NCG030556_Monitoring Report_20220829

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Storinwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For,quidonceon lillinlr uu t this/brm. please visit:: httn://oortal nWell rore/weh/wolves/sn/npdessw:rr i-�
Permit No. ti/C/_ _, _ _, _, _, _/ or Certificate a Coverage No.:
Facility Nance: IAMer- , _n ldlre }7 ect_ t e,2
County. rh tc k L en to , r Phone No. 7
Inspector: G'
Date of Inspection: IN (22
Time of Inspection: 9-2 s RM
Total Event Precipitation (inches): r ZZ
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
M Yes ❑ No
Please verily whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-horn- storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
signature, I certify that this report is accurate and complete to the best of my knowledge:
of Permittee or Designee)
Pagel of 2

I. Outfall Description:
(Ju Ball No. _F� Z_ structtire (pipe, ditch, etc.)
Receiving Sti c�arrr: �_r�r'�; .,� 1-' a 1A
Describe the industrial activities that: occur within the outfall drainage area: Pa1Lk Lo +
2. Color: Describe the color of tlae discharge using basic colors (red, brawn, blue, etc.) and tint
(light, medium, dark) :a, cie ,criptors: _ L � cSn
:3. Odor: Describe airy distinct oclors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 0o N 2
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
"�1
/ 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes N l`
8. Is there an oil sheen in the stormwater discharge? Yes ON
9. Is there evidence of erosion or deposition at the outfall? Yes �/
1.0. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2

�GC�CIx
AjZA`%&- �p
NCDENR m IN �
Storniwater Discharge Outfall (SDO)
Qualitative Monitoring Report
rot 'guidunceoil filliusy out tht.sJavn, please visit: hero://mortal ncclrnrot�lweh/uv51/ws/su/nndesstvt+tah
Permit No,: N/( /—/—/_/—/—/_.1—/ or Certificate of Coverage No.: NJ(:/G/ q/3/U/5I,S1(y/
P.i(ihty Name: f)Mer , c � Tp, ,.o 47 c. h i e ,2
County: M-C( k I In Irn)rL Phone No, 7cY- 351'S 3(es—
I nspector: C-U a v I fw,n., A
Date of Inspection:
Time of Inspection:
Total Event Precipitation (inches): _0a +
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
5 Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
re of Permittee or Designee)
Page 1 of 2

(. 011tfall Description.
( 1`.:'t;.lH i`1o' _6 i —� Structure tpil)e, ditcil, otc.�
liMl'F'il'lllg SL.rE'(-iill: Lo T 1AA'r j�jci . l(�� n l
Describe the indUSt.rial aCLIV ties that oCCUr Withill the olltfall drainage area:
2. Color: Describe the color of the discharge U.Siilg basic colors (red, brown, blue, etc.) and tint
(Ii;,11L, medium, dark► as descriptors:
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): N o N
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 0 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater- discharge, where 1 is no solids and 5 is the surface covered with floating solids:
C' 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
2 3 4 5
7. Is there any foam in the stormwater discharge? Yes zo
8. Is there an oil sheen in the stormwater discharge? Yes (No
9. is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2

SWPPP Form 3: Rain Event Data
This form will be used to document any rainfall data starting at least 72 hours before the
expected representative storm event.
Personnel I �o P2y kjqm e-.S
Date/ Time/Rainfall 615 O'D
Date/Time/Rainfai! jo 10 j22 f+'I'` 0
Date/Time/Rainfall b I/ II ZZ 1z: f r,- I D
Date/Time/Rainfall 47M p l C)
Date/Time/Rainfall �/ jz/zz i zs (30/91) o
I i
I Date/Time/Rainfall 1(2,'c)oe"`
i
Date/Time/Rainfall 16/N(z2 ( 1?-ov p, ( , Z7
;tormwater Pollution Prevention Plan Appendices

ST( YWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCG030000 SAMPLES COLLECTED DURING CALENDAR YEAR: �O' .-
CERTIFICATE OF COVERAGE NO. NCG03114- (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME A Me( -,",A TCye42SPQ .Tn C COUNTY MECYCnlnuf4
PERSON COLLECTING SAMPLES(rA2y I F).nn2s PHONENO.(�I>L( ),72-5 (nrv-
CERTIFIED LABORATORY -era is b o 2Cq R Y Lab #
r—Lab # PLEASE SIGN ON THE REVERSE 4
Part A: Specific Monitoring Requirements
Ot tfall
No,
I)ato
Sample ,CoDl:etedy
uto/dd! r
T.: F a'.`U0530
U0400
01051
00556
78141
TotaliSuspended Solids,
in /L
pll,
Standard units
Lead, nig/L
Oil and Grease,
nip L
' Total ' oxic Organics,
ni g/L
Benchmark
`". 100
Within 6,0 - 9,0
0.033
30
1 .,
2
.3
N
ni',-
t
Note: If you report a sampled value in excess of the benchmark value, or outside the oenclunerK range for pri, you must implement f ter t ur f ter L respunses.
See General Permit text.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _no
(if yes, complete Part B)
err B: Whole
Outfall:.
No.
1n4oltcu.... a
`Date
Sample CoOected; ;
nio/dd/ r ..
--- ---- ----- - -
OOSSG `
00530
00400
Oil and Grease,
_. tiro/L
'Total Suspended Solids,
ni dL
PH,
Standardunits:Annual
New Motor_Oil Usage,
average gallimi
Benchmark
- 30
100
6.0 - 9.0
Note: If you report a sampled value in excess of the benchmark value, or outside the benclunark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
STORM EVENT CHARACTERISTICS:
Date (9� (first event sampled) i
Total Event Precipitation (inches): 02
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SWU-245-102107
Pagel of 2

Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or
manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject
to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for
electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stomtwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent
management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the
discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I
certify that to the best of my knowledge and belief, no dumping of concentrated toxic,organics into the stormwater or areas which are exposed to rainfall or stormwater
runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management
plan included in the Stormwater Pollution Prevention Plan."
GP-2y WIVUe s
Name (Print name)
PC, - A+en 0 n.c v`
tie (Prints title)
( gn re) (Date)
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
tiie possibility of fines and imprisonment for knowing violations."
Permittee)
III �Z Z
(Date)
SWU-245-102107

aceAnalytical s
vrvw.paeNapa.com
June 30, 2022
Mr. Gary Hames
American Truetzschler, Inc.
PO Box 669228
5315 Heavy Equipment School Rd
Charlotte, NC 28266
RE: Project: STORMWATER TESTING
Pace Project No.: 92610035
Dear Mr. Hames:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Enclosed are the analytical results for sample(s) received by the laboratory on June 15, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
Pace Analytical Services - Charlotte
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
9114r,�U�
Sarah Graham
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This repon shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC.
Pagel of 34

�;ZeAnalyfical*
/ w ..pacdahs.cam
i
Project: STORMWATER TESTING
Pace Project No.: 92610035
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification M PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification IF 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Flonda/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Missouri Certification #: 236
Montana Certification #: Carl 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
lnrginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virgmia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 34

aceAnalytical"
www.wesabaxats
I
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
STORMWATER TESTING
92610035
Analytes
Lab ID
SamplelD
Method
Analysts
Reported
laboratory
92610036001
At
EPA 1664E
REL
1
PASI-C
EPA 200.8 Rev 5.4
DBB1
12
PASI-A
EPA 245.1 Rev 3.01994
NMP
1
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
38
PASI-C
SM 264OD-2015
MAB2
1
PASI-A
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 9040C
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 335.4
JH2
1
PASI-O
EPA 420.4 Rev 1.0 1993
NOS
1
PASI-A
92610035002
A2
EPA 1664E
REL
1
PASI-C
EPA 200.8 Rev 5.4
DBB1
12
PASI-A
EPA 245.1 Rev 3.01994
NMP
1
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
38
PASI-C
SM 254OD-2015
MAB2
1
PASI-A
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 9040C
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 335.4
JH2
1
PASI-O
EPA 420.4 Rev 1.0 1993
NOS
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 34

