WQ0004797_Monitoring (Report)_20071221

SUBMIT FORM ON YELLOW PAPER ONLY
UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
ILITY INFORMATION mease t-nnr cieany or Type
ity Name: Clement Papas
tit Name (if different):
ityAddress: 125 Industrial Park
(Street)
jntain Home NC 28792 County Henderson
(City) (Stale) (zip)
act Person: Mr. Blake Kehoe Telephone#: [phone]
Location/Site Name: Irriaation Area No. of wells to be sampled: 6
06
PERMIT Number: Expiration Date: 11/30/2011
Non -Discharge W00004797 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
© Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
L ID NUMBER (from Permit): MW-2R Date sample collected: 11/13/2007
Depth: 11.5 ft. Well Diameter: _ 2 in.
i to Water Level: 8_46 ft, below measuring point Screened Interval: 6 ft. to ft.
luring Point is 3.77 ft, above land surface Relative M.P. Elevation: 2063.0 ft.
ne of water pumped/bailed before sampling: 1.50 gallons
)les for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO
a sample analyzed: varies; see analytical
-
IAMETERS NOTE: Values should reflect dissolv
COD
mg/I
Colifo�trm: MF Fecal
< 1.1 /100ml
.�Coliform: MF Total
/100ml
'(Mtevs'e MPN method for highly turbid samples)
tc if:'r
Dissolved, Solids: Total
82.0 mg/l
pH (.when analyzed)
units
�_i I TOC
5.9 mg/I
p! Chloride
16.7 mg/I
0 `�-
f Arsenic
mg/I
Grease
and Oils
mg/I
ZI cy
t
p
! Phenol
mg/l
Crl
<.
Sulfate
6.9 mg/I
,$peclfic-,
onductance
µMhos
Total Ammonia <
0.10 mg/I
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
TKN as N mg/I
FIELD S:
pH 5.28 u is Temp. 16.48 eC
Spec. 90 µMhos
Odor none
Appearance
_ Laboratory Name: Pace Analytical Services, Inc. Certification No. 37712
and colloidal concentrations.
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Nitrate (NO3) as N
2.9 mg/I
Zn - Zinc mg/I t L ➢
m
Phosphorus: Total as P
mg/I
I
I f
Orthophosphate
m /I
Other (Specify Compounds and Concentration Units)i0_' C
Al - Aluminum RECZVED
Ba - Barium mg/I
Ca - Calcium
Cd - Cadmium mg/I
Chromium: Total 1 fnrmatinn Procem§M LIn''
Cu - Copper
DWQ/1Jufi'tg/I
ORGANICS: (by GC, GC/MS, HPLC) r"
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
K - Potassium
mg/I
VOC , method # 621 OD
Mg - Magnesium
mg/I
method #
Mn - Manganese
mg/I
method #
Ni - Nickel
I mg/I
method #
of a
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, acc
DWQ-certified laboratory I am aware that there are significant penalties for submitting false informatioi
l �
Penniftee (or Authorized Agent) Name and Title- Please print or
GW-59 Rev.1/2007
mg/L Effluent Total VOCs: mg/L VOC Removal%
Authorized Agent)
at
of
EN
KI

SUBMIT FORM ON YELLOW PAPER ONLY
t0.
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM e s-M "Rw
1CILITY INFORMATION Please PdnrCleadyorType 7Non-Discharge
MIT Number;s Expiration Date: 11/3012011
Icility Name: Clement Papas W00004797 UIC
irmit Name (if different): ES Other
icility Address: 125 Industrial Park TYPE OF PERMITTED OPERATION BEING MONITORED
fountain Home (Street) NC 28792 County Henderson ❑ Lagoon ❑ Remediation: Infiltration Gallery
(city) (state) (zip) ® Spray Field ❑ Remediation:
)ntact Person: Mr. Blake Kehoe Telephone* [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
ell Location/Site Name:._Irriaation Area No, of wells to be sampled: 6 ❑ Water Source Heat Pump ❑ Other:
WELL ID NUMBER (from Permit): MW 4
Well Depth: 16.17ft, *relative to land surface
Depth to Water Level: 9.89 ft. below measuring point
Measuring Point is 2.43 ft. above land surface
Volume of water pumped/bailed before sampling:
Samples for metals were collected unfiltered: ❑YES
Date sample collected: _11/13/2007
Well Diameter: tin,
Screened Interval: 8 ft, to 1 6. 1 ft.
Relative M.P. Elevation: 2064.E ft.
4.50 gallons
❑ NO and field acidified: ❑ YES ❑ NO
FIELD KA[-'?SE
pH 5A Its Temp. 16.28 cC
Spec. Cond. 187 µMhos
Odor none
Appearance
WAS
DRY at
time of
sampling,
check
here: ❑
LABORATORY INFORMATION
Date sample analyzed: varies; see analytical
Laboratory Name: Pace Analytical Services,
Inc. Certification No. 37712
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N mg/I
Pb - Lead mg/I
Coliform: MF Fecal < 1.1 /100ml
Nitrate (NO3) as N < 0.10 mg/1
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 152 mg/I
Al - Aluminum mg/I
pH (when analyzed)
TOC 16;mg�'Ca
Ba - Barium 11
Calcium IV�,Chloride
-
1mg/I
Cd = Cadmium mg/I
Arsenic mg/I
Chromium: Total DEC I SgR00
Grease and Oils mg/I
Cu - Copper mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron Information Pr( sing �S�ecify test and method #. ATTACH LAB REPORT.)
Sulfate 25.0 mg/I
Hg - Mercury mgh'
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium mg/I
VOC method # 621 OD
Total Ammonia < 0,10 mg/I
Mg - Magnesium mg/l
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese mg/I
method #
. TKN as N mg/I,
Ni - Nickel mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please PrinfCleadyorType
PERMIT Number:
Expiration Date: 11/30/2011
Facility Name: Clement Papas
Non -Discharge W00004797
UIC
Permit Name (if different):
NPDES
Other
Facility Address: 125 Industrial Park
TYPE OF PERMITTED OPERATION BEING MONITORED
Mountain Home (Street)
NC 28792
County Henderson
❑ Lagoon
❑ Remediation: Infiltration Gallery
(city) (State) (zip)
® Spray Field
❑ Remediation:
Contact Person: Mr. Blake Kehoe
Telephone#: [phone]
❑ Rotary Distributor
❑ Land Application of Sludge
Well Location/Site Name: Irrigation Area
No. of wells to be sampled: 6_
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
LL ID NUMBER (from Permit): MW-5
Date sample collected: 11/13/2007
FIELD A AtYSE .
WAS
Well Depth: 19 ft.
Well Diameter: tin,
pH 5.14 units
Temp. 16.23 °C
DRY at
Depth to Water Level: 11.00 ft. below measuring point
Screened Interval: 9 ft. to 199
ft, Spec. Co
168 µMhos
time li
sampling,
Measuring Point is 3.00 ft. above land surface
Relative M.P. Elevation: 2086.4 ft.
Odor none
check
Volume of water pumped/bailed before sampling:
4.0 gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: [:]YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: varies; see analytical
Laboratory Name: Pace Analytical Services, Inc. Certification No. 37712
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N mg/I
Pb - Lead
mg/I
Coliform: MF Fecal < 1.1 /100ml
Nitrate (NO3) as N 0•25 mg/I
Zn - Zinc
mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate mg/I
Other (Specify Compounds
and Concentration Units):
Dissolved Solids: Total 112 mg/I
Al - Aluminum mg/I
-'
pH (when analyzed) units
Ba - Barium mg/I
TOC 4.2 mg/)
Ca - Calcium mg/I
Chloride 41.3 mg/I
Cd - Cadmium
IV
Arsenic mg/I
Chromium: Total mg
Grease and Oils mg/I
Cu - Copper Tg/4
7nO?RGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate < 5.0 mg/I
Hg -Mercury mg/l_rz,;;;JZeport
Attached?
® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium r' r mgil-,ti;l?• VOC
method # 6210D
Total Ammonia < 0.10 mg/I
Mg - Magnesium mg/I
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese mg/I
method #
TKN as N mg/I
Ni - Nickel mg/I
method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs: mg/L Effluent Total VOCs:
mg/L VOC Removal%
I certify that, to the best of my knowledge and belief, the information submitted
DWO-certified laboratory I am aware that there are significant penalties for
in this report is true, accurate, and complete, and that the laboratory
Submitting false information, including the possibility of fines and imprisonment
analytical data was produced using
for knowinq violations
approved methods of analysis by a
A MIT
and Title - Please print or type
Signature of Permittee (or Authorized Anent) (Date)
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
id
NDWATER QUALITY MONITORING:
LIANCE REPORT FORM
TY INFORMATION viease rnnr wearry or type
Name: Clement Papas
Name (if different):
Address: 125_Industrial Park
tain Home (Street) NC 28792 County Henderson
act Person: Mr. Blake Kehoe Telephone* [phone]
Location/Site Name: Irrigation Area No. of wells to be sampled: 6
Number: Expiration Date;
,harge W00004797 UIC
'DES Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-6
Date sample collected: 11 /13/2007
FIELD ANALYSES•
29 °C
WAS
DRY at
Well Depth: 10.ft.
Well Diameter: in,
pH 5.77 Temp. 16.13
Depth to Water Level: 7 85 ft. below measuring point
_2
Screened Interval: 5 ft. to eft.
Spec. Cond. 75 µMhos
time of sampling,
Measuring Point is 3.00 ft, above land surface
Relative M.P. Elevation: 2061.9 ft.
Odor none
check
Volume of water pumped/bailed before sampling:
1.25 gallons
Appearance
here:
Samples for metals were collected unfiltered: El YES
❑ NO and field acidified: ❑ YES ' ❑ NO
sample analyzed: varies; see analytical
Laboratory Name: Pace Analytical Services, Inc. Certification No. 37712
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
_:1—
Coliform: MF Fecal3.6 /100ml
Nitrate (NO3) as N
0.24 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
114 mg/I
Al -Aluminum
mg/I
pH (when analyzed)
units
Ba - Barium
TOC
5.7 mg/I
Ca - Calcium
Chloride
10.7 mg/I
Cd - Cadmium
mg/I
Arsenic
mgn
Chromium: Total n F (, rito
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
t tt��,ma,i�nrng/f `i `' (Specify test and method #. ATTACH LAB REPORT.)
Sulfate
5.8 mg/I
Hg - Mercury
''`mg11''
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method # 621 OD
Total Ammonia
0.24 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total).
Mn - Manganese
mg/I
method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Perm ttee (or Authorized Agent) I
GW-59 Rev.1/2007
Signature of Perrnittee (or Authorized Agent) (Date)

