WQ0000485_Monitoring - 07-2022_20220817

n ..
DWR - NonDischarge Monitoring Report Submittal y. •4 ..
NORTH CAROLINA
Enrlranmenlel QHaflly
Monitoring Report Submittal
..............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Permit Number#* WQ0000485
Name of Facility:* Valley Proteins-Rose Hill
Month:* July Year:* 2022
Report Information
Type* Upload Document*
GW-59 scan WQ0000485 GW-59 3.93MB
2022-07 VPRH.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2,NDMLR,GW-59).
Confirmation Email Address:* [e-mail]
Name of Submitter:* Corey Lanier
Signature:
Date of submittal: 8/17/2022
This will be filled in automatically
Initial Review
..............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Reviewer: Gerald,Wanda

Is the project number correct?* WQ0000485
Is the monitoring report accepted?* Yes No
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 8/29/2022

V TY PR ,TEINS, .INC.
August 15, 2022
Division of Water Resources
Attn: Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Ground Water Quality Monitoring Report (GWQMR)
Valley Proteins Inc. — Rose Hill
To whom it may concern,
Please find enclosed the Groundwater Quality Monitoring Compliance Report for
Surface Irrigation for the month of July 2022 for our Rose Hill Division.
Should you require any additional information or wish to discuss this matter,
please feel free to contact me at 910.289.2083 x 25119.
Sincerely,
41/1/11
Larry Holt
General Manager
cc: VP Corporate Office
469 Yellow Curt Road
Rose Hill,NC 28458
e 540.8772590
866.558.0994
Making a Sustainable Difference. Transportation 866.6518175
valleyproteuns.com

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Enter date monitoring results were due.(08131/2022)Will this monitoring report(GW-59 end GW-59A)
be submitted after the established due date? No
2 Was any required information missing on the GW-59 report forms? No
IF the answer to question 1 or 2 is"YES"list in the space provided below the well identification number(s)and explain the
problems encountered in obtaining the required information.
MW-8A was damaged by farm equipment and is scheduled to be closed and replaced by Register Well Co,INC;moving the
replacement well 10'due North per DEQ direction.
3 Are any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missing cap,missingidentificadon
'..... plate,area overgrown,etc.)?If the answer is"Yes",contact the Regional Office for guidance.. No
4 Are any monitored constituents equal to or above the established standards? YES
If the answer to question 4 is'NO,skip to section 8.
If the answer to question 4 is"YES"list the affected wells individually with constituent(s)and concentration(s)exceeding
standards in the space provided below:
SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT
5 For the constituents Identified In question 4 above,have standards been exceeded previously for the same
constituent(s)In the same well(s)In the last two years? YES
If the answer to question 5 is NO",skip to section 8.
If the answer to question 5 is"YES';list in the space provided below,each well with constituent(s)exceeding standards,
concentration(s)reported,and sample collection date for each occurrence(for the last two years).
SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT
6 Are the monitoring wells listed In section 6 located at or beyond the review boundary? YES
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE
IMMEDIATELY FOR GUIDANCE.If the answer is "NO",monitoring wells may be improperly located;contact the
Regional Office.
7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality
'problem? YES
'if the answer to question 7 is'YES",describe those actions in the space provided below.
If the answer to question 71s"NO';contact the Reg/onel Office within 90 days;an evaluation may En
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility.Failure to do so may subject the permitee toe Notice of Violation,
Isles,andfor penalties.
Additional monitoring was performed to identify constituents of TOC in MW No.9.The facility has been
communicating with Mr.Geoff Kegley in the Wilmington Regional Office.
8 1 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this form with
G W-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted In this report
((Compliance Report GW-59A)is true and complete to the best of my knowledge.
fir i
Signet re of P ttee(o : thorized Agent) Date
ire"ifirU,.9 I,A1,,,M;i;JP„d,°7:VDtl7:Pl

Valley Proteins,Inc-Rose Hill(WQ0000485)Groundwater Monitoring Well 2 Year Exceedance History Report
TDS 500 10A 11A 14A
July-22 772 510 1280
March-22 783 527 1100
November-21 _ 801 722 1230
July-21 706 522 1010
March-21 684 866
_
November-20 642 844
July-20 592 908
pH 6.5-8.5 2 4 7A 8A 9 10A 11A 12B 13A 14A
July-22 t 6.40 6.3 5.1 5.3 6.4 4.2 4.6 4 5.1 4.9
March-22 6.40 5.9 4.7 4.6 4.6 4.4 4.2 4.7 5.2
November-21 5.50 4.30 4.50 6.30 4.00 4.30 4.20 4.20 5.00
July-21 6.10 5.60 4.90 4.60 5.90 _ 4.70 4.60 5.40 5.00
March-21 6.40 5.70 4.90 4.70 5.30 5.00 5.10 5.90 5.40
November-20 6.40 4.50 5.00 4.60 5.00 4.80 5.30 5.70
July-20 6.20 5.10 5.60 6.30 5.60 4.30 4.20 5.00 5.80
- TOC10 9
July-22 45.1
March-22 34.9
November-21 26.4
July-21 25.9
March-21 32.9
November-20 43.2
-
July-20 37.7
Chloride 250 10A 14A
_
July-22 261 356
March-22 294 325
November-21 353
July-21 425 275
March-21
November-20 295 1 285
July-20 299
Sulfate 250 14A
July-22 287
March-22 277
November-21 322
July-21
March-21
November-20
July-20

SUBMIT FORM ON YELLOW PAPER ONLY
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GROUNDWATER QUALITY MONITORING: to: b . -o ® :a � ��
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FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill,NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name No. of wells to be sampled. 11 ❑ Water Source Heat Pump ❑ Other:
(from Pe€mstl
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-1 Date sample collected: 7/18/2022 FIELD ANALYSES: WAS
Well Depth: 12.46 ft. Well Diameter: 2 in. pH45ooHB 6.40 units Temp.00010: 26.5 °C DRY at
Depth to Water Level 82546: 3.0 Screened Interval: 12.46 ft. to 2.46 ft. Spec. Cond. 000.94: µMhos time of
Measuring Point is 1.17 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear chec
Samples for metals were collected unfiltered: X YES DNO and field acidified: X YES ❑ NO here:
LABORATORY INFORMATION
Date sample analyzed: 07/18/2022-07/29/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead o1051 ug!L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 0.38 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.04 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 129,00 mg/L Al-Aluminum o11os mg/L Sodium 8.46 mg/L
pH (Lab)00403 6.40 units Ba-Barium 01007 ug/L
TOC 00680 0.9 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 7 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS::(by GC,GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 61 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? • Yes(0) ❑ No(0)
specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 78732: , method# SM 6200C
Total Ammonia oos10 <0.2 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH,as N;Ammonia Nitrogen,Total) Mn-Manganese o1055 ug/L , method#
TKN as N 00625 0.7 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory,.I am aware that there are signifTcantpenalfies for submitting false information,including the os ibi:ityy of fines and tmprnscnninnt for•stowing violations
Larry Holt-General Manager r ' ' 7<c'Zo2Z
Permittee(or Authorized Agent)Name and Title-Please print or type Signature$1ermn•--(or Authorized Agent) (Pate)
GW-59 Rev_8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
. Mail original and I \ - \\\\
GROUNDWATER QUALITY MONITORING. "` \\
1 copy to m \\ ��o ,��� \� \\\�� yob\ o \\\\COMPLIANCE REPORT FORM , _ \\ \:
FACILITY INFORMATION Please Pnnt Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3131/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field 0 Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name No.of wells to be sampled: 11 ❑ Water Source Heat Pump 0 Other:
tftew Pe€mlfl
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-2 Date sample collected: 7/18/2022 FIELD ANALYSES: WAS
Well Depth: 31.00 ft. Well Diameter: 2 in. pHa5ooHB 6.70 units Temp.00010: 20.7 oC DRY at
Depth to Water Level 82546: 13.8 ft. below measuring point Screened Interval: 30.15 ft. to 20.15ft. Spec. Cond.00094: µMhos time of
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan
check
here:
Samples for metals were collected unfiltered: X YES 0 NO and field acidified: X YES 0 NO
LABORATORY INFORMATION
Date sample analyzed: 07/18/2022-07/29/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1.0 /100mL Nitrate(NO3)as N 00620 0.12 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 0.13 mg/L
(Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 287.00 mg/L Al-Aluminum 01105 mg/L Sodium 11.8 mg/L
pH(Lab)00403 6.70 units Ba-Barium 01007 ug/L
TOC 00680 1.2 mg/L Ca-Calcium oosls mg/L
Chloride oosao 10 mg/L Cd-Cadmium 01027 ug/L
Arsenic 0100z ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate oosas 9 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? I. Yes(0) El No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 78732: , method# SM 6200C
Total Ammonia o0s10 <0.2 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N 00625 0.5 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR certified laboratory. I am aware that there are significant penalties for subinittrng false information including the possibility of fines and imprisonment for knowing violations.
Larry Holt-General Manager . A i Zoz Z
Permittee(or Authorized Agent)Name and Title-Please print or type Signatu- .1 P• tttee for Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original and ,�9, , ', . �;r a° ' ®, m `-N
GROUNDWATER QUALITY MONITORING: ���, � ,�" ;���
COMPLIANCE REPORT FORM 1 copy to ',�� ���
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FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ00 0485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd, TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill. NC 28458 County Duplin ❑ Lagoon El Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-4 Date sample collected: 7/18/2022 FIELD ANALYSES: WAS
Well Depth: 28.93 ft. Well Diameter: 2 in. pH4500HB 6.30 units Temp. 00010: 23.7 °C DRY at
Depth to Water Level 82546: 6.2 ft. below measuring point Screened Interval: 28.93 ft. to 18.93ft_ Spec. Cond. 00094: µMhos time of
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan Tint check
here: 1
Samples for metals were collected unfiltered: X YES❑ NO and field acidified: X YES El NO
LABORATORY INFORMATION
Date sample analyzed: 07/18/2022-07/29/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 0_02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3)as N o0620 <0.02 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.43 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 205.00 mg/L Al-Aluminum 01105 mg/L Sodium 9.69 mg/L
pH (Lab)00403 6.30 units Ba-Barium 01007 ug/L
TOC 00680 0.50 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 <5.0 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug!L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 <5.0 mg/L Hg-Mercury 71900 ug!L Lab Report Attached? I Yes(0) El No(0)
Specific Conductance woes µMhos K-Potassium 00937 mg/L VOC 78732: , method# SM 6200C
Total Ammonia o0610 <0.2 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N 00625 <0.5 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory I am aware that there are significant<penalties for su rr)tting false information,inctud€ng the possibility of fines and imprisonment for knowing violations.
._
Larry Holt-General Manager ter_ r 2
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of F emit-= or, ,orzad Agent) (Date)
GW-59 Rev.8/2013

