WQ0004797_Monitoring (Report)_20070710

SUBMIT FORM ON YELLOW PAPER ONLY P10
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM s17 M/UL SERy10E CENTER, R/EI�H N4�2]999 16-f7phone;g,(919) j$3=322
XILITY INFORMATION Please Print Clearly orType
PERMIT Number: Expiration Date: 6/30/2007
Icility Name: Clement Papas Non -Discharge WQ0004797 UIC
trmit Name (if different): NPDES Other
icility Address: 1 5 Ind (atrial Park TYPE OF PERMITTED OPERATION BEING MONITORED
lountain Home (Street) NC
28792 County Henderson ❑Lagoon ❑Remediation: Infiltration Gallery
(city) (state) (zip) (] Spray Field ❑ Remediation:
intact Person: Mr. Blake Kehoe Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
ell Location/Site Name:Irriaation Area No. of wells to be sampled: 6 ❑ Water Source Heat Pump ❑ Other:
aAMr IN" frvrUKIVIA I IVN
If WELL
WELL ID NUMBER (from Permit): MW-2R
Date sample collected: 05/18/2007
FIELD ANALYSES:
WAS
Well Depth: 11.5 ft.
Well.Diameter: _2 in.
pH 5.55 units
Temp. 12.2 eC
DRY at
Depth to Water Level: 7,-g4 ft. below measuring point
Screened Interval: 6 ft, to
11 ft.
Spec. Cond.
81.1 µMhos
time ofsampling,
Measuring Point is 3,77 ft, above land surface
Relative M.P. Elevation: 2063.0 ft.
Odor none
check
Volume of water pumped/bailed before sampling:
2.0 gallons .
Appearance
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATOR_ Y INFOR_M_ ATION
Date sample analyzed: Varies; see analytical
Laboratory Name: Pace Analytical
Se
Certification No. 37712
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/1
Nitrite (NO2) as N
mg/I
Pb - Lead.
mg/I JUL 1 C
Coliform: MF Fecal < 1.0 /loom]
Nitrate (NO3) as N B 56
mg/I
Zn - Zinc
mg/1
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note; Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 82 mg/l
Al -Aluminum
mg/I
-
pH (when analyzed) units
Ba -Barium
mg/I
a ,
_ _-
TOC 4.9 mg/I
Ca - Calcium
mg/I
Chloride 6 mg/I
Cd -Cadmium
mg/I
ii�
_
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
14 mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method # 6230D
Total Ammonia
< 0.10 mg/I
Mg - Magnesium
mg/l
sVOC method # 827n
(Ammonia Nitrogen; NH3 as N; Ammonia
Nitrogen, Total)
Mn -Manganese
mgll
,method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
rot- memeolatton systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wh

SI IRMIT RIPM nM VFI 101A/ PAPFP OMI v
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
•
.
0EpARTEN Mr O �t�/�RO _ M d, NATl1 RE30Uf C S'
stoFwa�ua`� ,f i=oNi r o 4 ocssso'uN `
1817Mui.SER�i(ccPtrEoti�� is1�„ Ph aa.:(Rg9�ssgaa�
FACILITY INFORMATION Please Print
Clearly or Type
PERMIT Number: Expiration Date: 613012OQ7
Facility Name: Clement Papas
Non -Discharge WQ0004797 UIC
Permit Name (if different):
NPDES Other.
Facility Address: 125 Industrial Park
TYPE OF PERMITTED OPERATION BEING MONITORED
Mountain Home (Street) NC 28792
County Henderson
❑Lagoon ❑Remediation: Infiltration Gallery
(city) (state) (zip)
© Spray Field ❑ Remediation:
Contact Person: Mr. Blake Kehoe
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: lrrloation Area
No. of wells to be sampled: 6
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): MW-4
Date sample collected: _05/1812007
FIELD ANALYSES:
If WELL
WAS
Well Depth: 16.17ft• 'relative to land surface
Well Diameter: ��in.
pH 6.10 units Temp. °. 12.7 C
DRY at
Depth to Water Level: ft. below measuring point
g.42 9 p
Screened Interval: 8 ft. to
6.1
ft. Sec. Cond. 2 Mhos
p 1 µ
time of
Measuring Point is 2,43 ft. above land surface
Relative M.P. Elevation: 2064.6 ft.
Odor none
sampling,check
Volume of water pumped/bailed before sampling: 4.75 gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: El YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:_ varies; see analytical
LaboratoryName: _pace Analytical
Se
Certification No, 37712
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal < 1.0 /100ml
Nitrate (NO3) as N < 0 to
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units) `
Dissolved Solids: Total Aoo mg/I
AI - Aluminum
mg/I
r yg -,'4.
pH (when analyzed) units
Ba - Barium
mg/I
TOC 8.5 mg/I
Ca - Calcium
mg/I
Chloride 8.9 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method A ATTACH LAB REPORT.)
Sulfate 29 mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mgll
VOC , method # 6230D
Total Ammonia < 0,10 mg/I
Mg - Magnesium
mg/I
method # 8270
• (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
_SV0C
method #
TKN as N mg/I
Ni - Nickel
mg/l
method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs: mg/L
Effluent Total VOCs: mg/L VOC Removal°/,
l certify that. to the best of my knowledge and belief, the inforrnation submitted
in this report is true, accurate, and complete, and that the
laboratory
analytical data was produced using approved methods of analysis by a
u T l A't`J rLA+ 7' I
n$ee (or Authorized Agent) Name and Title -Please print or type
GW-59 Rev.1/2007

JUtlMI I t-UKM UIV YtLLUW VAVtK UNLY
TER QUALITY MONITORING:
E REPORT FORM
ILITY INFORMATION t-tease r-nnt nearly or type
ity Name: Clement Papas
tit Name (if different):
ityAddress: 125 Industrial Park
intain Home (Street) NC 28792 County Henderson
(City) (Stale) (zip)
act Person: Mr. Blake Kehoe Telephone#: [phone]
Location/Site Name: Irrigation Area No. of wells to be sampled: 6
L ID NUMBER (from Permit): MW 5
Depth: 19 ft.
i to Water Level: 1Qft. below measuring point
luring Point is 3,00 ft. above land surface
PERMIT Number: Expiration Date: 6/30/2007
Non -Discharge W00004797 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑>C Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other: _
Date sample collected: _05/18/2007
Well Diameter:,2in.
Screened Interval: 9 ft. to �ft.
Relative M.P. Elevation: 2086.4 ft.
ne of water pumped/bailed before sampling: 4.75 gallons
Tlple analyzed: varies; E
ETERS NOTE: Values
COD
Coliform: MF Fecal
mg/I
< 1.0 /100ml
Coliform: MF Total /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
13n mg/I
pH (when analyzed)
units
TOC
1.7 mg/I
Chloride
42 mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
< 5.0 mg/I
Specific Conductance
µMhos
Total Ammonia
<0,10mg/I
(Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total)
TKN as N mg/I
WELL
FIELD ANALYSES: WAS
pH 5.38 units Temp. 13.2 eC DRY at
Mhos time of
Spec. Cond. 179.1 µ sampling,
Odor none check
Appearance here: ❑
_ Laboratory Name: Pace Analytical Se Certification No. 37712
and colloidal concentrations.
Nitrite (NO2) as N mg/I Pb - Lead mg/I
Nitrate (NO3) as N n 1 R 1119/1 . Zn - Zinc mg/I
.Phosphorus: Total as P
mg/I
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
AI - Aluminum
mg/I
Ba - Barium
m /l
Ca - Calcium
mg/I
Cd -Cadmium
mg/I
:ac e tl+ c7UU/
Chromium: Total
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
K - Potassium
mg/I
VOC , method # 6230D
Mg - Magnesium
mg/I
SVOC method # 2ti 70
Mn - Manganese
mg/I
method #
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs; mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.112007

SUBMIT FORM ON YFI_I.OW PAPER ONI Y
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DF�P�A�;T�IA�NT�O�E�(IROMME1��k3 NA7Ui�Al R�SQURCE� � ` �
lIVISIQ411(ATFtRftlJ1jN�F[¢I�TiOfROCE$�SJt�ARM;
�Pho
a��slulAlt SEgvici= cEN E cH�Nc sleds-��� s1s)a�ss szzl r?
FACILITY INFORMATION Please PrintCleadyorType
PERMIT Number: Expiration Date: 30/20 7
Facility Name: Clement Papas
Non -Discharge W00004797 UIC
Permit Name (if different):
NPDES Other
Facility Address:' 125 Industrial Park
TYPE OF PERMITTED OPERATION BEING MONITORED
Mountain Home (street) NC 28792
County
El Lagoon ❑ Remediation: Infiltration Gallery
(city) (stele) (zip)
© Spray Field ❑ Remediation:
Contact Person: Mr. Blake Kehoe
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Irrigation Area
No. of wells to be sampled: 6
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-6
Date sample collected: Q5/18/2007
FIELD ANALYSES:
WAS
Well Depth: 10 ft.
Well Diameter: _2 in.
pH 5.62 units Temp. 13.7 °C
DRY at
Depth to Water Level: —eft. below measuring point
Screened Interval: 5 ft. to
100
ft. Spec. Cond. 86,1 µMhos
time of
MeasuringPoint is 3.00 ft. above land surface
Relative M.P.'Elevation: 2061.9 ft.
Odor none
sampling,
check
Volume of water pumped/bailed before sampling: 2.75 gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATQRY INFORMATION
Date sample analyzed: varies; See analytical
Laboratory Name: pace Analytical
Se
Certification No. 37712
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/l
Pb - Lead mg/l
Coliform: MF Fecal < 1.0 /100ml
Nitrate (NO3) as N < 0 10
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note; Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration _Units):
Dissolved Solids: Total _ 5R mg/I
Al -Aluminum
mg/I
pH (when analyzed) units
ea - Barium
mg/I
- � y' ' ' -e,_I!9Pl. iJ ;i @f
TOC 3.9 mg/i
Ca - Calcium
mg/I
w�
Chloride 9.4 mg/I
Cd - Cadmium
mg/l
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 9.1 mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 6230D
Total Ammonia 0.12 mg/I
Mg - Magnesium
mg/I
SVOC method # R970
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese'
mg/I
, method #
TKN as%N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs: mg/L
Effluent Total VOCs: mg/L VOC Removal%
i, certify that, to the best of my knowledge and belief, tile Information submitted
DWQ-certified laboratory. I am aware that there are siairificast #eT?Ities for
in this report Is true, accurate, and complete, and that the
subtirdkirt fqlse iifsrn��ni i—l-ehis *. —i"ifif—f fl­
laboratory
..d
analytical data was produced using approved
r., [--A .
s64",
itteegor Authorized Agent) Name and Title -
GW-59 Rev.112007

SUBMIT FORM nN YFI I nim PAPFR nMI v
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT
r
r . r
r
DEpARE T�FN1jiONfl��k� iNAyRAI�'EOI�RCE$ " w.
� S ° '� � �p N as , T QN:Pr GPEsslnGIV
FORM
61- lql -S!kR cE'CENTER RALE�(3Fj;N�2788818770Phone>.(819)733=3221
PERMIT Number: Expiration Date: 6 00
FACILITY INFORMATION Please PrintClearfyorType
Facility Name:. Clement Papas
Non -Discharge W00004797 UIC
Permit Name (if different):
NPDES Other
Facility Address: 125 Industrial Park
TYPE OF PERMITTED OPERATION BEING MONITORED
ountain Home(Street) NC 28792
County'
J�nderson
❑ Lagoon ❑ Remediation: Infiltration Gallery
(City) (state) (zip)
❑fc Spray Field ❑ Remediation:
Contact Person: Mr. Blake Kehoe
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Irrigation Area
No. of wells to be sampled: 6
❑ Water Source Heat Pump ❑ Other:
from Permit)
-
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): MW-7
Date sample collected: 05/18/2007
FIELD ANALYSES:
If WELL
WAS
Well Depth: - 15 ft.
Well Diameter: _2 in.
pH 5.45 units Temp. 13.6 °C
DRY at
Depth to Water Level: 11.02 ft. below measuring point
Screened Interval: 5 ft, to
15
ft. Spec. Cond. 116 0 µMhos
time of
MeasuringPoint is .00 ft, above land surface
Relative M.P. Elevation: 2062.7 ft.
Odor none
sampling,
Volume of water pumped/bailed before sampling:
3.0 gallons
Appearance
check
here:
Samples for metals were collected unfiltered: DYES
❑ NO and Feld acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: varies; see analytical
Laboratory Name: pace Analytical
Se
Certification No. 37712
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD _ mg/I
Nitrite (NO2) as N
mg/l
Pb -Lead mg/I
Coliform: MF Fecal < 1.0 /100ml
Nitrate (NO3) as N 3 0
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/l
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 70 mg/I
Al - Aluminum
mg/I
I„, A:l(-; `ITYlI--1.1 i
pH (when analyzed) units
Ba - Barium
,
TOC 3.6 mg/I
Ca - Calcium
mg/I
, M4
Chloride 8.6 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/l
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 5.9 mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC # 6230D
Total Ammonia < 0.10 mg/I
Mg - Magnesium
mg/I
-,method
SVOG method # 8270
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs: mg/L
Effluent Total VOCs: mg/L VOC Removal%
J, certify that, to the best of my knowledge and belief, the information submitted
•-certified laboratory. I am aware that trere are simrifica-itnefalties fir...
in this report is true, accurate, and complete, and that the
.. _ ... .. .
laboratory
analytical data was produced using approved methods of analysis by a
it ee:(or Author a AQent) Name and Title - Please print or type
GW-59 Rev.1/2007
2616

SURMIT FnRM ON VFI I 01A1 PAPFR Mll V
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
TY INFORMATION mease t-nnt weany or Type
Name: Clement Papas
Name (if different),:
Address: 125 Industrial Park
tain(Street)rHome NC 28792 County Henderson
act Person: Mr. Blake Kehoe Telephone#: [phone]
Location/Site Name: Irrigation Area No. of wells to be sampled: G—_
Number: Expiration Date:
harge W00004797 UIC
Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑fC Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
WELL ID NUMBER (from Permit): MW-8
Date sample collected: _05/18/2007
FIELD ANALYSES:
If WELL
WAS
Well Depth: 13 ft.
Well Diameter: _tin.
pH 5.77 units Temp. _ 13.2 eC
DRY at
Depth to Water Level: 10 -'11 ft. below measuring point
Screened Interval: 3 ft. to 133 ft.
Spec, Cond, 157 2 µMhos
time of
MeasuringPoint is 3.00 ft. above land surface
Relative M.P. Elevation: 2061.4 ft.
Odor none
sampling,
Volume of water pumped/bailed before sampling:
2.0 gallons
Appearance
check
here:
Sam les for metals were collected unfiltered: El YES
❑ NO and field acidified: ❑ YES ❑ NO
sample analyzed: varies; see anE
kMETERS NOTE: Values should
COD
Coliform: MF Fecal
meal Laboratory Name: '.Pace Analytical Se
eflect dissolved and colloidal concentrations.
mg/I Nitrite (NO2) as N mg/I Pb - Lead
/100 1
Certification No. 37712
mg/I
< 1.0 m Nitrate (NOs) as N R 0 mg/I i Zn -Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/l
Other
(Specify Compounds and Concert"tration Uriits)_
Dissolved Solids: Total
2An mg/I
Al -Aluminum
mg/I
-
pH (when analyzed)
. units
Ba - Barium
mg/I�-�J
TOC
5 0 n
. mg
Ca - Calcium
mg/I
Chloride
15 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/1
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
13 mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method # 6230D
Total Ammonia
< 0.10 mg/I
Mg - Magnesium
mg/I
SVO(; method # 827r)
(Ammonia Nitrogen; NH3 as N; Ammonia
-
Nitrogen, Total)
Mn -Manganese
mg/l
,method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
�• •- .. Yy 111. Willy (MLLCUAI LiIU ICWPULLSJ: Innuent i otai vuus: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.1/2007

!GW 59A COMPLIANCE REPORT FORM Permit # WQ0004797
(Subndt one each monitoring period with GW-59 forms.)
1
Enter date monitoring results were due. (06/3012007 ) Will this monitoring report (GIN-59 and GW-59A)
YES
NO
be submitted after the established due date?
•
2
Was any required information missing on the GW-59 report forms?
YES
NO
•
IFthe answer to question 1 or 2 is 'YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance.
4
Are any monitored constituents equal to or above the established standards?
YES
NO
•
If the answer to question 4 is 'NO', slip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below.
MW-5: tetratchloroehtene 320 ug/L; trichloroethene 47 ug/L
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the. last two years?
If the answer to question 5 is 'NO",. swp to section 8.
If the answer to question 51s "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
MW-5:
tetratchloroethene: 1900 ug/L 11/03/05; 350 ug/L 11/09/06;.320 ug/L 05/18/2007
trichloroethene:210 ug/L 11/03/05; 74 ug/L 11/09/06; 47 ug/L 05/18/07
6 .
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
NO
•
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
7.
Is the permittee implementing previously approved actions required by the Division involving this
NO
groundwater quality problem?
•
®
if the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 71s "NO", contact the Regional Office within 90days; an evaluation may be
required to determine the Impact the waste disposal system Is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the•permittee to a Notice of Violation,
fines, and/or penalties.
The compounds exceeding the Standards are suspected to be from an adjacent site/property.
g
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with G W-59 dorms for required wells to the address provided at the top of the current G W-59 form.
7 here *y 4cknowledge that the above mfoimat�on was evalualed`and the information submrtte m this y
?repork(Compl/ance�RepA GW-59A) is tr #Mnd;complefe to'th4�_ t of My,knowledge,
Signature of Pe tt (or Authorized Agent) D e
GW-59A 12/8/2003

aceAnalytical °
www.pacelabs.com
May 30, 2007
Mr. Chris Gilbert
Altamont Environmental
50 College St.
Asheville, NC 28801
RE: Lab Project Number: 92144916
Client Project ID: Clement Pappas
Dear Mr. Gilbert:
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
7f 7r--3
!!��it-'?
JUN ? 2007
f-0wgw4��wn�®a®®OC�DBcea®eo
Enclosed are the analytical results for sample(s) received by the laboratory on May 18, 2007. Results reported
herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of
the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If you have any questions_ concerning this report please feel free to contact me.
*re
i
@pacelabs.com
[phone]
Project Manager
Enclosures
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
tE0 %N ACCO,,'
4c
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

ace Analytical °
www.pacelabs.com
Lab Sample No: 928404235
Client Sample ID: MW-02R
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-001 Date Collected: 05/18/07 12:31
Matrix: Water Date Received: 05/18/07 17:26
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Microbiology
Fecal Coliform in Water Method: SM 9222D
Coliform. Fecal ND col/100ml 1.0 05/18/07 17:30 JMW
Wet Chemistry
Total Dissolved Solids
Total Dissolved Solids
Chloride (Mercuric Nitrate)
Chloride
Ammonia
Nitrogen, Ammonia
48 Hour NO3 / NO2 / NOX
Nitrate as N
Sulfate,Turbidimetric
Sulfate
Total Organic Carbon
Total Organic Carbon
GUMS Semivolatiles
Semivolatile Organics
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(k)fluoranthene
Benzo(b)fluoranthene
Benzo(a)anthracene
Benzoic acid
Benzo(g,h,i)perylene
Benzyl alcohol
Benzo(a)pyrene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
Date: 05/30/07
Method: EPA 160.1
62. mg/l
Method: EPA 325.2
6.0 mg/l
Method: EPA 350.1
ND mg/l
Method: EPA 353.2
0.56 mg/l
Method: EPA 375.4
14. mg/l
Method: SM 5310B
4.9 mg/l
20. 05/20/07 17:36 SER
5.0 05/21/07 12:30 JDA1 16887-00-6
0.10 05/22/07 17:34 SAJ 7727-37-9
0.10 05/18/07 22:23 JMW
5.0 05/25/07 09:12 JDA1
1.0 05/21/07 19:00 SAJ 7440-44-0
Prep/Method: EPA 3510 / EPA 8270
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
ND
ug/l
12.
NO
ug/l
12.
NO
ug/l
62.
NO -
ug/l
12.
NO
ug/l
25.
NO
ug/l
12.
ND
ug/l
12.
NO
ug/l
12.
NO
ug/l
25.
05/24/07 14:34 BET 83-32-9
05/24/07 14:34 BET 208-96-8
05/24/07 14:34 BET 62-53-3
05/24/07 14:34 BET 120-12-7
05/24/07 14:34 BET 207-08-9
05/24/07 14:34 BET 205-99-2
05/24/07 14:34 BET 56-55-3
05/24/07 14:34 BET 65-85-0
05/24/07 14:34 BET 191-24-2
05/24/07 14:34 BET 100-51-6
05/24/07 14:34 BET 50-32-8
05/24/07 14:34 BET 101-55-3
05/24/07 14:34 BET 85-68-7
05/24/07 14:34 BET 59-50-7
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
Sc 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 ��o `" ACCOg0gy
W�F
Page: 1 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Lab Sample No: 928404235
Client Sample ID: MW-02R
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax:[phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-001 Date Collected: 05/18/07 12:31
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
4-Chloroaniline
ND
ug/l
25.
05/24/07
14:34
BET
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/l
12.
05/24/07
14:34
BET
111-91-1
bis(2-Chloroethyl) ether
ND
ug/l
12.
05/24/07
14:34
BET
111-44-4
bis(2-Chloroisopropyl) ether
ND
ug/l
12.
05/24/07
14:34
BET
39638-32-9
2-Chloronaphthalene
ND
ug/l
12.
05/24/07
14:34
BET
91-58-7
2-Chlorophenol
ND
ug/l
12.
05/24/07
14:34
BET
95-57-8
4-Chlorophenylphenyl ether
ND
ug/l
12.
05/24/07
14:34
BET
7005-72-3
Chrysene
ND
ug/l
12.
05/24/07
14:34
BET
218-01-9
Dibenz(a,h)anthracene
ND
ug/l
12.
05/24/07
14:34
BET
53-70-3
Dibenzofuran
ND
ug/l
12.
05/24/07
14:34
BET
132-64-9
1.2-Dichlorobenzene
ND
ug/l
12.
05/24/07
14:34
BET
95-50-1
1,3-Dichlorobenzene
ND
ug/l
12.
05/24/07
14:34
BET
541-73-1
1,4-Dichlorobenzene
ND
ug/l
12.
05/24/07
14:34
BET
106-46-7
3.3'-Dichlorobenzidine
ND
ug/l
25.
05/24/07
14:34
BET
91-94-1
2,4-Dichlorophenol.
ND
ug/l
12.
05/24/07
14:34
BET
120-83-2
Diethylphthalate
ND
ug/l
12.
05/24/07
14:34
BET
84-66-2
2,4-Dimethylphenol
ND
ug/l
12.
05/24/07
14:34
BET
105-67-9
Dimethylphthalate
ND
ug/l
12.
05/24/07
14:34
BET
131-11-3
Di-n-butylphthalate
ND
ug/l
12.
05/24/07
14:34
BET
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/l
62.
05/24/07
14:34
BET
534-52-1
2,4-Dinitrophenol
ND
ug/l
62.
05/24/07
14:34
BET
51-28-5
2,4-Dinitrotoluene
ND
ug/l
12.
05/24/07
14:34
BET
121-14-2
2,6-Dinitrotoluene
ND
ug/l
12.
05/24/07
14:34
BET
606-20-2
Di-n-octylphthalate
ND
ug/l
12.
05/24/07
14:34
BET
117-84-0
1,2-Diphenylhydrazine
ND
ug/l
25.
05/24/07
14:34
BET
122-66-7
bis(2-Ethylhexyl)phthalate
ND
ug/l
12.
05/24/07
14:34
BET
117-81-7
Fluoranthene
ND
ug/l
12.
05/24/07
14:34
BET
206-44-0
Fluorene
ND
ug/l
12.
05/24/07
14:34
BET
86-73-7
Hexachloro-1,3-butadiene
ND
ug/l
12.
05/24/07
14:34
BET
87-68-3
Hexachlorobenzene
ND
ug/l
12.
05/24/07
14:34
BET
118-74-1
Hexachlorocyclopentadiene
ND
ug/l
12.
05/24/07
14:34
BET
77-47-4
Hexachloroethane
ND
ug/l
12.
05/24/07
14:34
BET
67-72-1
Indeno(1.2.3-cd)pyrene
ND
ug/l
12.
05/24/07
14:34
BET
193-39-5
Isophorone
ND
-ug/l
12.
05/24/07
14:34
BET
78-59-1
1-Methylnaphthalene
ND
ug/l
12.
05/24/07
14:34
BET
90-12-0
2-Methylnaphthalene
ND
ug/l
12.
05/24/07
14:34
SET
91-57-6
2-Methylphenol (o-Cresol)
ND
ug/l
12.
05/24/07
14:34
BET
95-48-7
3&4-Methylphenol
ND
ug/l
12.
05/24/07
14:34
BET
Naphthalene
ND
ug/l
12.
05/24/07
14:34
BET
91-20-3
Date: 05/30/07
Page: 2 of 54
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Certification INNC
Wastewater
NC Drinking Water
40
37712
This report shall not be reproduced, except in full,
NC Wastewater
12
Sc
99030
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water
37706
FL NELAP
E87648
�E° %" A°`°"°�
Sc
FL NELAP
99006
E87627
a
�n'e!