aceAnalytical4
WYY.pssWM.sse
i
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
Project: STORMWATER TESTING
Pace Project No.: 92610035
Sample: Al
Lab IO: 92610036001 Collected:
06/14/22 08:05
Received: 06/15/22 12:56 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No.
Oual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
NO
mg/L
4.8
1
06/20/22 23:30
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4
Preparation Method: EPA 200.8 Rev 5.4
Pace Analytical Services -Asheville
Antimony
NO
ug/L
1.0
1
06/17/22 11:28
06/20/22 03:57
7440-36-0
Arsenic
NO
ug/L
1.0
1
06/17/22 11:28
06/20122 03:57
7440-38-2
Beryllium
NO
ug/L
0.10
1
06/17/22 11:28
06/2022 03:57
7440-41-7
Cadmium
NO
ug/L
0.20
1
06/17/22 11:28
06/20/22 03:57
744043-9
Chromium
NO
ug/L
1.0
1
06/17/22 11:28
06/20/22 03:57
7440-47-3
Copper
2.5
ug/L
2.0
1
06/1722 11:28
06/2022 03:57
7440-50-8
Lead
NO
ug/L
1.0
1
0611722 11:28
062022 03:57
7439-92-1
Nickel
NO
ug/L
1.0
1
06/1722 11:28
06/2022 03:57
7440-02-0
Selenium
NO
ug/L
2.0
1
06/1722 11:28
06/2022 03:57
778249-2
Silver
NO
ug/L
0.40
1
06/1722 11:28
0612022 03:57
7440-224
Thallium
NO
ug/L
0.47
1
06/1722 11:28
0612022 03:57
7440-28-0
Zinc
61.2
ug/L
10.0
1
06/17/22 11:28
06/2022 03:57
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0
1994 Preparation
Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
NO
ug/L
0.20
1
06/27/22 12:26
06/28/22 12:46
7439-97-6
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
Acenaphthylene
NO
ug/L
5.0
1
06/21/22 10:50
06/212216:17
208-96-8
Anthracene
NO
ug/L
5.0
1
06121/22 10:50
06121/22 16:17
120-12-7
Benzidine
ND
ug/L
50.0
1
06121/22 10:50
06/21/22 16:17
92-87-5
Benzo(a)anthracene
NO
ug/L
5.0
1
06/21/22 10:50
06/2112216:17
56-55-3
L1
Benzo(a)pyrene
NO
ug/L
5.0
1
06/21/22 10:50
0612122 16:17
50-32-8
Ll
Benzo(b)fluoranthene
NO
ug/L
5.0
1
06/21/22 10:50
06/21/22 16:17
205-99-2
L1
Benzo(g,h,i)perylene
NO
ug/L
5.0
1
06/21/22 10:50
061212216:17
191-24-2
Benzo(k)fluoranthene
NO
ug/L
5.0
1
06/21/22 10:50
0612122 16:17
207-08-9
4-Bromophenylphenyl ether
NO
ug/L
5.0
1
06/21/22 10:50
06121/22 16:17
101-55-3
L1
Butylbenzylphthalate
ND
ug/L
&0
1
06/21/22 10:50
06/21/22 16:17
85-68-7
L1
4-Chloro-3-methylphenol
NO
ug/L
5.0
1
06/2122 10:50
06/21/22 16:17
59-50-7
L1
bis(2-Chloroethoxy)methane
NO
ug/L
10.0
1
06/2112210:50
06121/22 16:17
111-91-1
bis(2-Chloroethyl) ether
NO,
ug/L
5.0
1
06/2122 10:50
0612122 16:17
111-444
2-Chloronaphthalene
NO
ug/L
5.0
1
06/212210:50
06121/22 16:17
91-58-7
2-Chlorophenol
NO
ug/L
6.0
1
06/2122 10:50
06/21/22 16:17
95-57-8
4-Chlorophenylphenyl ether
NO
ug/L
5.0
1
0612122 10:50
06121/22 16:17
7005-72-3
Chrysene
NO
ug/L
5.0
1
06/21/22 10:50
06/21/22 16:17
218-01-9
Dibenz(a,h)anthracene
NO
ug/L
5.0
1
06121/22 10:50
06121/22 16:17
53-70-3
3,3'-Dichlorobenzidine
NO
ug/L
10.0
1
06/2112210:60
06/2112216:17
91-94-1
2,4-Dichlorophenol
NO
ug/L
5.0
1
06/2112210:60
06/21/22 16:17
120-83-2
Diethylphthalate
NO
ug/L
5.0
1
0612112210:50
06/21/22 16:17
84-66-2
L1
2,4-Dimelhylphenol
NO
ug/L
10.0
1
06/21/22 10:50
06/21/22 16:17
105-67-9
L1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full.
Date: 06/30/2022 03:02 PM
without the wriaen consent of Pace Analytical Services, L-C.
Page 4 of 34

ZeAnalyfical'
www.pacelabsxom
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: STORMWATER TESTING
Pace Project No.: 92610035
Sample: At Lab ID: 92610035001 Collected: 06/14/22 08:05 Received: 06/1522 12:56 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
Dimethylphthalate
ND
ug/L
5.0
1
06/21/22 10:50
06/2112216:17
131-11-3
L1
Di-n-butylphthalate
ND
ug/L
5.0
1
06/21/22 10:50
06/21/22 16:17
84-74-2
Ll
4,6-Dinitro-2-methylphenol
ND
ug/L
10.0
1
06/21/22 10:50
06/2112216:17
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
06/21/22 10:50
06/21/22 16:17
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
06/21/22 10:50
06/2112216:17
121-14-2
L1
2,6-Dinitrotoluene
ND
ug/L
5.0
1
06/21/22 10:50
06/2112216:17
606-20-2
Ll
Di-n-octylphlhalate
ND
ug/L
5.0
1
06/21/22 10:50
06/21/22 16:17
117-84-0
Ll
1,2-Diphenylhydrazine
ND
ug/L
5.0
1
06/21/22 10:50
06/2122 16:17
122-66-7
Ll
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
06121/22 10:50
06/212216:17
117-81-7
L1
Fluoranthene
ND
ug/L
5.0
1
06/21/22 10:50
06/2122 16:17
206.44-0
Ll
Fluorene
ND
ug/L
5.0
1
0612122 10:50
06/2122 16:17
86-73-7
L1
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
06I212210:50
06/212216:17
87-68-3
L2
Hexachlorobenzene
ND
ug/L
5.0
1
0612122 10:50
06/2122 16:17
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
0612122 10:50
06/2122 16:17
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
06121/22 10:50
06/212216:17
67-72-1
L2
Indeno(1,2,3-od)pyrene
ND
ug/L
5.0
1
06121/22 10:50
06/2122 16:17
193-39-5
Isophorone
ND
ug/L
10.0
1
06/21/22 10:50
06/2122 16:17
78-59-1
Naphthalene
ND
ug/L
5.0
1
06/21/22 10:50
06/2122 16:17
91-20-3
Nitrobenzene
NO
ug/L
5.0
1
06/21/22 10:50
06/2122 16:17
98-95-3
2-Nitrophenol
NO
ug/L
5.0
1
06/2112210:50
061212216:17
88-75-5
4-Nitrophenol
NO
ug/L
10.0
1
06121/22 10:50
06/212216:17
100-02-7
N-Nitrosodimethylamine
NO
ug/L
5.0
1
06121/22 10:50
0612122 16:17
62-75-9
N-Nitroso-di-n-propylamine
NO
ug/L
5.0
1
06/21/22 10:50
06/212216:17
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1
06212210:50
061212216:17
86-30-6
Pentachlorophenol
NO
ug/L
10.0
1
06/212210:50
06/212216:17
87-86-5
Phenanthrene
NO
ug/L
5.0
1
06/21/22 10:50
06121/22 16:17
85-01-8
Ll
Phenol
ND
ug/L
5.0
1
06/21/22 10:50
06121/22 16:17
108-95-2
Pyrene
NO
ug/L
5.0
1
06/21/22 10:50
0612112216:17
129-00-0
1-1
12,4-Tdchlorobenzene
NO
ug/L
5.0
1
0612112210:50
06121/22 16:17
120-82-1
1-2
2,4,6-Trichlorophenol
NO
ug/L
10.0
1
06121/22 10:50
06/2112216:17
88-06-2
Li
Surrogates
Nitrobenzene-d5 (S)
62
%
10-120
1
06/21/22 10:50
06121/22 16:17
4165-60-0
2-Fluorobiphenyl(S)
29
%
15-120
1
06/2122 10:50
06/21/22 16:17
321-60-8
Terphenyl-d14 (S)
164
%
11-131
1
06/2122 10:50
06121/22 16:17
1718-51-0
S3
Phenol-d6 (S)
37
%
10-120
1
062122 10:50
06121/22 16:17
13127-88-3
2-Fluorophenol (S)
46
%
10-120
1
06/2122 10:50
06121/22 16:17
367-124
2,4,6-Tribromophenol(S)
98
%
10-137
1
06/21/22 10:50
0612122 16:17
118-79-6
624 Volatile Organics Acrolein
Analytical Method: EPA 624.1
Pace Analytical
Services - Charlotte
Acrolein
NO
ug/L
5.0
1
06116/2219:53
107-02-8
Acrylonitrile
ND
ug/L
5.0
1
06/16/2219:53
107-13-1
Benzene
ND
ug/L
1.0
1
06/16/22 19:53
7143-2
Bromodlchloromethane
ND
ug/L
2.0
1
06116/2219:53
75-274
Bromoform
ND
ug/L
2.0
1
06116/2219:53
75-25-2
Bromomethane
ND
ug/L
2.0
1
06116/2219:53
74-83-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 34

Pace Analytical Services, LLC
Kiny Ave. Suite 100
Zemalyfical" 9900Hunersville, NC 28078
OMM.pledatt Cat
(704)8759092
ANALYTICAL RESULTS
Project: STORMWATER TESTING
Pace Project No.: 92610035
Sample: Al Lab ID: 92610035001 Collected: 06/14/22 08:05 Received: 06/15/22 12:56 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
624 Volatile Organics Acrolein
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
Carbon tetrachloride
NO ug/L
2.0
1
06/16/22 19:53
56-23-5
Chlorobenzene
NO ug/L
2.0
1
06/16/22 19:53
108-90-7 M1
Chloroethane
NO ug/L
2.0
1
06116/22 19:53
75-00-3
2-Chloroethylvinyl ether
NO ug/L
5.0
1
06/16/22 19:53
110-75-8
Chloroform
ND ug/L
2.0
1
0611612219:53
67-66-3
Chloromethane
NO ug/L
2.0
1
06/1612219:53
74-87-3
Dibromochloromethane
NO ug/L
2.0
1
06/1612219:53
124-48-1
1,2-Dichlorobenzene
NO ug/L
2.0
1
06/1612219:53
95-50-1
1,3-Dichlorobenzene
NO ug/L
2.0
1
06/16/22 19:53
541-73-1
1,4-Dichlorobenzene
ND ug/L
2.0
1
0611622 19:53
106-46-7
1,1-Dichloroethane
ND ug/L
2.0
1
06/16/22 19:53
75-34-3
1,2-Dichloroethane
NO ug/L
2.0
1
06/1622 19:53
107-06-2
1,1-Dichloroethene
NO ug/L
2.0
1
06/162219:53
75-35-4
cis-1,2-Dichloroethene
NO ug/L
2.0
1
06/16/22 19:53
156-59-2
trans-1,2-Dichloroethene
NO ug/L
2.0
1
06/16/22 19:53
156-60-5
1,2-Dichloropropane
ND ug/L
2.0
1
06/16/22 19:53
78-87-5
cis-1,3-Dichloropropene
NO ug1L
2.0
1
06/16/22 19:53
10061-01-5
trans-1,3-Dichloropropene
NO ug1L
2.0
1
06/1622 19:53
10061-02-6
Ethylbenzene
NO ug/L
1.0
1
06/16/22 19:53
100-414
Hexachloro-1,3-butadiene
NO ug/L
5.0
1
0611612219:53
87-68-3
Methylene Chloride
NO ug/L
2.0
1
06/1622 19:53
75-09-2
Naphthalene
NO ug1L
5.0
1
061162219:53
91-20-3
1,1,2,2-Tetrachloroethane
NO ug/L
2.0
1
06/16/22 19:53
79-34-5
Tetrachloroethene
NO ug/L
2.0
1
06/16/22 19:53
127-184
Toluene
NO ug/L
1.0
1
06/16/22 19:53
108-88-3
1. 1, 1 -Trichloroethane
NO ug/L
2.0
1
06/16/22 19:53
71-55-6
1,1,2-Trichloroethane
NO ug/L
2.0
1
06/16/22 19:53
79-00-5
Trchloroethene
NO ug/L
2.0
1
06/1622 19:53
79-01-6
Vinyl chloride
NO ug/L
2.0
1
06/1622 19:53
75-014
Surrogates
4-Bromofluorobenzene (S)
104 %
70-130
1
06/1622 19:53
460-004
Toluene-d8 (S)
104 %
70-130
1
06/1622 19:53
2037-26-5
1,2-Dichloroethane-d4 (S)
102 %
70-130
1
06/1622 19:53
17060-07-0
2640D Total Suspended Solids
Analytical Method: SM 25400-2015
Pace Analytical Services -Asheville
Total Suspended Solids
NO mg/L
2.5
1
0611722 11:01
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
Sulfide
NO ri
0.10
1
06/1822 04:29
18496-25-8
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
7.3 Std. Units
0.10
1
06/2422 11:51
H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 34

