WQ0038087_2021 Residual Annual Report_20220524 (2)

Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0038087
ApplicantlPermittee Terra Renewal Services, Inc.
Email Notifications
Does this need review by the hydrogeologist?* Yes No
Regional Office
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* David Coyle
Email Address*
[e-mail]
Project Information
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
479-747-8192
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
hftps://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Perm it Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number: *
WQ0038087
Has Current Existing permit number
Applicant/Permittee Address*
P.O. Box 1746 Watkinsville, GA 30677
Facility Name*
Terra Renewal Services Class B Residuals Program
Please provide comments/notes on your current submittal below.
The copy of the 2021 annual report for WQ0038087 is revised based on comments presented
by review of the Winston-Salem Regional office. The staff has been notified of submission. If
there are questions or complications, please contact David Coyle at 479-747-8192. Thanks.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
NC WQ0038087 Terra
— — 33.56M6
Renewal_AnnualReport_2021_REVISED_May 2022.pdf
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
a�aeh��

Submission Date 5/24/2022

"I L
T. E IR'IR A
r e IIP iii e �%&r a I
PO BOX 399 - DARDANELLE - ARKANSAS - 72834
479.747.8192
terrarenewal.com
2021 ANNUAL REPORT
for NC Land Application Permit Number-
WQ0038087
(Class B Residuals)
REVISED / CORRECTED: May 2022
Permittee / Submitted By:
Terra Renewal Services
P.O. Box 399
Dardanelle, AR 72834
Attention:
North Carolina Department of Environmental Quality
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
512 N. Salisbury Street; 6 th Floor
Raleigh, NC 27604

IIIE R I? A,
u" FN 111 ON W (I II
May 24, 2022
Caitlin Caudle; Environmental Specialist I
Division of Water Resources
North Carolina Department of Environmental Quality
Winston Salem Regional Office
450 West Hanes Mill Rd; Suite 300
Winston Salem, NC 27105
East Region Environmental Office
P.O. Box 1746
Watkinsville, GA 30677
phone [phone]
RE: Revised / Corrected 2021 Annual Report for Land Application Permit No. WQ0038087
Permittee: Terra Renewal Services, Inc
Dear Ms Caudle,
In response to your comments and questions provided via email on May 10, 2022, Terra Renewal is
providing a revised version of the annual report for the above referenced permit for calendar year 2021.
Responses are provided below in the order presented in the email:
1) No residuals were land applied under this permit in 2021 from Mathis-1 (storage facility), Hunter
Farms-Highpoint, or Brakebush Brothers-Mocksville. Samples were collected from the Mathis-1
storage tanks in case residuals were land applied and the data provided with the annual report;
however, removal of residuals from the storage tanks did not commence until 2022.
2) There were no residuals from AdvancePierre Foods -Claremont applied to the fields listed. The
source was entered on form LAFSF for these fields during the process of transferring data from
one field report to the other in Excel but a value of "0" was entered for volume applied.
3) A clerical error resulted in the AdvancePierre Foods -Claremont nitrogen and total solids data from
the June 10 sample being input incorrectly on forms RSSF, RSSF(B) and LAFSF (for the fields
listed). The data has been corrected and the corrected forms included in this revised report.
4) The acreage utilized for field NC-WK-MRF-06 was reported based on the previous acreage prior
to the construction of the storage tanks. This has been corrected and revised forms MFLSF,
FSF, an FSF(Supp) are provided with this version of the report.
5) The soil samples for the ASJ Mathis Farms were collected and processed by a third -party
consultant in 2021. The suite of parameters tested did not include copper, manganese, or acidity.
This was not detected until the annual report was compiled in February 2022. Terra Renewal is
in the process of collecting additional soil samples and that will include these parameters and will
provide that data to the Division upon completion.
6) See Item 4 above.
7) The incorrect PAN value for Tyson -Wilkesboro entered on form RSSF(B) was a typo. This has
been corrected and a revised form provided in this version of the report. All other data related to
this N values from the January 28 analysis are correct throughout the report.

8) Terra Renewal tracks precipitation and soil conditions as part of the daily inspection forms that
are required by the permit. It would be burdensome to both Terra Renewal and the Division to
enter residuals applications for each day based on the reporting format. This data can be made
available to the Division in the form of copies of the daily inspection logs and a separate summary
of precipitation and soil conditions if desired.
9) There were no additional Nitrogen sources applied to any of the fields to which residuals were
applied in 2021, other than poultry litter.
10) The fields listed were overseeded with a winter cover crop; however, the intent of this crop was
not to be harvested and was "burned down" prior to planting corn in the spring of 2022.
Additionally, the total dry tons and acreage applied for the year changed from 1,599 to 1,596 and 697 to
693 respectively based on the revisions. An amended copy of form ACF is included in the updated
version of the report. The Executive Summary table in Section 7 of the report under "Complimentary
Data" was also revised to include all changes made during these corrections.
Please contact me via phone or email if you have further questions or require additional information.
Thank you for your cooperation and attention to this matter.
Sincerely,
David C. Coyle
Senior Environmental Manager
NC LSS #1315

IIIE R I? A,
u" FN 111 ON W (1 II
March 1, 2022
North Carolina Department of Environmental Quality
Division of Water Resources
Water Quality Permit Section
Non -Discharge Permitting Unit
Information Processing Unit
6th Floor
512 N. Salisbury Street
Raleigh, NC 27699
East Region Environmental Office
P.O. Box 1746
Watkinsville, GA 30677
phone [phone]
RE: 2021 Annual Report for Land Application Permit No. WQ0038087
Permittee: Terra Renewal Services, Inc
Dear Sir or Madam,
The enclosed documentation is intended to serve as the annual report for the land application of residuals
sources related to the above referenced permit in Wilkes and Yadkin Counties.
The following information is provided:
PPrmittPP-
Terra Renewal Services, Inc.
P.O. Box 399
Dardanelle, AR 72834
Preparer & Contact:
Terra Renewal Services, Inc
David C. Coyle; Senior Environmental Manager
P.O. Box 1746
Watkinsville, GA 30677
phone: [phone]
email: david.coyle(cDterrarenewal.com
These items are included with the report (in order):
1) The Annual Land Application Certification Form (ACF)
2) The Annual Residuals Sampling Summary Form (RSSF) and Annual Residuals Sampling
Summary Form — B (RSSF-B) for each residuals source
3) The Annual Metals Field Loading Summary Form (MFLSF), Annual Land Application Field
Summary Form (FSF), and Annual Land Application Field Summary Form Supplement (FSF-
SUP)
4) Lab Analyses for Residuals:
— Nutrients, Metals, TCLP, Other
— Fecal Density (Seven Set)
5) Annual Pathogen and Vector Attraction Reduction Form for NCAC 2T Rules (PVRF 2T)
6) Soil Test Reports (for fields applied in 2020)

Page 2
2021 Annual Report
WQ0038087
7) Complimentary Data:
— Executive Summary
— Fecal Analysis Summary
— Poultry Litter Analysis Summary and Poultry Litter Analyses
If additional information is required or there are any questions regarding this annual report, please contact
David Coyle via the information listed above. Thank you for your cooperation and attention to this matter.
Sincerely,
David C. Coyle
Senior Environmental Manager
NC LSS #1315

3308 Bernice Avenue
Russellville, AR 72802
479.498.5000
March 19, 2019
North Carolina Department of Environmental Quality
Division of Water Resources
Water Quality Permits Section
Non -Discharge Permitting Unit
512 N. Salisbury Street
Raleigh, NC 27604
RE: Letter of Delegation for Signature Authority
1" E Hai° R A,
en ,eraai
P.O. Box 399
479.498.5000
This "Letter of Delegation" authorizes David C. Coyle, Environmental Manager, as a
representative and employee of Denali Water Solutions and Terra Renewal to produce, review,
or certify via signature any documentation associated with the following:
- Permit application, modification, and renewal
- Site & residuals source certification
- Reporting
- Permit transfer and termination
This authorization is provided under the guidelines of Rule 15A NCAC 02T .0106(b) and any
other applicable rules regarding compliance with the NC DEQ regulations.
For questions or further information regarding this matter, I may be contacted at
[e-mail] or 479-668-4502.
Sincerely,
/-r%, C-;Z0i&
Andy McNeill
Chief Executive Officer
Denali Water Solutions

1
Annual Land Application Certification Form (ACF)

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0038087 County: Wilkes & Yadkin Year:
Facility Name (as shown on permit):
Land Application Operator:
Terra Renewal Services, Inc
2021
Terra Renewal Services, Inc Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
E Yes D No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
57
Total number of fields utilized for land application during the year:
23
Total amount of dry tons applied during the year for all application sites:
1,596
Total number of acres utilizes for land application during the year:
693
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 21 Yes No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T . I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
David C. Coyle; Environmental Manager
Permittee Name and Title (type or print)
2/28/2022
Signature of Permittee
Date
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)