Mail original and ! _ � \, ,
GROUNDWATER QUALITY MONITORING: 1 copyto � -- - � C\\
COMPLIANCE REPORT FORM `= — \
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number.. W00000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd, TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill,NC 28458 County Duplin 0 Lagoon ❑Remediation:Infiltration Gallery
X Spray Field ❑Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor 0 Land Application of Sludge
Well Location/Site Name: No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION if WELL
WELL ID NUMBER(from Permit): MW-TA Date sample collected: 7/18/2022 FIELD ANALYSES: WAS
Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.10 units Temp.0001o: 26.2 °C DRY at
Depth to Water Level 82546: 21.9 ft.below measuring point Screened Interval: 16 ft. to 6 ft. Spec.Cond.00094: µMhos time of
Measuring Point is 2.42 ft.above land surface Relative M.P.Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5,0 gallons Appearance Clear check
Samples for metals were collected unfiltered: X YES f NO and field acidified: X YES 0 NO here} 1
LABORATORY INFORMATION
Date sample analyzed: 07118/2022-07/29/202 Laboratory Name: Environmental Chemists,Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N o0615 <0.02 mg/L Pb-Lead o10s1 uglL
Coliform:MF Fecal 31616 <1 /100mL Nitrate(NO3)as N o0620 <0.02 mg/L Zn-Zinc 01os2 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 0.55 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 240.00 mg/L Al-Aluminum o11 cis mg/L Sodium 21.9 mg/L
pH(Lab)00403 5.10 units Ba-Barium 01007 ug/L
TOC 00680 0.6 mg/L Ca-Calcium 00916 mg/L
Chloride cow 88 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium:Total o1034 uglL
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS,HPLC)
Phenol 32730 ug/L Fe-Iron 01045 uglL (Specify test and method#.ATTACH LAB REPORT.)
Sulfate Oo945 20 mg/L Hg-Mercury71900 uglL Lab Report Attached? •Yes(0) ❑ No(0)
Specific Conductance 000ss Mhos K-Potassium 00937 mg/L VOC 78732: ,method# SM 6200C
Total Ammonia oos10 <0.2 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen;NI-),as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ---- ug!L ,method#
TKN as N 00625 <0.5 mg/L Ni-Nickel 01067 uglL ,method#
For Remediation Systems Only(Attach Lab Reports): influent Total VOCs: rng/L Effluent Total VOCs: mg/L VOC Removal%
I grit,tt;3�to tf o LHsr 7f tt? -..ia,1go> o Y�=).et the I.tformot'-,ra vttbm t er in t. s r€., r.-t,,ie OcnLee and w- Ole qr.-L.U 3t tee lar-z:ria rt of101 O,_,,al f"atu r OrO UCOf'sr lrt:000roe T€-[?-,cue Ot art f.i-Cep 3
L4,,,, r;ifred'.`dcreenry I am aware th1t tfere 4te 01ar a` nt p>enalt f�swt.�;4t no Oar,e-first t ir7_,,,l,r,t3 i00; -bii,[,Cr IIre�..and,inik i rrn ,rnn.,rt l .,la'�o
Larry Holt-General Manager - - LZ
Perrnittee(or Authorized Agent)Name and Title-Please print or type Signature of.ermittee •r Authorized Agent) (Date)

Mail original Is \tea ®t\� \ \ \ ®\ , \\\\\\N \�\
GROUNDWATER QUALITY MONITORING: a-, t o i11 e ®® 7 \\\
and 1 copy to p�\�� \��\\ \\ \\\\\\
COMPLIANCE REPORT FORM .��®': ��,�. ������ ���.. �� `�p„���..�� ��� �..,
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Dater 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill,NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
•F `=' X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] E Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name Field 5-damaged by farm equip/to replace No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-8A Date sample collected: 7/18/202_2 FIELD ANALYSES: WAS
Well Depth: 16 ft. Well Diameter: 2 in. pH450olnte 5.30 units Temp.00010: 25s °C DRY at
Depth to Water Level 82546: 5.8 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec.Cond.00094 ftMhos time of
Measuring Point is 2.5 ft. above land surface Relative M.P.Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sam 0 5.0 gallons Appearance Clear check
Samples for metals were collected unfiltered: X YES U NO and field acidified: X YES ❑ NO hole
LABORATORY INFORMATION
Date sample analyzed: 07/18/2022-07/29/2022 Laboratory Name: Environmental Chemists. Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform:MF Fecal 31616 41 /100mL Nitrate(NO3)as N 00620 0.7 mg/L Zn-Zinc o1os2 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 0.09 mg/L
(Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
issolved Solids:Total 70300 57.00 mg/L Al-Aluminum 01105 mg/L Sodium 1.55 mg/L
pH(Lab)00403 5.30 units Ba-Barium 01007 ug/L
TOC 00680 0.90 mg/L Ca-Calcium oos16 mg/L
Chloride 00940 <5.0 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 20 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? al Yes(0) ❑ No(0)
specific Conductance 00095 RMhos K-Potassium 00937 mg/L VOC 78732: ,method# SM 6200C
Total Ammonia o0610 <0.2 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen;Nyas N;Ammonia Nitrogen,Total) Mn-Manganese o1055 --- ug/L ,method#
TKN as N 00625 0.7 mg/L Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mgiL VOC Removal,
I certify that,to the best of my knowledge and belief the information submitted in this report is true accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR certified ratory;I am aware that there are mornriccntpenaltr for ssbnitlirrg false information including the poaSthi tty of fines and imprisonment for know:ng violations
47
Larry Holt-General Manager -ZoZZ
Permittee(or Authorized Agent)Name and Title-Please print or type Signature- Permitt (or Authorized Agent) (Date)

���o
GROUNDWATER QUALITY MONITORING: N
COMPLIANCE REPORT FORM _,, ,_,,_„ ,_.,„,,„ N, y, ,„.,„ •: ,\o.„>\\
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000465 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill,NC 28458 County Duylin ❑ Lagoon ❑Remediation: Infiltration Gallery
= X Spray Field ❑Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name No of wells to be sampled: 11 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-9 Date sample collected: 7/18/2022 FIELD ANALYSES: WAS
Well Depth: 13.73 ft. Well Diameter: 2 in. pH4500HB 6.40 units Temp.0o01o: 23.4 °C DRY at
Depth to Water Level 82546: 5.2 ft.below measuring point Screened Interval: 13.73 ft. to 3.73 ft. Spec.Cond.00094: µMhos time of
Measuring Point is 3.50 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan check
Samples for metals were collected unfiltered: X YES❑ NO and field acidified: X YES ❑ NO here:
LABORATORY INFORMATION
Date sample analyzed: 07/18/2022-07/29/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 0.10 mg/L Pb-Lead 01051 ug/L
Coliform:MF Fecal 31616 35 /100mL Nitrate(NO3)as N 00620 0.02 mg/L Zn-Zinc 01092 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 0.24 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 228.00 mg/L Al-Aluminum o1105 mg/L Sodium 4.26 mg/L
pH(Lab)00403 6.40 units Ba-Barium 01007 ug/L
TOC 00680 45.1 mg/L Ca-Calcium oo91s mg/L
Chloride 00940 11 mg/L Cd-Cadmium 01027 _ug/L
Arsenic o1o02 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS,HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 15 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? •Yes(0) ❑ No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 70732: , method# SM 6200C
Total Ammonia oosso <0.2 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;Nyas N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method#
TKN as N 00625 1.8 mg/L Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports): influent Total VOCs: rng/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete and that the laboratory analytical data was produced using approved methods of analysis by a --
DWR-certified latoilury I am aware that there are significant ueriaitres for subm lung false information,including the pussrbt[i y of fines and imorusenmeril fr.r trimming;violations
Larry Holt-General Manager ;' _ ,�`Or zOZZ
Permittee(or Authonzed Agent)Name and Title-Please print or type Signature=.-`ermi • . Authorized Agent) (Date)

Mail`original r< , ��VI ® e s sip t - 7 a��\ -;11,-
\ �� �\
GROUNDWATER QUALITY MONITORING: and 1 copy to: ��O\ � ��A -- ��
COMPLIANCE REPORT FORM +-�_ �� e
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
_Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] E Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-10A Date sample collected: 7/18/2022 FIELD ANALYSES: WAS
Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.20 units Temp.0001( 271 °C DRY at
Depth to Water Level 82546: 4.0 ft.below measuring point Screened Interval: 16 ft. to 6 ft. Spec.Cond.00094: µMhos time of
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085 None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Red Tint deck
Samples for metals were collected unfiltered: X YES 17 NO and field acidified: X YES I- NO here:
LABORATORY INFORMATION
Date sample analyzed: 07/18/2022-07/29/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N oasis 0.02 mg/L Pb-Lead o1051 ug/L
Coliform:MF Fecal 31616 <1 /100mL Nitrate(NO3)as N ooszo 1.31 mg/L Zn-Zinc o1092 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 0.12 mg/L
(Note Use MPN method for highly turbid samples) Orthophosphate 70507. mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 772.00 mg/L Al-Aluminum 01105 mg/L Sodium 90.5 mg/L
pH(Lab)00403 4.20 units Ba-Barium 01007 ug/L
TOC 00680 3.7 mg/L Ca-Calcium oasis mg/L _
Chloride()ow 261 mg/L Cd-Cadmium 01027 ug/L
Arsenic o10oz ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate oosas 121 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ®Yes(0) ❑ No(0)
peciftc Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 78732: , method# SM 6200C
Total Ammonia 00610 0.40 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;Nh)as N;Ammonia Nitrogen,Total) Mn-Manganese°loss uglL ,method#
TKN as N 00625 1.00 mg/L Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: me/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
■WR certified laboratory I am aware that there are slur:ft�ant panaiti for submitting false infoi matron including the possibility of fines and imprisonment for kfTiMill violations.
117
Larry Holt-General Manager tile ' 1sZ-022'
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of germ (or Authorized Agent) {Pate)