8ceAna1jfta1
/ WWW.paeYaOf.fsn
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER TESTING
Pace Project No.: 92610035
Sample: Al Lab ID: 92610035001 Collected: 06/14/22 08:05 Received: 06/15/22 12:56 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Sulfate ND mgli- 1.0 1 06/17/22 01:35 14808-79-8
335.4 Cyanide, Total Analytical Method: EPA 335.4 Preparation Method: EPA 335.4
Pace Analytical Services - Ormond Beach
Cyanide ND mg/L 0.010 1 06/22/22 09:23 06/22/22 13:41 57-12-5
420.4 Phenolics, Total Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services -Asheville
Phenolics, Total Recoverable 0.021 mg/L 0.020 1 06/21/22 14:02 06/22/22 16:43 64743-03-9
Sample: A2 Lab ID: 92610036002 Collected: 06/14/22 08:25 Received: 06/15/22 12:56 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Oil and Grease
NO mg/L
5.0
1
06/20/22 23:30
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4
Preparation Method: EPA 200.8
Rev 5.4
Pace Analytical Services - Asheville
Antimony
NO ug/L
1.0
1
06/17/22 11:28
06/20/22 04:01
7440-36-0
Arsenic
NO ug/L
1.0
1
06/17122 11:28
06/20/22 04:01
7440-38-2
Beryllium
NO ug/L
0.10
1
06/1712211:28
06120/2204:01
7440-41-7
Cadmium
NO ug/L
0.20
1
06/17/22 11:28
06120/2204:01
7440-43-9
Chromium
NO ug/L
1.0
1
06/17/22 11:28
06/20/22 04:01
7440-47-3
Copper
NO ug/L
2.0
1
06/17/22 11:28
06/20/22 04:01
7440-50-8
Lead
ND ug/L
1.0
1
06/17/22 11:28
06/20/22 04:01
7439-92-1
Nickel
ND ug/L
1.0
1
06/17/22 11:28
06/20/22 04:01
7440-02-0
Selenium
ND ug/L
2.0
1
06/17/22 11:28
06/20122 04:01
778249-2
Silver
ND ug/L
0.40
1
06/17/22 11:28
06/20/22 04:01
7440-22-4
Thallium
ND ug/L
0.47
1
06/17/22 11:28
06/20/22 04:01
7440-28-0
Zinc
61.4 ug/L
10.0
1
06/1722 11:28
06/20122 04:01
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0
1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
ND ug/L
0.20
1
06/27/2212:26
06/282212:48
7439-97-6
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
Acenaphthylene
ND ug/L
5.0
1
06/21/22 10:50
06/2122 16:42
208-96-8
Anthracene
ND ug/L
5.0
1
06121/2210:50
061212216:42
120-12-7
Benzidine
ND ug/L
50.0
1
06/2122 10:50
06/21/22 16:42
92-87-5
Benzo(a)anlhracene
NO ug/L
5.0
1
06/21/22 10:50
06/21/22 16:42
56-55-3 L1
Benzo(a)pyrene
NO ug/L
5.0
1
06/21/22 10:50
06/21/22 16:42
50-32-8 L1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, U.C.
Page 7 of 34

Pace Analytical Services, LLC
ace Analytical a 9800 KinceyAve. Suite 100
Huntersville, NC 28078
W" Pacelabs.com
(704)8759092
I
ANALYTICAL RESULTS
Project: STORMWATER TESTING
Pace Project No.: 92610035
Sample: A2 Lab ID: 92610035002 Collected: 06/14122 08:25 Received: 06115/22 12:56 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua]
626 RVE
Analytical Method: EPA625.1 Preparation Method: EPA625.1
Pace Analytical Services - Charlotte
Benzo(b)fluoranthene
NO
ug/L
5.0
1
06121/22 10:50
06/21/22 16:42
205-99-2
L1
Benzo(g,h,i)perylene
NO
uglL
5.0
1
06121/22 10:50
06/212216:42
191-24-2
Benzo(k)fluoranthene
NO
ug/L
5.0
1
06/2122 10:50
06/2122 16:42
207-08-9
4-Bromophenylphenyl ether
NO
ug/L
5.0
1
0612122 10:50
06/2122 16A2
101-55-3
L1
Butylbenzylphthalate
NO
ug/L
5.0
1
06/21/22 10:50
06/21/22 16A2
85-68-7
L1
4-Chloro-3-methylphenol
NO
ug/L
5.0
1
06121/22 10:50
061212216:42
59-50-7
1-1
bis(2-Chloroethoxy)methane
NO
uglL
10.0
1
06121/22 10:50
06/21/22 16:42
111-91-1
bis(2-Chloroethyl) ether
NO
ug/L
5.0
1
06/21/22 10:50
06121/22 16:42
111-44-4
2-Chloronaphthalene
NO
ug/L
5.0
1
06/21/22 10:50
06/21/22 16:42
91-58-7
2-Chlorophenol
NO
ug/L
5.0
1
06/21/22 10:50
06/21/22 16:42
95-57-8
4-Chlorophenylphenyl ether
NO
ug/L
5.0
1
06/21/22 10:50
0612122 16:42
7005-72-3
Chrysene
NO
ug/L
5.0
1
06121/22 10:50
06/21/22 16:42
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
06/21/22 10:50
061212216A2
53-70-3
3,3'-Dichlorobenzidine
NO
ug/L
10.0
1
0612112210:50
061212216:42
91-94-1
2,4-Dichlorophenol
NO
ug/L
5.0
1
06121/22 10:50
06/2122 16A2
120-83-2
Diethylphthalate
NO
ug/L
5.0
1
06121/22 10:50
06121/22 16:42
84-66-2
L1
2,4-Dimethylphenol
NO
ug/L
10.0
1
06121/22 10:50
06/2122 16:42
105-67-9
11
Dimethylphthalate
NO
ug/L
5.0
1
06121/22 10:50
06/2112216:42
131-11-3
Ll
Di-n-butylphthalate
NO
ug/L
5.0
1
06/2112210:50
0612112216:42
84-74-2
-1
4,6-Dinitro-2-methylphenol
NO
ug/L
10.0
1
06/2112210:50
06/21/22 16:42
534-52-1
2,4-Dinitrophenol
NO
ug/L
50.0
1
06/21/22 10:50
06/21/22 16:42
51-28-5
2,4-Dinilrotoluene
NO
ug/L
5.0
1
06/2122 10:50
06/21/22 16:42
121-14-2
1-1
2,6-Dinitrotoluene
NO
ug/L
5.0
1
06/212210:50
06121/22 16:42
606-20-2
11
Di-n-octylphthalate
NO
ug/L
5.0
1
06121/22 10:50
061212216:42
117-84-0
L1
1,2-Diphenylhydrazine
NO
ug/L
5.0
1
06/2122 10:50
0612122 16:42
122-66-7
1-1
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
1
06/2112210:50
061212216:42
117-81-7
Ll
Fluoranthene
NO
ug/L
5.0
1
06/21122 10:50
06121/22 16:42
206-44-0
Ll
Fluorene
NO
ug/L
5.0
1
06/21122 10:50
0612122 16:42
86-73-7
L1
Hexachloro-1,3-butadiene
NO
ug/L
5.0
1
06/21/22 10:50
06/21/22 16:42
87-68-3
L2
Hexachlorobenzene
NO
ug/L
5.0
1
06121/22 10:50
06/21/22 16:42
118-74-1
Hexachlorocyclopentadiene
NO
ug/L
10.0
1
06121/22 10:50
06121/22 16:42
77-47-4
Hexachlomethane
NO
ug/L
5.0
1
06/21/22 10:50
06/21/22 16:42
67-72-1
L2
Indeno(1,2,3-cd)pyrene
NO
ug/L
5.0
1
0621122 10:50
06/21/22 16:42
193-39-5
Isophorone
NO
ug/L
10.0
1
062122 10:50
06121122 16:42
78-59-1
Naphthalene
NO
ug/L
5.0
1
06/21/22 10:50
0612122 16:42
91-20-3
Nitrobenzene
NO
ug/L
5.0
1
06/21/22 10:50
06/212216:42
98-95-3
2-Nitrophenol
NO
ug/L
5.0
1
0612112210:50
06121/22 16:42
88-75-5
4-Nitrophenol
NO
ug1L
10.0
1
06/21122 10:50
06/21/22 16:42
100-02-7
N-Nitrosodimethylamine
NO
ug/L
5.0
1
06121/22 10:50
06121/22 16:42
62-75-9
N-Nitroso-di-n-propylamine
NO
ug/L
5.0
1
06/21/22 10:50
06121/22 16:42
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1
06/21/22 10:50
06121/22 16:42
86-30-6
Pentachlorophenol
NO
ug/L
10.0
1
06/2122 10:50
06121/22 16:42
87-86-5
Phenanthrene
NO
ug/L
5.0
1
06/212210:50
06121/22 16:42
85-01-8
L1
Phenol
NO
ug/L
5.0
1
06/21/22 10:50
06121/22 16:42
108-95-2
Pyrene
NO
ug/L
5.0
1
06/21/22 10:50
06/21/22 16:42
129-00-0
L1
1,2,4-Trtchlorobenzene
ND
ug/L
5.0
1
06/21/22 10:50
06/2122 16:42
120-82-1
L2
REPORT
OF LABORATORY
ANALYSIS
This report shell not be reproduced, except
in full,
Date: 06/30/2022 03:02 PM
without the written consent of Pace Analytical Services, I.I.C.
Page 8 of 34

aceAnalytical
/ 1YMW.wcNrua.cam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER TESTING
Pace Project No.: 92610035
Sample: A2 Lab ID: 92610036002 Collected: 06/14/22 08:25 Received: 06/15/22 12:56 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
2.4.6-Trichlorophenol
ND
ug/L
10.0
1
06/21/22 10:50
06/21/22 16:42
88-06-2 Ll
Surrogates
Nitrobenzene-05(S)
110
%
10-120
1
06/212210:50
06/21/22 16:42
4165-60-0
2-Fluorobiphenyl (S)
50
%
15-120
1
06/21/22 10:50
06/2122 16:42
321-60-8
Terphenyl-014 (S)
170
%
11-131
1
06/21/22 10:50
06/21/22 16:42
1718-51-0 S3
Phenol-06 (S)
66
%
10-120
1
06/2122 10:50
06/2122 16:42
13127-88-3
2-Fluorophenol (S)
62
%
10-120
1
06/21/22 10:50
06/2122 16A2
367-12-4
2,4,6-Tribromophenol(S)
105
%
10-137
1
06/21/22 10:50
06/2122 1642
118-79-6
624 Volatile Organics Acrolein
Analytical Method:
EPA 624.1
Pace Analytical
Services - Charlotte
Acrolein
NO
ug/L
5.0
1
06/16/22 20:11
107-02-8
Acrylonitrile
NO
ug/L
5.0
1
06/1622 20:11
107-13-1
Benzene
NO
ugli-
1.0
1
06/16/2220:11
71-43-2
Bromodichloromethane
NO
ug/L
2.0
1
06/16/22 20:11
75-27-4
Bromoform
NO
ug/L
2.0
1
06/1622 20:11
75-25-2
Bromomethane
NO
ug/L
2.0
1
06/16/22 20:11
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1
06116/22 20:11
56-23-5
Chlorobenzene
NO
ug/L
2.0
1
06/16/22 20:11
108-90-7
Chloroethane
NO
ug/L
2.0
1
0611622 20:11
75-00-3
2-Chloroethylvinyl ether
NO
ug/L
5.0
1
06/16/22 20:11
110-75-8
Chloroform
NO
ug/L
2.0
1
06/1622 20:11
67-66-3
Chloromethane
NO
ug/L
2.0
1
06/16122 20:11
74-87-3
Dibromochloromethane
NO
ug/L
2.0
1
06/16/22 20:11
124-48-1
1,2-Dichlorobenzene
NO
ug/L
2.0
1
06/16/22 20:11
95-50-1
1,3-Dichlorobenzene
NO
ug/L
2.0
1
06116/22 20:11
541-73-1
1,4-Dichlorobenzene
NO
ug/L
2.0
1
06/16/22 20:11
10646-7
1,1-Dichloroethane
NO
ug/L
2.0
1
06116/2220:11
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
1
06/16/22 20:11
107-06-2
1,1-Dichloroethene
NO
ug/L
2.0
1
06/16/22 20:11
75-354
cis-1,2-Dichloroethene
NO
ug/L
2.0
1
06116/2220:11
156-59-2
trans-1,2-Dichloroethene
NO
ug/L
2.0
1
06/16/22 20:11
156-60-5
1,2-Dichloropropane
NO
ug/L
2.0
1
06116/2220:11
78-87-5
cis-1,3-Dichloropropene
NO
ug/L
2.0
1
061162220:11
10061-01-5
tmns-1,3-Dichloropropene
NO
ug/L
2.0
1
0611612220:11
10061-02-6
Ethylbenzene
NO
ug/L
1.0
1
0611622 20:11
100414
Hexachloro-1,3-butadiene
NO
ug/L
5.0
1
06116/2220:11
87-68-3
Methylene Chloride
NO
ug/L
2.0
1
0611622 20:11
75-09-2
Naphthalene
NO
ug/L
5.0
1
06116/2220:11
91-20-3
1,1,2,2-Tetrachloroethane
NO
ug/L
2.0
1
06/16/22 20:11
79-34-5
Tetrachloroethene
ND
ug/L
2.0
1
06/16/22 20:11
127-184
Toluene
NO
ug/L
1.0
1
06/16/22 20:11
108-88-3
1,1,1-Trichloroethane
NO
ug/L
2.0
1
06/16/22 20:11
71-55-6
1,1,2-Trichloroethane
NO
ug/L
2.0
1
06/16/22 20:11
79-00-5
Trichloroethane
ND
ug/L
2.0
1
06/16/22 20:11
79-01-6
Vinyl chloride
NO
ug/L
2.0
1
06/16/22 20:11
75-014
REPORT OF LABORATORY ANALYSIS
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Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 34

aceAnalytical e
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: STORMWATER TESTING
Pace Project No.: 92610035
Sample: A2 Lab ID: 92610036002 Collected: 06/14/22 08:25 Received: 06/15/22 12:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
624 Volatile Organics Acrolein
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
25400 Total Suspended Solids
Total Suspended Solids
4500S20 Sulfide Water
Sulfide
9040 pH
pH at 25 Degrees C
300.0 IC Anions 28 Days
Sulfate
336.4 Cyanide, Total
Cyanide
420.4 Phenolics, Total
Phenolics, Total Recoverable
Date: 06/30/2022 03:02 PM
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
100 % 70-130
1
06/16/22 20:11
460-00-4
102 % 70-130
1
06/16/22 20:11
2037-26-5
104 % 70-130
1
06/16/22 20:11
17060-07-0
Analytical Method: SM 254OD-2015
Pace Analytical Services -Asheville
ND mg/L 2.5
1
0611712211:01
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
NO mg/L 0.10
1
06/18/22 04:30
18496-25-8
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
4.3 Std. Units 0.10
1
06/24/22 12:01
H3
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
5.0 mg/L 1.0
1
06/17/22 01:51
14808-79-8
Analytical Method: EPA 335.4 Preparation Method:
EPA 336.4
Pace Analytical Services - Ormond Beach
NO mg/L 0.010
1 06/22/22 09:23
06/22/22 13:42
57-12-5
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4
Rev 1.01993
Pace Analytical Services - Asheville
NO mg/L 0.020
1 0612912211:08
06/30/2211:56
64743-03-9 M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 34

ZeAnalXical'
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i
QUALITY CONTROL DATA
Project: STORMWATER TESTING
Pace Project No.: 92610035
QC Batch: 705466 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92610035001, 92610035002
METHOD BLANK: 3681100 Matrix: Water
Associated Lab Samples: 92610035001, 92610035002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L NO 5.0 06/20/22 23:30
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Q04>878-9092
LABORATORY CONTROL SAMPLE: 3681101
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Oil and Grease mglL 40 32.6 82 78-114
MATRIX SPIKE SAMPLE:
Parameter
3681102
Units
92610320002
Result
Spike MS MS % Rec
Conc. Result %Rec Limits Qualifiers
Oil and Grease
mg/L
ND
38.8 35.5 84 78-114
SAMPLE DUPLICATE: 3681103
92610322001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Oil and Grease
mg/L
NO
1.2J
Results presented on this page are in the units indicated by the "Units' column except wlmre an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 34

aceAnaljftal e
Mw.peeMeW.eae
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I
QUALITY CONTROL DATA
Project: STORMWATER TESTING
Pace Project No.: 92610035
QC Batch: 707112 Analysis Method: EPA 245.1 Rev 3.0 1994
OC Batch Method: EPA 245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92610035001, 92610035002
Pace Analyt cal Services, LLC
9800 KnceyAve. Suite too
Huntersville, NC 28078
(704)8759092
METHOD BLANK: 3688665
Matrix:
Water
Associated Lab Samples: 92610035001, 92610035002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
ug/L
ND
0.20
06/28/22 12:36
LABORATORY CONTROL SAMPLE:
3688666
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
ug/L
2.5
2.5
98 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3688667
3688668
MS
MSD
92609856001 Spike
Spike
MS
MSD MS MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result %Rec %Rec Limits RPD Qual
Mercury ug/L ND 2.5
2.5
2.5
2.5 95 95 70-130 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3688669
3688670
MS
MSD
92611380002 Spike
Spike
MS
MSD MS MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result %Rec %Rec Limits RPD Qua[
Mercury ug/L ND 2.5
2.5
2.4
2.3 94 92 70-130 1
Results presented an this page are in the units indicated by the "Units" column except where an altemate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, L-C.
Page 12 of 34

aceAnalytical'
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I
I
QUALITY CONTROL DATA
Project: STORMWATER TESTING
Pace Project No.: 92610035
QC Batch: 705206 Analysis Method: EPA 200.8 Rev 5.4
QC Batch Method: EPA 200.8 Rev 5.4 Analysis Description: 200.8 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92610035001, 92610035002
METHOD BLANK: 3679784
Associated Lab Samples: 92610035001, 92610035002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
Antimony
ug/L
NO
1.0
06/20/22 03:07
Arsenic
ug/L
NO
1.0
06/20/22 03:07
Beryllium
ug/L
NO
0.10
06/20/22 03:07
Cadmium
ug/L
NO
0.20
06120/22 03:07
Chromium
ug/L
NO
1.0
06/20/22 03:07
Copper
ug/L
NO
2.0
06/20/22 03:07
Lead
ug/L
NO
1.0
06120/22 03:07
Nickel
ug/L
NO
1.0
06/20/22 03:07
Selenium
ug/L
NO
2.0
06/20/22 03:07
Silver
ug/L
NO
0.40
06/20/22 03:07
Thallium
ug/L
NO
0.47
06/20/22 03:07
Zinc
ug/L
NO
10.0
06/20/22 03:07
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3679785
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
50
45.4
91
85-115
Arsenic
ug/L
50
44.7
89
85-115
Beryllium
ug/L
50
46.1
92
85-115
Cadmium
ug/L
50
46.6
93
85-115
Chromium
ug/L
50
46.2
92
85-115
Copper
ug/L
50
46.8
94
85-115
Lead
ug/L
50
48A
96
85-115
Nickel
ug/L
50
46.8
94
85-115
Selenium
ug/L
50
46.3
93
85-115
Silver
ug/L
25
23.5
94
85-115
Thallium
ug/L
25
23.5
94
85-115
Zinc
ug/L
50
46.8
92
85-115
Pace Analytical Services, LLC
9800 Vincey Ave. Suite 100
Hunters lle, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3679786
3679787
MS
MSD
92610278002 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conic.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
NO 50
50
48.5
49.6
95
98
70-130
2
Arsenic
ug/L
1.5 50
50
48.4
50.3
94
98
70-130
4
Beryllium
ug/L
0.14 50
50
47.2
46.8
94
93
70-130
1
Cadmium
ug/L
NO 50
50
48.1
49.4
96
98
70-130
3
Results presented on this Page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, LLC,
Page 13 of 34

aceftljftal
wro�w�ln.rnm
i
QUALITY CONTROL DATA
Project: STORMWATER TESTING
Pace Project No.: 92610035
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3679786
3679787
MS
MSD
92610278002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Chromium
ug/L
1.3
50
50
49.0
51.3
95
100
70-130
5
Copper
ug/L
4.0
50
50
68.4
62.6
129
97
70-130
26 RI
Lead
ug/L
ND
50
50
50.4
51.1
101
102
70-130
1
Nickel
ug/L
26.9
50
50
72.4
75.1
91
96
70-130
4
Selenium
ug/L
2.6
50
50
48.7
49.8
92
95
70-130
2
Silver
ug/L
ND
25
25
23.7
24.3
95
97
70-130
2
Thallium
ug/L
ND
25
25
25.2
25.5
99
101
70-130
1
Zinc
ug/L
17.0
50
50
70.0
65.0
106
96
70-130
7
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3679788
MS
92609813020 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3679789
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
50
50
48.0
45.5
96
91
70-130
5
Arsenic
ug/L
0.191
50
50
47.5
45.5
95
91
70-130
4
Beryllium
ug/L
0.074.1
50
50
44.8
43.8
90
87
70-130
2
Cadmium
ug/L
ND
50
50
48.5
47.2
97
94
70-130
3
Chromium
ug/L
3.0
50
50
51.7
49.8
97
94
70-130
4
Copper
ug/L
ND
50
50
48.3
47.2
95
93
70-130
2
Lead
ug/L
ND
50
50
50.2
48.3
100
97
70-130
4
Nickel
ug/L
4.3
50
50
52.0
50.9
95
93
70-130
2
Selenium
ug/L
ND
50
50
46.6
46.6
93
93
70-130
0
Silver
ug/L
ND
25
25
23.8
22.8
95
91
70-130
4
Thallium
ug/L
ND
25
25
24.6
23.6
98
94
70-130
4
Zinc
ug/L
2.8J
50
50
50.2
49.0
95
93
70-130
2
Results presented on this page are in the units Indicated by the "Units" column except wnem an alternate uun is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/3012022 03:02 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 34

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Project: STORMWATER TESTING
Pace Project No.: 92610035
OC Batch: 704964
OC Batch Method: EPA 624.1
Associated Lab Samples: 92610035001, 92610035002
QUALITY CONTROL DATA
Analysis Method: EPA 624.1
Analysis Description: 624 MSV with Acrolein
Laboratory: Pace Analytical Services - Charlotte
METHOD BLANK: 3678373
Associated Lab Samples: 92610035001, 92610035002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1,1-Trichlomethane
ug/L
ND
2.0
06/16/22 13:08
1,1,2,2-Tetrachloroethane
ug/L
NO
2.0
06/16/22 13:08
1.1,2-Trichloroethane
ug/L
NO
2.0
06/162213:08
1,1-Dichloroethane
ug/L
NO
2.0
06/16/22 13:08
1,1-Dichloroelhene
ug/L
NO
2.0
06/16/22 13:08
1.2-Dichlorobenzene
ug/L
NO
2.0
06/16/22 13:08
1,2-Dichloroelhane
ug/L
NO
2.0
06/162213:08
1,2-Dichloropropane
ug/L
NO
2.0
06116/2213:08
1,3-Dichlorobenzene
ug/L
NO
2.0
061162213:08
1,4-Dichlorobenzene
ug/L
NO
2.0
06/1612213:08
2-Chloroethylvinyl ether
ug/L
NO
5.0
06/16/22 13:08
Acrolein
ug/L
NO
6.0
06/16/22 13:08
Acrylonitrile
ug/L
NO
5.0
06116/2213:08
Benzene
ug/L
NO
1.0
06116/22 13:08
Bromodichloromethane
ug/L
NO
2.0
06/16/22 13:08
Bromoform
ug/L
NO
2.0
06116/2213:08
Bromomethane
ug/L
NO
2.0
061162213:08
Carbon tetrachloride
ug/L
NO
2.0
06/16/22 13:08
Chlorobenzene
ug/L
NO
2.0
06/16/22 13:08
Chloroethane
ug/L
NO
2.0
06/16/22 13:08
Chloroform
ug/L
NO
2.0
06116/2213:08
Chloromethane
ug/L
NO
2.0
06116/2213:08
cis-1,2-Dichloroethene
ug/L
NO
2.0
06/162213:08
ds-1,3-Dichloropropene
ug/L
NO
2.0
06/16/22 13:08
Dibromochloromethane
ug/L
NO
2.0
06/16/22 13:08
Ethylbenzene
ug/L
NO
1.0
06116/22 13:08
Hexachloro-1,3-butadiene
ug/L
NO
5.0
06/16/22 13:08
Methylene Chloride
ug/L
NO
2.0
06/16/22 13:08
Naphthalene
ug/L
NO
5.0
06/16/22 13:08
Telrachloroethene
ug/L
NO
2.0
06116/2213:08
Toluene
ug/L
NO
1.0
06/16/22 13:08
trans-1,2-Dichloroethene
ug/L
NO
2.0
06/16/22 13:08
trans-1,3-Dichloropropene
ug/L
NO
2.0
061162213:08
Trichloroethene
ug/L
NO
2.0
06/1W213:08
Vinyl chloride
ug/L
NO
2.0
06/16/22 13:08
1,2-Dichloroethane-d4 (S)
%
102
70-130
06/16/22 13:08
4-Bromofluorobenzene (S)
%
105
70-130
06/16/22 13:08
Toluene-08 (S)
%
104
70-130
06/16/22 13:08
Qualifiers
Pace Analytical Services, LLC
9800 Kinsey Ave. Sutte 100
Hunlersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except whom an anemate unit is presentee to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 34

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QUALITY CONTROL DATA
Project: STORMWATER TESTING
Pace Project No.: 92610035
LABORATORY CONTROL SAMPLE:
Parameter
3678374
Units
Spike
Conc.
LCS
Result
LCS
% Rec
%Rec
Limits
1,1,1-Trichloroethane
ug/L
20
16.6
83
70-130
1,1,2,2-Tetrachloroethane
ug/L
20
15.7
79
70-130
1,1,2-Trichloroethane
ug/L
20
17.6
88
70-130
1,1-Dichloroethane
ug/L
20
17.6
88
70-130
1,1-Dichloroethene
ug/L
20
17.5
87
70-132
1,2-Dichlorobenzene
ug/L
20
17.2
86
70-130
1,2-Dichloroethane
ug/L
20
17.4
87
70-130
1,2-Dichloropropane
ug/L
20
17.7
88
70-130
1,3-Dichlorobenzene
ug/L
20
17.5
87
70-130
1,4-Dichlombenzene
uglL
20
16.9
84
70-130
2-Chloroethylvinyl ether
ug/L
40
31.3
78
67-130
Acrolein
ug/L
100
96.6
97
60-140
Acrylonitrile
ug/L
100
87.9
88
70-130
Benzene
ug/L
20
16.7
84
70-130
Bromodichloromethane
ug/L
20
18.3
91
70-130
Bromofonn
ug/L
20
14.5
72
70-130
Bromomelhane
ug/L
20
16.5
82
30-177
Carbon tetrachloride
ug/L
20
17.4
87
70-130
Chlorobenzene
ug/L
20
16.3
82
70-130
Chlomethane
ug/L
20
18.9
94
46-131
Chloroform
ug/L
20
17.2
86
70-130
Chloromethane
ug/L
20
17.2
86
49-130
as-1,2-Dichloroethene
ug/L
20
17.6
88
70-130
cis-1,3-Dichloropropene
ug/L
20
17.8
89
70-130
Dibromochloromethane
ug/L
20
15.9
79
70-130
Ethylbenzene
ug/L
20
16.2
81
70-130
Hexachloro-1,3-butadiene
ug/L
20
15.3
77
70-131
Methylene Chloride
ug/L
20
17.4
87
68-130
Naphthalene
ug/L
20
17.6
88
70-133
Tetrachloroelhane
ug/L
20
15.5
77
70-130
Toluene
ug/L
20
17.5
88
70-130
trans-1,2-Dichloroethene
ug/L
20
16.9
85
70-130
trans-1,3-Dichloropropene
ug/L
20
16.9
85
70-130
Trichloroethene
ug/L
20
17.6
88
70-130
Vinyl chloride
ug/L
20
16.8
84
59-142
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
101
70-130
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 3678376 3678376
MS MSD
92610035001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Cone. Result Result %Rec %Rec Limits RPD Qual
1,1,1-Trichloroethane ug/L NO 20 20 21.5 19.1 108 95 70-148 12
1, 1,2,2-Tetrachloroethane ug/L ND 20 20 16.9 14.8 84 74 70-131 13
Results presented on this page are In the units indicated by the "units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, LLC, Page 16 of 34