ace Analytical °
www.pacelabs.com
Lab Sample No: 928404235
Client Sample ID: MW-02R
Parameters
Results
Units
2-Nitroaniline
ND
ug/l
3-Nitroaniline
ND
ug/l
4-Nitroaniline
ND
ug/l
Nitrobenzene
ND
ug/l
2-Nitrophenol
ND
ug/l
4-Nitrophenol
ND
ug/l
N-Nitrosodimethylamine
ND
ug/l
N-Nitroso-di-n-propylamine
ND
ug/l
N-Nitrosodiphenylamine
ND
ug/l
Pentachlorophenol
ND
ug/l
Phenanthrene
ND
ug/l
Phenol
ND
ug/l
Pyrene
ND
ug/l
1,2,4-Trichlorobenzene
ND
ug/l
2,4,5-Trichlorophenol
ND
ug/l
2,4,6-Trichlorophenol
ND
ug/l
Nitrobenzene-d5 (S)
79
%
2-Fluorobiphenyl (S)
95
%
Terphenyl-d14 (S)
101
%
Phenol-d5 (S)
48
X
2-Fluorophenol (S)
54
X
2,4,6-Tribromophenol (S)
109
X
Date Extracted
05/22/07
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax. [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-001 Date Collected: 05/18/07 12:31
Matrix: Water Date Received: 05/18/07 17:26
Report Limit
Analyzed
By
CAS No. Qual RegLmt
62.
05/24/07
14:34
BET
88-74-4
62.
05/24/07
14:34
BET
99-09-2
62.
05/24/07
14:34
BET
100-01-6
12.
05/24/07
14:34
BET
98-95-3
12.
05/24/07
14:34
BET
88-75-5
62.
05/24/07
14:34
BET
100-02-7
12.
05/24/07
14:34
BET
62-75-9
12.
05/24/07
14:34
BET
621.64-7
12.
05/24/07
14:34
BET
86-30-6
62.
05/24/07
14:34
BET
87-86-5
12.
05/24/07
14:34
BET
85-01-8
12.
05/24/07
14:34
BET
108-95-2
12.
05/24/07
14:34
BET
129-00-0
12.
05/24/07
14:34
BET
120-82-1
62.
05/24/07
14:34
BET
95-95-4
12.
05/24/07
14:34
BET
88-06-2
05/24/07
14:34
BET
4165-60-0
05/24/07
14:34
BET
321-60-8
05/24/07
14:34
BET
1718-51-0
05/24/07
14:34
BET
4165-62-2
05/24/07
14:34
BET
367-12-4
05/24/07
14:34
BET
118-79-6
05/22/07
GC Volatiles
GC VOCs in Water
Method:
SM 6230D
Benzene
ND
mg/l
0.00050
05/26/07
13:18
PPM
71-43-2
Bromobenzene
ND
mg/l
0.00050
05/26/07
13:18
PPM
108-86-1
Bromochloromethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
74-97-5
Bromodichloromethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
75-27-4
Bromoform
ND
mg/l
0.00050
05/26/07
13:18
PPM
75-25-2
Bromomethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
74-83-9
n-Butylbenzene
ND
mg/l
0.0010
05/26/07
13:18
PPM
104-51-8
sec-Butylbenzene
ND
mg/l
0.00050
05/26/07
13:18
PPM
135-98-8
tert-Butylbenzene
ND
mg/l
0.00050
05/26/07
13:18
PPM
98-06-6
Carbon tetrachloride
ND
mg/l
0.00050
05/26/07
13:18
PPM
56-23-5
Chlorobenzene
ND
mg/l
0.00050
05/26/07
13:18
PPM
108-90-7
Chloroethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
75-00-3
Chloroform
ND
mg/l
0.00050
05/26/07
13:18
PPM
67-66-3
Date: 05/30/07
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712
This report shall
not be reproduced,
except in full,
SC 99030
without
the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
`" A`C0",
o re
Page: 3 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Lab Sample No: 928404235
Client Sample ID: MW-02R
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-001 Date Collected: 05/18/07 12:31
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Chloromethane
ND
mg/l
0.0020
05/26/07
13:18
PPM
74-87-3
2-Chlorotoluene
ND
mg/l
0.00050
05/26/07
13:18
PPM
95-49-8
4-Chlorotoluene
ND
mg/l
0.00050
05/26/07
13:18
PPM
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/l
0.0020
05/26/07
13:18
PPM
96-12-8
Dibromochloromethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/l
0.00050
05/26/07
13:18
PPM
106-93-4
Dibromomethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
74-95-3
1,2-Dichlorobenzene
ND
mg/l
0.0010
05/26/07
13:18
PPM
95-50-1
1,3-Dichlorobenzene
ND
mg/l
0.0010
05/26/07
13:18
PPM
541-73-1
1,4-Dichlorobenzene
ND
mg/l
0.0010
05/26/07
13:18
PPM
106-46-7
Dichlorodifluoromethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
75-71-8
1,1-Dichloroethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
75-34-3
1.2-Dichloroethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
107-06-2
1,1-Dichloroethene
ND
mg/l
0.00050
05/26/07
13:18
PPM
75-35-4
cis-1.2-Dichloroethene
ND
mg/l
0.00050
05/26/07
13:18
PPM
156-59-2
trans-1,2-Dichloroethene
ND
mg/l
0.00050
05/26/07
13:18
PPM
156-60-5
1.2-Dichloropropane
ND
mg/l
0.00050
05/26/07
13:18
PPM
78-87-5
1,3-Dichloropropane
ND
mg/l
0.00050
05/26/07
13:18
PPM
142-28-9
2,2-Dichloropropane
ND
mg/l
0.00050
05/26/07
13:18
PPM
594-20-7
1.1-Dichloropropene
ND
mg/l
0.00050
05/26/07
13:18
PPM
563-58-6
cis-1,3-Dichloropropene
ND
mg/l
0.00050
05/26/07
13:18
PPM
10061-01-5
trans-1.3-Dichloropropene
ND
mg/l
0.00050
05/26/07
13:18
PPM
10061-02-6
Diisopropyl ether
ND
mg/l
0.00050
05/26/07
13:18
PPM
108-20-3
Ethylbenzene
ND
mg/l
0.00050
05/26/07
13:18
PPM
100-41-4
Hexachloro-1,3-butadiene
ND
mg/l
0.0020
05/26/07
13:18
PPM
87-68-3
Isopropylbenzene (Cumene)
ND
mg/l
0.00050
05/26/07
13:18
PPM
98-82-8
p-Isopropyltoluene
ND
mg/l
0.0010
05/26/07
13:18
PPM
99-87-6
Methylene chloride
ND
mg/l
0.0020
05/26/07
13:18
PPM
75-09-2
Methyl-tert-butyl ether
ND
mg/l
0.00050
05/26/07
13:18
PPM
1634-04-4
Naphthalene
ND
mg/l
0.0020
05/26/07
13:18
PPM
91-20-3
n-Propylbenzene
ND
mg/l
0.00050
05/26/07
13:18
PPM
103-65-1
Styrene
ND
mg/l
0.00050
05/26/07
13:18
PPM
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
630-20-6
1,1,2.2-Tetrachloroethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
79-34-5
Tetrachloroethene
ND
mg/l
0.00050
05/26/07
13:18
PPM
127-18-4
Toluene
ND
mg/l
0.00050
05/26/07
13:18
PPM
108-88-3
1,2,3-Trichlorobenzene
ND
mg/l
0.0020
05/26/07
13:18
PPM
87-61-6
1,2,4-Trichlorobenzene
ND
mg/l
0.0020
05/26/07
13:18
PPM
120-82-1
1,1.1-Trichloroethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
71-55-6
Date: 05/30/07
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 wew
g ACCOgA\�
Page: 4 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Lab Sample No: 928404235
Client Sample ID: MW-02R
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-001 Date Collected: 05/18/07 12:31
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
1,1,2-Trichloroethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
Trichloroethene
ND
mg/l
0.00050
05/26/07
13:18
PPM
Trichlorofluoromethane
ND
mg/l
0.00050
05/26/07
13:18
PPM
1,2,3-Trichloropropane
ND
mg/l
0.00050
05/26/07
13:18
PPM
1.2,4-Trimethylbenzene
ND
mg/1
0.00050
05/26/07
13:18
PPM
1,3,5-Trimethylbenzene
ND
mg/l
0.00050
05/26/07
13:18
PPM
Vinyl chloride
ND
mg/l
0.00050
05/26/07
13:18
PPM
m&p-Xylene
ND
mg/1
0.00050
05/26/07
13:18
PPM
o-Xylene
ND
mg/l
0.00050
05/26/07
13:18
PPM
1-Chloro-3-fluorobenzene (S)
98
%
05/26/07
13:18
PPM
Date: 05/30/07
Asheville certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
Sc 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 %I' p°°°
R
CAS No
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
625-98-9
Qual RegLmt
Page: 5 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

a, ce Analytical °
www.pacelabs.com
Lab Sample No: 928404243
Client Sample ID: MW-04
Pace Analytical Services, Inc.
9800 Kincey /lvehue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-002 Date Collected: 05/18/07 11:36
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Microbiology
Fecal Coliform in Water
Method: SM 9222D
Coliform, Fecal
ND
col/100ml
1.0
05/18/07
17:30
JMW
Wet Chemistry
Total Dissolved Solids
Method: EPA
160.1
Total Dissolved Solids
300
mg/l
20.
05/20/07
17:37
SER
Chloride (Mercuric Nitrate)
Method: EPA
325.2
Chloride
8.9
mg/l
5.0
05/21/07
12:37
JDA1
16887-00-6
Ammonia
Method: EPA
350.1
Nitrogen, Ammonia
ND
mg/l
0.10
05/22/07
17:34
SAJ
7727-37-9
48 Hour NO3 / NO2 / NOX
Method: EPA
353.2
Nitrate as N
ND
mg/l
0.10
05/18/07
22:23
JMW
Sulfate,Turbidimetric
Method: EPA
375.4
Sulfate
29.
mg/l
5.0
05/25/07
09:12
JDA1
Total Organic Carbon
Method: SM 5310B
Total Organic Carbon
8.5
mg/l
1.0
05/21/07
19:00
SAJ
7440-44-0
GUMS Semivolatiles
Semivolatile Organics
Prep/Method:
EPA 3510 /
EPA 8270
Acenaphthene
NO
ug/l
11.
05/24/07
14:55
BET
83-32-9
Acenaphthylene
ND
ug/l
11.
05/24/07
14:55
BET
208-96-8
Aniline
ND
ug/l
11,
05/24/07
14:55
BET
62-53-3
Anthracene
ND
ug/l
11.
05/24/07
14:55
BET
120-12-7
Benzo(k)fluoranthene
NO
ug/l
11.
05/24/07
14:55
BET
207-08-9
Benzo(b)fluoranthene
ND
ug/l
11.
05/24/07
14:55
BET
205-99-2
Benzo(a)anthracene
ND
ug/l
11.
05/24/07
14:55
BET
56-55-3
Benzoic acid
NO
ug/1
57.
05/24/07
14:55
BET
65-85-0
Benzo(g,h,i)perylene
NO
ug/l
11.
05/24/07
14:55
BET
191-24-2
Benzyl alcohol
NO
ug/l
23.
05/24/07
14:55
BET
100-51-6
Benzo(a)pyrene
NO
ug/l
11.
05/24/07
14:55
BET
50-32-8
4-Bromophenylphenyl ether
NO
ug/l
11.
05/24/07
14:55
BET
101-55-3
Butylbenzylphthalate
ND
ug/l
11.
05/24/07
14:55
BET
85-68-7
4-Chloro-3-methylphenol
ND
ug/l
23.
05/24/07
14:55
BET
59-50-7
Date: 05/30/07
Page: 6 of 54
Asheville Certification IN
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IN
NC Wastewater
NC Drinking Water
40
37712
This report shall not be reproduced, except in full,
NC Wastewater
12
Sc
99030
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water
37706
Sc
99006
FL NELAP
E87648
N A°°°p°
lF' �9
( x
FL NELAP
E87627

aceAnalytical °
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Lab Sample No: 928404243 Project Sample Number: 92144916-002 Date Collected: 05/18/07 11:36
Client Sample ID: MW-04 Matrix: Water Date Received: 05/18/07 17:26
arameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
4-Chloroaniline
ND
ug/l
23.
05/24/07
14:55
BET
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/l
11.
05/24/07
14:55
BET
111-91-1
bis(2-Chloroethyl) ether
NO
ug/l
11.
05/24/07
14:55
BET
111-44-4
bis(2-Chloroisopropyl) ether
NO
ug/l
11.
05/24/07
14:55
BET
39638-32-9
2-Chloronaphthalene
ND
ug/l
11.
05/24/07
14:55
BET
91-58-7
2-Chlorophenol
NO
ug/l
11.
05/24/07
14:55
BET
95-57-8
4-Chlorophenylphenyl ether
ND
ug/l
11.
05/24/07
14:55
BET
7005-72-3
Chrysene
ND
ug/l
11.
05/24/07
14:55
BET
218-01-9
Dibenz(a,h)anthracene
NO
ug/l
11.
05/24/07
14:55
BET
53-70-3
Dibenzofuran
ND
ug/l
11.
05/24/07
14:55
BET
132-64-9
1,2-Dichlorobenzene
NO
ug/l
11.
05/24/07
14:55
BET
95-50-1
1.3-Dichlorobenzene
NO
ug/l
11.
05/24/07
14:55
BET
541-73-1
1,4-Dichlorobenzene
NO
ug/l
11.
05/24/07
14:55
BET
106-46-7
3,3'-Dichlorobenzidine
NO
ug/l
23.
05/24/07
14:55
BET
91-94-1
2.4-Dichlorophenol
NO
ug/l
11.
05/24/07
14:55
BET
120-83-2
Diethylphthalate
NO
ug/l
11.
05/24/07
14:55
BET
84-66-2
2,4-Dimethylphenol
ND
ug/l
11.
05/24/07
14:55
BET
105-67-9
Dimethylphthalate
ND
ug/l
11.
05/24/07
14:55
BET
131-11-3
Di-n-butylphthalate
NO
ug/l
11.
05/24/07
14:55
BET
84-74-2
4,6-Dinitro-2-methylphenol
NO
ug/l
57.
05/24/07
14:55
BET
534-52-1
2.4-Dinitrophenol
NO
ug/l
57.
05/24/07
14:55
BET
51-28-5
2,4-Dinitrotoluene
ND
ug/l
11.
05/24/07
14:55
BET
121-14-2
2,6-Dinitrotoluene
NO
ug/l
11.
05/24/07
14:55
BET
606-20-2
Di-n-octylphthalate
ND
ug/l
11.
05/24/07
14:55
BET
117-84-0
1,2-Diphenylhydrazine
NO
ug/l
23.
05/24/07
14:55
BET
122-66-7
bis(2-Ethylhexyl)phthalate
ND
ug/l
11.
05/24/07
14:55
BET
117-81-7
Fluoranthene
NO
ug/l
11.
05/24/07
14:55
BET
206-44-0
Fluorene
ND
ug/l
11.
05/24/07
14:55
BET
86-73-7
Hexachloro-1,3-butadiene
ND
ug/l
11.
05/24/07
14:55
BET
87-68-3
Hexachlorobenzene
NO
ug/l
11.
05/24/07
14:55
BET
118-74-1
Hexachlorocyclopentadiene
ND
ug/l
11.
05/24/07
14:55
BET
77-47-4
Hexachloroethane
NO
ug/l
11.
05/24/07
14:55
BET
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/l
11.
05/24/07
14:55
BET
193-39-5
Isophorone
NO
ug/l
11.
05/24/07
14:55
BET
78-59-1
1-Methylnaphthalene
ND
ug/l
11.
05/24/07
14:55
BET
90-12-0
2-Methylnaphthalene
NO
ug/l
11.
05/24/07
14:55
BET
91-57-6
2-Methylphenol (o-Cresol)
NO
ug/l
11.
05/24/07
14:55
BET
95-48-7
3&4-Methylphenol
ND
ug/l
11.
05/24/07
14:55
BET
Naphthalene
ND
ug/l
11.
05/24/07
14:55
BET
91-20-3
Date: 05/30/07
Page: 7 of 54
Asheville Certification IN REPORT OF LABORATORY ANALYSIS Charlotte Certification IN
NC Wastewater 40 NC Wastewater 12
NC Drinking Water 37712 This report shall not be reproduced, except in full, NC Drinking Water 37706
Sc 99030 without the written consent of Pace Analytical Services, Inc. Sc 99006
FL NELAP E87648 NAC FL NELAP E87627
R
-VIA

ace Analytical °
www.pacelabs.com
Lab Sample No: 928404243
Client Sample ID: MW-04
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-002 Date Collected: 05/18/07 11:36
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
2-Nitroaniline
ND
ug/l
57.
05/24/07
14:55
BET
88-74-4
3-Nitroaniline
ND
ug/l
57.
05/24/07
14:55
BET
99-09-2
4-Nitroaniline
ND
ug/l
57.
05/24/07
14:55
BET
100-01-6
Nitrobenzene
ND
ug/l
11.
05/24/07
14:55
BET
98-95-3
2-Nitrophenol
ND
ug/l
11.
05/24/07
14:55
BET
88-75-5
4-Nitrophenol
ND
ug/l
57.
05/24/07
14:55
BET
100-02-7
N-Nitrosodimethylamine
ND
ug/l
11.
05/24/07
14:55
BET
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/l
11.
05/24/07
14:55
BET
621-64-7
N-Nitrosodiphenylamine
ND
ug/l
11.
05/24/07
14:55
BET
86-30-6
Pentachlorophenol
ND
ug/l
57.
05/24/07
14:55
BET
87-86-5
Phenanthrene
ND
ug/l
11.
05/24/07
14:55
BET
85-01-8
Phenol
ND
ug/l
11.
05/24/07
14:55
BET
108-95-2
Pyrene
ND
ug/l
11.
05/24/07
14:55
BET
129-00-0
1,2.4-Trichlorobenzene
ND
ug/l
11. '
05/24/07
14:55
BET
120-82-1
2,4,5-Trichlorophenol
ND
ug/l
57.
05/24/07
14:55
BET
95-95-4
2,4.6-Trichlorophenol
ND
ug/l
11.
05/24/07
14:55
BET
88-06-2
Nitrobenzene-d5 (S)
63
%
05/24/07
14:55
BET
4165-60-0
2-Fluorobiphenyl (S)
75
%
05/24/07
14:55
BET
321-60-8
Terphenyl-d14 (S)
100
%
05/24/07
14:55
BET
1718-51-0
Phenol-d5 (S)
39
%
05/24/07
14:55
BET
4165-62-2
2-Fluorophenol (S)
44
%
05/24/07
14:55
BET
367-12-4
2,4.6-Tribromophenol (S)
105
%
05/24/07
14:55
BET
118-79-6
Date Extracted
05/22/07
05/22/07
GC Volatiles
GC VOCs in Water
Method: SM
6230D
Benzene
ND
mg/l
0.00050
05/26/07
14:00
PPM
71-43-2
Bromobenzene
ND
mg/l
0.00050
05/26/07
14:00
PPM
108-86-1
Bromochloromethane
ND
mg/l
0.00050
05/26/07
14:00
PPM
74-97-5
Bromodichloromethane
NO
mg/l
0.00050
05/26/07
14:00
PPM
75-27-4
Bromoform
ND
mg/l
0.00050
05/26/07
14:00
PPM
75-25-2
Bromomethane
ND
mg/l
0.00050
05/26/07
14:00
PPM
74-83-9
n-Butylbenzene
ND
mg/l
0.0010
05/26/07
14:00
PPM
104-51-8
sec-Butylbenzene
ND
mg/l
0.00050
05/26/07
14:00
PPM
135-98-8
tert-Butylbenzene
ND
mg/l
0.00050
05/26/07
14:00
PPM
98-06-6
Carbon tetrachloride
ND
mg/l
0.00050
05/26/07
14:00
PPM
56-23-5
Chlorobenzene
ND
mg/l
0.00050
05/26/07
14:00
PPM
108-90-7
.Chloroethane
ND
mg/l
0.00050
05/26/07
14:00
PPM
75-00-3
Chloroform
ND
mg/l
0.00050
05/26/07
14:00
PPM
67-66-3
Date: 05/30/07
Page: 8 of 54
Asheville Certification IN
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IN
NC Wastewater
NC Drinking Water
40
37712
This report shall not be reproduced, except in full,
NC Wastewater
12
SC
99030
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water
37706
FL NELAP
E87648
° Itpc`°'°96
lF
Sc
FL NELAP
99006
E87627
imp' �£