SUBMIT FORM ON YELLOW PAPER ONLY
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
TY INFORMATION Ptease Pnnt cteany or Type
Name: Clement Papas
Name (if different):
Address: 125 Industrial Park
tan Home (Street) NC 28792 County Henderson
act Person: Mr. Blake Kehoe Telephone#: [phone]
Location/Site Name: lrriaation Area No. of wells to be sampled: 6
L ID NUMBER (from Permit): MW-7 Date sample collected: 11/13/2007
Depth: _ 5 ft. . Well Diameter: _din,
h to Water Level: 11.76 ft. below measuring point Screened Interval: 5 ft. to 15 ft.
;wring Point is 3.00 ft. above land surface Relative M.P. Elevation: 2062.7 ft,
Tie of water pumped/bailed before sampling: 2.75 gallons
sample analyzed: varies; see analytical
1AMETERS NOTE: Values should reflect dissolved
COD
mg/I
Coliform: MF Fecal
< 1.1 /100ml
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
42.0 mg/I
pH (when analyzed)
units
TOC
4.2 mg/I
Chloride
6.8 mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
< 5.0 mg/I
Specific Conductance
µMhos
Total Ammonia
< 0.10 mg/I
(Ammonia Nitrogen; NH�as N; Ammonia Nitrogen, Total)
TKN as N mg/I
RMIT Number: Expiration Date: 11/30/2011
n-Discharge W00004797 UIC
'DES Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
© Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD AN LXSES'WAS
pH 5.08 it Temp. 15.98 eC DRY at
Mhos time of
. Spec. Con 49 µ sampling,
Odor none check
Appearance here:
Laboratory Name: Pace Analytical Services,
Inc. Certification No, 37712
colloidal concentrations.
Nitrite (NO.) as N
mg/1
Pb- Lead mg/I
Nitrate (NO3) as N
1.7 mg/I
Zn - Zinc mg/I
Phosphorus: Total as P
mg/I
Orthophosphate
mg/I
Other (Specify Co be i or Units):
REC WE-
Al - Aluminum
mg/I
Ba - Barium
mg/I
DEG
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
in{ter-rn,;, r, �, ,�sir7� Jr1i4
Chromium: Total
mg/l
PAIQ/80G
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
K - Potassium
mg/I
VOC , method # 621 OD
Mg - Magnesium
mg/I
Mn - Manganese
mg/1
Ni - Nickel
mg/I
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
ortvpe
Signature of Pennittee (or Authorized Anent) (Date)
GW-59 Rev.112007

SUBMIT FORM ON YELLOW PAPER ONLY
C!
DWATER QUALITY MONITORING:
IANCE REPORT FORM
TY INFORMATION measePnnrcreanyorType
Name: Clement Papas
Name (if different):
Address: 125 Industrial Park
tain Home (Street) NC 28792 County Henderson
(City) (State) (Zip)
act Person: Mr. Blake Kehoe Telephone#: [phone]
Location/Site Name: Irriaation Area . No, of wells to be sampled: 6
PERMIT Number: Expiration Date: 11/30/2011
Non -Discharge W00004797 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: infiltration Gallery
© Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
LL ID NUMBER (from Permit): MW-8
Date sample collected: 11/13/2007
FIELD
WAS
I Depth: 13 ft.
Well Diameter: in.
�5.Z
pH Temp. 15.47 °C
DRY at
th to Water Level: 11.Og ft. below measuring point
_2
Screened Interval: 3 ft, to eft.
Spec, C1 gg µMhos
time
sampling,
Isuring Point is 3.00 ft. above land surface
Relative M.P. Elevation: 2061.4 ft.
Odor none
check
ime of water pumped/bailed before sampling:
1.50 gallons
Appearance
here:
1Dles for metals were collected unfiltered: El YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: varies; see analytical
Laboratory Name: Pace Analytical Services,
Inc. Certification No. 37712
PARAMETERS NOTE: Values should reflect dissolved and
colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
< 1.1 /100ml
Nitrate (NO3) as N
0.97 mg/I
Zn - Zinc m �
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compibullfg-2onceriMir Units):
Dissolved Solids: Total
154 mg/I
Al -Aluminum
mg/I
PH (when analyzed)
units
Ba , Barium
mg/l
On►`
TOC
8.3 mg/I
Ca- Calcium
mg/I
Chloride
19.6 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
26.6 mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method # 621 OD
Total Ammonia
< 0.10 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NHaas N; Ammonia
Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%a
GW-59 Rev.1/2007

GW 59A COMPLIANCE REPORT FORM Permit # WQ0004797
(Submit one each monitoring period with GW-59 forms)
1
Enter date monitoring results were due. (12/30/2007) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
0
2
Was any required iinformation missing on the GW-59 report forms?
YES
NO
IF the answer to question 1 'or 2 is 'YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
. 3•
Are anyof the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate;.area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance.
4
Are,any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is "NO" skip to section 8.
!f the answer to question 4 Is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
MW-4: total organic carbon 16.7 mg/L
MW-5: tetratchloroehtene 1150 ug/L; trichloroethene 217 ug/L; cis-1,2-dichioroethene 209 ug/L; vinyl chloride 3.4 ug/L
MW-6: fecal coliform 3.6 MPNi100ml-
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
if the answer to question 5 is "NO", skip to section B.
If the answer to question 5 is "YES". list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
MWA: total organic carbon: 16 mg/L 11/03/05, 19 mg/L 5/24106; 16.7 mg/L 11/13/07
MW-5: tetratchloroehhene: 1900 ug/L 11/03/05; 350 ug/L 11109/06; 320 ug/L 05/18/2007; 1150 ug/L 11/13/07
trichloroethene: 210 ug/L 11103/05; 74 ug/L 11109106; 47 ug/L 05118/07; 217 ug/L 11/13/07
cis-1,2-dichloroethene: 220 ug/L 11/03/05, 209 ug/L 11/13/07
Vinyl chloride: 1.2 ug/L 11/09/06, 3.4 ug/L 11/13/07
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
•
if the answer is "YES". a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE If the answer is "NO", monitoring wells may be improperly
located;. contact the Regional Office.
7
Is the pennittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality -problem? - .
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 71s "NO", contact the Regional Office within 90 days; an evaluation may be
reautred to determine the impact the waste disposal system Is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the Permittee to a Notice of Violation,
tines, and/orpenalties.
MW-4: VOC and SVOC analyses were completed for all samples during the May 2007 groundwater sampling
event. The TOC is not attributable to VOCs or SVOCs.
MW-5: The compounds exceeding the Standards are suspected to be from an adjacent site/property.
g
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for rr—Ctlilss provided at the top of the current GW-59 form.
h ?eb}l�acknowl�dge�hat the above infoiination was e`valtiate� and 4he informafiort sub�n tttec��n this
i�epor�(Compliance,Report_GV19A,�uf,t�iiecomplete _to�.fhebhest of tirykr�owledge������.�
irnforrnation Processing Unit
Signature of Permittee (or Autho en Date
GW-59A 12/8/2003

` Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aceAnalyiical
s.www.pece1a6s.c0m Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Sample: MW-2R
Lab ID:. 927698001 Collected: 11/13/07 12:57 Received:
11/13/07 15:54 Matrix: Water
Parameters
Results Units
Report Limit
DF Prepared
Analyzed
CAS No. Qual
92210E Fecal Coliform, MPN
Analytical Method: SM 9221C/E
Fecal Coliforms, MPN
0.1 MPN/100mL
1.0
1
11/13/0717:05
6210 MSV
Analytical Method: SM.6210
Benzene
ND ug/L
0.50
1
11/21/07 03:22
71-43-2
Bromobenzene
ND ug/L
0.50
1
11/21/07 03:22
108-86-1
Bromochloromethane
ND ug/L
0.50
1
11/21/07 03:22
74-97-5
Bromodichloromethane
ND ug/L
0.50
1
11/21/07 03:22
'75-27-4
Bromoform
ND ug/L
'0.50
1
11/21/07 03:22
75-25-2
Bromomethane '
ND ug/L
1.0
1
11/21/07 03:22
74-83-9
n-Butylbenzene
ND ug/L
0.50
1.
11/21/07 03:22
104-51-8
sec -Butyl benzene
ND ug/L
0.50
1
11/21/07 03:22
135-98-8
tert-Butyl benzene
ND ug/L
0.50
1
11/21/07 03:22
98-06-6
Carbon tetrachloride
ND ug/L
0.50
1
11/21/07 03:22
56-23-5
Chlorobenzene
ND ug/L
0.50
1
11/21/07 03:22
108-90-7
Chloroethane
ND ug/L
1.0
1
11/21/07 03:22
75-00-3
Chloroform
ND ug/L
0.50
1
11/21/07 03:22
67-66-3
Chloromethane
ND ug/L
1.0
1
11/21/07 03:22
74-87-3
2-Chlorotoluene
ND ug/L
0.50
1
11/21/07 03:22
95-49-8
4-Chlorotoluene
ND ug/L
0.50
1
11/21/07 03:22
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
1.0
1
11/21/07 03:22
96-12-8
Dibromochloromethane
ND ug/L
0.50
1.
11/21/07 03:22
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
0.50
1
11/21/07 03:22
106-93-4
Dibromomethane
ND ug/L
0.50
1
11/21/07 03:22
74-95-3
1,2-Dichlorobenzene
ND ug/L
0.50
1
11/21/07 03:22
95-50-1
1,3-Dichlorobenzene
ND ug/L
0.50
1
11/21/07 03:22
541-73-1
1,4-Dichlorobenzene
ND ug/L
0.50
1
11/21/07 03:22
106-46-7
Dichlorodifluoromethane
ND ug/L
0.50
1
11/21/07 03:22
75-71-8
1,1-Dichloroethane
ND ug/L
0.50
1
11/21/07 03:22
75-34-3
1,2-Dichloroethane
ND ug/L
0.50
1
11/21/07 03:22
107-06-2
1,1-Dichloroethene
ND ug/L
0.50
11
11/21/07 03:22
75-35-4
cis-1,2-Dichloroethene
ND ug/L
0.50
1
11/21/07 03:22
156-59-2
trans-1;2-Dichloroethene
ND ug/L
0.50
1
11/21/07 03:22
156-60-5
1,2-Dichloropropane
ND ug/L -
0.50
1
11/21/07 03:22
78-87-5
1,3-Dichloropropane
ND ug/L
0.50
1
11/21/07 03:22
142-28-9
2,2-Dichloropropane
ND ug/L
0.50
1
11/21/07 03:22
594-20-7
1,1-Dichloropropene
ND ug/L
0.50
1
11/21/07 03:22
563-58-6
cis-1,3-Dichloropropene
ND ug/L
0.50
1
11/21/07 03:22
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
0.50
1
11/21/07 03:22
10061-02-6
Diisopropyl ether
ND ug/L
0.50
1
11/21/07 03:22
108-20-3
Ethylbenzene
ND ug/L
0.50
1
11/21/07 03:22
10041-4
Hexachloro-1,3-butadiene
ND ug/L
2.0
1
11/21/07 03:22
87-68-3
Isopropylbenzene (Cumene)
ND ug/L
0.50
1
11/21/07 03:22
98-82-8
p-Isopropyltoluene
ND ug/L
0.50
1
11/21/07 03:22
99-87-6
Methylene Chloride
ND ug/L
2.0
1
11/21/07 03:22
75-09-2
Methyl-tert-butyl ether
ND ug/L
0.50
1
11/21/07 03:22.
1634-04-4
Naphthalene
ND ug/L
2.0
1
11/21/07 03:22
91-20-3
n-Propylbenzene
ND ug/L
0.50
1
11/21/07 03:22
103-65-1
Date:12/04/2007 09:28 AM
REPORT OF LABORATORY ANALYSIS
Page 3 of 31
This report shall
not be reproduced,
except in full,
without the written consent
of Pace Analytical Services, Inc..