aceAnalytical e
rnw.wetlW.wm
QUALITY CONTROL DATA
Pace Analytical services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER TESTING
Pace Project No.: 92610035
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3678375
3678376
MS
MSD
92610035001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1.1,2-Trichloroethane
ug/L
NO
20
20
19.4
16.4
97
82
70-136
17
1,1-Dichloroethane
ug/L
NO
20
20
21.0
17.9
105
89
71-143
16
1,1-Dichloroethene
ug/L
NO
20
20
22.7
20.4
113
102
70-158
11
1,2-Dichlorobenzene
ug/L
NO
20
20
18.9
16.0
95
80
70-133
17
1,2-Dichloroethane
ug/L
NO
20
20
20.1
18.0
101
90
72-137
11
1,2-Dichloropropane
ug/L
NO
20
20
20.6
17.5
103
88
70-138
16
1,3-Dichlorobenzene
ug/L
NO
20
20
19.4
16.4
97
82
75-133
17
1,4-Dichlorobenzene
ug/L
NO
20
20
18.8
15.7
94
78
70-133
18
2-Chloroethylvinyl ether
ug/L
NO
40
40
30.6
27.4
76
69
10-200
11
Acrolein
ug/L
NO
100
100
118
103
118
103
50-150
14
Acrylonitrile
ug/L
NO
100
100
102
90.4
102
90
68-140
12
Benzene
ug/L
NO
20
20
19.6
16.7
98
84
75-125
16
Bromodichloromethane
ug/L
NO
20
20
20.1
17.4
100
87
70-138
14
Bromoform
ug/L
NO
20
20
16.2
14.1
81
71
57-138
14
Bromomethane
ug/L
NO
20
20
13.9
13.5
70
67
10-200
3
Carbon tetrachloride
ug/L
NO
20
20
22.8
19.1
114
95
70-126
18
Chlorobenzene,
ug/L
NO
20
20
18.4
16.1
92
81
82-137
14 M1
Chloroethane
ug/L
NO
20
20
23.0
21.1
115
105
51.166
9
Chloroform
ug/L
NO
20
20
20.7
18.5
103
92
70-121
11
Chloromethane
ug/L
NO
20
20
20.9
18.8
105
94
24-161
11
cis-1,2-Dichloroethene
ug/L
NO
20
20
20.6
18.8
103
94
67-148
9
cis-1,3-Dichloropropene
ug/L
NO
20
20
19.6
16.7
98
84
70-142
16
Dibromochloromethane
ug/L
NO
20
20
18.0
15.4
90
77
69-133
15
Ethylbenzene
ug/L
NO
20
20
19.0
16.6
95
83
75-134
14
Hexachloro-1,3-butadiene
ug/L
NO
20
20
18.0
14.2
90
71
62-151
24
Methylene Chloride
ug/L
NO
20
20
20.0
17.5
100
87
64-148
14
Naphthalene
ug/L
NO
20
20
16.6
14.8
83
74
57-150
12
Tetrachloroethene
ug/L
NO
20
20
19.0
16.4
95
82
70-133
15
Toluene
ug/L
NO
20
20
19.6
17.3
96
85
75-134
12
trans-1,2-Dichloroethene
ug/L
NO
20
20
21.5
19.1
107
96
70-143
12
trans-1,3-Dichloropropene
ug/L
NO
20
20
18.9
16.5
94
83
70-138
13
Trichloroethene
ug/L
NO
20
20
20.9
18.4
104
92
75-138
13
Vinyl chloride
ug/L
NO
20
20
22.1
19.1
110
96
55-172
15
1,2-Dichloroethane-d4 (S)
%
103
108
70-130
4-Bromofluorobenzene (S)
%
100
100
70-130
Toluene-d8(S)
%
102
101
70-130
Results presented on this page are In the units Indicated by the 'Units' column except ehen, an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 34

aceAnalXical
wrpecYeMsgn
QUALITY CONTROL DATA
Project: STORMWATER TESTING
Pace Project No.: 92610035
QC Batch: 706808 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92610035001, 92610035002
METHOD BLANK: 3682472
Associated Lab Samples: 92610035001, 92610035002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1.2,4-Trichlorobenzene
ug/L
ND
5.0
06/21/22 13:20
12-Diphenylhydrazine
ug/L
ND
5.0
06121/22 13:20
2,4,6-Tdchlorophenol
ug/L
ND
10.0
06/21/22 13:20
2,4-Dichlorophenol
ug/L
ND
&0
06/21/22 13:20
2,4-Dimethylphenol
ug/L
ND
10.0
06/2112213:20
2,4-Dinitrophenol
ug/L
NO
50.0
06/212213:20
2,4-Dinitrotoluene
ug/L
NO
5.0
06121/22 13:20
2,6-Dinitrotoluene
ug/L
NO
5.0
06/2112213:20
2-Chloronaphthalene
ug/L
NO
5.0
06/2122 13:20
2-Chlorophenol
ug/L
NO
5.0
06/212213:20
2-Nitrophenol
ug/L
NO
5.0
061212213:20
3.3'-Dichlorobenzidine
ug/L
NO
10.0
06/21/22 13:20
4,6-Dinitro-2-methylphenol
ug/L
NO
10.0
06/212213:20
4-Bromophenylphenyl ether
ug/L
NO
5.0
06/2122 13:20
4-Chloro-3-methylphenol
ug/L
NO
5.0
06/212213:20
4-Chlorophenylphenyl ether
ug/L
NO
6.0
06/21/22 13:20
4-Nitrophenol
ug/L
NO
10.0
06/21/22 13:20
Acenaphthylene
ug/L
NO
5.0
06/21/22 13:20
Anthracene
ug/L
NO
5.0
06/21/22 13:20
Benzidine
ug/L
ND
50.0
06121/22 13:20
Benzo(a)anthracene
ug/L
ND
5.0
06/21/22 13:20
Benzo(a)pyrene
ug/L
ND
5.0
06121/22 13:20
Benzo(b)fluoranthene
ug/L
ND
5.0
06/21/22 13:20
Benzo(g,h,i)perylene
ug/L
NO
5.0
06121/22 13:20
Benzo(k)fluoranthene
ug/L
NO
5.0
06121/22 13:20
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
0612112213:20
bis(2-Chloroethyl) ether
ug/L
NO
5.0
06121/22 13:20
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
06/21/22 13:20
Butylbenzylphthalate
ug/L
NO
5.0
0612112213:20
Chrysene
ug/L
NO
5.0
06/21/22 13:20
Di-n-butylphthalate
ug/L
NO
5.0
06/21/22 13:20
Di-n-octylphthalate
ug/L
NO
5.0
06121/22 13:20
Dibenz(a,h)anthracene
ug/L
ND
5.0
06121/22 13:20
Diethylphthalate
ug/L
NO
5.0
06121/22 13:20
Dimethylphthalate
ug/L
ND
5.0
06121/22 13:20
Fluoranthene
ug/L
NO
5.0
06/2112213:20
Fluorene
ug/L
ND
5.0
06121/22 13:20
Hexachloro-1,3-butadiene
ug/L
ND
5.0
0612112213:20
Hexachlorobenzene
ug/L
NO
5.0
06/2112213:20
Hexachlorocyclopentadiene
ug/L
NO
10.0
06/21/22 13:20
Qualifiers
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, L-C. Page 18 of 34

aceAnalXical e
www.pscNe6s.csre
QUALITY CONTROL DATA
Project: STORMWATER TESTING
Pace Project No.: 92610035
METHOD BLANK: 3682472
Matrix:
Water
Associated Lab Samples: 92610035001, 92610035002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Hexachloroethane
ug/L
NO
5.0
06/21/2213:20
Indeno(1,2,3-cd)pyrene
ug/L
NO
5.0
06/2112213:20
Isophorone
ug/L
NO
10.0
06/21/2213:20
N-Nitroso-di-n-propylamine
ug/L
NO
5.0
06/21/2213:20
N-Nitrosodimethylamine
ug/L
NO
5.0
06121/2213:20
N-Nitrosodiphenylamine
ug/L
NO
10.0
06/2112213:20
Naphthalene
ug/L
NO
5.0
06121/2213:20
Nitrobenzene
ug/L
NO
5.0
06/212213:20
Pentachlorophenol
ug/L
NO
10.0
06/21/2213:20
Phenanthrene
ug/L
NO
5.0
06/21/2213:20
Phenol
ug/L
NO
5.0
06121/2213:20
Pyrene
ug/L
NO
5.0
06121/2213:20
2,4,6-Tribromophenol(S)
%
86
10-137
06/21/22 13:20
2-Fluorobiphenyl(S)
%
71
15-120
06121/22 13:20
2-Fluorophenol (S)
%
63
10-120
06/21/22 13:20
Nitrobenzene-d5 (S)
%
85
10-120
06/21/22 13:20
Phenol-d6 (S)
%
64
10-120
06/21/22 13:20
Terphenyl-d14 (S)
e/
136
11-131
06/2112213:20 S3
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
HuntersNlle, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
3682473
Units
Spike
Conic.
LCS
Result
LCS
%Rec
%Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
14.1
28
44-142 L2
1,2-Diphenylhydrazine
ug/L
50
84.8
170
25-150 L1
2,4,6-Trichlorophenol
ug/L
50
73.7
147
37-144 Lt
2,4-Dichlorophenol
ug/L
50
57.5
115
1-191
2,4-Dimelhylphenol
ug/L
50
73.8
148
32-119 L1
2,4-Dinitrophenol
ug/L
250
380
152
1-181
2,4-Dinitrotoluene
ug/L
50
83.5
167
39-139 L1
2,6-Dinitrotoluene
ug/L
50
83.0
166
50-158 L1
2-Chloronaphthalene
ug/L
50
48.1
96
60-118
2-Chlorophenol
ug/L
50
55.1
110
23-134
2-Nitrophenol
ug/L
50
60.5
121
29-182
33-Dichlorobenzidine
ug/L
100
166
166
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
149
149
1-181
4-Bromophenylphenyl ether
ug/L
50
69.0
138
53-127 L1
4-Chloro-3-methylphenol
ug/L
100
163
163
22-147 Lt
4-Chlorophenylphenyl ether
ug/L
50
62.4
125
25-158
4-Nitrophenol
ug/L
250
255
102
1-132
Acenaphthylene
ug/L
50
59.2
118
33-145
Anthracene
ug/L
50
63.2
126
1-166
Benzidine
ug/L
100
53.4
53
10-130
Benzo(a)anthracene
ug/L
50
73.0
146
33-143 L1
Benzo(a)pyrene
ug/L
50
83.8
168
17-163 L1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, U.C. Page 19 of 34