ace Analytical °
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersvifle, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Lab Sample No: 928404243
Project Sample
Number: 92144916-002 Date Collected: 05/18/07 11:36
Client Sample ID: MW-04
Matrix: Water
Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Chloromethane
NO
mg/l
0.0020
05/26/07
14:00
PPM
74-87-3
2-Chlorotoluene
NO
mg/l
0.00050
05/26/07
14:00
PPM
95-49-8
4-Chlorotoluene
NO
mg/l
0.00050
05/26/07
14:00
PPM
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/l
0.0020
05/26/07
14:00
PPM
96-12-8
Dibromochloromethane
NO
mg/l
0.00050
05/26/07
14:00
PPM
124-48-1
1,2-Dibromoethane (EDB)
NO
mg/l
0.00050
05/26/07
14:00
PPM
106-93-4
Dibromomethane
NO
mg/l
0.00050
05/26/07
14:00
PPM
74-95-3
1.2-Dichlorobenzene
ND
mg/l
0.0010
05/26/07
14:00
PPM
95-50-1
1,3-Dichlorobenzene
NO
mg/l
0.0010
05/26/07
14:00
PPM
541-73-1
1,4-Dichlorobenzene
NO
mg/l
0.0010
05/26/07
14:00
PPM
106-46-7
Dichlorodifluoromethane
NO
mg/l
0.00050
05/26/07
14:00
PPM
75-71-8
1.1-Dichloroethane
NO
mg/l
0.00050
05/26/07
14:00
PPM
75-34-3
1,2-Dichloroethane
NO
mg/l
0.00050
05/26/07
14:00
PPM
107-06-2
1,1-Dichloroethene
NO
mg/l
0.00050
05/26/07
14:00
PPM
75-35-4
cis-1.2-Dichloroethene
NO
mg/l
0.00050
05/26/07
14:00
PPM
156-59-2
trans-1.2-Dichloroethene
ND
mg/l
0.00050
05/26/07
14:00
PPM
156-60-5
1,2-Dichloropropane
NO
mg/l
0.00050
05/26/07
14:00
PPM
78-87-5
1,3-Dichloropropane
NO
mg/l
0.00050
05/26/07
14:00
PPM
142-28-9
2,2-Dichloropropane
NO
mg/l
0.00050
05/26/07
14:00
PPM
594-20-7
1,1-Dichloropropene
NO
mg/l
0.00050
05/26/07
14:00
PPM
563-58-6
cis-1.3-Dichloropropene
ND
mg/l
0.00050
05/26/07
14:00
PPM
10061-01-5
trans-1,3-Dichloropropene
NO
mg/l
0.00050
05/26/07
14:00
PPM
10061-02-6
Diisopropyl ether
NO
mg/l
0.00050
05/26/07
14:00
PPM
108-20-3
Ethylbenzene
NO
mg/l
0.00050
05/26/07
14:00
PPM
100-41-4
Hexachloro-1,3-butadiene
NO
mg/l
0.0020
05/26/07
14:00
PPM
87-68-3
Isopropylbenzene (Cumene)
NO
mg/l
0.00050
05/26/07
14:00
PPM
98-82-8
p-Isopropyltoluene
NO
mg/l
0.0010
05/26/07
14:00
PPM
99-87-6
Methylene chloride
NO
mg/1
0.0020
05/26/07
14:00
PPM
75-09-2
Methyl-tert-butyl ether
NO
mg/l
0.00050
05/26/07
14:00
PPM
1634-04-4
Naphthalene
NO
mg/l
0.0020
05/26/07
14:00
PPM
91-20-3
n-Propylbenzene
NO
mg/l
0.00050
05/26/07
14:00
PPM
103-65-1
Styrene
NO
mg/l
0.00050
05/26/07
14:00
PPM
100-42-5
1,1,1,2-Tetrachloroethane
NO
mg/l
0.00050
05/26/07
14:00
PPM
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/l
0.00050
05/26/07
14:00
PPM
79-34-5
Tetrachloroethene
NO
mg/l
0.00050
05/26/07
14:00
PPM
127-18-4
Toluene
ND
mg/l
0.00050
05/26/07
14:00
PPM
108-88-3
1,2,3-Trichlorobenzene
NO
mg/l
0.0020
05/26/07
14:00
PPM
87-61-6
1,2,4-Trichlorobenzene
NO
mg/l
0.0020
05/26/07
14:00
PPM
120-82-1
1.1,1-Trichloroethane
NO
mg/l
0.00050
05/26/07
14:00
PPM
71-55-6
Date: 05/30/07 Page: 9 of 54
Asheville Certification IN
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IN
NC Wastewater
NC Drinking Water
40
37712
This report shall not be reproduced, except in full,
NC Wastewater
12
Sc
99030
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water
37706
FL NELAP
E87648
`�o ,H ACCO,O
Sc
FL NELAP
99006
E87627
¢r PPi4

ace Analytical °
www.paceiabs.com
Lab Sample No: 928404243
Client Sample ID: MW-04
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-002 Date Collected: 05/18/07 11:36
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
1,1,2-Trichloroethane
ND
mg/l
0.00050
05/26/07
14:00
PPM
Trichloroethene
ND
mg/l
0.00050
05/26/07
14:00
PPM
Trichlorofluoromethane
NO
mg/l
0.00050
05/26/07
14:00
PPM
1,2.3-Trichloropropane
NO
mg/l
0.00050
05/26/07
14:00
PPM
1.2,4-Trimethylbenzene
ND
mg/l
0.00050
05/26/07
14:00
PPM
1,3,5-Trimethylbenzene
ND
mg/l
0,00050
05/26/07
14:00
PPM
Vinyl chloride
NO
mg/l
0.00050
05/26/07
14:00
PPM
m&p-Xylene
NO
mg/l
0.00050
05/26/07
14:00
PPM
o-Xylene
ND
mg/l
0.00050
05/26/07
14:00
PPM
1-Chloro-3-fluorobenzene (S)
97
Y
05/26/07
14:00
PPM
Date: 05/30/07
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
. This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
%Il ACCp9p, C
WF
V
CAS No
79-00-5
79.01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
625-98-9
Qual RegLmt
Page: 10 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Lab Sample No: 928404250
Client Sample ID: MW-05
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-003 Date Collected: 05/18/07 14:20
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
_ Analyzed
By
CAS No. Qual RegLmt
Microbiology
Fecal Coliform in Water
Method: SM
9222D
Coliform, Fecal
NO
col/100ml
1.0
05/18/07
17:30
JMW
Wet Chemistry
Total Dissolved Solids
Method: EPA
160.1
Total Dissolved Solids
130
mg/l
20.
05/20/07
17:37
SER
Chloride (Mercuric Nitrate)
Method: EPA
325.2
Chloride
42.
mg/l
25.
05/21/07
12:50
JDA1
16887-00-6
Ammonia
Method: EPA
350.1
Nitrogen, Ammonia
NO
mg/l
0.10
05/22/07
17:34
SAJ
7727-37-9
48 Hour NO3 / NO2 / NOX
Method: EPA
353.2
Nitrate as N
0.16
mg/l
0.10
05/18/07
22:23
JMW
Sulfate.Turbidimetric
Method: EPA
375.4
Sulfate
ND
mg/l
5.0
05/25/07
09:12
JDA1
Total Organic Carbon
Method: SM 5310B
Total Organic Carbon
1.7
mg/l
1.0
05/21/07
19:00
SAJ
7440-44-0
GUMS Semivolatiles
Semivolatile Organics
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(k)fluoranthene
Benzo(b)fluoranthene
Benzo(a)anthracene
Benzoic acid
Benzo(g,h,i)perylene
Benzyl alcohol
Benzo(a)pyrene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
Date: 05/30/07
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
Prep/Method: EPA 3510 / EPA 8270
NO
ug/l
12.
NO
ug/l
12.
ND
ug/1
12.
ND
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
ND
ug/l
12.
NO
ug/l
60.
NO
ug/l
12.
NO
ug/1
24.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
ND
ug/l
24.
05/24/07 15:58 BET 83-32-9
05/24/07 15:58 BET 208-96-8
05/24/07 15:58 BET 62-53-3
05/24/07 15:58 BET 120-12-7
05/24/07 15:58 BET 207-08-9
05/24/07 15:58 BET 205-99-2
05/24/07 15:58 BET 56-55-3
05/24/07 15:58 BET 65-85-0
05/24/07 15:58 BET 191-24-2
05/24/07 15:58 BET 100-51-6
05/24/07 15:58 BET 50-32-8
05/24/07 15:58 BET 101-55-3
05/24/07 15:58 BET 85-68-7
05/24/07 15:58 BET 59-50-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
LF,V ,N ACCO.9,
Page: 11 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

aceAnalytical °
www.pacelahs.com
Lab Sample No: 928404250
Client Sample ID: MW-05
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax:[phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-003 Date Collected: 05/18/07 14:20
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
4-Chloroaniline
ND
ug/l
24.
05/24/07
15:58
BET
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/l
12.
05/24/07
15:58
BET
111-91-1
bis(2-Chloroethyl) ether
ND
ug/l
12.
05/24/07
15:58
BET
111-44-4
bis(2-Chloroisopropyl) ether
ND
ug/l
12.
05/24/07
15:58
BET
39638-32-9
2-Chloronaphthalene
ND
ug/l
12.
05/24/07
15:58
BET
91-58-7
2-Chlorophenol
ND
ug/l
12.
05/24/07
15:58
BET
95-57-8
4-Chlorophenylphenyl ether
ND
ug/l
12.
05/24/07
15:58
BET
7005-72-3
Chrysene
ND
ug/l
12.
05/24/07
15:58
BET
218-01-9
Dibenz(a,h)anthracene
ND
ug/l
12.
05/24/07
15:58
BET
53-70-3
Dibenzofuran
ND
ug/l
12.
05/24/07
15:58
BET
132-64-9
1,2-Dichlorobenzene
ND
ug/l
12.
05/24/07
15:58
BET
95-50-1
1.3-Dichlorobenzene
ND
ug/l
12.
05/24/07
15:58
BET
541-73-1
1,4-Dichlorobenzene
ND
ug/l
12.
05/24/07
15:58
BET
106-46-7
3,3'-Dichlorobenzidine
ND
ug/l
24.
05/24/07
15:58
BET
91-94-1
2.4-Dichlorophenol
ND
ug/l
12.
05/24/07
15:58
BET
120-83-2
Diethylphthalate
ND
ug/l
12.
05/24/07
15:58
BET
84-66-2
2.4-Dimethylphenol
ND
ug/l
12.
05/24/07
15:58
BET
105-67-9
Dimethylphthalate
ND
ug/l
12.
05/24/07
15:58
BET
131-11-3
Di-n-butylphthalate
ND
ug/l
12.
05/24/07
15:58
BET
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/l
60.
05/24/07
15:58
BET
534-52-1
2,4-Dinitrophenol
ND
ug/l
60.
05/24/07
15:58
BET
51-28-5
2,4-Dinitrotoluene
ND
ug/l
12.
05/24/07
15:58
BET
121-14-2
2.6-Dinitrotoluene
ND
ug/l
12.
05/24/07
15:58
BET
606-20-2
Di-n-octylphthalate
ND
ug/l
12.
05/24/07
15:58
BET
117-84-0
1.2-Diphenylhydrazine
ND
ug/l
24.
05/24/07
15:58
BET
122-66-7
bis(2-Ethylhexyl)phthalate
ND
ug/l
12.
05/24/07
15:58
BET
117-81-7
Fluoranthene
ND
ug/l
12.
05/24/07
15:58
BET
206-44-0
Fluorene
ND
ug/l
12.
05/24/07
15:58
BET
86-73-7
Hexachloro-1.3-butadiene
ND
ug/l
12.
05/24/07
15:58
BET
87-68-3
Hexachlorobenzene
ND
ug/l
12.
05/24/07
15:58
BET
118-74-1
Hexachlorocyclopentadiene
ND
ug/l
12.
05/24/07
15:58
BET
77-47-4
Hexachioroethane
ND
ug/l
12.
05/24/07
15:58
BET
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/l
12.
05/24/07
15:58
BET
193-39-5
Isophorone
ND
ug/l
12.
05/24/07
15:58
BET
78-59-1
1-Methylnaphthalene
ND
ug/l
12.
05/24/07.15:58
BET
90-12-0
2-Methylnaphthalene
ND
ug/l
12.
05/24/07
15:58
BET
91-57-6
2-Methylphenol (o-Cresol)
ND
ug/l
12.
05/24/07
15:58
BET
95-48-7
3&4-Methylphenol
ND
ug/l
12.
05/24/07
15:58
BET
Naphthalene
ND
ug/l
12.
05/24/07
15:58
BET
91-20-3
Date: 05/30/07
Page: 12 of 54
Asheville Certification IN
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IN
NC Wastewater
NC Drinking Water
40
37712
This report shall not be reproduced, except in full,
NC Wastewater
12
Sc
99030
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water
37706
FL NELAP
E87648
° `" Ac`°"°
Sc
FL NELAP
99006
E87627

aceAnalytical °
www.pacelabs.com
Lab Sample No: 928404250
Client Sample ID: MW-05
Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax. [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-003 Date Collected: 05/18/07 14:20
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
2-Nitroaniline
NO
ug/l
60.
05/24/07
15:58
BET
88-74-4
3-Nitroaniline
NO
ug/l
60.
05/24/07
15:58
BET
99-09-2
4-Nitroaniline
NO
ug/l
60.
05/24/07
15:58
BET
100-01-6
Nitrobenzene
ND
ug/l
12.
05/24/07
15:58
BET
98-95-3
2-Nitrophenol
ND
ug/l
12.
05/24/07
15:58
BET
88-75-5
4-Nitrophenol
ND
ug/l
60.
05/24/07
15:58
BET
100-02-7
N-Nitrosodimethylamine
ND
ug/l
12.
05/24/07
15:58
BET
62-75-9
N-Nitroso-di-n-propylamine
NO
ug/l
12.
05/24/07
15:58
BET
621-64-7
N-Nitrosodiphenylamine
NO
ug/l
12.
05/24/07
15:58
BET
86-30-6
Pentachlorophenol
ND
ug/l
60.
05/24/07
15:58
BET
87-86-5
Phenanthrene
NO
ug/l
12.
05/24/07
15:58
BET
85-01-8
Phenol
ND
ug/l
12.
05/24/07
15:58
BET
108-95-2
Pyrene
ND
ug/l
12.
05/24/07
15:58
BET
129-00-0
1,2,4-Trichlorobenzene
ND
ug/1
12.
05/24/07
15:58
BET
120-82-1
2,4.5-Trichlorophenol
NO
ug/l
60.
05/24/07
15:58
BET
95-95-4
2,4,6-Trichlorophenol
NO
ug/l
12.
05/24/07
15:58
BET
88-06-2
Nitrobenzene-d5 (S)
81
X
05/24/07
15:58
BET
4165-60-0
2-Fluorobiphenyl (S)
92
X
05/24/07
15:58
BET
321-60-8
Terphenyl-d14 (S)
102
X
05/24/07
15:58
BET
1718-51-0
Phenol-d5 (S)
46
05/24/07
15:58
BET
4165-62-2
2-Fluorophenol (S)
56
X
05/24/07
15:58
BET
367-12-4
2,4,6-Tribromophenol (S)
98
X
05/24/07
15:58
BET
118-79-6
Date Extracted
05/22/07
05/22/07
GC Volatiles
GC VOCs in Water
Method: SM
6230D
Benzene
NO
mg/l
0.0050
05/26/07
14:42
PPM
71-43-2
Bromobenzene
NO
mg/l
0.0050
05/26/07
14:42
PPM
108-86-1
Bromochloromethane
ND
mg/l
0.0050
05/26/07
14:42
PPM
74-97-5
Bromodichloromethane
NO
mg/l
0.0050
05/26/07
14:42
PPM
75-27-4
Bromoform
ND
mg/l
0.0050
05/26/07
14:42
PPM
75-25-2
Bromomethane
NO
mg/l
0.0050
05/26/07
14:42
PPM
74-83-9
n-Butylbenzene
NO
mg/l
0.010
05/26/07
14:42
PPM
104-51-8
sec-Butylbenzene
NO
mg/l
0.0050
05/26/07
14:42
PPM
135-98-8
tert-Butylbenzene
NO
mg/l
0.0050
05/26/07
14:42
PPM
98-06-6
Carbon tetrachloride
ND
mg/l
0.0050
05/26/07
14:42
PPM
56-23-5
Chlorobenzene
NO
mg/l
0.0050
05/26/07
14:42
PPM
108-90-7
Chloroethane
NO
mg/l
0.0050
05/26/07
14:42
PPM
75-00-3
Chloroform
NO
mg/1
0.0050
05/26/07
14:42
PPM
67-66-3
Date: 05/30/07
Page: 13 of 54
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IDs
NC Wastewater
NC Drinking Water
40
37712
This report shall not be reproduced, except in full,
NC Wastewater
12
Sc
99030
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water
37706
FL NELAP
E87648
1� '2
Sc
FL NELAP
99006
E87627

ace Analytical °
www.pacelabs.com
Lab Sample No: 928404250
Client Sample ID: MW-05
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-003 Date Collected: 05/18/07 14:20
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Chloromethane
ND
mg/l
0.020
05/26/07
14:42
PPM
74-87-3
2-Chlorotoluene
ND
mg/l
0.0050
05/26/07
14:42
PPM
95-49-8
4-Chlorotoluene
ND
mg/l
0.0050
05/26/07
14:42
PPM
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/l
0.020
05/26/07
14:42
PPM
96-12-8
Dibromochloromethane
ND
mg/l
0.0050
05/26/07
14:42
PPM
124-48-1
1.2-Dibromoethane (EDB)
ND
mg/l
0.0050
05/26/07
14:42
PPM
106-93-4
Dibromomethane
ND
mg/l
0.0050
05/26/07
14:42
PPM
74-95-3
1,2-Dichlorobenzene
ND
mg/l
0.010
05/26/07
14:42
PPM
95-50-1
1,3-Dichlorobenzene
ND
mg/l
0.010
05/26/07
14:42
PPM
541-73-1
1,4-Dichlorobenzene
ND
mg/l
0.010
05/26/07
14:42
PPM
106-46-7
Dichlorodifluoromethane
ND
mg/l
0.0050
05/26/07
14:42
PPM
75-71-8
1,1-Dichloroethane
ND
mg/l
0.0050
05/26/07
14:42
PPM
75-34-3
1.2-Dichloroethane
ND
mg/l
0.0050
05/26/07
14:42
PPM
107-06-2
1.1-Dichloroethene
ND
mg/l
0.0050
05/26/07
14:42
PPM
75-35-4
cis-1,2-Dichloroethene
0.060
mg/l
0.0050
05/26/07
14:42
PPM
156-59-2
trans-1.2-Dichloroethene
ND
mg/l
0.0050
05/26/07
14:42
PPM
156-60-5
1,2-Dichloropropane
ND
mg/l
0.0050
05/26/07
14:42
PPM
78-87-5
1,3-Dichloropropane
ND
mg/l
0.0050
05/26/07
14:42
PPM
142-28-9
2,2-Dichloropropane
ND
mg/l
0.0050
05/26/07
14:42
PPM
594-20-7
1,1-Dichloropropene
ND
mg/l
0.0050
05/26/07
14:42
PPM
563-58-6
cis-1,3-Dichloropropene
ND
mg/l
0.0050
05/26/07
14:42
PPM
10061-01-5
trans-1,3-Dichloropropene
ND
mg/l
0.0050
05/26/07
14:42
PPM
10061-02-6
Diisopropyl ether
ND
mg/l
0.0050
05/26/07
14:42
PPM
108-20-3
Ethylbenzene
ND
mg/l
0.0050
05/26/07
14:42
PPM
100-41-4
Hexachloro-1,3-butadiene
ND
mg/l
0.020
05/26/07
14:42
PPM
87-68-3
Isopropylbenzene (Cumene)
ND
mg/l
0.0050
05/26/07
14:42
PPM
98-82-8
p-Isopropyltoluene
ND
mg/l
0.010
05/26/07
14:42
PPM
99-87-6
Methylene chloride
ND
mg/l
0,020
05/26/07
14:42
PPM
75-09-2
Methyl-tert-butyl ether
ND
mg/l
0.0050
05/26/07
14:42
PPM
1634-04-4
Naphthalene
ND
mg/l
0.020
05/26/07
14:42
PPM
91-20-3
n-Propylbenzene
ND
mg/l
0.0050
05/26/07
14:42
PPM
103-65-1
Styrene
ND
mg/l
0.0050
05/26/07
14:42
PPM
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/l
0.0050
05/26/07
14:42
PPM
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/l
0.0050
05/26/07
14:42
PPM
79-34-5
Tetrachloroethene
0.32
mg/l
0.0050
05/26/07
14:42
PPM
127-18-4
Toluene
ND
mg/l
0.0050
05/26/07
14:42
PPM
108-88-3
1,2,3-Trichlorobenzene
ND
mg/l
0.020
05/26/07
14:42
PPM
87-61-6
1.2,4-Trichlorobenzene
ND
mg/l
0.020
05/26/07
14:42
PPM
120-82-1
1,1,1-Trichloroethane
ND
mg/l
0.0050
05/26/07
14:42
PPM
71-55-6
Date: 05/30/07
Page: 14 of 54
Asheville Certification IN
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IDs
NC Wastewater
NC Drinking Water
40
37712
This report shall not be reproduced, except in full,
NC Wastewater
12
Sc
99030
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water
37706
FL NELAP
E87648
C C^,
W
Sc
FL NELAP
99006
E87627
�\1