i
aceAnalytical
< www pacelabsxom
i
1
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-2R
Lab ID: 927698001 Collected:
11/13/07 12:57
Received: 11/13/07 15:54 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
6210 MSV
Analytical Method: SM 6210
Styrene
ND ug/L
0.50
1
11/21/07 03:22
.100-42-5
1,1,1,2-Tetrachloroethane.
ND ug/L
0.50
1
11/21/07 03:22
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
0.50
1
11/21/07 03:22
79-34-5
Tetrachloroethene
ND,ug/L
0.50
1
11/21/07 03:22:
127-18-4
Toluene
ND ug/L
0.50
1
11/21/07 03:22
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
2.0
1
11/21/07 03:22
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
2.0
1
11/21/07 03:22
120-82-1
1,1,1-Trichloroethane
ND ug/L
0.50
1
11/21/07 03:22
71-55-6
1,1,2-Trichloroethane
ND ug/L
0.50
1 ..
11/21/07 03:22
79-00-5
Trichloroethene
ND ug/L
0.50
1
11/21/07 03:22
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
11/21/07 03:22
75-69-4
1,2,3-Trichloropropane
ND ug/L
0.50
1
11/21/07 03:22
96-18-4
1,2,4-Trimethylbenzene
ND ug/L
0.50
1
11/21/07 03:22
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
0.50
1
11/21/07 03:22
108-67-8
Vinyl chloride
ND ug/L
1.0
1
11/21/07 03:22
75-01-4
m&p-Xylene
ND ug/L
1.0
1
11/21/07 03:22
-1330-20-7
o-Xylene
ND ug/L
0.50
1
11/21/07 03:22
95-47-6
1,2-Dichloroethane-d4 (S)
95 %
60-140
1
11/21/07 03:22
17060-07-0
Dibromofluoromethane (S)
101 %e
60-140
1
.11/21107 03:22
1868-53-7
4-Bromofluorobenzene(S)
98 %
60-140
1
11/21/07 03:22
460-00-4
Toluene-d8 (S)
98 %
60-140
1
11/21/07 03:22
.2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 2540C
Total Dissolved Solids
82.0 mg/L
20.0
1
11/14/07 23:38
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
ND mg/L
0.10
.1
11/18/07 11:25
7764-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
2.9 mg/L
0.10
1
11/14/07 07:52
4500 Chloride
Analytical. Method: SM 4500-CI-E
Chloride
16.7 mg/L
5.0
1
11/17/0715:35
16887-00-6
5310E TOC
Analytical Method: SM 53106
Total Organic Carbon
5.9 mg/L
1.0
1
11/25/07 10:00
7440-44-0
ASTM D5.16-9002 Sulfate Water
Analytical Method: ASTM D516-90,02
Sulfate
6.9 mg/L
5.0
1
11/14/0710:56
14808-79-8
Date: 12/04/2007 09:28 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc...
' .. •CCpgC
Page 4 of 31

aceAnalytical
www.pacelabs.com
Project: , Clement Pappas 2081.01
Pace Project No.: 927698
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-4 Lab ID: 927698002 Collected: 11/13/07 14:39 Received: 11/13/07 15:54 Matrix: Water
Parameters 'Results Units Report Limit DF Prepared Analyzed CAS No. Qual
92210E Fecal Coliform, MPN Analytical Method: SM 9221C/E
Fecal Coliforms, MPN <1.1 MPN/100mL 1.0 1 11/13/07 17:05
6210 MSV Analytical Method: SM 6210
Benzene
ND ug/L
0.50
1
11/21/07 03:46
71-43-2
Bromobenzene
ND ug/L
0.50
1
11/21/07 03:46
108-86-1
Bromochloromethane
ND ug/L
0.50
1
11/21/07 03:46
74-97-5
Bromodichloromethane
ND ug/L
0.50,
1
11/21/07 03:46
75-27-4
Bromoform
ND ug/L
0.50
1
11/21/07 03:46
75-25-2
Bromomethane
ND ug/L
1.0
1
11/21/07 03:46
74-83-9
n-Butylbenzene
ND ug/L
0.50
1
11i21/07 03:46
104-51-8
sec-Butylbonzene
ND ug/L
0.50
1
11/21/07 03:46
135-98-8
tert-Butyl benzene
ND ug/L
0.50
1
11/21/07 03:46
98-06-6
Carbon tetrachloride
ND ug/L
0.50
1
11/21/07 03:46
56-23-5
Chlorobenzene
ND ug/L
0.50
1
11/21/07 03:46
108-90-7
Chloroethane
ND ug/L
1.0
1
11/21/07 03:46
75-00-3
Chloroform
ND ug/L
0.50
1
11/21/07 03:46
67-66-3
Chlorometharie -
ND ug/L
1.0
1
11/21/07 03:46
74-87-3
2-Chlorotoluene
ND ug/L
0.50
1
11/21/07 03:46
95-49-8
4-Chlorotoluene
ND ug/L
0.50
1
11/21/07 03:46
106-43-4
•1,2-Dibromo-3-chloropropane
ND ug/L
1.0
1
11/21/07 03:46
96-12-8
Dibromochloromethane
ND ug/L
0.50
1
•11/21/07 03:46
.124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
0.50
1
.11121/07 03:46
106-93-4
Dibromomethane
ND ug/L
0.50
1
11/21/07 03:46
74-95-3
1,2-Dichlorobenzene
ND ug/L
0.50
1
11/21/07 03:46
95-50-1
1,3-Dichlorobenzene
ND ug/L
0.50
1
11/21/07 03:46
541-73-1
1,4-Dichlorobenzene
ND ug/L
0.50
1 .
11/21/07 03:46
106-46-7
Dichlorodifluoromethane
ND ug/L
0.50
1
11/21/07 03:46
75-71-8
1,1-Dichloroethane
ND ug/L
0.50
1
11/21/07 03:46
75-34-3
11,2-Dichloroethane
ND ug/L
0.50
1
11/21/07 03:46'
107-06-2
1,1-Dichloroethene
ND ug/L
0.50
1
11/21/07 03:46
75-35-4
cis-1,2-Dichloroethene
ND ug/L
0.50
1
11/21/07 03:46
156-59-2
trans-1,2-Dichloroethene
ND ug/L
0.50
1
11/21/07 03:46
156-60-5
1,2-Dichloropropane
ND ug/L
0.50
1
11/21/07 03:46
78-87-5
1,3-Dichloropropane
ND ug/L
0.50
1
11/21/07 03:46
142-28-9
2,2-Dichloropropane
ND ug/L
0.50
1
11/21/07 03:46
594-20-7
1,1-Dichloropropene
ND ug/L
0.50
1
11/21/07 03:46
563-58-6
cis-1,3-Dichloropro pene
ND ug/L
0.50
1
11/21/07 03:46
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
0.50
1
11/21/07 03:46
10061-02-6
Diisopropyl ether
ND ug/L
0.50
1
11/21/07 03:46
108-20-3 -
Ethylbenzene
ND ug/L
0.50
1
11/21/07 03:46
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
2.0
1
11/21/07 03:46
87-68-3
Isopro pyl benzene (Cumene)
ND ug/L
0.50
1
11/21/07 03:46
98-82-8
p-Isopropyltoluene
ND ug/L
0.50
1
11/21/07 03:46
99-87-6
Methylene Chloride
ND ug/L
2.0
1
11/21/07 03:46
75-09-2
Methyl-tert-butyl ether
ND ug/L
0.50
1
11/21/07 03:46
1634-04-4
Naphthalene,
ND ug/L
2.0
1
11/21/07 03:46
91-20-3
n-Propylbenzene
ND ug/L
0.50
1
11/21/07 03:46
103-65-1
Date;12/04/2007 09:28 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written
'
consent of Pace Analytical Services, Inc..
h •CCDgD'
el
Page 5 of 31

acejnty!i��l
+
i
Project: Clement Pappas 2081.01
Pace'Project No.: 927698
Sample: MW-4
Parameters
6210 MSV
Styrene
1, 1, 1,2-Tetrachloroetha ne
1,1, 2,2-Tetra chloroetha ne
Tetrachloroethene
Toluene
1,2,3 Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1, 3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
1,2-Dichloroethane-d4 (S)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
5310E TOC
Total Organic Carbon
ASTM D516-9002 Sulfate Water
Sulfate
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 927698002 Collected: 11/13/07 14:39,
Received: 11/13/07 15:54 Matrix: Water
Results Units Report Limit
DF
Prepared Analyzed
CAS No.
Analytical Method: SM 6210
ND ug/L
0.50
1
11/21/07 03:46
100-42-5
ND ug/L
0.50
1
11/21/07 03:46
630-20-6
ND ug/L
0.50
1
11/21/07 03:46
79-34-5
ND ug/L
0.50
1
11/21/07 03:46
127-18-4
r ND ug/L
0:50
1
11/21/07 03:46
108-88-3
ND ug/L
2.0
1
11/21/07 03:46
87-61-6
ND ug/L
2.0
1
11/21/07 03:46
120-82-1
ND ug/L
0.50-
1
11/21/07 03:46
71-55-6
ND ug/L
0.50
1
11/21/07 03:46
79-00-5
ND ug/L
0.50
1
11/21/07 03:46
79-01-6
ND ug/L
1.0
1
11/21/07 03:46
75-69-4
ND ug/L
0.50
1
11/21/07 03:46
96-18-4
ND ug/L
0.50
1
.11/21/07 03:46
95-63-6
ND ug/L
0.50
1.
11/21/07 03:46
108-67-8
ND ug/L
1.0
1
11/21/07 03:46
75-01-4
ND ug/L
1.0
1
11/21/07 03:46
1330-20-7
ND ug/L
0.50
1
11/21/07 03:46
95-47-6
94 %
60-140
1
11/21/07 03:46.
17060-07-0 .
101 %
60-140
1
11/21/07 03:46
1868-53-7
99 %
60-140
1
11/21/07 03:46
460-00-4
98 %
60-140
1
11/21/07 03:46
2037-26-5
Analytical Method: SM 2540C
152 mg/L
20.0
1
11/14/07 23:40
Analytical Method: EPA 350.1
ND mg/L
0.10
1
11/18/0711:26
7764-41-7
Analytical Method: EPA 353.2
ND mg/L
0.10 .
1
11/14/07 07:45
Analytical Method: SM 4500-CI-E
11.3 mg/L
5.0
1
11/17/0715:35
_16887-00-6
Analytical Method: SM 5310B
16.7 mg/L
1.0
1
11/25/07 10:00
7440-44-0
Analytical Method: ASTM D516-90,02
25.0 mg/L
5.0
1
11/14/07 10:58
14808-79-8
Date: 12/04/2007 09:28 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
CC^qo
���llri�lJs
Qual
Page 6 of 31

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aoAnalytical
www.pacetabs.com Asheville, NC 213804 Huntersville, NC 28078
f� s [phone] [phone]
ANALYTICAL RESULTS
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Sample: MW-5 Lab ID: 927698003 Collected: 11/13/07 13:53 Received: 11/13/07 15:54 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
92210E Fecal Coliform, MPN Analytical Method: SM 9221C/E
Fecal Coliforms, MPN <1.1 MPN/100mL 1.0 1 11/13/07 17:05
6210 MSV An Method: SM 6210
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec -Butyl benzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorod ifluoro methane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichl6ropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis- 1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropyl benzene (Cumene)
p-lsopropyltoluene
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Date: 12/04/2007 09:28 AM
ND. ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50 ,
1
ND ug/L
0.50
.1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
1.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
1.0 ug/L
0.50
1
209 ug/L
10.0
20
2.0 ug/L,
0.50
1
ND ug/L
0.50
1
ND ug/L
. 0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
0.50
1'.
ND ug/L
0.50
1
ND ug/L
0.50
.1
ND ug/L
0.50
1
ND ug/L
2.0
1
ND ug/L
0.50
1
ND ug/L
0.50
1
ND ug/L
2.0
1
ND ug/L
0.50
1
ND ug/L
2.0
1.1
ND ug/L
0.50
1
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
without the written'consent of Pace Analytical Services, Inc..
11/21/07 04:10
71-43-2
11/21/07 04:10-
108-86-1
11/21/07 04:10
74-97-5
11/21/07 04:10
75-27-4
11/21/07 04:10
75-25-2
11/21/07 04:10
74-83-9
11/21/07 04:10
104-51-8
11/21/07 04:10
135-98-8
11/21/07 04:10
98-06-6
11/21/0704:10,
56-23-5
11/21/07 04:10
108-90-7
11/21/07 04:10
75-00-3
11/21/07 04:10
67-66-3
11/21/07 04:10
74-87-3
11/21/07 04:10
95-49-8
11/21/07 04:10
106-43-4
11/21/07 04:10
96-12-8
11/21/07 04:10
124-48-1
11121 /07 04:10
106-93-4
11/21/07 04:10
74-95-3
11121 /07 04:10
95-50-1
11/21/07 04:10
541-73-1
11/21/07 04:10
106-46-7
11/21/07 04:10
75-71-8
'11/21/07 04:10
75-34-3
11/21/07 04:10
107-06-2
11/21/07 04:10
75-35A
11/21/07 14:55
156-59-2
11/21/07 04:10
156-60-5
11/21/07 04:10
78-87-5
11/21/07 041:10
142-28-9
11/21/07 04:10
594-20-7
11/21/07 04.10
563-58-6
11/21/07 04:10
10061-01-5
11/21/07 04:10
10061-02-6
11/21/07 04:10
108-20-3
11/21/07 04:10
100-41-4
11/21/07 04:10,
87-68-3
11/21/07 04:10
98-82-8
11/21/07 04:10
99-87-6
11/21/07 04:10
75-09-2
11/21/07 04:10
1634-04-4
11/21/07 04:10
91-20-3
11/21/07 04:10
103-65-1
Page 7 of 31