2
Annual Residuals Sampling Summary Form (RSSF)
Annual Residuals Sampling Summary Form — B (RSSF-B)

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3
Annual Metals Field Loading Summary Form (MFLSF)
Annual Land Application Field Summary Form (FSF)
Annual Land Application Field Summary Form Supplement (FSF-SUPP)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 39.63
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
21.8 Acres Permitted: 21.8 Site #: WK-CH-01 Field #:
10.4
Danripple
WK-CH-01
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......1......
Advance
Pierre
6/10/21
2....
RVAF
6/l/21
3....
Tyson-
Wilkes
6/l/21
4....
5....
6....
....
....
9....
10
11
12
% Solids
3.7
3.6
4.8
Arsenic
6.7
6.4
4.9
Cadmium
2.2
2.1
1.6
Copper
640.0
6.8
28.0
Chromium
Lead
6.2
4.3
3.3
Mercury
2.0
2.2
1 1.6
Molyb-
denum
18.0
17.0
13.0
Nickel
34.0
17.0
13.0
Selenium
8.9
8.6
6.5
Zinc
280.0
30.0
63.0
Total
Phos-
horus
7,400
6,400
2,800
Annual Heavy Metal Field Loadings Walculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
1.32
0.50
Arsenic
0.000
0.017
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Cadmium
0.000
0.006
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.000
0.018
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.046
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.011
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Mercury
0.000
0.006
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Molyb-
0.000
0.045
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
denum
Nickel
0.000
0.045
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Selenium
0.000
0.023
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Zinc
0.000
0.079
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.142
Total
Phos-
0.000
16.922
2.778
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
19.699
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/25/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 87.15
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
41.6 Acres Permitted: 41.6 Site #: WK-CH-03 Field #:
11.6
Banister
WK-CH-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......1......
Advance
Pierre
6/10/21
2....
RVAF
6/l/21
3....
Tyson-
Wilkes
6/l/21
4....
5....
6....
....
....
9....
10
11
12
% Solids
3.7
3.6
4.8
Arsenic
6.7
6.4
4.9
Cadmium
2.2
2.1
1.6
Copper
640.0
6.8
28.0
Chromium
Lead
6.2
4.3
3.3
Mercury
2.0
2.2
1 1.6
Molyb-
denum
18.0
17.0
13.0
Nickel
34.0
17.0
13.0
Selenium
8.9
8.6
6.5
Zinc
280.0
30.0
63.0
Total
Phos-
horus
7,400
6,400
2,800
Annual Heavy Metal Field Loadings Walculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.05
1.30
0.75
Arsenic
0.001
0.017
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
Cadmium
0.000
0.005
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
0.058
0.018
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.117
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.001
0.011
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Mercury
0.000
0.006
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Molyb-
0.002
0.044
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
denum
Nickel
0.003
0.044
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Selenium
0.001
0.022
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
Zinc
0.025
0.078
0.095
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.198
Total
Phos-
0.666
16.627
4.206
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
21.499
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
Permit #: WQ0038087 Cation Exchange Capacity (non 503 only):
Operator: Terra Renewal Services Owner: Mathis Properties, LLC Predominant Soil Series:
Acres Used: 35.8 Acres Permitted: 35.8 Site #: WK-CH-04 Field #:
97.91
10.9
Codorus
WK-CH-04
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......�......
Advance
Pierre
6/10/21
2....
RVAF
6/l/21
3....
Tyson-
Wilkes
6/l/21
4....
5....
6........
8....
9....
10
11
12
% Solids
3.7
3.6
4.8
Arsenic
6.7
6.4
4.9
Cadmium
2.2
2.1
1.6
Copper
640.0
6.8
28.0
Chromium
Lead
6.2
4.3
3.3
Mercury
2.0
2.2
1 1.6
Molyb-
denum
18.0
17.0
13.0
Nickel
34.0
17.0
13.0
Selenium
8.9
8.6
6.5
Zinc
280.0
30.0
63.0
Total
Phos-
horus
7,400
6,400
2,800
Annual Heavy Metal Field Loadings Walculated in Ibs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.03
2.24
0.47
Arsenic
0.000
0.029
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Cadmium
0.000
0.009
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
0.033
0.030
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.090
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.019
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Mercury
0.000
0.010
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Molyb-
0.001
0.076
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.089
denum
Nickel
0.002
0.076
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.090
Selenium
0.000
0.039
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.045
Zinc
0.015
0.134
0.059
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.208
Total
Phos-
0.385
28.659
2.632
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
31.676
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z-
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
Permit #: WQ0038087 Cation Exchange Capacity (non 503 only):
Operator: Terra Renewal Services Owner: Mathis Properties, LLC Predominant Soil Series:
Acres Used: 13.2 Acres Permitted: 13.2 Site #: WK-MF-09 Field #:
24.26
10.6
Fairview
W K-MF-09
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......�......
Advance
Pierre
6/10/21
2....
RVAF
9/2/21
3....
Tyson-
Wilkes
8/26/21
4....
5....
6........
8....
9....
10
11
12
% Solids
3.7
6.4
5.8
Arsenic
6.7
3.7
4.1
Cadmium
2.2
1.2
1.4
Copper
640.0
4.5
5.3
Chromium
Lead
6.2
2.5
2.8
Mercury
2.0
1.2
1 1.3
Molyb-
denum
18.0
9.9
11.0
Nickel
34.0
9.9
11.0
Selenium
8.9
5.0
5.5
Zinc
280.0
27.0
62.0
Total
Phos-
horus
7,400
9,100
3,600
Annual Heavy Metal Field Loadings Walculated in Ibs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
0.85
0.99
Arsenic
0.000
0.006
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Cadmium
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper
0.000
0.008
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.004
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Mercury
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.000
0.017
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.039
denum
Nickel
0.000
0.017
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.039
Selenium
0.000
0.008
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Zinc
0.000
0.046
0.123
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.168
Total
Phos-
0.000
15.452
7.121
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
22.573
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
Permit #: WQ0038087 Cation Exchange Capacity (non 503 only):
Operator: Terra Renewal Services Owner: Mathis Properties, LLC Predominant Soil Series:
Acres Used: 19.6 Acres Permitted: 19.6 Site #: WK-MF-10 Field #:
31.97
10.9
Fairview
WK-MF-10
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......�......
Advance
Pierre
6/10/21
2....
RVAF
9/2/21
3....
Tyson-
Wilkes
8/26/21
4....
5....
6........
8....
9....
10
11
12
% Solids
3.7
6.4
5.8
Arsenic
6.7
3.7
4.1
Cadmium
2.2
1.2
1.4
Copper
640.0
4.5
5.3
Chromium
Lead
6.2
2.5
2.8
Mercury
2.0
1.2
1 1.3
Molyb-
denum
18.0
9.9
11.0
Nickel
34.0
9.9
11.0
Selenium
8.9
5.0
5.5
Zinc
280.0
27.0
62.0
Total
Phos-
horus
7,400
9,100
3,600
Annual Heavy Metal Field Loadings Walculated in Ibs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
0.82
0.81
Arsenic
0.000
0.006
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Cadmium
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.000
0.007
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.004
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Mercury
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.000
0.016
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
denum
Nickel
0.000
0.016
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Selenium
0.000
0.008
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Zinc
0.000
0.044
0.101
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.145
Total
Phos-
0.000
14.869
5.861
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
20.730
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 32.27
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
22.5 Acres Permitted: 22.5 Site #: WK-MF-11 Field #:
9.8
Fairview
WK-MF-11
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......1......
Advance
Pierre
6/10/21
2....
RVAF
9/2/21
3....
Tyson-
Wilkes
8/26/21
4....
5....
6........
8....
9....
10
11
12
% Solids
3.7
6.4
5.8
Arsenic
6.7
3.7
4.1
Cadmium
2.2
1.2
1.4
Copper
640.0
4.5
5.3
Chromium
Lead
6.2
2.5
2.8
Mercury
2.0
1.2
1 1.3
Molyb-
denum
18.0
9.9
11.0
Nickel
34.0
9.9
11.0
Selenium
8.9
5.0
5.5
Zinc
280.0
27.0
62.0
Total
Phos-
horus
7,400
9,100
3,600
Annual Heavy Metal Field Loadings Walculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
0.85
0.58
Arsenic
0.000
0.006
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Cadmium
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.000
0.008
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.004
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Mercury
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.000
0.017
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.030
denum
Nickel
0.000
0.017
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.030
Selenium
0.000
0.009
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Zinc
0.000
0.046
0.072
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.118
Total
Phos-
0.000
15.543
4.176
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
19.719
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
WQ0038087
Terra Renewal Services Owner:
33.8 Acres Permitted:
Cation Exchange Capacity (non 503 only):
Mathis Properties, LLC Predominant Soil Series:
33.8 Site #: WK-MF-13 Field #;
96.09
12.0
Fairview
WK-MF-13
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......�......
Advance
Pierre
11/30/21
2....
RVAF
11/30/21
3....
Tyson-
Wilkes
11/30/21
4....
5....
6........
8....
9....
10
11
12
% Solids
7.0
3.8
5.0
Arsenic
1.0
6.5
4.8
Cadmium
0.3
2.2
1.6
Copper
450.0
13.0
27.0
Chromium
Lead
1.9
4.3
3.2
Mercury
0.3
2.1
1 1.7
Molyb-
denum
2.6
17.0
13.0
Nickel
35.0
17.0
13.0
Selenium
1.3
8.7
6.4
Zinc
140.0
56.0
38.0
Total
Phos-
horus
800
19,000
3,700
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
0.84
2.00
Arsenic
0.000
0.011
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.030
Cadmium
0.000
0.004
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Copper
0.000
0.022
0.108
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.130
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.007
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Mercury
0.000
0.004
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Molyb-
0.000
0.029
0.052
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.081
denum
Nickel
0.000
0.029
0.052
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.081
Selenium
0.000
0.015
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.040
Zinc
0.000
0.095
0.152
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.246
Total
Phos-
0.000
32.072
14.793
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
46.865
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
..........
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 17.27
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
23.4 Acres Permitted: 23.4 Site #: WK-MF-14 Field #:
10.1
Fairview
WK-MF-14
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......1......
Advance
Pierre
11/30/21
2....
RVAF
11/30/21
3....
Tyson-
Wilkes
11/30/21
4....
5....
6....
....
....
9....
10
11
12
% Solids
7.0
3.8
5.0
Arsenic
1.0
6.5
4.8
Cadmium
0.3
2.2
1.6
Copper
450.0
13.0
27.0
Chromium
Lead
1.9
4.3
3.2
Mercury
0.3
2.1
1 1.7
Molyb-
denum
2.6
17.0
13.0
Nickel
35.0
17.0
13.0
Selenium
1.3
8.7
6.4
Zinc
140.0
56.0
38.0
Total
Phos-
horus
800
19,000
3,700
Annual Heavy Metal Field Loadings Walculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
0.20
0.54
Arsenic
0.000
0.003
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Cadmium
0.000
0.001
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
0.000
0.005
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Mercury
0.000
0.001
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
0.000
0.007
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
denum
Nickel
0.000
0.007
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Selenium
0.000
0.004
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Zinc
0.000
0.023
0.041
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Total
Phos-
0.000
7.714
3.959
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.673
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 32.98
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
13.8 Acres Permitted: 13.8 Site #: WK-MF-15 Field #:
10.4
Fairview
WK-MF-15
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......1......
Advance
Pierre
11/30/21
2....
RVAF
11/30/21
3....
Tyson-
Wilkes
11/30/21
4....
5....
6....
....
....
9....
10
11
12
% Solids
7.0
3.8
5.0
Arsenic
1.0
6.5
4.8
Cadmium
0.3
2.2
1.6
Copper
450.0
13.0
27.0
Chromium
Lead
1.9
4.3
3.2
Mercury
0.3
2.1
1 1.7
Molyb-
denum
2.6
17.0
13.0
Nickel
35.0
17.0
13.0
Selenium
1.3
8.7
6.4
Zinc
140.0
56.0
38.0
Total
Phos-
horus
800
19,000
3,700
Annual Heavy Metal Field Loadings Walculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
0.76
1.63
Arsenic
0.000
0.010
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Cadmium
0.000
0.003
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Copper
0.000
0.020
0.088
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.108
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.007
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Mercury
0.000
0.003
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Molyb-
0.000
0.026
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.068
denum
Nickel
0.000
0.026
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.068
Selenium
0.000
0.013
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Zinc
0.000
0.085
0.124
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.209
Total
Phos-
0.000
28.804
12.077
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
40.881
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 108.16
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
59.2 Acres Permitted: 59.2 Site #: WK-MF-23 Field #:
8.7
Fairview
W K-MF-23
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......1......
Advance
Pierre
6/10/21
2....
RVAF
9/2/21
3....
Tyson-
Wilkes
8/26/21
4....
5....
6........
8....
9....
10
11
12
% Solids
3.7
6.4
5.8
Arsenic
6.7
3.7
4.1
Cadmium
2.2
1.2
1.4
Copper
640.0
4.5
5.3
Chromium
Lead
6.2
2.5
2.8
Mercury
2.0
1.2
1 1.3
Molyb-
denum
18.0
9.9
11.0
Nickel
34.0
9.9
11.0
Selenium
8.9
5.0
5.5
Zinc
280.0
27.0
62.0
Total
Phos-
horus
7,400
9,100
3,600
Annual Heavy Metal Field Loadings Walculated in Ibs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
0.92
0.91
Arsenic
0.000
0.007
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Cadmium
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper
0.000
0.008
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.005
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Mercury
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.000
0.018
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.038
denum
Nickel
0.000
0.018
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.038
Selenium
0.000
0.009
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Zinc
0.000
0.050
0.112
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.162
Total
Phos-
0.000
16.744
6.530
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
23.274
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
WQ0038087
Terra Renewal Services Owner:
18.9 Acres Permitted:
Cation Exchange Capacity (non 503 only):
Mathis Properties, LLC Predominant Soil Series:
18.9 Site #: WK-NMF-03 Field #;
52.18
15.1
Danripple
W K-MRF-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......�......
Advance
Pierre
12/3/20
2....
RVAF
11/19/20
3....
Tyson-
Wilkes
11/19/20
4....
Advance
Pierre
2A/21
5....
RVAF
1/28/21
.....6....
Tyson-
Wilkes
1/28/21
7....
8.....
.....9....
10
11
12
% Solids
2.7
9.4
6.2
6.5
3.1
6.2
Arsenic
9.3
2.6
4.0
0.7
8.0
3.9
Cadmium
3.1
0.9
1.3
0.2
2.7
1.3
Copper
490.0
1.7
31.0
31.0
8.7
34.0
Chromium
Lead
6.2
1.7
2.7
0.5
5.4
2.6
Mercury
2.8
0.9
1 1.2
1.2
2.6
1 1.2
Molyb-
denum
25.0
7.0
11.0
1.8
21.0
10.0
Nickel
25.0
7.0
11.0
2.2
21.0
10.0
Selenium
12.0
3.5
5.4
0.9
11.0
5.2
Zinc
82.0
8.7
69.0
8.0
60.0
82.0
Total
Phos-
horus
14,000
4,500
3,800
5,700
8,100
2,600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
1.12
0.99
0.00
0.41
0.25
Arsenic
0.000
0.006
0.008
0.000
0.007
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Cadmium
0.000
0.002
0.003
0.000
0.002
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.000
0.004
0.061
0.000
0.007
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.089
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.004
0.005
0.000
0.004
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Mercury
0.000
0.002
0.002
0.000
0.002
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Molyb-
0.000
0.016
0.022
0.000
0.017
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.059
denum
Nickel
0.000
0.016
0.022
0.000
0.017
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.059
Selenium
0.000
0.008
0.011
0.000
0.009
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.030
Zinc
0.000
0.019
0.136
0.000
0.049
0.040
0.000
0.000
0.000
0.000
0.000
0.000
0.245
Total
Phos-
0.000
10.080
7.486
0.000
6.642
1.279
0.000
0.000
0.000
0.000
0.000
0.000
25.487
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 73.98
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
14.1
Danripple
25.3 Acres Permitted: 25.3 Site #: WK-NIRF-05 Field #: WK-MRF-05
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......1......
Advance
Pierre
12/3/20
2....
RVAF
11/19/20
3....
Tyson-
Wilkes
11/19/20
4....
Advance
Pierre
2A/21
5....
RVAF
1/28/21
6........
Tyson-
Wilkes
1/28/21
8....
9....
10
11
12
% Solids
2.7
9.4
6.2
6.5
3.1
6.2
Arsenic
9.3
2.6
4.0
0.7
8.0
3.9
Cadmium
3.1
0.9
1.3
0.2
2.7
1.3
Copper
490.0
1.7
31.0
31.0
8.7
34.0
Chromium
Lead
6.2
1.7
2.7
0.5
5.4
2.6
Mercury
2.8
0.9
1 1.2
1.2
2.6
1 1.2
Molyb-
denum
25.0
7.0
11.0
1.8
21.0
10.0
Nickel
25.0
7.0
11.0
2.2
21.0
10.0
Selenium
12.0
3.5
5.4
0.9
11.0
5.2
Zinc
82.0
8.7
69.0
8.0
60.0
82.0
Total
Phos-
horus
14,000
4,500
3,800
5,700
8,100
2,600
Annual Heavy Metal Field Loadings Walculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
0.84
0.74
0.06
0.67
0.61
Arsenic
0.000
0.004
0.006
0.000
0.011
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Cadmium
0.000
0.001
0.002
0.000
0.004
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Copper
0.000
0.003
0.046
0.004
0.012
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.106
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.003
0.004
0.000
0.007
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Mercury
0.000
0.002
0.002
0.000
0.004
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Molyb-
0.000
0.012
0.016
0.000
0.028
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.069
denum
Nickel
0.000
0.012
0.016
0.000
0.028
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.069
Selenium
0.000
0.006
0.008
0.000
0.015
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.035
Zinc
0.000
0.015
0.102
0.001
0.081
0.101
0.000
0.000
0.000
0.000
0.000
0.000
0.299
Total
Phos-
0.000
7.533
5.594
0.730
10.919
3.188
0.000
0.000
0.000
0.000
0.000
0.000
27.963
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
Permit #: WQ0038087 Cation Exchange Capacity (non 503 only):
Operator: Terra Renewal Services Owner: Mathis Properties, LLC Predominant Soil Series:
Acres Used: 20.4 Acres Permitted: 20.4 Site #: WK-NMF-06 Field #:
52.18
14.8
Danripple
W K-MRF-06
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......�......
Advance
Pierre
12/3/20
2....
RVAF
11/19/20
3....
Tyson-
Wilkes
11/19/20
4....
Advance
Pierre
2A/21
5....
RVAF
1/28/21
.....6....
Tyson-
Wilkes
1/28/21
7....
8.....
.....9....
10
11
12
% Solids
2.7
9.4
6.2
6.5
3.1
6.2
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9.3
2.6
4.0
0.7
8.0
3.9
Cadmium
3.1
0.9
1.3
0.2
2.7
1.3
Copper
490.0
1.7
31.0
31.0
8.7
34.0
Chromium
Lead
6.2
1.7
2.7
0.5
5.4
2.6
Mercury
2.8
0.9
1 1.2
1.2
2.6
1 1.2
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denum
25.0
7.0
11.0
1.8
21.0
10.0
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25.0
7.0
11.0
2.2
21.0
10.0
Selenium
12.0
3.5
5.4
0.9
11.0
5.2
Zinc
82.0
8.7
69.0
8.0
60.0
82.0
Total
Phos-
horus
14,000
4,500
3,800
5,700
8,100
2,600
Annual Heavy Metal Field Loadings Walculated in Ibs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
1.04
0.30
0.00
0.53
0.68
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0.000
0.005
0.002
0.000
0.009
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Cadmium
0.000
0.002
0.001
0.000
0.003
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.007
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0.000
0.004
0.019
0.000
0.009
0.047
0.000
0.000
0.000
0.000
0.000
0.000
0.078
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
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0.000
0.004
0.002
0.000
0.006
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.014
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0.000
0.002
0.001
0.000
0.003
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.007
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0.000
0.015
0.007
0.000
0.022
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.057
denum
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0.000
0.015
0.007
0.000
0.022
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.057
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0.000
0.007
0.003
0.000
0.012
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.029
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0.000
0.018
0.042
0.000
0.064
0.112
0.000
0.000
0.000
0.000
0.000
0.000
0.236
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Phos-
0.000
9.342
2.310
0.000
8.618
3.557
0.000
0.000
0.000
0.000
0.000
0.000
23.828
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
Permit #: WQ0038087 Cation Exchange Capacity (non 503 only):
Operator: Terra Renewal Services Owner: Mathis Properties, LLC Predominant Soil Series:
Acres Used: 25.1 Acres Permitted: 25.1 Site #: WK-NMF-12 Field #:
79.69
12.5
Pfafftown
W K-MRF-12
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......�......
Advance
Pierre
12/3/20
2....
RVAF
11/19/20
3....
Tyson-
Wilkes
11/19/20
4....
Advance
Pierre
2A/21
5....
RVAF
1/28/21
.....6....
Tyson-
Wilkes
1/28/21
7....
8.....
.....9....
10
11
12
% Solids
2.7
9.4
6.2
6.5
3.1
6.2
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9.3
2.6
4.0
0.7
8.0
3.9
Cadmium
3.1
0.9
1.3
0.2
2.7
1.3
Copper
490.0
1.7
31.0
31.0
8.7
34.0
Chromium
Lead
6.2
1.7
2.7
0.5
5.4
2.6
Mercury
2.8
0.9
1 1.2
1.2
2.6
1 1.2
Molyb-
denum
25.0
7.0
11.0
1.8
21.0
10.0
Nickel
25.0
7.0
11.0
2.2
21.0
10.0
Selenium
12.0
3.5
5.4
0.9
11.0
5.2
Zinc
82.0
8.7
69.0
8.0
60.0
82.0
Total
Phos-
horus
14,000
4,500
3,800
5,700
8,100
2,600
Annual Heavy Metal Field Loadings Walculated in Ibs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.05
1.59
0.47
0.07
0.68
0.31
Arsenic
0.001
0.008
0.004
0.000
0.011
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Cadmium
0.000
0.003
0.001
0.000
0.004
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Copper
0.053
0.005
0.029
0.004
0.012
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.125
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.001
0.005
0.003
0.000
0.007
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Mercury
0.000
0.003
0.001
0.000
0.004
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.009
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0.003
0.022
0.010
0.000
0.029
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.070
denum
Nickel
0.003
0.022
0.010
0.000
0.029
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Selenium
0.001
0.011
0.005
0.000
0.015
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Zinc
0.009
0.028
0.065
0.001
0.082
0.051
0.000
0.000
0.000
0.000
0.000
0.000
0.235
Total
Phos-
1.512
14.337
3.602
0.741
11.016
1.607
0.000
0.000
0.000
0.000
0.000
0.000
32.815
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
WQ0038087 Cation Exchange Capacity (non 503 only):
Terra Renewal Services Owner: Mathis Properties, LLC Predominant Soil Series:
52.3 Acres Permitted: 52.3 Site #: WK-MRF-20 Field #:
290.74
10.4
Dan River
WK-MRF-20
Residual Analysis Data (Heavy Metals and Total Phosphorus use m2U, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
Advance
Pierre
6/10/21
.......2
RVAF
9/2/21
3
Tyson-
Wilkes
8/26/21
4
Advance
Pierre
11/30/21
5 1
RVAF
11/30/21
6
Tyson-
Wilkes
11/30/21
7
8.....
9.....
...9.....
1...1.......
1..2.....
% Solids
1 3.7
6.4
5.8
1 7.0
3.8
5.0
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6.7
3.7
4.1
1.0
6.5
4.8
Cadmium
2.2
1.2
1.4
0.3
2.2
1.6
Copper
640.0
4.5
5.3
450.0
13.0
27.0
Chromium
Lead
6.2
2.5
2.8
1.9
4.3
3.2
Mercury
2.0
1.2
1.3
0.3
2.1
1.7
Molyb-
denum
18.0
9.9
11.0
2.6
17.0
13.0
Nickel
34.0
1 9.9
11.0
35.0
17.0
13.0
Selenium
8.9
5.0
5.5
1.3
8.7
6.4
Zinc
280.0
27.0
62.0
140.0
56.0
38.0
Total
Phos-
horus
7,400
9,100
3,600
800
19,000
3,700
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
y
0
App.
Event
0.02
2.60
1.44
0.02
0.47
1.01
Arsenic
1 0.000
0.019
0.012
1 0.000
0.006
0.010
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.047
Cadmium
0.000
0.006
0.004
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Copper
0.023
0.023
0.015
0.016
0.012
0.054
0.000
0.000
0.000
0.000
0.000
0.000
0.145
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.013
0.008
0.000
0.004
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.032
Mercury
0.000
0.006
0.004
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Molyb-
0.001
0.052
0.032
0.000
0.016
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.126
denum
Nickel
0.001
0.052
0.032
0.001
0.016
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.128
Selenium
0.000
0.026
0.016
0.000
0.008
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Zinc
0.010
0.141
0.179
0.005
0.053
0.076
0.000
0.000
0.000
1 0.000
0.000
0.000
0.464
Total
Phos-
0.266
47.356
10.390
0.029
17.974
7.437
0.000
0.000
0.000
0.000
0.000
0.000
83.452
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
WQ0038087 Cation Exchange Capacity (non 503 only):
Terra Renewal Services Owner: Mathis Properties, LLC Predominant Soil Series:
27.8 Acres Permitted: 27.8 Site #: WK-MRF-21 Field #:
104.25
12.3
Dan River
WK-MRF-21
Residual Analysis Data (Heavy Metals and Total Phosphorus use m2U, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
Advance
Pierre
6/10/21
.......2
RVAF
6/1/21
3
Tyson-
Wilkes
6/1/21
4
RVAF
9/2/21
5 1
Tyson-
Wilkes
8/26/21
6
7
8.....
9.....
...9.....
1...1.......
1..2.....
% Solids
1 3.7
3.6
4.8
1 6.4
5.8
Arsenic
6.7
6.4
4.9
3.7
4.1
Cadmium
2.2
2.1
1.6
1.2
1.4
Copper
640.0
6.8
28.0
4.5
5.3
Chromium
Lead
6.2
4.3
3.3
2.5
2.8
Mercury
2.0
2.2
1.6
1.2
1.3
Molyb-
denum
18.0
17.0
13.0
9.9
11.0
Nickel
34.0
1 17.0
13.0
9.9
11.0
Selenium
8.9
8.6
6.5
5.0
5.5
Zinc
280.0
30.0
63.0
27.0
62.0
Total
Phos-
horus
7,400
6,400
2,800
9,100
3,600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
y
0
App.
Event
0.03
0.45
0.52
1.44
1.31
Arsenic
1 0.000
0.006
0.005
1 0.011
0.011
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.033
Cadmium
0.000
0.002
0.002
0.003
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
0.042
0.006
0.029
0.013
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.104
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.004
0.003
0.007
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Mercury
0.000
0.002
0.002
0.003
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Molyb-
0.001
0.015
0.013
0.029
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.087
denum
Nickel
0.002
0.015
0.013
0.029
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.088
Selenium
0.001
0.008
0.007
0.014
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
Zinc
0.018
0.027
0.065
0.078
0.162
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.351
Total
Phos-
0.488
5.811
2.901
26.208
9.396
0.000
0.000
0.000
0.000
0.000
0.000
0.000
44.804
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
WQ0038087 Cation Exchange Capacity (non 503 only):
Terra Renewal Services Owner: Barker, Kim Tharpe Predominant Soil Series:
57.8 Acres Permitted: 57.8 Site #: WK-RJ-02 Field #:
19.48
7.9
Dan River
WK-RJ-02
Residual Analysis Data (Heavy Metals and Total Phosphorus use m2U, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
Advance
Pierre
2/4/21
.......2
RVAF
1/28/21
3
Tyson-
Wilkes
1/28/21
4
5 1
6
7
8.....
9.....
...9.....
1...1.......
1..2.....
% Solids
1 6.5
3.1
6.2
Arsenic
0.7
8.0
3.9
Cadmium
0.2
2.7
1.3
Copper
31.0
8.7
34.0
Chromium
Lead
0.5
5.4
2.6
Mercury
1.2
2.6
1.2
Molyb-
denum
1.8
21.0
10.0
Nickel
2.2
1 21.0
10.0
Selenium
0.9
11.0
5.2
Zinc
8.0
60.0
82.0
Total
Phos-
horus
5,700
8,100
2,600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
•
D
Event
11
1
11:
1 111
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1 11
1 11
1 11 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 111
1 1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 111
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11•
®
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
Total
Phos-
1 •
••
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 187.62
WQ0038087
Terra Renewal Services Owner:
45.1 Acres Permitted:
Cation Exchange Capacity (non 503 only):
Johnson, J L Predominant Soil Series:
45.1 Site #: WK-RJ-05 Field #:
11.5
Dan River
WK-RJ-05
Residual Analysis Data (Heavy Metals and Total Phosphorus use m2U, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
Advance
Pierre
2/4/21
.......2
RVAF
1/28/21
3
Tyson-
Wilkes
1/28/21
4
Advance
Pierre
11/30/21
5 1
RVAF
11/30/21
6
Tyson-
Wilkes
11/30/21
7
8.....
9.....
...9.....
1...1.......
1..2.....
% Solids
1 6.5
3.1
6.2
1 7.0
3.8
5.0
Arsenic
0.7
8.0
3.9
1.0
6.5
4.8
Cadmium
0.2
2.7
1.3
0.3
2.2
1.6
Copper
31.0
8.7
34.0
450.0
13.0
27.0
Chromium
Lead
0.5
5.4
2.6
1.9
4.3
3.2
Mercury
1.2
2.6
1.2
0.3
2.1
1.7
Molyb-
denum
1.8
21.0
10.0
2.6
17.0
13.0
Nickel
2.2
1 21.0
10.0
35.0
17.0
13.0
Selenium
0.9
11.0
5.2
1.3
1 8.7
6.4
Zinc
8.0
60.0
82.0
140.0
56.0
38.0
Total
Phos-
horus
5,700
8,100
2,600
800
19,000
3,700
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
y
0
App.
Event
0.04
1.00
1.10
0.00
0.61
1.42
Arsenic
1 0.000
0.016
0.009
1 0.000
0.008
0.014
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.046
Cadmium
0.000
0.005
0.003
0.000
0.003
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Copper
0.002
0.017
0.075
0.000
0.016
0.076
0.000
0.000
0.000
0.000
0.000
0.000
0.187
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.011
0.006
0.000
0.005
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.031
Mercury
0.000
0.005
0.003
0.000
0.003
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Molyb-
0.000
0.042
0.022
0.000
0.021
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.122
denum
Nickel
0.000
0.042
0.022
0.000
0.021
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.122
Selenium
0.000
0.022
0.011
0.000
0.011
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.062
Zinc
0.001
0.120
0.181
0.000
0.068
0.108
0.000
0.000
0.000
1 0.000
0.000
0.000
0.477
Total
Phos-
0.410
16.151
5.725
0.000
23.218
10.471
0.000
0.000
0.000
0.000
0.000
0.000
55.976
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
WQ0038087 Cation Exchange Capacity (non 503 only):
Terra Renewal Services Owner: Red Oak Meadows, LLC Predominant Soil Series:
24.6 Acres Permitted: 24.6 Site #: WK-RJ-07 Field #:
43.44
11.2
Fairview
WK-RJ-07
Residual Analysis Data (Heavy Metals and Total Phosphorus use m2U, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
Advance
Pierre
2/4/21
.......2
RVAF
1/28/21
3
Tyson-
Wilkes
1/28/21
4
5 1
6
7
8.....
9.....
...9.....
1...1.......
1..2.....
% Solids
1 6.5
3.1
6.2
Arsenic
0.7
8.0
3.9
Cadmium
0.2
2.7
1.3
Copper
31.0
8.7
34.0
Chromium
Lead
0.5
5.4
2.6
Mercury
1.2
2.6
1.2
Molyb-
denum
1.8
21.0
10.0
Nickel
2.2
1 21.0
10.0
Selenium
0.9
11.0
5.2
Zinc
8.0
60.0
82.0
Total
Phos-
horus
5,700
8,100
2,600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
•
D
Event
1 11
1 ••
1
1 111
1 1
1 11:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
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1 111
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 11
1 11 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 111
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11•
1 111
1 1 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 111
1 1 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
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1 111
1 1:
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
Total
Phos-
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
Permit #: WQ0038087 Cation Exchange Capacity (non 503 only):
Operator: Terra Renewal Services Owner: Mathis Properties, LLC Predominant Soil Series:
Acres Used: 13.5 Acres Permitted: 13.5 Site #: YK-YF-01 Field #:
18.91
12.6
Nathalie
YK-YF-01
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......�......
Advance
Pierre
11/30/21
2....
RVAF
11/30/21
3....
Tyson-
Wilkes
11/30/21
4....
5....
6........
8....
9....
10
11
12
% Solids
7.0
3.8
5.0
Arsenic
1.0
6.5
4.8
Cadmium
0.3
2.2
1.6
Copper
450.0
13.0
27.0
Chromium
Lead
1.9
4.3
3.2
Mercury
0.3
2.1
1 1.7
Molyb-
denum
2.6
17.0
13.0
Nickel
35.0
17.0
13.0
Selenium
1.3
8.7
6.4
Zinc
140.0
56.0
38.0
Total
Phos-
horus
800
19,000
3,700
Annual Heavy Metal Field Loadings Walculated in Ibs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.07
0.78
0.56
Arsenic
0.000
0.010
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Cadmium
0.000
0.003
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper
0.063
0.020
0.030
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.113
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.007
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Mercury
0.000
0.003
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.000
0.026
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.041
denum
Nickel
0.005
0.026
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.046
Selenium
0.000
0.013
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Zinc
0.020
0.087
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.149
Total
Phos-
0.112
29.450
4.114
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
33.676
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 44.56
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
22.3 Acres Permitted: 22.3 Site #: YK-YF-03 Field #:
13.3
Clifford
YK-YF-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......1......
Advance
Pierre
6/10/21
2....
RVAF
9/2/21
3....
Tyson-
Wilkes
8/26/21
4....
Advance
Pierre
11/30/21
5....
RVAF
11/30/21
6........
Tyson-
Wilkes
11/30/21
8....
9....
10
11
12
% Solids
3.7
6.4
5.8
7.0
3.8
5.0
Arsenic
6.7
3.7
4.1
1.0
6.5
4.8
Cadmium
1 2.2
1.2
1.4
0.3
2.2
1.6
Copper
1 640.0
4.5
5.3
450.0
13.0
27.0
Chromium
Lead
6.2
2.5
2.8
1.9
4.3
3.2
Mercury
2.0
1.2
1 1.3
0.3
2.1
1 1.7
Molyb-
denum
18.0
9.9
11.0
2.6
17.0
13.0
Nickel
34.0
9.9
11.0
35.0
17.0
13.0
Selenium
8.9
5.0
5.5
1.3
8.7
6.4
Zinc
280.0
27.0
62.0
140.0
56.0
38.0
Total
Phos-
horus
7,400
9,100
3,600
800
19,000
3,700
Annual Heavy Metal Field Loadings Walculated in Ibs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
0.86
0.59
0.00
0.21
0.34
Arsenic
0.000
0.006
0.005
0.000
0.003
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Cadmium
0.000
0.002
0.002
0.000
0.001
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
0.000
0.008
0.006
0.000
0.006
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.038
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.004
0.003
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Mercury
0.000
0.002
0.002
0.000
0.001
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Molyb-
0.000
0.017
0.013
0.000
0.007
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.046
denum
Nickel
0.000
0.017
0.013
0.000
0.007
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.046
Selenium
0.000
0.009
0.006
0.000
0.004
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Zinc
0.000
0.047
0.073
0.000
0.024
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.169
Total
Phos-
0.000
15.688
4.219
0.000
8.094
2.494
0.000
0.000
0.000
0.000
0.000
0.000
30.495
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
WQ0038087
Terra Renewal Services Owner:
23.3 Acres Permitted:
Cation Exchange Capacity (non 503 only):
Mathis Properties, LLC Predominant Soil Series:
23.3 Site #: YK-YF-04 Field #;
11.30
13.2
Clifford
YK-YF-04
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......�......
Advance
Pierre
11/30/21
2....
RVAF
11/30/21
3....
Tyson-
Wilkes
11/30/21
4....
5....
6........
8....
9....
10
11
12
% Solids
7.0
3.8
5.0
Arsenic
1.0
6.5
4.8
Cadmium
0.3
2.2
1.6
Copper
450.0
13.0
27.0
Chromium
Lead
1.9
4.3
3.2
Mercury
0.3
2.1
1 1.7
Molyb-
denum
2.6
17.0
13.0
Nickel
35.0
17.0
13.0
Selenium
1.3
8.7
6.4
Zinc
140.0
56.0
38.0
Total
Phos-
horus
800
19,000
3,700
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
0.16
0.32
Arsenic
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Cadmium
0.000
0.001
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
0.000
0.004
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.001
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Mercury
0.000
0.001
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.000
0.006
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
denum
Nickel
0.000
0.006
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Selenium
0.000
0.003
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Zinc
0.000
0.018
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.043
Total
Phos-
0.000
6.194
2.383
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.577
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 50.06
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
13.2
Fairview
51.5 Acres Permitted: 51.5 Site #: WK-YK-YF-5 Field #: WK-YK-YF-5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
......1......
Advance
Pierre
11/30/21
2....
RVAF
11/30/21
3....
Tyson-
Wilkes
11/30/21
4....
5....
6....
....
....
9....
10
11
12
% Solids
7.0
3.8
5.0
Arsenic
1.0
6.5
4.8
Cadmium
0.3
2.2
1.6
Copper
450.0
13.0
27.0
Chromium
Lead
1.9
4.3
3.2
Mercury
0.3
2.1
1 1.7
Molyb-
denum
2.6
17.0
13.0
Nickel
35.0
17.0
13.0
Selenium
1.3
8.7
6.4
Zinc
140.0
56.0
38.0
Total
Phos-
horus
800
19,000
3,700
Annual Heavy Metal Field Loadings Walculated in Ibs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
IF
y
DT/Ac./
App.
14
Event
0.00
0.46
0.51
Arsenic
0.000
0.006
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Cadmium
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.000
0.012
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.040
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.004
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Mercury
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.000
0.016
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
denum
Nickel
0.000
0.016
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Selenium
0.000
0.008
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Zinc
0.000
0.052
0.039
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.091
Total
Phos-
0.000
17.556
3.774
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
21.330
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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4
Laboratory Analyses:
- Nutrients, Metals, TCLP, Other

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:WA29002
Date Completed:02/11/2021
02/12/2021 9:26 AM
Approved and released by:
Project Manager II: Lucas Odom
,�i
A4W
AMP VOWN Acr K er AI $1114ld
i
FA[ (' R F D 1 F IE D
o1SriuraA3,01PAI�3Y
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WA29002
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids, the initial sample amount used for the following samples was 3x more than the
standard procedure: WA29002-001, WA29002-002. The LOQ has been adjusted accordingly.
The following samples were not fully oxidized after the addition of 15mL of HNO3: WA29002-001,
WA29002-002. This is indicated by the samples exhibiting persistent brown fumes after complete acid
addition. Due to being biosolids and having low percent solids, the samples will not be weighed to a lower
mass and analysis will proceed as usual.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 12

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WA29002
Sample Number Sample ID Matrix Date Sampled Date Received
001 Tyson/Wilkesboro Solid 01/28/2021 1430 01/29/2021
002 Tyson/Harmony Solid 01/28/2021 1530 01/29/2021
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WA29002
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Tyson/Wilkesboro
Solid
% Volatile Solids
SM 2540G-
98
%
5
001
Tyson/Wilkesboro
Solid
Ammonia - N (gas
350.1
1500
mg/kg
5
001
Tyson/Wilkesboro
Solid
Nitrate -Nitrite - N (soluble)
353.2
21
mg/kg
5
001
Tyson/Wilkesboro
Solid
Phosphorus
365.1
2600
mg/kg
5
001
Tyson/Wilkesboro
Solid
TKN
351.2
62000
mg/kg
5
001
Tyson/Wilkesboro
Solid
Aluminum
601OD
500
mg/kg
6
001
Tyson/Wilkesboro
Solid
Copper
601OD
34
mg/kg
6
001
Tyson/Wilkesboro
Solid
Zinc
601OD
82
mg/kg
6
002
Tyson/Harmony
Solid
% Volatile Solids
SM 2540G-
90
%
7
002
Tyson/Harmony
Solid
Ammonia - N (gas
350.1
24000
mg/kg
7
002
Tyson/Harmony
Solid
Nitrate -Nitrite - N (soluble)
353.2
45
mg/kg
7
002
Tyson/Harmony
Solid
Phosphorus
365.1
8100
mg/kg
7
002
Tyson/Harmony
Solid
TKN
351.2
46000
mg/kg
7
002
Tyson/Harmony
Solid
Aluminum
601OD
14000
mg/kg
8
002
Tyson/Harmony
Solid
Calcium
601OD
23000
mg/kg
8
002
Tyson/Harmony
Solid
Copper
601OD
8.7
mg/kg
8
002
Tyson/Harmony
Solid
Potassium
601OD
5600
mg/kg
8
002
Tyson/Harmony
Solid
Sodium
601OD
6900
mg/kg
8
002
Tyson/Harmony
Solid
Zinc
601OD
60
mg/kg
8
(19 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 12