ace Analytical °
www.pacelabs.com
Lab Sample No: 928404250
Client Sample ID: MW-05
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-003 Date Collected: 05/18/07 14:20
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
1,1.2-Trichloroethane
NO
mg/l
0.0050
05/26/07
14:42
PPM
79-00-5
Trichloroethene
0.047
mg/l
0.0050
05/26/07
14:42
PPM
79-01-6
Trichlorofluoromethane
NO
mg/l
0.0050
05/26/07
14:42
PPM
75-69-4
1,2,3-Trichloropropane
NO
mg/l
0.0050
05/26/07
14:42
PPM
96-18-4
1,2,4-Trimethylbenzene
NO
mg/l
0.0050
05/26/07
14:42
PPM
95-63-6
1,3,5-Trimethylbenzene
NO
mg/l
0.0050
05/26/07
14:42
PPM
108-67-8
Vinyl chloride
NO
mg/l
0.0050
05/26/07
14:42
PPM
75-01-4
m&p-Xylene
NO
mg/l
0.0050
05/26/07
14:42
PPM
o-Xylene
NO
mg/l
0.0050
05/26/07
14:42
PPM
95-47-6
1-Chloro-3-fluorobenzene (S)
97
%
05/26/07
14:42
PPM
625-98-9
Date: 05/30/07
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 ��a ,N ACCOR'q
Page: 15 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Lab Sample No: 928404268
Client Sample ID: MW-06
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-004 Date Collected: 05/18/07 13:33
Matrix: Water Date Received: 05/18/07 17:26
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Microbiology
Fecal Coliform in Water Method: SM 9222D
Coliform, Fecal NO c0l/100ml 1.0 05/18/07 17:30 JMW
Wet Chemistry
Total Dissolved Solids
Total Dissolved Solids
Chloride (Mercuric Nitrate)
Chloride
Ammonia
Nitrogen, Ammonia
48 Hour NO3 / NO2 / NOX
Nitrate as N
Sulfate.Turbidimetric
Sulfate
Total Organic Carbon
Total Organic Carbon
GUMS Semivolatiles
Semivolatile Organics
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(k)fluoranthene
Benzo(b)fluoranthene
Benzo(a)anthracene
Benzoic acid
Benzo(g,h,i)perylene
Benzyl alcohol
Benzo(a)pyrene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
Date: 05/30/07
Method: EPA 160.1
58. mg/l
Method: EPA 325.2
9.4 mg/l
Method: EPA 350.1
0.12 mg/l
Method: EPA 353.2
NO mg/l
Method: EPA 375.4
9.1 mg/l
Method: SM 5310B
3.9 mg/l
20. 05/20/07 17:38 SER
5.0 05/21/07 12:37 JDA1 16887-00-6
0.10 05/22/07 17:34 SAJ 7727-37-9
0.10 05/18/07 22:23 JMW
5.0 05/25/07 09:12 JDA1
1.0 05/21/07 19:00 SAJ 7440-44-0
Prep/Method: EPA 3510 / EPA 8270
ND
ug/l
12.
ND
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
62.
NO
ug/l
12.
NO
ug/l
25.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
25.
05/24/07 16:19 BET 83-32-9
05/24/07 16:19 BET 208-96-8
05/24/07 16:19 BET 62-53-3
05/24/07 16:19 BET 120-12-7
05/24/07 16:19 BET 207-08-9
05/24/07 16:19 BET 205-99-2
05/24/07 16:19 BET 56-55-3
05/24/07 16:19 BET 65-85-0
05/24/07 16:19 BET 191-24-2
05/24/07 16:19 BET 100-51-6
05/24/07 16:19 BET 50-32-8
05/24/07 16:19 BET 101-55-3
05/24/07 16:19 BET 85-68-7
05/24/07 16:19 BET 59-50-7
Ashevi
REPORT OF LABORATORY ANALYSIS
WasteC tericationOIDs
NO Drinking Water 37712
This report shall not be reproduced, except in full,
SC 99030
without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
A
c
Page: 16 of 54
Charlotte Certification IDs
NO Wastewater 12
NO Drinking Water 37706
SC 99006
FL NELAP E87627

aceAnalytical°
www. pacelahs. cam
Lab Sample No: 928404268
Client Sample ID: MW-06
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-004 Date Collected: 05/18/07 13:33
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
4-Chloroaniline
ND
ug/l
25.
05/24/07
16:19
BET
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/l
12.
05/24/07
16:19
BET
111-91-1
bis(2-Chloroethyl) ether
ND
ug/l
12.
05/24/07
16:19
BET
111-44-4
bis(2-Chloroisopropyl) ether
ND
ug/l
12.
05/24/07
16:19
BET
39638-32-9
2-Chloronaphthalene
ND
ug/l
12.
05/24/07
16:19
BET
91-58-7
2-Chlorophenol
ND
ug/l
12.
05/24/07
16:19
BET
95-57-8
4-Chlorophenylphenyl ether
ND
ug/l
12.
05/24/07
16:19
BET
7005-72-3
Chrysene
ND
ug/l
12.
05/24/07
16:19
BET
218-01-9
Dibenz(a,h)anthracene
ND
ug/l
12.
05/24/07
16:19
BET
53-70-3
Dibenzofuran
ND
ug/l
12.
05/24/07
16:19
BET
132-64-9
1,2-Dichlorobenzene
ND
ug/l
12.
05/24/07
16:19
BET
95-50-1
1,3-Dichlorobenzene
ND
ug/l
12.
05/24/07
16:19
BET
541-73-1
1,4-Dichlorobenzene
ND
ug/l
12.
05/24/07
16:19
BET
106-46-7
3,3'-Dichlorobenzidine
ND
ug/l
25.
05/24/07
16:19
BET
91-94-1
2,4-Dichlorophenol
ND
ug/l
12.
05/24/07
16:19
BET
120-83-2
Diethylphthalate
ND
ug/l
12.
05/24/07
16:19
BET
84-66-2
2,4-Dimethylphenol
ND
ug/l
12.
05/24/07
16:19
BET
105-67-9
Dimethylphthalate
ND
ug/l
12.
05/24/07
16:19
BET
131-11-3
Di-n-butylphthalate
ND
ug/l
12.
05/24/07
16:19
BET
84-74-2
4,6-Dinitro-2-methylphenol
NO
ug/l
62.
05/24/07
16:19
BET
534-52-1
2.4-Dinitrophenol
ND
ug/l
62.
05/24/07
16:19
BET
51-28-5
2,4-Dinitrotoluene
ND
ug/l
12.
05/24/07
16:19
BET
121-14-2
2,6-Dinitrotoluene
ND
ug/1
12.
05/24/07
16:19
BET
606-20-2
Di-n-octylphthalate
ND
ug/l
12.
05/24/07
16:19
BET
117-84-0
1.2-Diphenylhydrazine
ND
ug/l
25.
05/24/07
16:19
BET
122-66-7
bis(2-Ethylhexyl)phthalate
ND
ug/l
12.
05/24/07
16:19
BET
117-81-7
Fluoranthene
ND
ug/l
12.
05/24/07
16:19
BET
206-44-0
Fluorene
ND
ug/l
12.
05/24/07
16:19
BET
86-73-7
Hexachloro-1,3-butadiene
ND
ug/l
12.
05/24/07
16:19
BET
87-68-3
Hexachlorobenzene
ND
ug/l
12.
05/24/07
16:19
BET
118-74-1
Hexachlorocyclopentadiene
ND
ug/l
12.
05/24/07
16:19
BET
77-47-4
Hexachloroethane
ND
ug/l
12.
05/24/07
16:19
BET
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/l
12.
05/24/07
16:19
BET
193-39-5
Isophorone
ND
ug/l
12.
05/24/07
16:19
BET
78-59-1
1-Methylnaphthalene
ND
ug/l
12.
05/24/07
16:19
BET
90-12-0
2-Methylnaphthalene
ND
ug/l
12.
05/24/07
16:19
BET
91-57-6
2-Methylphenol (o-Cresol)
ND
ug/1
12.
05/24/07
16:19
BET
95-48-7
3&4-Methylphenol
ND
ug/l
12.
05/24/07
16:19
BET
Naphthalene
ND
ug/l
12.
05/24/07
16:19
BET
91-20-3
Date: 05/30/07
Page: 17 of 54
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IDs
NC Wastewater
NC Drinking Water
40
37712
This report shall not be reproduced, except in full,
NC Wastewater
12
Sc
99030
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water
37706
FL NELAP
E87648
p0 c
Sc
FL NELAP
99006
E87627

ice Analytical °
www.pacelabs.com
Lab Sample No: 928404268
Client Sample ID: MW-06
Parameters
Results
Units
2-Nitroaniline
ND
ug/l
3-Nitroaniline
ND
ug/l
4-Nitroaniline
ND
ug/l
Nitrobenzene
ND
ug/l
2-Nitrophenol
ND
ug/l
4-Nitrophenol
ND
ug/l
N-Nitrosodimethylamine
ND
ug/l
N-Nitroso-di-n-propylamine
ND
ug/l
N-Nitrosodiphenylamine
ND
ug/l
Pentachlorophenol
ND
ug/l
Phenanthrene
ND
ug/l
Phenol
ND
ug/l
Pyrene
ND
ug/l
1,2.4-Trichlorobenzene
ND
ug/l
2,4,5-Trichlorophenol
ND
ug/l
2,4,6-Trichlorophenol
ND
ug/l
Nitrobenzene-d5 (S)
90
%
2-Fluorobiphenyl (S)
92
X
Terphenyl-d14 (S)
84
%
Phenol-d5 (S)
52
%
2-Fluorophenol (S)
62
X
2,4,6-Tribromophenol (S)
99
X
Date Extracted
05/22/07
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax. [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-004 Date Collected: 05/18/07 13:33
Matrix: Water Date Received: 05/18/07 17:26
Report Limit
Analyzed
By
CAS No. Qual RegLmt
62.
05/24/07
16:19
BET
88-74-4
62.
05/24/07
16:19
BET
99-09-2
62.
05/24/07
16:19
BET
100-01-6
12.
05/24/07
16:19
BET
98-95-3
12.
05/24/07
16:19
BET
88-75-5
62.
05/24/07
16:19
BET
100-02-7
12.
05/24/07
16:19
BET
62-75-9
12.
05/24/07
16:19
BET
621-64-7
12.
05/24/07
16:19
BET
86-30-6
62.
05/24/07
16:19
BET
87-86-5
12.
05/24/07
16:19
BET
85-01-8
12.
05/24/07
16:19
BET
108-95-2
12.
05/24/07
16:19
BET
129-00-0
12,
05/24/07
16:19
BET
120-82-1
62.
05/24/07
16:19
BET
95-95-4
12.
05/24/07
16:19
BET
88-06-2
05/24/07
16:19
BET
4165-60-0
05/24/07
16:19
BET
321-60-8
05/24/07
16:19
BET
1718-51-0
05/24/07
16:19
BET
4165-62-2
05/24/07
16:19
BET
367-12-4
05/24/07
16:19
BET
118-79-6
05/22/07
GC Volatiles
GC VOCs in Water
Method:
SM 6230D
Benzene
ND
mg/l
0.00050
05/26/07
15:24
PPM
71-43-2
Bromobenzene
ND
mg/l
0.00050
05/26/07
15:24
PPM
108-86-1
Bromochloromethane
ND
mg/l
0.00050
05/26/07
15:24
PPM
74-97-5
Bromodichloromethane
ND
mg/l
0.00050
05/26/07
15:24
PPM
75-27-4
Bromoform
ND
mg/l
0.00050
05/26/07
15:24
PPM
75-25-2
Bromomethane
ND
mg/l
0.00050
05/26/07
15:24
PPM
74-83-9
n-Butylbenzene
ND
mg/l
0.0010
05/26/07
15:24
PPM
104-51-8
sec-Butylbenzene
ND
mg/l
0.00050
05/26/07
15:24
PPM
135-98-8
tert-Butylbenzene
ND
mg/l
0.00050
05/26/07
15:24
PPM
98-06-6
Carbon tetrachloride
ND
mg/l
0.00050
05/26/07
15:24
PPM
56-23-5
Chlorobenzene
ND
mg/l
0.00050
05/26/07
15:24
PPM
108-90-7
Chloroethane
ND
mg/l
0.00050
05/26/07
15:24
PPM
75-00-3
Chloroform
ND
mg/l
0.00050
05/26/07
15:24
PPM
67-66-3
Date: 05/30/07
Asheville Certification IN
'
REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712
This report shall
not be reproduced,
except in full,
SC 99030
without
the written consent of Pace Analytical Services,
Inc.
FL NELAP E87648
`" ACC°R
0 5,y
'3� ;' £.
:mil
Page: 18 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacelahs.com
Lab Sample No: 928404268
Client Sample ID: MW-06
Parameters
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1.2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
Date: 05/30/07
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-004 Date Collected: 05/18/07 13:33
Matrix: Water Date Received: 05/18/07 17:26
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
ND
mg/l
0.0020
05/26/07
15:24
PPM
74-87-3
ND
mg/l
0.00050
05/26/07
15:24
PPM
95-49-8
ND
mg/l
0.00050
05/26/07
15:24
PPM
106-43-4
ND
mg/l
0.0020
05/26/07
15:24
PPM
96-12-8
ND
mg/l
0.00050
05/26/07
15:24
PPM
124-48-1
ND
mg/l
0.00050
05/26/07
15:24
PPM
106-93-4
ND
mg/l
0.00050
05/26/07
15:24
PPM
74-95-3
ND
mg/l
0.0010
05/26/07
15:24
PPM
95-50-1
ND
mg/l
0.0010
05/26/07
15:24
PPM
541-73-1
ND
mg/l
0.0010
05/26/07
15:24
PPM
106-46-7
ND
mg/l
0.00050
05/26/07
15:24
PPM
75-71-8
ND
mg/l
0.00050
05/26/07
15:24
PPM
75-34-3
ND
mg/l
0.00050
05/26/07
15:24
PPM
107-06-2
ND
mg/l
0.00050
05/26/07
15:24
PPM
75-35-4
ND
mg/l
0.00050
05/26/07
15:24
PPM
156-59-2
ND
mg/l
0.00050
05/26/07
15:24
PPM
156-60-5
ND
mg/l
0.00050
05/26/07
15:24
PPM
78-87-5
ND
mg/l
0.00050
05/26/07
15:24
PPM
142-28-9
ND
mg/l
0.00050
05/26/07
15:24
PPM
594-20-7
ND
mg/l
0.00050
05/26/07
15:24
PPM
563-58-6
ND
mg/l
0.00050
05/26/07
15:24
PPM
10061-01-5
ND
mg/l
0.00050
05/26/07
15:24
PPM
10061-02-6
ND
mg/l
0.00050
05/26/07
15:24
PPM
108-20-3
ND
mg/l
0.00050
05/26/07
15:24
PPM
100-41-4
ND
mg/l
0,0020
05/26/07
15:24
PPM
87-68-3
ND
mg/l
0.00050
05/26/07
15:24
PPM
98-82-8
ND
mg/l
0.0010
05/26/07
15:24
PPM
99-87-6
ND
mg/l
0.0020
05/26/07
15:24
PPM
75-09-2
ND
mg/l
0.00050
05/26/07
15:24
PPM
1634-04-4
ND
mg/l
0.0020
05/26/07
15:24
PPM
91-20-3
ND
mg/l
0.00050
05/26/07
15:24
PPM
103-65-1
ND
mg/l
0.00050
05/26/07
15:24
PPM
100-42-5
ND
mg/l
0.00050
05/26/07
15:24
PPM
630-20-6
ND
mg/l
0.00050
05/26/07
15:24
PPM
79-34-5
ND
mg/l
0.00050
05/26/07
15:24
PPM
127-18-4
ND
mg/l
0.00050
05/26/07
15:24
PPM
108-88-3
ND
mg/l
0.0020
05/26/07
15:24
PPM
87-61-6
ND
mg/l
0.0020
05/26/07
15:24
PPM
120-82-1
ND
mg/l
0.00050
05/26/07
15:24
PPM
71-55-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 19 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

aceAnalytical °
www.pacelabs.com
Lab Sample No: 928404268
Client Sample ID: MW-06
Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-004 Date Collected: 05/18/07 13:33
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
1,1,2-Trichloroethane
NO
mg/l
0.00050
05/26/07
15:24
PPM
79-00-5
Trichloroethene
NO
mg/l
0.00050
05/26/07
15:24
PPM
79-01-6
Trichlorofluoromethane
NO
mg/l
0.00050
05/26/07
15:24
PPM
75-69-4
1,2,3-Trichloropropane
NO
mg/l
0.00050
05/26/07
15:24
PPM
96-18-4
1,2,4-Trimethylbenzene
NO
mg/l
0.00050
05/26/07
15:24
PPM
95-63-6
1,3,5-Trimethylbenzene
NO
mg/l
0.00050
05/26/07
15:24
PPM
108-67-8
Vinyl chloride
NO
mg/l
0.00050
05/26/07
15:24
PPM
'75-01-4
m&p-Xylene
NO
mg/l
0.00050
05/26/07
15:24
PPM
o-Xylene
NO
mg/l
0.00050
05/26/07
15:24
PPM
95-47-6
1-Chloro-3-fluorobenzene (S)
97
%
05/26/07
15:24
PPM
625-98-9
Date: 05/30/07
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,N RCCO,,"
O cf
Page: 20 of 54
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

ace Analytical °
www.pacelabs.cnm
Lab Sample No: 928404276
Client Sample ID: MW-07
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-005 Date Collected: 05/18/07 15:10
Matrix: Water Date Received: 05/18/07 17:26
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Microbiology
Fecal Coliform in Water Method: SM 9222D
Coliform, Fecal ND col/100ml 1.0 05/18/07 17:30 JMW
Wet Chemistry
Total Dissolved Solids Method: EPA 160.1
Total Dissolved Solids 70. mg/l
Chloride (Mercuric Nitrate) Method: EPA 325.2
Chloride 8.6 mg/l
Ammonia
Nitrogen, Ammonia
48 Hour NO3 / NO2 / NOX
Nitrate as N
Sulfate,Turbidimetric
Sulfate
Total Organic Carbon
Total Organic Carbon
GUMS Semivolatiles
Semivolatile Organics
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(k)fluoranthene
Benzo(b)fluoranthene
Benzo(a)anthracene
Benzoic acid
Benzo(g,h,i)perylene
Benzyl alcohol
Benzo(a)pyrene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
Date: 05/30/07
Method: EPA 350.1
NO mg/1
Method: EPA 353.2
2.2 mg/l
Method: EPA 375.4
5.9 mg/1
Method: SM 5310B
3.6 mg/l
20. 05/20/07 17:48 SER
5.0 05/21/07 12:37 JDA1 16887-00-6
0.10 05/22/07 17:34 SAJ 7727-37-9
0.10 05/18/07 22:23 JMW
5.0 . 05/25/07 09:15 JDA1
1.0 05/21/07 19:00 SAJ 7440-44-0
Prep/Method: EPA 3510 / EPA 8270
NO
ug/1
12.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
ND
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
62.
NO
ug/l
12.
NO
ug/l
25.
ND
ug/l
12.
ND
ug/l
12.
ND
ug/l
12.
ND
ug/l
25.
05/24/07 16:40 BET 83-32-9
05/24/07 16:40 BET 208-96-8
05/24/07 16:40 BET 62-53-3
05/24/07 16:40 BET 120-12-7
05/24/07 16:40 BET 207-08-9
05/24/07 16:40 BET 205-99-2
05/24/07 16:40 BET 56-55-3
05/24/07 16:40 BET 65-85-0
05/24/07 16:40 BET 191-24-2
05/24/07 16:40 BET 100-51-6
05/24/07 16:40 BET 50-32-8
05/24/07 16:40 BET 101-55-3
05/24/07 16:40 BET 85-68-7
05/24/07 16:40 BET 59-50-7
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 �" ACCO,, 9
�o
a \_
Page: 21 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Lab Sample No: 928404276
Client Sample ID: MW-07
race Hud►yucd► aerv►ces, ►nc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
race Hna►y►rca► aerv►ces, inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-005 Date Collected: 05/18/07 15:10
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
4-Chloroaniline
ND
ug/l
25.
05/24/07
16:40
BET
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/l
12.
05/24/07
16:40
BET
111-91-1
bis(2-Chloroethyl) ether
ND
ug/l
12.
05/24/07
16:40
BET
111-44-4
bis(2-Chloroisopropyl) ether
ND
ug/l
12.
05/24/07
16:40
BET
39638-32-9
2-Chloronaphthalene
ND
ug/l
12.
05/24/07
16:40
BET
91-58-7
2-Chlorophenol
ND
ug/l
12.
05/24/07
16:40
BET
95-57-8
4-Chlorophenylphenyl ether
ND
ug/l
12.
05/24/07
16:40
BET
7005-72-3
Chrysene
ND
ug/1
12.
05/24/07
16:40
BET
218-01-9
Dibenz(a,h)anthracene
ND
ug/l
12.
05/24/07
16:40
BET
53-70-3
Dibenzofuran
ND
ug/l
12.
05/24/07
16:40
BET
132-64-9
1,2-Dichlorobenzene
ND
ug/l
12.
05/24/07
16:40
BET
95-50-1
1,3-Dichlorobenzene
ND
ug/l
12.
05/24/07
16:40
BET
541-73-1
1.4-Dichlorobenzene
ND
ug/l
12.
05/24/07
16:40
BET
106-46-7
3.3'-Dichlorobenzidine
ND
ug/l
25.
05/24/07
16:40
BET
91-94-1
2,4-Dichlorophenol
ND
ug/l
12.
05/24/07
16:40
BET
120-83-2
Diethylphthalate
ND
ug/l
12.
05/24/07
16:40
BET
84-66-2
2.4-Dimethylphenol
ND
ug/l
12.
05/24/07
16:40
BET
105-67-9
Dimethylphthalate
ND
ug/l
12.
05/24/07
16:40
BET
131-11-3_
Di-n-butylphthalate
ND
ug/1
12.
05/24/07
16:40
BET
84-74-2
4.6-Dinitro-2-methylphenol
ND
ug/l
62.
05/24/07
16:40
BET
534-52-1
2,4-Dinitrophenol
ND
ug/l
62.
05/24/07
16:40
BET
51-28-5
2.4-Dinitrotoluene
ND
ug/l
12.
05/24/07
16:40
BET
121-14-2
2,6-Dinitrotoluene
ND
ug/l
12.
05/24/07
16:40
BET
606-20-2
Di-n-octylphthalate
ND
ug/l
12.
05/24/07
16:40
BET
117-84-0
1.2-Diphenylhydrazine
ND
ug/l
25.
05/24/07
16:40
BET
122-66-7
bis(2-Ethylhexyl)phthalate
ND
ug/l
12.
05/24/07
16:40
BET
117-81-7
Fluoranthene
ND
ug/l
12.
05/24/07
16:40
BET
206-44-0
Fluorene
ND
ug/l
12.
05/24/07
16:40
BET
86-73-7
Hexachloro-1,3-butadiene
ND
ug/l
12.
05/24/07
16:40
BET
87-68-3
Hexachlorobenzene
ND
ug/l
12.
05/24/07
16:40
BET
118-74-1
Hexachlorocyclopentadiene
ND
ug/1
12.
05/24/07
16:40
BET
77-47-4
Hexachloroethane
ND
ug/l
12.
05/24/07
16:40
BET
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/l
12.
05/24/07
16:40
BET
193-39-5
Isophorone
ND
ug/l
12.
05/24/07
16:40
BET
78-59-1
1-Methylnaphthalene
ND
ug/l
12.
05/24/07
16:40
BET
90-12-0
2-Methylnaphthalene
ND
ug/l
12.
05/24/07
16:40
BET
91-57-6
2-Methylphenol (o-Cresol)
ND
ug/l
12.
05/24/07
16:40
BET
95-48-7
3&4-Methylphenol
ND
ug/l
12.
05/24/07
16:40
BET
Naphthalene
ND
ug/l
12.
05/24/07
16:40
BET
91-20-3
Date: 05/30/07 Page: 22 of 54
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS Charlotte Certification IN
NC Wastewater 40 NC Wastewater 12
NC Drinking Water 37712 This report shall not be reproduced, except in full, NC Drinking Water 37706
Sc 99030 without the written consent of Pace Analytical Services, Inc. Sc 99006
FL NELAP E87648 ° `µ pc`°�'° FL NELAP E87627
lE
< ( x