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
q,,aa�iI ® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
lwww.pacelabsxom ar'e/'UlAsheville, NC 28804 Huntersville, NC 28078
.com
I
[phone] [phone]
ANALYTICAL RESULTS
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Sample: MW-5 Lab ID: 927698003 Collected: 11/13/07 13:53 Received: 11/13/07 15:54 Matrix: Water
Parameters Results. Units Report Limit DF Prepared Analyzed CAS No. Qual
6210 MSV,
Styrene
1,1,1,2-Tetrachloroetha ne
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1 -Trichloroetha ne
1,1, 2-Trichl oroetha ne
Trichloroethene
Trichlorofluorometha ne
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1, 3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
1,2-Dichloroethane-d4 (S)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
5310B TOC
Total Organic Carbon
ASTM D516-9002 Sulfate Water
Sulfate
Date: 12/04/2007 09:28 AM
Analytical Method: SM 6210
ND ug/L
ND ug/L
ND ug/L
1150 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
217 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
3.4 ug/L
ND ug/L
ND ug/L
95 % `
101 %
98 %
96 %
Analytical Method: SM 2540C
112 mg/L
Analytical Method: EPA 350.1
ND mg/L
Analytical Method: EPA 353.2
0.25 mg/L
Analytical Method: SM 4500-CI-E
41.3 mg/L
Analytical Method: SM 5310B
4.2 mg/L
Analytical Method: ASTM D516-90,02
ND mg/L
0.50
1
11/21/07 04:10
100-42-5
0.50
1
11/21/07 04:10
630-20-6 .
0.50
1
11/21/07 04:10
79-34-5
10.0
20
11/21/0714:55
127-18-4
0.50
1
11/21/07 04:1.0
108-88-3
2.0
1
11/21/07 04:10
87-61-6
2.0
1
11/21/07 04:10
120-82-1
0.50
1
11/21/07 04:10
71-55-6
0.50
1
11/21/07 04:10
79-00-5
10.0
20
11/21/0714:55
79-01-6
1.0
1
11/21/07 04:10
75-69-4
0.50
1
11/21/07 04:10
96-18-4
0.50
1
11/21/07 04:10
95-63-6
0.50
1
11/21/07 04:10
108-67-8
1.0
1
11/21/07 04:10
75-01-4
1.0
1
11/21/07 04:10
1330-20-7
0.50
1
11/21/07 04:10
95-47-6.
60-140
1
11/21/07 04:10
17060-07-0
60-140
1
11/21/07 04:10
1868-53-7
60-140
1
11/21/07 04:10
460-004
60-140
1
11/21/07 04:10
2037-26-5
20.0
1
11/14/07 23:42
0.10
1
11118/0711:30
7764-41-7
0.10
1
11/14/07 07:45
10.0
2
11/17/0715:50
16887-00-6
1.0
1
11 /25/07 10:00
7440-44-0
5.0
1
11/14/07 10:58
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 31

aceAnalytical
+ www.pacetabs.com
i
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Sample: MW-6
Parameters
92210E Fecal Coliform, MPN
Fecal Coliforms, MPN
6210 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromod ichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec -Butyl benzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochlorometha ne
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3 Dichloropropene
traps-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1, 3-butadiene
Isopropyl benzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Date: 12/04/2007 09:28 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 927698004 Collected: 11/13/07 13:09 Received: 11/13/07 15:54 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No.
Analytical Method: SM 9221C/E
3.6 MPN/100mL 1.0 1 11/13/0717:05
Analytical Method: SM 6210
ND ug/L
0.50
1
11/21/07 14:29
71-43-2
ND ug/L
0.50
1
11/21/07 14:29
108-86-1
ND ug/L
0.50
1
11/21/07 14:29
74-97-5
ND ug/L
0.50
1
11/21/07 14:29
75-274
ND ug/L
0.50
1
11/21/0714:29
75-25-2
ND u9/L
1.0
1
11/21/07 14:29
'74-83-9
ND ug/L
0.50
1
11/21/07 14:29
104-51-8
ND ug/L
0.50
1
11/21/07 14:29
135-98-8
ND ug/L
0.50
1
11/21/07 14:29
98-06-6
ND ug/L
0.50
1
11/21/07 14:29
56-23-5
ND ug/L
0.50
1
11/21/07 14:29
108-90-7
ND ug/L
1.0
1
11/21/07 14:29
75-00-3
ND ug/L
0.50
1
11/21/07 14:29
67-66-3
ND ug/L
1.0
1
11/21/07 14:29
74-87-3
ND ug/L
0.50
1
11/21/07 14:29
95-49-8
ND ug/L
0.50
1
11/21/07 14:29
106-43-4
ND ug/L
1.0
1
11/21/07 14:29
96-12-8
ND ug/L
0.50
1
11/21/07 14:29
124-48-1
ND ug/L
0.50
1
11/21/07 14:29
106-93-4
ND ug/L
0.50
1
11/21/07 14:29
74-95-3
ND ug/L
0.50
1
11/21/07 14:29
95-50-1
ND ug/L
0.50
1
11/21/07 14:29
541-73-1
ND ug/L
0.50
1
11/21/07 14:29
106-46-7
ND ug/L
0.50
1
11/21/07 14:29
75-7178
ND ug/L
0.50
1
11/21/07 14:29
75-34-3
ND ug/L
0.50
1
11/21/07 14:29
107-06-2
ND ug/L
0.50
1
11/21/07 14:29
75-35-4
ND ug/L
0.50
1
11/21/07 14:29
156-59-2
ND ug/L
0.50
1
11/21/07 14:29
156-60-5
ND ug/L
0.50
1
11/21/07 14:29
78'-87-5
ND ug/L
0.50
1
11/21/07 14:29
142-28-9
ND ug/L
0.50
1
11/21/07 14:29
594-20-7
ND ug/L
0.50
1
11/21/07 14:29
563-58-6
ND ug/L
0.50
1
11/2110714:29
10061-01-5
ND ug/L
0.50
1
11/21/07 14:29
10061-02-6
ND ug/L
0.50
1
11/21/07 14:29
108-20-3
ND ug/L
0.50
1
11/21/07 14:29
100-41-4
ND ug/L
2.0
1
11/21/07 14:29
87-68-3
ND ug/L
0.50
1
11/2110714:29
98-82-8
ND ug/L
0.50
1
11/2110714:29
99-87-6
ND ug/L
2.0
1
11/21/07 14:29
75-09-2
ND ug/L
0.50
1
11/21/07 14:29
.1634-04A
ND ug/L
2.0
1
11/21/07 14.:29
91-20-3
ND ug/L
0.50
1
11/21/07 14:29
103=65-1
Qual
REPORT OF LABORATORY ANALYSIS Page 9 of 31
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
oRo
r �a

_ aceAnalytical e
t www.pacefabs.com
I -
Project:
Pace Project No.:
Sample: MW-6
6210 MSV
Clement Pappas 2081.01
927698
Parameters
Styrene
1,1,1,2-Tetra chloroetha ne
1,1,2,2=Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1 Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometha ne
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride:
m&p-Xylene
o-Xylene
1',2-Dichloroethane-d4 (S)
Dibromofluoromethane (S)
4-B romofluoro benzene (S)
Toluene-d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
350.1 Ammonia
Nitrogen, Ammonia
3512 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
531013 TOC
Total'Organic Carbon
ASTM D516-9002 Sulfate Water
Sulfate
, Date: 12/04/2007 09:28 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
. [phone]
Lab ID: 927698004 Collected.: 11/13/0.7 13:09
Received: 11/13/07 15:54 Matrix Water
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
Analytical Method: SM 6210
ND ug/L
0.50
1
11/21/07 14:29
100-42-5
ND ug/L
0.50
1'
11/21/07 14:29
630-20-6
ND ug/L
0.50
1
11/21/07 14:29
79-34-5
ND ug/L
0.50
1
11/21/07 14:29
127-18-4
ND ug/L
0.50
1
11/21/07 14:29
108-88-3
ND ug/L
2.0
1
11121/0714:29
87-61-6
ND ug/L
2.0
1
11/21/07 14:29
120-82-1
ND ug/L
0.50
11
11/21/07 14:29
71-55-6
ND ug/L
0.50
1
11/21/0714:29
79-00-5
ND ug/L
0.50
1
11/21/07 14:29
79-01-6
ND ug/L
1.0
1
11/21/07 14:29
75-69-4
ND ug/L
0.50
1
11121/0714:29
96-18-4
ND ug/L
0.50
1
11/21/07 14:29
95-63-6
ND ug/L
0.50
1
11/21/07 14:29
108-67-8
ND ug/L
1.0
1
11/21/07 14:29
.75-01-4
ND ug/L
1.0
1
11/21/07 14:29
1330-20-7
ND ug/L
0.50
1
11/21/07 14:29
95-47-6
93 %
60-140
1
11/21/07 14:29
17060-07-0
100 %
'60-140
1
11121/07.14:29
1868-53-7
98 %
60-140
1
11/2110714:29
460-00-4
98 %
60-140
1
11/21/07 14:29
2037-26-5
Analytical Method: SM 2540C
114 mg/L 20.0 1
Analytical Method: EPA 350.1
0.24 mg/L 0.10 1
Analytical Method: EPA 353.2
0.24 mg/L 0.10 1
Analytical Method: SM 4500-CI-E
10.7 mg/L 5.0 1
Analytical Method: SM 5310B
5.7 mg/L 1.0 1
Analytical Method: ASTM D516-90,02
5.8 mg/L .
5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
N � 4CCq
act.
11/14/07 23:43
11/18/0711:32 7764-41-7
11/14/07 07:52
11 /17/07 15:40 16887-00-6
11/25/0710:00 7440-44-0
11/14/07 10:58 14808-79-8
Page 10 of 31