Mail original ' � ` \,� "\
GROUNDWATER QUALITY MONITORING: copy ��� �� �� y '���
COMPLIANCE REPORT FORM and 1 co to \
�
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number WQ0000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor LI Land Application of Sludge
Well Location/Site Name No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑Other:
(from Permit) '..
SAMPLING INFORMATION if WELL
WELL ID NUMBER(from Permit): MW-11A Date sample collected: 7/18/2022 FIELD ANALYSES: WAS
Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.60 units Temp.000tr 2s"3 °C DRY at
Depth to Water Level 82546: 5 Screened Interval: 16 ft. to 6 ft. Spec.Cond.00094: uMhos time of
Measuring Point is 3.3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear the
Samples for metals were collected unfiltered: X YES❑ NO and field acidified: X YES n NO here.
LABORATORY INFORMATION
Date sample analyzed 07/18/2022-07/29/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N mists <0.02 mg/L Pb-Lead o1os1 ug/L
Coliform:MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 1.19 mg/L Zn-Zinc mow mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 0.04 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 _ mg/L Other(Specify Compounds and Concentration Units)..
)issolved Solids:Total 70300 510.00 mg/L Al-Aluminum of 1os mg/L Sodium 64.8 mg/L
pH(Lab)00403 4.60 units Ba-Barium 01007 ug/L
TOC 00680 2.60 mg/L Ca-Calcium mists mg/L
Chloride oos4o 135 mg/L Cd-Cadmium 01027 ug/L
Arsenic room ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS,HPLC)
Phenol 32730 ug1L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 162.0 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? EYes(0) ❑ No(0)
Specific Conductance 00095 uMhos K-Potassium 00937 mg/L VOC 78732: , method# SM 6200C
Total Ammonia oosto <0.2 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;Nljas N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method#
TKN as N 00625 0.6 mg/L Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports) Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I rtrf-y that,la the h.si of my tcn:wIed e and b.le.the tn(a mathon submitt t rt this report,e true do urate.and camptetm.and Mai Inc tabocattarY anaiyileat data was Pccduccid using apptehed methods of anetysis oy
Dtri+R= ttifed'tadorat€ . I am aware that there are signt scant penattresfor su ltrng false information,rn udsng the pima)w.y of fin and ttilp-t nmentforknt trig wofat' ns
Z OLZ
Larry Holt-General Manager = -__
Permittee(or Authorized Agent)Name and Title-Please print or type Signature. _' Idee I,-Au -._bed Agent) (Date)

Mail original !� kN #` \\\�\�
GROUNDWATER QUALITY MONITORING: - t
and 1 copy t0 \`cam \ �g �o _, o��ti o\moo\ \, \�;
COMPLIANCE REPORT FORM \, \\\ �
�_, ti �,�
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number W00000485 Expiration Date: 3131/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill,NC 28458 County Duplin ❑ Lagoon ❑ Remediation:Infiltration Gallery
_,,..
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well.Location/Site Name: No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-12B Date sample collected: 7/18/2022 FIELD ANALYSES: WAS
Well Depth: 16 ft. Well Diameter: 2 in. pHHa 4.00 unit Temp.000to: 24.9 °C DRY at
Depth to Water Level 82546: 6.4 ft.below measuring point Screened Interval: 20 ft. to 10 ft. Spec Cond.Oat ; uMhos time of
Measuring Point is 3 ft.above land surface Relative M.P.Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear check
Samples for metals were collected unfiltered: X YES n NO and field acidified: X YES ❑NO here:7
LABORATORY INFORMATION
Date sample analyzed: 07/18/2022-07/2g1202 Laboratory Name: Environmental Chemists.Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform:MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 006zo 0.10 mg/L Zn-Zinc o1o9z mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P o0665 0.25 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 467.00 mg/L Al-Aluminum 01105 mg/L Sodium 83.1 mq/L
pH(Lab)00403 4.00 units Ba-Barium 01007 ug/L
TOC 00680 2.00 mg/L Ca-Calcium o0916 mg/L
Chloride oo940 128 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01o02 uglL Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS,HPLC)
Phenol 32730 uglL Fe-Iron o1045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 155 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? in Yes(0) ❑ No(0)
Specific Conductance o0095 uMhos K-Potassium 00937 mg/L VOC 78732: ,method# SM 6200C
Total Ammonia 00610 <0.2 mg/L Mg-Magnesium 00927 mg/L ,method#
(Ammonia Nitrogen;Nftes N,Ammonia Nitrogen:Totel) Mn-Manganese o1055 ug/L ,method#
TKN as N 00625 0.60 mg/L Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that to the best of my knowledge and belief the information submitted in this report is true,accurate and complete..and that the laboratory analytical data was produced using approved methods of analysis by a
DINR certified elxsrf�t. I am aware that there are significant penalties for subii3lit+ng..false information including R��-�sPlhty of fines a id irrapfl: unten€for knowing violations, ,..
Larry Holt-General Manager44151r �,���Z Z
Permittee(or Authorized Agent)Name and Title-Please print or type Signature. ermttt= (or thornz Agent) (Date)

Mail original and '°> �,�, o ,,—., ��tioo,ti,o, ,o ti� e o, .�o,� \\\ ,,, \
GROUNDWATER QUALITY MONITORING: t t \� \\�-
,COMPLIANCE REPORT FORM 1 copy to �` \\\\-\\\_ \
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number WQ0000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill,NC 28458 County Duplin ❑ Lagoon ❑ Remediation:Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application Of Sludge
Well Location/Site Name: No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other:
(from Permit) --
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-13A Date sample collected: 7/18/2022 FIELD ANALYSES: WAS
Well Depth: 16 ft. Well Diameter: 2 in. pi- Hs 5.10 units Temp.00010: 2ss °C DRY at
Depth to Water Level 82546: 5.3 ft.below measuring point Screened Interval: 16 ft. to 6 ft. Spec.Cond.00c94 uMhos time of
Measuring Point is 3 ft.above land surface Relative M.P.Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear check
Samples for metals were collected unfiltered: X YES n NO and field acidified: X YES n NO here:
LABORATORY INFORMATION
Date sample analyzed: 07/18/2022-07/29/2022 Laboratory Name: Environmental Chemists.Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 0.02 mg/L Pb-Lead 01051 ug/L
Coliform:MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 0.09 mg/L Zn-Zinc 01092 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 0.28 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 40.00 mg/L Al-Aluminum 01105 mg/L Sodium 4.13 mg/L
pH(Lab)00403 5.10 units Ba-Barium 01007 ug/L
TOC 00680 0.60 mg/L Ca-Calcium 00916 mg/L
Chloride 0os4o 8 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug!L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS,HPLC)
Phenol 32730 uglL Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 <5.0 mg/L Hg-Mercury 71900 ug!L Lab Report Attached? - Yes(0) ❑ No(0)
Specific Conductance 00095 uMhos K-Potassium 00937 mg/L VOC 78732: ,method# SM 6200C
Total Ammonia ooeio <0.20 mg/L Mg-Magnesium 00927 mg/L _,method#
(Ammonia Nitrogen,NFGas N;Ammonia Nitrogen,Total) Mn-Manganese moss uglL ,method#
TKN as N 00625 <0.50 mg/L Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
1 ze,I ty tra to the hoot or n j i-lea., e.s. )of:tom sn*.-r-as n submit. ,fl j . o two; o d rrt 0.0,and Ina i1w;abi-o4. arol ,c oard a prodtt�-d us; ,aop.. rrg1P s of'arrialys6 7 e
ire €: =t, t7 a zee°....I a�aa=arn!hat treero'.ere S U.rsi Lant::,e a..1_:.:-a sebe,ttial 2.else sSfr-rd.tan .3c3uri`at 3, r00i _ity.--a f rr n ad m =:]mmr tar roar o S.. sr55. —.
Larry Holt-General Manager _. ` , 1°1 --2a2--
Permittee(or Authorized Agent)Name and Title-Please print or type &ratite of Pr. ittee(or..diortnd Agent) (Date)

Mail original it' tom* \,
e `- -- �`������� ' '\ ova �'� \\\�O
GROUNDWATER QUALITY MONITORING: ��
COMPLIANCE REPORT FORM and 1 copy to `�` ���\�\���� �� �0�� 0 ��\\O b
[FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WC10000485 Expiration Date: 3/31/2025
Facility Name: Valley Proteins Inc.-Rose Hill Non-Discharge UIC
Permit Name(if different): NPDES Other
_Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name No.of wells to be sampled: 11 ❑ Water Source Heat Pump ❑Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-14A Date sample collected 7/18/2022 FIELD ANALYSES: WAS
Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.90 units Temp.noon26'8 °C DRY at
Depth to Water Level 82546: 4.4 ft. below measuring point Screened Interval: 10 ft. to 2.5 ft. Spec.Cond.00094: µMhos time of
Measuring Point is 3 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan Tint check
Samples for metals were collected unfiltered: X YES n NO and field acidified: X YES • NO here:
LABORATORY INFORMATION
Date sample analyzed: 07/18/2022-07/29/2022 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead o1051 ug/L
Coliform:MF Fecal 31616 <1.0 /100mL Nitrate(NO3)as N oos2o 3.03 mg/L Zn-Zinc o1092 mg/L
Coliform:MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.04 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 1280.00 mg/L Al-Aluminum o1105 mg/L Sodium 113 mg/L
pH(Lab)00403 4.90 units Ba-Barium 01007 ug/L
TOC 00680 4.20 mg/L Ca-Calcium oo916 mg/L
Chloride wear) 356 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC,GC/MS, HPLC)
Phenol 32730 _uglL Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 287 mg/L Hg-Mercury 7190o ug/L Lab Report Attached? NYes(0) ❑ No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 78732: ,method# SM 6200C
Total Ammonia 00s10 <0.20 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen,Nljas N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L ,method#
TKN as N 00625 0.70 mg/L Ni-Nickel 01067 ug/L ,method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOGs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory.,:I am aware that there are sr riift nt penalties for aubi�`se tt[no false information including the possibility of fines and is p5sor"tsent for Nenw.Inn violations.
Larry Holt General Manager ����
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Pe: ' Aethorised Agent) (Date)