Client: Terra Renewal Services, Inc. Laboratory ID: WA29002-001
Description: Tyson/Wilkesboro Matrix: Solid
Date Sampled:01/28/2021 1430 % Solids: 6.18 01/29/2021 2327
Date Received:01/29/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
02/04/2021 0109 MOM
81767
1 350.1
(Ammonia - N ) 350.1
5
02/04/2021 1205 DRD
81813
1
(Nitrate-Nitr) 353.2
1
02/08/2021 2200 SRB
82243
1
(Phosphorus) 365.1
5
02/04/2021 1006 DMA
02/02/2021 1829 81587
1
(Soil pH meas) 9045D
1
02/03/2021 1834 AAB
81768
1 351.4
(TKN) 351.2
5
02/03/2021 1111 DMA
02/02/2021 1829 81582
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
98
%
1
Ammonia - N (gas diffusion)
350.1
1500
810
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
21
3.2
mg/kg
1
Phosphorus
7723-14-0 365.1
2600
400
mg/kg
1
Soil pH measured in water @ 18.1 o C
9045D
3.9
su
1
TKN
351.2
62000
2000
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 02/04/2021 1218 NCM
02/02/2021 2115 81616
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
280
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
280
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
280
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
280
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
280
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
280
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
280
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
109 41-132
Tetrachloro-m-xylene
103 35-106
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 02/02/2021 0923 JAB2 02/02/2021 0622 81496
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471B ND 1.2 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 12

Client: Terra Renewal Services, Inc. Laboratory ID: WA29002-001
Description: Tyson/Wilkesboro Matrix: Solid
Date Sampled:01/28/2021 1430 % Solids: 6.18 01/29/2021 2327
Date Received:01/29/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601OD 1 02/04/2021 1334 KSH2 02/02/2021 1115 81355
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
500
100
mg/kg
1
Arsenic
7440-38-2
601OD
ND
3.9
mg/kg
1
Cadmium
7440-43-9
601OD
ND
1.3
mg/kg
1
Calcium
7440-70-2
601OD
ND
1300
mg/kg
1
Copper
7440-50-8
6010D
34
2.6
mg/kg
1
Lead
7439-92-1
601OD
ND
2.6
mg/kg
1
Magnesium
7439-95-4
601OD
ND
1300
mg/kg
1
Molybdenum
7439-98-7
601OD
ND
10
mg/kg
1
Nickel
7440-02-0
601OD
ND
10
mg/kg
1
Potassium
7440-09-7
601OD
ND
1300
mg/kg
1
Selenium
7782-49-2
601OD
ND
5.2
mg/kg
1
Sodium
7440-23-5
601OD
ND
1300
mg/kg
1
Zinc
7440-66-6
6010D
82
13
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 12

Client: Terra Renewal Services, Inc. Laboratory ID: WA29002-002
Description: Tyson/Harmony Matrix: Solid
Date Sampled:01/28/2021 1530 % Solids: 3.10 01/29/2021 2327
Date Received:01/29/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
02/04/2021 0109 MOM
81767
1 350.1
(Ammonia - N ) 350.1
25
02/04/2021 1213 DRD
81813
1
(Nitrate-Nitr) 353.2
1
02/08/2021 2201 SRB
82243
2
(Phosphorus) 365.1
10
02/04/2021 1850 DMA
02/02/2021 1829 81587
1
(Soil pH meas) 9045D
1
02/03/2021 1759 AAB
81768
1 351.4
(TKN) 351.2
2
02/03/2021 1112 DMA
02/02/2021 1829 81582
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
90
%
1
Ammonia - N (gas diffusion)
350.1
24000
8100
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
45
6.5
mg/kg
1
Phosphorus
7723-14-0 365.1
8100
1600
mg/kg
2
Soil pH measured in water @ 17.3 o C
9045D
6.1
su
1
TKN
351.2
46000
1600
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 02/04/2021 1231 NCM
02/02/2021 2115 81616
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
550
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
550
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
550
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
550
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
550
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
550
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
550
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
106 41-132
Tetrachloro-m-xylene
106 35-106
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 02/02/2021 0931 JAB2 02/02/2021 0622 81496
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471B ND 2.6 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 12

Client: Terra Renewal Services, Inc. Laboratory ID: WA29002-002
Description: Tyson/Harmony Matrix: Solid
Date Sampled:01/28/2021 1530 % Solids: 3.10 01/29/2021 2327
Date Received:01/29/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601OD 1 02/04/2021 1338 KSH2 02/02/2021 1115 81355
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
14000
210
mg/kg
1
Arsenic
7440-38-2
601OD
ND
8.0
mg/kg
1
Cadmium
7440-43-9
601OD
ND
2.7
mg/kg
1
Calcium
7440-70-2
6010D
23000
2700
mg/kg
1
Copper
7440-50-8
6010D
8.7
5.4
mg/kg
1
Lead
7439-92-1
601OD
ND
5.4
mg/kg
1
Magnesium
7439-95-4
601OD
ND
2700
mg/kg
1
Molybdenum
7439-98-7
601OD
ND
21
mg/kg
1
Nickel
7440-02-0
601OD
ND
21
mg/kg
1
Potassium
7440-09-7
6010D
5600
2700
mg/kg
1
Selenium
7782-49-2
601OD
ND
11
mg/kg
1
Sodium
7440-23-5
6010D
6900
2700
mg/kg
1
Zinc
7440-66-6
6010D
60
27
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 12

Chain of Custody
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 12

PACE ANALYTICAL SERVICES. LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 12
7

PACE ANALYTICAL SERVICES, LLC
North Carolina Perm'it Parameters
z. Rni(Wals shall bQq"lye ii) dwn=strato ffiey am l, ce Cbnservation
and Rmovery Act (R(,TkA� The aTi#ga==�� ............... . w
JFMft—Mhjalff��, ��Tle-lkj�y spbeifiM in
Attachmtnt an.d. the Purnittee, sIVO mziT,,t Uin LLIAM Dsalts f(w to EftiEurrAun Wit" years.
sxzcpL OIIL-, fi-Ort fl-r, Nq11i-U,1=r1uq 41 thiE con'ditioil shall LN5 6po7,1Mlle in.,%Ud.:l1'=t A.
Tile,jiWaly�is shall.nclu-:ie the f o(lowing poaranaetem (t1w rug:ilatory level ifl milligram$ PcIf:liter
is pprent, Bscs)�
3. An analy6x; aiall rrAi&wIs filcm each �'fjurue RCWTOlting FNL�14 a 'ale
5Ver,ifiod in AdachmeiLt A� and the Nmiiuee shail mabitwirl [ho result$fOr Pi T-1in-iIuUw- Of five Yca
The anal yma ih&2 imlude the foll&-A^ng Parar�IeO-f-L
Al,xiuwnfituai
Cadmium
Caldum
Copper
Z
Lelia
.............
E-
Mmury
Nick&
Nitrpw-,NiiriLeMtroset
p=mi Total, Solids
. . ..........
L
'TERRA RENEWAL SERVICES
47q-747-8102
Attachment to COC fW-----8OUrC95::
Potassium
8OjCTL,Lt1r1
TKN
Zb)JQ
Volatilo Solids
71M
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 12

PACE ANALYTICAL SERVICES, LLC
samples Receipt Checklist JSPjC) (MEDDISC-15) RL:visf ed-9PT2020
issuing Ailho ri ty; Nice ENV -, WCUL pa"zpe I Of I
Sample! Receipt Checklist (SRO
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in WIV LS th- VOA vi-als?
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K.w.� Date: nt�29;ZD21
balrc,*� labl!i rPpp-Jed bY:
C'tbrrurelits;
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 12

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:WB05005
Date Completed:02/22/2021
02/22/2021 3:14 PM
Approved and released by:
Project Manager II: Lucas Odom
,�i
A4W
AMP VOWN Acr K er AI $1114ld
i
FA[ (' R F D 1 F IE D
o1SriuraA3,01PAI�3Y
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WBO5005
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
% Volatile Solids
The following samples were analyzed outside of analytical holding time due to analyst oversight:
WB05005-001, WB05005-002.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 12

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WB05005
Sample Number Sample ID Matrix Date Sampled Date Received
001 Adv. Foods/Claremont Solid 02/04/2021 1430 02/05/2021
002 Perdue/Concord Solid 02/04/2021 1500 02/05/2021
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WB05005
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Adv. Foods/Claremont
Solid
% Volatile Solids
SM 2540G-
90 H
%
5
001
Adv. Foods/Claremont
Solid
Ammonia - N (gas
350.1
340
mg/kg
5
001
Adv. Foods/Claremont
Solid
Nitrate -Nitrite - N (soluble)
353.2
16
mg/kg
5
001
Adv. Foods/Claremont
Solid
Phosphorus
365.1
5700
mg/kg
5
001
Adv. Foods/Claremont
Solid
TKN
351.2
25000
mg/kg
5
001
Adv. Foods/Claremont
Solid
Aluminum
601OD
870
mg/kg
6
001
Adv. Foods/Claremont
Solid
Copper
601OD
31
mg/kg
6
001
Adv. Foods/Claremont
Solid
Nickel
601OD
2.2
mg/kg
6
001
Adv. Foods/Claremont
Solid
Sodium
601OD
260
mg/kg
6
001
Adv. Foods/Claremont
Solid
Zinc
601OD
8.0
mg/kg
6
002
Perdue/Concord
Solid
% Volatile Solids
SM 2540G-
84 H
%
7
002
Perdue/Concord
Solid
Ammonia - N (gas
350.1
860
mg/kg
7
002
Perdue/Concord
Solid
Nitrate -Nitrite - N (soluble)
353.2
40
mg/kg
7
002
Perdue/Concord
Solid
Phosphorus
365.1
26000
mg/kg
7
002
Perdue/Concord
Solid
TKN
351.2
33000
mg/kg
7
002
Perdue/Concord
Solid
Aluminum
601OD
34000
mg/kg
8
002
Perdue/Concord
Solid
Potassium
601OD
7000
mg/kg
8
002
Perdue/Concord
Solid
Sodium
601OD
11000
mg/kg
8
(18 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 4 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WB05005-001
Description: Adv. Foods/Claremont Matrix: Solid
Date Sampled:02/04/2021 1430 % Solids: 6.54 02/10/2021 2345
Date Received:02/05/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
02/15/2021 0025 MOM
82943
1 350.1
(Ammonia - N) 350.1
1
02/08/2021 1647 KFE
82140
1
(Nitrate-Nitr) 353.2
1
02/16/2021 2135 SRB
82951
3
(Phosphorus) 365.1
10
02/21/2021 1048 DMA
02/19/2021 1753 83053
1
(Soil pH meas) 9045D
1
02/09/2021 2014 AAB
82081
3 351.4
(TKN) 351.2
2
02/17/2021 1206 DMA
02/16/2021 1828 83036
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
90 H
%
1
Ammonia - N (gas diffusion)
350.1
340
150
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
16
3.1
mg/kg
1
Phosphorus
7723-14-0 365.1
5700
760
mg/kg
3
Soil pH measured in water @ 18.9 ° C
9045D
4.5
su
1
TKN
351.2
25000
760
mg/kg
3
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A 1 02/15/2021 1103 NCM
02/14/2021 1119
82827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
260
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
260
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
260
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
260
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
260
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
260
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
260
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
93 41-132
Tetrachloro-m-xylene
90 35-106
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 02/09/2021 1353 JAB2 02/09/2021 0707 82263
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471B ND 1.2 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WB05005-001
Description: Adv. Foods/Claremont Matrix: Solid
Date Sampled:02/04/2021 1430 % Solids: 6.54 02/10/2021 2345
Date Received:02/05/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601OD 1 02/11/2021 2353 KSH2 02/10/2021 0956 82277
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
601OD
870
18
mg/kg
1
Arsenic
7440-38-2
601OD
ND
0.68
mg/kg
1
Cadmium
7440-43-9
601OD
ND
0.23
mg/kg
1
Calcium
7440-70-2
601OD
ND
230
mg/kg
1
Copper
7440-50-8
601OD
31
0.45
mg/kg
1
Lead
7439-92-1
601OD
ND
0.45
mg/kg
1
Magnesium
7439-95-4
601OD
ND
230
mg/kg
1
Molybdenum
7439-98-7
601OD
ND
1.8
mg/kg
1
Nickel
7440-02-0
601OD
2.2
1.8
mg/kg
1
Potassium
7440-09-7
601OD
ND
230
mg/kg
1
Selenium
7782-49-2
601OD
ND
0.90
mg/kg
1
Sodium
7440-23-5
601OD
260
230
mg/kg
1
Zinc
7440-66-6
601OD
8.0
2.3
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WB05005-002
Description: Perdue/Concord Matrix: Solid
Date Sampled:02/04/2021 1500 % Solids: 4.73 02/05/2021 2331
Date Received:02/05/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
02/15/2021 0025 MOM
82943
1 350.1
(Ammonia - N) 350.1
1
02/08/2021 1649 KFE
82140
1
(Nitrate-Nitr) 353.2
1
02/16/2021 2136 SRB
82951
3
(Phosphorus) 365.1
25
02/21/2021 1130 DMA
02/19/2021 1753 83053
1
(Soil pH meas) 9045D
1
02/09/2021 2016 AAB
82081
3 351.4
(TKN) 351.2
2
02/17/2021 1206 DMA
02/16/2021 1828 83036
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
84 H
%
1
Ammonia - N (gas diffusion)
350.1
860
210
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
40
4.2
mg/kg
1
Phosphorus
7723-14-0 365.1
26000
2600
mg/kg
3
Soil pH measured in water @ 19 ° C
9045D
5.3
su
1
TKN
351.2
33000
1100
mg/kg
3
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A 1 02/15/2021 1117 NCM
02/14/2021 1119
82827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
350
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
350
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
350
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
350
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
350
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
350
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
350
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
80 41-132
Tetrachloro-m-xylene
81 35-106
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 02/09/2021 1355 JAB2 02/09/2021 0707 82263
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471B ND 1.6 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WB05005-002
Description: Perdue/Concord Matrix: Solid
Date Sampled:02/04/2021 1500 % Solids: 4.73 02/05/2021 2331
Date Received:02/05/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601OD 1 02/11/2021 2356 KSH2 02/10/2021 0956 82277
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
601OD
34000
400
mg/kg
1
Arsenic
7440-38-2
601OD
ND
15
mg/kg
1
Cadmium
7440-43-9
601OD
ND
5.0
mg/kg
1
Calcium
7440-70-2
601OD
ND
5000
mg/kg
1
Copper
7440-50-8
601OD
ND
10
mg/kg
1
Lead
7439-92-1
601OD
ND
10
mg/kg
1
Magnesium
7439-95-4
601OD
ND
5000
mg/kg
1
Molybdenum
7439-98-7
601OD
ND
40
mg/kg
1
Nickel
7440-02-0
601OD
ND
40
mg/kg
1
Potassium
7440-09-7
601OD
7000
5000
mg/kg
1
Selenium
7782-49-2
601OD
ND
20
mg/kg
1
Sodium
7440-23-5
601OD
11000
5000
mg/kg
1
Zinc
7440-66-6
601OD
ND
50
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 12

PACE ANALYTICAL SERVICES, LLC
r
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 12

PACE ANALYTICAL SERVICES, LLC
North Carinfina Permit Parameters
1 RnsidiuKW Shall be. to clemoLstrale 6cy CSC h?ll S LR$Constrvaliun,
aud. Rccovcry A (Re '). Ple ari l yes
a uency sp- M fierI in
,ttgahMdi1t wed file F'erw1llrtee shad rr'tRIM:Win these rwalts fcr a iriiTtil-11 UM ref' five ' a7s1 Any
Oxocptloaa fw-OM Lhe "Ui'�a1�rour's in this 00ii6tion strait be, speroitied in A twhm cnt A.
111eaalyais shall fiwW& tho fAowirig P21M=trrs (the nagulatnry ltwol in milUiga= per ,iris
is ixxg@3�.3s',
I An analysis shaL l tinted o11 =,rdumlF. frrma each 5ourcc gmwiutinfwbq at he ftoqmnoy
sect. in Attaj�lu, tjt A, ftrd thL PuTmittca Fhall. maiMia d rmul.ts aor a, winimum ixf Ilya: years,
ile analysis sltail,i1101aicl,r: Chu ft'llumingparameters:
A I io rcukwwi; r--Ditty-D8=
C,Arii_rwut
Qikium
Col,perr
Iewl
�vTr�wi�arn
orcur'y
Mulyb ,znum
Nickel
Nitrate-Nitritt, N'itm,gm
pk�rcelat,lblal Sohda
_ LAI
phosphorus
TERRA RENEWAL SERVICES
475-747-8192
P��t0.ssruuui
Sodium
zinc
Volatile Solids
pad
Atta.chmant to COC for.....9�r.u.rw
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 12

PACE ANALYTICAL SERVICES, LLC
�jvmplj!s Receipt Checklist (SM) (M EOO WAS)
Reifted-9/2917070
lssoi-ip Autharly, Pace MV - VOCOL
Pago 10 1
Sam . pie Receipt Chevidist SRC)
Term RVjlQ-.VHL I Jill W.MO-VLW2 L WOUJON
. ............ Other;
Means of 1-06611t: We ,� Client
Lly��jl PINT 71, %'rKVLA',-rlII.cllL the ccioJar?
Ljlve?,l 0 K(1LL'/JNXf! if custody s'�mhj were t)rTFjr, weretbry int"ItunAl wokwokafi
. . . ............. — =n 1111
Chlcwine Strip Tustud by. 'A
. ....... T[ -
OTil."ifflil. ternri,01 S71LTIU UrDE. reoaizit I Derived (Corrjxtcd� lompetritrile Upm rccoipl; ��Sofid Snkip-Cup .
...........
M O:La -C KA fNA oC NA I LNA DC NA rNA o(-
5
Mcih-c-d; ET21L-penturr, BlArk E34gainst Butllr,,� I R Gun ID: IR Gun. Curp-eti 01:1 Fact
Oc
MotbrM 121,Cnolant.. �2] )Art;,� [-,e E] Ice llams El Dry Scv 0 Not 0
IL]Ncs
M N A I Iftomponfli'lru Ofany cc-&Jer 6-01�1(,, was 11rujutA Maiinger NOJ(1ed?
LjNu
P M wkm N mi Ili ed by.- phora I tmail ? faceto-faluz (P iTclu "ne).
EJ Yes
No
-f -KA
Z Is Ow vowmercj.,j ccmjrjrr'c; packng slip atmhcdto biN forlin?
1, Mstody prixed -c-
5, were Pro. RE ute& (t I1aqulshe&'ec.6v9d) fukv-4?
NO
F,i] Ye
o
0. WLi-c santple IN [istril m the COC?
Goo
V�'��rc $tjrtjpla lj)�s Jj3(egt L)c ail sampic comineFs?
—toye&
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8, %Vkq, cL)IjLctjcn c[utc &- I,iime I isted on the
es
10
yes & Il ctioln tlr Fr rjrn l steel n sell trwarlrlr; con Suers"?
7"P Yes
No
10. Did all containcr lal-►LA inrim"juation (ED, mate, Norse) agree with 11= COC?
Y.
Nd
ry
I 11. Wvrr- Lusl.& to be pjfurmcd hsted on. flic COC?
0 y,,'-sl 0
Ye5j [JNO
12, Oid all Sal I, pies anive in the Fora corktaLncirs for cw:h test Luidool' in ' goon. condition
(unlivokell, lid" slab, m')?
1.3. Was u6equatd salu .!(3 Vq! Imle avai I able!
-4. %VL-re al'. sairimpbes receives within V, the holid3r9th-ne orrlg hor.in. %vhjchcvcrcorn,O fil',9t?
115. Vvcrr any Samples conmi nlrrs Mjr4 j11'p/eXri7Z,% (circles orm) Ill Jes Not listr:d cm COU!
16, Fo-, VOA and KSK- t 7 5 samples„ wc rc btlbbl,es 1) Fesei a 61r M, h dilarnalerf
NI'A ii any oCth:e VOA vlegIls?
A 'A u17
T7- Wen- rill [MOinietal,shlutuiclit sj-mZ1.rs received st EL p,
,� 3NE4A M Were all cyaToitk mairripies re"Md M a p11:, 12 and
0,YLs-1 ONoll MNA
.reeeixed at.N pH > -W
!Ly5ormple's rir6 ol-
El Yes [--]No : �WINA 20- 1%lere clivit 1re.minrksireques15 (ix. rLN,ueJAMST)
sctd dilutions, S6esfgnatlom:, ac,
-ztlytraL1rr-'r["JMi fimrritlieC'(�C jrLtothcwjrjrriejilseajon uAIMS?
77—v.. -rT—N-,. I %V�vi lilt UUL)LC flumb"V'Asttki M It" lubul? lfy&q!, Quote A'!
........ ..................
Mple(s) wc-c pxxiyod Lnemrectly pro5civrd mut werc @djusl:Od Occ,�Vfingly
v1MP!.e rec&vinz will, MA I r L of circlo on.- 1.1 2SU4, 11 NO3, HC 1, NaOH asing:SR 0 "J'
. M-%
rrlL,� ol'prtservaim,., — -. I ,' j n ore diari one preservari vc is TLQ;;d4;j, pj"m e� mote ju. the irf imMen ts Le low.
NA
v,ere roDoived with bubbles >6 Rim in ;!4w110er.
W, %V1I.hTRC>0.5
NA
bliri.�jde labels applied 1.Yy' IK5G
Comm xnts--
Date.,
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 12

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:WF02004
Date Completed:06/14/2021
06/15/2021 8:45 AM
Approved and released by:
Project Manager II: Lucas Odom
,�i
A4W
AMP VOWN Acr K er AI $1114ld
i
FA[ (' R F D 1 F IE D
o1SriuraA3,01PAI�3Y
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WF02004
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low percent solids, the following samles were weighed at 3x the standard procedure: WF02004-
001 and WF02004-002. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 12