ace�n4t��l
/
1
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Sample: MW-7 Lab ID: 927698005 Collected: 11/13/07 11:35 Received: 11/13/07 15:54 Matrix. Water '
Parameters Results Units Report Limit DF Prepared Analyzed , CAS No. Qual
92210E Fecal Coliform, MPN
Analytical Method: SM 9221C/E
Fecal Coliforms, MPN
'<1.1 MPN/100ml-
1.0
1
11%13/07 17:05
6210 MSv
Analytical Method: SM 6210
Benzene
ND ug/L
0.50
1
11/21/07 05:21
71-43-2
Bromobenzene
ND ug/L
0.50
1
11/21/07 05:21
108-86-1
Bromochloromethane
ND ug/L
0.50
1
11/21/07 05:21
74-97-5
Bromodichloromethane
ND ug/L
0.50
1
11/21/07 05:21
75-27-4
Bromoform
ND ug/L
0.50
1
11/21/07 05:21
75-25-2
Bromomethane
ND ug/L
1.0
1
11/21/07 05:21
74-83-9
n-Butylbenzene
ND ug/L
0.50
1
11/21/07 05:21
104-51-8
sec -Butyl benzene
ND ug/L
0.50
1
11/21/07 05:21
135-98-8
tert-Butyl benzene
ND ug/L-
0.50
1
11/21/07 05:21
98-06-6
Carbon tetrachloride
ND ug/L
0.50
1
11/21/07 05:21
56-23-5
Chlorobenzene
ND ug/L
0.50
1
11/21/07 05:21
108-90-7
Chloroethane
ND ug/L
1.0
1
11/21/07 05:21
75-00-3
Chloroform
ND ug/L
0.50
1
11/21/07 05:21
67-66-3
Chloromethane
ND ug/L
1.0
1
11/21/07 05:21
74-87-3
2-Chlorotoluene
ND ug/L
0.50
1
11/21/07 05:21
95-49-8
4-Chlorotoluene
ND ug/L
0.50 `
1
11/21/07 05:21
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
1.0
1
11/21/07 05:21
96-12-8
Dibromochloromethane
ND ug/L
0.50
1
11/21/07 05:21
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
0.50
1
11/21/07 05:21
106-93-4
Dibromomethane
ND ug/L
0.50
1
11/21/07 05:21
74-95-3
1,2-Dichlorobenzene
ND ug/L
0.50
1
11/21/07 05:21
95-50-1
1,3-Dichlorobenzene
ND ug/L
0.50
1
11/21/07 05:21
541-73-1
1,4-Dichlorobenzene
ND ug/L
0.50
1
11/21/07 05:21
106-46-7
Dichlorodifluoromethane
ND ug/L
0.50
1
11/21/07 05:21
75-71-8
1,1-Dichloroethane
ND ug/L'
0.50
1
11/21/07 05:21
75-34-3
1,2-Dichloroethane
ND ug/L
0.50
A
11/21/07 05:21
107-06-2
1,1-Dichloroethene
ND ug/L
0.50
1
11/21/07 05:21
75-354
cis-1,2-Dichloroethene
ND ug/L
0.50
1
11/21/07 05:21
156-59-2
trans-1,2-Dichloroethene
ND ug/L
0.50
1
11/21/07 05:21
156-60-5
1,2-Dichloropropane
ND ug/L
0.50
1
11/21/07 05:21
78-87-5
1,3-Dichloropropane
ND ug/L
0.50
1
11/21/07 05:21
142-28-9
2,2-Dichloropropane
ND ug/L
0.50
1
11/21/07 05:21
594-20-7
1,1-Dichloropropene
ND ug/L
0.50
1
11/21/07 05:21
563-58-6
cis-1,3-Dichloropropene
ND ug/L
0.50
1
11/21/07 05:21
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
0.50
1
11/21/07 05:21
10061-02-6
Diisopropyl ether
ND ug/L
0.50
1
11/21/07 05:21
108-20-3
Ethylbenzene
ND ug/L
0.50
1
11/21/07 05:21
100-41-4
Hexachloro-1,3-butadiene
ND ug/L.
2.0
1
11/21/07 05:21
87-68-3
Isopropylbenzene (Cumene)
ND ug/L
0.50
1
11/21/07 05:21
98-82-8
p-Isopropyltoluene
ND ug/L.
0.50
1
11/21/07 05:21
99-87-6
Methylene Chloride
ND ug/L
2.0
1
11/21/07 05:21
75-09-2
Methyl-tert-butyl ether
ND ug/L
0.50
1
11/21/07 05:21
1634-04-4
Naphthalene
ND ug/L
2.0
1
11/21/07 05:21
91-20-3
n-Propylbenzene
ND ug/L
0.50
1
11/21/07 05:21
103-65-1
Date:12/04/2007 09:28 AM
REPORT OF LABORATORY
ANALYSIS
Page 11 of 31
This report shall
not be reproduced, except in full,
.without the written consent of Pace Analytical
Services, Inc..
ACCCq

aceAnalytical
www.pacela6s.com
1 / y
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Sample: MW-7 Lab ID: 927698005 Collected: 11/13/07 11:35 Received: 11/13/07 15:54 Matrix: Water
Parameters
6210 MSV
Styrene
1,1,1,2-Tetrachloroetha ne
1,1,2,2-Tetrachloroetha ne
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzehe
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropa ne
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
1,2-Dichloroethane-d4 (S)
Dibromofluorom ethane (S)
4-Bromofluorobenzene (S)
Toluene=d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
5310E TOC
Total Organic Carbon
ASTM D516-9002 Sulfate Water
Sulfate
Date: 12/04/2007 09:28 AM
Results Units Report Limit - OF Prepared Analyzed CAS No. Qual
Analytical Method: SM 6210
NO ug/L
0.50
1
11/21/07 05:21
100-42-5
NO ug/L
0.50
1
11/21/07 05:21
630-20-6
ND ug/L
0.50
1
11/21/07 05:21
79-34-5
NO ug/L
0.50
1
11/21/07 05:21
127-18-4
NO ug/L
0.50
1
11/21/07 05:21
108-88-3
NO ug/L
2.0
1
11/21/07 05:21
87-61-6
NO. ug/L
2.0
1
11/21/07 05:21
120-82-1
NO ug/L
0.50
1
11/21/07 05:21
71-55-6
NO ug/L
0.50
1
11/21/07 05:21.
79-00-5
NO ug/L
0.50
1
11/21/07 05:21
79-01-6
NO ug/L
1.0
1
11/21/07 05:21
75-69-4
ND ug/L
0.50
1
11/21/07 05:21
96-18-4
ND ug/L
0.50
1
11/21/07 05:21
95-63-6
NO ug/L
0.50
1
11/21/07 05:21
108-67-8
NO ug/L
1.0
1
11/21/07 05:21
75-01-4
NO ug/L
1.0
1
11/21/07 05:21
1330-20-7
NO ug/L
0.50
1
11/21/07 05:21
95-47-6
95 %
60-140
1
11/21/07 05:21
17060-07-0
101 %
60-140
1
11/21/07 05:21
1868-53-7
97 %
60-140
1
11/21/07 05:21
460-00-4
98 %
60-140
1
11/21/07 05:21
2037-26-5
Analytical Method: SM 2540C
42.0 mg/L
20.0 1
Analytical Method: EPA 350.1
NO mg/L
0.10 1
Analytical Method: EPA 353.2
1.7 mg/L
0.10 1
Analytical Method: SM 4500-CI-E
6.8 mg/L
5.0 1
Analytical Method: SM 5310B
4.2 mg/L
1.0 1
Analytical Method`. ASTM D516-90,02
NO mg/L
5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
ACC,
11 /14/0123:44
11/18/0711:34 7764-41-7
11/14/07 07:52
11 / 17/07 15:40 16887-0 0-6
11/25/0710:00 7440-44-0
11 /14/0710:58 14808-79-8
Page 12 of 31

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
®
aceAnalytical 2226 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville, NC 28804 Huntersville, NC 28078
2� www.pacelabs.com
ti (828)2547176. [phone]
ANALYTICAL RESULTS
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Sample: MW-8
Parameters
Lab ID: 927698006 Collected:' 11/13/07 10:51
Results Units Report Limit DF
Received: 11/13/07 15:54 Matrix: Water
Prepared Analyzed CAS No. Qua[
92210E Fecal Coliform, MPN
Analytical Method: SM 9221C/E
Fecal Coliforms, MPN
<1.1 MPN/100ml-
1.0
1
11/13/07 17:05
6210 MSV
Analytical Method: SM 6210
Benzene
ND ug/L
0.50
1
11/21/07 05:45
71-43-2
Bromobenzene
ND ug/L
0.50
1
11/21/07 05:45
108-86-1
Bromochloromethane
ND ug/L
0.50
1
11/21/07 05:45
74-97-5
Bromodichloromethane
ND ug/L
0.50
1
11/21/07 05:45
75-27-4
Bromoform
ND ug/L
0.50
1
11/21/07 05:45
75-25-2
Bromomethane
ND ug/L
1.0
1
11/21/07 05:45
74-83-9
n-Butylbenzene
ND ug/L
0.50
1
11/21/07 05:45
104-51-8
sec -Butyl benzene
ND ug/L
0.50
1
11/21/07 05:45
135-98-8
tert-Butyl benzene
ND ug/L
0.50
1
11/21/07 05:45
98-06-6
Carbon tetrachloride
ND ug/L
0.50
1
11/21/07 05:45
56-23-5
Chlorobenzene
ND ug/L
0.50
1
11/21/07 05:45
108-90-7
Chloroethane
ND ug/L
1.0
1
11/21/07 05:45
75-00-3
Chloroform
ND ug/L
0.50
1
11/21/07 05:45,
67-66-3 L
Chloromethane
ND ug/L
1.0
1
11/21/07 05:45
74-87-3 .
2-Chlorotoluene
ND ug/L
0.50
1
11/21/07 05:45
9549-8
4-Chlorotoluene
ND ug/L
0.50
1
11/21/07 05:45
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
1.0
1
11/21/07 05:45
96-12-8
Dibromochloromethane
ND ug/L
0.50
1
11/21/07 05:45
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
0.50.
1
11/21/07 05:45
106-93-4
Dibromomethane
ND ug/L
0.50
1
11/21/07 05:45
74-95-3
1,2-Dichlorobenzene
ND ug/L
0.50
1
11/21/07 05:45
95-50-1
1,3-Dichlorobenzene
ND ug/L
0.50
1
11/21/07 05:45
541-73-1
1,4-Dichlorobenzene
ND ug/L
0.50
1
1-1/21/07 05:45
106-46-7
Dichlorodifluoromethane
ND ug/L
0.50
1
11/21/07 05:45
75-71-8
1,1-Dichloroethane
ND ug/L
0.50
1
11/21/07 05:45
75-34-3
1,2-Dichloroethane
ND ug/L
0,50
1
11/21/07 05:45
107-06-2
1,1-Dichloroethene
ND ug/L
0.50
1
11/21/07 05:45
75-35-4
cis-1,2-Dichloroethene
ND ug/L
0.50
1
11/21/07 05:45
156-59-2
trans-1,2-Dichloroethene
ND ug/L
0.50
1
11/21/07 05:45
156-60-5
1,2-Dichloropropane
ND ug/L
0.50
1
11/21/07 05:45
78-87-5
1,3-Dichloropropane
ND ug/L
0.50
1
11/21/07 05:45
142-28-9
2,2-Dichloropropane
ND ug/L
0.50
1
11/21/07 05:45
594-20-7
1,1-Dichloropropene
ND ug/L
0.50
1
11/21/07 05:45
563-58-6
cis-1,3-Dichloropropene
'ND ug/L
0.50
1
11/21/07-05:45
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
0.50
1
11/21/07 05:45
10061-02-6
Diisopropyl ether
ND ug/L
0.50
1
11/21/07 05:45
108-20-3
Ethylbenzene
ND ug/L
0.50
1
11/21/07 05:45
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
2.0
1
11/21/07 05:45
87-68-3
Isopropylbenzene (Cumene)
ND ug/L
0.50
1
11/21/07 05:45
98-82-8
p-Isopropyltoluene
ND ug/L
0.50
1
11/21/07 05:45
99-87-6
Methylene Chloride
ND ug/L '
2.0
1
11/21/07 05:45
75-09-2
Methyl-tert-butyl ether
ND ug/L
0.50
1
11/21/07 05:45
1634-04-4
Naphthalene
ND ug/L
2.0
1
11/21/07 05:45
91-20-3
n-Propy►benzene
ND 41-
0.50
1
11/21/07 05:45
103-65-1
Date:12/04/2007 09:28 AM I I REPORT OF LABORATORY ANALYSIS Page 13 of 31
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
•CCCq�+
fief =