aceAnalytical°
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Lab Sample No: 928404276 Project Sample Number: 92144916-005 Date Collected: 05/18/07 15:10
Client Sample ID: MW-07 Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
2-Nitroaniline
ND
ug/l
62.
05/24/07
16:40
BET
88-74-4
3-Nitroaniline
ND
ug/l
62.
05/24/07
16:40
BET
99-09-2
4-Nitroaniline
ND
ug/l
62.
05/24/07
16:40
BET
100-01-6
Nitrobenzene
ND
ug/l
12.
05/24/07
16:40
BET
98-95-3
2-Nitrophenol
ND
ug/l
12.
05/24/07
16:40
BET
88-75-5
4-Nitrophenol
ND
ug/l
62.
05/24/07
16:40
BET
100-02-7
N-Nitrosodimethylamine
ND
ug/l
12.
05/24/07
16:40
BET
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/l
12.
05/24/07
16:40
BET
621-64-7
N-Nitrosodiphenylamine
ND
ug/l
12.
05/24/07
16:40
BET
86-30-6
Pentachlorophenol
ND
ug/l
62.
05/24/07
16:40
BET
87-86-5
Phenanthrene
ND
ug/l
12.
05/24/07
16:40
BET
85-01-8
Phenol
ND
ug/l
12.
05/24/07
16:40
BET
108-95-2
Pyrene
ND
ug/l
12.
05/24/07
16:40
BET
129-00-0
1,2.4-Trichlorobenzene
ND
ug/l
12.
05/24/07
16:40
BET
120-82-1
2,4.5-Trichlorophenol
ND
ug/l
62.
05/24/07
16:40
BET
95-95-4
2.4.6-Trichlorophenol
ND
ug/l
12.
05/24/07
16:40
BET
88-06-2
Nitrobenzene-d5 (S)
86
%
05/24/07
16:40
BET
4165-60-0
2-Fluorobiphenyl (S)
100
%
05/24/07
16:40
BET
321-60-8
Terphenyl-d14 (S)
102
%
05/24/07
16:40
BET
1718-51-0
Phenol-d5 (S)
50
%
05/24/07
16:40
BET
4165-62-2
2-Fluorophenol (S)
57
%
05/24/07
16:40
BET
367-12-4
2.4.6-Tribromophenol (S)
108
%
05/24/07
16:40
BET
118-79-6
Date Extracted
05/22/07
05/22/07
GC Volatiles
GC VOCs in Water
Method: SM
6230D
Benzene
ND
mg/l
0.00050
05/26/07
16:06
PPM
71-43-2
Bromobenzene
ND
mg/l
0.00050
05/26/07
16:06
PPM
108-86-1
Bromochloromethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
74-97-5
Bromodichloromethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
75-27-4
Bromoform
ND
mg/l
0.00050
05/26/07
16:06
PPM
75-25-2
Bromomethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
74-83-9
.n-Butylbenzene
ND
mg/l
0.0010
05/26/07
16:06
PPM
104-51-8
sec-Butylbenzene
ND
mg/l
0.00050
05/26/07
16:06
PPM
135-98-8
tert-Butylbenzene
ND
mg/l
0,00050
05/26/07
16:06
PPM
98-06-6
Carbon tetrachloride
ND
mg/l
0.00050
05/26/07
16:06
PPM
56-23-5
Chlorobenzene
ND
mg/l
0.00050
05/26/07
16:06
PPM
108-90-7
Chloroethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
75-00-3
Chloroform
ND
mg/l
0.00050
05/26/07
16:06
PPM
67-66-3
Date: 05/30/07 Page: 23 of 54
Asheville Certification IN REPORT OF LABORATORY ANALYSIS Charlotte Certification IDs
NC Wastewater 40 NC Wastewater 12
NC Drinking Water 37712 This report shall not be reproduced, except in full, NC Drinking Water 37706
Sc 99030 without the written consent of Pace Analytical Services, Inc. SC 99006
FL NELAP E87648 0 ,N ACCpRo
Aye FL NELAP E87627

ace Analytical °
www.paceiabs.com
Lab Sample No: 928404276
Client Sample ID: MW-07
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-005 Date Collected: 05/18/07 15:10
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Chloromethane
ND
mg/l
0.0020
05/26/07
16:06
PPM
74-87-3
2-Chlorotoluene
ND
mg/l
0.00050
05/26/07
16:06
PPM
95-49-8
4-Chlorotoluene
ND
mg/l
0.00050
05/26/07
16:06
PPM
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/l
0.0020
05/26/07
16:06
PPM
96-12-8
Dibromochloromethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/l
0.00050
05/26/07
16:06
PPM
106-93-4
Dibromomethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
74-95-3
1,2-Dichlorobenzene
ND
mg/l
0.0010
05/26/07
16:06
PPM
95-50-1
1,3-Dichlorobenzene
NO
mg/l
0.0010
05/26/07
16:06
PPM
541-73-1
1,4-Dichlorobenzene
ND
mg/l
0.0010
05/26/07
16:06
PPM
106-46-7
Dichlorodifluoromethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
75-71-8
1.1-Dichloroethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
75-34-3
1,2-Dichloroethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
107-06-2
1,1-Dichloroethene
ND
mg/l
0.00050
05/26/07
16:06
PPM
75-35-4
cis-1,2-Dichloroethene
ND
mg/l
0.00050
05/26/07
16:06
PPM
156-59-2
trans-1,2-Dichloroethene
ND
mg/l
0.00050
05/26/07
16:06
PPM
156-60-5
1.2-Dichloropropane
ND
mg/l
0.00050
05/26/07
16:06
PPM
78-87-5
1,3-Dichloropropane
ND
mg/l
0.00050
05/26/07
16:06
PPM
142-28-9
2,2-Dichloropropane
ND
mg/l
0.00050
05/26/07
16:06
PPM
594-20-7
1,1-Dichloropropene
ND
mg/l
0.00050
05/26/07
16:06
PPM
563-58-6
cis-1,3-Dichloropropene
ND
mg/l
0.00050
05/26/07
16:06
PPM
10061-01-5
trans-1,3-Dichloropropene
ND
mg/l
0.00050
05/26/07
16:06
PPM
10061-02-6
Diisopropyl ether
ND
mg/l
0.00050
05/26/07
16:06
PPM
108-20-3
Ethylbenzene
ND
mg/l
0.00050
05/26/07
16:06
PPM
100-41-4
Hexachloro-1.3-butadiene
ND
mg/l
0.0020
05/26/07
16:06
PPM
87-68-3
Isopropylbenzene (Cumene)
ND
mg/l
0.00050
05/26/07
16:06
PPM
98-82-8
p-Isopropyltoluene
ND
mg/l
0.0010
05/26/07
16:06
PPM
99-87-6
Methylene chloride
ND
mg/l
0.0020
05/26/07
16:06
PPM
75-09-2
Methyl-tert-butyl ether
ND
mg/l
0.00050
05/26/07
16:06
PPM
1634-04-4
Naphthalene
ND
mg/l
0.0020
05/26/07
16:06
PPM
91-20-3
n-Propylbenzene
ND
mg/l
0.00050
05/26/07
16:06
PPM
103-65-1
Styrene
ND
mg/l
0.00050
05/26/07
16:06
PPM
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
79-34-5
Tetrachloroethene
ND
mg/l
0.00050
05/26/07
16:06
PPM
127-18-4
Toluene
ND
mg/l
0.00050
05/26/07
16:06
PPM
108-88-3
1,2,3-Trichlorobenzene
ND
mg/l
0.0020
05/26/07
16:06
PPM
87-61-6
1,2,4-Trichlorobenzene
ND
mg/l
0.0020
05/26/07
16:06
PPM
120-82-1
1,1,1-Trichloroethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
71-55-6
Date: 05/30/07
Page: 24 of 54
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IDs
NC Wastewater
NC Drinking Water
40
37712
This report shall not be reproduced, except in full,
NC Wastewater
12
Sc
99030
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water
37706
FL NELAP
E87648
0 ,H AC Cl'
��
_WA'
Sc
FL NELAP
99006
E87627
% P[:N4

q
e Analytical °
www.pacelabs.com
Lab Sample No: 928404276
Client Sample ID: MW-07
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-005 Date Collected: 05/18/07 15:10
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
1,1,2-Trichloroethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
79-00-5
Trichloroethene
ND
mg/1
0.00050
05/26/07
16:06
PPM
79-01-6
Trichlorofluoromethane
ND
mg/l
0.00050
05/26/07
16:06
PPM
75-69-4
1.2,3-Trichloropropane
ND
mg/l
0.00050
05/26/07
16:06
PPM
96-18-4
1,2,4-Trimethylbenzene
ND
mg/l
0.00050
05/26/07
16:06
PPM
95-63-6
1,3,5-Trimethylbenzene
ND
mg/l
0.00050
05/26/07
16:06
PPM
108-67-8
Vinyl chloride
ND -
mg/l
0.00050
05/26/07
16:06
PPM
75-01-4
m&p-Xylene
ND
mg/l
0.00050
05/26/07
16:06
PPM
o-Xylene
ND
mg/l
0.00050
05/26/07
16:06
PPM
95-47-6
1-Chloro-3-fluorobenzene (S)
96
%
05/26/07
16:06
PPM
625-98-9
Date: 05/30/07
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 .�� " FCpOgo4y
Page: 25 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

are Analytical °
www.pacelabs.com
Lab Sample No: 928404284
Client Sample ID: MW-08
Parameters
Microbiology
Fecal Coliform in Water
Coliform, Fecal
Wet Chemistry
Total Dissolved Solids
Total Dissolved Solids
Chloride (Mercuric Nitrate)
Chloride
Ammonia
Nitrogen. Ammonia
48 Hour NO3 / NO2 / NOX
Nitrate as N
Sulfate.Turbidimetric
Sulfate
Total Organic Carbon
Total Organic Carbon
GUMS Semivolatiles
Semivolatile Organics
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(k)fluoranthene
Benzo(b)fluoranthene
Benzo(a)anthracene
Benzoic acid
Benzo(g,h.i)perylene
Benzyl alcohol
Benzo(a)pyrene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
Date: 05/30/07
Results
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-006 Date Collected: 05/18/07 15:55
Matrix: Water Date Received: 05/18/07 17:26
Units Report Limit Analyzed By CAS No. Qual RegLmt
Method: SM 9222D
NO col/100ml
Method: EPA 160.1
290 mg/l
Method: EPA 325.2
15. mg/l
Method: EPA 350.1
NO mg/l
Method: EPA 353.2
3.0 mg/l
Method: EPA 375.4
13. mg/l
Method: SM 5310B
5.0 mg/l
1.0 05/18/07 17:30 JMW
20. 05/20/07 17:48 SER
5.0 05/21/07 12:37 JDA1 16887-00-6
0.10 05/22/07 17:34 SAJ 7727-37-9
0.10 05/18/07 22:23 JMW
5.0 05/25/07 09:15 JDA1
1.0 05/21/07 19:00 SAJ 7440-44-0
Prep/Method: EPA 3510 / EPA 8270
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
ND
ug/l
12.
NO
ug/l
12.
NO
ug/l
12.
NO
ug/l
60.
NO
ug/l
12.
NO
ug/l
24.
NO
ug/l
12.
ND
ug/l
12.
NO
ug/l
12.
NO
ug/l
24.
05/24/07 17:01.BET 83-32-9
05/24/07 17:01 BET. 208-96-8
05/24/07 17:01 BET 62-53-3
05/24/07 17:01 BET 120-12-7
05/24/07 17:01 BET 207-08-9
05/24/07 17:01 BET 205-99-2
05/24/07 17:01 BET 56-55-3
05/24/07 17:01 BET 65-85-0
05/24/07 17:01 BET 191-24-2
05/24/07 17:01 BET 100-51-6
05/24/07 17:01 BET 50-32-8
05/24/07 17:01 BET 101-55-3
05/24/07 17:01 BET 85-68-7
05/24/07 17:01 BET 59-50-7
Asheville Certification lDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 " ACC,.,"
� 4
Page: 26 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

dce Analytical °
www.pacelabs.com
Lab Sample No: 928404284
Client Sample ID: MW-08
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-006 Date Collected: 05/18/07 15:55
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No.Qua] RegLmt
4-Chloroaniline
ND
ug/l
24.
05/24/07
17:01
BET
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/l
12.
05/24/07
17:01
BET
111-91-1
bis(2-Chloroethyl) ether
ND
ug/l
12.
05/24/07
17:01
BET
111-44-4
bis(2-Chloroisopropyl) ether
ND
ug/l
12.
05/24/07
17:01
BET
39638-32-9
2-Chloronaphthalene
ND
ug/1
12.
05/24/07
17:01
BET
91-58-7
2-Chlorophenol
ND
ug/l
12.
05/24/07
17:01
BET
95-57-8
4-Chlorophenylphenyl ether
ND
ug/l
12.
05/24/07
17:01
BET
7005-72-3
Chrysene
ND
ug/l
12.
05/24/07
17:01
BET
218-01-9
Dibenz(a,h)anthracene
ND
ug/l
12.
05/24/07
17:01
BET
53-70-3
Dibenzofuran .
ND
ug/l
12.
05/24/07
17:01
BET
132-64-9'
1,2=Dichlorobenzene
ND
ug/l
12.
05/24/07
17:01
BET
95-50-1
1.3-Dichlorobenzene
ND
ug/l
12.
05/24/07
17:01
BET
541-73-1
1,4-Dichlorobenzene
ND
ug/l
12.
05/24/07
17:01
BET
106-46-7
3,3'-Dichlorobenzidine
ND
ug/l
24.
05/24/07
17:01
BET
91-94-1
2,4-Dichlorophenol
ND
ug/l
12.
05/24/07
17:01
BET
120-83-2
Diethylphthalate
ND
ug/l
12.
05/24/07
17:01
BET
84-66-2
2,4-Dimethylphenol
ND
ug/l
12.
05/24/07
17:01
BET
105-67-9
Dimethylphthalate
ND
ug/l
12.
05/24/07
17:01
BET
131-11-3
Di-n-butylphthalate
ND
ug/l
12.
05/24/07
17:01
BET
84-74-2
4.6-Dinitro-2-methylphenol
ND
ug/l
60.
05/24/07
17:01
BET
534-52-1
2,4-Dinitrophenol
ND
ug/l
60.
05/24/07
17:01
BET
51-28-5
2.4-Dinitrotoluene
ND
ug/l
12.
05/24/07
17:01
BET
121-14-2
2,6-Dinitrotoluene
ND
ug/l
12.
05/24/07
17:01
BET
606-20-2
Di-n-octylphthalate
ND
ug/l
12.
05/24/07
17:01
BET
117-84-0
1,2-Diphenylhydrazine
ND
ug/1
24.
05/24/07
17:01
BET
122-66-7
bis(2-Ethylhexyl)phthalate
ND
ug/l
12.
05/24/07
17:01
BET
117-81-7
Fluoranthene
ND
ug/l
12.
05/24/07
17:01
BET
206-44-0
Fluorene
ND
ug/l
12.
05/24/07
17:01
BET
86-73-7
Hexachloro-1,3-butadiene
ND
ug/1
12.
05/24/07
17:01
BET
87-68-3
Hexachlorobenzene
ND
ug/l
12.
05/24/07
17:01
BET
118-74-1
Hexachlorocyclopentadiene
ND
ug/l
12.
05/24/07
17:01
BET
77-47-4
Hexachloroethane
ND
ug/l
12.
05/24/07
17:01
BET
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/l
12.
05/24/07
17:01
BET
193-39-5
Isophorone
ND
ug/l
12.
05/24/07
17:01
BET
78-59-1
1-Methylnaphthalene
ND
ug/l
12.
05/24/07
17:01
BET
90-12-0
2-Methylnaphthalene
ND
ug/l
12.
05/24/07
17:01
BET
91-57-6
2-Methylphenol (o-Cresol)
ND
ug/1
12.
05/24/07
17:01
BET
95-48-7
3&4-Methylphenol
ND
ug/l
12.
05/24/07
17:01
BET
Naphthalene
ND
ug/l
12.
05/24/07
17:01
BET
91-20-3
Date: 05/30/07
Page: 27 of 54
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
Sc 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,N AC Co,,,,
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax. [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Lab Sample No: 928404284
Project Sample
Number:
92144916-006 Date Collected: 05/18/07 15:55
Client Sample ID: MW-08
Matrix:
Water
Date Received: 05/18/07 17:26
Parameters
Results
Units Report Limit
Analyzed
By
CAS No. Qual RegLmt
2-Nitroaniline
ND
ug/l
60.
05/24/07
17:01
BET
88.74-4
3-Nitroaniline
ND
ug/l
60.
05/24/07
17:01
BET
99-09-2
4-Nitroaniline
ND
ug/l
60,
05/24/07
17:01
BET
100-01-6
Nitrobenzene
ND
ug/l
12.
05/24/07
17:01
BET
98-95-3
2-Nitrophenol
ND
ug/l
12.
05/24/07
17:01
BET
88-75-5
4-Nitrophenol
ND
ug/l
60.
05/24/07
17:01
BET
100-02-7
N-Nitrosodimethylamine
ND
ug/l
12.
05/24/07
17:01
BET
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/l
12.
05/24/07
17:01
BET
621-64-7
N-Nitrosodiphenylamine
ND
ug/l
12.
05/24/07
17:01
BET
86-30-6
Pentachlorophenol
ND
ug/l
60.
05/24/07
17:01
BET
87-86-5
Phenanthrene
ND
ug/l
12.
05/24/07
17:01
BET
85-01-8
Phenol
ND
ug/l
12.
05/24/07
17:01
BET
108-95-2
Pyrene
ND
ug/l
12.
05/24/07
17:01
BET
129-00-0
1,2,4-Trichlorobenzene
ND
ug/l
12.
05/24/07
17:01
BET
120-82-1
2,4,5-Trichlorophenol
ND
ug/l
60.
05/24/07
17:01
BET
95-95-4
2,4,6-Trichlorophenol
ND
ug/l
12.
05/24/07
17:01
BET
88-06-2
Nitrobenzene-d5 (S)
87
%
05/24/07
17:01
BET
4165-60-0
2-Fluorobiphenyl (S)
96
%
05/24/07
17:01
BET
321-60-8
Terphenyl-d14 (S)
106
%
05/24/07
17:01
BET
1718-51-0
Phenol-d5 (S)
48
%
05/24/07
17:01
BET
4165-62-2
2-Fluorophenol (S)
54
Y.
05/24/07
17:01
BET
367-12-4
2,4,6-Tribromophenol (S)
110
%
05/24/07
17:01
BET
118-79-6
Date Extracted
05/22/07
05/22/07
GC Volatiles
GC VOCs in Water
Method: SM 6230D
Benzene
ND
mg/l
0.00050
05/26/07
16:48
PPM
71-43-2
Bromobenzene
ND
mg/l
0.00050
05/26/07
16:48
PPM
108-86-1
Bromochloromethane
ND
mg/l
0.00050
05/26/07
16:48
PPM
74-97-5
Bromodichloromethane
ND
mg/l
0.00050
05/26/07
16:48
PPM
75-27-4
Bromoform
ND
mg/l
0.00050
05/26/07
16:48
PPM
75-25-2
Bromomethane
ND
mg/l
0.00050
05/26/07
16:48
PPM
74-83-9
n-Butylbenzene
ND
mg/l
0.0010
05/26/07
16:48
PPM
104-51-8
sec-Butylbenzene
ND
mg/l
0.00050
05/26/07
16:48
PPM
135-98-8
tert-Butylbenzene
ND
mg/l
0.00050
05/26/07
16:48
PPM
98-06-6
Carbon tetrachloride
ND
mg/l
0.00050
05/26/07
16:48
PPM
56-23-5
Chlorobenzene
ND
mg/l
0.00050
05/26/07
16:48
PPM
108-90-7
Chloroethane
ND
mg/l
0.00050
05/26/07
16:48
PPM
75-00-3
Chloroform
ND
mg/l
0.00050
05/26/07
16:48
PPM
67-66-3
Date: 05/30/07
Page: 28 of 54
Asheville Certification IDs
REPORT OF
LABORATORY ANALYSIS
Charlotte Certification IDs
NC Wastewater 40
NC Wastewater 12
NC Drinking Water 37712
This report
shall
not be reproduced,
except in full,
NC Drinking Water 37706
Sc 99030
without the
written
consent of Pace Analytical Services, Inc.
Sc
FL NELAP E87648
N ACCpg0
4,*f-
99006
FL NELAP E87627
C
W �P

aceAnalytical °
www.pacelabs.com
Lab Sample No: 928404284
Client Sample ID: MW-08
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-006 Date Collected: 05/18/07 15:55
Matrix: Water Date Received: 05/18/07 17:26
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Chloromethane
NO
mg/l
0.0020
05/26/07
16:48
PPM
74-87-3
2-Chlorotoluene
NO
mg/l
0.00050
05/26/07
16:48
PPM
95-49-8
4-Chlorotoluene
NO
mg/l
0.00050
05/26/07
16:48
PPM
106-43-4
1,2-Dibromo-3-chloropropane
NO
mg/l
0.0020
05/26/07
16:48
PPM
96-12-8
Dibromochloromethane
NO
mg/l
0.00050
05/26/07
16:48
PPM
124-48-1
1,2-Dibromoethane (EDB)
NO
mg/l
0.00050
05/26/07
16:48
PPM
106-93-4
Dibromomethane
NO
mg/l
0.00050
05/26/07
16:48
PPM
74-95-3
1,2-Dichlorobenzene
NO
mg/l
0.0010
05/26/07
16:48
PPM
95-50-1
1,3-Dichlorobenzene
NO
mg/l
0.0010
05/26/07
16:48
PPM
541-73-1
1,4-Dichlorobenzene
NO
mg/l
0.0010
05/26/07
16:48
PPM
106-46-7
Dichlorodifluoromethane
ND
mg/l
0.00050
05/26/07
16:48
PPM
75-71-8
1.1-Dichloroethane
NO
mg/l
0.00050
05/26/07
16:48
PPM
75-34-3
1,2-Dichloroethane
NO
mg/l
0.00050
05/26/07
16:48
PPM
107-06-2
1.1-Dichloroethene
NO
mg/l
0.00050
05/26/07
16:48
PPM
75-35-4
cis-1,2-Dichloroethene
NO
mg/l
0.00050
05/26/07
16:48
PPM
156-59-2
trans-1,2-Dichloroethene
NO
mg/l
0.00050
05/26/07
16:48
PPM
156-60-5
1,2-Dichloropropane
NO
mg/l
0.00050
05/26/07
16:48
PPM
78-87-5
1,3-Dichloropropane
NO
mg/l
0.00050
05/26/07
16:48
PPM
142-28-9
2,2-Dichloropropane
ND
mg/l
0.00050
05/26/07
16:48
PPM
594-20-7
1.1-Dichloropropene
NO
mg/l
0.00050
05/26/07
16:48
PPM
563-58-6
cis-1,3-Dichloropropene
NO
mg/l
0.00050
05/26/07
16:48
PPM
10061-01-5
trans-1,3-Dichloropropene
NO
mg/l
0.00050
05/26/07
16:48
PPM
10061-02-6
Diisopropyl ether
NO
mg/l
0.00050
05/26/07
16:48
PPM
108-20-3
Ethylbenzene
NO
mg/l
0.00050
05/26/07
16:48
PPM
100-41-4
Hexachloro-1.3-butadiene
NO
mg/l
0.0020
05/26/07
16:48
PPM
87-68-3
Isopropylbenzene (Cumene)
NO
mg/l
0.00050
05/26/07
16:48
PPM
98-82-8
p-Isopropyltoluene
NO
mg/l
0.0010
05/26/07
16:48
PPM
99-87-6
Methylene chloride
NO
mg/l
0.0020
05/26/07
16:48
PPM
75-09-2
Methyl-tert-butyl ether
ND
mg/l
0.00050
05/26/07
16:48
PPM
1634-04-4
Naphthalene
NO
mg/l
0.0020
05/26/07
16:48
PPM
91-20-3
n-Propylbenzene
NO
mg/l
0.00050
05/26/07
16:48
PPM
103-65-1
Styrene
NO
mg/l
0.00050
05/26/07
16:48
PPM
100-42-5
1,1,1,2-Tetrachloroethane
NO
mg/l
0,00050
05/26/07
16:48
PPM
630-20-6
1,1,2,2-Tetrachloroethane
NO
mg/l
0.00050
05/26/07
16:48
PPM
79-34-5
Tetrachloroethene
NO
mg/l
0.00050
05/26/07
16:48
PPM
127-18-4
Toluene
NO
mg/l
0.00050
05/26/07
16:48
PPM
108-88-3
1,2,3-Trichlorobenzene
NO
mg/l
0.0020
05/26/07
16:48
PPM
87-61-6
1.2,4-Trichlorobenzene
NO
mg/l
0.0020
05/26/07
16:48
PPM
120-82-1
1,1,1-Trichloroethane
NO
mg/l
0.00050
05/26/07
16:48
PPM
71-55-6
Date: 05/30/07
Page: 29 of 54
Asheville Certification IN
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IN
NC Wastewater
NC Drinking Water
40
37712
This report shall not be reproduced, except in full,
NC Wastewater
12
Sc
99030
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water
37706
Sc
99006
FL NELAP
E87648
N Ac`°"°
FL NELAP
E87627
4

ace Analytical °
www.pacelabs.com
Lab Sample No: 928404284
Client Sample ID: MW-08
Parameters
Results
1,1,2-Trichloroethane
ND
Trichloroethene
ND
Trichlorofluoromethane
ND
1,2,3-Trichloropropane
ND
1,2,4-Trimethylbenzene
ND
1,3,5-Trimethylbenzene
ND
Vinyl chloride
ND
m&p-Xylene
ND
o-Xylene
ND
1-Chloro-3-fluorobenzene (S)
99
Date: 05/30/07
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Project Sample Number: 92144916-006 Date Collected: 05/18/07 15:55
Matrix: Water Date Received: 05/18/07 17:26
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
mg/l
0.00050
05/26/07
16:48
PPM
79-00-5
mg/l
0.00050
05/26/07
16:48
PPM
79-01-6
mg/l
0.00050
05/26/07
16:48
PPM
75-69-4
mg/l
0.00050
05/26/07
16:48
PPM
96-18-4
mg/l
0.00050
05/26/07
16:48
PPM
95-63-6
mg/l
0.00050
05/26/07
16:48
PPM
108-67-8
mg/l
0.00050
05/26/07
16:48
PPM
75-01-4
mg/l
0.00050
05/26/07
16:48
PPM
mg/l
0.00050
05/26/07
16:48
PPM
95-47-6
%
05/26/07
16:48
PPM
625-98-9
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full,
Sc 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 „ AC CARD
Page: 30 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
PARAMETER FOOTNOTES
Method 9071E modified to use ASE.
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid.
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
(S) Surrogate
Date: 05/30/07
Asheville certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 " "`°°q q
Page: 31 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical Phone: [phone] Phone: [phone]
Fax: [phone] Fax., 828.252.4618
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92144916
Client Project ID: Clement Pappas
QC Batch: 189785 Analysis Method: SM 6230D
QC Batch Method: SM 6230D Analysis Description: GC VOCs in Water
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276
928404284
METHOD BLANK: 928432087
Associated Lab Samples:
928404235
928404243
928404250 928404268 928404276 928404284
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Benzene
ug/l
ND
0.50
Bromobenzene
ug/l
ND
0.50
Bromochloromethane
ug/l
ND
0.50
Bromodichloromethane
ug/l
ND
0.50
Bromoform
ug/l
NO
0.50
Bromomethane
ug/l
NO
0.50
n-Butylbenzene
ug/l
ND
1.0
sec-Butylbenzene
ug/l
ND
0.50
tert-Butylbenzene
ug/l
NO
0.50
Carbon tetrachloride
ug/l
NO
0.50
Chlorobenzene
ug/l
NO
0.50
Chloroethane
ug/l
ND
0.50
Chloroform
ug/l
NO
0.50
Chloromethane
ug/l
NO
2.0
2-Chlorotoluene
ug/l
NO
0.50
4-Chlorotoluene
ug/l
ND
0.50
1,2-Dibromo-3-chloropropane
ug/l
ND
2.0
Dibromochloromethane
ug/l
NO
0.50
1,2-Dibromoethane (EDB)
ug/l
NO
0.50
Dibromomethane
ug/l
NO
0.50
1,2-Dichlorobenzene
ug/l
NO
1.0
1,3-Dichlorobenzene
ug/l
NO
1.0
1,4-Dichlorobenzene
ug/l
ND
1.0
Dichlorodifluoromethane
ug/l
NO
0.50
1.1-Dichloroethane
ug/l
NO
0.50
1,2-Dichloroethane
ug/l
NO
0.50
1.1-Dichloroethene
ug/l
NO
0.50
cis-1,2-Dichloroethene
ug/l
ND
0.50
trans-1.2-Dichloroethene
ug/l
ND
0.50
1,2-Dichloropropane
ug/l
NO
0.50
Date: 05/30/07
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 �Eo ,N ACC0,9
Page: 32 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Analytical o Phone: 704.875.909
Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
METHOD BLANK: 928432087
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276 928404284
Blank
Reporting
Parameter
Units-
Result
Limit Footnotes
1,3-Dichloropropane
ug/l
NO
0.50
2,2-Dichloropropane
ug/l
ND
0.50
1,1-Dichloropropene
ug/l
NO
0.50
cis-1,3-Dichloropropene
ug/l
NO
0.50
trans-1,3-Dichloropropene
ug/l
NO
0.50
Diisopropyl ether
ug/l
NO
0.50
Ethylbenzene
ug/l
NO
0.50
Hexachloro-1,3-butadiene
ug/l
NO
2.0
Isopropylbenzene (Cumene)
ug/l
ND
0.50
p-Isopropyltoluene
ug/l
NO
1.0
Methylene chloride
ug/l
ND
2.0
Methyl-tert-butyl ether
ug/l
ND
0.50
Naphthalene
ug/l
NO
2.0
n-Propylbenzene
ug/l
ND
0.50
Styrene
ug/l
ND
0.50
1,1,1,2-Tetrachloroethane
ug/l
ND
0.50
1,1,2.2-Tetrachloroethane
ug/l
ND
0.50
Tetrachloroethene
ug/l
NO
0.50
Toluene
ug/l
ND
0.50
1,2,3-Trichlorobenzene
ug/l
ND
2.0
1,2.4-Trichlorobenzene
ug/l
ND
2.0
1,1,1-Trichloroethane
ug/l
NO
0.50
1,1,2-Trichloroethane
ug/l
NO
0.50
Trichloroethene
ug/l
ND
0.50
Trichlorofluoromethane
ug/l
ND
0.50
1,2,3-Trichloropropane
ug/l
ND
0.50
1,2.4-Trimethylbenzene
ug/l
ND
0.50
1.3,5-Trimethylbenzene
ug/l
ND
0.50
Vinyl chloride
ug/l
ND
0.50
m&p-Xylene
ug/l
NO
0.50
o-Xylene
ug/l
NO
0.50
1-Chloro-3-fluorobenzene (S)
%
98
Date: 05/30/07
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 N ACppg`Sy (lam
Page: 33 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
'Analytical o Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92144916
Client Project ID: Clement Pappas
LABORATORY CONTROL SAMPLE & LCSD: 928432095 928432103
Spike
LCS
LCSD
LCS
LCSD
Parameter
Units
Conc.
Result
Result
i Rec
i Rec
RPD
Benzene
ug/l
20.00
20.89
20.89
104
104
0
Bromobenzene
ug/l
20.00
20.97
22.35
105
112
6
Bromochloromethane
ug/l
20.00
21.43
20.76
107
104
3
Bromodichloromethane
ug/l
20.00
19.46
18.15
97
91
7
Bromoform
ug/l
20.00
23.76
22.68
119
113
5
Bromomethane
ug/l
20.00
21.20
21.95
106
110
3
n-Butylbenzene
ug/l
20.00
19.99
19.98
100
100
0
sec-Butylbenzene
ug/l
20.00
20.18
20.10
101
101
0
tert-Butylbenzene
ug/l
20.00
20.48
20.27
102
101
1
Carbon tetrachloride
ug/l
20.00
22.18
21.40
111
107
4
Chlorobenzene
ug/l
20.00
22.29
21.68
111
108
3
Chloroethane
ug/l
20.00
18.12
18.26
91
91
1
Chloroform
ug/l
20.00
21.58
19.91
108
100
8
Chloromethane
ug/l
20.00
14.02
14.12
70
71
1
2-Chlorotoluene
ug/l
20.00
24.27
22.97
121
115
6
4-Chlorotoluene
ug/l
20.00
21.25
23.16
106
116
9
1,2-Dibromo-3-chloropropane
ug/l
20.00
21.86
22.28
109
111
2
Dibromochloromethane
ug/l
20.00
21.62
21.24
108
106
2
1.2-Dibromoethane (EDB)
ug/l
20.00
22.89
21.31
114
107
7
Dibromomethane
ug/l
20.00
17.91
17.35
90
87
3
1,2-Dichlorobenzene
ug/l
20.00
22.60
23.36
113
117
3
1,3-Dichlorobenzene
ug/l
20.00
21.08
21.69
105
108
3
1,4-Dichlorobenzene
ug/l
20.00
20.41
21.33
102
107
4
Dichlorodifluoromethane
ug/l
20.00
14.51
14.56
72
73
0
1,1-Dichloroethane
ug/l
20.00
23.73
23.11
119
116
3
1,2-Dichloroethane
ug/l
20.00
21.98
20.23
110
101
8
1.1-Dichloroethene
ug/l
20.00
21.74
22.31
109
112
3
cis-1,2-Dichloroethene
ug/l
20.00
21.54
20.62
108
103
4
trans-1,2-Dichloroethene
ug/l
20.00
23.03
22.40
115
112
3
1,2-Dichloropropane
ug/l
20.00
20.90
21.06
104
105
1
1,3-Dichloropropane
ug/l
20.00
21.52
21.12
108
106
2
2.2-Dichloropropane
ug/l
20.00
20.77
19.64
104
98
6
1.1-Dichloropropene
ug/l
20.00
22.32
20.54
112
103
8
cis-1.3-Dichloropropene
ug/l
20.00
18.70
18.65
94
93
0
trans-1.3-Dichloropropene
ug/l
20.00
21.93
21.17
110
106
4
Diisopropyl ether
ug/l
20.00
19.03
19.08
95
95
0
Ethylbenzene
ug/l
20.00
21.57
21.44
108
107
1
Date; 05/30/07
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 \" ACCogo4
¢ s
Fnntnnfnc
Page: 34 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical0 Phone: [phone] Phone: [phone]
Fax [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92144916
Client Project ID: Clement Pappas
LABORATORY CONTROL SAMPLE & LCSD: 928432095 928432103
Spike
LCS
LCSD
LCS
LCSD
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
RPD
Hexachloro-1,3-butadiene
ug/l
20.00
21.11
21.98
106
110
4
Isopropylbenzene (Cumene)
ug/l
20.00
20.23
20.09
101
100
1
p-Isopropyltoluene
ug/l
20.00
20.67
20.53
103
103
1
Methylene chloride
ug/l
20.00
23.87
24.83
119
124
4
Methyl-tert-butyl ether
ug/l
20.00
19.61
19.64
98
98
0
Naphthalene
ug/l
20.00
19.26
20.19
96
101
5
n-Propylbenzene
ug/l
20.00
20.70
19.60
104
98
5
Styrene
ug/l
20.00
21.64
20.77
108
104
4
1,1,1,2-Tetrachloroethane
ug/l
20.00
20.78
20.53
104
103
1
1,1.2,2-Tetrachloroethane
ug/l
20.00
18.37
20.30
92
102
10
Tetrachloroethene
ug/l
20.00
19.39
18.47
97
92
5
Toluene
ug/l
20.00
20.25
20.06
101
100
1
1,2,3-Trichlorobenzene
ug/l
20.00
20.60
22.02
103
110
7
1,2,4-Trichlorobenzene
ug/l
20.00
19.82
21.03
99
105
6
1,1,1-Trichloroethane
ug/l
20.00
22.17
21.98
ill
110
1
1,1,2-Trichloroethane
ug/l
20.00
22.22
21.53
111
108
3
Trichloroethene
ug/l
20.00
18.77
18.47
94
92
2
Trichlorofluoromethane
ug/l
20.00
14.45
15.78
72
79
9
1,2,3-Trichloropropane
ug/l
20.00
23.25
21.79
116
109
7
1,2,4-Trimethylbenzene
ug/l
20.00
20.74
20.70
104
104
0
1,3,5-Trimethylbenzene
ug/l
20.00
20.20
20.23
101
101
0
Vinyl chloride
ug/l
20.00
15.51
15.93
78
80
3
m&p-Xylene
ug/l
40.00
37.46
36.91
94
92
1
o-Xylene
ug/l
20.00
19.00
19.46
95
97
2
1-Chloro-3-fluorobenzene (S)
104
103
SAMPLE DUPLICATE: 928432111
928401660
DUP
Parameter
Units
Result
Result
RPD Footnotes
Benzene
mg/l
ND
NO
NC
Bromobenzene
mg/l
ND
ND
NC
Bromochloromethane
mg/l
ND
NO
NC
Bromodichloromethane
mg/l
ND
NO
NC
Bromoform
mg/l
NO
NO
NC
Bromomethane
mg/l
ND
ND
NC
Date: 05/30/07
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NO Wastewater 40 This report shall not be reproduced, except in full,
NO Drinking Water 37712
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 ACCO,
i
a_
Footnotes
Page: 35 of 54
Charlotte Certification IDs
NO Wastewater 12
NO Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical o Phone: [phone] Phone: [phone]
Fax., 704.875.9091 Fax: [phone],
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92144916
Client Project ID: Clement Pappas
SAMPLE DUPLICATE: 928432111
928401660
DUP
Parameter
Units
Result
Result
RPD
n-Butylbenzene
mg/l
NO
ND
NC
sec-Butylbenzene
mg/1
NO
NO
NC
tert-Butylbenzene
mg/l
NO
NO
NC
Carbon tetrachloride
mg/l
NO
NO
NC
Chlorobenzene
mg/l
NO
NO
NC
Chloroethane
mg/l
NO
NO
NC
Chloroform
mg/l
ND
NO
NC
Chloromethane
mg/l
ND
NO
NC
2-Chlorotoluene
mg/l
ND
NO
NC
4-Chlorotoluene
mg/l
ND
ND
NC
1,2-Dibromo-3-chloropropane
mg/l
NO
ND
NC
Dibromochloromethane
mg/l
NO
NO
NC
1,2-Dibromoethane (EDB)
mg/l
NO
NO
NC
Dibromomethane
mg/l
NO
NO
NC
1,2-Dichlorobenzene
mg/l
ND
ND
NC
1,3-Dichlorobenzene
mg/1
NO
NO
NC
1,4-Dichlorobenzene
mg/l
NO
NO
NC
Dichlorodifluoromethane
mg/l
ND
NO
NC
1,1-Dichloroethane
mg/1
ND
NO
NC
1,2-Dichloroethane
mg/l
ND
NO
NC
1,1-Dichloroethene
mg/l
NO
ND
NC
cis-1,2-Dichloroethene
mg/l
NO
ND
NC
trans-1.2-Dichloroethene
mg/l
NO
NO
NC
1,2-Dichloropropane
mg/l
ND
NO
NC
1,3-Dichloropropane
mg/l
ND
NO
NC
2,2-Dichloropropane
mg/l
ND
NO
NC
1,1-Dichloropropene
mg/l
ND
NO
NC
cis-1,3-Dichloropropene
mg/l
ND
NO
NC
trans-1,3-Dichloropropene
mg/l
NO
ND
NC
Diisopropyl ether
mg/l
NO
NO
NC
Ethylbenzene
mg/l
NO
NO
NC
Hexachloro-1,3-butadiene
mg/l
ND
NO
NC
Isopropylbenzene (Cumene)
mg/l
ND
ND
NC
p-Isopropyltoluene
mg/l
ND
ND
NC
Methylene chloride
mg/l
NO
ND
NC
Methyl-tert-butyl ether
mg/l
NO
NO
NC
Naphthalene
mg/l
NO
NO
NC
Date: 05/30/07
Footnotes
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
N ACCCRQ
FL NELAP E87648 �Eo ,�
it 11AO\£.
Page: 36 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical'
Phone: [phone] Phone: [phone]
A
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92144916
Client Project ID: Clement Pappas
SAMPLE DUPLICATE: 928432111
928401660
DUP
Parameter
Units
Result
Result
RPD Footnotes
n-Propylbenzene
mg/l
ND
ND
NC
Styrene
mg/l
ND
ND
NC
1,1,1,2-Tetrachloroethane
mg/l
ND
ND
NC
1,1,2,2-Tetrachloroethane
mg/l
ND
ND
NC
Tetrachloroethene
mg/l
ND
ND
NC
Toluene
mg/l
ND
ND
NC
1,2,3-Trichlorobenzene
mg/l
ND
ND
NC
1,2,4-Trichlorobenzene
mg/l
ND
ND
NC
1,1,1-Trichloroethane
mg/l
ND
ND
NC
1,1,2-Trichloroethane
mg/l
ND
ND
NC
Trichloroethene
mg/l
ND
ND
NC
Trichlorofluoromethane
mg/l
ND
ND
NC
1,2,3-Trichloropropane
mg/l
ND
ND
NC
1,2,4-Trimethylbenzene
mg/l
ND
ND
NC
1,3,5-Trimethylbenzene
mg/l
ND
ND
NC
Vinyl chloride
mg/1
ND
ND
NC
m&p-Xylene
mg/l
ND
ND
NC
o-Xylene
mg/l
ND
ND
NC
1-Chloro-3-fluorobenzene (S)
%
97
100
Date: 05/30/07
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 "uin]P`11-1�t
"
11
Page: 37 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