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WF02004
Sample Number Sample ID Matrix Date Sampled Date Received
001 Tyson - Wilksboro Solid 06/01/2021 1330 06/02/2021
002 Tyson - Harmony Solid 06/01/2021 1430 06/02/2021
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WF02004
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Tyson - Wilksboro
Solid
% Volatile Solids
SM 2540G-
99
%
5
001
Tyson - Wilksboro
Solid
Ammonia - N (gas
350.1
12000
mg/kg
5
001
Tyson - Wilksboro
Solid
Nitrate -Nitrite - N (soluble)
353.2
38
mg/kg
5
001
Tyson - Wilksboro
Solid
Phosphorus
365.1
2800
mg/kg
5
001
Tyson - Wilksboro
Solid
TKN
351.2
79000
mg/kg
5
001
Tyson - Wilksboro
Solid
Aluminum
601 OD
310
mg/kg
6
001
Tyson - Wilksboro
Solid
Copper
601 OD
28
mg/kg
6
001
Tyson - Wilksboro
Solid
Zinc
601 OD
63
mg/kg
6
002
Tyson - Harmony
Solid
% Volatile Solids
SM 2540G-
89
%
7
002
Tyson - Harmony
Solid
Ammonia - N (gas
350.1
27000
mg/kg
7
002
Tyson - Harmony
Solid
Nitrate -Nitrite - N (soluble)
353.2
51 S
mg/kg
7
002
Tyson - Harmony
Solid
Phosphorus
365.1
6400
mg/kg
7
002
Tyson - Harmony
Solid
TKN
351.2
43000
mg/kg
7
002
Tyson - Harmony
Solid
Aluminum
601 OD
4600
mg/kg
8
002
Tyson - Harmony
Solid
Calcium
601 OD
15000
mg/kg
8
002
Tyson - Harmony
Solid
Copper
601 OD
6.8
mg/kg
8
002
Tyson - Harmony
Solid
Potassium
601 OD
3900
mg/kg
8
002
Tyson - Harmony
Solid
Sodium
601 OD
5200
mg/kg
8
002
Tyson - Harmony
Solid
Zinc
601 OD
30
mg/kg
8
(19 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 4 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WF02004-001
Description: Tyson - Wilksboro Matrix: Solid
Date Sampled:06/01/2021 1330 % Solids: 4.83 06/03/2021 0023
Date Received:06/02/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
06/08/2021 2358 MOM
94835
1 350.1
(Ammonia - N) 350.1
25
06/08/2021 1456 KFE
94701
1
(Nitrate-Nitr) 353.2
1
06/03/2021 2034 AAB
94397
1
(Phosphorus) 365.1
5
06/03/2021 1616 DMA
06/03/2021 1133 94171
1
(Soil pH meas) 9045D
1
06/11/2021 1924 DAK
95346
1 351.4
(TKN) 351.2
5
06/10/2021 1339 DMA
06/09/2021 1758 94960
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
99
%
1
Ammonia - N (gas diffusion)
350.1
12000
5200
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
38
4.1
mg/kg
1
Phosphorus
7723-14-0 365.1
2800
520
mg/kg
1
Soil pH measured in water @ 21.6 ° C
9045D
5.8
su
1
TKN
351.2
79000
5200
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A 1 06/11/2021 1550 JPB
06/09/2021 2133 94992
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
350
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
350
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
350
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
350
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
350
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
350
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
350
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
90 41-132
Tetrachloro-m-xylene
78 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 06/10/2021 1702 CMS2 06/09/2021 1510 94942
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471B ND 1.6
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WF02004-001
Description: Tyson - Wilksboro Matrix: Solid
Date Sampled:06/01/2021 1330 % Solids: 4.83 06/03/2021 0023
Date Received:06/02/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601OD 1 06/10/2021 1228 JMH 06/10/2021 0417 94929
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
601OD
310
130
mg/kg
1
Arsenic
7440-38-2
601OD
ND
4.9
mg/kg
1
Cadmium
7440-43-9
601OD
ND
1.6
mg/kg
1
Calcium
7440-70-2
601OD
ND
1600
mg/kg
1
Copper
7440-50-8
601OD
28
3.3
mg/kg
1
Lead
7439-92-1
601OD
ND
3.3
mg/kg
1
Magnesium
7439-95-4
601OD
ND
1600
mg/kg
1
Molybdenum
7439-98-7
601OD
ND
13
mg/kg
1
Nickel
7440-02-0
601OD
ND
13
mg/kg
1
Potassium
7440-09-7
601OD
ND
1600
mg/kg
1
Selenium
7782-49-2
601OD
ND
6.5
mg/kg
1
Sodium
7440-23-5
601OD
ND
1600
mg/kg
1
Zinc
7440-66-6
601OD
63
16
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 6 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WF02004-002
Description: Tyson - Harmony Matrix: Solid
Date Sampled:06/01/2021 1430 % Solids: 3.64 06/03/2021 0023
Date Received:06/02/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
06/08/2021 2358 MOM
94835
1 350.1
(Ammonia - N) 350.1
25
06/08/2021 1416 KFE
94701
1
(Nitrate-Nitr) 353.2
1
06/03/2021 2035 AAB
94397
1
(Phosphorus) 365.1
5
06/03/2021 1617 DMA
06/03/2021 1133 94171
1
(Soil pH meas) 9045D
1
06/11/2021 1926 DAK
95346
1 351.4
(TKN) 351.2
2
06/10/2021 1339 DMA
06/09/2021 1758 94960
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
89
%
1
Ammonia - N (gas diffusion)
350.1
27000
6900
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
51 S
5.5
mg/kg
1
Phosphorus
7723-14-0 365.1
6400
690
mg/kg
1
Soil pH measured in water @ 21.6 ° C
9045D
5.9
su
1
TKN
351.2
43000
2700
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A 1 06/11/2021 1604 JPB
06/09/2021 2133 94992
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
470
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
470
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
470
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
470
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
470
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
470
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
470
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
103 41-132
Tetrachloro-m-xylene
95 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 06/10/2021 1705 CMS2 06/09/2021 1510 94942
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471B ND 2.2
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WF02004-002
Description: Tyson - Harmony Matrix: Solid
Date Sampled:06/01/2021 1430 % Solids: 3.64 06/03/2021 0023
Date Received:06/02/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601OD 1 06/10/2021 1418 JMH 06/10/2021 0417 94929
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
601OD
4600
170
mg/kg
1
Arsenic
7440-38-2
601OD
ND
6.4
mg/kg
1
Cadmium
7440-43-9
601OD
ND
2.1
mg/kg
1
Calcium
7440-70-2
601OD
15000
2100
mg/kg
1
Copper
7440-50-8
601OD
6.8
4.3
mg/kg
1
Lead
7439-92-1
601OD
ND
4.3
mg/kg
1
Magnesium
7439-95-4
601OD
ND
2100
mg/kg
1
Molybdenum
7439-98-7
601OD
ND
17
mg/kg
1
Nickel
7440-02-0
601OD
ND
17
mg/kg
1
Potassium
7440-09-7
601OD
3900
2100
mg/kg
1
Selenium
7782-49-2
601OD
ND
8.6
mg/kg
1
Sodium
7440-23-5
601OD
5200
2100
mg/kg
1
Zinc
7440-66-6
601OD
30
21
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 12

PACE ANALYTICAL SERVICES, LLC
F.
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 12

PACE ANALYTICAL SERVICES, LLC
North Carolina Permit Parameters
I Residuals shall be anflynd tri dLm-Lmz1rHW Lhc y Constrvauon
zrW ReQovory Act i(R MA), T!,w M
sp"i1a
AtiiAmzrtt. A, and the Permilme ShRU, Maintdin thr%e restAls fw a nikEnnon of five ysars- Any
eyc2pticms frrjrn ffI,, rqWreiiients iri d-As�mndiifoki shM'l be spCcifal in wit djltezit'k
The--1 nYiysig shall indade di.- parametcns (ffie replataxy keel in ffiflligruns per liter
aB iupwolllheses�
:.n an�jysis shall, 'm monducted un iduals from e=h =roe geatrating fadhILY V the, ftituuTkey
Specified in Attactimmit A, sind tbu P.-iimitLee :1-mU r�:iiitaia drosQts fa a mir-imilm d Ew, yoars,
11c analysi& shalt irsbidu fl-,Q fnllnwing pm4rnrixxs:
Al'urilinutu
Mumiry -PuLEL�SiUILU
I
. ...........
Vim
Arseiiiio
Nickul
---------
Cadrrzi r
-----
iLrate-Vitrite Mtn, gen
. . ...........................
........................ .........
Calciuw.
Ptrwnt Tool Solid; TKN
7inc
("Opper
PH
L&ad
ptlosphorus
Vola'11c Soli�,ds
. .
. ...................................
..... .
Z)
PCB's
TERRA RENEWAL SERVICES
479-747-8192
Attachment to COC fan.—Soureas, 'r�jr-' 4'-z'
..........
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 12

PACE ANALYTICAL SERVICES, LLC
5arnples ijeceipt 11 cMit%k (S1 j (MF13t11SC-bS) Ftev1.5-2d:9f29,r2m,O
dc° f x` iyPh�E� 1s5garg Ai it'fiorite Picc EM) -WCOIL a e .i of I
Sample Receipt Chetkiist (SRC'
C,:licmt: C: >raler I-bR c°ted by dam; rRG2 r NM2!202<. L11L 14: tXEdY' 04
i ftrl �rfiv.1tutPt tardc� tt
mew ' w hit
1 _ Werer-,3'; dV 5e,a1s 17-CI.Wilt O',j 'dle
Yes moo
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pH Strip 1D.
r T�, tort 1�,�
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n nt. npt %Solid S;wP-("JP H�'��..
7riins B mprratr�rc rtpn cllrter�Id C"rurtir orl�lrml,�n araaax upon
3°4 ,e34 -C
NA jN.),, aC NA ,rNA o(,, 'NA. NNA "'C
ui od: ❑fern per"aturc Blank proll rFi,11i �S 1K. Gur: ID: � IR Gun lr,l';1'ITI."rl ion Fadcr: I� °�C
M dd of cools
c El WeiIce: Iex, r' ick.% C Div lee ❑ None
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r �` l`1e�L I If t n l rcrlacrt lwTarta�er
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�I 51V��ll.r d 1,I�V r11�nrI r��rrr a �� �rw-1 � �I
c'urcle crre1.
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4�. Is die commercial cnn_ri.,rlit pinking Ali attach l to this I�a__al�
w"' "Y 'S
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a3,: Were poper cu0ndy p-oc !.FRFS 'b 111nG1bltlsllErJ�"ra�u iw V} hall av°ct]'>
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9, Wft.i 011311120 icln dtli , & liir c Iiisl. d on all sarnpl,os corn arltca"�?
0 Yes
LjNo
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i��
- it libel ins s y�na , nx�t" u.
1iN. Lli,tJ tll u'gylnCegk[WUf r�MR1i�1[[t�ll ]«, date, tl'rtpr �i nay � h tM ce
" S
1 dh
11, Were wml to be p,-i-fDri ed lrsltYd oil Idre;C()C.1
e
c
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1--" .Did a]11 �s, , pLes a1f Ike tt6 V1hu P,TL►fJI C :dln'Ca'Ln�rs fD1' ac17 test �nah°a"rr log �f�QLI C41�{�ltl4;n
('w1�hr01=, Iid ,*, on, ct "�"� _...
14,. Were all svrr„ipke 5 moxivW'ifllia .the 1101rding linac or 48 hour's, mlhi.cheve'r conmc�,s fir°.�°
" .es
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.correctly fans ribrd from The. COC ir' ul lLQ ounlrunt Rcction in Li.M' 7
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Sample Pmes�rw��ir3t (�rS1�„ ��nPi�td �tll�;�Pitts fA�:-�Iurwcal arr tiv.'a'tlt 11.cfad5pF1ce.) 9
�3�n�d r] R �.r�
- - wfre received itict"�I't'ceffy 'esel'vged ft:jd wiser 11dj uxled AC e� a>� in��'' �
1
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lit rdl rre er' ^' i t NA ° If rr1L3% thnan rmre p�scrw'8tiv e -s mccdex� fjlc'aRc' no-c itn tliv a cll rnerhi k]d?'i cyw.
rtJrrpdr�sd t `
_.................... �wrer� reocivcd with bubbles>�. mini in dianrmil.
----------
were rejci'e°tn"ti,1 with't'➢t1, > 111,:1 rntel.. (Il'4'l'9 Ls no) and Wei
,Itt�xd me uruingly in aamplle,, m 't'QUI,(�', WiJ1 31}diuni rI'r](NatlrsA- (Nl020,) '4 ich .Shealy la NIA ..
SR blyrcrlde Ilhls ,
1pd:ed by: �JR02 Date! O(N9LP2M1
I:om w, cots:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 12

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:WF11024
Date Completed:06/25/2021
06/25/2021 2:51 PM
Approved and released by:
Project Manager II: Lucas Odom
,�i
A4W
AMP VOWN Acr K er AI $1114ld
i
FA[ (' R F D 1 F IE D
o1SriuraA3,01PAI�3Y
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WF11024
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to percent solids, the following samples were weighed out at 3x the standard procedure: WF11024-
001, WF11024-002. The LOQ has been adjusted.
PCBs by GC
The following sample was diluted due to the nature of the sample matrix: WF11024-002. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 12

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WF11024
Sample Number Sample ID Matrix Date Sampled Date Received
001 Perdue/Concord Solid 06/10/2021 1430 06/11/2021
002 Advanced Foods/Claremont Solid 06/10/2021 1530 06/11/2021
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WF11024
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
Perdue/Concord
Solid
% Volatile Solids
SM 2540G-
89
%
5
001
Perdue/Concord
Solid
Ammonia - N (gas
350.1
3000
S
mg/kg
5
001
Perdue/Concord
Solid
Nitrate -Nitrite - N (soluble)
353.2
27
S
mg/kg
5
001
Perdue/Concord
Solid
Phosphorus
365.1
22000
S
mg/kg
5
001
Perdue/Concord
Solid
TKN
351.2
47000
mg/kg
5
001
Perdue/Concord
Solid
Aluminum
601OD
19000
mg/kg
6
001
Perdue/Concord
Solid
Calcium
601OD
2200
mg/kg
6
001
Perdue/Concord
Solid
Copper
601OD
7.3
mg/kg
6
001
Perdue/Concord
Solid
Potassium
601OD
6300
mg/kg
6
001
Perdue/Concord
Solid
Sodium
601OD
7800
mg/kg
6
001
Perdue/Concord
Solid
Zinc
601OD
83
mg/kg
6
002
Advanced Foods/Claremont
Solid
% Volatile Solids
SM 2540G-
89
%
7
002
Advanced Foods/Claremont
Solid
Ammonia - N (gas
350.1
1500
mg/kg
7
002
Advanced Foods/Claremont
Solid
Nitrate -Nitrite - N (soluble)
353.2
36
mg/kg
7
002
Advanced Foods/Claremont
Solid
Phosphorus
365.1
7400
S
mg/kg
7
002
Advanced Foods/Claremont
Solid
TKN
351.2
7700
mg/kg
7
002
Advanced Foods/Claremont
Solid
Aluminum
601OD
14000
mg/kg
8
002
Advanced Foods/Claremont
Solid
Calcium
601OD
4400
mg/kg
8
002
Advanced Foods/Claremont
Solid
Copper
601OD
640
mg/kg
8
002
Advanced Foods/Claremont
Solid
Lead
601OD
6.2
mg/kg
8
002
Advanced Foods/Claremont
Solid
Nickel
601OD
34
mg/kg
8
002
Advanced Foods/Claremont
Solid
Potassium
601OD
2200
mg/kg
8
002
Advanced Foods/Claremont
Solid
Sodium
601OD
13000
mg/kg
8
002
Advanced Foods/Claremont
Solid
Zinc
601OD
280
mg/kg
8
(24 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 4 of 12

Client:Terra Renewal Services, Inc. Laboratory ID: WF1 1024-001
Description: Perdue/Concord Matrix: Solid
Date Sampled:06/10/2021 1430 % Solids: 5.70 06/12/2021 2001
Date Received: 06/11/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
06/17/2021 2357 MOM
95937
1 350.1
(Ammonia - N) 350.1
5
06/16/2021 1452 KFE
95636
1
(Nitrate-Nitr) 353.2
1
06/16/2021 2108 AAB
95887
1
(Phosphorus) 365.1
25
06/14/2021 1345 DMA
06/11/2021 1709 95282
1
(Soil pH meas) 9045D
1
06/13/2021 1952 NBW
95369
1 351.4
(TKN) 351.2
5
06/14/2021 1326 DMA
06/11/2021 1800 95288
CAS Analytical
Parameter
Number Method
Result
Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
89
%
1
Ammonia - N (gas diffusion)
350.1
3000
S
880
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
27
S
3.5
mg/kg
1
Phosphorus
7723-14-0 365.1
22000
S
2200
mg/kg
1
Soil pH measured in water @ 21.3 ° C
9045D
4.5
su
1
TKN
351.2
47000
4400
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A 1 06/24/20211403 JPB
06/18/2021 1511
96014
CAS Analytical
Parameter
Number Method
Result
Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
300
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
300
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
300
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
300
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
300
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
300
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
300
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
95 41-132
Tetrachloro-m-xylene
94 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 06/16/2021 1738 CMS2 06/15/2021 1638 95526
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471B ND 1.4
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID: WF1 1024-001
Description: Perdue/Concord Matrix: Solid
Date Sampled:06/10/2021 1430 % Solids: 5.70 06/12/2021 2001
Date Received:06/11/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601OD 1 06/17/2021 0655 JMH 06/16/2021 1038 95491
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
601OD
19000
110
mg/kg
1
Arsenic
7440-38-2
601OD
ND
4.0
mg/kg
1
Cadmium
7440-43-9
601OD
ND
1.3
mg/kg
1
Calcium
7440-70-2
601OD
2200
1300
mg/kg
1
Copper
7440-50-8
601OD
7.3
2.7
mg/kg
1
Lead
7439-92-1
601OD
ND
2.7
mg/kg
1
Magnesium
7439-95-4
601OD
ND
1300
mg/kg
1
Molybdenum
7439-98-7
601OD
ND
11
mg/kg
1
Nickel
7440-02-0
601OD
ND
11
mg/kg
1
Potassium
7440-09-7
601OD
6300
1300
mg/kg
1
Selenium
7782-49-2
601OD
ND
5.3
mg/kg
1
Sodium
7440-23-5
601OD
7800
1300
mg/kg
1
Zinc
7440-66-6
601OD
83
13
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 6 of 12

Client:Terra Renewal Services, Inc. Laboratory ID: WF1 1024-002
Description: Advanced Foods/Claremont Matrix: Solid
Date Sampled:06/10/2021 1530 % Solids: 3.71 06/12/2021 2001
)ate Received: 06/11/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
06/17/2021 2357 MOM
95937
1 350.1
(Ammonia - N) 350.1
2
06/16/2021 1458 KFE
95636
1
(Nitrate-Nitr) 353.2
1
06/16/2021 2112 AAB
95887
2
(Phosphorus) 365.1
10
06/17/2021 1816 DMA
06/11/2021 1709 95282
1
(Soil pH meas) 9045D
1
06/13/2021 1953 NBW
95369
1 351.4
(TKN) 351.2
1
06/14/2021 1233 DMA
06/11/2021 1800 95288
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
89
%
1
Ammonia - N (gas diffusion)
350.1
1500
540
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
36
5.4
mg/kg
1
Phosphorus
7723-14-0 365.1
7400 S
1300
mg/kg
2
Soil pH measured in water @ 21.4 ° C
9045D
5.5
su
1
TKN
351.2
7700
1300
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A 5 06/24/20211535 JPB
06/18/2021 1511
96014
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
2300
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
2300
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
2300
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
2300
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
2300
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
2300
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
2300
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
47 41-132
Tetrachloro-m-xylene
54 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 06/16/2021 1741 CMS2 06/15/2021 1638 95526
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471B ND 2.0
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 12

Client:Terra Renewal Services, Inc. Laboratory ID: WF1 1024-002
Description: Advanced Foods/Claremont Matrix: Solid
Date Sampled:06/10/2021 1530 % Solids: 3.71 06/12/2021 2001
Date Received:06/11/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601OD 1 06/17/2021 0659 JMH 06/16/2021 1038 95491
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
601OD
14000
180
mg/kg
1
Arsenic
7440-38-2
601OD
ND
6.7
mg/kg
1
Cadmium
7440-43-9
601OD
ND
2.2
mg/kg
1
Calcium
7440-70-2
601OD
4400
2200
mg/kg
1
Copper
7440-50-8
601OD
640
4.5
mg/kg
1
Lead
7439-92-1
601OD
6.2
4.5
mg/kg
1
Magnesium
7439-95-4
601OD
ND
2200
mg/kg
1
Molybdenum
7439-98-7
601OD
ND
18
mg/kg
1
Nickel
7440-02-0
601OD
34
18
mg/kg
1
Potassium
7440-09-7
601OD
2200
2200
mg/kg
1
Selenium
7782-49-2
601OD
ND
8.9
mg/kg
1
Sodium
7440-23-5
601OD
13000
2200
mg/kg
1
Zinc
7440-66-6
601OD
280
22
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 12

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 12

PACE ANALYTICAL SERVICES, LLC
North Carolina Permit
2. 11CS1 .ukb sLI11 l r, :'arl!Ay nd to. df—'U1CYaa.g� Wtt Natty+ we�raur 'vn J? atYGwra
aid Recaz"r ry a* rd.l:R h' a ' E
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TERRA REHILEV"i�,kLL SERVICES
t'tw.rVJ!rnr,R taiC o,,.,�°urce;:.. Date;
\eM-Fiuia t,Cl Sneq� et atit, ';+'P, ..kl Ft a si at 1
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 12

PACE ANALYTICAL SERVICES, LLC
Samples Receipt:�L'taeckllst(S j(MEUGIK-15) Re"d. d:9j'i!9 zIJ20
d� . ra ^ � Issulwg /Wthorlty_ PAc,p IFNV - WCOla �ad,ga 1 OF S
Sample Recc.ipt 'hc-eklist (' RQ
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Hearts,o*..'recNpt'. Paco C'.1iel~t Ll UPS M OedEx Ot'I'aen
l_ Were ct,stcmdy seals ruin can l]dj;� wok?
es NO
a" NA
?, 1Fuu8(cJ' wizv scat, wcrc they intact and unbroken?
f)H 5trij) Illi.l; NA t: kllrurin ;'trip I.I.. ; .N�A__. Tested >~+y; I"",
ri], ina,l trrm,p—m trmm a pryer rr,cclpt i Dcrivcd (Corrected,) teniperaru_e u1mm ieze]iA %3 v)idSnap-Cup ILA, 21 239
......... .......
1.8 ii 4.9 - NA d HA ,C NA e NA r� NA f NA `DC
Meth ❑ od: Teia uax, f� pena-, mm.._. _._..
yt,teaalk [Dkgairnsi l3(iltU+_,-5 II+k dawra li:}t � _.._.a i!� Gwra G,�1•I�+ectiora �l�act�oa,.; tl
Methodl o`` coolant. WJ wet ice ice pac,� � , , icu r done
3 llf"P�n1Y Craiwf�.u�aLary �r.d�slcr`�.^c�;� cxl it l5_IF �rw�a:s TM-jrct Managev NDtitiec."?
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7. Were 41 alp Ilex Ir.lus] c.u. arll �:arnplc ccantaina�°s?
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Il.Sllr � ].) sw�rra I
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arnisle ) r.vp _ kvcr-. ruc;oNcd irlum"ectly rmevv,md and were alucoeciingly
in s.arraple receivi7jv with NA .__MLO('air�"lie ow;; K4S,04,1AN03, ]1(1: NaOM t.5fgg SR d, NA
r r11) ofpreserya:ior_ NA Trrraclrc th,aan one preservative, is cdcd, please nue iita dig ,%nrnrnt,rits Ibeloww'_
r'arrr ,ir( �' _. w c x rec iiured v.-ith ba6blt�s 6 mr°ra in .lierrseter.
&lrrlpins(s wry .....-._._ _ .. + yru amrclvc d with °] lkC > tl.°s inpli, (rrH19 is no) aild wi�rc;;
agjustad acz ardlrn ly in salmp9e Fmcivijig witli sodium tlkiasullfull . (Na2:,0,) with SI'tl"at,l}'' ID: h(A
T t rcciclr:la9lbeIs9ppliedby .RGZ t�CplVM,21
CC}il'rmeri
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 12

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Tyson Wilkesboro
Lot Number:WH27011
Date Completed:09/10/2021
09/10/2021 2:52 PM
Approved and released by:
Project Manager II: Lucas Odom
,�i
A4W
AMP VOWN Acr K er AI $1114ld
i
FA[ (' R F D 1 F IE D
o1SriuraA3,01PAI�3Y
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WH27011
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the low percent solids, the following sample had an initial weight that is 3x greater than standard
procedure: WH27011-001. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 10

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WH27011
Sample Number Sample ID Matrix Date Sampled Date Received
001 Tyson Wilkesboro Solid 08/26/2021 1400 08/27/2021
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 10

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WH27011
Sample Sample ID
Matrix
Parameter Method
Result Q
Units
Page
001
Tyson Wilkesboro
Solid
% Volatile Solids SM 2540G-
98
%
5
001
Tyson Wilkesboro
Solid
Ammonia - N (gas 350.1
940 S
mg/kg
5
001
Tyson Wilkesboro
Solid
Nitrate -Nitrite - N (soluble) 353.2
36
mg/kg
5
001
Tyson Wilkesboro
Solid
Phosphorus 365.1
3600
mg/kg
5
001
Tyson Wilkesboro
Solid
TKN 351.2
57000
mg/kg
5
001
Tyson Wilkesboro
Solid
Copper 601OD
5.3
mg/kg
6
001
Tyson Wilkesboro
Solid
Zinc 601OD
62
mg/kg
6
(7 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 4 of 10

Client:Terra Renewal Services, Inc. Laboratory I D: WH2701 1 -001
Description: Tyson Wilkesboro Matrix: Solid
Date Sampled:08/26/2021 1400 % Solids: 5.78 09/01/2021 0138
Date Received:08/27/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
08/31/2021 2357 MOM
14024
1 350.1
(Ammonia - N) 350.1
2
08/31/2021 2212 DRD
13796
1
(Nitrate-Nitr) 353.2
1
09/01/2021 2039 AAB
14288
1
(Phosphorus) 365.1
5
08/31/2021 1536 DMA
08/27/2021 2030 13643
1
(Soil pH meas) 9045D
1
08/29/2021 1934 NBW
13723
1 351.4
(TKN) 351.2
5
09/07/2021 1756 DMA
09/02/2021 1634 14260
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
98
%
1
Ammonia - N (gas diffusion)
350.1
940 S
350
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
36
3.5
mg/kg
1
Phosphorus
7723-14-0 365.1
3600
430
mg/kg
1
Soil pH measured in water @ 20.9 ° C
9045D
4.1
su
1
TKN
351.2
57000
4300
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A 1 09/02/2021 2027 DALI
08/30/2021 1706 13817
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
290
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
290
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
290
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
290
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
290
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
290
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
290
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
83 41-132
Tetrachloro-m-xylene
86 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 09/02/2021 1658 CMS2 09/01/2021 1527 14067
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471B ND 1.3
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 10