aOAnalytical
.www.pacera6s.eom
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-8 Lab ID: 927698006 Collected: 11/13/07 10:51 Received: 11/13/07 15:54 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6210 MSV
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3 Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
1,2-Dichloroethane-d4 (S)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
5310E TOC
Total Organic Carbon
ASTM D516-9002 Sulfate Water
Sulfate
Date: 12/04/2007 09:28 AM
Analytical Method: SM 6210
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L !
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
96 %
102 %
97 %
97 %
Analytical Method: SM 2540C
154 mg/L
Analytical Method: EPA 350.1
ND mg/L
Analytical Method: EPA 353.2
0.97 mg/L
Analytical Method: SM 4500-CI-E
19.6 mg/L
Analytical Method: SM 5310B
8.3 mg/L
Analytical Method: ASTM D516-90,02
26.6 mg/L
0.50
1
11/21/07 05:45
100-42-5
0.50
1
11/21/07 05:45
630-20-6
0.50
1
11/21/07 05:45
79-34-5
0.50
1
11/21/07 05:45
127-18-4
0.50
1
11/21/07 05:45
108-88-3
2.0
1
11/21/07 05:45
87-61-6
2.0
1
11/21/07 05:45
120-82-1
0.50
1
11/21/07 05:45
71-55-6
0.50
1
11/21/07 05:45
79-00-5
0.50
1
11/21/07 05:45
79-01-6
1.0
1
11/21/07 05:45
75-69-4
0.50
1
11/21/07 05:45
96-184
0.50.
1
11/21/07 05:45
95-63-6
0.50
1
11/21/07 05:45
108-67-8
1.0 ,
1
11/21/07 05:45
75-01-4
1.0
1
11/21/07 05:45
1330-20-7
0.50
1
11/21/07 05:45
9547-6
60-140
1
11/21/07 05:45
17060-07-0
60-140
1
11/21/07 05:45
1868-53-7
60-140
1
11/21/07 05:45
460-00-4
60-140
1
11/21/07 05:45
2037-26-5
20.0 1
0.10 . 1
0.10 1
5.0 1
1.0 1
5.0, 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
.«a„o
'elac
11/14/07 23:47
11/18/0711:35 7764-41-7
11/14/07 07:52
11 /17/07 15:40 16887-00-6
11125/0710:00 7440-44-0
11 /16/07 15:37 14808-79-8
Page 14 of 31

aceAnalytical
-www.pacelabs.com
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Pace Analytical Services, Inc.
2225 Riverside Dr. -
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/1581 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 927698002, 927698003
METHOD BLANK: 40118
Associated Lab Samples: 927698002, 927698003
Blank Reporting
Parameter Units Result Limit Qualifiers
Nitrogen, Nitrate mg/L ND 0.10
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
40119
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Nitrogen, Nitrate
mg/L
5 5.4
107
90-110
MATRIX SPIKE SAMPLE:
40120
927609001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Nitrogen, Nitrate
mg/L
ND 5
5.6
111
75-125
Date: 12/04/2007 09:28 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc:.
tCi •CChH \Np
h'eh
Page 15 of 31

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aceAnalytical
Asheville, NC 28804 Huntersville, NC 28078
! +www.pacelabs.com
[phone] [phone]
QUALITY CONTROL DATA
Project: Clement Pappas 2081.01
Pace Project No.: 927698
QC Batch: WETA/1589
Analysis Method:
EPA 353.2
QC Batch Method: EPA 353.2
Analysis Description:
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 927698001, 927698004, 927698005, 927698006
METHOD BLANK: 40698
Associated Lab Samples: 927698001, 927698004, 927698005, 927698006
Blank Reporting
Parameter Units
Result Limit
Qualifiers
Nitrogen, Nitrate mg/L
ND 0.10
LABORATORY CONTROL SAMPLE: 40699
Spike' LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Nitrogen, Nitrate mg/L
5 5.3
106 90-110
MATRIX SPIKE SAMPLE:
Parameter
40700
Units
927673010
Result
Spike MS MS % Rec
Cone. Result % Rec Limits Qualifiers
Nitrogen, Nitrate
mg/L
2.6
5 8.0 108 75-125
SAMPLE DUPLICATE: 40702
927628002
Dup
Parameter
Units
Result
Result RPD Qualifiers
Nitrogen, Nitrate
mg/L
ND
NO 0
Date: 12/04/2007 09:28 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 31

aceAnalyfical
• www.pacelabs.com
1 � .
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/1591 Analysis Method: ASTM D516-90,02
QC Batch Method: ASTM D516-90,02 Analysis Description: ASTM D516-9002 Sulfate Water
Associated Lab Samples: 927698001, 927698002, 927698003, 927698004, 927698005
METHOD BLANK: 40810
Associated Lab Samples: 927698001, 927698002, 927698003, 927698004, 927698005
Blank Reporting
Parameter Units Result Limit Qualifiers -
Sulfate mg/L ND 5.0
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
40811
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Sulfate
mg/L
20
19.8
99
90-110
MATRIX SPIKE SAMPLE:
40812
927518001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Sulfate
mg/L
ND 20
20.8
106
75-125
SAMPLE DUPLICATE: 40813
927518002
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Sulfate
mg/L
8.7
8.7
.2
Date: 12/04/2007 09:28 AM REPORT OF LABORATORY ANALYSIS Page 17 of 31
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
ACCpgO\y
a

'7;aceAnaiytical
a w www.pacela6s.com
1
f
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WET/2093 Analysis Method: SM 2540C
QC Batch Method: SM 2540C Analysis Description: 2540C Total Dissolved Solids
Associated Lab Samples: 927698001, 927698002, 927698003, 927698004, 927698005, 927698006
METHOD BLANK: 41565
Associated Lab Samples: 927698001, 927698002, 927698003, 927698004, 927698005, 927698006
Blank Reporting
Parameter Units Result Limit Qualifiers
Total Dissolved Solids mg/L ND 20.0
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 41566
Spike LCS LCS % Rec
Parameter Units Conc. - Result % Rec. Limits Qualifiers
Total Dissolved Solids mg/L 250 188 75 80-120 LO
SAMPLE DUPLICATE: 41567
Parameter
Total Dissolved Solids
Date: 12/04/2007 09:28 AM
927442001 Dup
Units Result Result
mg/L 226 222
RPD Qualifiers
2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
•CCpgq
�heh
Page 18 of 31

aceAnalytical
..wwwpacelabs.com
Project: Clement Pappas 2081.01
Pace Project No.: 927698
QC Batch: WETA/1612
QC Batch Method: ASTM D516-90,02
Associated Lab Samples: 927698006
METHOD BLANK: 42399
Associated Lab Samples: 927698006
Parameter Units
mg/L
Sulfate
LABORATORY CONTROL SAMPLE: 42400
Parameter Units
Sulfate mg/L
MATRIX SPIKE SAMPLE: 42401
Parameter Units
Sulfate mg/L
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: ASTM D516-90,02
Analysis Description: ASTM.D516-9002 Sulfate Water
Blank Reporting
Result Limit Qualifiers
ND 5.0
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
20 20.2 101 90-110
927767001 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 20 22.5 115 75-125
SAMPLE DUPLICATE: 42402
927767002 Dup
Parameter Units Result Result RPD
Sulfate mg/L ND ND
Date: 12/04/2007 09:28 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
M •��Oq
(LI_eh
Qualifiers
Page 19 of 31

aceAnalytical
�www.pace/a6s.com
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/1617 Analysis Method: SM 4500-CI-E
QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride
Associated Lab Samples: 927698001, 927698002, 927698003, 927698004, 927698005, 927698006
METHOD BLANK: 43067
Associated Lab Samples: 927698001, 927698002, 927698003, 927698004, 927698005, 927698006
Blank Reporting
Parameter Units Result Limit Qualifiers
Chloride mg/L ND 5.0
LABORATORY CONTROL SAMPLE: 43068
Parameter Units
Chloride mg/L
MATRIX SPIKE SAMPLE: 43069
Parameter Units
Chloride mg/L
SAMPLE DUPLICATE: 43070
Parameter
Chloride
Date: 12/04/2007 09:28 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
20 21.3 107 90-110
927809001 Spike MS MS % Rec
Result Cone. Result % Rec Limits Qualifiers
6.1 20 27.2 106 75-125
927809002 Dup
Units Result Result
mg/L 52.9 53.6
RPD Qualifiers
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
•CC^qC
Page 20 of 31

aeeAnalytical
.www.pacelabs.com
Project Clement Pappas 2081.01
Pace Project No.: 927698 -
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/1621 Analysis Method: EPA 350.1
QC Batch Method: EPA 350.1 Analysis Description:. 350.1 Ammonia
Associated Lab Samples: 927698001, 9276980012
METHOD BLANK: 43119
Associated Lab Samples: 927698001, 927698002
Parameter Units
Nitrogen, Ammonia mg/L
LABORATORY CONTROL SAMPLE: 43120
Parameter Units
Nitrogen, Ammonia mg/L
Blank Reporting
Result Limit Qualifiers
ND 0.10
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
5 4.8 97 90-110
.MATRIX SPIKE.SAMPLE: 43121
928075002 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/L ND 5 5.1 102 75-125
SAMPLE DUPLICATE: 43122
927195001 Dup
Parameter Units Result Result RPD Qualifiers
Nitrogen, Ammonia mg/L 14.6 14.5 .5
Date: 12/04/2007 09:28 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
1`0
Page 21 of 31

aoAnalytical
t www.pecolabs.com
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/1622 Analysis Method: EPA 350.1
QC Batch Method: EPA 350.1 Analysis Description: 350.1 Ammonia
Associated Lab Samples: 927698003, 927698004, 927698005, 927698006
METHOD BLANK: 43123
Associated Lab Samples: 927698003, 927698004, 927698005, 927698006
Blank Reporting
Parameter Units Result Limit Qualifiers
Nitrogen, Ammonia mg/L ND 0.10
LABORATORY CONTROL SAMPLE:
43124
Parameter
Units
Nitrogen, Ammonia
mg/L
MATRIX SPIKE SAMPLE:
43125
Parameter
Units
Nitrogen, Ammonia
mg/L
SAMPLE DUPLICATE: 43126
Parameter
Nitrogen, Ammonia
Date: 12/04/2007 09:28 AM
Spike LCS LCS
Conc. Result % Rec
5 5.2 105
927698003 Spike MS
Result Conc. Result
ND 5 5.2
927698004 Dup
Units Result Result
mg/L 0.24 0.24
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
90-110
MS % Rec
% Rec Limits Qualifiers
105 75-125
RPD Qualifiers
.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
M •�COq
06
Page 22 of 31

aceAnalyticai
. www.pacelabs.com
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: . MBIO/1361 Analysis Method: SM 9221C/E
QC Batch Method: SM 9221C/E Analysis Description: 92210E Fecal Coliform, MPN
Associated Lab Samples: 927698001, 927698002, 927698003, 927698004, 927698005, 927698006
METHOD BLANK: 43387
Associated Lab Samples: 927698001, 927698002, 927698003, 927698004, 927698005, 927698006
Blank Reporting
Parameter Units Result Limit Qualifiers
Fecal Coliforms, MPN MPN/100rk negative 1.0
Date: 12/04/2007 09:28 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
pp.�ago'
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 31