aceAnalytical
rwr.pecYehssgm
QUALITY CONTROL DATA
Project: STORMWATER TESTING
Pace Project No.: 92610035
Pace Analytical Services, LLC
980010ncey Ave. Suite 100
Huntersville, NC 28078
(/04)875-9092
LABORATORY CONTROL SAMPLE:
Parameter
3682473
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Benzo(b)0uoranthene
ug/L
50
90.6
181
24-159 Ll
Benzo(g,h,i)perylene
ug/L
50
83.2
166
1-219
Benzo(k)fiuoranthene
ug/L
50
77.1
154
11-162
bis(2-Chloroethoxy)methane
ug/L
50
64.2
128
33-184
bis(2-Chloroethyp ether
ug/L
50
52.9
106
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
94.0
188
8-158 L1
Butylbenzylphthalate
ug/L
50
97.2
194
1-152 L1
Chrysene
ug/L
50
67.4
135
17-168
Di-n-butylphthalate
ug/L
50
81.5
163
1-118 L1
Di-n-octylphthalate
ug/L
50
96.6
193
4-146 Ll
Dibenz(a,h)anthracene
ug/L
50
82.9
166
1-227
Diethylphthalate
ug/L
50
72.0
144
1-114 L1
Dimethylphthalate
ug/L
50
70.1
140
1-112 L1
Fluoranthene
ug/L
50
72.3
145
26-137 Ll
Fluorene
ug/L
50
64.6
129
59-121 L1
Hexachloro-1,3-butadiene
ug/L
50
4.5J
9
24-116 L2
Hexachlorobenzene
ug/L
50
62.2
124
1-152
Hexachlorocyclopentadiene
ug/L
50
17.8
36
25-150
Hexachlomethane
ug/L
50
4.9J
10
40-113 L2
Indeno(1,2,3-od)pyrene
ug/L
50
85.0
170
1-171
Isophorone
ug/L
50
55.6
111
21-196
N-Nltroso-di-n-propylamine
ug/L
50
66.5
133
1-230
N-Nitrosodimethylamine
ug/L
50
42.0
84
25-150
N-Nitrosodiphenylamine
ug/L
50
71.5
143
25-150
Naphthalene
ug/L
50
28.2
56
21-133
Nitrobenzene
uglL
50
55.6
111
35-180
Pentachlorophenol
ug/L
100
157
157
14-176
Phenanthrene
ug/L
50
67.7
135
54-120 L1
Phenol
ug/L
50
54.4
109
5-112
Pyrene
ug/L
50
76.2
152
52-115 L1
2,4,6-Tribromophenol (S)
%
160
10-137 SO
2-Fluorobiphenyl(S)
%
67
15-120
2-Fluorophenol(S)
%
83
10-120
Nitrobenzene-d5(S)
%
109
10-120
Phenol-d6 (S)
%
102
10-120
Terphenyl-d14(S)
%
162
11-131 SO
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3682474
3682475
MS
MSD
92605561013 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,2,4-Tdchlorobenzene
ug/L
ND 50
50
18.5
13.1
37
26
44-142
34 MO,Rl
1,2-Diphenylhydrazine
ug/L
ND 50
50
72.0
67.5
144
115
25-150
22
2,4,6-Tnchlorophenol
ug/L
ND 50
50
34.3
37.3
69
75
37-144
8
2,4-Dichlorophenol
ug/L
NO 50
50
43.7
36.6
87
73
1-191
18
Results presented on this page are In the units Indicated by the "Units' column except then an alternate unit Is presented to the right of the mount.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, U.C. Page 20 of 34

aceAnalXical
ww.paaNaM.um
I
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suke 190
Huntersville, NC 28078
[phone]
Project: STORMWATER TESTING
Pace Project No.: 92610035
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3682474
3682475
MS
MSD
92605561013
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
2,4-Dimethylphenol
ug/L
NO
50
50
63.3
46.9
127
94
32-119
30 MO
2,4-Dinitrophenol
ug/L
NO
250
250
NO
26.6.1
7
11
1-181
2,4-Dinitrotoluene
ug/L
NO
50
50
74.2
60.5
148
121
39-139
20 MO
2,6-Dinitrotoluene
ug/L
NO
50
50
75.7
60.7
151
121
50-158
22
2-Chloronaphthalene
ug/L
NO
50
50
52.5
36.3
105
73
60-118
36 R1
2-Chlorophenol
ug/L
NO
50
50
41.9
37.5
84
75
23-134
11
2-Nitrophenol
ug/L
NO
50
50
44.8
39.8
90
80
29-182
12
3,3'-Dichlorobenzidine
ug/L
NO
100
100
143
121
143
121
1-262
16
4,6-Dinitro-2-methylphenol
ug/L
NO
100
100
21.1
31.6
21
32
1-181
40 R1
4-Bromophenylphenyl ether
ug/L
NO
50
50
60.1
49.4
120
99
53-127
20
4-Chloro-3-methylphenol
ug/L
NO
100
100
137
107
137
107
22-147
24
4-Chlorophenylphenyl ether
ug/L
NO
50
50
55.1
44.3
110
89
25-158
22
4-Nitrophenol
ug/L
NO
250
250
36.1
46.8
14
19
1-132
26
Acenaphthylene
ug/L
NO
50
50
55.7
42.9
ill
86
33.145
26
Anthracene
ug/L
NO
50
50
56.2
46.6
112
93
1-166
19
Benzidine
ug/L
NO
100
100
38.3J
57.7
38
58
10-130
Benzc(a)anthracene
ug/L
NO
50
50
69.0
66.6
138
113
33-143
20
Benzo(a)pyrene
ug/L
NO
50
50
76.0
62.9
152
126
17-163
19
Benzc(b)fluoranthene
ug/L
NO
50
50
81.4
62.7
163
125
24-159
26 MO
Benzo(g,h,i)perylene
ug/L
NO
50
50
88.4
72.3
177
145
1-219
20
Benzo(k)fluoranthene
ug/L
NO
50
50
68.6
58.0
137
116
11-162
17
bis(2-Chloroethoxy)methane
ug/L
NO
50
50
53.0
41.9
106
84
33-184
24
bis(2-Chloroethyl) ether
ug/L
NO
50
50
47.5
40.2
95
80
12-158
17
bis(2-Ethylhexyl)phthalate
ug/L
NO
50
50
88.1
69.8
176
140
8-158
23 MO
Butylbenzylphthalate
ug/L
NO
50
50
91.2
70.3
182
141
1-152
26 MO
Chrysene
ug/L
NO
50
50
61.1
49.7
122
99
17-168
21
Di-n-butylphthalale
ug/L
NO
50
50
70.3
62.1
141
124
1-118
12 MO
Di-n-octylphthalate
ug/L
NO
50
50
87.5
73.1
175
146
4-146
18 MO
Dibenz(a,h)anthracene
ug/L
NO
50
50
89.8
73.6
180
147
1-227
20
Diethylphthalate
ug/L
NO
50
50
65.3
54.5
131
109
1-114
18 MO
Dimethylphthalate
ug/L
NO
50
50
62.3
50.8
125
102
1-112
20 MO
Fluoranthene
ug/L
NO
50
50
61.1
53.1
122
106
26-137
14
Fluorene
ug/L
NO
50
50
61.7
47.2
123
94
59-121
27 MO
Hexachloro-1,3-butadiene
ug/L
NO
50
50
7.7
6.7
15
13
24-116
13 MO
Hexachlorobenzene
ug/L
NO
50
50
53.9
44.8
108
90
1-152
18
Hexachlorocyclopentadiene
ug/L
NO
50
50
25.1
13.6
50
27
25-150
60 R1
Hexachloroethane
ug/L
NO
50
50
6.7
9.7
13
19
40-113
37 MO,R1
Indeno(1,2,3-cd)pyrene
ug/L
NO
50
50
85.6
71.7
171
143
1-171
18
Isophorone
ug/L
NO
50
50
46.7
37.1
93
74
21-196
23
N-Nitroso-di-n-propylamine
ug/L
NO
50
50
55.4
45.8
ill
92
1-230
19
N-Nitrosodimelhylamine
ug/L
NO
50
50
40.0
30.2
80
60
25-150
28
N-Nitrosodiphenylamine
ug/L
NO
50
50
63.0
52.3
126
105
25-150
19
Naphthalene
ug/L
NO
50
50
29.5
22.0
59
44
21-133
29
Nitrobenzene
ug/L
NO
50
50
47.6
38.9
95
78
35-180
20
Pentachlorophenol
ug/L
NO
100
100
41.3
57.9
41
58
14-176
33 R1
Phenanthrene
ug/L
NO
50
50
59.7
52.5
119
105
54-120
13
Results presented on this page am In
the units indicated by the
"Units" column
except where
an altemete unit Is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, L-C. Page 21 of 34

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QUALITY CONTROL DATA
Project: STORMWATER TESTING
Pace Project No.: 92610035
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntewiffe, NC 28078
[phone]
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE:
3682474
3682475
MS
MSD
92605561013 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conic.
Conic,
Result
Result
% Rec
% Rec
Limits RPD Qual
Phenol
ug/L
ND 50
50
46.3
36.5
93
73
5-112 24
Pyrene
ug/L
ND 50
50
71.2
58.3
142
117
52-116 20 MO
2,4,6-Tribromophenol(S)
%
96
102
10-137
2-Fluorobiphenyl (S)
%
79
55
15.120
2-Fluorophenol(S)
%
56
53
10-120
Nitrobenzene-d5(S)
%
103
84
10-120
Phenol-d6 (S)
%
89
68
10-120
Terphenyl-d14(S)
%
141
113
11-131 SO
Results presented an this page am In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, LLC.
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I
QUALITY CONTROL DATA
Project: STORMWATER TESTING
Pace Project No.: 92610035
QC Batch: 705096 Analysis Method: SM 2540D-2015
OC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92610035001, 92610035002
METHOD BLANK: 3679503 Matrix: Water
Associated Lab Samples: 92610035001, 92610035002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L NO 2.5 06/17/22 %55
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite too
Huntersville, NC 28078
Q04i87S9092
LABORATORY CONTROL SAMPLE: 3679504
Spike 1-CS 1-CS % Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 250 100 90-110
SAMPLE DUPLICATE: 3679980
92610057001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 274 290 6
SAMPLE DUPLICATE: 3679981
92610017001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 2960 2440 19
Results presented on this page am In Me unite indicated by the'0n8s' column except when an alternate unn Is presented to the dent of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/30/2022 03:02 PM without the wr iten consent or Pace Analytical Services, L-C. Page 23 of 34