Client:Terra Renewal Services, Inc. Laboratory I D: WH2701 1 -001
Description: Tyson Wilkesboro Matrix: Solid
Date Sampled:08/26/2021 1400 % Solids: 5.78 09/01/2021 0138
Date Received:08/27/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601OD 1 09/02/20211609 JMH 09/01/2021 0137 13906
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
601OD
ND
110
mg/kg
1
Arsenic
7440-38-2
601OD
ND
4.1
mg/kg
1
Cadmium
7440-43-9
601OD
ND
1.4
mg/kg
1
Calcium
7440-70-2
601OD
ND
1400
mg/kg
1
Copper
7440-50-8
601OD
5.3
2.8
mg/kg
1
Lead
7439-92-1
601OD
ND
2.8
mg/kg
1
Magnesium
7439-95-4
601OD
ND
1400
mg/kg
1
Molybdenum
7439-98-7
601OD
ND
11
mg/kg
1
Nickel
7440-02-0
601OD
ND
11
mg/kg
1
Potassium
7440-09-7
601OD
ND
1400
mg/kg
1
Selenium
7782-49-2
601OD
ND
5.5
mg/kg
1
Sodium
7440-23-5
601OD
ND
1400
mg/kg
1
Zinc
7440-66-6
601OD
62
14
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 6 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 10

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 10

PACE ANALYTICAL SERVICES, LLC
North Carolina P,ennii�t Parameters
2, Rcsidllil[Y, sb,911 k!nillyml tL) t.jC.TM3l'15[rM- Ih
; crj
arid RaLov�.,zy .W- (RCRA� The 0-014-MWO
i Abs. vroi&d i[2
A(wo7ii.-iwat A, aua [duo Fmzjdu� lralR tulairul aex the miulb fur 0 Mlilnuln of fin ycur& Aiky
emcc-ptior s fmm t1w rcquirenn-mr, in this.,conditior 60 be spenib ed to AaaOwnea A�
T1:83-4'LYS1S 311JI illOjIlde Lik'-
is in parentl1cm):
I An qjwly�,ir* Ow4l, L& oouducwd rv. msWi4ob ftuxt pa kow-4Sezera6i% faoJity at the: fkequewcv
arxdfjod it Ar�aeuuant A, and tha 1'emiltee shall maimtairi thE5 resuits for a minimum L%f fhv yeErs.
Tac aa@1yS4 W" igicLa 11m, fokwiag poromt�tem
A It I mini I iE,
M& raury
'POWAId . LUI
Ampnuuia-Nitrop
Molybdunutu
Suk;TdUM
Amu=
S luni
TKN
Cadmium
CQ�AJWII
lqftrno-Nkrite Nitropm
Fel Tce:a Rita. SOU
L=f
PH
Phov.phoms
ziu.
vc1atile Solids
FhO B.'s
TERRA RENEWAL SERVICES
479-747-8192
Afinh ment W, COC for,- -Souroes; Dialer
1VQQOX936J 'kfusiou 1.0 SbnJ Verq�nj 140210 PApa 9 id L)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
{:hunt: 'I unit ldclwwai
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, ,,. rNo
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eq
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17. Wen: ell L11ROinietals, Iv i dent w.•rnt nee reCe:CvmCj rlt as aH of-, ??
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18. Were all ennl k q.trit-,leA m&e%-vcd at a pH r> 12 and suh.-L& sm_u:jlrs rCcciVCd oit ar PH .• 4Y?
No
19. Were edt ajtplicailrle�ll-0.�T�Tof`ay,lnirltrll,lvrn��l+(i�.�,] tU�.3 (�;G.51v "L,lsamples; ree:ofF
re.'rduatl chlorine?
ycs"1 No
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70, Were client m mulaiic.Vrr;:quicsls (1 c,rcc'uc'sted dilut.irms, 'oASi �fS[) dcsivalions„ c'it -)
ct��an=- ;.lw inaz5unk.") a -am the LC.L.nto die c{ar'Itment seclioil mla Ld?o1 ?
�CS No
1, Was the q uctc nuirlacr Fsmd on 11t-� Qon(aiRer label'? 1f veg, Quote 0
Sample Prrrwinr ltion (Must mu t r,mpl�tet� tier am,�' i WtvtrfOlia(�) iff�r�wert"t�° pnr sd rv�rl ar veitl, Inea»rls vxa e.�
-SaMpl) NA wvcrc I ti i Ld i�r ;;ow tl+' pinrs:.7 " it ainri u"rr� it ]LrS v Ci irrdCb[' lta�l
in sanvple reeeiv- ntylth H^ rw,l. orcd= to ui:w: H2SO4, H"NO3, Hal, ',laCilI min; SR # N
11--m ofpreservatioit N"" - elf iturC Ji uuunr. presurvativc isnceded, p1aasa note in j1e� cotrtrnenlw bk^1f1w.
��_,•
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., _ c F J
a�I.jtlrttead ae�°:�valclirvc.➢}� in srirrtp_e nrti�„;,LWrtlg with sraciimrLn "tlai�aau.lfllc ('����� �'v will] w weal; "' Ili; tk.A __........• "
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m.•,ry
1t In ,r odc Labels app-ued by,, rt .tt�'4�' haute,, tSx.�7,
Cvorlments:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 10

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Mathis Storage
Lot Number:WH27009
Date Completed:09/20/2021
09/21/2021 7:21 AM
Approved and released by:
Project Manager II: Lucas Odom
,�i
A4W
AMP VOWN Acr K er AI $1114ld
i
FA[ (' R F D 1 F IE D
o1SriuraA3,01PAI�3Y
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WH27009
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the low percent solids, the following sample had an initial weight that is 3x greater than standard
procedure: WH27009-001. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 12

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WH27009
Sample Number Sample ID Matrix Date Sampled Date Received
001 Mathis Storage Solid 08/26/2021 1400 08/27/2021
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WH27009
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Mathis Storage
Solid
% Volatile Solids
SM 2540G-
44
%
5
001
Mathis Storage
Solid
Ammonia - N (gas
350.1
170000
mg/kg
5
001
Mathis Storage
Solid
Flashpoint (Pensky-
1010B
>140
° F
5
001
Mathis Storage
Solid
Nitrate -Nitrite - N (soluble)
353.2
430 S
mg/kg
5
001
Mathis Storage
Solid
Paint Filter Test
9095B
Fail
pass/fail
5
001
Mathis Storage
Solid
Phosphorus
365.1
28000
mg/kg
5
001
Mathis Storage
Solid
TKN
351.2
220000
mg/kg
5
001
Mathis Storage
Solid
3+4-Methylphenol
8270E
1.9
mg/L
6
001
Mathis Storage
Solid
Calcium
601OD
72000
mg/kg
8
001
Mathis Storage
Solid
Potassium
601OD
43000
mg/kg
8
001
Mathis Storage
Solid
Sodium
601 OD
27000
mg/kg
8
(11 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WH27009-001
Description: Mathis Storage Matrix: Solid
Date Sampled:08/26/2021 1400 % Solids: 0.416 09/01/2021 2332
Date Received: 08/27/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
08/31/2021 2357 MOM
14024
3 350.1
(Ammonia - N) 350.1
20
09/17/2021 1444 MSG
15693
1
(Flashpoint Q 1010B
1
08/30/2021 1016 KMC
13812
1
(Nitrate-Nitr) 353.2
1
09/01/2021 2035 AAB
14288
1
(Paint Filter) 9095B
1
08/30/2021 1217 KMC
1
(Phosphorus) 365.1
5
08/31/2021 1536 DMA
08/27/2021 2030 13643
1
(Reactive Cya) 7.3.3
1
08/31/2021 2053 AAB
08/31/2021 1649
1
(Reactive Sul) 7.3.4
1
09/01/2021 0012 DMA
08/31/2021 1649
1
(Soil pH meas) 9045D
1
08/29/2021 1933 NBW
13723
1 351.4
(TKN) 351.2
1
08/30/2021 1325 DMA
08/27/2021 1854 13592
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
44
%
1
Ammonia - N (gas diffusion)
350.1
170000
48000
mg/kg
3
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
° F
1
Nitrate -Nitrite - N (soluble)
353.2
430 S
48
mg/kg
1
Paint Filter Test
9095B
Fail
pass/fail
1
Phosphorus
7723-14-0 365.1
28000
6000
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 20.7 ° C
9045D
5.0
su
1
TKN
351.2
220000
12000
mg/kg
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 09/10/20210308 JDF
14928 09/07/2021 1804
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1, 1 -Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WH27009-001
Description: Mathis Storage Matrix: Solid
Date Sampled:08/26/2021 1400 % Solids: 0.416 09/01/2021 2332
Date Received:08/27/2021
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
95 70-130
1,2-Dichloroethane-d4
98 70-130
Toluene-d8
98 70-130
TCLP Semivolatiles
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E 1 09/10/20211910 SCD 09/08/20211830
14793 09/02/2021 0041
2 1311/3520C
8270E 5 09/11/20210015 SCD 09/08/20211830
14793 09/02/2021 0041
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7 8270E
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2 8270E
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1 8270E
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3 8270E
ND
0.040
mg/L
1
Hexachloroethane
67-72-1 8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270E
1.9
0.20
mg/L
2
Nitrobenzene
98-95-3 8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270E
ND
0.20
mg/L
1
Pyridine
110-86-1 8270E
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
0.040
mg/L
1
Run 1 Acceptance Run 2
Acceptance
Surrogate
Q % Recovery Limits Q % Recovery Limits
2-Fluorobiphenyl
71 37-129 73
37-129
2-Fluorophenol
52 24-127 50
24-127
Nitrobenzene-d5
78 38-127 83
38-127
Phenol-d5
78 28-128 92
28-128
Terphenyl-d14
95 10-148 74
10-148
2,4,6-Tribromophenol
85 41-144 66
41-144
TCLP Herbicides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/8151A 8151A 1 09/14/20211045 CMF 09/08/2021 1819 14790 09/02/2021 0041
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
2,4-D 94-75-7 8151A ND 0.020 mg/L 1
2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 mg/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
DCAA 81 50-112
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WH27009-001
Description: Mathis Storage Matrix: Solid
Date Sampled:08/26/2021 1400 % Solids: 0.416 09/01/2021 2332
Date Received:08/27/2021
PCBs by GC
Run Prep Method
Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C
366013/3665A 8082A
1 09/02/2021 2014 DALI
08/30/2021 1706 13817
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
4000
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
4000
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
4000
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
4000
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
4000
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
4000
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
4000
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
82 41-132
Tetrachloro-m-xylene
82 35-106
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 09/13/20211732 DALI
09/08/2021 163014770 09/02/2021 0041
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9
8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9
8081B
ND
0.0040
mg/L
1
Endrin
72-20-8
8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8
8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3
8081 B
ND
0.00040
mg/L
1
Methoxychlor
72-43-5
8081B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2
8081 B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
79 20-131
Tetrachloro-m-xylene
85 26-132
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 09/02/2021 1655 CMS2 09/01/2021 1527 14067
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471B ND 18 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WH27009-001
Description: Mathis Storage Matrix: Solid
Date Sampled:08/26/2021 1400 % Solids: 0.416 09/01/2021 2332
Date Received:08/27/2021
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
601OD
1 09/03/20211131 JMH
09/03/2021 0121 14330 09/02/2021 0041
1 1311/7470A
7470A
1 09/03/2021 1835 CMS2
09/03/2021 1427 14392 09/02/2021 0041
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 601OD
ND
0.15
mg/L
1
Barium
7440-39-3 601OD
ND
0.25
mg/L
1
Cadmium
7440-43-9 601OD
ND
0.050
mg/L
1
Chromium
7440-47-3 601OD
ND
0.10
mg/L
1
Lead
7439-92-1 601OD
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 601OD
ND
0.20
mg/L
1
Silver
7440-22-4 601OD
ND
0.10
mg/L
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 09/02/20211601 JMH
09/01/2021 0137 13906
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 601OD
ND
1600
mg/kg
1
Arsenic
7440-38-2 601OD
ND
58
mg/kg
1
Cadmium
7440-43-9 601OD
ND
19
mg/kg
1
Calcium
7440-70-2 601OD
72000
19000
mg/kg
1
Copper
7440-50-8 601OD
ND
39
mg/kg
1
Lead
7439-92-1 601OD
ND
39
mg/kg
1
Magnesium
7439-95-4 601OD
ND
19000
mg/kg
1
Molybdenum
7439-98-7 601OD
ND
160
mg/kg
1
Nickel
7440-02-0 601OD
ND
160
mg/kg
1
Potassium
7440-09-7 601OD
43000
19000
mg/kg
1
Selenium
7782-49-2 601OD
ND
78
mg/kg
1
Sodium
7440-23-5 601OD
27000
19000
mg/kg
1
Zinc
7440-66-6 601OD
ND
190
mg/kg
1
Footnote(s): *Paint Filter: 100mL collected;
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 12

PACE ANALYTICAL SERVICES, LLC
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 12

PACE ANALYTICAL SERVICES, LLC
North Caroline Permit Parameters
2, Rogiftils 9h,911 he wtqlynd '14) demosntvate they we z umc COMMaliun
wil "Rt��-ovaty MT FRCF.N-), Um ai�ajyw�. (Vorrosivity, JigniWttilbilii ., rpact;W arid tawlelty
"lot tv�" �C"X1jwa(jyy ziptawd ilk ch.aractiBristle [andiffig, proCEdnre TCLP' �;Ilnot �L
AU,act-meiit: A, aad 'le ParimiUm skull ingiarku those results far a mitximir, of live yewi;- Any
excqtlons froni tbe mcU.Arunw-nts in tbi�.- 4,,xindil-im ShFi I I h= 4r3VL:i rail inAI.I'3LJ,m11nMLi A.
`I'LeTCr P analvs: s shall -iichide the followin,g paramttcn (the itpila-AD* bne'4 in mil ligams per liter
is in.pwcuthcscs):
.PL-senic (5k)
----------------------------
1,4-DiQh1orubvLi=w (7�5)
---- --- -
'Nir vobo=ae, ( 2,0),
B'ariwyl (I IDO 0)
(0.5)
Pentachlorciplictiol (10M)
1,1-Dichloroethylone ((1.7)
(5"0)
cadMIUM (1.0)
�'4,Diubxmdumln'(0-13)
. ...... ... ... ..............
ca.-Ibm tet-rublorwe Y
Endi"'n (0.02)
sil-ver (5,0)
Chlordaii-o (0.03)
lUxachlorobanimoe (0-13)
Tetinchkwine-ITylene
0o,O)
-
He�tachlix (aud its hydroxidz)
Toxapherit (0-5)
Clues uforzi (6.0)
-------------------------------
-------
(400.0)
rA-Crew'.1
I-nd (5.0)
2A64"Eickloruptimul (2,0)
O"Cresol (200,0)
LindFlno (9.4)
(Silvex) (I k)
Vinyl ulil—oxide (0-2)
P-er'-sol
IVInn-iii-y (0.2)
crescd (200.0)
(10.011
MAY ad FYI
3. An dnalysi3 abull be u.uidwwdl ou jv;5UjAs Lota etch 3mircc generating boility of 'I-te freqliellcy
np,,-,Jfind in Anackmemt A, aid tha Perrnit-ce snall mafi:ta�-L the results !"Orb MirdIEL47A ('j' f2we years.
Thr, ma1vsis Aliall iu!ulua LLu fullowbig paewiv4ita s:
.omTrmi H-Ki rragcn
u, J ii ni
MOM Sodium
(6,
A.Tscnic
Cadmilm
Nkrte-N'-Ete Mjhocn
LLI
z
falelPaPercatzt
Total SfAlift
TKN
copvcr
-?, H
Zi n
P'1-L4)qp1hQ1-aS
Volade SoCds
W,
Lid
zl
a tlCauutil
PCITS
Z
w00036936 veysioa 1,10
TERRA RENEWAL SERVICE�$
479-747,81 a2
';"l yersim 1402" --•7
P%L)'n' 8 of 12
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 12

PACE ANALYTICAL SERVICES, LLC
Samp les Recttl nt Checklist �SIRCI I ME001SC-151Revised; a/29'; uzu
P4kwAii,*,,jr;?^7i IssuingAuthority: Pace ENV— Vi 1+zg,e 1 0` 1
Ample Receipt Checklist (S,R
Client- I°, n,, V41) wait C oi hisveatied hVdale_ .a I r QPZ?QQI Lot it; INH2 009
Wailstt'1'rt°alful'` aGe J" lJpa ....... F 'Ex l lhtr:
..,.
i. %11111 015tudy seals pmentolithe cooler?
L1yi;;s1 FjNolNA
1.1, Ircwtota sixls W" )rrswnt were 11twy intwL iurid ?tr.ltn*f,.n?
pH Stripy ID:
C'hloramac'S'eripr IL), tag Tasreid day: NA
li�lntal LeAtrPULLIUM U-,IQ&3 I L1 JQ La'e<dvi i (Ccarreacd) ternperatut+e upon race ip it ^"nY�dtlid �rn2pb a'•lllk lit: � I"Y`I�
�"lelhn,rl; icnt e�tln�we Cilard. O'1��„�Itt,�f B
p .,. _ olydo lK G un D-. 1R C;un �l" oc meti(m Ric � '1;.
.._..
�atltor ua-Cralxalr�r:h � u'' tlae Ice�'P'a k.tiDry Ica NO-ne
EJ Y e"s ©'N+lY ;_", JNA � 11'ik°I�'SjI:'�t'.�y"�
M wa5 Notified 1]y. phone i efrmii d facr-Un.Fwm (r'imic o ng.).
r`vr,
O
N,rr
T. , x fOtelcJ�lcottrier"s 3211 LFLn Sli )!Atui:'h,u i to lh 3 fbnO _
wr=, Yas..
No
5. Were proper uwil>;;wiy parctr;-i (rdingauishudi`rweived) foillowo�?
1
Ur1'
,fa. Were s,e narlx M
Y:,
� K�
7- Were !La'Irl i " I�l� s kir'I nn j4[1 sgmp �+�°w r�J�r+� j
9.� col Iei', op, Jaw & firilu Iisn; l on�tH'�L�
®`
No
9. was Collection dale.. fihulite li5trd on all sample: coataiuer:;?
1 h
10. Llit[ all coa:talrJej- IaYtdn] Inlwrrultion did , gate, dirt.e) ant Wilh rite CDC?
,!v�' yes
C~10
11, Were tests to the oerEwr'rriv(] lrslrxl rrwtr tllr C7
12,. Dd all xatmplr% nirrivc ill tifao pa-Opex coittaliners fUT eUca test mr-WoT in good conudutian
(i.uttin-Dkon, lids on, etc.)'
y7ys
r
13. R'10111111e aVgi bj1 —?
Zv5
L Na�
14. ��'rrcrC� rL11 sarrPles r eiv&lwithin o 48 kv:YIi.i:vvt'r unpi u., FiTs't?
iEl,
rhour."a+
Br� exl�l-�LIrl:1�:e
15_ Were any 3amp lee Containers_ rrlple-s Not listed an C017I?
®'t''es
❑ NJ
r�1
16. For'��4' A ;jud 1�t,*1,K - I i s;implics„ were b4 bbess pr��I'rllt>L1�G"a_SJXAJ l 15trijlt in diar-lwFber)
in any ofthe VOA vials?
Vies
Na
� CIA
17-... ern. till. ..._._
L1l;rfi�o°art+atais�trrt'ttr�ierrtsaxar �,
� --. ..,�.Yle.� rorr'�r��� rrl la �ffi �p�l'�e, '""�
.Llr tsi
No
� i'MA
8, ii all cy3_nlde salllp�.c� uticz- +.vd YA it p1 -, '1 ': and suIt•ide lain ley p�l
—1 No
yIA
19_ Were all np7llcalble. N1I. "]'K WeyaLoldelphumo Li I iL. , ,3' < 10.5 Ill@j'`L) NurrijF1u,, fruv Yrl'
El e;�,
r�'
'�, `�r'ceq re client remarksIruests (ix. riicqu O ct.lttttioni, hfS: MSD Jusugntltions, zixi—)
co-rcatly llianscri d I-ro m 1'h� COC 111to this Graulunelit s&CLi{rir ill ],IMS?
es
'Nc-
21 Was title' god nunibar listed art the contahier lahol? IFy cs;, till<3tr.41
I tMttapalc "t°,w scrwaRi r�; l:tW�ust I4v L0°rtr,10,e:i nor sMlttp c s -act] irs a°'e1' ci` vt' Ill hcwe.l palls e.
,15ai
in tvnl and were Irlju.-Ao ls_ucur:I[ngly
in salml)le-'eeit�iYr�
a+ OL m rr1L caf'aira:c nt1a; l]? ;Cy , lYllrrR it IICI, hlaS]�ly ttsarr,&S� ltdN
KA IfFna'etl:ahy rine preqervilivr is Prii 1;39c se.. n-2te in Ow iz?gna'm;ta# w, uvvi
]'ilne elf"isle, k attar ri .... ....
Sarni
...,,...
were received with ltu bbles ;�(, min in dijanle_er-
sMC r �w�+LS} MA.
were received) with TRC - 0.5 rnig L (I fA9 isno } arid t'ii
aailttsLLA'amnAiilgly to si rccwty°irt&wil!:7 SOdWnl tlliosWIl'latu` k7 tl, aMCI`a Wi'SItmly ID,
;SR 'haivodltlabrbapagrlicid by:..'1I6I7` D" Jlc- (JSP712O I
Ciommcnts:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 12

aceAnalytical 0
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:W103004
Date Completed:09/27/2021
09/27/2021 1:27 PM
Approved and released by:
Project Manager II: Lucas Odom
lA C. C R F 0 1 G E D
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: W103004
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following reported analyses are currently not listed on
our TNI scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 601 OD, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the low percent solids, the initial weight of the following samples is 3x greater than standard
procedure: W103004-001, W103004-002. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 12

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: W103004
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
Tyson/Harmony
Solid
09/02/2021 1330
09/03/2021
002
Solid
09/02/2021 1430
09/03/2021
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: W103004
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Tyson/Harmony
Solid
% Volatile Solids
SM 2540G-
91
%
5
001
Tyson/Harmony
Solid
Ammonia - N (gas
350.1
9600
mg/kg
5
001
Tyson/Harmony
Solid
Nitrate -Nitrite - N (soluble)
353.2
25
mg/kg
5
001
Tyson/Harmony
Solid
Phosphorus
365.1
9100
mg/kg
5
001
Tyson/Harmony
Solid
TKN
351.2
60000
mg/kg
5
001
Tyson/Harmony
Solid
Aluminum
601OD
4800
mg/kg
6
001
Tyson/Harmony
Solid
Calcium
601OD
11000
mg/kg
6
001
Tyson/Harmony
Solid
Copper
601OD
4.5
mg/kg
6
001
Tyson/Harmony
Solid
Potassium
601OD
1900
mg/kg
6
001
Tyson/Harmony
Solid
Sodium
601OD
2000
mg/kg
6
001
Tyson/Harmony
Solid
Zinc
601OD
27
mg/kg
6
002
1
1
1
1
1
1
1
1
1
(21 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 4 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:W103004-001
Description: Tyson/Harmony Matrix: Solid
Date Sampled:09/02/2021 1330 % Solids: 6.36 09/09/2021 0031
Date Received:09/03/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
09/09/2021 2341 MOM
14922
3 350.1
(Ammonia - N) 350.1
15
09/25/2021 1603 DRD
16480
1
(Nitrate-Nitr) 353.2
1
09/11/2021 0913 AAB
15082
1
(Phosphorus) 365.1
25
09/07/2021 1601 DMA
09/03/2021 1806 14449
1
(Soil pH meas) 9045D
1
09/05/2021 1409 NBW
14531
1 351.4
(TKN) 351.2
5
09/17/2021 1150 DMA
09/16/2021 1346 15511
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
91
%
1
Ammonia - N (gas diffusion)
350.1
9600
2400
mg/kg
3
Nitrate -Nitrite - N (soluble)
353.2
25
3.1
mg/kg
1
Phosphorus
7723-14-0 365.1
9100
2000
mg/kg
1
Soil pH measured in water @ 18.7 ° C
9045D
5.7
su
1
TKN
351.2
60000
3900
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A 1 09/10/20211344 NCM
09/05/2021 1745 14536
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
260
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
260
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
260
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
260
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
260
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
260
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
260
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
94 41-132
Tetrachloro-m-xylene
90 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 09/10/2021 1430 CMS2 09/09/2021 1342 14850
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471B ND 1.2
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:W103004-001
Description: Tyson/Harmony Matrix: Solid
Date Sampled:09/02/2021 1330 % Solids: 6.36 09/09/2021 0031
Date Received:09/03/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601OD 1 09/08/20210821 JMH 09/08/2021 0041 14562
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
601OD
4800
99
mg/kg
1
Arsenic
7440-38-2
601OD
ND
3.7
mg/kg
1
Cadmium
7440-43-9
601OD
ND
1.2
mg/kg
1
Calcium
7440-70-2
601OD
11000
1200
mg/kg
1
Copper
7440-50-8
601OD
4.5
2.5
mg/kg
1
Lead
7439-92-1
601OD
ND
2.5
mg/kg
1
Magnesium
7439-95-4
601OD
ND
1200
mg/kg
1
Molybdenum
7439-98-7
601OD
ND
9.9
mg/kg
1
Nickel
7440-02-0
601OD
ND
9.9
mg/kg
1
Potassium
7440-09-7
601OD
1900
1200
mg/kg
1
Selenium
7782-49-2
601OD
ND
5.0
mg/kg
1
Sodium
7440-23-5
601OD
2000
1200
mg/kg
1
Zinc
7440-66-6
601OD
27
12
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 6 of 12

