NCG100024_2022 DMR_20220623

46
Mid Atlantic
Experienced. Customer Focused. Innovative.
REPORT DATE: May 6, 2022
PROJECT NO: R2066.04
STORMWATER SAMPLING
RESULTS
Foss Recycling Inc
1915 Riddle Road, Durham, Durham County, North Carolina
ENGINEERING & ENVIRONMENTAL SOLUTIONS
PREPARED FOR: PREPARED BY -
Foss Recycling Inc. MID ATLANTIC ASSOCIATES, INC.
1915 Riddle Road 409 Rogers View Court,tRIeigh, NC 27610
Durham, NC 27713 919.250.99181 MAAON€ CQ[yl
���� Atlantic

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG100000
Used Motor Vehicles
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG10 00024 Person Collecting Samples:
Facility Name: Foss Recycling Inc. Laboratory Name: Pace Analytical
Facility County: Durham Laboratory Cert. No.: 12
Discharge during this period: U Yes Lj No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? Dyes 0 No
If so, which Tier (I, II, or III)?
A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR Yes ❑ No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Redl
Parameter
Code
Parameter
Outfall 01
Outfall
Outfall
Outfall
Outfall
N/A
Receiving Stream Class
WS-V;NSW
N/A
Date Sample Collected MM/DD/YYYY
04/19/2022
46529
24-Hour Rainfall in inches
0.24
C0530
TSS in mg/L (100 or 50*)
10.3
00400
pH in standard units (6.0-9.0 FW,
7.1
6.8 — 8.5 SW)
00340
Chemical Oxygen Demand in mg/L
(120)
N/A
01051
Lead, total recoverable (as Pb) in
<0.005
mg/ L (0.075 FW, 0.22 SW)
Ethylene Glycol in mg/ L (any amount
77023
detected Tier One; 8,000 mg/L Tier
<5.0
Two and Three)
00552
Non -Polar Oil & Grease in mg/L (15)
<5.0
NCOIL
Estimated New Motor/Hydraulic Oil
Usage in gal/month
N/A
' outtalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L
FW (Freshwater) SW (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations."
Signature
Email
Authorized Individual
e,�
Date
9i�- /.40C
Phone Number

aceAna1jdka1
www.poeNobi.com
May 05, 2022
Chuck Hoffman
Mid -Atlantic Associates, Inc
409 Rogers View Court
Raleigh, NC 27610
RE: Project: FOSS RECYCLING INC DURHAM
Pace Project No.: 92600072
Dear Chuck Hoffman:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 20, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Indianapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Ron Davis, Mid Atlantic Associatees, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

aceAnalytical
ww.p&Wabs.com
Project: FOSS RECYCLING INC DURHAM
Pace Project No.: 92600072
Pace Analytical Services Indianapolis
7726 Moller Road, Indianapolis, IN 46268
Illinois Accreditation #: 200074
Indiana Drinking Water Laboratory #: C49-06
Kansas/TNI Certification #: E-10177
Kentucky UST Agency Interest #: 80226
Kentucky WW Laboratory ID #: 98019
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
Michigan Drinking Water Laboratory #9050
Ohio VAP Certified Laboratory #: CL0065
Oklahoma Laboratory #: 9204
Texas Certification #: T104704355
Wisconsin Laboratory #: 999788130
USDA Soil Permit #: P330-19-00257
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 13

ace malytical
www.pacslabs.com
Project: FOSS RECYCLING INC DURHAM
Pace Project No.: 92600072
Lab ID Sample ID
92600072001 OUTFALL NO 1
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-I = Pace Analytical Services - Indianapolis
SAMPLE ANALYTE COUNT
Method
Analysts
EPA 1664B
ICO
EPA 8015 Alcohol -Glycol
CPH
EPA 601 OD
CBV
SM 254OD-2015
MAB2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Reported Laboratory
1 PASI-C
1 PASI-I
1 PASI-A
1 PASI-A
Page 3 of 13

aceAnalj6cal
rrww.psalsbssm
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: FOSS RECYCLING INC DURHAM
Pace Project No.: 92600072
Sample: OUTFALL NO 1 Lab ID: 92600072001 Collected: 04/19/22 14:19 Received: 04/20/22 09:50 Matrix: Water
Parameters Results U t
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
8015M Glycols in water
Ethylene glycol
6010 MET ICP
Lead
2540D Total Suspended Solids
Total Suspended Solids
Date: 05/05/2022 02:27 PM
nl s Report Limit DF Prepared
Analyzed CAS No. Qual
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
ND mg/L 5.0 1
04/20/22 22:50
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
ND mg/L 5.0 1
04/29/2218:52 107-21-1
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
ND ug/L 5.0 1 04/29/22 02:59
05/03/22 22:07 7439-92-1
Analytical Method: SM 2540D-2015
Pace Analytical Services - Asheville
10.3 mg/L 2.6 1
04/22/2211:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 13

aceAnalytical
urlrrw.Oal:Nablimm
Project:
FOSS RECYCLING INC DURHAM
Pace Project No.:
92600072
QC Batch:
692988
QC Batch Method:
EPA 1664B
Associated Lab Samples: 92600072001
METHOD BLANK
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 SGT-HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
3620367 Matrix: Water
Associated Lab Samples: 92600072001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L ND 5.0 04/20/22 22:50
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 3620368
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L 20 16.1 80 64-132
MATRIX SPIKE SAMPLE:
Parameter
3620369
Units
92599591001
Result
Spike MS MS % Rec
Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND
20 13.5 60
64-132 M1
SAMPLE DUPLICATE: 3620370
92599591003
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/05/2022 02:27 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 13

