
ND
20
20
19.3
22.1
97
111
60-140
13
Chloroform
ug/L
ND
20
20
21.2
18.2
106
91
60-140
15
Chloromethane
ug/L
ND
20
20
26.7
23.3
133
116
60-140
14
cis-1,2-Dichloroethene
ug/L
ND
20
20
23.3
20.9
117
104
60-140
11
cis-1,3-Dichloropropene
ug/L
ND
20
20
23.0
19.0
115
95
60-140
19
Dibromochloromethane
ug/L
ND
20
20
19.9
17.2
99
86
60-140
14
Dibromomethane
ug/L
ND
20
20
24.4
20.5
122
103
60-140
17
Dichlorodifluoromethane
ug/L
ND
20
20
22.8
25.2
114
126
60-140
10
Diisopropyl ether
ug/L
ND
20
20
22.8
18.0
114
90
60-140
24
Ethylbenzene
ug/L
ND
20
20
16.5
17.4
82
87
60-140
6
Hexachloro-1,3-butadiene
ug/L
ND
20
20
18.4
20.2
92
101
60-140
10
Isopropylbenzene (Cumene)
ug/L
ND
20
20
16.3
18.5
82
92
60-140
12
m&p-Xylene
ug/L
ND
40
40
32.8
33.9
82
85
60-140
3
Methyl-tert-butyl ether
ug/L
ND
20
20
23.0
17.6
115
88
60-140
27
Methylene Chloride
ug/L
ND
20
20
17.4
12.2
87
61
60-140
35 R1
n-Buhylbenzene
ug/L
ND
20
20
16.3
18.5
82
92
60-140
12
Date: 11/23/2009 01:16 PM REPORT OF LABORATORY ANALYSIS Page 26 of 29
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
JLJS�A.41

f
aceAnalj cal
www.paodab.com
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 364314
Parameter
n-Propylbenzene
Naphthalene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
Date:11/23/2009 01:16 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Units
9256882004
Result
MS
Spike
Conc.
MSD
Spike
Conc.
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
ug/L
ND
20
20
16.7
18.5
84
92
60-140
10
ug/L
ND
20
20
22.6
17.2
113
86
60-140
27
ug/L
ND
20
20
17.7
17.3
89
86
60-140
3
ug/L
ND
20
20
16.9
19.2
83
95
60-140
13
ug/L
ND
20
20
14.7
11.7
74
58
60-140
23 MO
ug/L
ND
20
20
17.5
19.9
87
99
60-140
13
ug/L
ND
20
20
15.8
19.0
79
95
60-140
18
ug/L
ND
20
20
18.0
17.8
90
89
60-140
1
ug/L
ND
20
20
19.5.
18.5
98-
92
60-140
6
ug/L
ND
20
20
23.9
18.6
120
93
60-140
25
ug/L
ND
20
20
18.7
19.6
93
98
60-140
5
ug/L
ND
20
20
15.8
19.5
79
98
60-140
21
ug/L
ND
20
20
28.5
28.8
142
144
60-140
1 MO
%
98
95
70-130
%
101
101
70-130
%
97
98
70-130
%
101
98
70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
EJLLL�ddCLS..�=
Page 27 of 29

Pace Analytical Services, Inc. Pace Analytical Services, Inc. `
aceMalXical ® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
vnnypacela6scom Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: CLEMENT PAPPAS 11105
Pace Project No.: 9256937
QC Batch: WETA/6209
Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 9256937001, 9256937002,
9256937003, 9256937004, 9256937005, 9256937006
METHOD BLANK: 363005
Matrix: Water
Associated Lab Samples: 9256937001, 9256937002,
9256937003, 9256937004, 9256937005, 9256937006
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Nitrogen, Nitrate
mg/L
ND 0.10 11/06/09 20:49
LABORATORY CONTROL SAMPLE:
363006
Spike LCS LCS % Rec
Parameter
Units
Cone. Result % Rec Limits Qualifiers
Nitrogen, Nitrate
mg/L
5 5.3 105 90-110
MATRIX SPIKE SAMPLE:
363007
9256937006 Spike MS MS % Rec
Parameter
Units
Result Cone. Result % Rec Limits Qualifiers
Nitrogen, Nitrate
mg/L
0.54 5 6.1 110 90-110
SAMPLE DUPLICATE: 363008
9256937005 Dup
Parameter
Units
Result Result RPD Qualifiers
Nitrogen, Nitrate
mg/L
2.3 2.2 0
Date: 11 /23/2009 01:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 28 of 29
itl

aceAnalytical
www.pacelabs.com
QUALIFIERS
Project: CLEMENT PAPPAS 11/05
Pace Project No.: 9256937
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
ANALYTE QUALIFIERS
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
R1 RPD value was outside control limits.
[phone]
Date: 11/23/2009 01:16 PM REPORT OF LABORATORY ANALYSIS Page 29 of 29
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

ceAnal ical
www.pacelabs.com
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CHAIN -OF -CUSTODY / Analytical Request Document
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Section A Section B Section C
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