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1 iiii.100-i li 1 0 7Whiihritm111111111111 6602 Windmill Way,Wilmington,NC 28405 4 910.392.0223 Lab * 910.392.4424 Fax
;11,11111 111111. q 1
111;iiiiin 8 710 Bowsertown Road,Manteo,NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 * 910.347.5843 Lab/Fax
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ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Valley Proteins-Rose Hill Date of Report: Jul 29, 2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-13482
Project ID: Monitoring Wells
—
Lab ID Sample ID: Collect Daterrime Matrix Sampled by
22-32737 Site:MW-1 7/18/2022 11:10 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear 07/18/2022
Depth to water, ft. Depth to Water,Ft. 3.0 feet 07/18/2022
Sodium EPA 200.7,Rev 4.4,1994 8.46 mg/L 07/22/2022
Sulfate EPA 300.0,Rev.2_1,1993 61 mg/L 07/19/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 07/27/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 07/18/2022
Odor Qualitative N/D 07/18/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 129 mg/L 07/19/2022
Temperature SM 2550 B-2010 26.5 C 07/18/2022
pH SM 4500 H13-2011 6.4 units 07/18/2022
Total Phosphorus SM 4500 P(F-H)-2011 <0.04 mg/L 07/27/2022
Total Organic Carbon(TOC) SM 5310 B-2014 0.9 mg/L 07/19/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 07/18/2022
Chloride SM4500 Cl E-2011 7 mg/L 07/21/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 07/18/2022
N itrate+Nitrite-Nitrog en EPA 353.2,Rev.2.0,1993 0.38 mg/L 07/22/2022
Nitrate Nitrogen Subtraction Method 0.38 mg/L 07/29/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 0.7 mg/L 07/27/2022
Total Nitrogen Total Nitrogen 1.1 mg/L 07/29/2022
Report#:: 2022-13482 Page 1 of 11

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111111111111111111111111111 IR In, p iitilihi 6602 Windmill Way,Wilmington,NC 28405 4 910.392.0223 Lab a 910.392.4424 Fax
111111111111111111111111111111111111m HE.. 111,114111111111iir4mi 710 Bowsertown Road,Manteo,NC 27954 w' 252.473.5702 Lab/Fax
II 255-A Wilmington Highway,Jacksonville,NC 28540 * 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info(denvironmentalchemists.com
Valley Proteins-Rose Hill Date of Report: Jul 29,2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-13482
Project ID: Monitoring Wells
.....----
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32738 Site: MW-2 7/18/2022 10:50 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear/Tan 07/18/2022
Depth to water, ft. Depth to Water,Ft. 13.8 feet 07/18/2022
Sodium EPA 200.7,Rev 4.4,1994 11.8 mg/L 07/22/2022
Sulfate EPA 300.0,Rev.2.1,1993 9 mg/L 07/19/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 07/27/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 07/18/2022
Odor Qualitative N/D 07/18/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 287 mg/L 07/19/2022
Temperature SM 2550 B-2010 20.7 C 07/18/2022
pH SM 4500 H B-2011 6.7 units 07/18/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.13 mg/L 07/27/2022
Total Organic Carbon(TOC) SM 5310 B-2014 1.2 mg/L 07/19/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 07/18/2022
Chloride SM4500 CI E-2011 10 mg/L 07/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 07/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.12 mg/L 07/22/2022
Nitrate Nitrogen Subtraction Method 0.12 mg/L 07/29/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 0.5 mg/L 07/27/2022
Total Nitrogen Total Nitrogen 0.6 mg/L 07/29/2022
..._ ,
o —.—..
Report#:: 2022-13492 Page 2 of 11

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II ill v11111111111111111111111114 pH liffilli 1.1. ,10
255-A Wilmington Highway,Jacksonville,NC 28540 w 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infokenvironmentalchemists.com
Valley Proteins-Rose Hill Date of Report: Jul 29, 2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-13482
Project ID: Monitoring Wells
„.....--„,
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32739 Site:MW-4 7/18/2022 10:15 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear/Tan Tint 07/18/2022
Depth to water,ft. Depth to Water,FL 6.2 feet 07/18/2022
Sodium EPA 200.7,Rev 4.4,1994 9.69 mg/L 07/22/2022
Sulfate EPA 300.0,Rev.2.1,1993 <5 mg/L 07/19/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 07/27/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 07/18/2022
Odor Qualitative N/D 07/18/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 205 mg/L 07/19/2022
Temperature SM 2550 B-2010 23.7 C 07/18/2022
pH SM 4500 H B-2011 6.3 units 07/18/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.43 mg/L 07/27/2022
Total Organic Carbon (TOG) SM 5310 B-2014 0.5 mg/L 07/19/2022
Fecal Coliform SM 9222 D-2015 ME <1 Colonies/100mL 07/18/2022
Chloride SM4500 Cl E-2011 <5 mg/L 07/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.02 mg/L 07/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.02 mg/L 07/22/2022
Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/29/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen (TKN) EPA 351.2,Rev.2.0,1993 <0.5 mg/L 07/27/2022
Total Nitrogen Total Nitrogen <0.5 mg/L 07/29/2022
....
Report#:: 2022-13482 Page 3 of 11

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IIIII*111111111111111111I1111111 75 000111111111111111111111111111111011111,1 , 710 Bowsertown Road,Manteo,NC 27954 * 252.473.5702 Lab/Fax
11111111111111111q011111111111111111111111111111111111111111111111111111101111IIIIIIIINIIIIIIIII IIIII
255-A Wilmington Highway,Jacksonville,NC 28540 * 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infora envi ron men talchemists.com
Valley Proteins-Rose Hill Date of Report: Jul 29, 2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-13482
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32740 Site:MW-7A 7/18/2022 11:40 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear 07/18/2022
Depth to water,ft. Depth to Water.Ft. 5.1 feet 07/18/2022
Sodium EPA 200.7,Rev 4.4,1994 21.9 mg/L 07/22/2022
Sulfate EPA 300.0,Rev.2.1,1993 20 mg/L 07/19/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 07/27/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 07/18/2022
Odor Qualitative N/D 07/18/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 240 mg/L 07/19/2022
Temperature SM 2550 B-2010 26.2 C 07/18/2022
pH SM 4500 H B-2011 5.1 units 07/18/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.55 mg/L 07/27/2022
Total Organic Carbon(TOC) SM 5310 B-2014 0.6 mg/L 07/19/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 07/18/2022
Chloride SM4500 CI E-2011 88 mg/L 07/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 07/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 07/22/2022
Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/29/2022
Total Nitr• .en(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 <0.5 mg/L 07/27/2022
Total Nitrogen Total Nitrogen <0.5 mg/L 07/29/2022
_....... ..._ _. _ _....................___ , ......._______ _ .
Report#:: 2022-13482 Page 4 of 11

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I MIIIIIIII11111111111111111111:11,111,111111111111111111 ,101111117111111111111111100
111111I11111 1111111111111111 1111111111111111111111111111111111111111111111111 710 Bowsertown Road,Manteo,NC 27954 * 252.473.5702 Lab/Fax
11 111111111111111011011111111111210I11111111111N101111111111111 111,111111 i,
255-A Wilmington Highway,Jacksonville,NC 28540 a 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info@,environmentalchemists.com
Valley Proteins-Rose Hill Date of Report: Jul 29,2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-13482
Project ID: Monitoring Wells
........ —....___.-....,....„,-
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32741 Site:MW-8A 7/18/2022 11:55 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear 07/18/2022
Depth to water, ft. Depth to Water,FL 5.8 feet 07/18/2022
Sodium EPA 200.7,Rev 4.4,1994 1.55 mg/L 07/22/2022
Sulfate EPA 300.0,Rev.2.1,1993 20 mg/L 07/19/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 07/27/2022
Gallons bailed before sampling Gallons Balled before sampling 5.0 gallons 07/18/2022
Odor Qualitative N/D 07/18/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 57 mg/L 07/19/2022
Temperature SM 2550 B-2010 25.9 C 07/18/2022
pH SM 4500 H B-2011 5.3 units 07/18/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.09 mg/L 07/27/2022
Total Organic Carbon(TOC) SM 5310 B-2014 0.9 mg/L 07/19/2022
Fecal Coliform SM 9222 D-2015 MF 41 Colonies/100mL 07/18/2022
Chloride SM4500 CI E-2011 <5 mg/L 07/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 07/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.70 mg/L 07/22/2022
Nitrate Nitrogen Subtraction Method 0.70 mg/L 07/29/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev 2.0,1993 0.7 mg/L 07/27/2022
Total Nitrogen Total Nitrogen 1.4 mg/L 07/29/2022
Report#:: 2022-13482 Page 5 of 11

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6602 Windmill Way,Wilmington,NC 28405 $ 910.392.0223 Lab $ 910.392.4424 Fax
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IIIIINEN III Pin illI11111111111111111111 1, 710 Bowsertown Road,Manteo,NC 27954 a 252.473.5702 Lab/Fax
oommilio1111111 1 255-A Wilmington Highway,Jacksonville,NC 28540 $ 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Valley Proteins-Rose Hill Date of Report: Jul 29, 2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-13482
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32742 Site:MW-9 7/18/2022 10:30 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Tan 07/18/2022
Depth to water, ft. Depth to Water,Ft. 5.2 feet 07/18/2022
Sodium EPA 200.7,Rev 4.4,1994 4.26 mg/L 07/22/2022
Sulfate EPA 300.0,Rev.2.1,1993 15 mg/L 07/19/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 07/27/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 07/18/2022
Odor Qualitative N/D 07/18/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 228 mg/L 07/19/2022
Temperature SM 2550 B-2010 23.4 C 07/18/2022
pH SM 4500 H B-2011 6.4 units 07/18/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.24 mg/L 07/27/2022
Total Organic Carbon(TOC) SM 5310 B-2014 45.1 mg/L 07/19/2022
Fecal Coliform SM 9222 D-2015 MF 35 Colonies/100mL 07/18/2022
Chloride SM4500 Cl E-2011 11 mg/L 07/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.10 mg/L 07/18/2022
Nitrate+N itrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.12 mg/L 07/22/2022
Nitrate Nitrogen Subtraction Method 0.02 mg/L 07/29/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 1.8 mg/L 07/27/2022
Total Nitrogen Total Nitrogen 1.9 mg/L 07/29/2022
. ...... .
„„....
Report#:: 2022-13482 Page 6 of 11