Desctription
mat ix
Date Received'®
...............
[--�_ ----- —..d
i P00 = Ltmot of Qcaabitatiork B z Detected m the nwftocl bWM E 7 Quarifilabm of comitwund exceeded ft caMalmn Tafige 0 =sureigate f"MIure
NO 7 Not detected at or above the LQQ N = Recovety is out of critena P = The RP0 between We CC cullumns exceed,, 40% L LCSICSD (aflure
H = Out of holding lime W = Repoded on,wel weight bass 5 MSIMSD fadwe
Pare An allyticall S itices, L L C (ftrmefiy Shea Cy Enveroamenrai Sermes, lew)
'106 Vantage Paint Drive West Columbia, SC 29172 (803)791-19700 FaX(803)79'j-9II1 wwwpacelabs.nor
mm�

M
M
mglkg
LIDO -' Uvid of QuanfRafloo B 7 Detected us the rnethod blmik E z Quanllaboln of compound exfA*eded Me caftWaftm range Q = Suprogate TaMure
NO = NO detected at or above the LQQ N = Recovery is out of criteria P = The RPO l)etween two CC collunins exceeds 40% L = LCSALCSD faMure
H = Out of hoMing tirne W = Repofted on,wel weight Emsis S = MSIMSD failure
Pace Analytical Services, LLC (formerly Sheafy Enwonmenifal Serwoe's, Inc)
106 Vantage Point Drive West Columbia:, SC 2,9172 (803) 791-917011, Pax (803),791-9111 wwwpacelabs-cionn
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 12

PPACE ANALYTICAL SERVICES, LLC
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Pace Anaitytjcae Services, LLC (formerly Shealy Emdruntmenhad Services, Mc.)
1!06 Vantage Poinit DOve West Columbia, SC 2,9172 (803) 7,91-9700 Fax (803) I(911-91 11 www.pacelalbs.com
Page 10 of 12

p" FACE AN�AL,YT'ICAL SERVICES, LLC
No'rth Ccur` lino Permit Parameters
2, Rosiduals u4l be P�rx[YANI 10 dimmuisu:arc li=y Art oJWA4° CutisftVauo"
ar.,d Romvery Act �,RGKA), The
in
Att4obtuent A, And t6c Pc7,T6Isw. .wupup_lj -uuuuwertaitt tlww jmpj1t5 for I ;vin4rnum of fiw yzam Any
exceptious fivau tht roqu'M in this,coudl'd= shal Im L ,V,.Jtadiux*t A
Theilmwoty'sis, Shan indole Ac fujhwwir.g pajal:Loters (the rtgatgot-y Jew! in miffigrams, porch titer
ih urea, pau'fltlu'=)�
7" Au aval'YUES 641H Ir'' onoduv4d on tc!sidk,,ob from t9id ow -cc twormiug fwdlit-Y At the fmquency
spccificd in oV.,w,tut out A, od Cv Nrraittoo 4,01 traintain rbc reaArs J.'cr u minimw w0 of fve yearl.
11 w, ualysLs ibll inchode, the fol'ImiaZ paramc-ters:
Alumlouo
Aino,oma-Mijogmi
Chdrairunt
Mercurf
*Ayhtim win
NA:Ikell
Nitutr4,' ,Iiknw Mlrogprt
potwdi Ana
Sc�rrh in
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PuTmat ToW 80116' TKN
cuppajPIT
tkad 1105hfwnlx volable 5011168
pCB'S
TERRA RENEWAL SERVICES
479-747­8192
Attachment to COC for.-, AOU DOW
W(XX*6936 Venijusi LO
"~ilea Vcrtomi 1410"YA:
Po W & of 12
Pace Analtyticad Services, LLC (former�A Shealy Emronmenfai Services, h7c.)
106 Vantage Point DOve West Columbia, SC 2,9172 [phone] Fax [phone] www.pacefaibs.com
mz�

PACE, ANALYTICAL SERVICES, LLC
r? saviaphis Remllpt Checklist (SRC) JMFOOISC-15) Rev istc -.1/29/2 020:
N%,jing Aufl,or[,Vn Par.p FUV - WCUL Pug, I r,,( t
Sample Receipt Checklist (SRC)
(Aiew Tun, Rem"Vot L*y dl,,,mv KSC ! (WOYMD L&A,
I CILr Z 1""PUFedl," OfficrLo l"Hmndy Walm�Iut Uo die clopirO
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7 y 7es No, I EN Al P M was 14 t sd I) ad, otioa e Onla 11 � f'aoc-tz ..face (c irc: e one
Y CE N DI NA 4 Is The canmi,=W Lb� e-A i ag slip arime1cd to dits form?
Yes Li N o 11 5, Wcrc prop'Ll CUAOdy perIIImoivM) followed?
Yrs Ljmw , 16. Weve %&np�n Mr, Hsed on the (70C?
YY �s Noi samplIc ll),m HNWd on all sample contminim?
Yes Nr) as VAIVOion, drtut a IiIII't knell Oil the Uljk?
�y es No 7n —%r0 t itte finin date & thim fisted on a] I sampic uvnIaimn'?
�y e "s Ej N O'� I Did ih coutairm Inkel in Formation � ID, (kille, Ome) mgme w ilh the rOC,?
r.7-I Yes 1I 1 1. Woe tests to be WTfomied Tktetf tm the CC)C7
CS, LI No 12, Did ulit suniallies arriva 11', ilin prol.'er Containen Awr ead,,a ttst widlor in good condv i.�n
(tAwtokwn, lids on. c,tc,),
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"its No i S. We re any &Nn"IPICS containc rs m 6sx.glex cen f1cirz;e one),samples Not h --pJvd on CXAC?
[7l Yer, F'l Nv�� U]NA 16. For VDA and KSK - l'O %mil-Aeg, y,K*re bubhIcs prcmma dj' 'jr(jj('ter','�
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y No, V NA 17, Wery all I DRUIILetglvaur. lel lt Samples rerAVNI '11 a nI I of (": 2?
%Icrc aril cyani& Atiniplas ttLelived at a pli 12,And sullfidie sainp[ei receIveld a, a �41 W?
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yes No n ,j� NA
-2 Y", 20.VAndimm
L FLII N A C("Imct ly '.1"Almvitn"d fmal the C,',OC inal fie cnounfAmt &nfiari in LIMS?
a-Y-1a &N 2! 11. W&s, lite q uoic aiamber listed on l,ic ciontai orr bbeP If yes, Qoote'rt
Samp lie Prestryakitsm
receind incoiTuvOy pms�--rvetl wid were adJusted ac,=Tdirjgly
NA mL mmilo! 142-SO4, I INUJ, 14C, N&OH oirss SR 4
Tim rm1 pm a raw atlamma crawlfmontlm-) omer.wreservativejs mcdcd, plc;m avw- in the comments bellow,
W
,,nfr, mzc6yM with bubbles >6 n"n in dmmeiwrw
,A) MA ivem recei'vcad with w (ir mg is set,) and wcm
mccordirialy in sattiplereceiving, w4lth j,,.)d�jAjqj, fltiaj,,mu!Jazc (M,132%) w!Oi Shealy ID, 'MA
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Pace AnalltyticaA Services, LLC (formeHy Shealy Enva ranrnental Services, hic.)
11016 Vantage Paiinit Drive West Columbla, SC 2'9172 1(8031 791-9700 Fax [phone] www.pacellailas.com
Page 12 of 12

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Mathis Storage Tank
Lot Number:W125016
Date Completed:10/27/2021
10/27/2021 10:30 AM
Approved and released by:
Project Manager II: Lucas Odom
,�i
A4W
AMP VOWN Acr K er AI $1114ld
i
FA[ (' R F D 1 F IE D
o1SriuraA3,01PAI�3Y
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: W125016
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 601 OD, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids, the initial sample amount used for the following sample deviated 3X greater than the
standard procedure: W125016-001. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 10

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: W125016
Sample Number Sample ID Matrix Date Sampled Date Received
001 Mathis Storage Tank Solid 09/23/2021 1330 09/24/2021
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 10

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: W125016
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Mathis Storage Tank
Solid
% Volatile Solids
SM 2540G-
92
%
5
001
Mathis Storage Tank
Solid
Ammonia - N (gas
350.1
28000
mg/kg
5
001
Mathis Storage Tank
Solid
Nitrate -Nitrite - N (soluble)
353.2
55 S
mg/kg
5
001
Mathis Storage Tank
Solid
Phosphorus
365.1
8900 S
mg/kg
5
001
Mathis Storage Tank
Solid
TKN
351.2
73000
mg/kg
5
001
Mathis Storage Tank
Solid
Aluminum
601 OD
2500
mg/kg
6
001
Mathis Storage Tank
Solid
Calcium
601 OD
15000
mg/kg
6
001
Mathis Storage Tank
Solid
Copper
601 OD
19
mg/kg
6
001
Mathis Storage Tank
Solid
Potassium
601 OD
8600
mg/kg
6
001
Mathis Storage Tank
Solid
Sodium
601 OD
4600
mg/kg
6
001
Mathis Storage Tank
Solid
Zinc
601 OD
43
mg/kg
6
(11 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 4 of 10

Client:Terra Renewal Services, Inc. Laboratory ID:WI25016-001
Description: Mathis Storage Tank Matrix: Solid
Date Sampled:09/23/2021 1330 % Solids: 4.02 09/28/2021 2314
Date Received:09/24/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
09/30/2021 2351 MOM
17282
1 350.1
(Ammonia - N) 350.1
25
10/07/2021 1835 DAK
18067
1
(Nitrate-Nitr) 353.2
1
09/30/2021 1530 AAB
17351
1
(Phosphorus) 365.1
10
10/06/2021 1209 DMA
09/30/2021 1140 17151
1
(Soil pH meas) 9045D
1
09/27/2021 2239 NBW
16750
2 351.4
(TKN) 351.2
5
10/05/2021 1824 DMA
10/05/2021 1216 17657
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
92
%
1
Ammonia - N (gas diffusion)
350.1
28000
6200
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
55 S
5.0
mg/kg
1
Phosphorus
7723-14-0 365.1
8900 S
1200
mg/kg
1
Soil pH measured in water @ 17.5 ° C
9045D
5.0
su
1
TKN
351.2
73000
6200
mg/kg
2
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A 1 10/26/20211017 CMF
10/19/2021 2053 19390
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
420
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
420
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
420
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
420
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
420
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
420
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
420
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
76 41-132
Tetrachloro-m-xylene
68 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 09/30/2021 1354 CMS2 09/29/2021 1239 16640
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471B ND 1.9
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 10

Client:Terra Renewal Services, Inc. Laboratory ID:WI25016-001
Description: Mathis Storage Tank Matrix: Solid
Date Sampled:09/23/2021 1330 % Solids: 4.02 09/28/2021 2314
)ate Received:09/24/2021
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD 1 09/29/20211537 JMH
09/28/2021 1049 16783
2 3050B
601OD 1 09/30/20210629 JMH
09/28/2021 1049 16783
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 601OD
2500
160
mg/kg
1
Arsenic
7440-38-2 601OD
ND
5.9
mg/kg
1
Cadmium
7440-43-9 601OD
ND
2.0
mg/kg
1
Calcium
7440-70-2 601OD
15000
2000
mg/kg
1
Copper
7440-50-8 601OD
19
3.9
mg/kg
1
Lead
7439-92-1 601OD
ND
3.9
mg/kg
1
Magnesium
7439-95-4 601OD
ND
2000
mg/kg
1
Molybdenum
7439-98-7 601OD
ND
16
mg/kg
1
Nickel
7440-02-0 601OD
ND
16
mg/kg
1
Potassium
7440-09-7 601OD
8600
2000
mg/kg
2
Selenium
7782-49-2 601OD
ND
7.9
mg/kg
1
Sodium
7440-23-5 601OD
4600
2000
mg/kg
1
Zinc
7440-66-6 601OD
43
20
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 10

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 10

PACE ANALYTICAL SERVICES, LLC
North Carolina Permit Pa ram oters
I ReSidUaIS Rlta] N� B-Ialy7ed to dMIOWT-31W, U10-y- im� .4%g Agg*11reacbmexvatian
And Rt',wVety Act (RCIW). I
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sr,ud iu Attachrutit A, ard the shall maitiiaifz ft. rewXIIF Or Fi mfnimi,im ff flv;! years.
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Lea,&
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WQC036936 VeTsion 1.0
Sha Veisiozii 14010
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
Sarnpaleg Receipt Checklist (SRC) I,MGGIII19C-151
rd��lraslflm�c ' CssUIrfRAut'hority. Pace ENV-a1MCOL
Sample Reeci pt Clltoddi t (SRC).
Client/ rorr„1111,xa1i COO[OT InrPicclssrll livrd;;ate; K&L' I., OW23�21121 r.AAp ; w1z5D15
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PTA Strip JD: NA _ [ mlorine Strip U), H,+ Tested �y_.r,
Original tcrnpzrautrc upon receipt a Derived (Crarrocl,4 k0mTwirm-im opal receipt %Slid Snalp-Cusp TD:
3,G m3.l,F o-sf Yet ll. c Pt �h.w o r lei 1NAeC
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Time cif pdiip5er 'Ara(ia"a NA .___..-._.. if moo tht�m uni; pr--sci .is needed. pie a nwe'in the cstrameist:. below.
smm—ile(S) KA Y C7i:•rti-CCNCd Wo'itl,-k bUbblcs'-6 inm in djamdior,
------------------------
Stream al j j -0'. mm 14^cram per lyer� %art TRC ., 0-5 am gig (ff 419J is Jat)1 aiud were
{7(i'usAl accordingly in sample mceivlll.nIirptl 7.,0diun) (N20.1) viffi Sllivwy 1U NA-- - --
R l,arcii Wbtxl;s of filiW Lk,; a o-1 Dai,a.: C%2S 121
Ctinrrraents;
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 10

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:WL01015
Date Completed:01/26/2022
Revision Date: 01/19/2022
01/27/2022 9:38 AM
Approved and released by:
Project Manager II: Lucas Odom
,�i
A4W
AMP VOWN Acr K er AI $1114ld
i
FA[ (' R F D 1 F IE D
o1SriuraA3,01PAI�3Y
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 20

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WL01015
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 601 OD, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
This report supersedes all other versions of the same report.
Inorganic Metals
Due to the matrix and low percent solids, these samples had an initial weight that is 3x greater than
standard procedure: WL01015-001, WL01015-002, WL01015-003. The LOQ has been adjusted
accordingly.
Report Revision 01/27/22
Due to client request the % solids result was reanalyzed for sample -003. The sample yielded a lower
result and has been reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 20

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WL01015
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
Tyson/Willisboro
Solid
11/30/2021 1130
12/01/2021
002
Tyson/Harmond
Solid
11/30/2021 1230
12/01/2021
003
Advanced Foods/Claramont
Solid
11/30/2021 1430
12/01/2021
(3 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 20