aceAnalj6cal
WWW.pcNsbs." nl
Project: FOSS RECYCLING INC DURHAM
Pace Project No.: 92600072
QC Batch: 673785
QC Batch Method: EPA 8015 Alcohol -Glycol
Associated Lab Samples: 92600072001
METHOD BLANK: 3102471
Associated Lab Samples: 92600072001
Parameter Units
Ethylene glycol mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 8015 Alcohol -Glycol
Analysis Description: EPA 8015 Modified
Laboratory: Pace Analytical Services - Indianapolis
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 04/29/2217:17
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 3102472
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Ethylene glycol mg/L 25 32.2 129 39-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102473 3102474
MS MSD
92600072001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
25 25 28.4 33.2 113 132 36-158 16
Ethylene glycol mg/L ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/05/2022 02:27 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 13

aceAna1xical
www.pacNobs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: FOSS RECYCLING INC DURHAM
Pace Project No.: 92600072
QC Batch: 694728
Analysis Method:
EPA 601OD
QC Batch Method: EPA 3010A
Analysis Description:
6010 MET
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92600072001
METHOD BLANK: 3628509
Matrix: Water
Associated Lab Samples: 92600072001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Lead ug/L
ND 5.0 05/03/22 20:39
LABORATORY CONTROL SAMPLE: 3628510
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Lead ug/L
500 494
99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3628511 3628512
MS MSD
92600072001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qua]
Lead ug/L ND
500 500 491
495 98 99 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/05/2022 02:27 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 13

aceAnalytical
www. fseNsbs cool
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: FOSS RECYCLING INC DURHAM
Pace Project No.: 92600072
QC Batch: 693391 Analysis Method: SM 254OD-2015
QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92600072001 Laboratory: Pace Analytical Services - Asheville
METHOD BLANK: 3622469 Matrix: Water
Associated Lab Samples: 92600072001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 04/22/22 11:15
LABORATORY CONTROL SAMPLE: 3622470
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 251 254 101 90-110
SAMPLE DUPLICATE: 3622824
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 3622825
Parameter
Total Suspended Solids
92600305001 Dup
Units Result Result RPD Qualifiers
mg/L 278 270 3
92599954001 Dup
Units Result Result RPD Qualifiers
mg/L 77.3 74.0 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/05/2022 02:27 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 13

ace.owpical
WMnr.Pum aks.an
QUALIFIERS
Project: FOSS RECYCLING INC DURHAM
Pace Project No.: 92600072
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
Date: 05/05/2022 02:27 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 13

acmnalytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: FOSS RECYCLING INC DURHAM
Pace Project No.: 92600072
Lab ID
92600072001
92600072001
92600072001
92600072001
Date: 05/05/2022 02:27 PM
Sample ID
QC Batch Method
OUTFALL NO 1
EPA 1664E
OUTFALL NO 1
EPA 8015 Alcohol -Glycol
OUTFALL NO 1
EPA 3010A
OUTFALL NO 1
SM 2540D-2015
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch Analytical Method
692988
673785
694728 EPA 6010D
693391
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
694965
Page 10 of 13

Document Name: Document Revised: November 15, 2021
Sample Condition Upon Receipt (SCUR) Page 1 of 2
�ceAnalPvt Document No.: Issuing Authority:
F-CAR-Cs-033-Rev.08 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ HuntersvillelSf Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
SampleClient Name: Project #: W0# . 9211600072
[I Courier: - Fed Ex ❑UPS []LISPS []Client 11111111111111111111111
Commercial []Pace []Other:—
92600i)72
Custody Seal Present? []Yes ❑No Seals Intact? ❑Yes ONO
Dale/Initials Person Examining Contents:
1 y//?� z
Packing Material: ❑Bubble Wrap ❑Bubble Bags []None ❑ Other Biological Tissue Frozen?
Thermometer: (f - �1 []Yes []No []N/A
fl IR Gun ID: — I Z TG rF E]wet ❑Blue ❑None
Type of Ice:
L� Correction Factor:
Cooler Temp: Add/Subtract (•C) (,/ Temp should be above freezing to VC
i X ❑Samples out of temp criteria. Samples on ice, cooling process
Cooler -Temp Corrected-(Q -- - — u
USDA Regulated soil ( Q N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Old samples originate from a foreign source (internationally,
nY>. nN,.
n —."'Snawdn dnu rueno KICO)e LfYES LfNo
Comments/Discrepancy:
Chain of Custody Present?
EjYes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
yes
[]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
Yes
otio
N/A
3.
Rush Turn Around Time Requested?
❑Yes
o
N/A
4.
Sufficient Volume?
Yes
No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
t3Yes
es
❑No
No
[]N/A
❑N/A
6.
Containers Intact?
' Yes
[]No
N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No `,
©N/A
8.
Sample labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
'jYes
l J T
❑No
❑N/A
9.
Headspace in VOA Vials (-,5.6mm)?
[I Yes
bN0
N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
PNo
❑No
❑N/A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Lot ID of split containers:
Date:
Date:
Field Data Required? ❑Yes ❑No
Page 11 of 13

Document Name: Document Revised. November 15, 2021
Analytical'
Sample Condition Upon Receipt (SOUR) Page 2 of 2
Document No.: Issuing Authority:
F-CAR•CS-033•Rev.09 Pace Carolinas Quality Office
Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHS
`*Bottom half of box is to list number of bottles
Project WOlt 92.600072
PM: T:[H ` Due Date: 05/04/22
CLIENT: 92-MID ATLAN
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pH Adjustment Log for Preserved Samples
Sample to Type of Preservative pH upon receipt Date preservation adjusted Time preservatlon Amount of Preservative Lot q
adjusted added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers,
Page 12 of 13

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# OF CONTAINERS
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13 of 13