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m r !1 11 1,1r !1� . 255-A Wilmington Highway,Jacksonville,NC 28540 6 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Valley Proteins-Rose Hill Date of Report: Jul 29, 2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-13482
Project ID: Monitoring Wells
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
22-32743 Site:MW-10A 7/18/2022 9:20 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear/Red Tint 07/18/2022
Depth to water,ft. Depth to Water,Ft. 4.0 feet 07/18/2022
Sodium EPA 200.7,Rev 4.4,1994 90.5 mg/L 07/22/2022
Sulfate EPA 300.0,Rev.2.1,1993 121 mg/L 07/19/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 0.4 mg/L 07/27/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 07/18/2022
Odor Qualitative N/D 07/18/2022
Total Dissolved Solids(IDS) SM 2540 C-2015 772 mg/L 07/19/2022
Temperature SM 2550 B-2010 27.1 C 07/18/2022
pH SM 4500 H B-2011 4.2 units 07/18/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.12 mg/L 07/27/2022
Total Organic Carbon (TOC) SM 5310 B-2014 3.7 mg/L 07/19/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 07/18/2022
Chloride SM4500 CI E-2011 261 mg/L 07/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.02 mg/L 07/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 1.33 mg/L 07/22/2022
Nitrate Nitrogen Subtraction Method 1.31 mg/L 07/29/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 1.0 mg/L 07/27/2022
Total Nitrogen Total Nitrogen 2.3 mg/L 07/29/2022
m
Report#:: 2022-13482 Page 7 of 11

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em#111111, 6602 Windmill Way,Wilmington,NC 28405 " 910.392.0223 Lab * 910.392.4424 Fax
q.1 11111111111P111 111111; 11111111111111r 710 Bowsertown Road,Manteo,NC 27954 ' 252.473.5702 Lab/Fax
1 Ivo 1011111111111111111111 II .... lifil11111111
255-A Wilmington Highway,Jacksonville,NC 28540 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Valley Proteins-Rose Hill Date of Report: Jul 29, 2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-13482
Project ID: Monitoring Wells
...—
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32744 Site:MW-11A 7/18/2022 9:32 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear 07/18/2022
Depth to water, ft. Depth to Water,Ft 5.0 feet 07/18/2022
Sodium EPA 200.7,Rev 4.4,1994 64.8 mg/L 07/22/2022
Sulfate EPA 300.0,Rev.21,1993 162 mg/L 07/19/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 07/27/2022
Gallons bailed before sampling Gallons Balled before sampling 5.0 gallons 07/18/2022
Odor Qualitative N/D 07/18/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 510 mg/L 07/19/2022
Temperature SM 2550 B-2010 26.3 C 07/18/2022
pH SM 4500 H B-2011 4.6 units 07/18/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.04 mg/L 07/27/2022
Total Organic Carbon (TOC) SM 5310 B-2014 2.6 mg/L 07/19/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 07/18/2022
Chloride SM4500 CI E-2011 135 mg/L 07/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 07/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 1.19 mg/L 07/22/2022
Nitrate Nitrogen - Subtraction Method 1.19 mg/L 07/29/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 0.6 mg/L 07/27/2022
Total Nitrogen Total Nitrogen 1.8 mg/L 07/29/2022
DIM ..,........n.pensinam agromau
Report#: 2022-13482 Page 8 of 11

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1144100a 1,11111,1.1.i1iI11 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 e 252.473.5702 Lab/Fax
I IILIIIIIIIIIIII tidl 11111,771111 11111111111111111111111M1hgililill!'1111111M111111111111111- 1,
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infoabenvironmentalcliemists.com
Valley Proteins-Rose Hill Date of Report: Jul 29,2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-13482
Project ID: Monitoring Wells
...............__
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32745 Site: MW-12B 7/18/2022 9:55 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear 07/18/2022
Depth to water,ft. Depth to Water,Ft. 6.4 feet 07/18/2022
Sodium EPA 200.7,Rev 4.4,1994 83.1 mg/L 07/22/2022
Sulfate EPA 300.0,Rev.2.1,1993 155 mg/L 07/20/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 07/27/2022
Gallons bailed before sampling Gallons Baited before sampling 5.0 gallons 07/18/2022
Odor Qualitative N/D 07/18/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 467 mg/L 07/19/2022
Temperature SM 2550 B-2010 24.9 C 07/18/2022
pH SNI 4500 H B-2011 4.0 units 07/18/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.25 mg/L 07/27/2022
Total Organic Carbon(TOC) SM 5310 B-2014 2.0 mg/L 07/19/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 07/18/2022
Chloride SM4500 CI E-2011 128 mg/L 07/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 07/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.10 mg/L 07/22/2022
Nitrate Nitrogen Subtraction Method 0.10 mg/L 07/29/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 0.6 mg/L 07/27/2022
Total Nitrogen Total Nitrogen 0.7 mg/L 07/29/2022
,--------.
Report#:: 2022-13482 Page 9 of 11

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710 Bowsertown Road,Manteo,NC 27954 * 252.473.5702 Lab/Fax
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ANALYTICAL&CONSULTING CHEMISTS info@,environmentalchemists.com
Valley Proteins-Rose Hill Date of Report: Jul 29,2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-13482
Project ID: Monitoring Wells
,....--..........„..... —
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32746 Site:MW-13A 7/18/2022 9:45 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear 07/18/2022
Depth to water,ft. Depth to Water,Ft 5.3 feet 07/18/2022
Sodium EPA 200.7,Rev 4.4,1994 4.13 mg/L 07/22/2022
Sulfate EPA 300.0,Rev.2.1,1993 <5 mg/L 07/19/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 07/27/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 07/18/2022
Odor Qualitative N/D 07/18/2022
Total Dissolved Solids(IDS) SM 2540 C-2015 40 mg/L 07/19/2022
Temperature SM 2550 B-2010 25.9 C 07/18/2022
pH SM 4500 H 8-2011 5.1 units 07/18/2022
Total Phosphorus SM 4500 P(F-H)-2011 0.28 mg/L 07/27/2022
Total Organic Carbon(TOC) SM 5310 B-2014 0.6 mg/L 07/19/2022
Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 07/18/2022
Chloride SM4500 CI E-2011 8 mg/L 07/21/2022
Nitrate Nitrogen(Cale)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.02 mg/L 07/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.11 mg/L 07/22/2022
Nitrate Nitrogen Subtraction Method 0.09 mg/L 07/29/2022
Total Nitrogen(Cale)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 <0.5 mg/L 07/27/2022
Total Nitrogen Total Nitrogen <0.5 mg/L 07/29/2022
ABOMIAIWI114410.M.IMMINMHIMMIMMA IMIYIVIMIIMMMIIOIIMIMPMIPWMI 11,1Millilrn1 II 1,1 MK,PAM. .16DIWEINNI MVIROMMONam.......—
Report IV 2022-13482 Page10o111

r 11 1 11. .
oil 1 II
Oil -II 11 v I Ili)t1 Oral 1111
1 le I " 1 II II a I I tail' i 'II, • 0 01 II ily....... 11 III 1 ists -.1111 ic.
6602 Windmill Way,Wilmington,NC 28405 s 910.392.0223 Lab s 910.392.4424 Fax
11111111111111111111111111v
1 II. 111111111111111111111111H111111101111111 I 11111HHIHIIIIIIII 11111IIII 710 Bowsertown Road,Manteo,NC 27954 s 252.473.5702 Lab/Fax
"`111,1111111111Ilviiiriiiiiiiii,
1 milli III
Mj Ili.
1' IIIIILI IIIIIi111111,1,,, 0 lio 255-A Wilmington Highway,Jacksonville,NC 28540 s 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Valley Proteins-Rose Hill Date of Report: Jul 29, 2022
Post Office Box 1026 Customer PO#:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Corey Lanier Report#: 2022-13482
Project ID: Monitoring Wells
,..----
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-32747 Site:MW-14A 7/18/2022 11:25 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color Color Clear/Tan Tint 07/18/2022
Depth to water, ft. Depth to Water,FL 4.4 feet 07/18/2022
Sodium EPA 200.7,Rev 4.4,1994 113 mg/L 07/25/2022
Sulfate EPA 300.0,Rev.2.1,1993 287 mg/L 07/19/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 07/27/2022
Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 07/18/2022
Odor Qualitative N/D 07/18/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 1280 mg/L 07/19/2022
Temperature SM 2550 B-2010 26.8 C 07/18/2022
pH SM 4500 H B-2011 4.9 units 07/18/2022
Total Phosphorus SM 4500 P(F-H)-2011 <0.04 mg/L 07/27/2022
Total Organic Carbon(TOC) SM 5310 B-2014 4.2 mg/L 07/19/2022
Fecal Col iform SM 9222 D-2015 MF <1 Colonies/100mL 07/18/2022
Chloride SM4500 CI E-2011 356 mg/L 07/21/2022
Nitrate Nitrogen(Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 <0.02 mg/L 07/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 3.03 mg/L 07/22/2022
Nitrate Nitrogen Subtraction Method 3.03 mg/L 07/29/2022
Total Nitrogen(Calc)
Total Kjeldahl Nitrogen(TKN) EPA 351.2,Rev.2.0,1993 0.7 mg/L 07/27/2022
Total Nitrogen Total Nitrogen 3.7 mg/L 07/29/2022
Comment:
Reviewed by: -14-
..._,........_......._ ..............................,__ _0., ..... ........._.......,...—
Report#:' 2022-13482 Page 11 of11