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WL01015
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
Tyson/Willisboro
Solid
% Volatile Solids
SM 2540G-
98
%
8
001
Tyson/Willisboro
Solid
Ammonia - N (gas
350.1
1500
mg/kg
8
001
Tyson/Willisboro
Solid
Flashpoint (Pensky-
1010B
>140
° F
8
001
Tyson/Willisboro
Solid
Nitrate -Nitrite - N (soluble)
353.2
44
S
mg/kg
8
001
Tyson/Willisboro
Solid
Paint Filter Test
9095B
Fail
pass/fail
8
001
Tyson/Willisboro
Solid
Phosphorus
365.1
3700
S
mg/kg
8
001
Tyson/Willisboro
Solid
TKN
351.2
52000
S
mg/kg
8
001
Tyson/Willisboro
Solid
Aluminum
601OD
150
mg/kg
11
001
Tyson/Willisboro
Solid
Copper
601OD
27
mg/kg
11
001
Tyson/Willisboro
Solid
Zinc
601OD
38
mg/kg
11
002
Tyson/Harmond
Solid
% Volatile Solids
SM 2540G-
87
%
12
002
Tyson/Harmond
Solid
Ammonia - N (gas
350.1
12000
mg/kg
12
002
Tyson/Harmond
Solid
Flashpoint (Pensky-
1010B
>140
° F
12
002
Tyson/Harmond
Solid
Nitrate -Nitrite - N (soluble)
353.2
58
mg/kg
12
002
Tyson/Harmond
Solid
Paint Filter Test
9095B
Fail
pass/fail
12
002
Tyson/Harmond
Solid
Phosphorus
365.1
19000
S
mg/kg
12
002
Tyson/Harmond
Solid
TKN
351.2
59000
mg/kg
12
002
Tyson/Harmond
Solid
3+4-Methylphenol
8270E
0.83
mg/L
13
002
Tyson/Harmond
Solid
Aluminum
601OD
8100
mg/kg
15
002
Tyson/Harmond
Solid
Calcium
601OD
39000
mg/kg
15
002
Tyson/Harmond
Solid
Copper
601OD
13
mg/kg
15
002
Tyson/Harmond
Solid
Potassium
601OD
3600
mg/kg
15
002
Tyson/Harmond
Solid
Sodium
601OD
3700
mg/kg
15
002
Tyson/Harmond
Solid
Zinc
601OD
56
mg/kg
15
003
Advanced Foods/Claramont
Solid
% Volatile Solids
SM 2540G-
95
%
16
003
Advanced Foods/Claramont
Solid
Ammonia - N (gas
350.1
170
mg/kg
16
003
Advanced Foods/Claramont
Solid
Flashpoint (Pensky-
1010B
>140
° F
16
003
Advanced Foods/Claramont
Solid
Nitrate -Nitrite - N (soluble)
353.2
3.8
mg/kg
16
003
Advanced Foods/Claramont
Solid
Paint Filter Test
9095B
Fail
pass/fail
16
003
Advanced Foods/Claramont
Solid
Phosphorus
365.1
800
mg/kg
16
003
Advanced Foods/Claramont
Solid
TKN
351.2
11000
mg/kg
16
003
Advanced Foods/Claramont
Solid
Aluminum
6010D
3400
mg/kg
19
003
Advanced Foods/Claramont
Solid
Calcium
6010D
570
mg/kg
19
003
Advanced Foods/Claramont
Solid
Copper
6010D
450
mg/kg
19
003
Advanced Foods/Claramont
Solid
Lead
6010D
1.9
mg/kg
19
003
Advanced Foods/Claramont
Solid
Nickel
6010D
35
mg/kg
19
003
Advanced Foods/Claramont
Solid
Potassium
6010D
540
mg/kg
19
003
Advanced Foods/Claramont
Solid
Sodium
6010D
1700
mg/kg
19
003
Advanced Foods/Claramont
Solid
Zinc
6010D
140
mg/kg
19
(39 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 4 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-001
Description: Tyson/Willisboro Matrix: Solid
Date SamplecIA 1/30/2021 1130 % Solids: 4.96 12/03/2021 0215
Date Received:1210112021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
12/07/2021 2024 MSG
24853
1 350.1
(Ammonia - N) 350.1
2
12/06/2021 1541 DMA
24642
1
(Flashpoint Q 1010B
1
12/08/2021 0850 KMC
24958
1
(Nitrate-Nitr) 353.2
1
12/04/2021 1640 AAB
24599
1
(Paint Filter) 9095B
1
12/10/2021 1118 KMC
1
(Phosphorus) 365.1
5
12/02/2021 1311 DMA
12/01/2021 1453 24173
1
(Reactive Cya) 7.3.3
1
12/03/2021 1030 AAB
12/02/2021 1117
1
(Reactive Sul) 7.3.4
1
12/08/2021 1626 SJL
12/02/2021 1117
1
(Soil pH meas) 9045D
1
12/12/2021 1927 NBW
25322
1 351.4
(TKN) 351.2
2
12/08/2021 1554 DMA
12/08/2021 1036 24899
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
98
%
1
Ammonia - N (gas diffusion)
350.1
1500
400
mg/kg
1
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
° F
1
Nitrate -Nitrite - N (soluble)
353.2
44
S
4.0
mg/kg
1
Paint Filter Test
9095B
Fail
*
pass/fail
1
Phosphorus
7723-14-0
365.1
3700
S
500
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 20.2 ° C
9045D
4.5
su
1
TKN
351.2
52000
S
2000
mg/kg
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 12120120211308 BWS
26259 12/07/2021 0012
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
Units
Run
Benzene
71-43-2
8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7
8260D
ND
0.050
mg/L
1
Chloroform
67-66-3
8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.050
mg/L
1
1, 1 -Dichloroethene
75-35-4
8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6
8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4
8260D
ND
0.010
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-001
Description: Tyson/Willisboro Matrix: Solid
Date SamplecIA 1/30/2021 1130 % Solids: 4.96 12/03/2021 0215
Date Received:1210112021
Run 1 Acceptance
Surrogate Q % Recovery Limits
Bromofluorobenzene 78 70-130
1,2-Dichloroethane-d4 116 70-130
Toluene-d8 94 70-130
TCLP Semivolatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 01110120221828 CMF 12/10/2021 1730 25236 12/08/2021 1827
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1
8270E
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.040
mg/L
1
Hexachloroethane
67-72-1
8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7
8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5
8270E
ND
0.040
mg/L
1
Nitrobenzene
98-95-3
8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5
8270E
ND
0.20
mg/L
1
Pyridine
110-86-1
8270E
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.040
mg/L
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
87
37-129
2-Fluorophenol
54
24-127
Nitrobenzene-d5
72
38-127
Phenol-d5
73
28-128
Terphenyl-d14
100
10-148
2,4,6-Tribromophenol
108
41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311 /8151 A
8151A 1 12/16/2021 1602 DALI
12/13/2021 0915
25336 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L 1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
55 50-112
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-001
Description: Tyson/Willisboro Matrix: Solid
Date SamplecIA 1/30/2021 1130 % Solids: 4.96 12/03/2021 0215
Date Received:1210112021
PCBs by GC
Run Prep Method
Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C
366013/3665A 8082A
1 12/15/2021 2243 DALI
12/03/2021 2140 24550
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
340
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
340
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
340
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
340
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
340
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
340
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
340
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
65 41-132
Tetrachloro-m-xylene
60 35-106
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 12/16/2021 1913 DALI
12/10/2021 1700 25232 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9
8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9
8081B
ND
0.0040
mg/L
1
Endrin
72-20-8
8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8
8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3
8081 B
ND
0.00040
mg/L
1
Methoxychlor
72-43-5
8081B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2
8081 B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
49 20-131
Tetrachloro-m-xylene
81 26-132
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 12/08/2021 0807 JAB2 12/08/2021 0331 24447
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471B ND 1.7 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-001
Description: Tyson/Willisboro Matrix: Solid
Date SamplecIA 1/30/2021 1130 % Solids: 4.96 12/03/2021 0215
Date Received:1210112021
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
601OD
1 12/10/2021 1230 KSH2
12/10/2021 0230 25139 12/08/2021 1827
1 1311/7470A
7470A
1 12/14/2021 1038 JAB2
12/14/2021 0642 25465 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 601OD
ND
0.15
mg/L
1
Barium
7440-39-3 601OD
ND
0.25
mg/L
1
Cadmium
7440-43-9 601OD
ND
0.050
mg/L
1
Chromium
7440-47-3 601OD
ND
0.10
mg/L
1
Lead
7439-92-1 601OD
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 601OD
ND
0.20
mg/L
1
Silver
7440-22-4 601OD
ND
0.10
mg/L
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 12/03/2021 1115 KSH2
12/03/2021 0250 24274
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 601OD
150
130
mg/kg
1
Arsenic
7440-38-2 601OD
ND
4.8
mg/kg
1
Cadmium
7440-43-9 601OD
ND
1.6
mg/kg
1
Calcium
7440-70-2 601OD
ND
1600
mg/kg
1
Copper
7440-50-8 601OD
27
3.2
mg/kg
1
Lead
7439-92-1 601OD
ND
3.2
mg/kg
1
Magnesium
7439-95-4 601OD
ND
1600
mg/kg
1
Molybdenum
7439-98-7 601OD
ND
13
mg/kg
1
Nickel
7440-02-0 601OD
ND
13
mg/kg
1
Potassium
7440-09-7 601OD
ND
1600
mg/kg
1
Selenium
7782-49-2 601OD
ND
6.4
mg/kg
1
Sodium
7440-23-5 601OD
ND
1600
mg/kg
1
Zinc
7440-66-6 601OD
38
16
mg/kg
1
Footnote(s): *Paint Filter: 59mL collected;
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-002
Description: Tyson/Harmond Matrix: Solid
Date SamplecIA 1/30/2021 1230 % Solids: 3.81 12/03/2021 0215
Date Received:1210112021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
12/07/2021 2024 MSG
24853
1 350.1
(Ammonia - N) 350.1
10
12/06/2021 1417 DMA
24642
1
(Flashpoint Q 1010B
1
12/08/2021 1006 KMC
24958
1
(Nitrate-Nitr) 353.2
1
12/04/2021 1645 AAB
24599
1
(Paint Filter) 9095B
1
12/10/2021 1118 KMC
1
(Phosphorus) 365.1
25
12/02/2021 1311 DMA
12/01/2021 1453 24173
1
(Reactive Cya) 7.3.3
1
12/03/2021 1043 AAB
12/02/2021 1117
1
(Reactive Sul) 7.3.4
1
12/08/2021 1626 SJL
12/02/2021 1117
1
(Soil pH meas) 9045D
1
12/12/2021 1928 NBW
25322
1 351.4
(TKN) 351.2
2
12/08/2021 1554 DMA
12/08/2021 1036 24899
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
87
%
1
Ammonia - N (gas diffusion)
350.1
12000
2600
mg/kg
1
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
° F
1
Nitrate -Nitrite - N (soluble)
353.2
58
5.3
mg/kg
1
Paint Filter Test
9095B
Fail
pass/fail
1
Phosphorus
7723-14-0 365.1
19000 S
3300
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 20.3 ° C
9045D
5.8
su
1
TKN
351.2
59000
2600
mg/kg
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 12120120211333 BWS
26259 12/07/2021 0012
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1, 1 -Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-002
Description: Tyson/Harmond Matrix: Solid
Date SamplecIA 1/30/2021 1230 % Solids: 3.81 12/03/2021 0215
Date Received:1210112021
Run 1 Acceptance
Surrogate Q % Recovery Limits
Bromofluorobenzene 80 70-130
1,2-Dichloroethane-d4 121 70-130
Toluene-d8 100 70-130
TCLP Semivolatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 01/12/2022 2303 CMF 12/10/2021 1730 25236 12/08/2021 1827
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1
8270E
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.040
mg/L
1
Hexachloroethane
67-72-1
8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7
8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5
8270E
0.83
0.040
mg/L
1
Nitrobenzene
98-95-3
8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5
8270E
ND
0.20
mg/L
1
Pyridine
110-86-1
8270E
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.040
mg/L
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
86
37-129
2-Fluorophenol
79
24-127
Nitrobenzene-d5
101
38-127
Phenol-d5
107
28-128
Terphenyl-d14
101
10-148
2,4,6-Tribromophenol
71
41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311 /8151 A
8151A 1 12/16/2021 1649 DALI
12/13/2021 0915
25336 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L 1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
68 50-112
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-002
Description: Tyson/Harmond Matrix: Solid
Date SamplecIA 1/30/2021 1230 % Solids: 3.81 12/03/2021 0215
Date Received:1210112021
PCBs by GC
Run Prep Method
Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C
366013/3665A 8082A
1 12/15/2021 2256 DALI
12/03/2021 2140 24550
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
440
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
440
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
440
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
440
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
440
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
440
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
440
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
73 41-132
Tetrachloro-m-xylene
71 35-106
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 12/16/2021 1928 DALI
12/10/2021 1700 25232 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9
8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9
8081B
ND
0.0040
mg/L
1
Endrin
72-20-8
8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8
8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3
8081 B
ND
0.00040
mg/L
1
Methoxychlor
72-43-5
8081B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2
8081 B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
81 20-131
Tetrachloro-m-xylene
80 26-132
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 12/08/2021 0815 JAB2 12/08/2021 0331 24447
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471B ND 2.1 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-002
Description: Tyson/Harmond Matrix: Solid
Date SamplecIA 1/30/2021 1230 % Solids: 3.81 12/03/2021 0215
Date Received:1210112021
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
601OD
1 12/10/2021 1249 KSH2
12/10/2021 0230 25139 12/08/2021 1827
1 1311/7470A
7470A
1 12/14/2021 1051 JAB2
12/14/2021 0642 25465 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 601OD
ND
0.15
mg/L
1
Barium
7440-39-3 601OD
ND
0.25
mg/L
1
Cadmium
7440-43-9 601OD
ND
0.050
mg/L
1
Chromium
7440-47-3 601OD
ND
0.10
mg/L
1
Lead
7439-92-1 601OD
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 601OD
ND
0.20
mg/L
1
Silver
7440-22-4 601OD
ND
0.10
mg/L
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 12/03/2021 1141 KSH2
12/03/2021 0250 24274
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 601OD
8100
170
mg/kg
1
Arsenic
7440-38-2 601OD
ND
6.5
mg/kg
1
Cadmium
7440-43-9 601OD
ND
2.2
mg/kg
1
Calcium
7440-70-2 601OD
39000
2200
mg/kg
1
Copper
7440-50-8 601OD
13
4.3
mg/kg
1
Lead
7439-92-1 601OD
ND
4.3
mg/kg
1
Magnesium
7439-95-4 601OD
ND
2200
mg/kg
1
Molybdenum
7439-98-7 601OD
ND
17
mg/kg
1
Nickel
7440-02-0 601OD
ND
17
mg/kg
1
Potassium
7440-09-7 601OD
3600
2200
mg/kg
1
Selenium
7782-49-2 601OD
ND
8.7
mg/kg
1
Sodium
7440-23-5 601OD
3700
2200
mg/kg
1
Zinc
7440-66-6 601OD
56
22
mg/kg
1
Footnote(s): *Paint Filter: 50mL collected;
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-003
Description: Advanced Foods/Claramont Matrix: Solid
Date SamplecIA 1/30/2021 1430 % Solids: 6.95 01/24/2022 2259
Date Received:1210112021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
12/07/2021 2024 MSG
24853
1 350.1
(Ammonia - N) 350.1
1
12/06/2021 1419 DMA
24642
1
(Flashpoint Q 1010B
1
12/08/2021 1040 KMC
24958
1
(Nitrate-Nitr) 353.2
1
12/04/2021 1647 AAB
24599
1
(Paint Filter) 9095B
1
12/10/2021 1118 KMC
1
(Phosphorus) 365.1
5
12/02/2021 1156 DMA
12/01/2021 1453 24173
1
(Reactive Cya) 7.3.3
1
12/03/2021 1032 AAB
12/02/2021 1117
1
(Reactive Sul) 7.3.4
1
12/08/2021 1626 SJL
12/02/2021 1117
1
(Soil pH meas) 9045D
1
12/12/2021 1932 NBW
25322
2 351.4
(TKN) 351.2
5
12/14/2021 1712 DMA
12/08/2021 1036 24899
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
95
%
1
Ammonia - N (gas diffusion)
350.1
170
41
mg/kg
1
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
° F
1
Nitrate -Nitrite - N (soluble)
353.2
3.8
0.82
mg/kg
1
Paint Filter Test
9095B
Fail
pass/fail
1
Phosphorus
7723-14-0 365.1
800
100
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 20.3 ° C
9045D
4.3
su
1
TKN
351.2
11000
1000
mg/kg
2
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 12120120211358 BWS
26259 12/07/2021 0012
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1, 1 -Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-003
Description: Advanced Foods/Claramont Matrix: Solid
Date SamplecIA 1/30/2021 1430 % Solids: 6.95 01/24/2022 2259
Date Received:1210112021
Run 1 Acceptance
Surrogate Q % Recovery Limits
Bromofluorobenzene 84 70-130
1,2-Dichloroethane-d4 122 70-130
Toluene-d8 101 70-130
TCLP Semivolatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 01110120221915 CMF 12/10/2021 1730 25236 12/08/2021 1827
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1
8270E
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.040
mg/L
1
Hexachloroethane
67-72-1
8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7
8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5
8270E
ND
0.040
mg/L
1
Nitrobenzene
98-95-3
8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5
8270E
ND
0.20
mg/L
1
Pyridine
110-86-1
8270E
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.040
mg/L
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
90
37-129
2-Fluorophenol
66
24-127
Nitrobenzene-d5
78
38-127
Phenol-d5
87
28-128
Terphenyl-d14
99
10-148
2,4,6-Tribromophenol
131
41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311 /8151 A
8151A 1 12/16/2021 1712 DALI
12/13/2021 0915
25336 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L 1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
65 50-112
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-003
Description: Advanced Foods/Claramont Matrix: Solid
Date SamplecIA 1/30/2021 1430 % Solids: 6.95 01/24/2022 2259
Date Received:1210112021
PCBs by GC
Run Prep Method
Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C
366013/3665A 8082A
1 12/15/2021 2309 DALI
12/03/2021 2140 24550
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
69
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
69
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
69
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
69
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
69
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
69
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
69
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
72 41-132
Tetrachloro-m-xylene
69 35-106
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 12/16/2021 1944 DALI
12/10/2021 1700 25232 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9
8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9
8081B
ND
0.0040
mg/L
1
Endrin
72-20-8
8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8
8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3
8081 B
ND
0.00040
mg/L
1
Methoxychlor
72-43-5
8081B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2
8081 B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
79 20-131
Tetrachloro-m-xylene
66 26-132
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 12/08/2021 0817 JAB2 12/08/2021 0331 24447
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471B ND 0.31 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-003
Description: Advanced Foods/Claramont Matrix: Solid
Date SamplecIA 1/30/2021 1430 % Solids: 6.95 01/24/2022 2259
Date Received:1210112021
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
601OD
1 12/10/2021 1300 KSH2
12/10/2021 0230 25139 12/08/2021 1827
1 1311/7470A
7470A
1 12/14/2021 1054 JAB2
12/14/2021 0642 25465 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 601OD
ND
0.15
mg/L
1
Barium
7440-39-3 601OD
ND
0.25
mg/L
1
Cadmium
7440-43-9 601OD
ND
0.050
mg/L
1
Chromium
7440-47-3 601OD
ND
0.10
mg/L
1
Lead
7439-92-1 601OD
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 601OD
ND
0.20
mg/L
1
Silver
7440-22-4 601OD
ND
0.10
mg/L
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 12/03/2021 1144 KSH2
12/03/2021 0250 24274
2 3050B
601OD
3 12/03/2021 1356 KSH2
12/03/2021 0250 24274
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 601OD
3400
26
mg/kg
1
Arsenic
7440-38-2 601OD
ND
0.96
mg/kg
1
Cadmium
7440-43-9 601OD
ND
0.32
mg/kg
1
Calcium
7440-70-2 601OD
570
320
mg/kg
1
Copper
7440-50-8 601OD
450
1.9
mg/kg
2
Lead
7439-92-1 601OD
1.9
0.64
mg/kg
1
Magnesium
7439-95-4 601OD
ND
320
mg/kg
1
Molybdenum
7439-98-7 601OD
ND
2.6
mg/kg
1
Nickel
7440-02-0 601OD
35
2.6
mg/kg
1
Potassium
7440-09-7 601OD
540
320
mg/kg
1
Selenium
7782-49-2 601OD
ND
1.3
mg/kg
1
Sodium
7440-23-5 601OD
1700
320
mg/kg
1
Zinc
7440-66-6 601OD
140
3.2
mg/kg
1
Footnote(s): *Paint Filter: 72mL collected;
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 20

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 20

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 20

PACE ANALYTICAL SERVICES, LLC
North Carolina Pennit IPa,Ira meters
2. kcsidAcr LIMIS, 87U11 N4 WMIYZW LO dUJr-L)jstratQ,. thoy conutirvatloa
and Ri�e*v m, (RCHA). Thc igikkabitity, read(9> and tffKkity
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�-,M=P64 HLi ifEtaaaa the 9ECIllitdaients, iti thiS�*tdffioti Oka] I he spac-ficd EL Atia6mcn4A,
The TCLP am lygis shall inc IV, dt Ov' fbilming pf nrut-L-N (th�_ ­V11al-ory 'level ill r-kiffigramils liter
rs ir. parcathormi);
set!&
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silvnx (5.0)
F�ac�iloroetlyytwilo,, (0-'i)
Togaphew (0-5)
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(400,0)
2,el,fi-Ttir-W -O-Ophcnoi (2.101)
2,4_5 T1' (Silvrw I
-ViDyl all Inride (0. Z)
3. An a3alysis shall bz ::;QxWuoW az rcsidilais ffom nw,,h murce genmuting fiacility al; ate Iitvqueacy
sprGifwd in ktachment A, and the PrrMjLtLT Fhtjjll 1Aai31.lalini Lhe results Tbr n tfirl:,trntm of five ycar&
11w- FliLailysis sllan. iuvluje toe following WxaEwI:CTt:
Allifn."
ituan M"polassaullC'Ury i
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Coppa
ill
ZiDQ
T.:.-wil
PhospLtcirnR
Vddl- Solids
L1 a
PCs's
TERRA RENEWAL SERVICES
4791 747-F319,?
V=ion 140G10
page 8 of 12
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Page 19 of 20

PACE ANALYTICAL SERVICES, LLC
Samiples Rereipt Checklist (SKI (mimuisr-is) KeVi"S E1&9/291J202�
lissLihierAl-IbI Nice ENV m WCOL Page 1 011
Sample ReCeipt U'leckfist (I
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Onti� 12aj:,`2Q21
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 20

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Mathis-1
Lot Number:WL10011
Date Completed:12/31/2021
01/04/2022 8:49 AM
Approved and released by:
Project Manager II: Lucas Odom
,�i
A4W
AMP VOWN Acr K er AI $1114ld
i
FA[ (' R F D 1 F IE D
o1SriuraA3,01PAI�3Y
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WL10011
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 601 OD, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix and low percent solids, the following samples have an initial weight that is 3x greater
than standard procedure: WL10011-001. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The following sample was analyzed outside of analytical holding time: WL10011-001. Sample has been
qualified with an "H" accordingly.
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 10

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WL10011
Sample Number Sample ID Matrix Date Sampled Date Received
001 Mathis-1 Solid 12/08/2021 1630 12/10/2021
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 10

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WL10011
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Mathis-1
Solid
% Volatile Solids
SM 2540G-
95 BH
%
5
001
Mathis-1
Solid
Ammonia - N (gas
350.1
17000
mg/kg
5
001
Mathis-1
Solid
Nitrate -Nitrite - N (soluble)
353.2
34 S
mg/kg
5
001
Mathis-1
Solid
Phosphorus
365.1
7000
mg/kg
5
001
Mathis-1
Solid
TKN
351.2
48000
mg/kg
5
001
Mathis-1
Solid
Aluminum
601OD
3100
mg/kg
6
001
Mathis-1
Solid
Calcium
601OD
11000
mg/kg
6
001
Mathis-1
Solid
Copper
601OD
56
mg/kg
6
001
Mathis-1
Solid
Potassium
601OD
3000
mg/kg
6
001
Mathis-1
Solid
Sodium
601OD
1600
mg/kg
6
001
Mathis-1
Solid
Zinc
601OD
110
mg/kg
6
(11 detections)
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 4 of 10

Client:Terra Renewal Services, Inc. Laboratory ID:WL10011-001
Description: Mathis-1 Matrix: Solid
Date SamplecIA 2/08/2021 1630 % Solids: 8.54 12/13/2021 2328
)ate Received:1211012021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
12/16/2021 1929 GAH
25969
2 350.1
(Ammonia - N) 350.1
50
12/30/2021 2230 DAK
27046
1
(Nitrate-Nitr) 353.2
1
12/17/2021 1118 AAB
26061
1
(Phosphorus) 365.1
25
12/14/2021 1219 DMA
12/11/2021 1559 25306
1
(Soil pH meas) 9045D
1
12/12/2021 2001 NBW
25322
1 351.4
(TKN) 351.2
5
12/15/2021 1757 DMA
12/15/2021 1231 25672
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
95 BH
%
1
Ammonia - N (gas diffusion)
350.1
17000
5900
mg/kg
2
Nitrate -Nitrite - N (soluble)
353.2
34 S
2.3
mg/kg
1
Phosphorus
7723-14-0 365.1
7000
1500
mg/kg
1
Soil pH measured in water @ 20.6 ° C
9045D
5.4
su
1
TKN
351.2
48000
2900
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A 1 12/16/2021 2245 DALI
12/12/2021 1825 25318
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
200
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
200
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
200
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
200
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
200
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
200
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
200
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
70 41-132
Tetrachloro-m-xylene
70 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 12/20/2021 0551 JAB2 12/20/2021 0225 25655
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471B ND 0.90
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 10

Client:Terra Renewal Services, Inc. Laboratory ID:WL10011-001
Description: Mathis-1 Matrix: Solid
Date SamplecIA 2/08/2021 1630 % Solids: 8.54 12/13/2021 2328
Date Received:1211012021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601OD 1 12/21/2021 0800 JMH 12/20/2021 0042 26150
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
601OD
3100
73
mg/kg
1
Arsenic
7440-38-2
601OD
ND
2.7
mg/kg
1
Cadmium
7440-43-9
601OD
ND
0.91
mg/kg
1
Calcium
7440-70-2
601OD
11000
910
mg/kg
1
Copper
7440-50-8
601OD
56
1.8
mg/kg
1
Lead
7439-92-1
601OD
ND
1.8
mg/kg
1
Magnesium
7439-95-4
601OD
ND
910
mg/kg
1
Molybdenum
7439-98-7
601OD
ND
7.3
mg/kg
1
Nickel
7440-02-0
601OD
ND
7.3
mg/kg
1
Potassium
7440-09-7
601OD
3000
910
mg/kg
1
Selenium
7782-49-2
601OD
ND
3.7
mg/kg
1
Sodium
7440-23-5
601OD
1600
910
mg/kg
1
Zinc
7440-66-6
601OD
110
9.1
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 6 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 10

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 10

PACE ANALYTICAL SERVICES, LLC
North Carolina Permit Parameters
esic4uaLs sb O be -°rta l_yzcd deflbba'Otr.alr tlx: s a ;r Cons rwatioa.
aulf a aa" (11(). ne cl.ji,l a
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Date: I f- 11 rz 4
WQC'036936 Vn7it)n 1,0 Shell Vef;4urx 140M -a,,,_ R'F 0
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 10 of 10

Laboratory Analyses:
- Seven Set Fecal Coliform Data

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 02/04/2021
Reported: 02/05/2021
For: Advance Claremont
Comments: GEOMETRIC MEAN: <241 MPN/g
i�4 A T' C A � �
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210204-16-01
Fecal Coliforms
Al
<208
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-01
Percent Solids
Al
9.6
%
SM2540B-2011
02/04/2021
MD
210204-16-02
Fecal Coliforms
A2
<258
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-02
Percent Solids
A2
7.76
%
SM2540B-2011
02/04/2021
MD
210204-16-03
Fecal Coliforms
A3
<263
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-03
Percent Solids
A3
7.6
%
SM2540B-2011
02/04/2021
MD
210204-16-04
Fecal Coliforms
A4
<203
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-04
Percent Solids
A4
9.87
%
SM2540B-2011
02/04/2021
MD
210204-16-05
Fecal Coliforms
A5
<258
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-05
Percent Solids
A5
7.74
%
SM2540B-2011
02/04/2021
MD
210204-16-06
Fecal Coliforms
A6
<257
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-06
Percent Solids
A6
7.79
%
SM2540B-2011
02/04/2021
MD
210204-16-07
Fecal Coliforms
A7
<248
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-07
Percent Solids
A7
8.07
%
SM2540B-2011
02/04/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210204-16-01 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210204-16-02 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210204-16-03 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210204-16-04 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210204-16-05 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210204-16-06 Temp on Arrival: 2.5
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210204-16-07 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4m4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 06/10/2021
Reported: 06/11 /2021
For: Advance Claremont
Comments: GEOMETERIC MEAN = 1399 MPN/g dry weight basis
i�4 A T' C A � �
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210610-17-01
Fecal Coliforms
AC1
<1732
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-01
Percent Solids
AC1
1.16
%
SM2540B-2011
06/10/2021
WC
210610-17-02
Fecal Coliforms
AC2
<1639
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-02
Percent Solids
AC2
1.22
%
SM2540B-2011
06/10/2021
WC
210610-17-03
Fecal Coliforms
AC3
719
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-03
Percent Solids
AC3
2.78
%
SM2540B-2011
06/10/2021
WC
210610-17-04
Fecal Coliforms
AC4
<1183
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-04
Percent Solids
AC4
1.69
%
SM2540B-2011
06/10/2021
WC
210610-17-05
Fecal Coliforms
AC5
<2041
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-05
Percent Solids
AC5
0.98
%
SM2540B-2011
06/10/2021
WC
210610-17-06
Fecal Coliforms
AC6
<2703
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-06
Percent Solids
AC6
0.74
%
SM2540B-2011
06/10/2021
WC
210610-17-07
Fecal Coliforms
AC7
<787
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-07
Percent Solids
AC7
2.54
%
SM2540B-2011
06/10/2021
WC
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210610-17-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210610-17-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210610-17-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210610-17-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210610-17-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210610-17-06 Temp on Arrival: 2.3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210610-17-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 03/30/2021
Reported: 03/31 /2021
For: TYSON HARMONY
Comments: GEOMETRIC MEAN: 46,939 MPN/g
i�4 A T' C A � �
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210330-17-01
Fecal Coliforms
TH1
36145
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-01
Percent Solids
TH1
0.83
%
SM2540B-2011
03/30/2021
MD
210330-17-02
Fecal Coliforms
TH2
61915
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-02
Percent Solids
TH2
O.81
%
SM2540B-2011
03/30/2021
MD
210330-17-03
Fecal Coliforms
TH3
50000
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-03
Percent Solids
TH3
1.0
%
SM2540B-2011
03/30/2021
MD
210330-17-04
Fecal Coliforms
TH4
31915
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-04
Percent Solids
TH4
0.94
%
SM2540B-2011
03/30/2021
MD
210330-17-05
Fecal Coliforms
TH5
83333
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-05
Percent Solids
TH5
0.96
%
SM2540B-2011
03/30/2021
MD
210330-17-06
Fecal Coliforms
TH6
74468
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-06
Percent Solids
TH6
0.94
%
SM2540B-2011
03/30/2021
MD
210330-17-07
Fecal Coliforms
TH7
22722
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-07
Percent Solids
TH7
1.01
%
SM2540B-2011
03/30/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210330-17-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210330-17-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210330-17-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210330-17-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210330-17-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210330-17-06 Temp on Arrival: 2.3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210330-17-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4m4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 06/01/2021
Reported: 06/03/2021
For: Tyson Harmony
Comments: GEOMETRIC MEAN: 22,303 MPN/g
i�4 A T' C A � �
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210601-16-01
Fecal Coliforms
TH1
12407
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-01
Percent Solids
TH1
4.03
%
SM2540B-2011
06/01/2021
MD
210601-16-02
Fecal Coliforms
TH2
23936
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-02
Percent Solids
TH2
3.76
%
SM2540B-2011
06/01/2021
MD
210601-16-03
Fecal Coliforms
TH3
34575
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-03
Percent Solids
TH3
3.76
%
SM2540B-2011
06/01/2021
MD
210601-16-04
Fecal Coliforms
TH4
45946
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-04
Percent Solids
TH4
3.7
%
SM2540B-2011
06/01/2021
MD
210601-16-05
Fecal Coliforms
TH5
21108
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-05
Percent Solids
TH5
3.79
%
SM2540B-2011
06/01/2021
MD
210601-16-06
Fecal Coliforms
TH6
21390
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-06
Percent Solids
TH6
3.74
%
SM2540B-2011
06/01/2021
MD
210601-16-07
Fecal Coliforms
TH7
12887
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-07
Percent Solids
TH7
3.88
%
SM2540B-2011
06/01/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210601-16-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-16-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-16-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-16-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-16-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-16-06 Temp on Arrival: 2.3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-16-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 09/02/2021
Reported: 09/07/2021
For: Tyson Harmony
Comments: GEOMETRIC MEAN: 31,173 MPN/g
i�4 A T' C A � �
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210902-15-01
Fecal Coliforms
1-11
40498
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-01
Percent Solids
1-11
3.21
%
SM2540B-2011
09/02/2021
MD
210902-15-02
Fecal Coliforms
H2
74866
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-02
Percent Solids
H2
3.74
%
SM2540B-2011
09/02/2021
MD
210902-15-03
Fecal Coliforms
H3
52147
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-03
Percent Solids
H3
3.26
%
SM2540B-2011
09/02/2021
MD
210902-15-04
Fecal Coliforms
H4
37333
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-04
Percent Solids
H4
3.75
%
SM2540B-2011
09/02/2021
MD
210902-15-05
Fecal Coliforms
H5
9346
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-05
Percent Solids
H5
3.21
%
SM2540B-2011
09/02/2021
MD
210902-15-06
Fecal Coliforms
H6
21164
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-06
Percent Solids
H6
3.78
%
SM2540B-2011
09/02/2021
MD
210902-15-07
Fecal Coliforms
H7
24499
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-07
Percent Solids
H7
4.49
%
SM2540B-2011
09/02/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210902-15-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210902-15-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210902-15-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210902-15-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210902-15-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210902-15-06 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210902-15-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4m4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 12/20/2021
Reported: 12/21 /2021
For: Tyson Harmony
Comments: Geometric Mean: 3601 MPN/g
i�4 A T' C A � �
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
211220-19-01
Fecal Coliforms
T-1
<3617
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-01
Percent Solids
T-1
5.53
%
SM2540B-2011
12/20/2021
CL
211220-19-02
Fecal Coliforms
T-2
<3534
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-02
Percent Solids
T-2
5.66
%
SM2540B-2011
12/20/2021
CL
211220-19-03
Fecal Coliforms
T-3
3610
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-03
Percent Solids
T-3
5.54
%
SM2540B-2011
12/20/2021
CL
211220-19-04
Fecal Coliforms
T-4
<3527
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-04
Percent Solids
T-4
5.67
%
SM2540B-2011
12/20/2021
CL
211220-19-05
Fecal Coliforms
T-5
<3745
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-05
Percent Solids
T-5
5.34
%
SM2540B-2011
12/20/2021
CL
211220-19-06
Fecal Coliforms
T-6
<3509
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-06
Percent Solids
T-6
5.70
%
SM2540B-2011
12/20/2021
CL
211220-19-07
Fecal Coliforms
T-7
<3670
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-07
Percent Solids
T-7
5.45
%
SM2540B-2011
12/20/2021
CL
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 211220-19-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211220-19-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211220-19-03 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211220-19-04 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211220-19-05 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211220-19-06 Temp on Arrival: 3.0
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211220-19-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4m4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 08/26/2021
Reported: 08/28/2021
For: Mathis
Comments:
i�4 A T' C A � �
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210826-16-01
Fecal Coliforms
M1
<4444
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-01
Percent Solids
M1
0.46
%
SM2540B-2011
08/26/2021
MD
210826-16-02
Fecal Coliforms
M2
<4444
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-02
Percent Solids
M2
0.45
%
SM2540B-2011
08/26/2021
MD
210826-16-03
Fecal Coliforms
M3
<4348
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-03
Percent Solids
M3
0.46
%
SM2540B-2011
08/26/2021
MD
210826-16-04
Fecal Coliforms
M4
<4348
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-04
Percent Solids
M4
0.46
%
SM2540B-2011
08/26/2021
MD
210826-16-05
Fecal Coliforms
M5
4255
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-05
Percent Solids
M5
0.47
%
SM2540B-2011
08/26/2021
MD
210826-16-06
Fecal Coliforms
M6
4348
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-06
Percent Solids
M6
0.46
%
SM2540B-2011
08/26/2021
MD
210826-16-07
Fecal Coliforms
M7
4255
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-07
Percent Solids
M7
0.47
%
SM2540B-2011
08/26/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 2