rdGC HlldlyllUdl OVI Vl(;M, MG.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Analytical o Phone: 704.875.909
Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
rdGC AildlyflUdl OUTMCS, 111G.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
QC Batch: 189343 Analysis Method: EPA 8270
QC Batch Method: EPA 3510 Analysis Description: Semivolatile Organics
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276
928404284
METHOD BLANK: 928414119
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276 928404284
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Acenaphthene
ug/l
NO
10.
Acenaphthylene
ug/l
ND
10.
Aniline
ug/l
NO
10.
Anthracene
ug/l
NO
10.
Benzo(k)fluoranthene
ug/l
NO
10.
Benzo(b)fluoranthene
ug/l
NO
10.
Benzo(a)anthracene
ug/l
ND
10.
Benzoic acid
ug/l
NO
50.
Benzo(g,h,i)perylene
ug/l
NO
10.
Benzyl alcohol
ug/l
NO
20.
Benzo(a)pyrene
ug/l
NO
10.
4-Bromophenylphenyl ether
ug/l
ND
10.
Butylbenzylphthalate
ug/l
NO
10.
4-Chloro-3-methylphenol
ug/l
NO
20.
4-Chloroaniline
ug/l
NO
20.
bis(2-Chloroethoxy)methane
ug/l
NO
10.
bis(2-Chloroethyl) ether
ug/l
ND
10.
bis(2-Chloroisopropyl) ether
ug/1
NO
10.
2-Chloronaphthalene
ug/l
NO
10.
2-Chlorophenol
ug/l
NO
10.
4-Chlorophenylphenyl ether
ug/l
NO
10.
Chrysene
ug/l
NO
10.
Dibenz(a,h)anthracene
ug/l
NO
10.
Dibenzofuran
ug/l
NO
10.
1,2-Dichlorobenzene
ug/l
NO
10.
1,3-Dichlorobenzene
ug/1
NO
10.
1,4-Dichlorobenzene
ug/l
ND
10.
3,3'-Dichlorobenzidine
ug/l
NO
20.
2,4-Dichlorophenol
ug/l
NO
10.
Diethylphthalate
ug/l
NO
10.
Date: 05/30/07
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 ppp %0 "°"°"°
♦ / 4'
FF
a x
Page: 38 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92144916
Client Project ID: Clement Pappas
METHOD BLANK: 928414119
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276 928404284
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
2,4-Dimethylphenoi
ug/1
NO
10.
Dimethylphthalate
ug/l
NO
10.
Di-n-butylphthalate
ug/l
NO
10.
4,6-Dinitro-2-methylphenol
ug/l
NO
50.
2,4-Dinitrophenol
ug/l
NO
50.
2,4-Dinitrotoluene
ug/l
NO
10.
2,6-Dinitrotoluene
ug/l
NO
10.
Di-n-octylphthalate
ug/l
NO
10.
1,2-Diphenylhydrazine
ug/l
NO
20.
bis(2-Ethylhexyl)phthalate
ug/l
NO
10.
Fluoranthene
ug/l
NO
10.
Fluorene
ug/l
NO
10.
Hexachloro-1.3-butadiene
ug/l
NO
10.
Hexachlorobenzene
ug/l
NO
10.
Hexachlorocyclopentadiene
ug/l
NO
10.
Hexachloroethane
ug/l
NO
10.
Indeno(1,2,3-cd)pyrene
ug/l
NO
10.
Isophorone
ug/l
NO
10.
1-Methylnaphthalene
ug/l
NO
10.
2-Methylnaphthalene
ug/l
NO
10.
2-Methylphenol (o-Cresol)
ug/l
NO
10,
3&4-Methylphenol
ug/l
NO
10.
Naphthalene
ug/l
NO
10.
2-Nitroaniline
ug/l
NO
50.
3-Nitroaniline
ug/l
NO
50.
4-Nitroaniline
ug/l
ND
50.
Nitrobenzene
ug/l
NO
10.
2-Nitrophenol
ug/l
NO
10.
4-Nitrophenol
ug/1
NO
50.
N-Nitrosodimethylamine
ug/l
NO
10.
N-Nitroso-di-n-propylamine
ug/l
NO
10.
N-Nitrosodiphenylamine
ug/l
NO
10.
Pentachlorophenol
ug/l
NO
50.
Phenanthrene
ug/l
- NO
10.
Phenol
ug/l
NO
10.
Pyrene
ug/l
NO
10.
Date: 05/30/07
Asheville Certification IN
NC Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
4�0 N AGCOgo y
W� A C�
C O 'r'r
Page: 39 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100 2225 Riverside Drive
Nuntersville, NC 28078 Asheville, NC 28804
Analytical o Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92144916
Client Project ID: Clement Pappas
METHOD BLANK: 928414119
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276 928404284
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
1.2,4-Trichlorobenzene
ug/l
NO
10.
2,4,5-Trichlorophenol
ug/l
NO
50.
2,4,6-Trichlorophenol
ug/l
NO
10.
Nitrobenzene-d5 (S)
%
86
2-Fluorobiphenyl (S)
%
92
Terphenyl-d14 (S)
%
92
Phenol-d5 (S)
Y
35
2-Fluorophenol (S)
%
41
2,4,6-Tribromophenol (S)
%
101
LABORATORY CONTROL SAMPLE: 928414127
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
Acenaphthene
ug/l
50.00
47.02
94
Acenaphthylene
ug/l
50.00
47.27
94
Aniline
ug/l
50.00
36.13
72
Anthracene
ug/l
50.00
47.43
95
Benzo(k)fluoranthene
ug/l
50.00
47.48
95
Benzo(b)fluoranthene
ug/l
50.00
40.29
81
Benzo(a)anthracene
ug/l
50.00
45.68
91
Benzoic acid
ug/l
50.00
12.37
25
Benzo(g,h,i)perylene
ug/l
50.00
49.37
99
Benzyl alcohol
ug/l
50.00
41.72
83
Benzo(a)pyrene
ug/l
50.00
50.93
102
4-Bromophenylphenyl ether
ug/l
50.00
49.56
99
Butylbenzylphthalate
ug/l
50.00
44.88
90
4-Chloro-3-methylphenol
ug/l
50.00
44.89
90
4-Chloroaniline
ug/l
50.00
50.51
101
bis(2-Chloroethoxy)methane
ug/l
50.00
47.73
96
bis(2-Chloroethyl) ether
ug/l
50.00
30.92
62
bis(2-Chloroisopropyl) ether
ug/l
50.00
36.16
72
2-Chloronaphthalene
ug/l
50.00
46.18
92
2-Chlorophenol
ug/l
50.00
37.69
75
4-Chlorophenylphenyl ether
ug/l
50.00
52.72
105
Date: 05/30/07
Fnnfnnffoc
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 tEo ,N AyC CpR'4y
Page: 40 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical � Phone: [phone] Phone: [phone]
Fax., 704.875.9091 Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 928414127
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Y. Rec
Chrysene
ug/l
50.00
50.69
101
Dibenz(a,h)anthracene
ug/l
50.00
50.21
100
Dibenzofuran
ug/l
50.00
50.44
101
1,2-Dichlorobenzene
ug/l
50.00
39.53
79
1,3-Dichlorobenzene
ug/l
50.00
38.59
77
1,4-Dichlorobenzene
ug/l
50.00
36.16
72
3,3'-Dichlorobenzidine
ug/l
100.00
33.70
34
2,4-Dichlorophenol
ug/l
50.00
47.13
94
Diethylphthalate
ug/l
50.00
51.19
102
2,4-Dimethylphenol
ug/l
50.00
43.86
88
Dimethylphthalate
ug/l
50.00
47.21
94
Di-n-butylphthalate
ug/l
50.00
44.86
90
4.6-Dinitro-2-methylphenol
ug/l
50.00
35.60
71
2,4-Dinitrophenol
ug/l
50.00
28.56
57
2,4-Dinitrotoluene
ug/l
50.00
49.15
98
2,6-Dinitrotoluene
ug/l
50.00
49.53
99
Di-n-octylphthalate
ug/l
50.00
44.51
89
1,2-Diphenylhydrazine
ug/l
50.00
30.73
62
bis(2-Ethylhexyl)phthalate
ug/l
50.00
43.24
86
Fluoranthene
ug/l
50.00
46.86
94
Fluorene
ug/1
50.00
48.84
98
Hexachloro-1,3-butadiene
ug/l
50.00
52.74
105
Hexachlorobenzene
ug/l
50.00
51.57
103
Hexachlorocyclopentadiene
ug/1
50.00
11.15
22
Hexachloroethane
ug/1
50.00
39.74
80
Indeno(1.2,3-cd)pyrene
ug/l
50.00
49.87
100
Isophorone
ug/l
50.00
57.82
116
1-Methylnaphthalene
ug/l
50.00
40.57
81
2-Methylnaphthalene
ug/l
50.00
49.53
99
2-Methylphenol (o-Cresol)
ug/l
50.00
33.83
68
3&4-Methylphenol
ug/l
50.00
30.99
62
Naphthalene
ug/l
50.00
44.36
89
2-Ni.troaniline
ug/l
50.00
39.39
79
3-Nitroaniline
ug/l
50.00
39.25
78
4-Nitroaniline
ug/l
.50.00
44.86
90
Nitrobenzene
ug/l
50.00
45.36
91
2-Nitrophenol
ug/l
50.00
43.69
87
Date: 05/3D/07
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Footnotes
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full,
Sc 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 ��o ,w ACC,,0
�`rA cc
Page: 41 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
LABORATORY CONTROL SAMPLE: 928414127
racy Hna/yllcal ourvlces, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Y Rec
4-Nitrophenol
ug/l
50.00
22.08
44
N-Nitrosodimethylamine
ug/l
50.00
33.51
67
N-Nitroso-di-n-propylamine
ug/l
50.00
41.95
84
N-Nitrosodiphenylamine
ug/l
50.00
48.75
98
Pentachlorophenol
ug/l
50.00
27.16
54
Phenanthrene
ug/l
50.00
41.82
84
Phenol
ug/l
50.00
17.31
35
Pyrene
ug/l
50.00
45.52
91
1,2,4-Trichlorobenzene
ug/l
50.00
50.36
101
2,4,5-Trichlorophenol
ug/l
50.00
41.90
84
2.4,6-Trichlorophenol
ug/l
50.00
46.93
94
Nitrobenzene-d5 (S)
89
2-Fluorobiphenyl (S)
89
Terphenyl-d14 (S)
87
Phenol-d5 (S)
37
2-Fluorophenol (S)
48
2,4,6-Tribromophenol (S)
88
LABORATORY CONTROL SAMPLE: 928418920
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec
Acenaphthene
ug/l
50.00
42.09
84
Acenaphthylene
ug/l
50.00
41.95
84
Aniline
ug/l
50.00
26.60
53
Anthracene
ug/l
50.00
44.99
90
Benzo(k)fluoranthene
ug/l
50.00
38.60
77
Benzo(b)fluoranthene
ug/l
50.00
32.05
64
Benzo(a)anthracene
ug/l
50.00
41.71
83
Benzoic acid
ug/l
50.00
13.60
27
Benzo(g,h,i)perylene
ug/l
50.00
34.93
70
Benzyl alcohol
ug/l
50.00
40.73
82
Benzo(a)pyrene
ug/l
50.00
47.23
94
4-Bromophenylphenyl ether
ug/l
50.00
49.37
99
Butylbenzylphthalate
ug/l
50.00
44.24
88
4-Chloro-3-methylphenol
ug/l
50.00
36.95
74
Date: 05/30/07
race Hnatyncai aervices, inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Footnotes
Footnotes
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NC Drinking Water
37712
This report shall not be reproduced, except in full,
Sc
99030
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
�Eo `" ACC,,4
Page: 42 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

aceAnalytical°
www.pacelabs.com
LABORATORY CONTROL SAMPLE: 928418920
Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
QUALITY CONTROL DATA
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Rec
4-Chloroaniline
ug/l
50.00
53.21
106
bis(2-Chloroethoxy)methane
ug/l
50.00
42.11
84
bis(2-Chloroethyl) ether
ug/l
50.00
28.17
56
bis(2-Chloroisopropyl) ether
ug/l
50.00
32.34
65
2-Chloronaphthalene
ug/l
50.00
42.25
84
2-Chlorophenol
ug/l
50.00
35.34
71
4-Chlorophenylphenyl ether
ug/l
50.00
45.86
92
Chrysene
ug/l
50.00
45.75
92
Dibenz(a,h)anthracene
ug/l
50.00
37.33
75
Dibenzofuran
ug/l
50.00
42.73
86
1,2-Dichlorobenzene
ug/l
50.00
33.43
67
1.3-Dichlorobenzene
ug/l
50.00
30.04
60
1.4-Dichlorobenzene
ug/l
50.00
32.15
64
3,3'-Dichlorobenzidine
ug/l
100.00
26.21
26
2,4-Dichlorophenol
ug/l
50.00
40.75
82
Diethylphthalate
ug/l
50.00
41.51
83
2,4-Dimethylphenol
ug/l
50.00
40.38
81
Dimethylphthalate
ug/l
50.00
42.95
86
Di-n-butylphthalate
ug/l
50.00
41.99
84
4,6-Dinitro-2-methylphenol
ug/l
50.00
18.07
36
2,4-Dinitrophenol
ug/l
50.00
10.57
21
2,4-Dinitrotoluene
ug/l
50.00
39.45
79
2.6-Dinitrotoluene
ug/l
50.00
41.54
83
Di-n-octylphthalate
ug/l
50.00
41.83
84
1,2-Diphenylhydrazine
ug/l
50.00
38.34
77
bis(2-Ethylhexyl)phthalate
ug/l
50.00
44.59
89
Fluoranthene
ug/l
50.00
40.04
80
Fluorene
ug/l
50.00
41.90
84
Hexachloro-1,3-butadiene
ug/l
50.00
37.16
74
Hexachlorobenzene
ug/l
50.00
50.51
101
Hexachlorocyclopentadiene
ug/l
50.00
10.77
22
Hexachloroethane
ug/l
50.00
27.37
55
Indeno(1,2,3-cd)pyrene
ug/l
50.00
37.94
76
Isophorone
ug/l
50.00
54.70
109
1-Methylnaphthalene
ug/l
50.00
34.14
68
2-Methylnaphthalene
ug/l
50.00
51.34
103
2-Methylphenol (o-Cresol)
ug/l
50.00
32.99
66
Date: 05/30/07
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
Fnnf-+-
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 " ACC0
LTV RO' c
Page: 43 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical Phone: [phone] Phone: [phone]
J. Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92144916
Client Project ID: Clement Pappas
LABORATORY CONTROL SAMPLE: 928418920
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
3&4-Methylphenol
ug/l
50.00
29.40
59
Naphthalene
ug/l
50.00
39.45
79
2-Nitroaniline
ug/l
50.00
36.59
73
3-Nitroaniline
ug/l
50.00
36.47
73
4-Nitroaniline
ug/l
50.00
30.84
62
Nitrobenzene
ug/l
50.00
44.50
89
2-Nitrophenol
ug/l
50.00
41.15
82
4-Nitrophenol
ug/l
50.00
12.42
25
N-Nitrosodimethylamine
ug/l
50.00
34.08
68
N-Nitroso-di-n-propylamine
ug/l
50.00
35.90
72
N-Nitrosodiphenylamine
ug/l
50.00
49.85
100
Pentachlorophenol
ug/l
50.00
9.750
20
Phenanthrene
ug/l
50.00
40.54
81
Phenol
ug/l
50.00
13.52
27
Pyrene
ug/l
50.00
47.30
95
1,2,4-Trichlorobenzene
ug/l
50.00
42.16
84
2,4.5-Trichlorophenol
ug/l
50.00
30.46
61
2,4.6-Trichlorophenol
ug/l
50.00
36.28
73
Nitrobenzene-d5 (S)
82
2-Fluorobiphenyl (S)
90
Terphenyl-d14 (S)
93
Phenol-d5 (S)
32
2-Fluorophenol (S)
36
2,4,6-Tribromophenol (S)
92
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 928414135 928414143
928404243 Spike MS MSD
MS
MSD
Parameter
Units
Result Conc. Result Result %
Rec %
Rec
RPD Footnotes
Acenaphthene
ug/l
0 100.00 103.3 104.5
103
104
1
4-Chloro-3-methylphenol
ug/l
0 100.00 82.82 85.11
83
85
3
2-Chlorophenol
ug/l
0 100.00 85.73 89.40
86
89
4
1,4-Dichlorobenzene
ug/l
0 100.00 85.30 89.54
85
90
5
2.4-Dinitrotoluene
ug/l
0 100.00 108.8 110.3
109
110
1
4-Nitrophenol
ug/l
0 100.00 42.89 46.60
43
47
8
Date: 05/30/07
Page: 44
of 54
Asheville Certification IN
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IN
NC Wastewater 40
NC Wastewater
12
NC Drinking Water 37712
This report shall not be reproduced, except in full,
NC Drinking Water
37706
Sc 99030
without the written consent of Pace Analytical Services, Inc.
Sc
99006
FL NELAP E87648
`�a ,N ACCCk�,9
FL NELAP
E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical o Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92144916
Client Project ID: Clement Pappas
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 928414135 928414143
928404243
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result
% Rec %
Rec
RPD Footnotes
N-Nitroso-di-n-propylamine
ug/l
0
100.00
91.98
94.92
92
95
3
Pentachlorophenol
ug/l
0
100.00
108.9
105.0
109
105
4
Phenol
ug/l
0
100.00
39.87
40.03
40
40
0
Pyrene
ug/l
0
100.00
103.3
106.8
103
107
3
1,2,4-Trichlorobenzene
ug/l
0
100.00
77.03
77.82
77
78
1
Nitrobenzene-d5 (S)
71
74
2-Fluorobiphenyl (S)
97
97
Terphenyl-d14 (S)
99
98
Phenol-d5 (S)
42
42
2-Fluorophenol (S)
51
54
2,4,6-Tribromophenol (S)
110
100
Date: 05/30/07 Page: 45 of 54
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IN
NC Wastewater
40
NC Wastewater
12
NC Drinking Water
37712
This report shall not be reproduced, except in full,
NC Drinking Water
37706
Sc
99030
without the written consent of Pace Analytical Services, Inc.
Sc
99006
FL NELAP
E87648
`�o ,N ACCOp09yC
FL NELAP
E87627

race Analyucal Jervlces, Inc. race Analyucal Jervices, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
07,P Analvtirgl R Phone: [phone] Phone: [phone]
Fax., 704.875.9091 Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92144916
Client Project ID: Clement Pappas
QC Batch: 189232 Analysis Method: SM 9222D
QC Batch Method: SM 9222D Analysis Description: Fecal Coliform in Water
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276
928404284
METHOD BLANK: 928408947
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276 928404284
Blank Reporting
Parameter Units Result Limit Footnotes
Coliform, Fecal col/100ml NO 1.0
SAMPLE DUPLICATE: 928408954
Parameter Units
Coliform, Fecal col/100ml
Date: 05/30/07
928404250 DUP
Result Result RPD Footnotes
NO NO NC
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 "CCO,90
C S
Page: 46 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Nuntersville, NC 28078 Asheville, NC 28804
Anali�tiral Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelahs.com QUALITY CONTROL DATA
Lab Project Number: 92144916
Client Project ID: Clement Pappas
QC Batch: 189151 Analysis Method: EPA 160.1
QC Batch Method: SM 2540C Analysis Description: Total Dissolved Solids
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276
928404284
METHOD BLANK: 928406677
Associated Lab Samples:
Parameter
Total Dissolved Solids
928404235 928404243 928404250 928404268 928404276 928404284
Blank Reporting
Units Result Limit Footnotes
mg/l NO 20.
LABORATORY CONTROL SAMPLE: 928406685
Parameter
Units
Total Dissolved Solids mg/l
SAMPLE DUPLICATE: 928406966
Parameter Units
Total Dissolved Solids mg/l
Date: 05/30/07
Spike LCS LCS
Conc. Result % Rec Footnotes
250.00 244.0 98
928376672 DUP
Result Result RPD Footnotes
100.0 120.0 18
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 %" "°°°
R
WOE 0� �o9ycf
Page: 47 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Anil i�tiral Phone: [phone] Phone: [phone]
Fax: [phone] Fax. [phone]
www.pacelahs.com QUALITY CONTROL DATA
Lab Project Number: 92144916
Client Project ID: Clement Pappas
QC Batch: 189105 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 48 Hour NO3 / NO2 / NOX
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276
928404284
METHOD BLANK: 928404441
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276 928404284
Blank Reporting
Parameter Units Result Limit Footnotes
Nitrate as N mg/l ND 0.10
LABORATORY CONTROL SAMPLE: 928404458
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Nitrate as N mg/l 5.000 4.720 94
MATRIX SPIKE: 928404466
928404094 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Nitrate as N mg/l 0.02000 5.000 5.170 103
SAMPLE DUPLICATE: 928404474
Parameter Units
Nitrate as N mg/l
Date: 05/30/07
928404102 DUP
Result Result RPD Footnotes
NO ND NC
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 ,„ AccoRo
Page: 48 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

aceAnalytical °
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
QC Batch: 189202 Analysis Method: EPA 325.2
QC Batch Method: SM 4500-Cl E Analysis Description: Chloride (Mercuric Nitrate)
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276
928404284
METHOD BLANK: 928408343
Associated Lab Samples:
Parameter
Chloride
928404235 928404243 928404250 928404268 928404276 928404284
Blank Reporting
Units Result Limit Footnotes
mg/l NO 5.0
LABORATORY CONTROL SAMPLE: 928408350
Parameter
Chloride
MATRIX SPIKE: 928408368
Units
mg/1
Spike LCS LCS
Conc. Result % Rec Footnotes
20.00 21.97 110
928383884 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Chloride mg/1 9410 20.00 11030 8115 1
SAMPLE DUPLICATE: 928408376
928404235 DUP
Parameter Units Result Result RPD Footnotes
Chloride mg/l 6.000 5.800 3
Date: 05/30/07
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 40 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
C
Page: 49 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax. [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
QC Batch: 189275 Analysis Method: SM 5310B
QC Batch Method: SM 5310B Analysis Description: Total Organic Carbon
Associated Lab Samples: 928404235
METHOD BLANK: 928410539
Associated Lab Samples: 928404235
Blank Reporting
Parameter Units Result Limit Footnotes
Total Organic Carbon mg/1 ND 1.0
LABORATORY CONTROL SAMPLE: 928410547
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
Total Organic Carbon mg/l 10.00 9.926 99
MATRIX SPIKE: 928410554
928357565 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Total Organic Carbon mg/l 12.70 10.00 20.55 78
SAMPLE DUPLICATE: 928410562
Parameter
Total Organic Carbon
Date: 05/30/07
928352327 DUP
Units Result Result RPD Footnotes
mg/l 1.500 ND NC
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
Page: 50 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
QC Batch: 189276 Analysis Method: SM 5310B
QC Batch Method: SM 5310B Analysis Description: Total Organic Carbon
Associated Lab Samples: 928404243 928404250 928404268 928404276 928404284
METHOD BLANK: 928410570
Associated Lab Samples: 928404243 928404250 928404268 928404276 928404284
Blank Reporting
Parameter Units Result Limit Footnotes
Total Organic Carbon mg/l NO 1.0
LABORATORY CONTROL SAMPLE: 928410588
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Total Organic Carbon mg/l 10.00 10.07 101
MATRIX SPIKE: 928410596
928404243 Spike MS MS
Parameter Units Result Conc. Result Y, Rec Footnotes
Total Organic Carbon mg/l 8.497 10.00 19.08 106
SAMPLE DUPLICATE: 928410604
Parameter
Total Organic Carbon
Date: 05/30/07
928404250 DUP
Units Result Result RPD Footnotes
mg/l 1.700 1.600 3
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
Page: 51 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

u ct Analytical °
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
QC Batch: 189370 Analysis Method: EPA 350.1
QC Batch Method: EPA 350.1 Analysis Description: Ammonia
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276
928404284
METHOD BLANK: 928415405
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276 928404284
Blank Reporting
Parameter Units Result Limit Footnotes
Nitrogen. Ammonia mg/l ND 0.10
LABORATORY CONTROL SAMPLE: 928415413
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Nitrogen, Ammonia mg/l 5.000 4.982 100
MATRIX SPIKE: 928415421
928394410 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Nitrogen, Ammonia mg/l 24.22 5.000 28.60 88
SAMPLE DUPLICATE: 928415439
Parameter Units
Nitrogen, Ammonia mg/l
Date: 05/30/07
928394428 DUP
Result Result RPD Footnotes
ND ND NC
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 ��a " Acco'� y
a �F
rIA
Page: 52 of 54
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical o Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92144916
Client Project ID: Clement Pappas
QC Batch: 189737 Analysis Method: EPA 375.4
QC Batch Method: EPA 375.4 Analysis Description: Sulfate.Turbidimetric
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276
928404284
METHOD BLANK: 928429745
Associated Lab Samples: 928404235 928404243 928404250 928404268 928404276 928404284
Blank Reporting
Parameter Units Result Limit Footnotes
Sulfate mg/l NO 5.0
LABORATORY CONTROL SAMPLE: 928429752
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
Sulfate mg/l 20.00 18.01 90
MATRIX SPIKE: 928429760
Parameter Units
Sulfate
SAMPLE DUPLICATE: 928429778
mg/1
928383793 Spike MS MS
Result Conc. Result % Rec Footnotes
338.0 20.00 270.4 0 1
928383801 DUP
Parameter Units Result Result RPD Footnotes
Sulfate mg/l 280.0 280.0 3
Date: 05/30/07
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NC Drinking Water.
37712
This report shall not be reproduced, except in full,
SC
99030
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
�U "°°°
I09 c
o
J F
Page: 53 of 54
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

aceAnalytical °
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92144916
Client Project ID: Clement Pappas
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate % Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
(S) Surrogate
Ell The spike recovery was outside acceptance limits for the MS and /or MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
Date: 05/30/07
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
Sc 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648' %" °"
Page: 54 of 54
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

aceAnalyIJcal
www.pacelabs.com
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields 'rnust. be completed accurately.
Section A Section B Section C
Page:
` of
Required Client Information: Required Project Information: Invoice Information:
Comp ny' / Report To: Attention: Jc
v�•
106 9828
Address: SO s
Copy To:
Company Name:
r
REGULATORY AGENCY a
LG
Address: � �
17 NPDES GROUND WATER [ DRINKING WATER
r UST j- RC,RA OTHER
Em it To: L Purchase
(,�. c'%pI
Order No.:
Pace Quote
..triw�C�t./.%17 L;tI.w
Reference:
j-
ones:, � (�(
uGI
Fay Project
G�� ,�f�
Name: /1
Protect `
Manager: (fi rr ` � �1
Site Location
STATE;
.+ ^
VNIE
'1.
Requested Due Date/TAT: Project
Number. �O� A
JPaco
Pace Profile #:
nc
R3
ueste'd`Anal
sfs`Filfered':77
Section D Valid Matrix Codes
RequtredCliont Information MATRIX CODE
c
COLLECTED
Preservatives
•.}
*t
�"
Y"
tV
r
�.>a ... `u,•
DRINKING WATER OW WT
WATER WW P
D
II
Z
LD
_
WASTE WATER SL
U
COMPOSITE
COMPOSITE
U
PRODUCT OL
SOIUSOLID WPOIL
=
co
START
END/GRAB
W
-�
J
z
r
SAMPLE ID WIPE oT
.-.
2
`�
'�
{
o
AIR TS
(A-Z, 0-9 / OTHER
v
F"
Lu
- ?
•
i'
q
1
C
Sample IDS MUST BE UNIQUE TISSUE
p
n.
g
~
Z
a)
X
J
J
O
a)O
o
((
w
~
¢
0O
n
O
p
DATE
TIME
DATE
TIME
0
2
2
2
Z
Z
�
O
b
Pace Project No./ Laub I.D.
1
rn L) - 0 Z 1�
W1r
/N
G
F-fY u
i`.
�
I I
�
`�
N'
F
I
.I
(
I
I(
i
23
:�.zl'
w- �
wr
'
s--(
I•
'2,
1
3
I
I
I
(
I
�3..
rhU.) - Ov
i
G
S`=i8
zo
r3
/
3
1
i
(
I
I
ZOO
Id
114
3
l
-6
IS: 6
ITA
11
14
's
(
I
1
y
1
1
ttrr
- 8
sss
�z
i
3
3
I
I
►
I
7
r3
g
105'
;12 ,
ADDITIONAL COMMENTS,
RELINQUISHED 13Y 1 AFFILIATION
—DATE i"
. '^TIMEAFFILIATION
DATE
SAMPLE CONDITIONS
�b� ?� hSLc•�
-
: 1C
SAMPLER NAME
J�ND SIGNATURE
r me
y
o
ORIGINAL
`
z
.g z
m
PRINT Name of SAMPLER:
~ s '
SIGNATURE of SAMPLER:
DATE SI ned
g
IT
t-
°' —
�
E
(MM/DID . —1
r°n
rn
i....o. oy mma tumt y.,u are accepting race's Nt I Uu day payment terms and agreeing to late charges of 1.5 % per month for any invoices not paWQV5in 30 days. F-ALL-Q-020rev.06, 2-Feb-2007

" ESN -G'A N. E e R:A7 -N--G' W? . H Y D R O G E OIL" O -G Y.
50 COLLEGE STREET, AsBEvILLE,.NC 28801
TEL. [phone] FAC .828.281.3351
www. altamontenvironmental. com
Well Sampling Log
FACILITY NAME: Clement Pappas
LOCATION: Henderson County, NC
SAMPLING PERSONNEL:. Jon Hazinski
DATE: 5/18/2007
SAMPLING TIME: j Z ' 3
WEATHER: Su n 4
WELL NUMBER:_ ►'h CU - 6 2 Z
WELL DIAMETER
TYPE OF CASING: PVC
MEASURING POINT:
FLUSH MOUN / STICK-UP
COM IENTSZ w�,. r ( �G:, �Gc�
6LIKllo�
re_,k,�9,•,Y&S
WELL DEPTH IN FEET (WD): P O START TIME: 12 06
WATER LEVEL IN FEET (WL):
LENGTH OF WATER COLUMN: FEET
(WD) -.(WL) = (LWC)
ONE CASING VOLUME: f GALLONS
(LWC) x (WCV) a
THREE CASING VOLUMES: -7 -S �{ GALLONS
ACTUAL VOLUME PURGED: 2.. 0 GALLONS
WELL CASING VOLUMES (WCV)
2" = 0.17 Gal/Ft 3" = 0.38 Gal/Ft 4" = 0.66 Gal/Ft 6" = 1.5 GaUFt 8" = 2.6 GaUFt 12" = 5.8 Gal/Ft
PURGE METHOD: BAILER-TEFLO AIL
- DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER:
SAMPLE METHOD: BAILER-TEFLO
BAILER-DISP. EDICATED PUMP WHALE PUMP GRUNDFOS OTHER:
READING
GALLONS
PURGED
pH UNITS
SPECIFIC
COND.
(µS)
TEMP (C°)
DISSOLVED
OXYGEN
(mg/L)
OXIDATION
REDUCTION
POTENTIAL
m
TURBIDITY
(NTU)
COMMENTS
3
2.. o
�. 5-.�-
!'. !
i Z. Z
4. S G
13 l
Y o, d
4
5
6
7
8
9
SAMPLING CONTAINER
NUMBER OF CONTAINERS
REQUESTED ANALYSIS
100 mL PLASTIC
3
Nitrate, AmmoniaNitrogen
250 ml PLASTIC
, Fecal Coliform..
500 mL PLASTIC
1
TDS C A joy: ,t,, Suj f,_,je
40 ml GLASS
5
TOC, VOCs by 621OD
1 L GLASS
SVOCs --�
PROTECTIVE CASING:- p � PAD: 6 K LOCK: 0 fG VEGETATION:O V ACCES GOOD / OOR
Sampling Personnel Signature:
Date: _�; r- 1 9 r-0 -7
Notes: µS = micro-Siemen
C° = degrees Celcius
mg/L =. milligrams per liter
mV =millivolt
NTU=-nephelometric turbidity units
P.\Templates\GW Drilling FormLs\Well, Sampling Log xls .
Page 1 of 1

50 COLLEGE STREEr, ASHEVILLE, NC 28801
TEL. [phone] TAc.828.281.3351
www. altamonteiMronmental.com
Well Sampling Log
FACILITY NAME. Clement Pappas
DATE: 5/18/2007
LOCATION. Henderson County, NC
SAMPLING TIME:
SAMPLING PERSONNEL: Jon Hazinski
WEATHER:-
-WELL NUMBER: 0 14
WELL DEPTH IN FEET (WD)-.' t3.
START TIME: 143
WELL DIAN[ETER.
WATER L,9VEL IN FEET (WL):
TYPE OF CASING: PV -r—
LENGTH OF WATER COLUMN:
FEET
MEASURING POINT: c
(WD) 7 (WL) = (LWC)
FLUSH MO TICK. -UP
ONE CASING VOLUME:
GALLONS'
COMMENTS:
(LWC) x (WCV)
THREE CASING VOLUMES: GALLONS
ACTUAL VOLUME PURGED: L4.- 7-57
GALLONS.
WELL CASING VOLUMES (WCV)
2" = 0.17 Gal/Ft 3"=_0_1SGal/Ft
4" = 0.66 Gal/Ft 6"=1.5Gal/Ft 8"=2.6Gal/Ft
12" = 5.8 Gal/Ft
PURGE METHOD:
BAILE R-DISP. DEDICATED PUMP WHALE PUMP
GRUNDFOS OTHER.
SAMPLE METHOD: e-5A—ILER-TEFL69
BAILER-DISP. DEDICATED PUMP WHALE PUMP
GRUNDFOS OTHER:
READING
GALLONS
pH TS
SPECIFIC
TENT (C-)
DISSOLVED
OXIDATION
TURBIDITY
COMMENTS
PURGED
COND.
OXYGEN
REDUCTION
(NTU)
01S)
(mg/L)
POTENTIAL
(my)
(0,qq
7
-7 ..7
2
1-s-
16./6
-z- is-
Z.-7
SO r,
5
3
3_0
ZZ c_
2,
Z. -7
93
3 _3V
4
5
6
7
8
9
SAMPLING CONTAINER
NUMBER OF CONTAINERS
UQUESTED ANALYSIS
100 mL PLASTIC
3
Nitrate, Ammonia Nitrogen
250 ml PLASTIC
49h4eride,-%�f , Fecal Coliform
500 ml, PLASTIC
1
IDS,
40 ml GLASS
.5
TOC, VOCs by 62 1 OD
I L GLASS
71 1§VOcs
PROTECTIVE CASING: 6.4 PAD: 01',e LOCK: 0 fC VEGETATION: 6iC ACCES.S-r03DPOOR
Sampling Personnel Signature: I
Date: -7 S7- -6
Notes: pS = micro-Siemen
C' = degrees Celcius
mg/L = milligrams per liter
mv = millivolt
NTU =nephelometric turbidity units
P:\Templates\GW Drilling Forms\Well. Sampling Log.xls Page 1 of 1

E'<N"G'A:N E E'Rol :N-G 's&`,:.H Y D R O G E Ot
50 COLLEGE STREET, ASHEvILLE, NC 28801
TEL. [phone] FAc .828.281.3351
www.altamontenviroamental.com
Well Sampling Log
FACILITY NAME: Clement Pappas
DATE: 5/18/2007
LOCATION: Henderson County, NC
SAMPLING TIME: It' Zo
SAMPLING PERSONNEL: Jon Hazinski
WEATHER: n n
WELL NUMBER:
WELL DEPTH IN FEET (WD): ' 14 4 START TIME:
WELL DIAMETER 2
WATER LEVEL IN FEET (WL): �, J
TYPE OF CASING: P V C
LENGTH OF WATER COLUMN: FEET
MEASURING POINT: 7_42PC
(WD) - (WL) _ (LWC)
FLUSH MOUN STRCK-�
ONE CASING VOLUME: I, S—GALLONS
COMMENTS:
(LWC) x (WCV)
THREE CASING VOLUMES: GALLONS
ACTUAL VOLUME PURGED:GALLONS
WELL CASING VOLUMES (WCV)
2" = 0.17 Gal/Ft 3" = 0.38 Gal/Ft
4" = 0.66 Gal/Ft 6" = 1.5 Gal/Ft 8" = 2.6 Gal/Ft -12" = 5.8 Gal/Ft
PURGE METHOD: AILE -
BAILER DISP. DEDICATED PUMP . WHALE PUMP GRUNDFOS OTHER:
SAMPLE METHOD: AILER
BAILER-DISP. DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER --
READING
GALLONS
pH UNITS
SPECIFIC
TEMP (C°)
DISSOLVED
OXIDATION
TURBIDITY
COMMENTS
PURGED
COND.
OXYGEN.
REDUCTION
(NTU)
(µs)
(mg/L)
POTENTIAL
mV
2
I.5-
s'. 4 1
te-7-5-
"y
`, CtR
167
y 2-0 •7
3
3,0
1 DA��"Z,
4
L75
9.
5
6
7
8
9
SAMPLING CONTAINER
NUMBER OF CONTAINERS
REQUESTED ANALYSIS
100 mL PLASTIC
3
Nitrate, Ammonia Nitrogen
250 ml PLASTIC
X
Rawg&_1 ; Fecal Colifform.
500 mL PLASTIC
1
TDS , G �. JOT,' f� i S✓f . l—�
40 ml GLASS
5
TOC, VOCs by 6210D .
1 L GLASS
SVOCs
PROTECTIVE CASING: 0 fC PAD:' O iC
LOCK: O 1C. VEGETATION: c9`C ACCES fO7O>OOR
Sampling Personnel Signature: /)
Date: _ 7
Notes: µS = micro-Siemen///
C°'= degrees Celcius
mg/L = milligrams per liter
mV = millivolt
NTU=-nephelometric turbidity units
P:\Templates\GW Drilling Forms\Well. Sampling.Log.xls • . Page 1 of 1.

021311
=E•-N':G"1.N E E�R,VWG44W,'H-Y DR O G E O:C
50 COLLEGE STREET, AsxEvu,LF, NC 28801
TEL. [phone] FAc .828.281.3351
www. altamontenvironmental. com
Well Sampling Log
FACILITY NAME: Clement Pappas
LOCATION: Henderson County, NC
SAMPLING PERSONNEL: Jon Hazinski
DATE: 5/18/2007
SAMPLING TIME: : 7�
WEATHER:
WELL NUMBER: IM 0 - OG
WELL DIAMETER Z
TYPE OF CASING: lave
MEASURING POINT:
FLUSH MOUNT TIC -
COMMENTS:
WELL DEPTH IN FEET (WD): ! _24 START TIME: ' • ! rs
WATER LEVEL IN FEET (WL): x-0
LENGTH OF WATER COLUMN: FEET
(WD) - (WL) _ (LWC)
ONE CASING VOLUME: d • 86 GALLONS
(LWC) x (WCV)
THREE CASING VOLUMES: 'Z, 5 % GALLONS
ACTUAL VOLUME PURGED: Z 7S GALLONS
WELL CASING VOLUMES (WCV)
2" = 0.17 Gal/Ft 3" = 0.38 Gal/Ft 4" = 0.66 Gal/Ft 6" = 1.5 Gal/Ft 8" = 2.6 Gal/Ft 12" = 5.8 Gal/Ft
PURGE METHOD: - -
AILER-DISP. DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER -
SAMPLE METHO BAILER-TEFLON
BAILER-DISP. DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER. -
READING
GALLONS
PURGED
pH UNITS
SPECIFIC
COND.
(µS)
TEMP (C°)
DISSOLVED
OXYGEN
(mg/L)
OXIDATION
REDUCTION
POTENTIAL
mV
TURBIDITY
(NTU)
COMMENTS
1
i:��`�!af
.(,
go. if
IS'. L4
Z.32
133
- Z
2
1, v
S&3
(33 , ,5-
13. S
`Z' 99
9 Lt
3 Z-.S
3
Z
C 1
7,
3. q z
(09.
4
2.7s
5
.1
13,7
197
'7t
17 " ,7
5
6
7
8
9
SAMPLING CONTAINER
NUMBER OF CONTAINERS
REQUESTED ANALYSIS
100 mL PLASTIC
3
Nitrate, Ammonia Nitrogen
250 ml PLASTIC
, Fecal Coliform
500 mL PLASTIC
1
TDS , G�
40 ml GLASS
5
TOC, VOCs by 6210D
1 L GLASS
ISVOCS
PROTECTIVE CASING: p 1L PAD: le LOCK:y (C VEGETATION: OiC ACCESS: OOD / OOR
Sau►pling Personnel Signature:
Date:
Notes:.. AS = micro-Siemen
C° = degrees Celcius
mgJL = milligrams per liter
mV = millivolt
NTU =•nephelometric turbidity units
P:\Templates\GW Drilling Forms\Well. Sampling Log.xls Page 1 of 1

E''N G'4 N E E7 R,4'N G' Wt-,. H.Y D R O G E O L O G•Y,
50 COLLEGE STREET, AsBEvu,LE, NC 28801
TEL. [phone] FAC .828.281.3351
www.altamontenvironmental.com
Well Sampling. Log
FACILITY NAME: Clement Pappas
LOCATION: Henderson County, NC
SAMPLING PERSONNEL: Jon Hazinski
DATE: 5/18/2007
SAMPLING TIME: lS f D
WEATHER: ✓�,� GtJ�v »,
WELL NUMBER: M f tJ ' 0 -7
WELL DIAMETER Z ri
TYPE OF CASING:
MEASURING POINT: j7OG
FLUSH MO TICK -UP
COMMENTS:
WELL DEPTH IN FEET (WD): C - 7 7- START TIIv)EJ414 7.
WATER LEVEL IN FEET (WL):' I I. 0 Z
LENGTH OF WATER COLUMN: R 7 O FEET
(WD) - (WL) _ (LWC)
ONE CASING VOLUME: ©• -7 GALLONS
(LWC) x (WCV)
THREE CASING VOLUMES: GALLONS
ACTUAL VOLUME PURGED: -3•y GALLONS
2" = 0.17 Gal/Ft " _ .38 Gal/Ft
WELL CASING VOLUMES (WCV).
4" = 0.66 GaLTt 6" = 1.5 Gal/Ft 8" = 2.6 Gal/Ft 12" = 5.8 Gal/Ft
PURGE METHOD: AILER-
O BAILER DISP. DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER
SAMPLE METHOD: AILER-TEFLO
BAILER-DISP. DEDICATED PUMP WHALE PUMP GRUNDFOS OTHER:
READING
GALLONS
PURGED
pH UNITS
SPECIFIC
COND.
(µS)
TEMP (C°)
DISSOLVED
OXYGEN
.(mg/L)
OXIDATION
REDUCTION
POTENTIAL
mV
TURBIDITY
(NTU)
COMMENTS
1
- •
914-3
Lj,W
j -2-1
13, 7"
2
0
SS Lt
l og. g
13,6
q• 6.0
i S
-LI-
3
2..6
5-, '4—
'I 18,.s
13,4
5 /
1s3
7-!L
4
.3"0
s
116,0
13,
5
4.5,5
l
ZC1.
s
6
7
8
9
SAMPLING CONTAINER
NUMBER OF CONTAINERS
REQUESTED ANALYSIS
100 mL PLASTIC
3
Nitrate, Ammonia Nitrogen
250 ml PLASTIC
fi e,-STdfate, Fecal Coliform
500 mL PLASTIC
1
TDS
40 ml GLASS
5
TOC, VOCs by 621OD
1 L GLASS
'Z
SVOCS
PROTECTIVE CASING: (C PAD: 014
LOCK: 0 iC VEGETATION: C9J.C- ACCESS: GOOD / POOR
Sampling Personnel Signature:
Date: 6 -7
Notes: µS = micro-Siemen /
C° = degrees Celcius.
mg/L = milligrams per liter
mV = millivolt
NTU=-nephelometric turbidity units
P:\Templates\GW Drilling Forms\Well. Sampling Log.xls
Page 1 of 1

i1
+1 `
�! E' N G-4-N E E"RBI-N-Gti- &"%.. H Y D R O'G E O
50 COLLEGE STREET, AsnEviLLE, NC 28801
TEL.[phone] FAc.828.281.3351
www.altamontenvironmental.com
Well Sampling Log
FACILITY NAME: Clement Pappas
DATE: 5/18/2007
LOCATION: Henderson County, NC
SAMPLING TIME:
SAMPLING PERSONNEL: Jon Hazinski
WEATHER:
WELL NUMBER: 1M U) - o
WELL DEPTH IN FEET (WD): 13, %U
START TIME: %S, -Z7
WELL DIAMETER "L
WATER LEVEL IN FEET (WL): 16. 3
TYPE OF CASING: 19 y 6
LENGTH OF WATER COLUMN: 3 , S�`7
FEET
MEASURING POINT: TOG
(WD) - (WL) _ (LWC)
FLUSH MO / STICK-
ONE CASING VOLUME: 0 ,
GALLONS
COMMENTS:
(LWC) x (WCV)
THREE CASING VOLUMES: 1,93
GALLONS
ACTUAL VOLUME PURGED:
GALLONS -
WELL CASING VOLUMES (WCV)
2" = 0.17 Gal/Ft " _ .38 Gal/Ft 4" = 0.66 Gal/Ft 6" = 1.5 Gal/Ft 8" 2.6 Gal/Ft 12" = 5.8 Gal/Ft
PURGE METHOD: ILER TEF
N BAILER DISP. DEDICATED PUMP WHALE PUMP
GRUNDFOS OTHER:
SAMPLE METHOD: -TE
BAILER-DISP. DEDICATED PUMP WHALE PUMP
GRUNDFOS OTHER:
READING
GALLONS
—SPECIFIC
TEMP (CO)
DISSOLVED
OXIDATION
TURBIDITY
COMMENTS
PURGED
COND.
OXYGEN
REDUCTION
(NTU)
(µS)
(mg/L)
POTENTIAL..
mV
I
13. %
Lf 3 i
i
0,66
2
0,75 .
S. -3
I39-L4
13-0
Lf,64
1
qlo 8
3
. sv
5 `7q
ill. 0
i Z .- C
q,q8
i
4
-2.
S•77
57. Z
13, 2.
`� s?
�SZ
' S Z
5
6.
7
8
9
SAMPLING CONTAINER
NUMBER OF CONTAINERS
REQUESTED ANALYSIS
.100 mL PLASTIC
3
Nitrate, Ammonia Nitrogen
250 ml PLASTIC
e, Fecal Coliform
500 ml, PLASTIC
I
TDS
40 ml GLASS
5
TOC, VOCs by 621OD'
1 L GLASS
ISVOCS
PROTECTIVE CASING: (3 t. PAD: O e LOCK: (C- VEGETATION: C'. ACCESS
GOOD POOR
Sampling Personnel Signature:
Date:
Notes: µS = micro-Siemen
C° = degrees Celcius
mg/L = milligrams per liter
mV = millivolt
NTU = nephelometric turbidity units
P:\Templates\GW Drilling Forms\Well, Sampling Log.xls - Page 1 of 1