;aceAnaljftal"
.--7
Vwww.pacelabs:com
Project: Clement Pappas 2081.01
Pace Project No.: 927698
QC Batch: MSW1852
QC Batch Method: SM 6210
Associated Lab Samples: 927698001
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 6210
Analysis Description: 6210 MSV
METHOD BLANK: 43746
Associated Lab Samples: 927698001
Blank
Reporting
Parameter
Units
Result
Limit Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
1,1,1-Trichloroethane
ug/L
ND
0.50
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
1,1,2-Trichloroethane
ug/L
ND
0.50
1,1-Dichloroethane
ug/L
ND
0.50
1,1-Dichloroethene
ug/L
ND
0.50
1,1-Dichloropropene
ug/L
ND
0.50
1,2,3-Trichlorobenzene
ug/L
ND
2.0
1,2,3-Trichloropropane
ug/L
ND
0.50
1,2,4-Trichlorobenzene
ug/L
ND
2.0
1,2,4-Trimethylbenzene
ug/L
ND
0.50
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
1,2-Dichlorobenzene
ug/L
ND
0.50
1,2-Dichloroethane
ug/L
ND
0.50
1,2-Dichloropropane
ug/L
ND
0.50
1,3,5-Trimethylbenzene
ug/L
ND
0.50
1,3-Dichlorobenzene
ug/L
ND
0.50
1,3-Dichloropropane
ug/L
ND
0.50
1,4-Dichlorobenzene
ug/L
ND
0.50
2,2-Dichloropropane
ug/L
ND
0.50
2-Chlorotoluene
ug/L
ND
0.50
4-Chlorotoluene
ug/L
ND
0.50
Benzene
ug/L
ND
0.50
Bromobenzene
ug/L
ND
0.50
Bromochloromethane
ug/L
ND
0.50
Bromodichloromethane
ug/L
ND
0.50
Bromoform
ug/L
ND
0.50
Bromomethane
ug/L
ND
1.0
Carbon tetrachloride
ug/L
ND
0.50
Chlorobenzene
ug/L
ND
0.50
Chloroethane
ug/L
ND
1.0
Chloroform
ug/L
ND
0.50
Chloromethane
ug/L
ND
1.0
cis-1,2-Dichloroethene
ug/L
ND
0.50
cis-1,3-Dichloropropene
ug/L
ND
0.50
Dibromochloromethane
ug/L
ND
0.50
Dibromomethane
ug/L
ND
0.50
Dichlorodifluoromethane
ug/L
ND
0.50
Diisopropyl ether
ug/L
ND
0.50
Ethylberizene
ug/L
ND
0.50
Hexachloro-1,3-butadiene•
ug/L
ND
2.0
Isopropylbenzene (Cumene)
ug/L
ND
0.50
Date: 12/04/2007 09:28 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
C;CpgO,
fl.\/j�.,i�� z
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 31

aceAnalXical
• www.pacelabs.com
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
METHOD BLANK: 43746
Associated Lab Samples:
Parameter
927698001
Units
Blank
Result
Reporting
Limit
m&p-Xylene
ug/L
ND
1.0
Methyl-tert-butyl ether
ug/L
ND
0.50
Methylene Chloride
ug/L
ND
2.0
n-Butylbenzene
ug/L
ND
0.50
n-Propylbenzene
ug/L
ND
0.50
Naphthalene
ug/L
ND
2.0
o-Xylene
ug/L
ND
0.50
p-Isopropyltoluene
ug/L
ND
0.50
sec -Butyl benzene
ug/L
ND
0.50
Styrene
ug/L
ND
0.50
tert-B utyl benzene
ug/L
ND
0.50
Tetrachloroethene
ug/L
ND
0.50
Toluene
ug/L
ND
0.50
trans-1,2-Dichloroethene
ug/L
ND
0.50
trans-1,3-Dichloropropene
ug/L
ND
0.50
Trichloroethene
ug/L
ND
0.50
Trichlorofluoromethane
ug/L
ND
1.0
Vinyl chloride
ug/L
ND
1.0
1,2-Dichloroethane-d4 (S)
%
94
60-140
4-Bromofluorobenzene (S)
%
98
60-140
Dibromofluoromethane (S)
%
100
60-140
TolueneA8 (S)
%
97
60-140
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 43747
Parameter Units
Spike
Conc.
43748
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
10
11.2
10.8
112
108
60-140
4
30
1,1,1-Trichloroethane .
ug/L
10
10.6
10.5
106
105
60-140-
.7
30
1,1,2,2-Tetrachloroethane
ug/L
10
9.9
9.5
99
95
60-140
4
30
1,1,2-Trichloroethane
ug/L
10
10.1
10.1
101
101
60-140
.02
30
1,1-Dichloroethane
ug/L
10
10.5
10.5
105
105
60-140
.08
30
1,1-Dichloroethene
ug/L
10
12.2
12.0
122
120
60-140
2
30
1,1-Dichloropropene
ug/L
10
10.4
10.2
104
102
60-140
2
30
1,2,3-Trichlorobenzene
ug/L
10
10.6
10.5
106
105
60-140
.7
30
1,2,3-Trichloropropane
ug/L
10
10.4
10.6
104
106
60-140
2
30
1,2,4-Trichlorobenzene
ug/L
10
10.5
10.4
105
104
60-140
2
30
1,2,4-Trimethylbenzene
ug/L
10
10.9
10.8
109
108
60-140
.8
30
1,2-Dibromo-3-chloropropane
ug/L
10
8:8
8.5
88
85
60-140
3
30
1,2-Dibromoethane (EDB)
ug/L
10
10.5
10.3
105
103
60-140
2
30
1,2-Dichlorobenzene
ug/L
10
10.8
10.6
108
106
60-140
2
30
1,2-Dichloroethane
ug/L
10
9.4
9.7
94
97
60-140
3
30
1,2-Dichloropropane
ug/L
10
10.4
10.3
104
103
60-140
.8
30
1,3,5-Trimethylbenzene
ug/L
10
11.0
10.9
' 110
109
60-140
.5
30
1,3-Dichlorobenzene
ug/L
10
10.4
10.3
104
103
607140
.5
30
1,3-Dichloropropane
ug/L
10
10.7
10.5
107
105
60-140
2
30
Date: 12/04/2007 09:28 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
♦CCCq
Page 25 of 31

aceAnalytical
gwww.pacetab&com
Project: Clement Pappas 2081.01
Pace Project No.: 927698
LABORATORY CONTROL SAMPLE & LCSD: 43747
Parameter
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
B romod ihloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1, 2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorod ifluorometha ne
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
m&p-Xylene
Methyl-tert-butyl ether
Methylene Chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
p-Isopropyltoluene
sec -Butyl benzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluorom etha ne
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
Date: 12/04/2007 09:28 AM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike
Units Conc.
43748
LCS LCSD
Result Result
ug/L
10
10.5
10.5
ug/L
10
11.1
11.0
ug/L
-10
10.4
10.5
ug/L
10
10.4
10.2
ug/L
10
10.2
10.3
ug/L
10,
10.2
10.3
ug/L
10
11.5
11.6
ug/L
10
10.2
10.1
ug/L
10
10
9.9
ug/L
10
16.0
15.8
ug/L
10
11.6
11.5
ug/L
10
11.4
11.3
ug/L
10
11.6
11.5
ug/L
10
10.9
11.0
ug/L
10
9.5
9.5
ug/L
10
10.9
10.8
ug/L
10
10.3
10.1
ug/L
10
10.3
10.0
ug/L
10
10.6
10.8
ug/L
10
12.8
12.9
ug/L
10
9.9
10.0
ug/L
10
11.0
10.8
ug/L
10
9.0
9.0
ug/L
10
11.2
11.0
ug/L
20
21.5
21.1
ug/L
10
9.8
10
ug/L
10
9.4
9.3
ug/L
10
11.1
10.8
ug/L
10
10.8
10.7
ug/L
10
12.6
12.2
ug/L
10
10.6
10.3
ug/L
10
11.1
11.1
ug/L
10
10.8
10.7
ug/L
10
11.0
10.7
ug/L
10
10.9
10.4
ug/L
10
11.1
10.9
ug/L
10
9.9
9.9
ug/L
10
10.5
10.6
ug/L
10
9.9
9.9
ug/L
10
10.8
10.7
ug/L
10
11.4
11.5
ug/L
10
11.2
11.2
LCS LCSD
% Rec % Rec
105 105
111 110
104 105
104 102
102 103
102 103
115 116
102 101
100 99
160 158
116 115
114 113
116 115
109 110
95 95
109 108
103 101
103 100
106 108
128 129
99 100
110 108
90 90
112 110
108 106
98 100
94 93
111 108
108 107
126 122
106 103
111 111
108 107
110 107
'109 104
111 109
99 99
105 106
99 99
108 107
114 115
112 112
94 95
99 97
101 102
98 98
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
•GGpgp'
% Rec
Limits
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
. 60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
RPD
.8
.9
.6
2
.9
2
1
.9
1
1
2
2
.9
.5
.6
1
2
3
1
.6
1
2
.2
2
2
2
2
2
.9
4
2
.6
.9
2
4
1
.2
.6
.4
.7
1
.05
Max
RPD Qualifiers
30
30
30
30
30
30
30
30
30
30 L3
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Page 26 of 31

�;a'OAnalytical
/ 7.vwwpacelabs.com
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/1853 Analysis Method: SM 6210
QC Batch Method: SM 6210 Analysis Description: 6210 MSV
Associated Lab.Samples: 927698002, 927698003, 927698004, 927698005, 927698006
METHOD BLANK: 43749
Associated Lab Samples: 927698002, 927698003, 927698004, 927698005,
927698006
Blank
Reporting
Parameter
Units
Result
Limit Qualifiers
1,1,1,2-Tetrachl6roethane
ug/L
ND
0.50
1,1,1-Trichloroethane
ug/L
ND
0.50
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
1,1,2 Trichloroethane
ug/L
ND
0.50
1,1-Dichloroethane
ug/L
ND
0.50
1,1-Dichloroethene
ug/L
ND
0.50
1,1-Dichloropropene
ug/L
ND
0.50
1,2,3-Trichlorobenzene
ug/L
ND
2.0
1,2,3-Trichloropropane
ug/L
ND
0.50
1,2,4-Trichlorobenzene
ug/L
ND
2.0
1,2,4-Trimethylbenzene
ug/L
ND
0.50
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
1,2-Dichlorobenzene
ug/L
ND
0.50
1,2-Dichloroethane
ug/L
ND
0.50
1,2-Dichloropropane
ug/L
ND
0.50
1,3,5-Trimethylbenzene
ug/L
ND
0.50
1,3-Dichlorobenzene
ug/L
ND
0.50
1,3-Dichloropropane
ug/L
ND
0.50
1,4-Dichlorobenzene
ug/L
ND
0.50
2,2-Dichloropropane
ug/L
ND
0.50
2-Chlorotoluene
ug/L
ND
0.50
4-Chlorotoluene
ug/L
ND
0.50
Benzene
ug/L
ND
0.50
Bromobenzene
ug/L
ND
0.50
Bromochloromethane
ug/L
ND
0.50
Bromodichloromethane
ug/L
ND
0.50
Bromoform
ug/L
ND
0.50
Bromomethane
ug/L
ND
1.0
Carbon tetrachloride
ug/L
ND
0.50
Chlorobenzene
ug/L
ND
0.50
Chloroethane
ug/L
ND
1.0
Chloroform
ug/L
ND
0.50
Chloromethane
ug/L
ND
1.0
cis-1,2-Dichloroethene
ug/L
ND
0.50
cis-1,3-Dichloropro pene
ug/L
ND
0.50
Dibromochloromethane
ug/L
ND
0.50
Dibromomethane
ug/L
ND
0.50
Dichlorodifluoromethane
ug/L
ND
0.50
Diisopropyl ether
ug/L
ND
0.50
Ethylbenzene
ug/L
ND
0.50
Hexachloro-1,3-butadiene
ug/L
ND
2.0.
Isopropyl benzene (Cumene)
ug/L
ND
0.50
Date:12/04/2007 09:28 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
h �CCOgq+
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 31

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
ICZI
/�,, / ® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
e/'U JCaI Asheville, NC 28804 Huntersville, NC 28078
7www.pacefa6scom
[phone] [phone]
QUALITY CONTROL DATA
Project: Clement Pappas 2081.01
Pace Project No.: 927698
METHOD BLANK: 43749
Associated Lab Samples: 927698002, 927698003, 927698004, 927698005, 927698006
Blank
Reporting
Parameter
Units
Result
Limit
Qualifiers
m&p-Xylene
ug/L
ND
1.0
Methyl-tert-butyl ether
ug/L
ND
0.50
Methylene Chloride
ug/L
ND
2.0
n-Butylbenzene
ug/L
ND
0.50
n-Propylbenzene
ug/L
ND
•
0.50
Naphthalene
ug/L
ND
2.0
o-Xylene
ug/L
ND
0.50
p-Isopropyltoluene
ug/L
ND
0.50
sec-Butylbenzene
ug/L
ND
0.50
Styrene
ug/L
ND
0.50
tert-Butyl benzene
ug/L
ND
0.50
Tetrachloroethene
ug/L
ND
0.50
Toluene
ug/L
ND
0.50
trans-1,2-Dichloroethene
ug/L
ND
0.50
trans-1,3-Dichloropropene
ug/L
ND
0.50
Trichloroethene
ug/L
ND
0.50
Trichlorofluoromethane
ug/L
ND
1.0
Vinyl chloride
ug/L
ND
1.0
1,2-Dichloroethane-d4 (S)
%
93
60-140
4-Bromofluorobenzene (S)
%
97
60-140
Dibromofluoromethane (S)
%
99
60-140
Toluene-d8 (S)
%
97
60-140
LABORATORY CONTROL SAMPLE & LCSD: 43750
43751
Spike
LCS
LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
10
10.7
10.7
107
107
60-140
.3
30
1,1,1-Trichloroethane
ug/L
10
10.3
10.4
103
104
60-140
.2
30
1,1,2,2-Tetrachloroethane
ug/L
10
9.6
9.7
96
97
60-140
.6
30
1,1,2-Trichloroethane
ug/L
10
10.2
10.1
102
101
60-140
1
30
1,1-Dichloroethane
ug/L
10
10.4
10.5
104
105'
60-140
1
30
1,1-Dichloroethene
ug/L
10
11.9
12.1
119
121
60-140
2
30
1,1-Dichloropropene
ug/L
10
10.2
10.3
102
103
60-140
2
30
1,2,3-Trichlorobenzene
ug/L
10
10.5
10.6
105
106
60-140
.7
30
1,2,3-Trichloropropane
ug/L
10
10
10.6
100
106
60-140
6
30
1,2,4-Trichlorobenzene
ug/L
10
10.3
10.4
103
104
60-140
.6
30
1,2,4-Trimethylbenzene
ug/L
10
10.7
10.8
107
108
60-140
.5
30
1,2-Dibromo-3-chloropropane
ug/L
10
8.8
8.8
88
88
60-140
.4
30
1,2-Dibromoethane (EDB)
ug/L
10
10.2
10.4
102
104
60-140
2
30
1,2-Dichlorobenzene
ug/L
10
10.7
10.6
107
106
60-140
.3
30
1,2-Dichloroethane
ug/L
10
9.5
9.6
95
96
60-140
1
30
1,2-Dichloropropane
ug/L
10
10.2
10.5
102
105
60-140
3
30
1,3,5-Trimethyl benzene
ug/L
10
10.7
10.8
107
108
60-140
.6
30
1,3-Dichlorobenzene
ug/L
10
10.2
10.4
102
104
60-140
2
30
1,3-Dichloropropane
ug/L
10
10.3
10.5
103
105
60-140
1
30
Date: 12/04/2007 09:28 AM REPORT OF LABORATORY ANALYSIS Page 28 of 31
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I
Project: Clement Pappas 2081.01
Pace Project No.: 927698'
LABORATORY CONTROL SAMPLE & LCSD: 43750
Parameter
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville,'NC 28804
[phone]
QUALITY CONTROL DATA
Spike
Units Conc.
43751
LCS LCSD
Result Result
LCS LCSD % Rec
% Rec % Rec Limits
1,4-Dichlorobenzene
ug/L
105
2,2-Dichloropropane
ug/L
108
2-Chlorotoluene
ug/L
103
4-Chlorotoluene
ug/L
102
Benzene
ug/L.
101
Bromobenzene
ug/L
102
Bromochloromethane
ug/L
116
Bromod ichloro methane
ug/L
101
Bromoform
ug/L
99
Bromomethane
ug/L
156
Carbon tetrachloride
ug/L
115
Chlorobenzene
ug/L
111
Chloroethane
ug/L
113
Chloroform
ug/L
108
Chloromethane
ug/L
93
cis-1,2-Dichloroethene
ug/L
107
cis-1,3-Dichloropropene
ug/L
101
Dibromochloromethane
ug/L
101
Dibromomethane
ug/L
105
Dichlorodifluorometha fie
ug/L
125
Diisopropyl ether
ug/L
99
Ethylbenzene
ug/L
106
Hexachloro-1,3-butadiene
ug/L
91
Isopropylbenzene (Cumene)
ug/L
108
m&p-Xylene
ug/L
104
Methyl-tert-butyl ether
ug/L
99
Methylene Chloride
ug/L
92
n-Butylbenzene
ug/L
108
n-Propylbenzene
ug/L
106
Naphthalene
ug/L
124
o-Xylene
ug/L
102
p-Isopropyltoluene
ug/L
110
sec -Butyl benzene
ug/L
106
Styrene
ug/L
106
tert-Butylbenzene
ug/L
103
Tetrachloroethene
ug/L
108
Toluene
ug/L
98
trans-1,2-Dichloroethene
ug/L
104
trans-1,3-Dichloropro pene
ug/L
101
Trichooroethene
ug/L
108
Trichlorofluoromethane
ug/L
112
Vinyl chloride
ug/L
111
1,2-Dichloroethane-d4 (S)
%
95
4-Bromofluorobenzene (S)
%
98
Dibromocuoromethane (S)
%
101
Toluene-d8 (S)
%
98
G
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10,
10
10
20
10
10
10,
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10.5
10.8
10.3
10.2
10.1
10.2
11.6
10.1
9.9
15.6
11.5
11.1
11.3
10.8
9.3
10.7
10.1
10.1
10.5
12.5
9.9
10.6
9.1
10.8
20.8
9.9
9.2
10.8
10.6
12.4
10.2
11.0
10.6
10.6
10.3
10.8
9.8
10.4
10.1
10:8
11.2
11.1
10.4
10.8
10.3
10.3
10.3
10.1
11.8
10.2
10.1
16.0
11.6
11.1
11.3
11.0
9.4
10.8
10.1
10.2
10.8
12.8
10
10.7
9.0
10.9
20.9
10.0
9.1
10.8
10.7
12.3
10.3
11.0
10.7
10.7
10.5
10.8
10
10.4
10.1
10.7
11.2
11.2
104 60-140
108 60-140
103 60-140
103 60-140
103 60-140
101 60-140
118 60-140
102 60-140
101 60-140
160 60-140
116 60-140
111 60-140
113 60-140
110 60-140
94 60-140
108 60-140
101 60-140
102 60-140
108 60-140
128 60-140
100 60-140
107 60-140
90 60-140
109 60-140
105 60-140
100 - 60-140
91 60-140
108 60-140
107 60-140
123 60-140
103 60-140
110 60-140
107 60-140
107 60-140
105 60-140
108 60-140
100 60-140
104 60-140
101 60-140
107 60-140
112 60-140
112 60-140
94 60-140
97 60-140
102 60-140
99 60-140
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
RPD
Max
RPD Qualifiers
.3
30
.1
30
.1
30
.6
30
2
30
.4
30
2
30
1
30
2
30
2
30 L3
.6
-30
.6
30
.2
30
2
30
1
30
2
30
.2
30
.9
30
3
30
2
30
1
30
.5
30
.9
30
.7
30
.4
30
1
30
1
30
.2
30
1
30
.6
30
.6
30
.1
30
1
30
1
30
2
30
.3
30
2
30
.1
30
.07
30
.3
30
.2
30
1
30
Date: 12/04/2007 09:28 AM REPORT OF LABORATORY ANALYSIS Page 29 of 31
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�cCo,
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aceAnalytical
!r T wwypacelabs.com
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/1656 Analysis Method: SM 5310B
QC Batch Method: SM 5310B Analysis Description: 5310B TOC
Associated Lab Samples: 92769800.1, 927698002, 927698003, 927698004, 927698005, 927698006
METHOD BLANK: 45102
Associated Lab Samples: 927698001, 927698002, 927698003, 927698004, 927698005, 927698006
Blank Reporting
Parameter Units Result Limit Qualifiers
Total Organic Carbon mg/L ND 1.0
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
45103
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits
Qualifiers
Total Organic Carbon
mg/L
10
10.1
101 90-110
MATRIX SPIKE SAMPLE:
45104
927550001
Spike
MS MS
% Rec
Parameter
Units
Result
Conc.
Result %Rec
Limits Qualifiers
Total Organic Carbon
mg/L
8.4 10
18.9 105
75-125
SAMPLE DUPLICATE: 45106
928075001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Organic Carbon
mg/L
44.8
51.4
14
Date: 12/04/2007 09:28 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 30 of 31

acmnalytical
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QUALIFIERS
Project: Clement Pappas 2081.01
Pace Project No.: 927698
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit. .
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
ANALYTE QUALIFIERS
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
[phone]
Date:12/04/2007 09:28 AM REPORT OF LABORATORY ANALYSIS Page 31 of 31
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ry •CCpq
elac .

J_.
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 2225 Riverside Dr, 9800 Kincey Ave. Suite 100
aceAnalytical Asheville, NC 28804 Huntersville, NC 28078
3 b ?' vww.pacelabs.com
Y
f [phone] [phone]
CERTIFICATIONS
Project: Clement Pappas 2081.01
Pace Project No.: 927698
Charlotte Certification IDs
North Carolina Drinking Water Certification Number: 37706
Tennessee Certification Number: 04010
North Carolina Wastewater Certification Number: 12
Virginia Certification Number: 00213
North Carolina Field Services Certification Number: 5342
Florida/NELAP Certification Number: E87627
South Carolina Certification Number: 990060001
Kansas Certification Number: E-10364
South Carolina Bioassay Certification Number: 990060003
Louisiana/LELAP Certification Number: 04034 .
Asheville Certification IDs
Florida/NELAP Certification Number: E87648
Pennsylvania Certification Number: 68-03578
Louisiana/LELAP Certification Number: 03095
South Carolina Certification Number: 99030001
New Jersey Certification Number: NC011
South Carolina Bioassay Certification Number: 99030002
North Carolina Drinking Water Certification Number: 37712
Tennessee Certification Number: 2980
North Carolina Wastewater Certification Number: 40
Virginia Certification Number: 00072
North Carolina Bioassay Certification Number: 9
Eden Certification IDs
North Carolina Drinking Water Certification Number: 37738 North Carolina Wastewater Certification Number: 633
Virginia Drinking Water Certification Number: 00424
REPORT OF LABORATORY ANALYSIS
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