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Page umu

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 10/12/2021
Reported: 10/14/2021
For: Mathis
Comments:
i�4 A T' C A � �
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
211012-32-01
Fecal Coliforms
M1
<7968
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-01
Percent Solids
M1
2.51
%
SM2540B-2011
10/12/2021
MD
211012-32-02
Fecal Coliforms
M2
<7353
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-02
Percent Solids
M2
2.72
%
SM2540B-2011
10/12/2021
MD
211012-32-03
Fecal Coliforms
M3
<8065
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-03
Percent Solids
M3
2.48
%
SM2540B-2011
10/12/2021
MD
211012-32-04
Fecal Coliforms
M4
<7874
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-04
Percent Solids
M4
2.54
%
SM2540B-2011
10/12/2021
MD
211012-32-05
Fecal Coliforms
M5
<8000
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-05
Percent Solids
M5
2.50
%
SM2540B-2011
10/12/2021
MD
211012-32-06
Fecal Coliforms
M6
<8065
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-06
Percent Solids
M6
2.48
%
SM2540B-2011
10/12/2021
MD
211012-32-07
Fecal Coliforms
M7
<8000
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-07
Percent Solids
M7
2.50
%
SM2540B-2011
10/12/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 211012-32-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 211012-32-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 211012-32-03 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 211012-32-04 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 211012-32-05 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 211012-32-06 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 211012-32-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4m4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 01/28/2021
Reported: 01 /29/2021
For: Tyson Wilkesboro
Comments: GEOMETRIC MEAN: <246 MPN/g
i�4 A T' C A � �
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210128-12-01
Fecal Coliforms
TW1
233
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-01
Percent Solids
TW1
8.6
%
SM2540B-2011
01/28/2021
MD
210128-12-02
Fecal Coliforms
TW2
<248
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-02
Percent Solids
TW2
8.05
%
SM2540B-2011
01/28/2021
MD
210128-12-03
Fecal Coliforms
TW3
<253
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-03
Percent Solids
TW3
7.92
%
SM2540B-2011
01/28/2021
MD
210128-12-04
Fecal Coliforms
TW4
<249
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-04
Percent Solids
TW4
8.03
%
SM2540B-2011
01/28/2021
MD
210128-12-05
Fecal Coliforms
TW5
<245
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-05
Percent Solids
TW5
8.16
%
SM2540B-2011
01/28/2021
MD
210128-12-06
Fecal Coliforms
TW6
<253
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-06
Percent Solids
TW6
7.92
%
SM2540B-2011
01/28/2021
MD
210128-12-07
Fecal Coliforms
TW7
<242
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-07
Percent Solids
TW7
8.25
%
SM2540B-2011
01/28/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210128-12-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210128-12-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210128-12-03 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210128-12-04 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210128-12-05 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210128-12-06 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210128-12-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4m4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 06/01/2021
Reported: 06/03/2021
For: Tyson Wilkesboro
Comments: GEOMETRIC MEAN: <230 MPN/g
i�4 A T' C A � �
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210601-15-01
Fecal Coliforms
TW1
<240
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-01
Percent Solids
TW1
8.32
%
SM2540B-2011
06/01/2021
MD
210601-15-02
Fecal Coliforms
TW2
<224
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-02
Percent Solids
TW2
8.92
%
SM2540B-2011
06/01/2021
MD
210601-15-03
Fecal Coliforms
TW3
<243
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-03
Percent Solids
TW3
8.24
%
SM2540B-2011
06/01/2021
MD
210601-15-04
Fecal Coliforms
TW4
<213
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-04
Percent Solids
TW4
9.39
%
SM2540B-2011
06/01/2021
MD
210601-15-05
Fecal Coliforms
TW5
<216
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-05
Percent Solids
TW5
9.27
%
SM2540B-2011
06/01/2021
MD
210601-15-06
Fecal Coliforms
TW6
<235
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-06
Percent Solids
TW6
8.51
%
SM2540B-2011
06/01/2021
MD
210601-15-07
Fecal Coliforms
TW7
<239
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-07
Percent Solids
TW7
8.36
%
SM2540B-2011
06/01/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210601-15-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-15-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-15-03 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-15-04 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-15-05 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-15-06 Temp on Arrival: 3.0
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-15-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 08/26/2021
Reported: 08/28/2021
For: TYSON WILKESBORO
Comments:
i�4 A T' C A � �
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210826-17-01
Fecal Coliforms
W1
<426
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-01
Percent Solids
W1
4.7
%
SM2540B-2011
08/26/2021
MD
210826-17-02
Fecal Coliforms
W2
<342
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-02
Percent Solids
W2
5.84
%
SM2540B-2011
08/26/2021
MD
210826-17-03
Fecal Coliforms
W3
<347
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-03
Percent Solids
W3
5.76
%
SM2540B-2011
08/26/2021
MD
210826-17-04
Fecal Coliforms
W4
<407
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-04
Percent Solids
W4
4.91
%
SM2540B-2011
08/26/2021
MD
210826-17-05
Fecal Coliforms
W5
<394
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-05
Percent Solids
W5
5.08
%
SM2540B-2011
08/26/2021
MD
210826-17-06
Fecal Coliforms
W6
<352
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-06
Percent Solids
W6
5.68
%
SM2540B-2011
08/26/2021
MD
210826-17-07
Fecal Coliforms
W7
<344
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-07
Percent Solids
W7
5.82
%
SM2540B-2011
08/26/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210826-17-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210826-17-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210826-17-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210826-17-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210826-17-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210826-17-06 Temp on Arrival: 2.3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210826-17-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

51)
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Page 4m4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 11/30/2021
Reported: 12/01 /2021
For: Tyson Wilkesboro
Comments:
i�4 A T' C A � �
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
211130-19-01
Fecal Coliforms
TW1
<364
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-01
Percent Solids
TW1
5.49
%
SM2540B-2011
11/30/2021
MD
211130-19-02
Fecal Coliforms
TW2
<359
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-02
Percent Solids
TW2
5.57
%
SM2540B-2011
11/30/2021
MD
211130-19-03
Fecal Coliforms
TW3
<368
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-03
Percent Solids
TW3
5.44
%
SM2540B-2011
11/30/2021
MD
211130-19-04
Fecal Coliforms
TW4
<363
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-04
Percent Solids
TW4
5.51
%
SM2540B-2011
11/30/2021
MD
211130-19-05
Fecal Coliforms
TW5
<366
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-05
Percent Solids
TW5
5.47
%
SM2540B-2011
11/30/2021
MD
211130-19-06
Fecal Coliforms
TW6
<370
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-06
Percent Solids
TW6
5.41
%
SM2540B-2011
11/30/2021
MD
211130-19-07
Fecal Coliforms
TW7
<362
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-07
Percent Solids
TW7
5.52
%
SM2540B-2011
11/30/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 211130-19-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211130-19-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211130-19-03 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211130-19-04 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211130-19-05 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211130-19-06 Temp on Arrival: 3.0
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211130-19-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

5
Annual Pathogen & Vector Attraction Reduction Form for NCAC 2T Rules
(FORM PVRF 2T)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: AdvancePierre Foods - Claremont, NC
NPDES Number: N/A
Monitoring Period: From l/l/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment) 7U73Abt.
C (Prior Testing)L-1
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs FJ
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost n
Heat Drying D
Heat Treatment D
Thermophilic13
Beta Ray 0
Gamma Ray �
Pasteurization 1
..............................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying E
Composting
Aerobic Digestion ID
Anaerobic Digestion
...................................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
203
241
263
MPN/g
0
1/YR
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) '
Alt. 3 (30-day bench) ETAlt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) [3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) L3
1AIt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: AdvancePierre Foods - Claremont, NC
NPDES Number: N/A
Monitoring Period: From l/l/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment) 7U73Abt.
C (Prior Testing)L-1
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs FJ
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost n
Heat Drying D
Heat Treatment D
Thermophilic13
Beta Ray 0
Gamma Ray �
Pasteurization 1
..............................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying E
Composting
Aerobic Digestion ID
Anaerobic Digestion
...................................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
719
1399
2703
MPN/g
0
1/YR
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) '
Alt. 3 (30-day bench) ETAlt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) [3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) L3
1AIt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
r 1•
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
W WTP Name: Mathis-1 (Storage Facility)
Monitoring Period: From l/l/2021 To
NPDES Number: N/A
12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment) 7U73Abt.
C (Prior Testing)L-1
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs FJ
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost n
Heat Drying D
Heat Treatment D
Thermophilic13
Beta Ray 0
Gamma Ray �
Pasteurization 1
..............................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying E
Composting
Aerobic Digestion ID
Anaerobic Digestion
...................................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
4255
4348
4444
MPN/g
0
1/YR
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) '
Alt. 3 (30-day bench) ETAlt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) [3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) L3
1AIt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
W WTP Name: Mathis-1 (Storage Facility)
Monitoring Period: From l/l/2021 To
NPDES Number: N/A
12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment) 7U73Abt.
C (Prior Testing)L-1
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs FJ
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost n
Heat Drying D
Heat Treatment D
Thermophilic13
Beta Ray 0
Gamma Ray �
Pasteurization 1
..............................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying E
Composting
Aerobic Digestion ID
Anaerobic Digestion
...................................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
7353
7900
8065
MPN/g
0
1/YR
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) '
Alt. 3 (30-day bench) ETAlt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) [3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) L3
1AIt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
r 1•
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
W WTP Name: RVAF (Tyson) - Harmony, NC
Monitoring Period: From l/l/2021 To
NPDES Number: N/A
3 /31 /2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment) 7U73Abt.
C (Prior Testing)L-1
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs FJ
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost n
Heat Drying D
Heat Treatment D
Thermophilic13
Beta Ray 0
Gamma Ray �
Pasteurization 1
..............................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying E
Composting
Aerobic Digestion ID
Anaerobic Digestion
...................................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
22722
46959
83333
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) '
Alt. 3 (30-day bench) ETAlt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) [3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) L3
1AIt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle: Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: RVAF (Tyson) - Harmony, NC
Monitoring Period: From 4/1/2021 To
NPDES Number: N/A
6/30/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment) 7U73Abt.
C (Prior Testing)L-1
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs FJ
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost n
Heat Drying D
Heat Treatment D
Thermophilic13
Beta Ray 0
Gamma Ray �
Pasteurization 1
..............................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying E
Composting
Aerobic Digestion ID
Anaerobic Digestion
...................................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
12407
22503
45946
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) '
Alt. 3 (30-day bench) ETAlt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) [3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) L3
1AIt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: RVAF (Tyson) - Harmony, NC
Monitoring Period: From 7/1/2021 To
NPDES Number: N/A
9/30/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment) 7U73Abt.
C (Prior Testing)L-1
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs FJ
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost n
Heat Drying D
Heat Treatment D
Thermophilic13
Beta Ray 0
Gamma Ray �
Pasteurization 1
..............................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying E
Composting
Aerobic Digestion ID
Anaerobic Digestion
...................................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
9346
31173
74866
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) '
Alt. 3 (30-day bench) ETAlt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) [3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) L3
1AIt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
r �1
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: RVAF (Tyson) - Harmony, NC
Monitoring Period: From 10/1/2021 To
NPDES Number: N/A
12/31 /2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment) 7U73Abt.
C (Prior Testing)L-1
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs FJ
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost n
Heat Drying D
Heat Treatment D
Thermophilic13
Beta Ray 0
Gamma Ray �
Pasteurization 1
..............................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying E
Composting
Aerobic Digestion ID
Anaerobic Digestion
...................................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
3509
3601
3745
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) '
Alt. 3 (30-day bench) ETAlt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) [3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) L3
1AIt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
r �1
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc. WQ Permit Number: WQ0038087
W WTP Name: Tyson - Wilkesboro, NC
Monitoring Period: From l/l/2021 To
NPDES Number: N/A
3 /31 /2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment) 7U73Abt.
C (Prior Testing)L-1
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs FJ
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost n
Heat Drying D
Heat Treatment D
Thermophilic13
Beta Ray 0
Gamma Ray �
Pasteurization 1
..............................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying E
Composting
Aerobic Digestion ID
Anaerobic Digestion
...................................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
233
246
253
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) '
Alt. 3 (30-day bench) ETAlt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) [3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) L3
1AIt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc. WQ Permit Number: WQ0038087
WWTP Name: Tyson - Wilkesboro, NC
Monitoring Period: From 4/1/2021 To
NPDES Number: N/A
6/30/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment) 7U73Abt.
C (Prior Testing)L-1
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs FJ
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost n
Heat Drying D
Heat Treatment D
Thermophilic13
Beta Ray 0
Gamma Ray �
Pasteurization 1
..............................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying E
Composting
Aerobic Digestion ID
Anaerobic Digestion
...................................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
213
230
243
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) '
Alt. 3 (30-day bench) ETAlt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) [3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) L3
1AIt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc. WQ Permit Number: WQ0038087
WWTP Name: Tyson - Wilkesboro, NC
Monitoring Period: From 7/1/2021 To
NPDES Number: N/A
9/30/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment) 7U73Abt.
C (Prior Testing)L-1
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs FJ
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost n
Heat Drying D
Heat Treatment D
Thermophilic13
Beta Ray 0
Gamma Ray �
Pasteurization 1
..............................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying E
Composting
Aerobic Digestion ID
Anaerobic Digestion
...................................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
342
372
426
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) '
Alt. 3 (30-day bench) ETAlt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) [3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) L3
1AIt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc. WQ Permit Number: WQ0038087
WWTP Name: Tyson - Wilkesboro, NC
Monitoring Period: From 10/1/2021 To
NPDES Number: N/A
12/31 /2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment) 7U73Abt.
C (Prior Testing)L-1
Alt.D (No Prior Test)
Process to Further Reduce Pathogengs FJ
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost n
Heat Drying D
Heat Treatment D
Thermophilic13
Beta Ray 0
Gamma Ray �
Pasteurization 1
..............................................
Class B:
jAlt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying E
Composting
Aerobic Digestion ID
Anaerobic Digestion
...................................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
359
365
370
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) '
Alt. 3 (30-day bench) ETAlt.
4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) [3
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) L3
1AIt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

6
Soil Test Reports
(for fields applied in 2021)

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7
COMPLIMENTARY DATA:
Executive Summary
Fecal Analysis Summary
Poultry Litter Analysis Summary
Poultry Litter Analyses

Executive Summary
Annual Report -2021
Permit No. WQ0038087
Permittee: Terra Renewal Services, Inc
Nor V&
DER R A
rrvrrEarw.6
Dry Tons ADDlied Der Source
Field ID
Permitted
Acres
Utilized
Acres
Application
Period
(Months)
Crop
RYE
PAN
(lb/ac)
Adjusted
2021PAN
(lb/ac)
PAN Applied
Residuals
(lb/ac)
PAN Applied
Supplement*
(lb/ac)
Total PAN
Applied
(lb/ac)
AdvPierre
Claremont
(DT/Field)
RVAF
Harmony
(DT/Field)
Tyson
Wilkesboro
(DT/Field)
Annual Dry
Tons Applied
(DT/Field)
NC-WK-CH-01
21.8
21.8
Apr -Jun
Corn Silage
179
145
127
127
28.8
10.8
39.6
NC-WK-CH-03
41.6
41.6
Apr -Jun
Corn Silage
285
220
146
31.2
177
1.9
54.0
31.2
87.1
NC-WK-CH-04
35.8
35.8
Apr -Jun
Corn Silage
270
220
187
31.2
218
0.9
80.2
16.8
97.9
NC-WK-MF-09
13.2
13.2
Aug -Sep
Sm Grains
98
98
97
97
11.2
13.1
24.3
NC-WK-MF-10
19.6
19.6
Sep
Sm Grains
98
98
87
87
16.0
16.0
32.0
NC-WK-MF-11
22.5
22.5
Sep
Sm Grains
80
80
78
78
19.2
13.1
32.3
NC-WK-MF-13
33.8
33.8
Dec
Corn Silage
214
201
139
139
28.5
67.6
96.1
NC-WK-MF-14
23.4
23.4
Dec
Corn Silage
174
164
36
36
4.8
12.5
17.3
NC-WK-MF-15
13.8
13.8
Dec
Corn Silage
174
167
118
118
10.5
22.5
33.0
NC-WK-MF-23
59.2
59.2
Aug -Sep
Sm Grains
98
98
97
97
54.5
53.7
108.2
NC-WK-MRF-03
18.9
18.9
Dec -Jan
Corn Silage
179
143
142
142
28.9
23.3
52.2
NC-WK-MRF-05
25.3
25.3
Dec -Jan
Corn Silage
212
199
154
31.2
185
1.6
38.2
34.1
73.9
NC-WK-MRF-06
20.4
20.4
Dec -Jan
Corn Silage
212
173
119
31.2
150
32.0
20.2
52.2
NC-WK-MRF-12
25.1
25.1
Dec -Jan
Corn Silage
219
187
139
31.2
170
3.0
57.1
19.7
79.8
NC-WK-MRF-20
52.3
52.3
Jul -Aug
Nov -Dec
Corn Silage
Corn Silage
237
224
178
223
73
223
73
1.9
160.8
128.0
290.7
NC-WK-MRF-21
27.8
27.8
Jun -Aug
Corn Silage
237
220
218
218
0.9
52.7
50.7
104.3
NC-WK-RJ-02
57.8
57.8
Mar
Corn Silage
237
230
20
20
1.6
13.2
4.7
19.5
NC-WK-RJ-05
45.1
45.1
Feb -Mar
Oct -Nov
Corn Silage
Corn Silage
237
221
207
123
68
31.2
31.2
155
99
1.6
72.5
113.5
187.6
NC-WK-RJ-07
24.6
24.6
Mar
Corn Silage
214
214
101
31.2
132
17.1
26.4
43.5
NC-YK-YF-01
13.5
13.5
Oct
Sm Grains
98
98
73
73
0.9
10.5
7.5
18.9
NC-YK-YF-03
22.3
22.3
Sep -Oct
Sm Grains
120
120
107
107
24.0
20.6
44.6
NC-YK-YF-04
23.3
23.2
Oct
Sm Grains
120
120
24
24
3.8
7.5
11.3
NC-WK-YK-YF-05
51.5
51.5
Oct
Sm Grains
120
120
51
51
23.8
26.3
50.1
TOTALS: 693 14 842 740 11,596

Fecal Analysis Summary - 2021
Permit No: WQ0038087
Permittee: Terra Renewal Services, Inc
AW VA
TERRA
VonOwa
Facility: AdvancePierre Foods -Claremont
Result (MPN/gram)
Sample Date 1 2 3 4 5 6 7 Geo Mean
2/4/2021 208 258 263 203 258 257 248 241
6/10/2021 1,732 1,639 719 1,183 2,041 2,703 787 1,399
Facility: RVAF
(Tyson) - Harmony
Sample Date
1
2
3/30/2021
36,145
61,915
6/1/2021
12,407
23,936
9/2/2021
40,498
74,866
12/20/2021
3,617
3,534
Result (MPN/gram)
3
4
5
6
7
Geo Mean
50,000
31,915
83,333
74,468
22,722
46,959
34,575
45,946
21,108
21,390
12,887
22,303
52,147
37,333
9,346
21,164
24,499
31,173
3,610
3,527
3,745
3,509
3,670
3,601
Facility: Tyson - Wilkesboro
Result (MPN/gram)
Sample Date
1
2
3 4
5
6
7
Geo Mean
1/28/2021
233
248
253 249
245
253
242
246
6/1/2021
240
224
243 213
216
235
239
230
8/26/2021
426
342
347 407
394
352
344
372
11/30/2021
364
359
368 363
366
370
362
365
Facility: Mathis-1 (Storage)
Result (MPN/gram)
Sample Date 1 2 3 4 5 6 7 Geo Mean
8/26/2021 4,444 4,444 4,348 4,348 4,255 4,348 4,255 4,348
10/12/2021 7,968 7,353 8,065 7,874 8,000 8,065 8,000 7,900

Poultry Litter Analysis Summary - 2021
Source: ASJ Mathis Farms
Sample ID
Total N
(ppm)
Dry Matter
N
PAN
(lb/ton)
MF-1
38,000
62.8
23.9
MF-2
22,600
33.9
7.7
MF-3
26,800
47.1
12.6
MF-4
32,300
28.7
9.3
MF-5
37,600
78.8
29.6
MF-6
23,400
35.5
8.3
MF-7
31,600
19.4
6.1
MF-8
22,800
63.3
14.4
MF-9
24,800
40.7
10.1
MF-10
35,600
84.3
30.0
MF-11
20,400
26.4
5.4
MF-12
29,500
68.1
20.1
MF-13
83,900
25.8
21.6
MF-14
22,600
73.5
16.6
MF-15
35,400
31.3
11.1
Average: 32,487 48.0 15.6
lb/ton = ((%DM/100)*2000 lb/ton) * (Total N ppm/1,000,000) * (MR)
MR = Mineralization Rate = 50% (expressed as decimal: 0.5)

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