Date: 2? \ i i i Ortifiention e
Facility Name: ri: C/,r i 0"-'':- ))V b I EITI,i 6.„;6L EIIIIJ 4
Analyst: a '1 ),1t(-,e,,v4- Permit : c.;21,1 r.i.„„LE:
pH
Reference Method:SM4500 14+B-2011 Instrument ID ...,,_
Calibration Time Cal Buffer 4.0 sm. Cal Buffer 10.0 su. Check Buffer 7.0 s u. Comments
1(4) D,1“:) ( ( '
) . ., ( )
IL ,,cyf
,......__ ,
*pH check buffer must read within±0,1 pH units of the buffer's true value.
4 su buffer Lot#/:_,Rier a 4112869 Rim 11/22 7 su buffer Lot/0: Ricca 2112A,38 Eury, 12123 10 su buffer Lodf: RICCA 2112750 Earl 5/23
. — ....... . ------...—„„„..---„„—„.„--.....—
Sample Collection Sample Analysis pH Result liorPost-analysts Buffer'
Sample location Comments/Data Qualifiers
Time* Time* s.0 Check value s.u. ..
4) 1 14(r) 1112„„„. 6 ,,..[L) 1.
„.„.
1 0".1 c",:,1 1 D: t 1
I\ 1\I 171 11- k Lt 0 11, ,L3k 2- 5„DB
e; Pki, 1 i 1E: 3 ‘ I .61 >
. Post analysis huller cheek is required when performing analyses at multiple sampling locations and must be within±0.1 units of the buffer'sTrue value
All pH values in pH units(i.e.,s.u.).Record all data to the nearest 0,01 s.u.and report to the nearest 0,1 s.u.
Total Residual Chlorine(TRC)
Reference Method:SM 4500 C1-020 I I' Hach 8167 IIR Please circle a Iteable Method ,Instioment ID
Daily Check Post-analysis Time check Sample Sample
Check Sid TRC Result
Standard Result Standard Sample Collection Analysis Comments/Data Qualifiers
pg/L or mg/L (when analyzing Analyzed Location
Time Time pgor mg/L
at multiple sites) ,
,
TRC Daily Check Standard true value µg/L or mg/L acceptance range µg/L or mg/L
Check standards must recover within±10%of the check standard's true value
Annual Calibration Curve Verification Date: LOT/1 1DEXX 2109792 Exp.Date: 08/31/22
Reagent Blank Value: (When applicable.Analyze and document a reagent blank when standards,sample dilutions or PT Samples are prepared)
Dissolved Oxygen(DO)
Reference MethottSM 4500 0 0.-2011 Instrument ID
1 •Post-analysis calibration
Calibration/ Calibration variable Meter reading verification(when necessary)
Verification or%efficiency Comments
Time Ternperature Barometric after calibration Theoretical Calculated '
pressure Value mj/L .... Value mg/IL 1
Use this row when performing a verification instead of
Sample Collection *Sample Analysis DO reading
Sample Location Comments/Data Qualifiers
Time Time mg/L
I ;
•When performing analyses at multiple locations,the meter must be recalibrated at each site before analysis or a post-analysis calibration verification must be performed
*If sample is measured directly in the stream and/or onsite,only time analyzed would be recorded with a note that they are measured in situ or immediately
Temperature
Reference MethodSM 2550 B-2010 Instrument ID.
• , ,— —. ...........---..—
Sample *Sample Temperature
Sample Location Collection Analysis °C Comments/Data Qualifiers
Time Time
II,A,VI L U11 0
61 20,,"3 L ..., _6_ ._ . .....
M. v's1 I-II II D I IS 0',11 2 16;1'1- „ „„„„,„„„„„„„„„„„„„„„„„,,,
_IA v,,,1 -1 A• 11')..10 HA? 2_6 2... , ___.. .
pt,,,,,t. vj lii,il 11 ' SIII1, 11 '. 51 29
*If sample is measured directly in the stream and/or on site,only lime analyzed would be recorded,with a note that they are mer tn sured situ or immediately
Annual Venfteation Date ?„,;,
Field Personnel Note: QA.001
Rev 1-2022

. , , t Cerziltioo if. 9-1
Date: -7 1 ti''Z' 2_2......... Facility Name: V'4"-v-v,...il VC,vvvvi,_I.'kr.C.J.ri:-..::.V v.,)I.,,,,
Analyst: 'vj -lit:?4,1,:,.::,,,..iv e.,v-..' Permit tit' Lrd, f'"'(ti,:
pH
Reference Method:Slv14500 HHB-201.I Instrument ID,
• .:
Calibration Time Cal Buffer 4.0 s.u. Cal Buffer 10.0 su. Check Buffer 7.0 s u Comments
LI ,0')-- i,0, 0 I —1 „D II
— ...
*pH check buffer must read within±0.1 pH units of the buffer's true value.
4 su buffer Lott//: Ricca 4102869 by II/22 7 su buffer Lotill:„...Leca 2112A38 Las' 12/23 10 su buffer Lot/I: RICCA 2112750 EXD,5/23
Sample Collection Sample Analysis pH Result Il•PosT:Malysis Buffer
Sample location Comments/Data Qualifiers
Time* Time* s.0 Check value s.u. .
„,..„,uvv_i I)N''..• ("A,2...z) ci,, 2:2,..... il, 19
1,,./‘v\1, -- ii, i 16\- ci 3 2 (:::i ?,i..
4,14,0
i\--A W-4 2-15 (:--i'S""'.'S. ci .•,...5 4....... qr.,D 2„..,. _ .._,„„„,.
D' i-.‘,5; . c.i.,-
- • .......,.
Is. Post analysis buffer check is required when performing analyses at multiple sampling locations and must be within±0.1 units of the buffers true value
All pH values in pH units(i.e.,s.0).Record all data to the nearest 0.01 s.0 and repon to the nearest 0 I s u
li\INQ a 1 Lif C.-)'" i ,-;ks' i ii °,240.
Total Residual Chlorine(TRC)
Reference Method:SM 4500 CI-G201I! Hach 8167 HR: Please circle a plicable Method, ln.strument 10
Post-analysis
Daily Check Time check Sample Sample
Check Std. Sample TRC Result
Standard Result i Standard Collection Analysis Comments/Data Qualifiers
(when analyzng Location pg/L or mg/L
pg/L or mg/L Analyzed Time Time
at multiple sites) I „ , ••.• -
TRC Daily Check Standard true value µg/L or mg/L acceptance range it.g/L,or mg/L
Check standards must recover within±10%of the check standard's true value
Annual Calibration Curve Verification Date: LOT# 1DEXX 21Q9792 Exp.Date: 08/31/22
Reagent Blank Value: (When applicable.Analyze and document a reagent blank when standards,sample dilutions or PT Samples are prepared)
Dissolved Oxygen(DO)
—
Reference Method:SM 45000 G(20 I 1 Instrument ID:
---- —
•Post-analysis calibration
Calibration/ Calibration variable Meter reading verification(when necessary)
Verification or%efficiency . Comments
Time Barometric after calibration Theoretical Calculated
Temperature
pressure Value mg/L , Value mg/L
......... ... - . ...
Use this row when performing a verification instead of
calibration
Sample Collection *Sample Analysis DO reading
Sample Location Comments/Data Qualifiers
Time Time m
... . . .
•When performing analyses at multiple locations,the meter must be recalibrated at each site before analysis or a post-analysis calibration verification must be performed.
*If sample is measured directly in the stream ancVor onsite,only time analyzed would be recorded with a note that they are measured in situ or immediately
Temperature
Reference Method SM 25.50 B-20110 instrument ID:
,_... .
Sample *Sample Temperature
Sample Location Collection Analysis °C Comments/Data Qualifiers
Time Time
. , ......... ,. MINIIIIIIII.IIIIMII
k,,,,, ...
i Pi Icalti ft q.7)(j . ci ', 2:7- 2..:(, ‘
A• ()1 ?)).... 9 I,3 4 ne,3
,. cils-) 2:...q.,,9
I 1
4'; I' .4.g .,.. .,5,,,,,,i
If,sample is measured directly in tht;.stream sad/or on site,only time analyzed would be rec.orded,with a note ohm they are measured in situ or immediately
Annual Verification Date ,? -2...J,
--.:it t II ,,240 2"-C—fe'Field Personnel, our: QA.001
Rev 1-2022

Environmental Chemist, |nc� Q�Urn NC
~ ^'m^=, O6OZ Windmill Way
Wilmington, KCZO40S
910.382.0223
S8Mqple ,*�ece;ptChecklist
� /- k
C|ient��1/�( D�` �~/��1-?��'-��� Date: Report Number:_ 3O22-
A I Were custody seals present on the cooler?
11 YES 11 NO N/A 2. If—custudy seals were present,
Origina I temperature upon rece!pt 3,o Corrected temperature upon receipt *C1
How temperature taken: 0 Temperature Blank Against Bottles
IR Gun (D:Thomas Traceable SIN 192511657 IR Gun Correction Factor*C: 0.0
YES 0 NO 1 3. If temperature of cooler exceeded 6*C, was Project Mgr'./QA notified?
YES NO _47-Were proper custody procedures(relinquished/received)followed?
YES 10 NO 5. Were sample ID's listed on the COC?
V, YES 11 NO 6, Were samp[es'ID's-listed on sample containers?
YES [I Were ze
NO -� O VV � ------- -- - '
_ ' ststo be performed listed on the COC? ----- ---
YES O - --- ------
-
ES Cl N 0 '10. Did-samples I a.rrive i-n good condition for e.a ch test?
0 NO
'r. YES Ill. Was adequate sample volume available?'
1pn YES M NO 12. Were samples received-within proper holding time for requested tests?
JQ41 YES 0 NO 13. Were acid preserved samples received at a pH of<2?
YES. El NO 16, Were NH3/TKN/Phenol received at a chlorine residu-'
YES 11 NO' 1 17. Were Sulfide/Cyanide�e`e~.ed at a chlorine residual or<u.5m/L/
|LJ YES JO
VVereorthophos�hate�amp|esM|�ered/--hefi---------minute�? --|
! ����--- ---- - ' - --
�*
' TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. |
i** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet, \
Sample Preservation: (Must be completed for any somp/e(s) incorrectly preserved ' r with headspa~-~-� �
'Sample(s) were
_ U
�by adding(c|ndeone[ HxSO4 HNO3 H(J NaOH ' /
ITlmeof preservation: � /f more than one preservative is needed, notate in comments below
Iwotp�Notify customer service immediately for incorrectly preserved samples.Obtain a new sample o,
i notify the state lab if directed uz analyzed by the cyso,mer Who date� � `-
VniablesSamp|e(s) � _ =� =� were received with ead�a�
COMMENTS:
DOC. Q\OO2 Rev 1