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Project:
STORMWATER TESTING
Pace Project No.:
92610035
OC Batch:
705430
QC Batch Method:
SM 4500-S2D-2011
Associated Lab Samples: 92610035001, 92610035002
METHOD BLANK: 3680961
Associated Lab Samples: 92610035001, 92610035002
Parameter Units
Sulfide mg/L
QUALITY CONTROL DATA
Analysis Method: SM 4500-S2D-2011
Analysis Description: 4500S2D Sulfide Water
Laboratory: Pace Analytical Services - Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 06/18/22 04:20
Pace Ana"cal services, LLC
98001Gncey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
LABORATORY CONTROL SAMPLE: 3680962
Spike LCS LCS % Rec
Parameter Units Conic. Result % Rec Limits Qualifiers
Sulfide mg/L 0.5 0.51 102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3680963
3680964
MS
MSD
92610068003 Spike
Spike
MS
MSD MS MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result % Rec % Rec Limits RPD Qual
Sulfide mg/L NO 0.5
0.5
0.49
0.50 96 97 80-120 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3680976 3680977
MS MSD
92609832007 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfide mg/L 0.0511 0.5 0.5 0.51 0.52 92 95 80-120 3
Results presented on this page are in the units Indicated by the'Uniti column except where an alternate una Is presaMed to the r19M of the ri
REPORT OF LABORATORY ANALYSIS
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Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, L-C.
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I
QUALITY CONTROL DATA
Project: STORMWATER TESTING
Pace Project No.: 92610035
OC Batch: 706750 Analysis Method: EPA 9040C
OC Batch Method: EPA 9040C Analysis Description: 9040 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92610035001, 92610035002
SAMPLE DUPLICATE: 3686985
92610035001
Cup
Parameter
Units
Result
Result RPD Qualifiers
pH at 25 Degrees C
Std. Units
7.3
7.4 1 H3
SAMPLE DUPLICATE: 3687263
92610501001
Dup
Parameter
Units
Result
Result RPD Qualifiers
pH at 25 Degrees C
Std. Units
7.7
7.7 0 H3
Pace Analytical Services, LLC
98001Wcey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on Nis page am in Me units Indicated! by Me'Unib' column except wlwm an atmmate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, L-C.
Page 25 of 34

aceAnaljftal
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i
QUALITY CONTROL DATA
Project: STORMWATER TESTING
Pace Project No.: 92610035
QC Batch: 705083 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92610035001, 92610035002
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)87b9092
METHOD BLANK: 3679458
Matrix: Water
Associated Lab Samples: 92610035001, 92610035002
Blank
Reporting
Parameter
Units
Result
Limit Analyzed Qualifiers
Sulfate
mg/L
ND 1.0 06/16/22 23:27
LABORATORY CONTROL SAMPLE:
3679459
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Sulfate
mg/L
50
49.5 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3679460 3679461
MS MSO
92609726001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 5.0 50 50 54.5 57.1 99 104 90-110 5
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3679462
3679463
MS
MSD
92609808005 Spike
Spike
MS
MSD
MS MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result
e/ Rec % Rec Limits RPD Qua[
Sulfate mg/L 70.6 50
50
102
102
63 63 90-110 0 Mt
Results presented on this page am in me units Indicated by Me'Unib' column except where an aitemate unit is presented to the right of the resulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, I.I.C.
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I
Project: STORMWATER TESTING
Pace Project No.: 92610035
QC Batch: 833869
QC Batch Method: EPA 335.4
Associated Lab Samples: 92610035001, 92610035002
METHOD BLANK: 4583767
Associated Lab Samples: 92610035001, 92610035002
Parameter Units
Cyanide mg/L
LABORATORY CONTROL SAMPLE: 4583768
Parameter Units
Cyanide mg/L
Pace Anatytical services, LLC
9800 K inceyAve. Suite 100
Hunters°ille, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 335.4
Analysis Description: 335.4 Cyanide, Total
Laboratory: Pace Analytical Services - Ormond Beach
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 0.010 06/2212213:36
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
0.05 0.050 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4584235 4584236
MS MSD
35725475001 Spike Spike MS MSD MS MSD °% Rec
Parameter Units Result Conc. Conc. Result Result °% Rec % Rec Limits RPD Qual
Cyanide mg/L 0.0050 0.025 0.025 0.024 0,025 96 99 90-110 3
U
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4584237
4584238
MS
MSD
35725833001 Spike
Spike
MS
MSD
MS MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result
°%Rec %Rec Limits RPD Dust
Cyanide mg/L 0.0050 0.025
0.025
0.023
0.023
90 93 90-110 3
U
Results presented on this page are in the units Indicated by the "Units' column except whereas altamate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, L-C.
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ZeAnal
yNcal
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Humersaille, NC 28078
[phone]
Project: STORMWATER TESTING
Pace Project No.: 92610035
QC Batch: 705823
Analysis Method: EPA 420.4 Rev 1.0 1993
QC Batch Method: EPA 420.4 Rev 1.0 1993
Analysis Description: 420.4 Phenolics
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92610035001
METHOD BLANK: 3682516
Matrix: Water
Associated Lab Samples: 92610035001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Phenolics, Total Recoverable mg/L
NO 0.020
06/22/22 14:47
LABORATORY CONTROL SAMPLE: 3682517
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Phenolics, Total Recoverable mg/L
0.05 0.051
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3682518 3682519
MS MSD
35724780001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qua]
Phenolics, Total Recoverable mg/L 0.0076
0.05 0.05 0.046
0.043 87 81
90-110 8 M1
U
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3682520 3682521
MS MSD
35724780002
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Phenolics, Total Recoverable mg/L 0.0076
0.05 0.05 0.046
0.047 93 95
90-110 2
U
Results presented on this page are in the units indicated by the "Units" column except "Oman alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, L-C.
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I
Project:
STORMWATER TESTING
Pace Project No.:
92610035
QC Batch:
707178
QC Batch Method:
EPA 420.4 Rev 1.0 1993
Associated Lab Samples: 92610035002
METHOD BLANK: 3688907
Associated Lab Samples: 92610035002
Parameter Units
Phenolics, Total Recoverable mg/L
LABORATORY CONTROL SAMPLE: 3688908
Parameter Units
Phenolics, Total Recoverable mg/L
Pace Analytical Services, LLC
9600 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 420.4 Rev 1.0 1993
Analysis Description: 420.4 Phenolics
Laboratory: Pace Analytical Services -Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 0.020 06/30/22 11:53
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
0.05 0.062 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3688909 3688910
MS MSD
92610035002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phenolics, Total Recoverable mg/L ND 0.05 0.05 0.087 0.084 167 161 90-110 4 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3688911
3688912
MS
MSD
357248270012
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits RPD Qual
Phenolics, Total Recoverable mg/L
ND
0.05
0.05
0.099
0.093
193 180
90-110 7 Mt
Results presented on this page are in the units indicated by the 'Units' column except where an ademate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2022 03:02 PM without the written consent of Pace Analytical Services, U.C.
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I
QUALIFIERS
Project: STORMWATER TESTING
Pace Project No.: 92610035
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL- Practical Ouanlitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitdle by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
Ll Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded OC limits. Balch accepted based on laboratory control sample (LCS) recovery.
Ri RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
STORMWATER TESTING
92610035
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92610035001
Al
EPA 1664B
705466
92610035002
A2
EPA 1664B
705466
92610036001
Al
EPA 200.8 Rev 6.4
705206
EPA 200.8 Rev 5.4
705370
92610035002
A2
EPA 200.8 Rev 5.4
705206
EPA 200.8 Rev 5.4
705370
92610035001
At
EPA 245.1 Rev 3.0 1994
707112
EPA 245.1 Rev 3.0 1994
707315
92610035002
A2
EPA 245.1 Rev 3.0 1994
707112
EPA 245.1 Rev 3.0 1994
707315
92610035001
At
EPA 625.1
705808
EPA 625.1
705957
92610035002
A2
EPA 625.1
705808
EPA 625.1
705957
92610035001
Al
EPA 624.1
704964
92610035002
A2
EPA 624.1
704964
92610035001
At
SM 2WO-2015
705096
92610035002
A2
SM 254OD-2015
705096
92610035001
At
SM 4500-S2D-2011
705430
92610035002
A2
SM 4500-S2D-2011
705430
92610035001
At
EPA 9040C
706750
92610035002
A2
EPA 9040C
706750
92610035001
At
EPA 300.0 Rev 2.1 1993
705083
92610035002
A2
EPA 300.0 Rev 2.1 1993
705083
92610035001
At
EPA 335.4
833869
EPA 335.4
833992
92610035002
A2
EPA 335.4
833869
EPA 335.4
833992
92610035001
Al
EPA 420.4 Rev 1.0 1993
705823
EPA 420.4 Rev 1.0 1993
706016
92610035002
A2
EPA 420.4 Rev 1.0 1993
707178
EPA 420.4 Rev 1.0 1993
707732
Date: 06/30/2022 03:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall nor be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 34

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Person contacted - Da[e/Tlmet
Project Manager SCURF Review: Oete
Qualtrax ID:69614
Page 1 of 2
Page 32 0134

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Effective Date: 051121202205/12/2022
*Check mark top half of box if pH and/or dechlorination is verified and
within the acceptance range for preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHB
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
.o;an. WO#:92610035
PM: Silo Due Date: 06/29/22
CLIENT: 92-Am Truet=
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot d
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Out of hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax ID: 69614 Page 2 of 2 Page 33 of 34

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Page 34 of 34