� �Asue , 6602 Windmill Way Wilmington,NC 28405
„ - ' OFFICE:910-392-0223 FAX [phone]
Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
COLLECTION l
Client:Valley Proteins-Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 22 _ 1, - ..)i--g- Z
ADDRESS: CONTACT NAME: Susan Price PO NO:
REPORT TO: Corey Lanier PHONE/FAX:
COPY TO: email:
Sampled By: c -- SAMPLE TYPE:I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
Collection 2. PRESERVATION
I a, c . s c El w
Sample Identification w A" c a` 15 a `o c E m z n aa,, c i o o_ = ANALYSIS REQUESTED
gm g o z a x
I=te Time Temp u U z z = = I Z f o
!r,-) C P
MW: I LC-' MW G G 5a13 X NO , Chloride,TDS, Sulfate
Depth to water: 3 I G G S X L zok( NO3, NH3, TP,TN (talc)
C P _
[Gallons bailed: G G X t Na
C P
pH (field): 62 -y J i G G X Fecal Coliform
C p
Odor: 4.i c G G X TOC
C P
Color: r-jec-/ G G X VOC(November only)
C P -
G G
C P
i - G G
C P
G G i
Transfer Relinquished By: Date/Time Received By: Date/Time
Temperature when Received°C: Accepted: ejected: Resamp a equested:
cfg
Delivered By: Received By: --- Date: & Time:
Comments: T RNAROUND:

---'----- . I - 0 T I T I
4 6602 Windmill Way Wilmington,NC 28405
---- --_, -77-7 8 OFFICE:910-392-0223 FAX [phone]
NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client:Valley Proteins-Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 2_2- - t 34 s- 2.
ADDRESS: CONTACT NAME: Susan Price PO NO:
REPORT TO: Corey Lanier PHONE/FAX:
COPY TO: email:
Sampled By: .17 A.cl:', C4-,*=..—,..- SAMPLE TYPE: I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
Collection , PRESERVATION
,,,, , .,,, 3 A'_, a iti
Sample Identification E ,, ao ... ... 0 0 01 111 ''i' Ili ..., 6 a x 0 g ANALYSIS REQUESTED
1,3 1.- a 0 = z El =
u - c) z z = gmz 1,7,
fate Time Temp (-)
Mil 1111-- r 0 1-.1 C P
L ta. 0-
3a, x mw: mw G G 41, NO2, Chloride, IDS, Sulfate
" P
Depth to water: iaG G ' D,
X - NO3, NH3, TP, TN (calc)
A
Gallons bailed: 6 G G X Na
k-
pH (field):
Fecal Coliform
IMII II I
=MIMI. 11 C GP Millill
Odor: to,„c_ 111MIEMIIIIII 111311 .))))-_-,
X TOC
1111...1111111 C P
Color: c.-1C-di r‘i MIMI G EN X VOC (November only)
III MG
Mal P
I C P III 111111111111 RE
C P
G G
IMMETIZI Relinquished By: Date/Time Received By: Date/Time
1.
2.
Temperature when Received*C: 5 C. Accepted: t------ ------ Rejegted: Resampie Requested:
Delivered By: Received(__Z . .
By: ------' (--------) --) 1 - - t------------Date: / .cK 22-- Time:
Comments: I TURNAROUND:

I - • T L I I 6602 Windmill Way Wilmington,NC 28405
OFFICE:910-392-0223 FAX [phone]
NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client:Valley Proteins-Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: Z 2-- I 31.-k- - 2
'ADDRESS: ,CONTACT NAME: Susan Price PO NO:
REPORT TO: Corey Lanier PHONE/FAX:
COPY TO: email:
Sampled By: CC._ k j CI SAMPLE TYPE:I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
Collection a ._ De PRESERVATION
Sample Identification 1 2 w --- w 0 c 0 ea .0 0 c 1 C.I
—
g ?...- a 8 l'-' 1 's Lo—en gi i w 0 Li ANALYSIS REQUESTED
iio, I.- g o e EL .cc., E ...jm 0
Date Time Temp c-) a Z zb-
,
1 it12,2., 101) C P
MW: ei 1 L.S. 3-c mw G G ‘... ,„-9-. ,iX NO2, Chloride, TDS, Sulfate
C P
Depth to water: 3'7 G G .- ,SI X -2 p1-4- NO3, NH3, TP,TN (calc)
C P
Gallons bailed: S G G X Na
C P
pH (field): . 3,m. G G I X Fecal Coliform
C P
Odor: .4 D.'"1- G G ‘ „..:4 X TOC
• C P
Color: i e da G G
X VOC (November only)
I if'
"fro'ij "I C P
G G
C P
G G
C P
G G Transfer Relinquished By: Date/Time Received By: i Date/Time
I
rl.
12.
. .
Temperature when Received aC: --3'C Accepted: k--- „.. ---14r—tru—-tej 111:1.e . Resample Requested:
Delivered By: E C___, _Received By --------11, r - k.--- Date: T VV 722.--- Time: -22.1-1-i.
Comments: /
TURNAROUND:

-------,.. -------_N-.'--- I a T k I- . 6602 Windmill Way Wilmington,NC 28405
L
.- x OFFICE:910-392-0223 FAX [phone]
`:- ----',- -,-- \-..—'---
NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
CIlent:Valley Proteins-Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: -22-\ \-1 g2_
ADDRESS: CONTACT NAME: Susan Price PO NO:
REPORT TO: Corey Lanier PHONE/FAX:
COPY TO: email:
Sampled By: :01-'" ' .R7c r'--71-1Influent,SAMPLE TYPE:I= E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
,a' cc PRESERVATION
I I Collection . ,,, 12 & C_, 0 Lu
Sample Identification E-R.., a-. E. 1,-. I 5 '5 -7B",- co Ca 11.1 ...1 3 " = 0 FL' ANALYSIS REQUESTED
;A r- g - cs
Z Z = 2 X Z 1-* la
Date Time Temp
—
7)Ig 1121 flo
, C P
MW. 1 4 iz c.2- mw G G X
— NO2, Chloride, TDS, Sulfate
II C P
...
6/
—1 ,....,
Depth to water: G G i r0...-' X ak)it NO3, NH3,TP, TN (calc)
...-- C P I
Gallons bailed: 5 1 G G i
, X Q jvlitt Na
C ,
P f '
pH (field): (.0? G G
0
. X Fecal Coliform
C P
&
Odor: P•al— G G X TOC
C P
C.be-e..../
Color: G G X VOC (November only)
C P
G G
C P
G G
C P
G G , r
Transfer Relinquished By: Date/Time Received By:-----1 Date/Time
1.
2.
Temperature when Received*C: 3 0c Accepted: \---- ' -ejected: Resampi Re uested:
Delivered By: Received BY;--------- . . i 1 \__ .1.--- ---- Date: 1 I 2-2---Time: i 44
Comments: TURNAROUND:

I . T A I T I 6602 Windmill Way Wilmington,NC 28405
''----:- -- --, 77'.--— 3 OFFICE:910-392-0223 FAX [phone]
NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client:Valley Proteins-Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 2_-2 — i l-S, 2_
ADDRESS: CONTACT NAME: Susan Price PO NO:
REPORT TO: Corey Lanier PHONE/FAX:
COPY TO: email:
Sampled By: j ' - Fc_ SAMPLE TYPE:I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
r
)2. - a) PRESERVATION
Collection a 5' c_, Ow C I
Sample Identification I gt a 8 La It,7 8, 8 'a En 1 . ..„ ANALYSIS REQUESTED
€7) 1— E CD E
Date Time Temp C) u t.) Z z - Ex z 1- 8
711411 i f c 3"--' C P
,mw: g 4 mw G G [ J14I X i NO2, Chloride, TDS, Sulfate
eg C P
Depth to water: Cr 7 G G e"0/CD , I X'1 2- ti NO3, NH3,TP, TN (calc)
C P _..1 ...._
I
Gallons bailed: (-- G G 1 X ,'e -'elf- Na
I --
C P
pH (field): C 7 3 G G X i Fecal Coliform
r —
C P 1
l ,..Al'
Odor: it'^c- G G X TOC
C P I
)
Color: c-fc-...../ G G X VOC(November only)
C P
G G
C P
G G C P
G G
Transfer Relinquished By: Date/Time Received By: Dateirime
1.
2. I
Temperature when Received°C: ;-
.,_ c-
Accepted:_ - ----' ---- ReOtted: Resample Requested:
Delivered By: Received By: 1,, ._,,,-K. ike-4, 1,,‘-, CC-, _A—Date: •I -2 - 1: i-lx-R-
-
Comments: , TURNAROUND:

.t 6602 Windmill Way Wilmington,NC 28405
1 . TAL - 1 1
OFFICE:910-392-0223 FAX [phone]
NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
r- r
Client: Valley Proteins-Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 2-2-- 1 aLl g? _
ADDRESS: CONTACT NAME: Susan Price PO NO:
REPORT TO: Corey Lanier PHONE/FAX:
COPY TO: email:
r.,
Sampled By: ,_ ; /.-- i r- SAMPLE TYPE: I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil SL=Sludge,Other:
Collection d, •.,
PRESERVATION
a , i1 06
Sample Identification La _j 21 g ...2c .3 i.% ANALYSIS REQUESTED
E
LI 0
Date Time Temp L) z
Cfrillinimill III
ill 11111
MW: NO2, Chloride,TDS, Sulfate
„
Depth to water: Cz ME P
MIIIIIIIMMINENIIIIIIIIIIIIIN03, NH3, TP,TN (calc)
111.=.11111111. P 1111111=1111. . III
Gallons bailed: r MMIIIIIIMENIZI1=111111.Main M.Na
pH (field): C. ?4"'" B
P
G Fecal Coliform
Odor: ft*ow-- lif
G 11111111111111111111TOC
MINH
P
®
I
Color: 4A„ii 7./4 6..„1. MEI El G 11.1111111111111111111VOC (November onl )
III
B! itilll
c P
G G
C P
G G II
Relinquished By: Date/Time Received By: Date/Time
1. IIMNIIIIIMINIII
---- -
Temperature when Received')C: -----)------, I_ C Accepted: x----- ; Rejected: Resample Requested:
Delivered By: T(4 —7 i - ' 7 7
Received B . i l'' —1 I 1 1----------------Date: , ,'6'-—T i m e: 1 1+LI-ci
Comments: TURNAROUND:

im al A L I I 6602 Windmill Way Wilmington,NC 26405
OFFICE:910-392-0223 FAX [phone]
NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client:Valley Proteins-Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 2_2_— (3(-1 g2—,
ADDRESS: CONTACT NAME: Susan Price PO NO:
REPORT TO: Corey Lanier PHONE/FAX:
COPY TO: email:
Sampled By: SAMPLE TYPE:I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
1 I I ---t
Collection a ,_ PRESERVATION
jib •.0 • S _, 0 Et, — -
Sample Identification E ga,- a 8 E :1"--' 8 5.-. zi Ea la W al 3 " = t:) Ei ANALYSIS REQUESTED
E 0 g 2 m 6 2 4 2 2, =
u u z z = = = 0
Date Time Temp u
IfitAL 92.3 a C P r
MW: I A 7„?..i 4 MW G G " X NO2, Chloride, TDS, Sulfate
C P
Depth to water:qi G G I-0 i'.> I X —et' NO3, NH3, TP,TN (calc)
C P
L 2 -A\
Gallons bailed: 6 G G X -V ' Na
C P
pH (field): 1.15 G G X Fecal Conform
C P •
Odor: A°At G G 1 _/' X TOC
, 1,0
Color: E,le. of c i•J f' 1 C P
i 4
G G X VOC (November only)
C P
G G
C
G G
C P
1 r G G _ J
1
Transfer Relinquished By: Date/Time Received By: Date/Time
1.
2. 1-,—. - -„-----
Temperature when Received*C: -3.1) c Accepted: ------- I ejected: Resampie Requested:
Delivered By: Ii
.--' Received By: %---. ,.,1,4-\'b----1,1,__C l'___ 5„,--___- Date: S 2-2— Time: i 41-1--
_
Comments: TURNAROUND:

6602 Windmill Way Wilmington,NC 28405
T A L I T 8 I OFFICE:910-392-0223 FAX [phone]
_
NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client:Valley Proteins-Rose Hill IPROJECT NAME: Monitoring Wells REPORT NO: ,D,...D.-- ( T4
ADDRESS: CONTACT NAME: Susan Price PO NO:
REPORT TO: Corey Lanier PHONE/FAX:
i COPY TO: email:
,
Sampled By: vj r I rLf::- SAMPLE TYPE: I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
Collection . 2 1, rt PRESERVATION
Sample Identification ,..., i
`"
E >, imos- — c, 2 Im con o ANALYSIS REQUESTED
Ccio, i— § 0 5 „. .. E 5 =
u (3 Z
Date Time Temp U
,
lts12 9,2„ C P
MW: i/A- bc'S mw IMEM G 3-i-J-9-14 NO2, Chloride,TDS, Sulfate
e•
Depth to water: Co MEM
0
11111MiCil IME P _
!MOEN NO3, NH3, TP,TN (calc)
III 11
...*" 11111111=1
111 11
Gallons bailed, 4, 1111111611 I 111E11113.111111_ — 111111 pH (field): 41-6.° =II P
G Fecal Colif mill or
1111111111111
Odor. 4'1'4" MIN Is II TOC
P
G
Color: &foe 11111 P
G IIIII VOC(November only)
IEIIIIIIIIIIIIIIIIEIIIIIIIIIIIIIIIIIIIIIII
C P
I
G G
C P
G G
Transfer Relinquished By: Date/Time Received By: I Date/Time
CIIIIIIMMIIIIIIIIIIIIIIIIIIIIIIIIIMIIIIIIIIIIIIIIIIIMIIIIIIIIIBIIIIIMIIIIIIIIIIMIIIIIMIIIIIIMILIMIIMIIIIIIMI
Temperature when Received *C: 4-, ' (-__ Accepted: ,------- R- acted: Resample Requested:
Delivered By: E-i , , )
7 t iti
Received By: L __- .e----- - 1,..,_k.:_. ' k---Date: 2-2-Time: '1
1
Comments: TURNAROUND:

1 . 0 T A T 1
6602 Windmill Way Wilmington,NC 28405
OFFICE:910-392-0223 FAX [phone]
NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 info®environmentalchemists.com
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client: Valley Proteins-Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 7_2- I 3vi ga-
1
ADDRESS: CONTACT NAME: Susan Price PO NO:
REPORT TO: Corey Lanier PHONE/FAX:
COPY TO: email:
Sampled By: L-Fr--1-P5 SAMPLE TYPE:I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
Collection s , PRESERVATION
Til .o 2 61 I _11 2 I°
a El 0 s- ra ny a. 7- --. 1:0 1 -
Sample Identification E >, 0.0 ,- •50 2gl 9 2 a., _1 g 8 6 o E ANALYSIS REQUESTED
g — csfl.
C-11 =C." Z 2 = EE = 1— 8
Date Time Temp 0 1
11 18b1-cc( C P
MW: IL ) 104.9 mw a G G 33-14 X , , NO2, Chloride, TDS, Sulfate
C P
, —2 Itil
Depth to water: it; I G G LDS x - NO3, NH3, TP,TN (caic)
C P I
Gallons bailed: .4 G G ; X 4-2?r Na
C P ;
pH (field): i.r. al° G G i X Fecal Coliform
C P I
Odor: A.1 A z G G \-- X TOC
C P
l
Color: (......(f-s-1 G G IX VOC(November only)
_____ r_ ___
C P I
G G
C P
I ,
G i G
, T
Transfer Relinquished By: Date/Time Received By: Date/Time
1.
Temperature when Received''`C: ,,..
-'--' '-- Accepted: Rejec ed:, Resampl Requested:
Delivered By: 4E_ CM Received By:
; i '- --10 -1-. --€.-----Date: IS -2-2--Time: 4149
Comments: i TUR AROUND:

I j° 0 ' - ' I 7 I 6602 Windmill Way Wilmington,NC 28405
OFFICE:910-392-0223 FAX [phone]
NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
Analytical 8.Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client: Valley Proteins-Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 2-'2- -- g 2-
ADDRESS: CONTACT NAME: Susan Price PO NO:
REPORT TO: Corey Lanier PHONE/FAX:
COPY TO: email:
Sampled By: i F SAMPLE TYPE:I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
Collection I a, PRESERVATION
C....I 2 1 1
Sample Identification g g; a 's la _, i g. ...., x , i Eig, ANALYSIS REQUESTED
Is 1-- §E ca g ,_ a- E .f,.It = S 0 En 2 51 -3-: =
0 u z z = 2 = z
Date Time Temp t3
•
' i 5: /V c"------1„, C P
MIN: /5 A , '
2 e
(..•' -, MW G G (a(
NO2 Chloride,TDS, Sulfate
L__ .
C P ,
, er
Depth to water: L 3 G G I i,) x Lz t90- NO3, NH3, TP, TN (calc)
C P
,Gallons bailed: S G G .gtrt
v X-7"-ert Na
1 C P
pH (field): •1-7' G G X Fecal Coliform
C P
Odor: /1 2"14 4 G G X = TOC
Color: e....fed,-1 1 C P
G G X VOC (November only)
C P
G G
-- -
C P
_______ G G i
C P
I G G .
Transfer I Relinquished By: DateMme Received By: Date/Time
,1. —
2. -I - -1- -------- e
Temperature when Received *C: 3 13. Accepted: — ----- jected: Resample Requested:
, ,,,
Delivered By: E- tiM Received By:'---------e-< Date: 7 0 b 12
-4-7-Time: 1 4149
Comments: TURNAROUND:

`-'----7'-, an T 6602 Windmill Way Wilmington,NC 28405
0 k L. I ,
I
OFFICE:910-392-0223 FAX [phone]
NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client: Valley Proteins-Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 2_2__ I 34g. 2-
ADDRESS: CONTACT NAME: Susan Price PO NO:
REPORT TO: Corey Lanier PHONE/FAX:
1COPY TO: email:
Sampled By: .cre_P--) i E.c . SAMPLE TYPE:I=Influent,E=Effluent,W=Weil,ST=Stream,SO=Soil,SL=Sludge,Other:
Collection 1 w , ,..
,_ PRESERVATION
., 9 ai
Sample Identification g-gt a .6 .7 1.3 8 Is lin' z c13 Lai Z 1 v in Z I 04
C3 0 0 Q a' ANALYSIS REQUESTED
(tan x z I-- 0
E m 0 (3 a z 4 R
Date I Time , Temp 0
1-5 /IL
C
MW: PI
i ,
) L.C.47
) MW • G G 2c),f-4711-X i - NO2, Chloride,TDS, Sulfate
C P
II @
'.-- C1
Depth to water: 3 G G 4-0?) I X .4 c) NO3, NH3, TP,TN (calc)
, 55—
C P
Gallons bailed: S 1 G G X ----2._c)IC Na
- 5
pH (field): lie 9/ i C P G G i X
, - 1 Fecal Coliform
C P 1
Odor: iI"*."4. G G ‘).„...L.,,,,,---- X TOC
C P I
Color: c te46,14141 i.I'A 11- G G i X VOC(November only)
r !C P
i G G
C P
G G
C P
GIG i
—
Transfer Relinquished By: Date/Time I Received By: Date/Time
1.
2.
Temperature when Received"'IC: -Th-L) L_ Accepted: - ..---- jected: Resample Requested:
Ii 1 C
Delivered By: . CW.,_ Received By: (.___..# IIII-61-/- ' A---------- Date: 1 1 a ii
Time: --1---C 1
Comments: TURNAROUND: