NC0089958_Modification_20220822

ROY COOPER ;, - ,
Governor ,p� M
ELIZABETH S.BISER a==
M,0a.
Secretary :.
RICHARD E.ROGERS,JR. NORTH CAROLINA
Director Environmental Quality
August 22, 2022
TGACSE Central Square, LLC
Attn: Barry James, Project Manager
121 W Trade St, Ste 2550
Charlotte, NC 28202
Subject: Permit Renewal
Application No. NC0089958
Central Square
Mecklenburg County
Dear Applicant:
The Water Quality Permitting Section acknowledges the August 19, 2022 receipt of your permit modification application
and supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW
permitting branch. Per G.S. 150B-3 your current permit does not expire until permit decision on the application is made.
Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The
permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a
timely manner to requests for additional information necessary to allow a complete review of the application and renewal
of the permit.
Information regarding the status of your renewal application can be found online using the Department of Environmental
Quality's Environmental Application Tracker at:
https://deci.nc.gov/permits-regulations/permit-guidance/environmental-application-tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
Sincerely
Wren Thedford
Administrative Assistant
Water Quality Permitting Section
cc: Joseph P. Nestor-ECS
ec: WQPS Laserfiche File w/application
=DE Q North Carolina Department of Environmental Quality I Division of Water Resources
Mooresville Regional Office 610 East Center Avenue,Suite 301 Mooresville.North Carolina 28115
704.663.1699

Emmumbilm.:
ECS SOUTHEAST, L L P "Setting the Standard for Service"
Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engneering Firm F-1076
M.. Registered Geotrg sts Firm C-553
SC Reg stored Engineering Firm 3239
August 15, 2022
John Hennessy RECEIVED
North Carolina Department of Environmental Quality l. 9
1 2022
Division of Water Resources
Water Quality Permitting Section-NPDES p�
1617 Mail Service Center NCDEQIDWRINPDES
Raleigh, NC 27699-1617
Reference: Request for Permit Modification for Flow
National Pollutant Discharge Elimination System (NPDES) Perrrfit No. NC0089958
Central Square
Located Southwest of Intersection of Central Avenue and Pecan Avenue
Charlotte, North Carolina
ECS Project No. 10756-C
Dear Mr. Hennessy:
ECS Southeast, LLP (ECS) prepared this request for flow modification for the referenced permit on behalf of
TGACSE Central Square, LLC. You may recall we had a conference call regarding this matter in June of this
year.
Construction activities are ongoing at this site. Foundation construction requires dewatering. The original
permit application assumed that no more than 50,000 gallons per day(GPD) (or 01.'050 million gallons per day
[MGD])of groundwater would be extracted and discharged. After construction began,it became apparent that
additional flow capacity is needed to dewater the area for foundation construction. Groundwater has been
extracted,treated,and discharged since March 2022. Although there were some low-level detections of volatile
organic compounds (VOCs) in the effluent in March 2022, the treatment system appears to be effectively
removing VOCs. There were no detections of VOCs in April, May, or June 2022. The VOC detection in March
2022 may have been the result of the granular activated carbon (GAC) media not being fully wetted at system
startup. Attached to this package are copies of electronic Discharge Monitoring Reports (eDMRs) and
laboratory reports for March,April,and May 2022. Also attached our lab reports for June 2022.
As we discussed during our conference call,we wish to have the permit modified to increase the permitted flow
to the rated capacity of the existing treatment system. The system is rated at 50 gallons per minute (GPM)
72,000 GPD or 0.072 MGD. No modifications of the system are proposed.
Per our discussions,we are submitting EPA Form 1,EPA Form 2C,and EPA Form 2E. Attachments are required
for each form are generally duplicative. Therefore, one set of attachments to the forms are included with
his submittal. We understand from our discussions that an Engineering Alternatives Analysis (EAA )is not
required for this permit modification request.
EPA Form 2C includes several tables for existing effluent data including the concentrations of certain parameters
in the effluent. For those tables, we utilized average concentrations from the effluent monitoring data for
March,April,May,and June 2022.
Also attached to this package is a check for$260 to cover the permit modification for a Minor Individual Permit.

Request for Permit Modification for Flow
NPDES Permit No. NC0089958
ECS Project No. 10756-C
August 15,2022
Page 2
If you have any questions or comments concerning the contents of the enclosed documents or other related
topics,please feel free to contact us.
Respectfully submitted,
ECS SOUTHEAST, LLP
I, P. ittW7
/seph P. Nestor, P.G., P.E. Roger A. Smith, P.G.
Environmental Principal Principal Geologist
[e-mail] [e-mail]
704-280-7422 704-552-5152
Enclosure: Check for Permit Modification Fees
EPA Form 1
EPA Form 2C
EPA Form 2E
Topographic Map
Map Showing City of Charlotte Stormwater System Infrastructure and Discharge Point
Line Drawing
Process& Instrumentation Diagram
eDMRS with Effluent Laboratory Data for March,April,and May 2022
Laboratory Reports for Effluent for June 2022

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 Cental Square OMB No.2040-0004
Form U.S. Environmental Protection Agency
1 *- EPA Application for NPDES Permit to Discharge Wastewater
NPDES GENERAL INFORMATION
SECTION 1.ACTIVITIES REQUIRING AN NPDES PERMIT(40 CFR 122.21(f)and(f)(1))
1.1 Applicants Not Required to Submit Form 1
Is the facility a new or existing publicly owned Is the facility a new or existing treatment works
1.1.1 12
treatment works? 1. . treating domestic sewage?
If yes, STOP. Do NOT complete ❑✓ No If yes, STOP. Do NOT No
Form 1. Complete Form 2A. complete Form 1. Complete
Form 2S.
1.2 Applicants Required to Submit Form 1
1.2.1 Is the facility a concentrated animal feeding 1.2.2 Is the facility an existing manufacturing,
operation or a concentrated aquatic animal commercial,mining,or silvicultural facility that is
n production facility? currently discharging process wastewater?
o ❑ Yes 3 Complete Form 1 E✓ No ✓❑ Yes 4 Complete Form ❑ No
a and Form 2B. 1 and Form 2C.
1.2.3 Is the facility a new manufacturing,commercial, 1.2.4 Is the facility a new or existing manufacturing,
rn mining, or silvicultural facility that has not yet commercial,mining,or silvicultural facility that
commenced to discharge? discharges only nonprocess wastewater?
Yes 4 Complete Form 1 0✓ No ❑ Yes 4 Complete Form �✓ No
and Form 2D. 1 and Form 2E.
1.2.5 Is the facility a new or existing facility whose
--.0 discharge is composed entirely of stormwater
a associated with industrial activity or whose
discharge is composed of both stormwater and
non-stormwater?
El Yes 4 Complete Form 1 0✓ No
and Form 2F
unless exempted by
40 CFR
122.26(b)(14)(x)or
b 15 .
SECTION 2.NAME,MAILING ADDRESS,AND LOCATION(40 CFR 122.21(f)(2))
2.1 Facility Name
Central Square
O 2.2 EPA Identification Number
co
co
0
-J
2.3 Facility Contact
Name(first and last) Title Phone number
Barry James ZConstruction Project Manager [phone]
a
rn Email address
:F$ [e-mail]
2.4 Facility Mailing Address
Street or P.O. box
c/o Crosland Southeast;201 South College Street,Suite 1300
City or town State ZIP code
Charlotte NC 28244
EPA Form 3510-1(revised 3-19) Page 1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 Cental Square OMB No.2040-0004
N 2.5 Facility Location
. . Street, route number,or other specific identifier
Q 0 1314 1318,1322,1324,1326,1330, 1332,1334,1336,1400,and 1426 Central Av&1111, 1113,and 1235 Pecan Av
c o County name County code(if known)
Mecklenburg
o
City or town State ZIP code
Charlotte NC 28205
-ECTION 3.SIC AND NAICS CODES(40 CFR 122.21(f)(3))
3.1 SIC Code(s) Description(optional)
653100100 Real Estate Agents and Mangers
62829905 Manager Of Mutual Funds,Contract or Fee Basis
TBD Tentants for retail space have not leased space
U
6513 Operators of Apartment Buildings
U
3.2 NAICS Code(s) Description(optional)
coo 531190 Lessors of Other Real Estate Property
U
523920 Portfolio Management
TBD Tentants for retail space have not leased space
531311 Residential Property Managers
.ECTION 4.OPERATOR INFORMATION(40 CFR 122.21(f)(4))
4.1 Name of Operator
TGACSE Central Square,LLC(Attn.Mr.Barry James)
0 4.2 Is the name you listed in Item 4.1 also the owner?
✓❑ Yes ❑ No
4.3 Operator Status
0
co ❑ Public—federal ❑ Public—state ❑ Other public(specify)
o ❑✓ Private ❑ Other(specify)
4.4 Phone Number of Operator
[phone]
4.5 Operator Address
Street or P.O. Box
cis
o L a'
City or town State ZIP code
o Charlote NC 28244
m U
Q Email address of operator
0 [e-mail]
SECTION 5.INDIAN LAND(40 CFR 122.21(f)(5))
a -0 5.1 Is the facility located on Indian Land?
Cco
J ❑ Yes ❑✓ No
EPA Form 3510-1(revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 Cental Square OMB No.2040-0004
.ECTION 6. EXISTING ENVIRONMENTAL PERMITS(40 CFR 122.21(f)(6))
6.1 Existing Environmental Permits(check all that apply and print or type the corresponding permit number for each)
❑ NPDES(discharges to surface ❑ RCRA(hazardous wastes) ❑ UIC(underground injection of
water) fluids)
o NC0089958
> E
w ❑ PSD(air emissions) ❑ Nonattainment program(CM) ❑ NESHAPs(CM)
w ❑ Ocean dumping(MPRSA) ❑ Dredge or fill(CWA Section 404) ❑ Other(specify)
.ECTION 7.MAP(40 CFR 122.21(f)(7))
7.1 Have you attached a topographic map containing all required information to this application?(See instructions for
e specific requirements.)
❑✓ Yes ❑ No ❑ CAFO—Not Applicable(See requirements in Form 2B.)
•ECTION 8.NATURE OF BUSINESS(40 CFR 122.21(f)(8))
8.1 Describe the nature of your business.
The site is being redeveloped as a vertically integrated mixed-use project.The site will be used for office,parking
(surface and below grade),retail,commercial,multifamily residential,recreational,and entertainment.
N
d
N
m
O
d)
CC
•ECTION 9.COOLING WATER INTAKE STRUCTURES(40 CFR 122.21(f)(9))
9.1 Does your facility use cooling water?
d ❑ Yes ❑ No 4 SKIP to Item 10.1.
i 9.2 Identify the source of cooling water. (Note that facilities that use a cooling water intake structure as described at
e 40 CFR 125, Subparts I and J may have additional application requirements at 40 CFR 122.21(r). Consult with your
o NPDES permitting authority to determine what specific information needs to be submitted and when.)
O R
U �
SECTION 10.VARIANCE REQUESTS(40 CFR 122.21(f)(10))
10.1 Do you intend to request or renew one or more of the variances authorized at 40 CFR 122.21(m)?(Check all that
apply.Consult with your NPDES permitting authority to determine what information needs to be submitted and
11, when.)
C ❑ Fundamentally different factors(CWA ❑ Water quality related effluent limitations(CWA Section
Section 301(n)) 302(b)(2))
El Non-conventional pollutants(CWA ❑ Thermal discharges(CWA Section 316(a))
Section 301(c)and(g))
❑✓ Not applicable
EPA Form 3510-1(revised 3-19) Page 3

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 Cental Square OMB No.2040-0004
SECTION 11.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d))
11.1 In Column 1 below, mark the sections of Form 1 that you have completed and are submitting with your application.
For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority. Note
that not all applicants are required to provide attachments.
Column 1 Column 2
❑✓ Section 1:Activities Requiring an NPDES Permit ❑ w/attachments
❑✓ Section 2: Name, Mailing Address,and Location ❑ w/attachments
❑✓ Section 3: SIC Codes ❑ w/attachments
❑✓ Section 4: Operator Information ❑ w/attachments
❑✓ Section 5: Indian Land ❑ w/attachments
❑ Section 6: Existing Environmental Permits ❑ w/attachments
El Section 7: Map ma topographic ❑✓ wl additional attachments
Y
❑✓ Section 8: Nature of Business ❑ w/attachments
w ❑✓ Section 9: Cooling Water Intake Structures ❑ w/attachments
CD
C ❑✓ Section 10:Variance Requests ❑ w/attachments
❑✓ Section 11:Checklist and Certification Statement ❑ w/attachments
11.2 Certification Statement
v
1 certify under penalty of law that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate,and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fine and imprisonment for knowing violations.
Name(print or type first and last name) Official title
641/11_44S.1 c t4a \ Uf -
Signature Date signed
€14
EPA Form 3510-1(revised 3-19) Page 4

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 OMB No.2040-0004
Central Square Excavation
Form U.S. Environmental Protection Agency
2C .sEPA Application for NPDES Permit to Discharge Wastewater
NPDES EXISTING MANUFACTURING,COMMERCIAL,MINING,AND SILVICULTURE OPERATIONS
SECTION 1.OUTFALL LOCATION(40 CFR 122.21(g)(1))
1.1 Provide information on each of the facility's outfalls in the table below.
o Numbelr Receiving Water Name Latitude Longitude
as
001 Trib.to Little Sugar Creek 35` 13' 25.0" 80° 19' 7.7'
11
y o
O
SECTION 2.LINE DRAWING(40 CFR 122.21(g)(2))
a, 2.1 Have you attached a line drawing to this application that shows the water flow through your facility with a water
_ 3 balance?(See instructions for drawing requirements.See Exhibit 2C-1 at end of instructions for example.)
co
❑✓ Yes ❑ No
SECTION 3.AVERAGE FLOWS AND TREATMENT(40 CFR 122.21(g)(3))
3.1 For each outfall identified under Item 1.1, provide average flow and treatment information.Add additional sheets if
necessary.
**Outfall Number** 001
Operations Contributing to Flow
Operation Average Flow
Dewatering 0.072 mgd
mgd
mgd
mgd
Treatment Units
Description Code from Final Disposal of Solid or
12 (include size,flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
retention time,etc.) by Discharge
18,000 Gallon Frac Tank 1-U LANDFILL
1,000 Gallonn Surge Tank 1-0
Rwo 1,000 Poun GAC Vesels 2-A LANDFILL
EPA Form 3510-2C(Revised 3-19) Page 1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 OMB No.2040-0004
Central Square Excavation
3.1 **Outfall Number**
cont. Operations Contributing to Flow
Operation Average Flow
mgd
mgd
mgd
mgd
Treatment Units
Description Code from Final Disposal of Solid or
(include size,flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
retention time,etc.) by Discharge
d
0
V
Qc
G
o
o
**Outfall Number**
Operations Contributing to Flow
o Operation Average Flow
mgd
a-
0
>
' mgd
mgd
mgd
Description Code from Final Disposal of Solid or
(include size,flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
retention time,etc.) by Discharge
3.2 Are you applying for an NPDES permit to operate a privately owned treatment works?
0 ❑✓ Yes ❑ No 4 SKIP to Section 4.
cn M 3.3 Have you attached a list that identifies each user of the treatment works?
❑ Yes ❑✓ No
EPA Form 3510-2C(Revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 OMB No.2040-0004
Central Square Excavation
SECTION 4.INTERMITTENT FLOWS(40 CFR 122.21(g)(4))
4.1 Except for storm runoff,leaks,or spills, are any discharges described in Sections 1 and 3 intermittent or seasonal?
❑ Yes ❑✓ No 4 SKIP to Section 5.
4.2 Provide information on intermittent or seasonal flows for each applicable outfall. Attach additional pages,if necessary.
Outfall Operation Frequency Flow Rate
Number (list) Average Average Long-Term Maximum Duration
Days/Week Months/Year Average Daily
days/week months/year mgd mgd days
days/week months/year mgd mgd days
u_
days/week months/year mgd mgd days
m days/week months/year mgd mgd days
.
.c.
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
SECTION 5.PRODUCTION(40 CFR 122.21(g)(5))
5.1 Do any effluent limitation guidelines(ELGs)promulgated by EPA under Section 304 of the CWA apply to your facility?
❑ Yes ❑✓ No 4 SKIP to Section 6.
u 5.2 Provide the following information on applicable ELGs.
ELG Category ELG Subcategory Regulatory Citation
d
.Q
a
5.3 Are any of the applicable ELGs expressed in terms of production(or other measure of operation)?
❑ Yes ❑ No 4 SKIP to Section 6.
O
5.4 Provide an actual measure of daily production expressed in terms and units of applicable ELGs.
Outfall Operation, Product,or Material Quantity per Day Unit of
-a Number Measure
d
fC
O
V
.O
O
L
a
EPA Form 3510-2C(Revised 3-19) Page 3

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 OMB No.2040-0004
Central Square Excavation
SECTION 6.IMPROVEMENTS(40 CFR 122.21(g)(6))
6.1 Are you presently required by any federal,state,or local authority to meet an implementation schedule for constructing,
upgrading,or operating wastewater treatment equipment or practices or any other environmental programs that could
affect the discharges described in this application?
❑ Yes ❑✓ No 4 SKIP to Item 6.3.
6.2 Briefly identify each applicable project in the table below.
Affected Final Compliance Dates
Brief Identification and Description of Outfalls Source(s)of
o Project (list outfall Discharge Required Projected
number)
co
G)
a
6.3 Have you attached sheets describing any additional water pollution control programs(or other environmental projects
that may affect your discharges)that you now have underway or planned?(optional item)
❑ Yes ❑ No ❑ Not applicable
SECTION 7.EFFLUENT AND INTAKE CHARACTERISTICS(40 CFR 122.21(g)(7))
See the instructions to determine the pollutants and parameters you are required to monitor and,in turn,the tables you must
complete. Not all applicants need to complete each table.
Table A.Conventional and Non-Conventional Pollutants
7.1 Are you requesting a waiver from your NPDES permitting authority for one or more of the Table A pollutants for any of
your outfalls?
❑✓ Yes ❑ No 4 SKIP to Item 7.3.
7.2 If yes, indicate the applicable outfalls below.Attach waiver request and other required information to the application.
Outfall Number 001 Outfall Number Outfall Number
7.3 Have you completed monitoring for all Table A pollutants at each of your outfalls for which a waiver has not been
requested and attached the results to this application package?
No; a waiver has been requested from my NPDES
✓❑ Yes ❑ permitting authority for all pollutants at all outfalls.
Table B.Toxic Metals,Cyanide,Total Phenols, and Organic Toxic Pollutants
7.4 Do any of the facility's processes that contribute wastewater fall into one or more of the primary industry categories
co
listed in Exhibit 2C-3?(See end of instructions for exhibit.)
❑ Yes ✓❑ No 4 SKIP to Item 7.8.
7.5 Have you checked"Testing Required"for all toxic metals,cyanide, and total phenols in Section 1 of Table B?
LL, ❑ Yes ❑ No
7.6 List the applicable primary industry categories and check the boxes indicating the required GC/MS fraction(s)identified
in Exhibit 2C-3.
Primary Industry Category Required GC/MS Fraction(s)
(Check applicable boxes.)
❑Volatile ❑Acid 0 Base/Neutral 0 Pesticide
❑Volatile 0 Acid 0 Base/Neutral 0 Pesticide
0 Volatile 0 Acid 0 Base/Neutral 0 Pesticide
EPA Form 3510-2C(Revised 3-19) Page 4

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 OMB No.2040-0004
Central Square Excavation
7.7 Have you checked"Testing Required"for all required pollutants in Sections 2 through 5 of Table B for each of the
GC/MS fractions checked in Item 7.6?
❑ Yes ❑ No
7.8 Have you checked"Believed Present"or"Believed Absent"for all pollutants listed in Sections 1 through 5 of Table B
where testing is not required?
❑✓ Yes 0 No
7.9 Have you provided(1)quantitative data for those Section 1,Table B, pollutants for which you have indicated testing is
required or(2)quantitative data or other required information for those Section 1,Table B, pollutants that you have
indicated are"Believed Present"in your discharge?
O Yes 0 No
7.10 Does the applicant qualify for a small business exemption under the criteria specified in the instructions?
❑ Yes 4 Note that you qualify at the top of Table B, ❑ No
then SKIP to Item 7.12.
03
= 7.11 Have you provided(1)quantitative data for those Sections 2 through 5,Table B, pollutants for which you have
o determined testing is required or(2)quantitative data or an explanation for those Sections 2 through 5,Table B,
N pollutants you have indicated are"Believed Present"in your discharge?
`—' ✓❑ Yes ❑ No
Table C.Certain Conventional and Non-Conventional Pollutants
7.12 Have you indicated whether pollutants are"Believed Present"or"Believed Absent"for all pollutants listed on Table C
for all outfalls?
heEl Yes El No
Y
7.13 Have you completed Table C by providing(1)quantitative data for those pollutants that are limited either directly or
= indirectly in an ELG and/or(2)quantitative data or an explanation for those pollutants for which you have indicated
"Believed Present"?
❑Q Yes ❑ No
LL, Table D.Certain Hazardous Substances and Asbestos
7.14 Have you indicated whether pollutants are"Believed Present"or"Believed Absent"for all pollutants listed in Table D for
all outfalls?
p Yes El No
7.15 Have you completed Table D by(1)describing the reasons the applicable pollutants are expected to be discharged
and(2)by providing quantitative data, if available?
❑✓ Yes ❑ No
Table E.2,3,7,8-Tetrachlorodibenzo-p-Dioxin(2,3,7,8-TCDD)
7.16 Does the facility use or manufacture one or more of the 2,3,7,8-TCDD congeners listed in the instructions,or do you
know or have reason to believe that TCDD is or may be present in the effluent?
❑ Yes 4 Complete Table E. ❑✓ No 4 SKIP to Section 8.
7.17 Have you completed Table E by reporting qualitative data for TCDD?
O Yes ❑ No
SECTION 8.USED OR MANUFACTURED TOXICS(40 CFR 122.21(g)(9))
8.1 Is any pollutant listed in Table B a substance or a component of a substance used or manufactured at your facility as
an intermediate or final product or byproduct?
CD
❑ Yes ✓❑ No 4 SKIP to Section 9.
ri 8.2 List the pollutants below.
g 1. 4. 7.
2. 5. 8.
M
3. 6. 9.
EPA Form 3510-2C(Revised 3-19) Page 5

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 OMB No.2040-0004
Central Square Excavation
SECTION 9.BIOLOGICAL TOXICITY TESTS(40 CFR 122.21(g)(11))
9.1 Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made
within the last three years on (1)any of your discharges or(2)on a receiving water in relation to your discharge?
,� ❑ Yes ❑ No 4 SKIP to Section 10.
I"- 9.2 Identify the tests and their Jurposes below.
Test(s) Purpose of Test(s) Submitted to NPDES Date Submitted
Permitting Authority?
0
I-
o ❑ Yes ❑ No
C)
_O
o
' ❑ Yes ❑ No
❑ Yes ❑ No
SECTION 10.CONTRACT ANALYSES(40 CFR 122.21(g)(12))
10.1 Were any of the analyses reported in Section 7 performed by a contract laboratory or consulting firm?
❑✓ Yes ❑ No 4 SKIP to Section 11.
10.2 Provide information for each contract laboratory or consulting firm below.
Laboratory Number 1 Laboratory Number 2 Laboratory Number 3
Name of laboratory/firm Waypoint Analytical
N
7, Laboratory address 449 Springbrook Road
Charlotte,NC 28217
a
R
L
Phone number
[phone]
Pollutant(s)analyzed
ph,VOCs,PAHs,metals
SECTION 11.ADDITIONAL INFORMATION(40 CFR 122.21(g)(13))
11.1 Has the NPDES permitting authority requested additional information?
❑ Yes ❑✓ No 4 SKIP to Section 12.
0
11.2 List the information requested and attach it to this application.
0
1. 4.
0
2. 5.
3. 6.
EPA Form 3510-2C(Revised 3-19) Page 6

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 Central Square Excavation OMB No.2040-0004
SECTION 12.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d))
12.1 In Column 1 below, mark the sections of Form 2C that you have completed and are submitting with your application.
For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority. Note
that not all applicants are required to complete all sections or provide attachments.
Column 1 Column 2
✓❑ Section 1: Outfall Location ❑✓ w/attachments
O Section 2: Line Drawing ✓❑ w/line drawing ❑ wl additional attachments
171 Section 3:Average Flows and wl list of each user of
Treatment ❑ w/attachments ❑ privately owned treatment
works
O Section 4: Intermittent Flows ❑ w/attachments
0 Section 5: Production ❑ w/attachments
w/optional additional
❑✓ Section 6: Improvements ❑ w/attachments ❑ sheets describing any
additional pollution control
plans
❑ w/request for a waiver and ❑ w/explanation for identical
supporting information outfalls
wl small business exemption w/other attachments
❑ request ❑
co Section 7: Effluent and Intake ❑ wl Table A © w/Table B
Characteristics
0
❑✓ wl Table C ❑✓ wl Table D
d ❑✓ wl Table E ❑ wl analytical results as an
c) attachment
R ❑✓ Section 8: Used or Manufactured ❑ wl attachments
Toxics
Section 9: Biological Toxicity
d ❑ Tests ❑ w/attachments
U
❑ Section 10: Contract Analyses ❑ w/attachments
❑✓ Section 11:Additional Information ❑ w/attachments
✓❑ Section 12:Checklist and ❑ wl attachments
Certification Statement
12.2 Certification Statement
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly
responsible for gathering the information, the information submitted is,to the best of my knowledge and belief, true,
accurate. and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fine and imprisonment for knowing violations.
Name(print or type first and last name) Official title
1,4 VI-► 1 u > A "`ic,,✓,
Signature Date signed
I\ zZ
EPA Form 3510-2C(Revised 3-19) Page 7

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation
TABLE A.CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(iii))1
Effluent Intake
Waiver — (Optional)
Pollutant Requested Units Maximum Maximum Long-Term
(if applicable) (specify) Daily Monthly Average Daily Number of Long-Term Number of
Discharge Discharge Discharge Analyses Average Value Analyses
(required) (if available) (if available)
❑ Check here if you have applied to your NPDES permitting authority for a waiver for all of the pollutants listed on this table for the noted outfall.
Biochemical oxygen demand Concentration
1. (BODs) ❑ Mass
Chemical oxygen demand Concentration
2.
(COD) ❑ Mass
Concentration
3. Total organic carbon(TOC) ❑✓
Mass
Concentration
4. Total suspended solids(TSS) 0
Mass No Data
Concentration
5. Ammonia(as N) ❑✓
Mass
6. Flow ❑ Rate 0.072 MGD
Temperature(winter) ❑✓ °C °C
7.
Temperature(summer) ❑✓ °C °C
pH(minimum) ❑ Standard units S.U. 6.09
8.
pH(maximum) ❑ Standard units S.U. 6.23
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e., methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I, subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 9

z
a)
ccs
vp
•
f-^

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
Daily
Discharge Discharge Discharge Analyses
Average Analyses
(required) (if available) Value
(if available)
❑ Check here if you qualify as a small business per the instructions to Form 2C and,therefore,do not need to submit quantitative data for any of the organic toxic pollutants in Sections
2 through 5 of this table. Note,however,that you must still indicate in the appropriate column of this table if you believe any of the pollutants listed are present in your discharge.
Section 1.Toxic Metals,Cyanide,and Total Phenols
Antimony,total Concentration
1.1 (7440-36-0) El 0 Mass
Arsenic,total Concentration
1.2 (7440-38-2) Mass
Beryllium,total Concentration
1.3 El
(7440-41-7) Mass
Cadmium,total Concentration
1.4 (7440 43 9) ❑✓ El
Mass
Chromium,total Concentration 4.29ug/L
1.5 (7440-47-3) Mass 0.003#
Copper, total Concentration
1.6 (7440-50-8) Mass
Lead, total Concentration 0.13 ug/L
1.7 0
(7439-92-1) El El Mass o.0001#
Mercury, total Concentration
1.8 (7439-97-6) Mass
1 9 Nickel,total El
Concentration 0.85 ug/L
(7440-02-0) Mass o.00i#
1.10 Selenium, total Concentration
(7782-49-2) Mass
1.11 Silver, total Concentration
El ElEl
(7440-22-4) Mass
EPA Form 3510-2C(Revised 3-19) Page 11

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Maximum Maximum Long-Term Long
(and CAS Number,if available) Required Believed Believed (specify) Average Number Number
Present Absent Daily Monthly Term
Daily of of
Discharge Discharge Average
(required) (if available) Discharge Analyses Analyses
Value
if available
Thallium,total Concentration
1.12 (7440-28-0) Mass
Zinc, total Concentration 1.6 ug/L
1.13 (7440-66-6) Mass o.001#
Cyanide, total Concentration
1.14 (57-12-5) Mass
1.15 Phenols,total ❑ 0 0
Concentration
Mass
Section 2. Organic Toxic Pollutants(GC/MS Fraction—Volatile Compounds)
Acrolein Concentration
2.1 (107-02-8) ✓ Mass
Acrylonitrile Concentration
2,2 (107-13-1) Mass
Benzene CI ❑ ❑ Concentration 0.12 ug/L
2.3 (71-43-2) Mass 0.00007 4
2.4 Bromoform Concentration
(75-25-2) Mass
2.5 Carbon tetrachloride � Concentration
(56-23-5) Mass
Chlorobenzene Concentration
2.6 (108-90-7) Mass
2.7 Chlorodibromomethane Concentration
(124-48-1) Mass
Chloroethane Concentration
2.8 (75-00-3) Mass
EPA Form 3510-2C(Revised 3-19) Page 12

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
PollutantlParameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
Daily of of
Discharge Discharge Average
(required) (if available) Dischar(ifavailable)ge Analyses Value Analyses
2-chloroethylvinyl ether Concentration
2.9 0 0 0 ,
(110-75-8)
Mass
2.10 Chloroform(67-66-3) E Concentration
Mass
2.11 Dichlorobromomethane ❑ 0 Concentration
(75-27-4) Mass
212 11-dichloroethane 0 0 Concentration
(75-34-3) Mass
1,2-dichloroethane ✓ Concentration 0.77ug/L
2.13 CI CI
(107-06-2) Mass 0.462#
2.14 1,1-dichloroethylene 0 ❑ Concentration
(75-35-4) Mass
2.15 12-dichloropropane ID 0 0 Concentration
(78-87-5) Mass
1,3-dichloropropylene Concentration
2.16 (542-75-6) Mass
2.17 Ethylbenzene Concentration 4.61 ug/L
(100-41-4) Mass 2.768#
2.18 Methyl bromide 0Q Concentration
(74-83-9) Mass
2.19 Methyl chloride Concentration
(74-87-3) Mass
2.20 Methylene chloride 00Concentration
(75-09-2) Mass
2.21 1,1,2,2-tetrachloroethane Concentration
(79-34-5) Mass
EPA Form 3510-2C(Revised 3-19) Page 13

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge Average
(required) (if available) Discharge Analyses Value Analyses
(if available)
2.22 Tetrachloroethylene 0 Concentration 1.03 ug/L
(127-18-4) Mass 0.618#
Toluene ❑ ❑ Concentration 0.64ug/L
2.23 (108-88-3) Mass 0.0384#
2.24 1,2-trans-dichloroethylene � Concentration
(156-60-5) Mass _
2.25 1 1,1-trichloroethane 0Concentration
(71-55-6) Mass
2.26 1,1,2-trichloroethane ❑✓ ElConcentration
(79-00-5) Mass
2.27 Trichloroethylene 0Concentration
(79-01-6) Mass
2.28 Vinyl chloride Concentration
(75-01-4) Mass
Section 3. Organic Toxic Pollutants(GC/MS Fraction-Acid Compounds)
3.1 2-chlorophenol Q Concentration
ID ED
(95-57-8) Mass
2,4-dichlorophenol Concentration
3.2 (120-83-2) Mass
2,4-dimethylphenol Concentration
3.3 (105-67-9) Mass
3.4 4,6-dinitro-o-cresol ❑ Concentration
(534-52-1) Mass
3.5 2,4-dinitrophenol 0Concentration
(51-28-5) Mass
EPA Form 3510-2C(Revised 3-19) Page 14

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units I Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
Discharge
(requied) (if available) Discharge Analyses AverageValue Analyses
(if available)
2-nitrophenol Concentration
3.6 (88-75-5) Mass
3.7 4-nitrophenol 0 Concentration
0 0
(100-02-7) Mass
3.8 p-chloro-m-cresol 0 Concentration
0 El
(59-50-7) Mass
3.9 Pentachlorophenol 0 Concentration
(87-86-5) Mass
Phenol Concentration
3.10 (108-95-2) Mass
3.11 2,4,6-trichlorophenol Concentration
(88-05-2) Mass
Section 4.Organic Toxic Pollutants(GC/MS Fraction—Base/Neutral Compounds)
4.1 Acenaphthene 0 Concentration
(83-32-9) Mass
4.2 Acenaphthylene � Concentration
El
(208-96-8) Mass
Anthracene Concentration
4.3 El El 0
(120-12-7) Mass
Benzidine 0 Concentration
4.4 (92 87 5) Mass
4.5 Benzo(a)anthracene 0 0 Concentration
(56-55-3) Mass
4.6 Benzo(a)pyrene Concentration
El El 0
(50-32-8) Mass
EPA Form 3510-2C(Revised 3-19) Page 15

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Long-Term
and CAS Number,if available) Required Believed Believed Maximum Maximum Long-
( q (specify) Average Number Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge Average
(required) (if available) Discharge Analyses Value Analyses
(if available)
3,4-benzofluoranthene ❑ Concentration
4.7 (205-99-2) Mass
4.8 Benzo(ghi)perylene L✓ Concentration
(191-24-2) Mass
Benzo(k)fluoranthene Concentration
4.9 (207-08-9) Mass
Bis(2-chloroethoxy)methane ❑ Concentration
4.10 (111-91-1) Mass
4.11 Bis(2-chloroethyl)ether 0 0Concentration
(111-44-4) Mass
4.12 Bis(2-chloroisopropyl)ether 0Concentration
(102-80-1) Mass
Bis(2-ethylhexyl) phthalate El ❑ ❑ Concentration
4.13 (117-81-7) Mass
4.14 4-bromophenyl phenyl ether ❑✓ ❑ 0Concentration
(101-55-3) Mass
4.15 Butyl benzyl phthalate 00Concentration
(85-68-7) Mass
4.16 2-chloronaphthalene 0 Concentration
(91-58-7) Mass
4.17 4-chlorophenyl phenyl ether 0Concentration
(7005-72-3) Mass
Chrysene 0 Concentration
4.18 0 El
(218-01-9) Mass
4.19 Dibenzo(a,h) anthracene Concentration
0 El ID
(53-70-3) Mass
EPA Form 3510-2C(Revised 3-19) Page 16

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number.if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
Daily of of
Discharge Discharge Average
(required) (if available) Discharge Analyses Value Analyses
(if available)
4.20 1 2-dichlorobenzene Concentration
El El 0
(95-50-1) Mass
4.21 1,3-dichlorobenzene 0Concentration
0 El
(541-73-1) Mass
4.22 1 4 dichlorobenzene 00Concentration
(106-46-7) Mass
4.23 3,3-dichlorobenzidine Concentration
(91-94-1) Mass
4.24 Diethyl phthalate El0Concentration
(84-66-2) Mass
4.25 Dimethyl phthalate 0Concentration
(131-11-3) Mass
4.26 Di n butyl phthalate © © Concentration
(84-74-2) Mass
4.27 2,4-dinitrotoluene � 0Concentration
(121-14-2) Mass
4.28 2,6-dinitrotoluene ❑ 0Concentration
(606-20-2) Mass
4.29 Di-n-octyl phthalate ❑✓ Concentration
El El
(117-84-0) Mass
1,2-Diphenylhydrazine Concentration
4.30 0 El
(as azobenzene)(122-66-7) Mass
4.31 Fluoranthene 0Concentration
El El
(206-44-0) Mass
4.32 Fluorene 0Concentration
(86-73-7) Mass
EPA Form 3510-2C(Revised 3-19) Page 17

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Maximum Maximum Long-Term Long-
(and CAS Number,if available) Required Believed Believed (specify) Daily Monthly Average Number Term Number
Present Absent of
Discharge Discharge Daily of Average
(required) (if available) Discharge Analyses Value Analyses
(if available)
Hexachlorobenzene Concentration
4.33 0 El
(118-74-1) ✓ Mass
Hexachlorobutadiene Concentration
4.34 (87-68-3) ✓ Mass
Hexachlorocyclopentadiene ❑ Concentration
4.35 ✓(77-47-4) Mass
Hexachloroethane ❑ Concentration
✓
4.36 (67-72-1) Mass
Indeno(1,2,3-cd) pyrene Concentration
4.37 ✓l El 0
(193-39-5) Mass
Isophorone Concentration
4.38 l El El
(78-59-1) ✓ Mass
Naphthalene Concentration
4.39 (91 20 3) ✓ Mass
4.40 Nitrobenzene Concentration
0 El
(98-95-3) Mass
4.41 N-nitrosodimethylamine ElConcentration
(62-75-9) Mass
N nitrosodi n propylamine Concentration
4.42 a 0 0
(621-64-7) Mass
N-nitrosodiphenylamine Concentration
4.43 ✓
86-30-6
( ) Mass
4.44 Phenanthrene a Concentration
El 0
(85-01-8) Mass
Pyrene Concentration
4.45 E✓ 0 0
(129 00 0)
Mass
EPA Form 3510-2C(Revised 3-19) Page 18

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))l
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
Discharge Discharge Daily °f Average °f
(required) (if available) Discharge Analyses Value Analyses
(if available) I
4.46 12,4-trichlorobenzene ElConcentration
(120-82-1) Mass
Section 5.Organic Toxic Pollutants(GCIMS Fraction-Pesticides)
Aldrin Concentration
5.1 (309-00-2) Mass
a-BHC Concentration
5.2 (319-84-6) Mass
R-BHC Concentration
5.3 (319-85-7) Mass
y-BHC Concentration
5.4 (58 89 9) Mass
b-BHC Concentration
5.5 (319-86-8) Mass
5.6 Chlordane Concentration
(57-74-9) Mass
4,4'-DDT Concentration
5.7 (50-29-3) Mass
4 4'-DDE Concentration
5.8 (72-55-9) Mass
4,4'-DDD Concentration
5.9 (72-54-8) Mass
5.10 Dieldrin Concentration
(60-57-1) Mass
5.11 a-endosulfan Concentration
(115-29-7) Mass
EPA Form 3510-2C(Revised -1 o 3 9) Page 19

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Long-Term
Maximum Maximum Long-
(and CAS Number,if available) Required Believed Believed (specify) Daily Monthly Average Number Term Number
Present Absent Daily of of
Discharge Discharge Average
(required) (if available) Discharge Analyses Value Analyses
(if available)
5.12 R-endosulfan Concentration
(115-29-7) Mass
Endosulfan sulfate Concentration
5.13 (1031-07-8) Mass
5.14 Endrin Concentration
(72-20-8) Mass
Endrin aldehyde Concentration
5.15 (7421 93 4) � � 0
Mass
5.16 Heptachlor Concentration
(76-44-8) Mass
Heptachlor epoxide Concentration
5.17 (1024-57-3) CI 0 0 Mass
PCB-1242 Concentration
5.18 (53469-21-9) 0 0 0 Mass
PCB-1254 Concentration
5.19 (11097-69-1) CI 0 C Mass
PCB-1221 Concentration
5.20 (11104-28-2) 0 0 CIMass
PCB-1232 Concentration
5.21 (11141-16-5) CI 0 0
Mass
PCB-1248 Concentration
5.22 (12672-29-6) CI CI 0
Mass
PCB-1260 Concentration
5.23 (11096-82-5) El El D
Mass
PCB-1016 Concentration
5.24 (12674-11-2) 0 0 C Mass
EPA Form 3510-2C(Revised 3-19) Page 20

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0089958 Central Square Excavation 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Long-Term
Maximum Maximum Long-
(and CAS Number,if available) Required Believed Believed (specify) Average Number Number
Present Absent Daily Monthly Term
Daily of of
Discharge Discharge Average
(required) (if available) Discharge Analyses Value Analyses
(if available)
Toxaphene Concentration
5.25 (8001-35-2) ❑ ❑ ✓I Mass
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I, subchapter N or 0. See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 21

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence Intake
(check one) Effluent (Optional)
Pollutant Units Maximum Long-Term
Believed Believed (specify) Maximum Daily Long-Term
Present Absent Discharge Monthly Average Daily Number of Average Number of
Discharge Discharge Analyses Analyses
(required) Value
(if available) (if available)
❑ Check here if you believe all pollutants on Table C to be present in your discharge from the noted outfall.You need not complete the"Presence or Absence"column of Table C for
each pollutant.
❑✓ Check here if you believe all pollutants on Table C to be absent in your discharge from the noted outfall.You need not complete the"Presence or Absence"column of Table C for
each pollutant.
1 Bromide 0 0 Concentration
(24959-67-9) Mass
Chlorine, total Concentration
2. residual ❑ 0 Mass
3. Color 0 0 Concentration
Mass
Concentration
4. Fecal coliform ❑ 0 Mass
5 Fluoride Concentration
(16984-48-8) El 0 Mass
6 Nitrate-nitrite 0 0 Concentration1111 IT
Mass
Nitrogen,total Concentration
7.
organic(as N) ❑ 0 Mass
8. Oil and grease ❑ Concentration
El
Mass
Phosphorus(as Concentration
9. P),total(7723-14-0) El 0 Mass
10. Sulfate(as SO4) ❑ Concentration
(14808-79-8) Mass
Concentration
11. Sulfide(as S) ❑ 0 Mass
EPA Form 3510-2C(Revised 3-19) Page 23

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence Intake
(check one) Effluent (Optional)
Units
Pollutant Maximum Long-Term
Believed Believed (specify) Maximum Daily Long-Term
Present Absent Discharge Monthly Average Daily Number of Average Number of
Discharge Discharge Analyses Analyses
(required) Value
(if available) (if available)
El
Sulfite(as SO3) El Concentration
la (14265-45-3) Mass
13. Surfactants El El
Concentration
Mass
14. Aluminum,total Concentration
(7429-90-5) 4 Mass
—.
15. Barium,total ❑ Concentration 34.04ug/L
(7440-39-3) Mass 0.020#
Boron, total Concentration
16. (7440-42-8) ❑ 1✓
Mass
1 Cobalt,total Concentration
(7440-48-4)
Mass
18 Iron, total ❑ ❑ Concentration
(7439-89-6)
Mass
19 Magnesium,total 0 ✓l Concentration
(7439-95-4) Mass
Molybdenum, Concentration
20. total ❑ 0 Mass
(7439-98-7)
21 Manganese, total ❑ 0 Concentration
(7439-96-5) Mass
22 Tin'total ❑ 0 Concentration
(7440-31-5) Mass
23 Titanium,total ❑ 0 Concentration
(7440-32-6) Mass
EPA Form 3510-2C(Revised 3-19) Page 24
I

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence
(check one) Effluent Intake
(Optional)
Pollutant Units Maximum Long-Term
Believed Believed (specify) Maximum Daily Long-Term
Present Absent Discharge Monthly Average Daily Number of Average Number of
Discharge Discharge Analyses Analyses
(required) Value
(if available) (if available)
24. Radioactivity
Alpha,total Concentration
Mass
Beta,total 0 Concentration
Mass
Radium,total Concentration
Mass
Radium 226,total 0✓ Concentration
Mass
' Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 25

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221 7 vii 1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
1. Asbestos ❑ ✓❑
2. Acetaldehyde ❑ 0
3. Allyl alcohol ❑ 0
4. Allyl chloride 0 ❑✓
5. Amyl acetate 0 ✓❑
6. Aniline 0 ❑✓
7. Benzonitrile 0 ❑✓
8. Benzyl chloride ❑ ❑✓
9. Butyl acetate 0 ✓❑
10. Butylamine 0 0
11. Captan 0 ❑✓
12. Carbaryl 0 ❑✓
13. Carbofuran 0 0
14. Carbon disulfide 0 ✓❑
15. Chlorpyrifos 0 0
16. Coumaphos ❑ 0
17. Cresol 0 ❑✓
18. Crotonaldehyde 0 ❑✓
19. Cyclohexane 0 ❑✓
EPA Form 3510-2C(Revised 3-19) Page 27

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
0MB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
20. 2,4-D (2,4-dichlorophenoxyacetic acid) ❑ ❑✓
21. Diazinon 0 ❑✓
22. Dicamba 0 ❑✓
23. Dichlobenil 0 ❑✓
24. Dichlone 0 ❑✓
25. 2,2-dichloropropionic acid 0 ❑✓
26. Dichlorvos 0 ❑✓
27. Diethyl amine 0 ✓❑
28. Dimethyl amine 0 ❑✓
29. Dintrobenzene 0 ❑✓
30. Diquat 0 ❑✓
31. Disulfoton 0 ❑✓
32. Diuron ❑ ❑✓
33. Epichlorohydrin 0 ❑✓
34. Ethion 0 ❑✓
35. Ethylene diamine 0 ❑✓
36. Ethylene dibromide ❑ p
37. Formaldehyde 0 ❑✓
38. Furfural 0 ❑✓
EPA Form 3510-2C(Revised 3-19) Page 28

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent _
39. Guthion ❑ p
40. Isoprene ❑ ✓❑
41. Isopropanolamine ❑ ✓❑
42. Kelthane ❑ p
43. Kepone ❑ ❑✓
44. Malathion ❑ ✓❑
45. Mercaptodimethur ❑ ✓❑
46. Methoxychlor ❑ ❑✓
47. Methyl mercaptan ❑ 0
48. Methyl methacrylate ❑ ❑✓
49. Methyl parathion ❑ ✓❑
50. Mevinphos 0 ✓❑
51. Mexacarbate ❑ ❑✓
52. Monoethyl amine ❑ ❑✓
53. Monomethyl amine ❑ ✓❑
54. Naled ❑ ✓❑
55. Naphthenic acid ❑ ✓❑
56. Nitrotoluene ❑ ❑✓
57. Parathion 0 0
EPA Form 3510-2C(Revised 3-19) Page 29

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
58. Phenolsulfonate 0 ❑✓
59. Phosgene 0 ❑✓
60. Propargite 0 ✓❑
61. Propylene oxide 0 ✓❑
62. Pyrethrins ❑ ✓❑
63. Quinoline ❑ ❑✓
64. Resorcinol ❑ ❑✓
65. Strontium ❑ ❑✓
66. Strychnine ❑ ❑✓
67. Styrene ❑ ❑✓
68. 2,4,5-T(2,4,5-trichlorophenoxyacetic ❑ ❑✓
acid)
69. TDE(tetrachlorodiphenyl ethane) ❑ ❑✓
70. 2,4,5-TP[2-(2,4,5-trichlorophenoxy) ❑ ✓❑
propanoic acid]
71. Trichlorofon 0 ❑✓
72. Triethanolamine 0 ❑✓
73. Triethylamine 0 ❑✓
74. Trimethylamine 0 ❑✓
75. Uranium ❑ ❑✓
76. Vanadium 0 ❑✓
EPA Form 3510-2C(Revised 3-19) Page 30

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation 001
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
77. Vinyl acetate ❑ ❑✓
78. Xylene ✓❑ ❑ Xylenes were detected during 2 of 6 monitoring events in 2022 Max 89.2 ug/L Ave 13.74 ug/L
79. Xylenol ❑ ✓❑
80. Zirconium ❑ ❑✓
Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 31

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
OMB No.2040-0004
NC0089958 Central Square Excavation
TABLE E.2,3,7,8 TETRACHLORODIBENZO P DIOXIN(2,3,7,8 TCDD)(40 CFR 122.21(g)(7)(viii))
TCDD Presence or
Congeners Absence
Pollutant Used or (check one) Results of Screening Procedure
Manufactured Believed Believed
Present Absent
2.3.7.8-TCDD ❑✓
Page 33 EPA Form 3510-2C(Revised 3-19)

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 Central Square Excavation
OMB No.2040-0004
U.S. Environmental Protection Agency
FORM �,► Application for NPDES Permit to Discharge Wastewater
NPDES \" EPA MANUFACTURING, COMMERCIAL, MINING,AND SILVICULTURAL FACILITIES WHICH
DISCHARGE ONLY NONPROCESS WASTEWATER
SECTION 1.OUTFALL LOCATION(40 CFR 122.21(h)(1))
1.1 Provide information on each of the facilit 's outfalls in the table below.
o Outfall Receiving Water Name Latitude Longitude
Number
0
0 001 zTrib.to Little Sugar Creek 35° 13' 25" 80° 19' 7 7"
0
SECTION 2.DISCHARGE DATE(40 CFR 122.21(h)(2))
2.1 Are you a new or existing discharger?(Check only one response.)
w ❑ New discharger ❑✓ Existing discharger 4 SKIP to Section 3.
N ' 2.2 Specify your anticipated discharge date:
07/15/2022
SECTION 3.WASTE TYPES(40 CFR 122.21(h)(3))
3.1 What types of wastes are currently being discharged if you are an existing discharger or will be discharged if you are a
new discharger?(Check all that apply.)
❑ Sanitary wastes ❑✓ Other nonprocess wastewater(describe/explain
ElRestaurant or cafeteria waste directly below)
Water produced from dewatering contianing
❑ Non-contact cooling water 1— 3.2 Does the facility use cooling water additives?
❑ Yes ❑✓ No 4 SKIP to Section 4.
3.3 List the cooling water additives used and describe their corn 3osition.
Cooling Water Additives Composition of Additives
(list) (if available to you)
SECTION 4.EFFLUENT CHARACTERISTICS(40 CFR 122.21(h)(4))
4.1 Have you completed monitoring for all parameters in the table below at each of your outfalls and attached the results to
this application package?
❑ Yes No;a waiver has been requested from my NPDES permitting authority
(attach waiver request and additional information) 4 SKIP to Section 5.
4.2 Provide data as requested in the table below.' (See instructions for specifics.)
Number of Maximum Daily Average Daily Source
Parameter or Pollutant Analyses Discharge Discharge (use codes
(if actual data (specify units) (specify units) per
reported) Mass Conc. Mass Conc. instructions)
Biochemical oxygen demand(BODE)
Total suspended solids(TSS)
Oil and grease
w Ammonia(as N)
Discharge flow
pH(report as range)
Temperature(winter)
Temperature(summer)
'Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant
parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2E(revised 3-19) Page 1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 Central Square Excavation OMB No.2040-0004
4.3 Is fecal coliform believed present,or is sanitary waste discharged(or will it be discharged)?
❑ Yes ✓❑ No 4 SKIP to Item 4.5.
4.4 Provide data as requested in the table below.1 (See instructions for specifics.)
Number of Maximum Daily Average Daily Source
Parameter or Pollutant Analyses Discharge Discharge (use codes
(if actual data (specify units) (specify units) per
reported) Mass Conc. Mass Conc. Instructions.)
Fecal coliform
d coilE. co
= Enterococci
v4.5 Is chlorine used(or will it be used)?
co ElYes ❑✓ No 4 SKIP to Item 4.7.
cn 4.6 Provide data as requested in the table below., (See instructions for specifics.)
Number of Maximum Daily Average Daily Source
co
Parameter or Pollutant Analyses Discharge Discharge (use codes
iic (if actual data (specif"units) (specify units) per
creported) Mass Conc. Mass l Conc. instructions)
O Total Residual Chlorine lI
w 4.7 Is non-contact cooling water discharged(or will it be discharged)?
0 Yes ❑✓ No 4 SKIP to Section 5.
4.8 Provide data as requested in the table below. (See instructions for specifics.)
Number of Maximum Daily Average Daily Source
y
Parameter or Pollutant
Analyses Discharge Discharge (use codes
(if actual data (specify units) (specify units) per
reported) Mass Conc. Mass Conc. instructions)
Chemical oxygen demand(COD)
Total organic carbon(TOC)
SECTION 5.FLOW(40 CFR 122.21(h)(5))
5.1 Except for stormwater water runoff, leaks,or spills, are any of the discharges you described in Sections 1 and 3 of this
application intermittent or seasonal?
❑ Yes 4 Complete this section. ❑✓ No 4 SKIP to Section 6.
0 5.2 Briefly describe the frequency and duration of flow.
1 The flow is expecte to be continuous and less than 72,000 GPD or 0.072 MGD.
SECTION 6.TREATMENT SYSTEM(40 CFR 122.21(h)(6))
6.1 Briefly describe any treatment system(s)used(or to be used).
E The system will include an 18,000-gallon frac tank for settling and grit removal followed by a 1,000-gallon surge/mixing
th
tank,followed by two particulate filters in series followed by two 1000-pound carbon vessels in series.A line drawing
cn
and AP and ID drawing are included with the permit application package.
CD
E
ra
m A carbon dioxide gas dosing system will be used upstream of the mixing/surge tank during construction dewatering.
L
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant
parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2E(revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0089958 Central Square Excavation OMB No.2040-0004
SECTION 7.OTHER INFORMATION(40 CFR 122.21(h)(7))
7.1 Use the space below to expand upon any of the above items. Use this space to provide any information you believe the
reviewer should consider in establishing permit limitations.Attach additional sheets as needed.
Dewatering began in March 2022. Effluent samples are collected bi-monthly and reported to NCDEQ in electronic
discharge monitoring reports. Copies of analytical results'for June 2020 to are attached to the permit application
package.
a;
SECTION 8.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d))
8.1 In Column 1 below, mark the sections of Form 2E that you have completed and are submitting with your application.
For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority. Note that
not all applicants are required to provide attachments.
Column 1 Column 2
❑✓ Section 1: Outfall Location ❑✓ w/attachments(e.g., responses for additional outfalls)
❑✓ Section 2: Discharge Date ❑ w/attachments
❑✓ Section 3:Waste Types ❑ w/attachments
_ ❑✓ Section 4: Effluent Characteristics ❑ w/attachments
❑✓ Section 5: Flow ❑ w/attachments
o 0Section 6:Treatment System ❑✓ w/attachments
❑✓ Section 7: Other Information ❑✓ w/attachments
❑✓ Section 8: Checklist and Certification Statement ❑ w/attachments
-a
8.2 Certification Statement
/certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who manage the system,or those persons directly
responsible for gathering the information, the information submitted is,to the best of my knowledge and belief true,
accurate,and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fine and imprisonment for knowing violations.
Name(print or type first and last name) Official title
1 Skis,„Nv5
Signature Date signed
er-1/4—? dE)1
EPA Form 3510-2E(revised 3-19) Page 3

F
TOPOGRAPHIC MAP
CENTRAL SQUARE NPDES PERMIT APPLICATION
U�(� U.S.DEPARTMENT OF THE INTERIOR CHARLOTTE EAST QUADRANGLE
dIgJ US.GEOLOGICAL SURVEY MA, w NORTH CAROLINA-AECIIIRNRURO COUNTY
NL<'US Topo ).5-MINUTE SERIES
N ly e u'
.4900
ROHIM l] 15.259942'NE 12 15 1T a )a
ryi5a i i �0. rr �r �- rd -,l +
....
' rd b B ,.,,,, `%0, ,
' -�.,` • N ! _,fit a
•
p/ R�✓�ri� +�3 /d \
rf !ter , r `
,,9e
•
lf 1 •
' a
s 3 '9
w ;lr e
NkoC `, /,, /'.<,!'` • (HARI Oi 1 E 1 56
u✓3' g ry. _....� ..,\ _.. 95
`.'_ r
94
•
•
•
r.
Ct'd` 9• .. �\
/V 1.
Wig } . .90
,,u w xa n `zz...a .onaa �Ts9
Produced by Om UNS a,GRRON(AI S('0 SCALE 1:24000 ROAD CLAm NGODN
49 NM
aNDN
d.,, .,..,,.�I.'Lla._N...,4F.--.n,.....T.,. �00 i ,. CHARLOTTE EAST,NC M
I

ty y yM
40
1�•,.< '�3- �,' :� "" >, � Tel 1,
S.
r
> /% „cr l 4 ti ti d +'}� 4 - 1 _-t,f
{
j
`. , ) / ILI Ili ' "svi,:,:i jg
s_ :t. DISCHARGE '
-rT" i
f
,J '4 I POINT ; � 1 ,`' I{
i, •
-) d i ,,? g t .'4 ° ki
! `r '+...., ' '" =`"'-.,*'w, ``ul '-�,, M E i k i y y- V T + 4 ,',+.
1
, .re, :''' ",\ _-- SITE . y; ' 6 r',
r� 04, ' 't: x :11'"' I s. _ S7 t M SI e s. ayY�
>r�`: r � r je+s � '•,'.h.� aw,."x I �'"�'�„", .a.• �}���W;_� .•.'.`- ^+ r Q4}, ,
r �£f= 1
,�„ 1` � oar './�-" ,+ "s( _'• I �j
� ,.. rr V '".:1
'r ( s` "} -ry r ' w j,-,.,4,..... _.,,_ , \ .. , 4 , ......,17,,,,,,.1 ithyr NNtip „. 1).44%.„. ....\.....t,..04.41 ., = - s-
4t bib
'4!
1:24...
1-1. ' ,31:7'.,_:
, I r ('` .., 'ry �"�` M',- ,� ..,_ '`*"6'x.. -. val„ t �. 1 +4 •' .` ', CC •
ft
C.ii�NRLC -1'. :... "'
:::,,,
—... „''', "1
, „..
J� '
05, ,
.,
i ,.„„ ..., , _., \r ,
/
LL SCALE 1:24
000
€ U.t� C M.1_O.MIETo?S I
,-- _ I i.
sue.
1 C_S 01 N
MILES _141Mii-5
1CV C luau :LOC k'xYl 4Jxh# SO1}C WOO 7GYJ01 SJJC 1(1C11C
I.LIT
UTM GRaO Alta t'IT NTFAR 1S NORTH
OfCU +.TION AT[ENTER Of SHEET
C{3HTO RR RITERYAL TO FELT
NORTH AMERICAN VERTICAL LMTUM OF TITES
SOURCE:
FIGURE 1
USGS TOPOGRAPHIC MAP SITE TOPOGRAPHIC LOCATION MAP
CAHRLOTTE EAST (--.' CENTRAL SQUARE
7.5 MINUTE QUADRANGLE I Central Avenue at Pecan Avenue
DATED 2019 Charlotte, Mecklenburg, North Carolina
�" y,5 ECS PROJECT NO.49-10756-C

-
it-
lir
DISCHARGE TO '-- ', ".`
.\.....,,,,,
UNNAED
TO LI TRIBUTARY
TTLE SUGAR °r,;
CREEK
::r.'*""- -"'N'N'''''-"*---""*".:, ,.:C'l
(OUTFALL ID
U LS020-S W O2S8000)
'\ , '
II
,.70NtSW4i FE 5YSTEN
DROP!NEED
L .4
4----,-( ) ,.
,,,_ .. 0......„.N4
"' T ' r gym, +rnr+me
/ _.,04P.°1*-
LEGEND
N
APPROXIMATE SITE BOUNDARY STORMWATER PIPE /jjjf...1`I...
M -r E
0 STORMWATER STRUCTURE FLOW DIRECTION c
SOURCE: si, . FIGURE 2
VIRTUAL CHARLOTTE WEB MAPPING APPLICATION DISCHARGE LOCATION MAP
ACCESSED APRIL 5, 2021 CENTRAL SQUARE
Central Avenue at Pecan Avenue
APPROXIMATE SCALE: Charlotte, Mecklenburg, North Carolina
1 INCH=382 FEET
0
382 FEET ECS PROJECT NO.49-10756-C
I J : ,,.
iR,
1

LINE DRAWING
CENTRAL SQUARE
NPDES PERMIT APPLICATION FOR GROUNDWATER PRODUCED BY DEWATERING
ECS PROJECT NO. 10756-C
CO2 GAS FOR PH ADJUSTMENT CARBON VESSELS
(AS NEEDED) NOS.1&2
PARTICULATE FILTERS (1,000 POUNDS GAC EACH)
NOS.1&2 <50,000 GPD
<50,000 GPD TO OUTFACE 001
FROM DEWATERING 18,000-GAL 1,000-GAL
FRAC TANK MIXING/SURGE
TANK
•
RECIRCULATION/MIXING LOOP
<14,440 GPD
ITEMS SHOWN IN RED WILL BE REMOVED WHEN
DEWATERING OPERATIONS TRANSITION FROM
CONSTRUCTION DEWATERING TO PERMANENT
BUILDING DEWATERING

,'
i SYSTEM NOTPES
4 4 me terl
'� n.a ev o�°ne.'mn 1 Q i a pp ° Use Clear PVC In select.sVC ofa new Opt
a damps
�I.. 7 ► Q ► f�'1,:',,..r�, I :" w>..M B.I. ll Plmnpsto be PVC PM sow Seals
tions.be Kam.wPii AL M.A.PS en
i Vam�%have BM Seale
rav j CO2 Cylinder and e Hem
owme,.r wi . re PVC Mrlenarsla4
]9�Cal
4 mee.e baw.,ed
► ► ■ na w..wr.2e.h.e. ► ►
Mlgn Loral alarm-22
•
Pump 2 em2.',OR 10•-----(1 t
5i
Ti
K;I� IC`I• rICI riO4 •
4 1�1 1Q •
...xax Q
Pomp
0 0 Qrt
► 101 �s-- OI MCI—►-�'}dam
c pips
to_ _......_... el.PVC pipe
low stowat.o
rm;..... r r
i
(�h-4 h i n n
w
I I
I /
\aYaew eae� a
—C a. Cnn.nt . ..� j NO Le_Marmw,atawhh / N
O INC B.MMead FM� , P.mpanDBNd raw�h \ ,
o-^ p-Nan*MPBeS•Olen 0 Flow Swea `Q
N .YB,IIe.t8V.S
8 ow psi pow.ow.
a eve Trwxlss/me,e O DMre nee IPrefeunSwitch HERIC SOLUTIONS.LLC
p, IVCOnaeallva,ve irui O P enepr PO Box548
. a..me vale.(Regulator 0 Fawcsalmlv.N. '�'I Pail Indian Tan,Rc:ao'2q
Ms /�
O O alapB O O geo-7Haep
Purer p
Pnmv d B 2 aer�. .m �-J 50 GPM Mobile Treatment Unit
on
no PVC 6ampMaand«a valve O Mow Mesmearr Tobago,
1-11 Pewm.Mr(See Tral —► Flow awns" Pumpt/Pump2 ReeksPump i Particle Fitters Pressure Switch pH Sensor Carbon Vessel Flow Switch ,FlowmeMr/Totalizer P 8 ID
�-�' PVC
°Size Reducer
-Ill— ^"Polen moeoisr`'' ..'rdel.Pn;z; delFSPx000` delC.,11., , In eFlatpHEle rod. MagroaMrFloswSen'so, Design Maximum Flow Rate-50GPM
f NCMtlSip "valve � Salenq 0.5.. 3Ms.1.Ph,10, M,Mp.,-Ph,,20VB tD5,32"DLBddy Mo Brxe Fired S] t.elp00Signet
Cp trT.3 ,➢CV-LPS-1000 to 0 oar 000Loer,00� PY
•r lmpe Ilex 3A6•Impelar ynieon cover Mures aatocroc wetted Pam nwr EasyD.I Virgin Coconut CarNon MMT020 Men Tee M Updated March 27,2020 by ECD
EaM Seals NEMA SS,1M•M.T PIP. d1 rDap ,2xe0Me.h BBOUD nir li np floe

DISCHARGE MONITORING REPORTS AND EFFLUENT ANALYTICAL REPORTS

DISCHARGE MONITORING REPORTS AND EFFLUENT ANALYTICAL REPORTS
MARCH 2022

NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1.0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-1 COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-1 ORC HAS CHANGED:No
eDMR PERIOD:03-2022(March 2022) VERSION: 1.0 STATUS:Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
50050 00400 01002 01007 76028 3140 01027 32106 C0034
I E _
F E i=
a - I Continuous Monthly 2 X month 2 X month Monthly 2 X month 2 X month Monthly .2 X month
E < F
p` Recorder Grab Grab Grab Grab Grab Grab ,Grab ,Grab
ew i U aC U h O O O 7 FLOW pH As-TOTAL BARIUM SEMI-VOL BENZENE CADMIUM CHLRFORM TOT CR CONC
2400 clock Hrs 2400 clock Hrs YB/N mgd su ug/1 ug/I ug/I ug/1 ug/1 ug/I ug/I
I 0
2 0
3 0
4 0
0
6 0
7 800 7.0 Y 0.04
a 800 2.5 Y 0.04
9 1300 .50 Y 0.041
10 1215 0 1100 1.5 Y 0.039 6.17 <I 5 50.5 0 94 I I 21/
it 0.039
12 0.039
13 0.039
14 1010 0 1010 I 0 Y 0.036
15 0.036
16 0.036
17 0.036
1e 715 7.00 1 0.034
19 0.034
20 0.034
21 0.034
22 0.034
23 0.034
24 1310 0 1300 1.00 Y 0.033 - I - I I 1 2 I
25 0.033
26 0.033
27 0.033
28 915 1.00 Y 0.032
29 0.032
30 0930 I Y 0.031
31 0.031
Monthly Average Limit:
Monthly Average: 0.028484 0 0 0 0.47 0 0 ,2.175
Daily Maximum: 0.041 6.17 0 0 0 0.94 0 0 2.18
Daily Minimum: 0 6.17 0 0 0 0 0 0 2.17
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday
Discharge Monitoring Report-Copy Of Record(COR_NC0089958_Ver 1.0_3_2022.pdf)

NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1.0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-I COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-I ORC HAS CHANGED:No
eDMR PERIOD:03-2022(March 2022) VERSION: 1.0 STATUS:Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
ii 01042 34371 00900 01051 COMER 01067 76029 TGE6C C0456 01147 34010
E E _ li
P. E .I v, o
i. 1- _ C w
E - E r 2 X month 2 X month Monthly 2 X month 2 X month 2 X month Monthly Monthly 2 X month 2 X month 2 X month
n e n
` < F f
;° — `a Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab
ii E c d reC
G U O I-. O O i COPPER ETHYLBEN TOT HARD LEAD MERCURY- NICKEL VOLATILE FTHD24PF PAH-CO .Se-TOTAL TOLUENE
2400 clock Hrs 2400 clock Hrs Y/BN ug/I ug/I mg/1 mg/I ug/I ug/I ug/I pass/fail ug/I ug/I ug/I
1
2
3
4 •
5
6
7 800 7.0 Y
8 800 2.5 Y
9 1300 .50 Y
10 1215 0 1 100 1.5 Y <2 <I 24 <I <0.0002 <5 3.07 <20.2 <5 <I
11
12
13
14 1010 0 1010 1.0 Y 100
15
16
17
18 715 7.00 Y
19
20
21
22
23
24 1310 0 1300 1.00 Y <2 <I <I <0.0002 <5 <20 <5 <1
25
26
27
28 915 1.00 Y
29
30 0930 1 Y
31
Monthly Average Limit:
Monthly Average: 0 0 24 0 0 0 3.07 100 0 0 0
Daily Maximum: 0 0 24 0 0 0 3.07 100 0 0 0
Daily Minimum: 0 0 24 0 0 0 3.07 100 0 0 0
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday
Discharge Monitoring Report-Copy Of Record(COR_NC0089958_Ver_1.0_3_2022.pdf)

NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1.0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-I COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-1 ORC HAS CHANGED:No
eDMR PERIOD:03-2022(March 2022) VERSION: 1.0 STATUS:Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
81551 01092 34316 01034
E E
F0 To
2 X month 2 X month
E < a
O = Grab Grab Grab Grab
e a d d u z"
U [- O O O Z XYLENE ZINC CLRFIOM,D Cr-TOTAL
2400 clock Hrs 2400 clock Hrs YAWN ug/1 ug/1 ug/I ug/1
1
2
3
4
5
6
7 800 7.0 Y
8 800 2.5 Y
9 1300 .50 Y
10 1215 0 1100 1.5 Y <I <10 <I '_.IS
11
12
13
14 1010 0 1010 1.0 Y
15
16
17
18 715 7.00 Y
19
20
21
22
23
24 1310 0 1300 1.00 Y <I .III <I i_17
25
26
27
28 915 1.00 Y
29
30 0930 I Y
31
3lanthly Average Limit:
Monthly Average: 0 0 0 2.175
Daily Maximum: 0 0 0 2.18
Daily Minimum: 0 0 0 2.17
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday
Discharge Monitoring Report-Copy Of Record(COR_NC0089958_Ver 1.0 3_2022.pdt)

NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1.0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-1 COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-I ORC HAS CHANGED:No
eDMR PERIOD:03-2022(March 2022) VERSION: 1.0 STATUS:Submitted
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:04/18/2022
Electronically Certified by Eric Christian Donnelly on 2022-04-18 08:01:08.023
ORC/Certifier Signature:Eric Christian Donnelly Phone # : [phone] Date
I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.The written submission shall be made as required by part II.E.6 of the
NPDES permit.
Electronically Signed by Eric Christian Donnelly on 2022-04-18 08:01:56.99
Permittee/Submitter Signature: ***Eric Christian Donnelly Phone #:[phone] Date
Permittee Address:201 S College St Ste 1300 Charlotte NC 28244 Permit Expiration Date: 11/30/2026
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:Waypoint Analytical
CERTIFIED LAB#:402
PERSON(s)COLLECTING SAMPLES:David Morris
PARAMETER CODES
Parameter Code assistance may be obtained by visiting https://deq.nc.gov/about/divisions/water-resources/edmr/user-documentation.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:YES indicates that No Flow/Discharge occurred and,as a result,no data is reported for any parameter on the DMR for the
entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).
Discharge Monitoring Report-Copy Of Record(COR_NC0089958_Ver_1.0_3_2022.pol)

NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1.0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-1 COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-1 ORC HAS CHANGED:No
eDMR PERIOD:03-2022(March 2022) VERSION: 1.0 STATUS:Submitted
Report Comments:
Please note that dewatering began on March 7,2022. Therefore,no flow readings were collected prior to 3/7/22.

•
Waypoint, 449 Springbrook Rd,Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www,waypointanalytical.com
3/30/2022
Heric Solutions, LLC
Eric Donnelly
P.O. Box 548
Indian Trail, NC, 28079
Ref: Analytical Testing
Lab Report Number: 22-069-0033
Client Project Description: Monthly
1111 Pecan Ave.
Project Number: Permit NC0089958
Dear Eric Donnelly:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/10/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
a ?"
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

4
V/aypoi lit Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
North Carolina State Program 37735 07/31/2022
North Carolina State Program 402 12/31/2022
South Carolina State Program 99012 07/31/2022
South Carolina State Program 99012 12/31/2022
Page 1 of 1 00016/22-069-0033

w
VVaVpoi fl , 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-069-0033
Client Project Description: Monthly
1111 Pecan Ave.
Lab No Client Sample ID Matrix Date Collected Date Received
95867 Effluent Aqueous 03/10/2022 12:15 03/10/2022 13:10
95868 Effluent-8270 PAH Aqueous 03/10/2022 12:15 03/10/2022 13:10
95869 Influent Aqueous 03/10/2022 12:05 03/10/2022 13:10
95870 Influent -8270 PAH Aqueous 03/10/2022 12:05 03/10/2022 13:10

wO
Waypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 03/10/2022
Indian Trail , NC 28079
Report Number :22-069-0033 REPORT OF ANALYSIS
Lab No : 95867 Matrix: Aqueous
Sample ID :Effluent Sampled: 3/10/2022 12:15
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Hardness 24.0 mg/L 10.0 1 03/18/22 12:50 CLB 2340C-2011
pH 6.17 s.u. 1 03/10/22 12:15 FLD FIELD
Temperature 12.5 C 0.1 1 03/10/22 12:15 FLD FIELD
Arsenic <1.00 u9/L 1.00 1 03/16/22 00:42 EDV 200.8
Barium <5.00 pg/L 5.00 1 03/16/22 00:42 EDV 200.8
Cadmium <1.00 pg/L 1.00 1 03/16/22 00:42 EDV 200.8
Chromium 2.18 u9/L 1.00 1 03/16/22 00:42 EDV 200.8
Copper <2.00 pg/L 2.00 1 03/16/22 00:42 EDV 200.8
Lead <1.00 pg/L 1.00 1 03/16/22 00:42 EDV 200.8
Mercury(Total) <0.000200 mg/L 0.000200 1 03/16/22 16:57 EDV 245.1
Nickel <5.00 pg/L 5.00 1 03/16/22 00:42 EDV 200.8
Selenium <5.00 pg/L 5.00 1 03/16/22 00:42 EDV 200.8
Zinc <10.0 u9/L 10.0 1 03/16/22 00:42 EDV 200.8
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

W point
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 03/10/2022
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95867 Matrix: Aqueous
Sample ID : Effluent Sampled: 3/10/2022 12:15
Analytical Method: 624.1 Prep Batch(es): V16235 03/16/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acetone <5.00 u9/L 5.00 1 03/16/22 22:04 JLB V16236
Acrolein <5.00 pg/L 5.00 1 03/16/22 22:04 JLB V16236
Acrylonitrile <5.00 pg/L 5.00 1 03/16/22 22:04 JLB V16236
Benzene 0.940 pg/L 0.500 1 03/16/22 22:04 JLB V16236
Bromodichloromethane <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
Bromoform <3.00 u9/L 3.00 1 03/16/22 22:04 JLB V16236
Bromomethane <2.00 pg/L 2.00 1 03/16/22 22:04 JLB V16236
Carbon Tetrachloride <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
Chlorobenzene <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
Chlorodibromomethane <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
Chloroethane <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
2-Chloroethylvinyl Ether <10.0 pg/L 10.0 1 03/16/22 22:04 JLB V16236
Chloroform <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
Chloromethane <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
1,2-Dichlorobenzene <1.00 u9/L 1.00 1 03/16/22 22:04 JLB V16236
1,3-Dichlorobenzene <1.00 ig/L 1.00 1 03/16/22 22:04 JLB V16236
1,4-Dichlorobenzene <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
1,1-Dichloroethane <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
1,2-Dichloroethane 3.07 ii9/L 1.00 1 03/16/22 22:04 JLB V16236
1,1-Dichloroethene <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
trans-1,2-Dichloroethene <2.00 pg/L 2.00 1 03/16/22 22:04 JLB V16236
1,2-Dichloropropane <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Waypoint, 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :03/10/2022
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95867 Matrix: Aqueous
Sample ID :Effluent Sampled: 3/10/2022 12:15
Analytical Method: 624.1 Prep Batch(es): V16235 03/16/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MOL DF Date/Time By Analytical
Analyzed Batch
cis-1,3-Dichloropropene <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
trans-1,3-Dichloropropene <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
Ethylbenzene <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
Methylene Chloride <2.00 pg/L 2.00 1 03/16/22 22:04 JLB V16236
1,1,2,2-Tetrachloroethane <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
Tetrachloroethene <0.750 pg/L 0.750 1 03/16/22 22:04 JLB V16236
Toluene <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
1,1,1-Trichloroethane <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
1,1,2-Trichloroethane <0.500 pg/L 0.500 1 03/16/22 22:04 JLB V16236
Trichloroethene <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236 1
Trichlorofluoromethane <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
1,2,3-Trichloropropane <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
1,2,4-Trimethylbenzene <0.500 pg/L 0.500 1 03/16/22 22:04 JLB V16236
Vinyl Chloride <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
o-Xylene <1.00 pg/L 1.00 1 03/16/22 22:04 JLB V16236
m,p-Xylene <2.00 pg/L 2.00 1 03/16/22 22:04 JLB V16236
Xylene(Total) <1.00 pg/L 1.00 1 03/16/22 22:04 KCC V16236
Surrogate:4-Bromofluorobenzene 99.4 Limits: 74-126% 1 03/16/22 22:04 JLB V16236
Surrogate: Dibromofluoromethane 105 Limits: 75-127% 1 03/16/22 22:04 JLB V16236
Surrogate: 1,2-Dichloroethane-d4 97.0 Limits: 67-136% 1 03/16/22 22:04 JLB V16236
Surrogate:Toluene-d8 99.0 Limits: 70-130% 1 03/16/22 22:04 JLB V16236
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Q
Wapoint 449 Springbrook Rd, Charlotte,NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 03/10/2022
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95867 Matrix: Aqueous
Sample ID : Effluent Sampled: 3/10/2022 12:15
Analytical Method: 625.1 Prep Batch(es): V16233 03/17/22 12:00
Prep Method: 625.1 (Prep)
Test Results Units MOL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Acenaphthylene <20.2 pg/L 20.2 1 03/18/22 18:31 JMV V16380
Anthracene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Benzidine <10.1 ug/L 10.1 1 03/18/22 18:31 JMV V16380
Benzo(a)anthracene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Benzo(a)pyrene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Benzo(b)fluoranthene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Benzo(g,h,i)perylene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Benzo(k)fluoranthene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Benzoic Acid <50.5 pg/L 50.5 1 03/18/22 18:31 JMV V16380
Benzyl alcohol <10.1 ug/L 10.1 1 03/18/22 18:31 JMV V16380
Bis(2-Chloroethoxy)methane <10.1 ug/L 10.1 1 03/18/22 18:31 JMV V16380
Bis(2-Chloroethyl)ether <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Bis(2-Chloroisopropyl)ether <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Bis(2-ethylhexyl)phthalate <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
4-Bromophenyl phenyl ether <20.2 pg/L 20.2 1 03/18/22 18:31 JMV V16380
Butyl benzyl phthalate <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
4-Chloro-3-methylphenol <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
2-Chloronaphthalene <20.2 lig/L 20.2 1 03/18/22 18:31 JMV V16380
2-Chlorophenol <10.1 ug/L 10.1 1 03/18/22 18:31 JMV V16380
4-Chlorophenyl phenyl ether <20.2 lJg/L 20.2 1 03/18/22 18:31 JMV V16380
Chrysene <10.1 ug/L 10.1 1 03/18/22 18:31 JMV V16380
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

4
WaypOlflt 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 03/10/2022
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95867 Matrix: Aqueous
Sample ID :Effluent Sampled: 3/10/2022 12:15
Analytical Method: 625.1 Prep Batch(es): V16233 03/17/22 12:00
Prep Method: 625.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Dibenz(a,h)anthracene <20.2 pg/L 20.2 1 03/18/22 18:31 JMV V16380
Dibenzofuran <20.2 pg/L 20.2 1 03/18/22 18:31 JMV V16380
1,2-Dichlorobenzene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
1,3-Dichlorobenzene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
1,4-Dichlorobenzene <10.1 u9/L 10.1 1 03/18/22 18:31 JMV V16380
3,3'-Dichlorobenzidine <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
2,4-Dichlorophenol <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Diethyl phthalate <20.2 pg/L 20.2 1 03/18/22 18:31 JMV V16380
Dimethyl phthalate <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
2,4-Dimethylphenol <20.2 pg/L 20.2 1 03/18/22 18:31 JMV V16380
Di-n-butyl phthalate <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
4,6-Dinitro-2-methylphenol <30.3 pg/L 30.3 1 03/18/22 18:31 JMV V16380
2,4-Dinitrophenol <30.3 pg/L 30.3 1 03/18/22 18:31 JMV V16380
2,4-Dinitrotoluene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
2,6-Dinitrotoluene <20.2 pg/L 20.2 1 03/18/22 18:31 JMV V16380
Di-n-Octyl Phthalate <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Fluoranthene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Fluorene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Hexachlorobenzene <20.2 pg/L 20.2 1 03/18/22 18:31 JMV V16380
Hexachlorobutadiene <20.2 pg/L 20.2 1 03/18/22 18:31 JMV V16380
Hexachlorocyclopentadiene <20.2 pg/L 20.2 1 03/18/22 18:31 JMV V16380
Hexachloroethane <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

0
Waypoint .
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :03/10/2022
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95867 Matrix: Aqueous
Sample ID : Effluent Sampled: 3/10/2022 12:15
Analytical Method: 625.1 Prep Batch(es): V16233 03/17/22 12:00
Prep Method: 625.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Indeno(1,2,3-cd)pyrene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Isophorone <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
1-Methylnaphthalene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
2-Methylnaphthalene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Naphthalene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Nitrobenzene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
2-Nitrophenol <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
4-Nitrophenol <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
N-Nitrosodiphenylamine <20.2 pg/L 20.2 1 03/18/22 18:31 JMV V16380
N-Nitroso-di-n-propylamine <20.2 pg/L 20.2 1 03/18/22 18:31 JMV V16380
Pentachlorophenol <50.5 pg/L 50.5 1 03/18/22 18:31 JMV V16380
Phenanthrene <10.1 ug/L 10.1 1 03/18/22 18:31 JMV V16380
Phenol <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
Pyrene <10.1 ug/L 10.1 1 03/18/22 18:31 JMV V16380
1,2,4-Trichlorobenzene <10.1 pg/L 10.1 1 03/18/22 18:31 JMV V16380
2,4,6-Trichlorophenol <20.2 ug/L 20.2 1 03/18/22 18:31 JMV V16380
Surrogate: Phenol-d5 22.0 Limits: 10-63% 1 03/18/22 18:31 JMV 625.1
Surrogate: 2-Fluorobiphenyl 53.7 Limits:49-118% 1 03/18/22 18:31 JMV V16380
Surrogate: 2-Fluorophenol 31.0 Limits: 22-84% 1 03/18/22 18:31 JMV V16380
Surrogate: Nitrobenzene-d5 49.9 Limits: 43-123% 1 03/18/22 18:31 JMV V16380
Surrogate: 4-Terphenyl-d14 77.8 Limits: 49-151% 1 03/18/22 18:31 JMV V16380
Surrogate: 2,4,6-Tribromophenol 77.2 Limits: 31-144% 1 03/18/22 18:31 JMV V16380
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

O .
\Waypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 03/10/2022
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95868 Matrix: Aqueous
Sample ID : Effluent-8270 PAH Sampled: 3/10/2022 12:15
Analytical Method: 8270E Prep Batch(es): V16234 03/17/22 12:00
Prep Method: 3510C
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <20.2 pg/L 20.2 1 03/18/22 21:07 JMV V16388
Acenaphthylene <20.2 pg/L 20.2 1 03/18/22 21:07 JMV V16388
Anthracene <10.1 IJg/L 10.1 1 03/18/22 21:07 JMV V16388
Benzo(a)anthracene <10.1 pg/L 10.1 1 03/18/22 21:07 JMV V16388
Benzo(a)pyrene <10.1 pg/L 10.1 1 03/18/22 21:07 JMV V16388
Benzo(b)fluoranthene <10.1 ug/L 10.1 1 03/18/22 21:07 JMV V16388
Benzo(g,h,i)perylene <10.1 ljg/L 10.1 1 03/18/22 21:07 JMV V16388
Benzo(k)fluoranthene <10.1 pg/L 10.1 1 03/18/22 21:07 JMV V16388
Chrysene <10.1 lig/L 10.1 1 03/18/22 21:07 JMV V16388
Dibenz(a,h)anthracene <20.2 pg/L 20.2 1 03/18/22 21:07 JMV V16388
Fluoranthene <10.1 pg/L 10.1 1 03/18/22 21:07 JMV V16388
Fluorene <10.1 pg/L 10.1 1 03/18/22 21:07 JMV V16388
Indeno(1,2,3-cd)pyrene <10.1 pg/L 10.1 1 03/18/22 21:07 JMV V16388
1-Methylnaphthalene <10.1 pg/L 10.1 1 03/18/22 21:07 JMV V16388
2-Methylnaphthalene <10.1 pg/L 10.1 1 03/18/22 21:07 JMV V16388
Naphthalene <10.1 pg/L 10.1 1 03/18/22 21:07 JMV V16388
Phenanthrene <10.1 pg/L 10.1 1 03/18/22 21:07 JMV V16388
Pyrene <10.1 pg/L 10.1 1 03/18/22 21:07 JMV V16388
Surrogate: 2-Fluorobiphenyl 55.4 Limits: 44-119% 1 03/18/22 21:07 JMV V16388
Surrogate: Nitrobenzene-d5 52.7 Limits: 44-120% 1 03/18/22 21:07 JMV V16388
Surrogate:4-Terphenyl-d14 61.8 Limits: 50-134% 1 03/18/22 21:07 JMV V16388
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

o
V"apourit 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :03/10/2022
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95869 Matrix: Aqueous
Sample ID :Influent Sampled: 3/10/2022 12:05
Analytical Method: 624.1 Prep Batch(es): V16235 03/16/22 09:00 V16599 03/24/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acetone 7.52 IJ9/L 5.00 1 03/16/22 22:28 JLB V16236
Acrolein <5.00 IJ9/L 5.00 1 03/16/22 22:28 JLB V16236
Acrylonitrile <5.00 pg/L 5.00 1 03/16/22 22:28 JLB V16236
Benzene 161 pg/L 50.0 100 03/24/22 17:02 JLB V16601
Bromodichloromethane <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
Bromoform <3.00 pg/L 3.00 1 03/16/22 22:28 JLB V16236
Bromomethane <2.00 IJ9/L 2.00 1 03/16/22 22:28 JLB V16236
Carbon Tetrachloride <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
Chlorobenzene <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
Chlorodibromomethane <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
Chloroethane <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
2-Chloroethylvinyl Ether <10.0 pg/L 10.0 1 03/16/22 22:28 JLB V16236
Chloroform <1.00 lJ9/L 1.00 1 03/16/22 22:28 JLB V16236
Chloromethane <1.00 lJ9/L 1.00 1 03/16/22 22:28 JLB V16236
1,2-Dichlorobenzene <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
1,3-Dichlorobenzene <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
1,4-Dichlorobenzene <1.00 lJ9/L 1.00 1 03/16/22 22:28 JLB V16236
1,1-Dichloroethane <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
1,2-Dichloroethane 9.39 pg/L 1.00 1 03/16/22 22:28 JLB V16236
1,1-Dichloroethene <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
trans-1,2-Dichloroethene <2.00 pg/L 2.00 1 03/16/22 22:28 JLB V16236
1,2-Dichloropropane <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

w
WaypoIut 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :03/10/2022
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95869 Matrix: Aqueous
Sample ID :Influent Sampled: 3/10/2022 12:05
Analytical Method: 624.1 Prep Batch(es): V16235 03/16/22 09:00 V16599 03/24/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
cis-1,3-Dichloropropene <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
trans-1,3-Dichloropropene <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
Ethylbenzene 32.4 u9/L 1.00 1 03/16/22 22:28 JLB V16236
Methylene Chloride <2.00pg/L 2.00 1 03/16/22 22:28 JLB V16236
Y
1,1,2,2-Tetrachloroethane <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
Tetrachloroethene 3.59 pg/L 0.750 1 03/16/22 22:28 JLB V16236
Toluene 3.67 pg/L 1.00 1 03/16/22 22:28 JLB V16236
1,1,1-Trichloroethane <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
1,1,2-Trichloroethane <0.500 pg/L 0.500 1 03/16/22 22:28 JLB V16236
Trichloroethene <1.00 IJ9/L 1.00 1 03/16/22 22:28 JLB V16236
Trichlorofluoromethane <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
1,2,3-Trichloropropane <1.00 u9/L 1.00 1 03/16/22 22:28 JLB V16236
1,2,4-Trimethylbenzene 15.1 pg/L 0.500 1 03/16/22 22:28 JLB V16236
Vinyl Chloride <1.00 pg/L 1.00 1 03/16/22 22:28 JLB V16236
o-Xylene 40.9 u9/L 1.00 1 03/16/22 22:28 JLB V16236
m,p-Xylene 48.3 pg/L 2.00 1 03/16/22 22:28 JLB V16236
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Waypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :03/10/2022 1
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95869 Matrix: Aqueous
Sample ID :Influent Sampled: 3/10/2022 12:05
Analytical Method: 624.1 Prep Batch(es): V16235 03/16/22 09:00 V16599 03/24/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Xylene(Total) 89.2 pg/L 1.00 1 03/16/22 22:28 V16236
Surrogate:4-Bromofluorobenzene 95.8 Limits: 74-126% 1 03/16/22 22:28 JLB V16236
Surrogate: Dibromofluoromethane 96.8 Limits: 75-127% 1 03/16/22 22:28 JLB V16236
Surrogate: 1,2-Dichloroethane-d4 95.0 Limits: 67-136% 1 03/16/22 22:28 JLB V16236
Surrogate:Toluene-d8 97.6 Limits: 70-130% 1 03/16/22 22:28 JLB V16236
1 Surrogate:4-Bromofluorobenzene 101 Limits: 74-126% 100 03/24/22 17:02 JLB V16601
Surrogate: Dibromofluoromethane 96.6 Limits: 75-127% 100 03/24/22 17:02 JLB V16601
Surrogate: 1,2-Dichloroethane-d4 91.8 Limits: 67-136% 100 03/24/22 17:02 JLB V16601
Surrogate:Toluene-d8 91.2 Limits: 70-130% 100 03/24/22 17:02 JLB V16601
Analytical Method: 625.1 Prep Batch(es): V16233 03/17/22 12:00
Prep Method: 625.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Acenaphthylene <20.2 pg/L 20.2 1 03/18/22 18:09 JMV V16380
Anthracene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Benzidine <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Benzo(a)anthracene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Benzo(a)pyrene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Benzo(b)fluoranthene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Benzo(g,h,i)perylene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Benzo(k)fluoranthene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Waypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :03/10/2022
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95869 Matrix: Aqueous
Sample ID :Influent Sampled: 3/10/2022 12:05
Analytical Method: 625.1 Prep Batch(es): V16233 03/17/22 12:00
Prep Method: 625.1(Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Benzoic Acid <50.5 u9/L 50.5 1 03/18/22 18:09 JMV V16380
Benzyl alcohol <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Bis(2-Chloroethoxy)methane <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Bis(2-Chloroethyl)ether <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Bis(2-Chloroisopropyl)ether <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Bis(2-ethylhexyl)phthalate <10.1 u9/L 10.1 1 03/18/22 18:09 JMV V16380
4-Bromophenyl phenyl ether <20.2 pg/L 20.2 1 03/18/22 18:09 JMV V16380
Butyl benzyl phthalate <10.1 ii9/L 10.1 1 03/18/22 18:09 JMV V16380
4-Chloro-3-methylphenol <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
2-Chloronaphthalene <20.2 pg/L 20.2 1 03/18/22 18:09 JMV V16380
2-Chlorophenol <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
4-Chlorophenyl phenyl ether <20.2 pg/L 20.2 1 03/18/22 18:09 JMV V16380
Chrysene <10.1 N9/L 10.1 1 03/18/22 18:09 JMV V16380
Dibenz(a,h)anthracene <20.2 u9/L 20.2 1 03/18/22 18:09 JMV V16380
Dibenzofuran <20.2 u9/L 20.2 1 03/18/22 18:09 JMV V16380
1,2-Dichlorobenzene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
1,3-Dichlorobenzene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
1,4-Dichlorobenzene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
3,3'-Dichlorobenzidine <10.1 Jg/L 10.1 1 03/18/22 18:09 JMV V16380
2,4-Dichlorophenol <10.1 u9/L 10.1 1 03/18/22 18:09 JMV V16380
Diethyl phthalate <20.2 pg/L 20.2 1 03/18/22 18:09 JMV V16380
Dimethyl phthalate <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

O
Waypoint, 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 03/10/2022
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95869 Matrix: Aqueous
Sample ID :Influent Sampled: 3/10/2022 12:05
Analytical Method: 625.1 Prep Batch(es): V16233 03/17/22 12:00
Prep Method: 625.1 (Prep)
Test Results Units MOL DF Date/Time By Analytical
Analyzed Batch
2,4-Dimethylphenol <20.2 IJg/L 20.2 1 03/18/22 18:09 JMV V16380
Di-n-butyl phthalate <10.1 ug/L 10.1 1 03/18/22 18:09 JMV V16380 1
4,6-Dinitro-2-methylphenol <30.3 ug/L 30.3 1 03/18/22 18:09 JMV V16380
2,4-Dinitrophenol <30.3 pg/L 30.3 1 03/18/22 18:09 JMV V16380
2,4-Dinitrotoluene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
2,6-Dinitrotoluene <20.2 pg/L 20.2 1 03/18/22 18:09 JMV V16380
Di-n-Octyl Phthalate <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Fluoranthene <10.1 ljg/L 10.1 1 03/18/22 18:09 JMV V16380
Fluorene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Hexachlorobenzene <20.2 pg/L 20.2 1 03/18/22 18:09 JMV V16380
Hexachlorobutadiene <20.2 lJg/L 20.2 1 03/18/22 18:09 JMV V16380
Hexachlorocydopentadiene <20.2 pg/L 20.2 1 03/18/22 18:09 JMV V16380
Hexachloroethane <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Indeno(1,2,3-cd)pyrene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Isophorone <10.1 u9/L 10.1 1 03/18/22 18:09 JMV V16380
1-Methylnaphthalene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
2-Methylnaphthalene <10.1 ljg/L 10.1 1 03/18/22 18:09 JMV V16380
Naphthalene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Nitrobenzene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
2-Nitrophenol <10.1 lig/L 10.1 1 03/18/22 18:09 JMV V16380
4-Nitrophenol <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
N-Nitrosodiphenylamine <20.2 pg/L 20.2 1 03/18/22 18:09 JMV V16380
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

4 II
w
\Waypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :03/10/2022
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95869 Matrix: Aqueous
Sample ID :Influent Sampled: 3/10/2022 12:05
Analytical Method: 625.1 Prep Batch(es): V16233 03/17/22 12:00
Prep Method: 625.1 (Prep)
Test Results Units MOL DF Date/Time By Analytical
Analyzed Batch
N-Nitroso-di-n-propylamine <20.2 ug/L 20.2 1 03/18/22 18:09 JMV V16380
Pentachlorophenol <50.5 pg/L 50.5 1 03/18/22 18:09 JMV V16380
Phenanthrene <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Phenol <10.1 pg/L 10.1 1 03/18/22 18:09 JMV V16380
Pyrene <10.1 ug/L 10.1 1 03/18/22 18:09 JMV V16380
1,2,4-Trichlorobenzene <10.1 ug/L 10.1 1 03/18/22 18:09 JMV V16380
2,4,6-Trichlorophenol <20.2 pg/L 20.2 1 03/18/22 18:09 JMV V16380
Surrogate: Phenol-d5 24.1 Limits: 10-63% 1 03/18/22 18:09 JMV 625.1
Surrogate: 2-Fluorobiphenyl 57.8 Limits: 49-118% 1 03/18/22 18:09 JMV V16380
Surrogate: 2-Fluorophenol 35.9 Limits: 22-84% 1 03/18/22 18:09 JMV V16380
Surrogate: Nitrobenzene-d5 54.5 Limits: 43-123% 1 03/18/22 18:09 JMV V16380
Surrogate:4-Terphenyl-d14 76.6 Limits: 49-151% 1 03/18/22 18:09 JMV V16380
Surrogate: 2,4,6-Tribromophenol 75.5 Limits: 31-144% 1 03/18/22 18:09 JMV V16380
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

O
Waypoint, 449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 03/30/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 03/10/2022
Indian Trail , NC 28079
Report Number:22-069-0033 REPORT OF ANALYSIS
Lab No : 95870 Matrix: Aqueous
Sample ID :Influent -8270 PAH Sampled: 3/10/2022 12:05
Analytical Method: 8270E Prep Batch(es): V16234 03/17/22 12:00
Prep Method: 3510C
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
<20.0 pg/L20.0 1 03 18 Acenaphthene 22 21:29 JMV V16388
p / /
Acenaphthylene <20.0 ug/L 20.0 1 03/18/22 21:29 JMV V16388
Anthracene <10.0 pg/L 10.0 1 03/18/22 21:29 JMV V16388
Benzo(a)anthracene <10.0 pg/L 10.0 1 03/18/22 21:29 JMV V16388
Benzo(a)pyrene <10.0 ug/L 10.0 1 03/18/22 21:29 JMV V16388
Benzo(b)fluoranthene <10.0 pg/L 10.0 1 03/18/22 21:29 JMV V16388
Benzo(g,h,i)perylene <10.0 pg/L 10.0 1 03/18/22 21:29 JMV V16388
Benzo(k)fluoranthene <10.0 pg/L 10.0 1 03/18/22 21:29 JMV V16388
Chrysene <10.0 pg/L 10.0 1 03/18/22 21:29 JMV V16388
Dibenz(a,h)anthracene <20.0 iJg/L 20.0 1 03/18/22 21:29 JMV V16388 1
Fluoranthene <10.0 ug/L 10.0 1 03/18/22 21:29 JMV V16388
Fluorene <10.0 pg/L 10.0 1 03/18/22 21:29 JMV V16388
Indeno(1,2,3-cd)pyrene <10.0 pg/L 10.0 1 03/18/22 21:29 JMV V16388
1-Methylnaphthalene <10.0 pg/L 10.0 1 03/18/22 21:29 JMV V16388
2-Methylnaphthalene <10.0 ug/L 10.0 1 03/18/22 21:29 JMV V16388
Naphthalene <10.0 pg/L 10.0 1 03/18/22 21:29 JMV V16388
Phenanthrene <10.0 ug/L 10.0 1 03/18/22 21:29 JMV V16388
Pyrene <10.0 ljg/L 10.0 1 03/18/22 21:29 JMV V16388
Surrogate: 2-Fluorobiphenyl 51.8 Limits:44-119% 1 03/18/22 21:29 JMV V16388
Surrogate: Nitrobenzene-d5 51.4 Limits: 44-120% 1 03/18/22 21:29 JMV V16388
Surrogate:4-Terphenyl-d14 56.6 Limits: 50-134% 1 03/18/22 21:29 JMV V16388
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

•
Waypoint.. 449 Springbrook Rd,Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:00004
Customer Name: Heric Solutions, LLC
Report Number: 22-069-0033
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: IIRT-15 1.7C
Shipping container/cooler uncompromised? 0 Yes 0 No
Number of coolers/boxes received [ 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody (COC) present? 0 Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? 0 Yes 0 No
Sample containers intact? 0 Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No 0 N/A
Water- VOA vials free of headspace 0 Yes 0 No 0 N/A
Trip Blanks received with VOAs 0 Yes 0 No 0 N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A
r High concentration container (48 hr) r Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) i Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: 1Sarah J. Locklear 1 Date &Time: 03/10/2022 15:33:30

f11llfl fill' 1fLli ii i� 33 CHAIN OF CUSTODY RECORD LAB USE ONLY
03-10 2022 PAGE OF / p TE a TOENSURE PROPER BILLING_ YES NO N A
Samples INTACT upon arrival? —
1524:50 -Henc Solutions.LLC �f! V PA
�/� Received IN ICE? / -
Monthiv Project Name: (� ^- t
Short Hold Anal sis (Yes) (No) UST Project: (Yes) (No) PROPER PRESERVATIVES indicated? Z___
'Please ATTACH any project specific reporting(QC LEVEL I I1 III IV) Received WITHIN HOLDING TIMES? / _.__
Client Company Name: i+�-{fjLG — provisions and/or QC Requirements
CUSTODY SEALS INTACT? �__
Report To/Contact Name: ---- Invoice To: VOLATILES reed W/OUT HEADSPACE? ' _
Reporting Address: -- Address: PROPER CONTAIN S used? -'
"- TEMP: Therm ID ..�Observed 1_. 'C/Co -1_"q
Phone:- Fax(Yes)(No): Purchase Order No./Billing Reference TO BE FILLED IN BY CULT/SAMPUNG PERSONNEL
Email Address: Requested Due Date J I Day J 2 Days J 3 Days J 4 Days J 5 Days J/
Certification: NC SC
EDD Type: PDF Excel Other "Working Days" J 6-9 Days J Standard 10 days J Rush Work Must Be
Site Location Name: Samples received after 15:00 will be processed next business day
Other N/A
Site Location Physical Address: Turnaround time Is based on business days.excluding weekends and holidays. Water Chlorinated: YES NO
(SEE REVERSE FOR TERMS S CONDITIONS REGARDING SERVICES
—___ RENDERED BY WAYPOINT ANALYTICAL.LLC TO CUENT) Samples Iced Upon Collection: YES O._,,.
T— ANALYSIS REQUESTED
TIME MATRIX SAMPLE CONTAINER / ,
CLIENT DATE COLLECTED (SOIL, �--- PRESERVA- ox
RS
ILITARY WATER., ID NO.
DESCRIPTIONSAMPLE DESCRIPTN COLLECTED MHOtI SLUDGE)R SEE g�pW+ NO. SIZETIVES �.
,,,,,,,,_
1 ,_ /. Amver
*
i _ 3o 1(
ev........-....-•-........-r. Y
. y ----k.? /7 - .._
, y 5 ig, 1-- ail
bit? 11.05- A-c__ 1..... /Ow //4944---
?‹ ali
/9 2 god
-1l j
- 3 y`' ci X — -
•
/J PRESS DOWN FIRMLY -2 COPIES
Samplers Signature ._........._ �' •• Sampled By(Print Name) I Ill' ertir
--'--- - �/_ - Affiliation.._- — LAB USE ONLY
Upon relinquishing,this Chain of Custo is your authorization for Waypoint Analytical to proceed with the analyses as requested above.Any changes must be
submitted in writing to the Waypoint Analytical Project Manager.There will be charges for any changes after analyses have been initialized. Situ Arrival Time:
R011 e,7;y (S . Hoot-m•d By.(Signature! -T Dale - MdaaryiFWurs
_AD '�r��'j 1/�r� Additional Comments
Site Departure Time:
Roll y•(Siena -•'(� Received By (Signature) Date Field Tech Fee.
Relinquished By.(Signature) Received For Waypo nl Analytical Ay Mileage'
Method of Shipment NOTE:ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FORT AN O TA TI T THE LABORATORY COC Group No
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY
SEE REVERSE FOR
J Fad Ex J UPS j Hand-delivered re Analytcal Fred Service J Other __._ _...__ ___ TERMS&CONDITIONS
NPDES:
UST: G (MD-WATER DRINKING"WATER: SOLID WASTE: RCRA: BRWNFLD LANDFILL -OTHER:-
JNCJSC JNC JSC JNC JSC JNC JSC ..INC JSC JNC JSC JNC JSC JNC JSC .JNC JSC
J J J L7 IJ J L] LI_ J ORIGINAL
I

ETT ! IIIOIIIIIIIIiNIIIIiII1IIIIIN1111l1lllll1 00004
0 4- 69-0033
Hens Solutions
M11onthIrmlhtV 15.24 SO
s _�.' Y ry
'' Page of
P L 60a 16.41z,Greenville,SC 29808-74 t4
[phone]. [phone] Fax.[phone]
Sh ping Address:4 Craftsman CI,Greer,SC 29650
W WW.CT-CNV,ROMMCIrAL.COM
Client: d'ideA 5. „.b"":' 'G�tyvs.< Program Containers Preservative Parameters
Facility:
Whole Effluent Textdcv
State: NPDES>': Acute Chronic Test Organisms _
.� _.
d =
c • c a .
a (Composite on!v) (Grab or Composite) o u 5 U 2 _ 7,4
u _
r Sign,and Print below 5 t5 o u o v '-"HCL e o o = ..Er.2 r ? v i e c
CI
the dotted lint = c r U .' ,.r4 o t = =' i e > _�.:I; `y
SAMPLE ID Ci Cempo,iu Sum Date lima Sample Coaection Dote Tinto Collected by U t`n c�ia 2 4e nr.. U > —�'#b.p Ac ¢ U U U1 2 it:, =I. 13 a Chemical Analysis&Other
�% rig �2 rzis -'-S- I x au X�►/ �
::___ ___ _ - ... __ __ . .� __.¢_.__�Special:s�:
b-/.24g,r- 4/(6,44,id
i.
Sample Custody Transfer Record ;Se test Receipt Sample
Date Time Relinquished By/Organization Received v I Orstani ttien i Area Temp Preserved?
3�� 2 3-� ',
2
f
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES —
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testlng the sample must first be used within 36 hours
Time Proportional: I sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bass. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after?2 hours from,sample collection
Flow Proportional:As per instructions in I.NPDES permit.

Waypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
4/1/2022
Heric Solutions, LLC
Eric Donnelly
P.O. Box 548
Indian Trail, NC, 28079
Ref: Analytical Testing
Lab Report Number: 22-073-0007
Client Project Description: Monthly
1111 Pecan Ave.
Project Number: Permit NC0089958
Dear Eric Donnelly:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/14/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
a (
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

Q
Vvaypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Certification Summary
LaboratoryID: WP CNC:Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
Yp Y
State Program Lab ID Expiration Date
North Carolina State Program 37735 07/31/2022
North Carolina State Program 402 12/31/2022
South Carolina State Program 99012 07/31/2022
South Carolina State Program 99012 12/31/2022
Page 1 of 1 00016/22-073-0007

Q
V/aypoint, 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-073-0007
Client Project Description: Monthly
1111 Pecan Ave.
Lab No Client Sample ID Matrix Date Collected Date Received
96035 Monthly Aqueous 03/14/2022 10:10 03/14/2022 14:00

' cmirontrtpnta.Inc. (C64)977-6£+42 .FAX[phone]
r O. Dox 1 E414, Greenv Ile. SC 29606 4 Craftsman Court, Gruer, SC 29650
Pimephales promelas 48 Hour Acute Definitive Test
EPA-821-R-02-012 Method 2000
Client: HERIC SOLUTIONS
Sample ID:EFFLUENT
NPDES#:NC0089923
Test Date: 15-Mar-22
Laboratory ID#: T61481
Test Reviewed and Approved By:
Robert W.Kelley,Ph.D. Patrick D.Timms
President QAJQC Officer
' Certification#E87819 SCDHEC Certification#23104
Test resultspresented in thisreport conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided sW les.age of 4
NCDENR Certification# 022
1

Effluent Toxicity Report Form-Chronic Pass/Fail and Acute LC50 Date 29-Mar-22
Facility: HERIC SOLUTIONS NPDES#NC0089923 Pipe# 001 County. Mecklenburg
Laboratory Performing Test: Comments
x
Signature of Operator in Responsible Charge �{
x � 474
Signature of Laboratory Supervisor
MAIL ORIGINAL TO Environmental Sciences Branch
Div.of Water Quality
N.C.DENR
1621 Mail Service Center
Raleigh,North Carolina 27699-1621
North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results
Calculated t=
Critical Value=
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction=
#Young Produced %Mortality Avg.Reprod.
Adult (L)ive (D)ead i
Control Control
Effluent%
Treatment 2 Treatment 2
Control CV
TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
#Young Produced %3rd Brood PASS FAIL
-
Adult (L)ive (D)ead I X I
Complete This for Either Test Test Start Date
Collection(Start)Date 15-Mar-22
pH 1st sample 1st sample 2nd sample Sample 1 14-Mar-22 Sample 2 NA
Control Sample Type(Duration)
Treatment 2 Grab 1 Comp Duration 1st 2nd
Sample 1 X Tox Tox
a
Sample 2 Dilution Sample Sample
start end start end start end
D.O. 1st samde 1st sample 2nd sample Hardness(mg/L) 83.7
Control Spec.Cond.(pmhos) 304 81
Treatment 2 Chlorine(mg/L) <0.05
Sample Temp.at receipt("C) 1.0
LC50/Acute Toxicity Test
(Mortality expressed as%,combining replicates)
0 6.25 12.5 25 50 100 Concentration
0 0 0 0 0 0 Mortality start/end start/end
LC50= >100 °Ao Method of Determination 7.8 8.2 Control 8.1 8.4
95%Confidence Limits Moving Average Probit ME 7.5 7.9 High Conc. 8.7 8.2
NA % NA % Spearman Karber Other X pH D.O.
Organism Tested Pimephales promelas I
DEM Form AT-1
Page 2 of 4

48 Hour Acute Toxicity Test
Test Method:EPA 821 R-02-012, Method 2000 Pimephales promelas
Client: HERIC SOLUTIONS Sample ID:EFFLUENT Lab 1D#: T61481
Start Date: 03/15/22 Time: 02:45 PM Set By: JG
End Date: 03/17/22 Time: 02:15 PM Ended By: JG
Test Vessel Test Solution Volume Incubator Transfer Volume Dilution Water
Fathead Minnows 500 mL plastic cup 200 mL #1 0.5 mL MHSF
Randomization pattern per SOP (Neonates from common holding vessel !Light: 50-100 ft-c. 16 hr light/8 hr dark
TEST ORGANISMS
for Ceriodaphnia dubia Comments:
Date Removed: Between: and:
Pimephales promelas Source: ABS lays old: 5
Mysidopsis bahia Source: Days old:
Test Organisms Pre Fed by: JG Time: 12:00
MORTALITY DATA
Conc. iooula Cumulative Mortality Final Initial Final
Cond/ Cond/
Rep venr Mortality Temp D.O. pH Salini By Temp D.O. pH Salini By
A 10 0 ` te" ">
� ° T S n
Control B 10 . . $ k s ,_ t.! h
C s ,,, {, ice zr in✓" 12,„;,. .: - .c.: :;c:.,, iAP :2
D 0% 24.5 8.1 7.8_JG 24.8 8.4 8.2_JG
A 10 0
6.3% B 10 0 x` f.'` z`C` 4' ` ` ,Z-r, ,,
C ., ., ,. � f,.,,. �' « ;fir irti;t k
D 0% 24.5 8.2 8.0_JG 24.8 8.3 8.2_JG
A 10 0 f' =fix e g `i Fa zf,«f.
12.5% B 10 0 , r� �
C T . # ,r w ii '0� ?? n w:z s -
il
D 0% 24.5 8.5 8.1 _JG 24.8 8.4 8.2_JG
25.0o a E t ' c
arC b?, .; ,F
D 0% 24.5 7.7 8.0 JG 24.8 8.2 8.1 JG
A 10 0 rW° ' e .+ r- -- rF -- ,s-
50.0% B 10 0 r r1 z A r r
C
D 0% 24.5 8.0 7.8_JG 24.8 8.3 8.1 _JG
A 10 0 " g�
100.0% B 10 0
r �(e
C " d-s r' L; v FR'M4i ^um"r r,.,:,:,,.:. '-.u. -._.i, ?tea u. `: "4.
D 0% 24.5 8.7 7.5 JG 24.8 8.2 7.9 JG
A
B �"l"i;': W, z; , ar, R
g ;x'g . r "Y r &--' 4:Vet"sa'�': sue'„
C °4r ,ire 'te - .=.,a`� `
D °C Ern PP I Millr!{NII PPT
Page 3 of 4

C AS OF CUSTODY RECORD
PO Box 16414,Greenvl fe,SC 29808-7414 /
inETT
�./Y
[phone], [phone] Faz 8 I \ L n //t I Y V !Page OI
Shipping Address:4 Craftsman Ct,Greer,SC 29650
W W W.rrrcN VIRONM CNTALC OM
111111MMIL• A
Facility: Preservative
Parameters
State: iYPDES#: Whore Effluent Toxicity
Q
Acute Chronic Test Organisms
r_,
^ <
U (Composite only) (Grab or Composite) ti .� o r ti
cj o rzt U ( U a 5 Z
Sl;n,and Print below 11 �' �a ,I' 0A — — - - L
U aHCL c 2 0 o c rn c :_' .the dotted line E U ,� c SAMPLE ID • -HNoa _ n -
C°mpasitc Stan Data Time o NaoH So E. o O - i= P. •= n = 2 N i !-
Sample Collactian Dal° Time Collected by U vi r, z 00. d Ts Ts 8 s-zmc u 'u - CP ^ y,.> T_ • g i_
3 /ct ZZ e-Omer ¢ < U U tJ Ci L 2 n ; U 3 Chemical Analysis Other
/^ lay- -/ __ - _.._
CD
(10
1 �1,-k,
A
O1.111
A
111111lII!111111111111111111111111ns, II �7
C
Monthly 13:35:35
1111
S e_' ---
s c,allnsmtciions - / _ -.__-.._ _-- --
Sample Custody Transfer Record
D� Time _Relin wished B /Or- Secure Receipt Sample
17 Re eiv d B /Or izztion
r � Are 2 Tzm -C Preserved?
Li,o'CILLOIt
MIN 0-ao '
COMPOSITE SAMPLING PROCEDURES - --
1 1
Composite samples must be collected over a 24 hour period. Sample temperature TEMPERATURE �uring collectionNITORING Oand transport must be between HOLD TIMEtyrPROCEDURES
Time Proportional:I sample each hour for 24 hours.Equal volu,0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample
ample lllecto the sample must first beos used�tplel.36 hours
or at minimum 1 sample every 4 hours over14 hnun ofsample collection(completion of composite sample?. —
F1owPruportional:As per instructions in NPDES permit Sample may not be used after 72 hours from sample collection.

WaypOlflt 449 Springbrook Rd, Charlotte, NC
Main 704.529.636428217
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:00004
Customer Name: Heric Solutions, LLC
Report Number: 22-073-0007
Shipping Method
0 Fed Ex 0 US Postal # Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: DIRT-15 4.0 C
Shipping container/cooler uncompromised? # Yes 0 No
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody (COC) present? # Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? 0 Yes 0 No
Sample containers intact? 0 Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. # Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved # Yes 0 No 0 N/A
Water- VOA vials free of headspace 0 Yes 0 No # N/A
Trip Blanks received with VOAs 0 Yes 0 No # N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A
r High concentration container (48 hr) P Low concentration EnCore samplers (48 hr)
r High concentration pre-weighed (methanol -14 d) r Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: 1Zoe S. Vigilant Date &Time: 03/14/2022 14:09:44 1

1
ETT CHAIN OF CUSTODY RECORD
•.r a .. �0.,,,.. 4 11 Page ,
PO Box 16414,Greenvi9e,SC 2S61 8-7414
[phone], [phone] P4x:[phone]
Shipping Acklress:4 Craftsman Ct,Greer.SC 299550
WwW.CTTC.V MONM eN7AL.Ct]M
Client: _
caL4),,,,,,,
Program Containers Pr .:^:.rive ' _, _....,
Facility:
Whole Cmucat Taaidr�- i ._
State: NPDES m: acute Chronic Teat Orynnisnts
' t I _ sa .- o c
(Composite arty) (Grab or Composite; G o u a rJ .3 0 ..
J d u _ `s t.H25M 'a - g - -
Sign,and Print below Si m o ?-HCt - Ea •°' ^ •., 'e
tJ l'l.dotted line L '? w �, u v 3 P '_ r _
SAMPLE ID C7 Cempetite S,u Date Time Sam le Conectien Date)Time Collectedt? cc,2 Z vt C y i=f0(1,nAc v r ,y a: .T.,
v by s.p,� < 4 t:J U U � � w .:, t;J = 3 2 Chemical Analysis&Other
,k', ? ! � �� ( x Ian.) x 1V)A I
- 111111111 ft 1111 I II ft 1 tIIIIIII "°; - __-
iAi:wi�.»lunrzt„s LLC -2022
13'35.35
Ni;athty .....
Instructions:
Cp-vr4, r�t 9. Goy— . )
Sample Custody Transfer Record Secure Receipt • Sample
Efate Time k i0I_
rstan"zauon 3iTTi2
Area Temp C . Preserved''
Ili.a-l' itict)IC
1
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MON/TORJNG PROCEDURES '£?OLD TIAlE PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional: I sample each hour for 24 hours.Equal volur 0,0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample),
or at minimum I sample every"4 hours over 24 hours. Sample may not be used after 72 hours front sample collection,
Flow Proportional:As per instructions in N(DES permit.

•
waypOI■ ■ . 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
4/11/2022
Heric Solutions, LLC
Eric Donnelly
P.O. Box 548
Indian Trail, NC, 28079
Ref: Analytical Testing
Lab Report Number: 22-083-0042
Client Project Description: Bi-Monthly
1111 Pecan Ave.
Project Number: Permit NC0089958
Dear Eric Donnelly:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/24/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

\/%ypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Certification Summary
LaboratoryID: WP CNC: Waypoint Analytical Carolina, Inc. C , Charlotte, NC
YP Y ( )
State Program Lab ID Expiration Date
North Carolina State Program 37735 07/31/2022
North Carolina State Program 402 12/31/2022
South Carolina State Program 99012 07/31/2022
South Carolina State Program 99012 12/31/2022
Page 1 of 1 00016/22-083-0042

'/ /aypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalyncal.com
Sample Summary Table
Report Number: 22-083-0042
Client Project Description: Bi-Monthly
1111 Pecan Ave.
Lab No Client Sample ID Matrix Date Collected Date Received
96877 Effluent Aqueous 03/24/2022 13:10 03/24/2022 14:45
96878 Effluent-8270 PAH Aqueous 03/24/2022 13:10 03/24/2022 14:45
96879 Influent Aqueous 03/24/2022 13:15 03/24/2022 14:45
96880 Influent -8270 PAH Aqueous 03/24/2022 13:15 03/24/2022 14:45

w
\/ Iapoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 04/11/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 03/24/2022
Indian Trail , NC 28079
Report Number:22-083-0042 REPORT OFANALYSIS
Lab No : 96877 Matrix: Aqueous
Sample ID : Effluent Sampled: 3/24/2022 13:10
Test Results Units MOL DF Date/Time By Analytical
Analyzed Method
pH 6.11 s.u. 1 03/24/22 13:10 FLD FIELD
Temperature 21.9 C 0.1 1 03/24/22 13:10 FLD FIELD
Arsenic <1.00 pg/L 1.00 1 03/30/22 15:52 EDV 200.8
Barium <5.00 pg/L 5.00 1 03/30/22 15:52 EDV 200.8
Cadmium <1.00 pg/L 1.00 1 03/30/22 15:52 EDV 200.8
Chromium 2.17 pg/L 1.00 1 03/30/22 15:52 EDV 200.8
Copper <2.00 pg/L 2.00 1 03/30/22 15:52 EDV 200.8
Lead <1.00 u9/L 1.00 1 03/30/22 15:52 EDV 200.8
Mercury(Total) <0.000200 mg/L 0.000200 1 03/29/22 17:24 EDV 245.1
Nickel <5.00 pg/L 5.00 1 03/30/22 15:52 EDV 200.8
Selenium <5.00 pg/L 5.00 1 03/30/22 15:52 EDV 200.8
Zinc <10.0 pg/L 10.0 1 03/30/22 15:52 EDV 200.8
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions MQL Method Quantitation Limit

r r�r
M��
Waypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.coin
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 04/11/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 03/24/2022
Indian Trail , NC 28079
Report Number:22-083-0042 REPORT OF ANALYSIS
Lab No : 96877 Matrix: Aqueous
Sample ID : Effluent Sampled: 3/24/2022 13:10
Analytical Method: 624.1 Prep Batch(es): V17197 04/07/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Benzene <0.500 pg/L 0.500 1 04/07/22 15:00 JLB V17200
Ethylbenzene <1.00 ug/L 1.00 1 04/07/22 15:00 JLB V17200
Toluene <1.00 ug/L 1.00 1 04/07/22 15:00 JLB V17200
o-Xylene <1.00 ug/L 1.00 1 04/07/22 15:00 JLB V17200
m,p-Xylene <2.00 pg/L 2.00 1 04/07/22 15:00 JLB V17200
Xylene(Total) <1.00 pg/L 1.00 1 04/07/22 15:00 V17200
Surrogate:4-Bromofluorobenzene 107 Limits: 74-126% 1 04/07/22 15:00 JLB V17200
Surrogate: Dibromofluoromethane 99.4 Limits: 75-127% 1 04/07/22 15:00 JLB V17200 1
Surrogate: 1,2-Dichloroethane-d4 107 Limits: 67-136% 1 04/07/22 15:00 JLB V17200
Surrogate:Toluene-d8 103 Limits: 70-130% 1 04/07/22 15:00 JLB V17200
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions MQL Method Quantitation Limit

Waypoint, 449 SPringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 04/11/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 03/24/2022
Indian Trail , NC 28079
Report Number:22-083-0042 REPORT OF ANALYSIS
Lab No : 96878 Matrix: Aqueous
Sample ID : Effluent-8270 PAH Sampled: 3/24/2022 13:10
Analytical Method: 8270E Prep Batch(es): V16827 03/31/22 10:00
Prep Method: 3510C
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <20.0 ug/L 20.0 1 03/31/22 22:16 JMV V16992
Acenaphthylene <20.0 pg/L 20.0 1 03/31/22 22:16 JMV V16992
Anthracene <10.0 ug/L 10.0 1 03/31/22 22:16 JMV V16992
Benzo a anthracene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
Benzo(a)pyrene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
Benzo(b)fluoranthene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
Benzo(g,h,i)perylene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
Benzo(k)fluoranthene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
Chrysene <10.0 ug/L 10.0 1 03/31/22 22:16 JMV V16992
Dibenz(a,h)anthracene <20.0 pg/L 20.0 1 03/31/22 22:16 JMV V16992
Fluoranthene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
Fluorene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
Indeno(1,2,3-cd)pyrene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
1-Methylnaphthalene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
2-Methylnaphthalene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
Naphthalene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
Phenanthrene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
Pyrene <10.0 pg/L 10.0 1 03/31/22 22:16 JMV V16992
Surrogate: 2-Fluorobiphenyl 59.0 Limits: 44-119% 1 03/31/22 22:16 JMV V16992
Surrogate: Nitrobenzene-d5 59.8 Limits: 44-1200/0 1 03/31/22 22:16 JMV V16992
Surrogate:4-Terphenyl-d14 82.8 Limits: 50-134% 1 03/31/22 22:16 JMV V16992
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions MQL Method Quantitation Limit

O
Waypoint, 449 Springbrook Rd, Charlotte, NC 28217
1
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 04/11/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :03/24/2022
Indian Trail , NC 28079
Report Number:22-083-0042 REPORT OF ANALYSIS
Lab No : 96879 Matrix: Aqueous
Sample ID :Influent Sampled: 3/24/2022 13:15
Analytical Method: 624.1 Prep Batch(es): V17197 04/07/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acetone <5.00 ug/L 5.00 1 04/07/22 15:48 JLB V17200
Acrolein <5.00 pg/L 5.00 1 04/07/22 15:48 JLB V17200
Acrylonitrile <5.00 ug/L 5.00 1 04/07/22 15:48 JLB V17200
Benzene 14.8 hg/L 0.500 1 04/07/22 15:48 JLB V17200
Bromodichloromethane <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
Bromoform <3.00 ug/L 3.00 1 04/07/22 15:48 JLB V17200
Bromomethane <2.00 lJg/L 2.00 1 04/07/22 15:48 JLB V17200
Carbon Tetrachloride <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
Chlorobenzene <1.00 hg/L 1.00 1 04/07/22 15:48 JLB V17200
Chlorodibromomethane <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
Chloroethane <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
2-Chloroethylvinyl Ether <10.0 pg/L 10.0 1 04/07/22 15:48 JLB V17200
Chloroform <1.00 Jg/L 1.00 1 04/07/22 15:48 JLB V17200
Chloromethane <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
1,2-Dichlorobenzene <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
1,3-Dichlorobenzene <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
1,4-Dichlorobenzene <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
1,1-Dichloroethane <1.00 Jg/L 1.00 1 04/07/22 15:48 JLB V17200
1,2-Dichloroethane 6.29 pg/L 1.00 1 04/07/22 15:48 JLB V17200
1,1-Dichloroethene <1.00 ug/L 1.00 1 04/07/22 15:48 JLB V17200
trans-1,2-Dichloroethene <2.00 pg/L 2.00 1 04/07/22 15:48 JLB V17200
1,2-Dichloropropane <1.00 ug/L 1.00 1 04/07/22 15:48 JLB V17200
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions MQL Method Quantitation Limit

w
V1aypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 04/11/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :03/24/2022
Indian Trail , NC 28079
Report Number :22-083-0042 REPORT OF ANALYSIS
Lab No : 96879 Matrix: Aqueous
Sample ID :Influent Sampled: 3/24/2022 13:15
Analytical Method: 624.1 Prep Batch(es): V17197 04/07/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MOL DF Date/Time By Analytical
Analyzed Batch
cis-1,3-Dichloropropene <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
trans-1,3-Dichloropropene <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
Ethylbenzene 4.45 pg/L 1.00 1 04/07/22 15:48 JLB V17200
Methylene Chloride <2.00 lg/L 2.00 1 04/07/22 15:48 JLB V17200
1,1,2,2-Tetrachloroethane <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
Tetrachloroethene 4.61 u9/L 0.750 1 04/07/22 15:48 JLB V17200
Toluene 1.43 IJg/L 1.00 1 04/07/22 15:48 JLB V17200
1,1,1-Trichloroethane <1.00 ug/L 1.00 1 04/07/22 15:48 JLB V17200
1,1,2-Trichloroethane <0.500 ug/L 0.500 1 04/07/22 15:48 JLB V17200
Trichloroethene <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
Trichlorofluoromethane <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
1,2,3-Trichloropropane <1.00 pg/L 1.00 1 04/07/22 15:48 JLB V17200
1,2,4-Trimethylbenzene 2.31 pg/L 0.500 1 04/07/22 15:48 JLB V17200
Vinyl Chloride <1.00 ii9/L 1.00 1 04/07/22 15:48 JLB V17200
o-Xylene 9.63 pg/L 1.00 1 04/07/22 15:48 JLB V17200
m,p-Xylene 11.1 pg/L 2.00 1 04/07/22 15:48 JLB V17200
Xylene(Total) 20.7 ug/L 1.00 1 04/07/22 15:48 V17200
Surrogate:4-Bromofluorobenzene 107 Limits: 74-126% 1 04/07/22 15:48 JLB V17200
Surrogate: Dibromofluoromethane 97.4 Limits: 75-127% 1 04/07/22 15:48 JLB V17200
Surrogate: 1,2-Dichloroethane-d4 104 Limits: 67-136% 1 04/07/22 15:48 JLB V17200
Surrogate:Toluene-d8 104 Limits: 70-130% 1 04/07/22 15:48 JLB V17200
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions MQL Method Quantitation Limit

Q
1 vaypoi nt 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 04/11/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :03/24/2022
Indian Trail , NC 28079
Report Number :22-083-0042 REPORT OF ANALYSIS
Lab No : 96879 Matrix: Aqueous
Sample ID :Influent Sampled: 3/24/2022 13:15
Analytical Method: 625.1 Prep Batch(es): V16828 03/31/22 10:00
Prep Method: 625.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Acenaphthylene <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
Anthracene <10.0 iJg/L 10.0 1 03/31/22 23:23 JMV V17044
Benzidine <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Benzo(a)anthracene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Benzo(a)pyrene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Benzo(b)fluoranthene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Benzo(g,h,i)perylene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Benzo(k)fluoranthene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Benzoic Acid <50.0 pg/L 50.0 1 03/31/22 23:23 JMV V17044
Benzyl alcohol <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Bis(2-Chloroethoxy)methane <10.0 IJg/L 10.0 1 03/31/22 23:23 JMV V17044
Bis(2-Chloroethyl)ether <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Bis(2-Chloroisopropyl)ether <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Bis(2-ethylhexyl)phthalate <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
4-Bromophenyl phenyl ether <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
Butyl benzyl phthalate <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
4-Chloro-3-methylphenol <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
2-Chloronaphthalene <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
2-Chlorophenol <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
4-Chlorophenyl phenyl ether <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
Chrysene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions MQL Method Quantitation Limit

• Q
WaVpolnt 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 04/11/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :03/24/2022
Indian Trail , NC 28079
Report Number:22-083-0042 REPORT OF ANALYSIS
Lab No: 96879 Matrix: Aqueous
Sample ID :Influent Sampled: 3/24/2022 13:15
Analytical Method: 625.1 Prep Batch(es): V16828 03/31/22 10:00
Prep Method: 625.1 (Prep)
Test Results Units MOL DF Date/Time By Analytical
Analyzed Batch
Dibenz(a,h)anthracene <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
Dibenzofuran <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
1,2-Dichlorobenzene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
1,3-Dichlorobenzene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
1,4-Dichlorobenzene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
3,3'-Dichlorobenzidine <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
2,4-Dichlorophenol <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Diethyl phthalate <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
Dimethyl phthalate <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
2,4-Dimethylphenol <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
Di-n-butyl phthalate <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
4,6-Dinitro-2-methylphenol <30.0 pg/L 30.0 1 03/31/22 23:23 JMV V17044
2,4-Dinitrophenol <30.0 pg/L 30.0 1 03/31/22 23:23 JMV V17044
2,4-Dinitrotoluene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
2,6-Dinitrotoluene <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
Di-n-Octyl Phthalate <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Fluoranthene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Fluorene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Hexachlorobenzene <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
Hexachlorobutadiene <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
Hexachlorocyclopentadiene <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
Hexachloroethane <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions MQL Method Quantitation Limit

Waoint, 449 Springbrook Rd, Charlotte, NC 28217
yp Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 04/11/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :03/24/2022
Indian Trail , NC 28079
Report Number :22-083-0042 REPORT OF ANALYSIS
Lab No : 96879 Matrix: Aqueous
Sample ID :Influent Sampled: 3/24/2022 13:15
Analytical Method: 625.1 Prep Batch(es): V16828 03/31/22 10:00
Prep Method: 625.1 (Prep)
Test Results Units MOL DF Date/Time By Analytical
Analyzed Batch
Indeno(1,2,3-cd)pyrene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Isophorone <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
1-Methylnaphthalene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
2-Methylnaphthalene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Naphthalene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Nitrobenzene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
2-Nitrophenol <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
4-Nitrophenol <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
N-Nitrosodiphenylamine <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
N-Nitroso-di-n-propylamine <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
Pentachlorophenol <50.0 pg/L 50.0 1 03/31/22 23:23 JMV V17044
Phenanthrene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Phenol <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
Pyrene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
1 1,2,4-Trichlorobenzene <10.0 pg/L 10.0 1 03/31/22 23:23 JMV V17044
2,4,6-Trichlorophenol <20.0 pg/L 20.0 1 03/31/22 23:23 JMV V17044
Surrogate: Phenol-d5 26.3 Limits: 10-63% 1 03/31/22 23:23 JMV 625.1
Surrogate: 2-Fluorobiphenyl 70.6 Limits: 49-118% 1 03/31/22 23:23 JMV V17044
Surrogate: 2-Fluorophenol 39.8 Limits: 22-84% 1 03/31/22 23:23 JMV V17044
Surrogate: Nitrobenzene-d5 64.0 Limits: 43-123% 1 03/31/22 23:23 JMV V17044
Surrogate:4-Terphenyl-d14 83.4 Limits: 49-151% 1 03/31/22 23:23 JMV V17044
22 23:23 JMV V17044
Limits: 31-144% 1 03 31
Surrogate: 2,4,6-Tribromophenol 80.6 / /
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions MQL Method Quantitation Limit

Waypoint, 449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 04/11/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 03/24/2022
Indian Trail , NC 28079
Report Number:22-083-0042 REPORT OF ANALYSIS
Lab No : 96880 Matrix: Aqueous
Sample ID :Influent -8270 PAH Sampled: 3/24/2022 13:15
Analytical Method: 8270E Prep Batch(es): V16827 03/31/22 10:00
Prep Method: 3510C
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <20.0 Ng/L 20.0 1 03/31/22 22:38 JMV V16992
Acenaphthylene <20.0 pg/L 20.0 1 03/31/22 22:38 JMV V16992
Anthracene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Benzo(a)anthracene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Benzo(a)pyrene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Benzo(b)fluoranthene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Benzo(g,h,i)perylene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Benzo(k)fluoranthene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Chrysene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Dibenz(a,h)anthracene <20.0 pg/L 20.0 1 03/31/22 22:38 JMV V16992
Fluoranthene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Fluorene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Indeno(1,2,3-cd)pyrene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
1-Methylnaphthalene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
2-Methylnaphthalene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Naphthalene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Phenanthrene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Pyrene <10.0 pg/L 10.0 1 03/31/22 22:38 JMV V16992
Surrogate: 2-Fluorobiphenyl 42.4 * Limits: 44-119% 1 03/31/22 22:38 JMV V16992
Surrogate: Nitrobenzene-d5 55.6 Limits: 44-120% 1 03/31/22 22:38 JMV V16992
Surrogate:4-Terphenyl-d14 70.8 Limits: 50-134% 1 03/31/22 22:38 JMV V16992
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions MQL Method Quantitation Limit

star momenta Ina. CEd, 977.6E+42 .1704 864 877.6930
P.O. Do; 1E414. GreenvIle, SC 29606 4 Craftsman Crum, Greer, SC 296.50
Pimephales promelas 24 Hour Acute Pass/Fail Test
EPA-821-R-02-012 Method 2000
Client: HERIC SOLUTIONS
Facility:PECAN AVE
NPDES#:NC0089958
Test Date: 25-Mar-22
Laboratory ID#: T61543
Test Reviewed and Approved By:
P
Robert W.Kelley,Ph.D. Patrick D.Timms
President QA/QC Officer
gQ ht411
..
Certification#E87819 SCDHEC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.included results pertain only to provided s les. NCDENR Certification# 022
Page 1 of 4

Effluent Aquatic Toxicity Report Form -Acute Pass/Fail Date: 04/01/22
Facility HERIC SOLUTIONS-PECAN AVE NPDES# NC0089958 Pipe# 001 County Mecklenburg •
Laboratory Performing Test ETT Environmental
X Comments
Signature of Operator in Responsible Charge ti4/4 t P.
X
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Div. of Water Quality
N.C.DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
North Carolina Acute Pass/Fail Toxicity Test
Collection Date: 3/24/22 Organism Tested:
Collection Time: 1310 Pimephales promelas
Test Start Date: 3/25/22
Sample Tyne/Duration Control 7.7 7.3
Grab Comp Duration pH Treatment 7.4 7.1
X -_
--_ Control Sample start end
Hardness(mg/L) 81.6 Control 8.0 7.0
Spec.Cond. (Nmhos) 311 170 D.O. Treatment 8.0 7.1
Chlorine(mg/L) <0.05
Sample temp.at receipt 3.4
Mortality Replicate Mean Mortality
Treatment 1 (Control) A B C D
0% 0% 0% 0% 0%
Treatment 2(Exposure) A B C D
Concentration 90% 0% 0% 0% 0% 0%
Tested
(NOTE): If mean control mortality exceeds 10%,the test is considered invalid)
Calculate using
Arc-Sine Calculated Student's t N/A PASS X
transformed
SquareRoot
Tabular Student's t 1.94 FAIL
data (ONE TAILED)
If the absolute value of the calculated t is less than or equal
to the absolute value of the tabular t, check PASS
If the absolute value of the calculated t is greater than the
absolute value of the tabular t, check FAIL.
If all vessels within each treatment have the same response
but the treatment two response is greater than the control, check FAIL.
DEM form AT-2(8/91)
Page 2 of 4

24 Hour Acute Toxicity Test
Test Method.EPA 821 R-02-012; Method 2000 Pimephales promelas
Client: HERIC SOLUTIONS Sample ID:PECAN AVE Lab 1D#: T61543
Start Date: 03/25/22 Time: 03:10 PM Set By: JZ
End Date: 03/26/22 Time: 03:42 PM Ended By: AM
Test Vessel Test Solution Volume Incubator Transfer Volume Dilution Water
Fathead Minnows 500 mL plastic cup 200 mL #1 0.5 mL MHSF
Randomization pattern per SOP !Neonates from common holding vessel 'Light: 50-100 ft-c. 16 hr light/8 hr dark
TEST ORGANISMS
for Ceriodaphnia dubia Comments:
Date Removed: Between: and:
Pimephales promelas Source: ABS lays old: 8
Mysidopsis bahia Source: Days old: ABS HACHED 3/17/22 1500-1630
Test Organisms Pre Fed by: JZ Time: 12:30 PM
MORTALITY DATA
Conc. [niriaik Cumulative Mortality Final initial Final
Cond/ Cond/
Rep. ureanisms as nr ax nr n n: as hr Marmn> Temp D O pH Salini By Temp D O pH Salini By
A 10 0
Control B 10 0
C 10 0
D 10 0 0% 24.6 8.0 7.7 JL 25.5 7.0 7.3 1 AM
A 10 0 '
90.0% B 10 0
C 10 0 Ave: �
D 10 0 0% 24.6 8.0 7.4 JL 25.5 7.1 7.1 AM
A
B
C
D
A
B
C
D I
A
B
c
D I
A
B ar a rl+-
C
D
A
B
C
D °C mg/L I I PPT I °C I mg/L I I PPT
Page 3 of 4

•
{ ` =., 111111111111111CCIIIII1IIflIII�IiIII111111N1 111111111I�IIII� 22 83-0042
4. wt
- 1F• Heric Solutions,LLC I 0 242022
Monthly 15:28:14
.-_.-z-L- e5 4 -- -,- .-' ,
PO Box 16414,Greenville,SC 29606-7414I
[phone], [phone] Faa(864)877 6938
Shipping Address:4 Craftsman Ct,Greer,SC 29650
VV WW_cTTEN V I RONM ENTAL.COM
Client: _ _jxe2
,Y,4 ,,nn,-, , Program Containers Preservative! Pa rametets
',Facility:
\`
•State:
NPDES hole LrlucntToxicity c^
- Acute Chronic Test Organisms r•,
I
i _ ^ti
-
n
C.) (Composite only) (Grab or Composite) < o _ O F U ES . ^
cp
U t o a 1=1-0504 s - "' ^ -
1 = • Sign,and Print below 3 - a =HCL G s
cS the dotted line _ _ E C u o a=moo `-' " 's
SAMPLE ID ii Composite Start D°tc Time Sample C°ticd°n Dnk Time Collected by U c to Z o R• p a=2nAc o o; -. %. tI _t —
/\)) 6=Oher <1J U U 2 n Ji_ y Chemie=_I n=_t}si=?Other
Jo
,D
to
0
A
O
A .
•
i
S.pecinl 1nSIII]clions .v.,... _ " —.,_ -,-_. - —-- __-- —---'--—— —_.M.r....�.._.._.._a�.._�.. _ ._._....-_
•
Sample Custody Transfer Record Secure Receipt Sample
• Date Time elinquished By/Organization Receiv ±By/- e,;iza'son Area Temp`C Preserved?2zz wr �
' - ii7 i/
i
COMPOSITE SAMPLING PROCEDURES TEMPERATURE ilIO.NITOIl_UArG PROCEDURES HOLD±Tlove_P^ D -
CC=D�r=
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity resting the 5am7,pU:aus first be used.,:.ithi- 'lone s
Time Proportional:1 sample each hour for 24 hours.Equal volut 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bas. _of sarnrtle collection co-to?•e:c,;.cr"_; o;i:-57-5;1._.
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 7 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit_

• 1
Waypoint . 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:00004
Customer Name: Heric Solutions, LLC
Report Number: 22-083-0042
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: IIRT-15 4.1C
Shipping container/cooler uncompromised? 0 Yes 0 No
Number of coolers/boxes received r 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody (COC) present? 0 Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? 0 Yes 0 No
Sample containers intact? 0 Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No 0 N/A
Water- VOA vials free of headspace 0 Yes 0 No 0 N/A
Trip Blanks received with VOAs 0 Yes 0 No 0 N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A
r High concentration container (48 hr) r Low concentration EnCore samplers (48 hr)
7 High concentration pre-weighed (methanol -14 d) r Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Sarah J. Locklear Date &Time: 03/24/2022 15:29:43

gqp I � 22 2 CH IN OF CUSTODY RECORD LAB
1111Itt� 11 03-24-2Q22 PAaE__- _-- Q M TO ENSURE PROPER BILLING:_ YES NO N/A
Hens Solutions.LLC 15'28.14 ` Samples INTACT upon arrival? ____
Monthly Project Name:_ Received IN ICE?
Short Hold Analysis (Yes) (No) UST Project: (Yes) (No) i PROPER PRESERVATIVES indicated? .""'.'
*Please ATTACH any project specific reporting(QC LEVEL I it III IV) Received WITHIN HOLDING TIMES? .r'� _____
a,nes+l►‘,.v+nNa+ry rvame: vow sr '"+y'" provisions and/or QC Requirements CUSTODY SEALS INTACT? ___ * '
Report To/Contact Name: invoice To: VOLATILES reed W/OUT HEADSPACE? r.
Reporting Address: . .. Address: PROPER CONTAINERS used?
TEMP: Therm(D:VeN-VS Observedlli "C!Corr. I., i `C
Phone: _Fax(Yes)(No): Purchase Order No./Billing Reference TO SE FILLEDIN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date J 1 Day J 2 Days J 3 Days J 4 Days J 5 Days Certification: NC SC
EDD Type: PDF Excel Other "Working Days" J 6.9 Days .J Standard 10 days J OtireshApWorkveMiust Be Other_. NIA______
Site Location Name: Samples received after 15:00 will be processed next business day,
Site Location Physical Address: Turnaround time is based on business days,excluding weekends and holidays. Water Chlorinated: YES ___,._...._NO
(SEE REVERSE FOR TERMS&CONDITIONS REGARDING SERVICES
_. RENDERED BY WAYPOINT ANALYTICAL,LLC TO CLIENT) Samples Iced Upon Collection: YES NO
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
CLIENT DATE COLLECTED (SOIL, t - PRESERVA- n
SAMPLE DESCRIPTION COLLECTED MILITARY WATER,OR "TYPE NO. SIZE TIVES 'V n A} (ti / �ifi REMARKS ID NO.
HOURS SLUDGE) SEE BELOW ki �A f
4.
I AIP _3 13� ' . ID> �V4/r- Y.
C- . , ludo roe.
cG' . 1 L1' tcL .
__.___..i J f li o f I 2i- )1 I X
.,,,
. ,
1 2 f
3 Lv EEL
' 4, // ,
PRESS DOWN FIRMLY-2 COPIES
_
j�
Sampler's Signature �... . Sampled By(Print Name) ( 1 k) /��i. j1hEV '1. Affiliation
LAD UsE onit v
Upon relinquishing,this Chain of Cus ody is your authorization for Waypoint Analytical to proceed with the analyses as requested above, nA y changesr must be I Site Arrival Time:
I sub r.tted in writing to the Waypoint Analytical Project Manager.There will be charges for any changes after analyses have been initialized.
Reh 410
8y( ) 2`r / , `y Received By:(Signature) .— Date Miktary/Hows Additional Comments: 'Site Departure Time:
r_L f7s Gr/
Rehnq... _. y:(Sg re)- Received By:(Sgnature) Date 1 Field Tech Fee:
Rehngiushed By.(Signature) y .. y y r� ( t/ I Mileage:
Method of Shipment NOTE:ALL SAMPLE COOLERS SHOULD BE TAPED SHUT I OR TRANSPORTATION TO THE LABORATORY. Group No.
SAMPLES ARE NOT EPTED AND VERIFIED AGAINS L EIVED AT THE LABORATORY.
SEE REVERSE FOR
J Fed Ex :J UPS J Hand-delivered point Ana+ytical Field Service Other__-_, ___._..._._—. _, .._.___.__P TERMS&CONDITIONS
NPDES: UST: G NDWATER: DRINKING WATER: SOLID WASTE: RCRA: BRWNFLD LANDFILL OTHER:
C]NC La SC U NC LI SC U NC J SC .J NC _I SC 3 NC U SC CI NC U SC ;:]NC J SC O NC O SC U NC U SC
J ❑ U U CI c a fl ORIGINAL
•n..ar•,air.•.trra one wrinre•_ . _ . r—P. --- w. -- V. n..._a._. ♦. —.._a_ . .. .. .. •.... -..�.._au�....__. . . _•..._._...__••_--w__._.

111II11111111111111111111111111111II 02 242 D
--- tit�;ntniV 15 28:14
,A Page of
[phone], [phone] F .:(884)87?893E
Snipping Address:4 Craftsman Ct,Greer,SC 24850
w WW.CTYCNVIMCN.a.-r*L.CD 4
Client: -
/ Program Containers Preservative` Parameters
Faculty:
Whole Effluent Tosteih
State: NPDES#t .acute Chronic Tess Oroonisms
"Cp j J
oc L .. '
a (Composi:e nn.+y) (Grab or Composite) < • L? c ^
a c `a ` - ._ t6H;SOJ = is I. ~� *� u tc
Sign,and Print belcti'' u o Hot g u o — :n a - =1
tC the dotted line K U a OH _ `o .` a` y —
w N 2 2 ^ , g
_ c p t v G 3 ° yr Y :s , `^,1.. u
u a�Zou u v r. `- — 3 g Chemical
� 'Q `o c � o "
SAMPLE Composite Sun Date Time Sample Coikctian Dale Tittle Collected by U Lq u1 .2 a's=`�7 6.0 <1 C UT�} V L� L'+ ,r] �, L i Analysis 8 Outer
I I
-F ' lrr.,/04‹,i 1 X l x Nd/4 I _ m
i
1
Special instructioas;
1-
i
Sample Custody Transfer Record Secure Receipt Sample
Date Time '.elinquishedByIOrrnation Reeeiy .By'ter' on Area Temp°C i Preserved?
— --Ted.,—2X21 i/47141( t "A._ fa
/r � 7
� 1
COMPOSITE SAMPLING PROCEDURES 7Ed-IPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must he between For toxicity testing the sample must 5rst be used within 36 hours
Time Proportional:I sample each hour for 24 hours.Equal volur 0.0 and 6-0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
for at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours sam
ple mple collection.
Flow Proportional:As per instructions in NPDES permit.

DISCHARGE MONITORING REPORTS AND EFFLUENT ANALYTICAL REPORTS
APRIL 2022

NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1.0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-I COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-1 ORC HAS CHANGED:No
eDMR PERIOD:04-2022(April 2022) VERSION:1.0 STATUS:Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
50050 00400 01002 01007 76028 34030 01027 32106 C0034
E E e
F F
O s
a
E r Continuous Monthly 2 X month 2 X month Monthly 2 X month 2 X month Monthly 2 X month
E < F 1'
u a a O e. Recorder Grab Grab Grab Grab Grab Grab Grab Grab
ca u a
c V F O O ce
O z. FLOW pH As-TOTAL BARIUM SEMI-VOL BENZENE CADMIUM CHLRFORM TOT CRCONC
2400 dock Hrs +2400 dock Hrs Y/B/N mgd su ug/1 ugll ugh ugh ug/I ug/I ug/I
I 0.031
2 0.031 .
3 0.031
4 915 10 1' 0.031
5 0.031
6 0935 0 0.031 6.15 - 1 5 <50 <0.5 I <1 2.15
7 1100 10 Y 0.031
8 0.031
9 0.031
Io 0.031
I I 0.031
12 0.031
13 0.031
14 715 6.5 Y 0.03
15 0.03
16 0.03
17 0.03
18 0.03
19 915 1.0 V 0.029
20 0.029
21 1420 0 0.029 <I <0.5 ' I 1.96
22 0.029
23 0.029
, 0.029
-- 900 1.0 Y 0.026
2e 930 10 Y 0.024
27 0.024
28 0.024
29 0.024
311 0.024
4.
Monthly Average Limit
Monthly Average: 0.0291 0 2.785 0 0 0 0 2.055
1
Daily Maximum: 0.031 6.15 0 5.57 0 0 0 0 2.15
Daily Minimum: 0.024 6.I5 0 0 0 0 0 0 1.96
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday
Discharge Monitoring Report-Copy Of Record(COR_NC0089958_Ver_1.0_4_2022.pd0

NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1.0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-1 COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-1 ORC HAS CHANGED:No
eDMR PERIOD:04-2022(April 2022) VERSION: 1.0 STATUS:Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
01042 34371 00900 01051 COMER 01067 76029 TGE6C C0456 01147 34010
R. E E
F h . n
O
E 2 X month 2 X month Monthly 2 X month 2 X month 2 X month Monthly Monthly 2 X month 2 X month 2 X month
I 17'
u - i O 'e. Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab
E w t d u a
c V [- O O at
O Z. COPPER ETHYLBEN TOT HARD LEAD MERCURY- NICKEL VOLATILE FTHD24PF PAH-CO Se-TOTAL TOLUENE
2400 clock Hrs 2400 clock Hrs YAWN ugh ug/I mg/I mg/I ug/I ug/1 ug/1 pass/fail ug/I ug/I ug/I
1
2
3
4 915 1.0 Y
5
6 0935 0 <2 <1 26 <I <0.0002 <5 1.7 100 <20 <5 <I
7 1100 1.0 Y
0
9
10
11
12
13
14 715 63 Y
15
16
17
10
19 915 I 0 Y
20
21 1420 0 <2 <I <I <0.0002 <5 <20.4 -5 <I
23
24
25 900 1 0 Y
26 930 1.0 5'
27
20
29
30
Monthly Average Limit:
Monthly Average: 0 0 26 0 0 0 1.7 100 0 0 0
Daily Maximum: 0 0 26 0 0 0 1.7 100 0 0 0
Daily Minimum: 0 0 26 0 0 0 1.7 100 0 0 0
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday
Discharge Monitoring Report-Copy Of Record(COR NC0089958_Ver 1.0_4_2022.pdf)

NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1.0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-1 COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-I ORC HAS CHANGED:No
eDMR PERIOD:04-2022(April 2022) VERSION:1.0 STATUS:Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
81551 01092
E E
F O
E — C
E 2 X month 2 X month
E I t
U O c Grab Grab
B w 0 0 C
G U F O O O 7.
XYLENE ZINC
2400 clock Hrs 2400 clock Hrs Y/B/N ughl ugh!
1
2
3
4 915 1.0 Y
5
6 0935 0 <1 <10
7 1100 1.0 Y
8
9
10
11
12
13
14 715 6.5 Y
15
16
17
18
19 915 1.0 Y
20
21 1420 0 <1 <10
22
23
24
25 900 1.0 Y
26 930 1.0 Y
27
28
I 29
30
:Monthly Average Limit:
Monthly Average: 0 0
Daily Maximum: 0 0
Daily Minimum: 0 0
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday
Discharge Monitoring Report-Copy Of Record(COR_NC0089958_Ver l.0_4_2022.pdf)

NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1.0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-1 COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-I ORC HAS CHANGED:No
eDMR PERIOD:04-2022(April 2022) VERSION: 1.0 STATUS:Submitted
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:05/09/2022
Electronically Certified by Eric Christian Donnelly on 2022-05-09 20:34:02.404
ORC/Certifier Signature: Eric Christian Donnelly Phone # : [phone] Date
I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Anyinformation shall beprovided orallywithin 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.The written submission shall be made as required by part II.E.6 of the
NPDES permit.
Electronically Signed by Eric Christian Donnelly on 2022-05-09 20:34:56.841
Permittee/Submitter Signature: ***Eric Christian Donnelly Phone #:[phone] Date
Permittee Address:201 S College St Ste 1300 Charlotte NC 28244 Permit Expiration Date: 11/30/2026
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:Waypoint Analytical
CERTIFIED LAB#:402
PERSON(s)COLLECTING SAMPLES:David Morris
PARAMETER CODES
Parameter Code assistance may be obtained by visiting https://deq.nc.gov/about/divisions/water-resources/edmr/user-documentation.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:YES indicates that No Flow/Discharge occurred and,as a result,no data is reported for any parameter on the DMR for the
entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).
Discharge Monitoring Report-Copy Of Record(COR_NC0089958_Ver_1.0_4_2022.pdf)

•
Waypoint 449 Springbrook Rd,Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
4/20/2022
Heric Solutions, LLC
Eric Donnelly
P.O. Box 548
Indian Trail, NC, 28079
Ref: Analytical Testing
Lab Report Number: 22-096-0036
Client Project Description: Monthly
1111 Pecan Ave.
Project Number: Permit NC0089958
Dear Eric Donnelly:
Waypoint Analytical, LLC (Charlotte) received samples) on 4/6/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
withthe applicable
accordance pp analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

• w
Waypoint ry 449 Springbrook Rd, Charlotte,NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytfcal.com
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
North Carolina State Program 37735 07/31/2022
North Carolina State Program 402 12/31/2022
South Carolina State Program 99012 07/31/2022
South Carolina State Program 99012 12/31/2022
Page 1 of 1 00016/22-096-0036

w
Itaypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-096-0036
Client Project Description: Monthly
1111 Pecan Ave.
Lab No Client Sample ID Matrix Date Collected Date Received
97857 EFF Aqueous 04/06/2022 09:35 04/06/2022 16:30
97858 EFF-8270 PAHs Aqueous 04/06/2022 09:35 04/06/2022 16:30

o
VVáypOi nt.. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 04/20/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :04/06/2022
Indian Trail , NC 28079
Report Number:22-096-0036 REPORT OF ANALYSIS
Lab No : 97857 Matrix: Aqueous
Sample ID :EFF Sampled: 4/6/2022 9:35
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Hardness 26.0 mg/L 5.00 1 04/13/22 12:05 CLB 2340C-2011
pH 6.15 s.u. 1 04/06/22 09:55 FLD FIELD
Temperature 20.1 C 0.1 1 04/06/22 09:55 FLD FIELD
Arsenic <1.00 pg/L 1.00 1 04/11/22 17:29 EDV 200.8
Barium <5.00 pg/L 5.00 1 04/11/22 17:29 EDV 200.8
Cadmium <1.00 pg/L 1.00 1 04/11/22 17:29 EDV 200.8
Chromium 2.15 u9/L 1.00 1 04/11/22 17:29 EDV 200.8
Copper <2.00 pg/L 2.00 1 04/11/22 17:29 EDV 200.8
Lead <1.00 pg/L 1.00 1 04/11/22 17:29 EDV 200.8
Mercury(Total) <0.000200 mg/L 0.000200 1 04/08/22 16:12 EDV 245.1
Nickel <5.00 pg/L 5.00 1 04/11/22 17:29 EDV 200.8
Selenium <5.00 pg/L 5.00 1 04/11/22 17:29 EDV 200.8
Zinc <10.0 pg/L 10.0 1 04/11/22 17:29 EDV 200.8
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions M Minimum value MQL Method Quantitation Limit

•
Waypoi ■t, 449 Springbrook Rd,Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 04/20/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :04/06/2022
Indian Trail , NC 28079
Report Number
:22-096-0036 REPORT OFANALYSIS'
Lab No : 97857 Matrix: Aqueous
Sample ID : EFF Sampled: 4/6/2022 9:35
Analytical Method: 624.1 Prep Batch(es): V17691 04/19/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acetone <5.00 pg/L 5.00 1 04/19/22 14:56 JLB V17692
Acrolein <5.00 pg/L 5.00 1 04/19/22 14:56 JLB V17692
Acrylonitrile <5.00 pg/L 5.00 1 04/19/22 14:56 JLB V17692
Benzene <0.500 pg/L 0.500 1 04/19/22 14:56 JLB V17692
Bromodichloromethane <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
Bromoform <3.00 pg/L 3.00 1 04/19/22 14:56 JLB V17692
Bromomethane <2.00 pg/L 2.00 1 04/19/22 14:56 JLB V17692
Carbon Tetrachloride <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
Chlorobenzene <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
Chlorodibromomethane <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
Chloroethane <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
2-Chloroethylvinyl Ether <10.0 pg/L 10.0 1 04/19/22 14:56 JLB V17692
Chloroform <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
Chloromethane <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
1,2-Dichlorobenzene <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
1,3-Dichlorobenzene <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
1,4-Dichlorobenzene <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
1,1-Dichloroethane <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
1,2-Dichloroethane 1.70 pg/L 1.00 1 04/19/22 14:56 JLB V17692
1,1-Dichloroethene <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
trans-1,2-Dichloroethene <2.00 pg/L 2.00 1 04/19/22 14:56 JLB V17692
pg/L 1 2-Dichloro ro ane <1.001.001 04/19/22 14:56 JLB V17692
p p
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions M Minimum value MQL Method Quantitation Limit

r
Q
WaYP0Irlt k Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 04/20/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :04/06/2022
Indian Trail , NC 28079
Report Number:22-096-0036 REPORT OF ANALYSIS
Lab No : 97857 Matrix: Aqueous
Sample ID :EFF Sampled: 4/6/2022 9:35
Analytical Method: 624.1 Prep Batch(es): V17691 04/19/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
1 cis-1,3-Dichloropropene <1.00 Ug/L 1.00 1 04/19/22 14:56 JLB V17692
trans-1,3-Dichloropropene <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
Ethylbenzene <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
Methylene Chloride <2.00 pg/L 2.00 1 04/19/22 14:56 JLB V17692
1,1,2,2-Tetrachloroethane <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
Tetrachloroethene <0.750 ug/L 0.750 1 04/19/22 14:56 JLB V17692
Toluene <1.00 lJg/L 1.00 1 04/19/22 14:56 JLB V17692
1,1,1-Trichloroethane <1.00 ug/L 1.00 1 04/19/22 14:56 JLB V17692
1,1,2-Trichloroethane <0.500 pg/L 0.500 1 04/19/22 14:56 JLB V17692
Trichloroethene <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
Trichlorofluoromethane <1.00 Ng/L 1.00 1 04/19/22 14:56 JLB V17692
1,2,3-Trichloropropane <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
1,2,4-Trimethylbenzene <0.500 pg/L 0.500 1 04/19/22 14:56 JLB V17692
Vinyl Chloride <1.00 pg/L 1.00 1 04/19/22 14:56 JLB V17692
o-Xylene <1.00 lg/L 1.00 1 04/19/22 14:56 JLB V17692
m,p-Xylene <2.00 ug/L 2.00 1 04/19/22 14:56 JLB V17692
Xylene(Total) <1.00 pg/L 1.00 1 04/19/22 14:56 V17692
Surrogate:4-Bromofluorobenzene 97.0 Limits: 74-126% 1 04/19/22 14:56 JLB V17692
Surrogate: Dibromofluoromethane 95.8 Limits: 75-127% 1 04/19/22 14:56 JLB V17692
Surrogate: 1,2-Dichloroethane-d4 85.4 Limits: 67-136% 1 04/19/22 14:56 JLB V17692
Surrogate:Toluene-d8 92.0 Limits: 70-130% 1 04/19/22 14:56 JLB V17692
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions M Minimum value MQL Method Quantitation Limit

r
1
Wa41pOiflt 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 04/20/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :04/06/2022
Indian Trail , NC 28079
Report Number :22-096-0036 REPORT OF ANALYSIS
Lab No : 97857 Matrix: Aqueous
Sample ID : EFF Sampled: 4/6/2022 9:35
Analytical Method: 625.1 Prep Batch(es): V17317 04/12/22 01:00
Prep Method: 625.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Acenaphthylene <20.0 pg/L 20.0 1 04/13/22 04:49 ANG V17450
Anthracene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Benzidine <10.0 ug/L 10.0 1 04/13/22 04:49 ANG V17450
Benzo(a)anthracene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Benzo(a)pyrene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Benzo(b)fluoranthene <10.0 IJg/L 10.0 1 04/13/22 04:49 ANG V17450
Benzo(g,h,i)perylene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Benzo(k)fluoranthene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Benzoic Acid <50.0 M pg/L 50.0 1 04/13/22 04:49 ANG V17450
Benzyl alcohol <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Bis(2-Chloroethoxy)methane <10.0 ug/L 10.0 1 04/13/22 04:49 ANG V17450
Bis(2-Chloroethyl)ether <10.0 ug/L 10.0 1 04/13/22 04:49 ANG V17450
Bis(2-Chloroisopropyl)ether <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Bis(2-ethylhexyl)phthalate <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
4-Bromophenyl phenyl ether <20.0 pg/L 20.0 1 04/13/22 04:49 ANG V17450
Butyl benzyl phthalate <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
4-Chloro-3-methylphenol <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
2-Chloronaphthalene <20.0 ug/L 20.0 1 04/13/22 04:49 ANG V17450
2-Chlorophenol <10.0 ug/L 10.0 1 04/13/22 04:49 ANG V17450
4-Chlorophenyl phenyl ether <20.0 pg/L 20.0 1 04/13/22 04:49 ANG V17450
Chrysene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions M Minimum value MQL Method Quantitation Limit

7
Waypoint
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 04/20/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 04/06/2022
Indian Trail , NC 28079
Report Number:22-096-0036 REPORT OF ANALYSIS
Lab No : 97857 Matrix: Aqueous
Sample ID : EFF Sampled: 4/6/2022 9:35
Analytical Method: 625.1 Prep Batch(es): V17317 04/12/22 01:00
Prep Method: 625.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Dibenz(a,h)anthracene <20.0 pg/L 20.0 1 04/13/22 04:49 ANG V17450
Dibenzofuran <20.0 ug/L 20.0 1 04/13/22 04:49 ANG V17450
1,2-Dichlorobenzene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
1,3-Dichlorobenzene <10.0 ug/L 10.0 1 04/13/22 04:49 ANG V17450
1,4-Dichlorobenzene <10.0 ug/L 10.0 1 04/13/22 04:49 ANG V17450
3,3'-Dichlorobenzidine <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
2,4-Dichlorophenol <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Diethyl phthalate <20.0 pg/L 20.0 1 04/13/22 04:49 ANG V17450
Dimethyl phthalate <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
2,4-Dimethylphenol <20.0 pg/L 20.0 1 04/13/22 04:49 ANG V17450
Di-n-butyl phthalate <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
4,6-Dinitro-2-methylphenol <30.0 pg/L 30.0 1 04/13/22 04:49 ANG V17450
2,4-Dinitrophenol <30.0 pg/L 30.0 1 04/13/22 04:49 ANG V17450
2,4-Dinitrotoluene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
2,6-Dinitrotoluene <20.0 pg/L 20.0 1 04/13/22 04:49 ANG V17450
Di-n-Octyl Phthalate <10.0 ug/L 10.0 1 04/13/22 04:49 ANG V17450
Fluoranthene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Fluorene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Hexachlorobenzene <20.0 ug/L 20.0 1 04/13/22 04:49 ANG V17450
Hexachlorobutadiene <20.0 pg/L 20.0 1 04/13/22 04:49 ANG V17450
Hexachlorocyclopentadiene <20.0 pg/L 20.0 1 04/13/22 04:49 ANG V17450
Hexachloroethane <10.0 M pg/L 10.0 1 04/13/22 04:49 ANG V17450 1
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions M Minimum value MQL Method Quantitation Limit

1
1
V*/apoint 9 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 04/20/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 04/06/2022
Indian Trail , NC 28079
Report Number:22-096-0036 REPORT OF ANALYSIS
Lab No : 97857 Matrix: Aqueous
Sample ID : EFF Sampled: 4/6/2022 9:35
Analytical Method: 625.1 Prep Batch(es): V17317 04/12/22 01:00
Prep Method: 625.1 (Prep)
Test Results Units MOL DF Date/Time By Analytical
Analyzed Batch
Indeno(1,2,3-cd)pyrene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Isophorone <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
1-Methylnaphthalene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
2-Methylnaphthalene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Naphthalene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Nitrobenzene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
2-Nitrophenol <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
4-Nitrophenol <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
N-Nitrosodiphenylamine <20.0 pg/L 20.0 1 04/13/22 04:49 ANG V17450
N-Nitroso-di-n-propylamine <20.0 pg/L 20.0 1 04/13/22 04:49 ANG V17450
Pentachlorophenol <50.0 pg/L 50.0 1 04/13/22 04:49 ANG V17450
Phenanthrene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Phenol <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
Pyrene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
1,2,4-Trichlorobenzene <10.0 pg/L 10.0 1 04/13/22 04:49 ANG V17450
2,4,6-Trichlorophenol <20.0 pg/L 20.0 1 04/13/22 04:49 ANG V17450
Surrogate: Phenol-d5 24.8 Limits: 10-63% 1 04/13/22 04:49 ANG 625.1
Surrogate: 2-Fluorobiphenyl 63.2 Limits:49-118% 1 04/13/22 04:49 ANG V17450
Surrogate: 2-Fluorophenol 40.4 Limits: 22-84% 1 04/13/22 04:49 ANG V17450
Surrogate: Nitrobenzene-d5 59.0 Limits:43-123% 1 04/13/22 04:49 ANG V17450 1
Surrogate:4-Terphenyl-d14 83.2 Limits:49-151% 1 04/13/22 04:49 ANG V17450
Surrogate: 2,4,6-Tribromophenol 72.3 Limits: 31-144% 1 04/13/22 04:49 ANG V17450
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions M Minimum value MQL Method Quantitation Limit

O
•
Vaypoi nt 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 04/20/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :04/06/2022
Indian Trail , NC 28079
Report Number:22-096-0036 REPORT OF ANALYSIS
Lab No : 97858 Matrix: Aqueous
Sample ID :EFF-8270 PAHs Sampled: 4/6/2022 9:35
Analytical Method: 8270E Prep Batch(es): V17385 04/13/22 09:15
Prep Method: 3510C
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <20.0 pg/L 20.0 1 04/13/22 18:33 ANG V17472
Acenaphthylene <20.0 pg/L 20.0 1 04/13/22 18:33 ANG V17472
Anthracene <10.0 ug/L 10.0 1 04/13/22 18:33 ANG V17472
Benzo(a)anthracene <10.0 ug/L 10.0 1 04/13/22 18:33 ANG V17472
Benzo(a)pyrene <10.0 ug/L 10.0 1 04/13/22 18:33 ANG V17472
Benzo(b)fluoranthene <10.0 pg/L 10.0 1 04/13/22 18:33 ANG V17472
Benzo(g,h,i)perylene <10.0 pg/L 10.0 1 04/13/22 18:33 ANG V17472
Benzo(k)fluoranthene <10.0 Ng/L 10.0 1 04/13/22 18:33 ANG V17472
Chrysene <10.0 pg/L 10.0 1 04/13/22 18:33 ANG V17472
Dibenz(a,h)anthracene <20.0 pg/L 20.0 1 04/13/22 18:33 ANG V17472
Fluoranthene <10.0 Ng/L 10.0 1 04/13/22 18:33 ANG V17472
Fluorene <10.0 pg/L 10.0 1 04/13/22 18:33 ANG V17472
Indeno(1,2,3-cd)pyrene <10.0 pg/L 10.0 1 04/13/22 18:33 ANG V17472
1-Methylnaphthalene <10.0 ug/L 10.0 1 04/13/22 18:33 ANG V17472
2-Methylnaphthalene <10.0 pg/L 10.0 1 04/13/22 18:33 ANG V17472
Naphthalene <10.0 Vg/L 10.0 1 04/13/22 18:33 ANG V17472
Phenanthrene <10.0 ug/L 10.0 1 04/13/22 18:33 ANG V17472
Pyrene <10.0 pg/L 10.0 1 04/13/22 18:33 ANG V17472
Surrogate: 2-Fluorobiphenyl 36.0 * Limits: 44-119% 1 04/13/22 18:33 ANG V17472
Surrogate: Nitrobenzene-d5 44.2 Limits: 44-120% 1 04/13/22 18:33 ANG V17472
Surrogate:4-Terphenyl-d14 77.8 Limits: 50-134% 1 04/13/22 18:33 ANG V17472
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions
M Minimum value MQL Method Quantitation Limit

t '1% 1
cm momenta,Inc. (C64)077-&'42 . 064)877.6930
P.O. Box 16414, Greenv lie. SC 29606 4 Craftsman Cunt, Grier, SC 29650
Pimephales promelas 24 Hour Acute Pass/Fail Test
EPA-821-R-02-012 Method 2000
Client: HERIC SOLUTIONS
Facility: PECAN AVE
NPDES#:NC0089958
Test Date: 07-Apr-22
Laboratory ID#: T61674
Test Reviewed and Approved By:
4 r aL It
Robert W.Kelley,Ph.D. Patrick D.Timms
President QA/QC Officer
":
• / Certification#E87819 SCDHEC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided s les. NCDENR Certification# 022
Page 1 of 4

Effluent Aquatic Toxicity Report Form -Acute Pass/Fail Date: 04/19/22
Facility HERIC SOLUTIONS-PECAN AVE NPDES# NC0089958 Pipe# 001 County Mecklenburg
Laboratory Performing Test ETT Environmental
X Comments
Signature of Operator in Responsible Charge a - /,
X
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Div.of Water Quality
N.C.DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
North Carolina Acute Pass/Fail Toxicity Test
Collection Date: 4/6/22 Organism Tested:
Collection Time: 0955 Pimephales promelas
Test Start Date: 4/7/22
Sample Type/Duration Control 7.7 8.2
Grab Comp Duration pH Treatment 7.2 8.0
X -_
Control Sample start end
Hardness(mg/L) 83.7 Control 7.8 7.2
Spec.Cond. (pmhos) 307 89 D.O. Treatment 9.0 7.3
Chlorine(mg/L) <0.05
Sample temp.at receipt 0.8
Mortality Replicate Mean Mortality
Treatment 1 (Control) A B C D
0% 0% 0% 0% 0%
Treatment 2(Exposure A B C D
Concentration 90% 0% 0% 0% 0% 0%
Tested
(NOTE): If mean control mortality exceeds 10%,the test is considered invalid)
Calculate using
Arc-Sine Calculated Student's t N/A PASS X
transformed
Square Root
Tabular Student's t 1.94 FAIL
data (ONE TAILED)
If the absolute value of the calculated t is less than or equal
to the absolute value of the tabular t, check PASS
If the absolute value of the calculated t is greater than the
absolute value of the tabular t, check FAIL.
If all vessels within each treatment have the same response
but the treatment two response is greater than the control, check FAIL.
DEM form AT-2(8/91)
Page 2 of 4
L - _ - -

24 Hour Acute Toxicity Test
Test Method:EPA 821 R-02-012; Method 2000 Pimephales promelas
Client: HERIC SOLD'IONS Sample ID:PECAN AVE Lab ID#: T61674
Start Date: 04/07/22 Time: 04:00 PM Set By: AM
End Date: 04/08/22 Time: 03:38 PM Ended By: JC
Test Vessel Test Solution Volume Incubator Transfer Volume Dilution Water
Fathead Minnows 500 mL plastic cup 200 mL #1 0.5 mL MHSF
Randomization pattern per SOP 'Neonates from common holding vessel 'Light: 50-100 ft-c.16 hr light/8 hr dark
TEST ORGANISMS
for Ceriodaphnia dubia Comments:
Date Removed: Between: and: FISH HATCHED ON 3/31/22 BTW 1500-1630 EI
Pimephales promelas Source: ABS lays old: 7
Mysidopsis bahia Source: Days old:
Test Organisms Pre Fed by: AM Time: 1315 I
MORTALITY DATA
Conc. Initial# Cumulative Mortality Final Initial Final
Cond/ Cond/
Rep. organisms za hr as hr 72 hr 96 hr m arraiir Temp D 0 pH Salmi By. Temp D.O. pH Saliri By.
A 10. 0
Control B 10 0
C 10 0
D 10 0 0% 2d.7 7 7 AM 24.8 7 2 8.2 JC
A 10' 0
90.0% B 10 0
C 10 0
D 10 0 0" 2; {) ill '_2I I.-NM 24.8 7.3 R_0 1('
A
B
C
D
A •
B
C II
D _L L
A
B
C
A
B
C
D I I I I
A
B
C
D I m,r I I HI I _ • me L 11'1'1
Page 3 of 4

. .
,.. T
, . CHAIN OF CUSTODY RECORD
r e1'2 sir e L; Paces of
PO Box 16414,Greenville,SC 29606-7414
(864)8 i 7-6942, [phone] Fa(854)877 6938
Shipping Address:4 Craftsman Ct,Greer,SC 29850
WN,ETENVMONm EN7AL.EOm
Client: ' r l
Z1 Program Containers Preservative Paraceters
Facility: v � 1 1
Whole Effluent Toniciry
State: NPDES#: cute Chronic Test Organisms —
t
ci
11
n r, O = J - -
(Composite only) (Grab or Composite) < o o c J '— — _ :7
U oti ` _ c I=i-LS04 - = = _ o .- v:
Sign;and Print below 3 = 5 u o ?=HCL = z z , —' _ o —
' v the dotted line 5 = r U .° v _ a-o° o o = , '\ = ( _
_ _  _ _ — _ _ > — d 1
SANII'LE ID U Compositeemr.Date Time Sample Collection Date Time Collected br U rq a] Z CO > 6=oth= < < V U U D. _ 2 s = F. - L Chemical Analysis a Other
.A
O _
A
-
I
I
Special Instructions:
cr2can 4ved .
Sample Custody Transfer Record Sec+re Receipt Sample
Date Time R_,• puished By/Organization c,:y.wed B• r aniz cion Area s Temp'C ! Preserved?
y 22 /,r1) �� �F�� //, )7 (1.1\p'E1lo.0
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity resting the sample must fr-be used v,ithin 36 hours
Time Proportional:I sample each hour for 24 hours.Equal voles 0.0 and 6.0'C.Samples must not be frozen.Use water ice in sealed bas. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used s er 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.

, o•
Waypoint . 449 Springbrook Rd,Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:00004
Customer Name: Heric Solutions, LLC
Report Number: 22-096-0036
Shipping Method
0 Fed Ex 0 US Postal # Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: IIRT-15 2.1 C
Shipping container/cooler uncompromised? # Yes 0 No
Number of coolers/boxes received �1
Custody seals intact on shipping container/cooler? 0 Yes 0 No # Not Present
Custody seals intact on sample bottles? 0 Yes 0 No J Not Present
Chain of Custody(COC) present? # Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed # Yes 0 No
Samples in proper containers? 0 Yes 0 No
Sample containers intact? # Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No 0 N/A
Water- VOA vials free of headspace #Yes 0 No 0 N/A
Trip Blanks received with VOAs 0 Yes 0 No # N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No J N/A
High concentration container (48 hr) r- Low concentration EnCore samplers (48 hr)
r High concentration pre-weighed (methanol -14 d) r Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: oe S. Vigilant Date &Time: 04/06/2022 18:04:54

I II ll 1111 111111 i III 111[1[1 ll 8,1°°42264396-°°36,
-..022 CHAIN OF CUSTODY RECORD LAB USE ONLY
YES NO N/A
hic:11(;SOILI11011S,LLC 18 03 58 PAGE /OF I QUOTE#TOENSURE PROPER BILLING:
Samples INTACT upon arrival? ......" _
montriiv
Project Name: Zegig"----
1 41441/4e— Received IN ICE? .00'
— --- -----
Short Hold Analy s (Yes) (No) UST Project: (Yes) (No) PROPER PRESERVATIVES indicated? .0•"'
e 'Please ATTACH any project specific reporting(QC LEVEL I II III IV) Received WITHIN HOLDING TIMES? ...""
Client Company Name: , CUSTODY SEALS INTACT?
-- provisions and/or QC Requirements -•.0-..f.:..r
Report To/Contact Name: Invoice To: VOLATILES rec'd W/OUT HEADSPACE? ,
Reporting Address: Address: PROPER CONTAINERS,4sed?
TEMP, Therm ID;ig--V t) Observed 1__-*C/Corr. 1..1.c
— ------- —J
Phone: Fax(Yes)(No): Purchase Order No./Billing Reference TO BE FILLEDIN BY CLIE,PSAMPLING PERSONNEL
Email Address: Requested Due Dale J 1 Day J 2 Days U 3 Days LI 4 Days J5 Days Certification: NC
EDD Type: PDF _Excel_____Other "Working Days" J 6-9 Days a Standard 10 days D FIUsh:urk Must Be
Site Location Name: Samples received after 15.00 will be processed next business d0Ved Other N/A_ay
,....,...-"'
Site Location Physical Address: _ ...... __. Turnaround(s(SEE
R lieeR isS E based
O R TERMSbU business
3 A days
.excludingCl l':IGeeskeE RndvsicaEn holidays Water Chlorinated: YES NO
SERVICES
RENDERED BY WAYPOINT ANALYTICAL LLC TO CUENT) Samples Iced Upon Collection: YES,___NO _
1 TIME MATRIX SAMPLE CONTAINER I AN: YS1S REQUESTED
CLIENT DATE ' COLLECTED (SOIL, PRESERVA- 0 / / 1? \X " 1
SAMPLE DESCRIPTION COLLECTED MILITARYN.
Y WATER.OR *TypE TIVES NO. SIZE , , (I/ r\/ /‘, REMARKS ID NO.
i H HOURS SLUDGE) SEE BELOW k\a'A
Eat
6 1 171 ••"22-IL)i 5 -. i 614.‘ c / 0 1 ik.7401.1
A /1, 6 ,4Id/V(1-
likil_ Zild/Y6—
111111111111111\1
.. _
IIII 11111111111111 3 0
111111
isI (
.....'"
1111
MIIIII __—__—_—_—_,-- —_--- -.—
1— MEMO' II ---.-------
PRESS DOWN FIRMLY - 2 COPIES (
I Sampled By(Print Name) i1/1 /S Affiliation___ -Ad 1=1111
_ t /
Upon relinquishing,this Chain of Custody is your authorization for Waypoint Analytical to proceed with the analyses as requested above.Any anges must be
'
su i in writing to the Waypoint Analytical Project Manager.There will be charges for any changes after analyses have beeninitialized. Site Arrival Time
initialized.
FirlIfl MINA y1/45igr
.--14.ec&ved By(Signakire) Date WiltarYl1i"3 Additional Comments: _Site Departure Time:
. ,
Hifinq By ISTgriatur ) Received By.(Signature) Date Fleki Tech Fee:
Relinquished By (Signature) Rem Far a nt I t ai B, Mileage: ,
72‘,/7 1 i 4!3 0 ._
'ikeillaFrol Shipment Went:ALL SAMPLE COOLERS-SROUffIE TAPED smut. C D L TRANSPORTATION TO THE LABORATORY. . C Group No
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST UN L CFJVED AT THE LABORATORY.
SEE REVERSE FOR
j Fee Ex J UPS ...1Hand-tleavered _ V vacant Analytical Field Service j _ - _
TERMS&CONDITIONS
....
NPDES: UST: G UNITOTAt ERi DRINKING WATER: SOLID WASTE: RCRA: BRWNFLD LANDFILL OTHER:
LI NC _1 SC J NC LI SC LI Nc J SC 1 -I NC J SC L3 NC LI SC LI NC LI SC CI NC U SC LI NC t.3 SC ta NC `LI SC
0 D 0 LI L) 0 U 0 0 ORIGINAL
- • —

f
C kr { {
J .111 OJl ^vY r/`. - ,-..7"Y1's r'K1!''s!'1'V'%Y'\
6.1
:Li ` i.,?: +Il,tt ital 111I I I�'III 1�`I I� �IF
� �I Pate of
-- 04-06 2022
PO Box 4641a,Greenville,SC 2953674'� Hem Solutions,art: tg 03 58
[phone], [phone] Fax[phone] Monthly
Shipping Address:4 Craftsman Ct,Greer,SC 29650
W ww.C1"•CNvi nD NM ENTAL.CO M
Client: "2/-8T`
�/ ,,, �y, , Program Containers Pre-serval-0' Parameters
Facility: �S i !
whole Emueet Toucan• xn
t-
Mate: NPDES i >Lu(e Chronic Test Organisms 1 , ,,
z
a ,
(Compasite only) (Grab or Composite) Z.` 9. 'n U 15 .t S — y
U E r
Cl' r '•H2S01 y �. a. 2 = u t ,
Sign.and Print below c m = 7'HCL r: _ _ u r,
to the lotted fine O E M a.N::Ot{ =� v C c = V _ d
SAMPLE ID S.— Composite Stu:Oars Time Sample Collection Date Tame Collected by J 0 VI Z a is 9 6.Otter E 4 J J V II r= 2 ,n .7 0 - 2 Chemical Analysis&Other
G' f/ 2a :� 'f ,, :"6 i ( K a) Y ,vvs t ) __ _._
_ _ _ . _ . _
1
Special instructions:
Sample Custody Transfer Record Secure I Receipt i Sample
Date Time R..i• uished 3v/Organization t ,ed8 .'t?f'ar,i 4 Area TemoeC I Preserved?
C -2� ( I 7-l�>f 91 .r _ _ re,� , I tv1-6 i,4' CI t ,'c
t !
— _ ._-_ -
COMPOSITE SA A=fPLLNG PROCEDURES T-TEil-rPERATURE MONITORING PROCEDURES HOLD TIASE PROCEDURES _
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must firs:be used within 36 hours
Time Proportional' I sample each hour for 24 hours.Equal volut 0.0 and 6.0'C.Samples must not be frozen.Use water ice in sealed baps, of sample collection(completion of composite sample).
or at minimum I sample every 4 how's over 24 hours. Sample may not be used after'2 hours from sample collection.
(Flow Proportional:As per instructions in NPDES permit.

Waypoint 449 Springbrook Rd,Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
5/2/2022
Heric Solutions, LLC
Eric Donnelly
P.O. Box 548
Indian Trail, NC, 28079
Ref: Analytical Testing
Lab Report Number: 22-111-0022
Client Project Description: Bi-Monthly
1111 Pecan Ave.
Project Number: Permit NC0089958
Dear Eric Donnelly:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/21/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

VVaypount. 449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
North Carolina State Program 37735 07/31/2022
North Carolina State Program 402 12/31/2022
South Carolina State Program 99012 07/31/2022
South Carolina State Program 99012 12/31/2022
Page 1 of 1 00016/22-111-0022

Q`
NC28217
Wáypoint. 449 Springbrook Rd, Charlotte,
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-111-0022
Client Project Description: Bi-Monthly
1111 Pecan Ave.
Lab No Client Sample ID Matrix Date Collected Date Received
99223 Bimonthly Aqueous 04/21/2022 14:20 04/21/2022 15:30

Q
Waypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 05/02/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 04/21/2022
Indian Trail , NC 28079
Report Number:22-111-0022 REPORT OF ANALYSIS
Lab No : 99223 Matrix: Aqueous
Sample ID :Bimonthly Sampled: 4/21/2022 14:20
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
pH 6.37 s.u. 1 04/21/22 14:20 FLD FIELD
Temperature 22.6 C 0.1 1 04/21/22 14:20 FLD FIELD
Arsenic <1.00 ii9/L 1.00 1 04/29/22 16:35 EDV 200.8
Barium 5.57 pg/L 5.00 1 04/29/22 16:35 EDV 200.8
Cadmium <1.00 pg/L 1.00 1 04/29/22 16:35 EDV 200.8
Chromium 1.96 pg/L 1.00 1 04/29/22 16:35 EDV 200.8
Copper <2.00 pg/L 2.00 1 04/29/22 16:35 EDV 200.8
Lead <1.00 pg/L 1.00 1 04/29/22 16:35 EDV 200.8
Mercury(Total) <0.000200 mg/L 0.000200 1 04/27/22 13:03 EDV 245.1
Nickel <5.00 pg/L 5.00 1 04/29/22 16:35 EDV 200.8
Selenium <5.00 pg/L 5.00 1 04/29/22 16:35 EDV 200.8
Zinc <10.0 pg/L 10.0 1 04/29/22 16:35 EDV 200.8
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Q
VVaypoint Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 05/02/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :04/21/2022
Indian Trail , NC 28079
Report Number:22-111-0022 REPORT OF ANALYSIS
Lab No : 99223 Matrix: Aqueous
Sample ID : Bimonthly Sampled: 4/21/2022 14:20
Analytical Method: 624.1 Prep Batch(es): V18166 04/28/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Benzene <0.500 pg/L 0.500 1 04/28/22 14:50 ANG V18168
Ethylbenzene <1.00 pg/L 1.00 1 04/28/22 14:50 ANG V18168
Toluene <1.00 pg/L 1.00 1 04/28/22 14:50 ANG V18168
o-Xylene <1.00 pg/L 1.00 1 04/28/22 14:50 ANG V18168
m,p-Xylene <2.00 pg/L 2.00 1 04/28/22 14:50 ANG V18168
Xylene(Total) <1.00 pg/L 1.00 1 04/28/22 14:50 KCC V18168
Surrogate:4-Bromofluorobenzene 98.6 Limits: 74-126% 1 04/28/22 14:50 ANG V18168
Surrogate: Dibromofluoromethane 99.8 Limits: 75-127% 1 04/28/22 14:50 ANG V18168
Surrogate: 1,2-Dichloroethane-d4 99.6 Limits: 67-136% 1 04/28/22 14:50 ANG V18168
Surrogate:Toluene-d8 90.6 Limits: 70-130% 1 04/28/22 14:50 ANG V18168
Analytical Method: 8270E Prep Batch(es): V17974 04/26/22 12:00
Prep Method: 3510C
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <20.4 pg/L 20.4 1 04/28/22 13:21 JMV V18177
Acenaphthylene <20.4 pg/L 20.4 1 04/28/22 13:21 JMV V18177
Anthracene <10.2 pg/L 10.2 1 04/28/22 13:21 JMV V18177
Benzo(a)anthracene <10.2 pg/L 10.2 1 04/28/22 13:21 JMV V18177
Benzo(a)pyrene <10.2 pg/L 10.2 1 04/28/22 13:21 JMV V18177
Benzo(b)fluoranthene <10.2 pg/L 10.2 1 04/28/22 13:21 JMV V18177
Benzo(g,h,i)perylene <10.2 pg/L 10.2 1 04/28/22 13:21 JMV V18177
Benzo(k)fluoranthene <10.2 pg/L 10.2 1 04/28/22 13:21 JMV V18177
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Waypoint, 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 05/02/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 04/21/2022
Indian Trail , NC 28079
Report Number:22-111-0022 REPORT OF ANALYSIS
Lab No : 99223 Matrix: Aqueous
Sample ID: Bimonthly Sampled: 4/21/2022 14:20
Analytical Method: 8270E Prep Batch(es): V17974 04/26/22 12:00
Prep Method: 3510C
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Chrysene <10.2 ug/L 10.2 1 04/28/22 13:21 JMV V18177
Dibenz(a,h)anthracene <20.4 pg/L 20.4 1 04/28/22 13:21 JMV V18177
Fluoranthene <10.2 pg/L 10.2 1 04/28/22 13:21 JMV V18177
Fluorene <10.2 pg/L 10.2 1 04/28/22 13:21 JMV V18177
Indeno(1,2,3-cd)pyrene <10.2 pg/L 10.2 1 04/28/22 13:21 JMV V18177
1-Methylnaphthalene <10.2 pg/L 10.2 1 04/28/22 13:21 JMV V18177
2-Methylnaphthalene <10.2 lig/L 10.2 1 04/28/22 13:21 JMV V18177
Naphthalene <10.2 lig/L 10.2 1 04/28/22 13:21 JMV V18177
Phenanthrene <10.2 lig/L 10.2 1 04/28/22 13:21 JMV V18177
Pyrene <10.2 pg/L 10.2 1 04/28/22 13:21 JMV V18177
Surrogate: 2-Fluorobiphenyl 53.5 Limits: 44-119% 1 04/28/22 13:21 JMV V18177
Surrogate: Nitrobenzene-d5 61.0 Limits: 44-120% 1 04/28/22 13:21 JMV V18177
Surrogate:4-Terphenyl-d14 92.5 Limits: 50-134% 1 04/28/22 13:21 JMV V18177
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

f
Waypoi nt 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:00004
Customer Name: Heric Solutions, LLC
Report Number: 22-111-0022
Shipping Method
0 Fed Ex 0 US Postal •J Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: IIRT-15 0.7 C
Shipping container/cooler uncompromised? 0 Yes 0 No
Number of coolers/boxes received I 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody (COC) present? 0 Yes 0 No
COC agrees with sample label(s)? #Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? j Yes 0 No
Sample containers intact? 0 Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. J Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No 0 N/A
Water- VOA vials free of headspace 0 Yes 0 No 0 N/A
Trip Blanks received with VOAs 0 Yes 0 No # N/A
Soil VOA method 5035—compliance criteria met O Yes 0 No 0 N/A
r High concentration container (48 hr) r Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) p Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Angela D Overcash Date & Time: 04/21/2022 15:42:18 11

•
VVa'ypoint., 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL uuww.wavoointanalytical.com
Kit ID: 179767 CHAIN-OF-CUSTODY
Initiated By: Angela Overcash -0022
111111111111111111111111111111111enc Solutions.LLC �22-tit,2022
Initiated Date: 3/2/2022
Project Comment Lab Sampling Event Eli-Monthly tsar 35
Company Name Company Number Client Project Manager/Contact Purchase Order Number
Heric Solutions,LLC 00004 Heric Solutions,LLC
Site Name Project Number Method of Shipment
E RUSH-Additional charges apply e till
Ej Fed Ex UPSUSPS
7 Special Detection Limits(s) Ei Courier i1 Client Drop Off
Pecan Ave.-BiMonthly Date Results Needed Other
LlMS Project ID Project Manager Phone# Project Manager Email Site/Facility ID#
980-721-2841
Grab/ #of
Date Time Sample ID Matrix Comp Cont Container Type Preservation Analyses
g-- f 7ZJ AQU v�- 1 Plastic 250mL HNO3
OAcid Nitric
Z Metals
/2z
AQU 1 Plastic-11 NONE oxicity
AQU 2 Amber Glass Liter NONE 8270PAH
624
Clear Glass Vial- HCL
AQU -sr- 3 40m1 Hydrochloric
Acid
1 j ,
L/26) j`� Field Readingsa
Date/Time L7--V'22'Initials 1/A �4^ pH - 17
Temp . 2 & Re CI Flow DO „ —'""-
For Laboratory Use Only Sampled by(Name-Print) Client Remarks/Comments
Ice Custody Lab Comments 1 V#0 461-11 c
Seals elinquished by:(SIGNATURE) Date Time Received by:(SIGNATURE) Date Time
ON Y Wit2L /s3)
elinquish d by:(SIGNATURE) Date Time Received by:(SIGNATURE) Date Time
Blank/Cooler Tern
I -\j Q; 1 t Relinquished by:(SIGNATURE) Date Time Received by: SIG TURE) Date Time
0 I c yi.;14 7;10
i/i

DISCHARGE MONITORING REPORTS AND EFFLUENT ANALYTICAL REPORTS
MAY 2022

NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1.0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-1 COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-I ORC HAS CHANGED:No
eDMR PERIOD:05-2022(May 2022) VERSION: 1.0 STATUS:Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
•
50050 00400 01002 01007 76028 34030 01027 32106 C0034
E E
P E = a
[a • . I Continuous Monthly2 X month 2 X month Monthly2 X month 2 X month Monthly2 X month
u, .... <` i- d r
g
o Recorder Grab Grab Grab Grab Grab Grab Grab Grab
B A i 0 z t
t] U h O 06 0 i FLOW pH As-TOTAL BARIUM SEMI-VOL BENZENE CADMIUM CHLRFORM TOT CR CONC
2400 dock Hrs 2400 dock Ilrs Y/B/N mgd su ug/1 ug/1 ug/1 ug/I ug/1 ug/I ugA
1 0.024
2 730 1.00 Y 0.049
3 1315 0 0.049 6.09 <I 106 <50 <0.5 <I <I 24.1
4 0.049
5 0.049
6 830 I.00 Y 0.049
7 0.049
8 0.049
9 0.049
to 845 I.00 Y 0.047
11 0.047
12 0.047
13 0.047
14 0.047
15 0.047
16 945 LS Y 0.046
17 0.046
18 730 4.0 Y 0.044
19 1530 0 0.044 <0.5 133 <0.5 <I 1.75
20 0.044
21 0.044
22 0.044
23 930 1.00 Y 0.043
24 0.043
25 0.043
26 945 1.00 Y 0.044
27 0.044
28 0.044
29 _ 0.044
30 0.044
31 0.044
Monthly Average Limit:
Monthly Average: 0.045258 0 119.5 0 0 0 0 12.94
Daily Maximum: 0.049 6.09 0 133 0 0 0 0 24.1
Daily Minimum: 0.024 6.09 0 106 0 0 0 0 1.78
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; EN V WTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday
Discharge Monitoring Report-Copy Of Record(COR_NC0089958_Ver_1.0_5_2022.pdt)

NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1.0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-1 COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-1 ORC HAS CHANGED:No
eDMR PERIOD:05-2022(May 2022) VERSION: 1.0 STATUS:Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
tl 01042 34371 00900 01051 COMER 01067 76029 TGE6C C0456 01147 34010
E E —
F" tE F o
E r 2 X month 2 X month Monthly 2 X month 2 X month 2 X month Monthly Monthly 2 X month 2 X month 2 X month
E ~
u 8 °a Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab 2.
Ts v 0 u s"
G I- O O cg
O 7
COPPER ETHYLBEN TOT HARD LEAD MERCURY- NICKEL VOLATILE FTHD24PF PAH-CO Se-TOTAL TOLUENE
2400 clock Mrs 2400 dock Hrs Y/B/N ug/I ug/I mg/I mg/1 ug/I ug/1 ug/I pass/fail ug/I ug/1 ug/I
1
2 730 1.00 Y
3 1315 0 <2 <I 22 <I <0.0002 6.82 1.39 100 <20 <5 <I
4
5
6 830 1.00 Y
7
8
9
10 845 1.00 Y
n
12
13
14
15
16 945 1.5 Y
17
18 730 4.0 Y
19 1530 0 1.24 <I <0.5 <0.0002 <0.5 <20 <I <I
20
21
22
23 930 1.00 Y
24
25
26 945 1.00 Y
27
28
29
30
31
Monthly Average Limit:
Monthly Averages 0.62 0 22 0 0 3.41 1.39 100 0 0 0
Daily Maximum: 1.24 0 22 0 0 6.82 1.39 100 0 0 0
Daily Minimum: 0 0 22 0 0 0 1.39 100 0 0 0
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday
Discharge Monitoring Report-Copy Of Record(COR_NC0089958_Ver_1.0_5_2022.pdf)

NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1.0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-1 COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-1 ORC HAS CHANGED:No
eDMR PERIOD:05-2022(May 2022) VERSION: 1.0 STATUS:Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
81551 01092
1
— E E 2 X month 2 X month
< E_ —
O Grab Grab
2: 8 8 5 K
u 2 O O O XYLENE ZINC
2400 clock Hrs 2400 clock Hrs YBIN ugh ug/1
1
2 730 1.00 Y
3 1315 0 <I <10
4
5
6 830 1.00 Y
7
9
10 845 1.00 Y
II
12
13
14
15
16 945 1 5 Y
17
18 730 4.0 Y
19 1530 0 I 20
20
21
22
23 930 1.00 Y
24
25
26 945 1.00 Y
27
28
29
30
31
Monthly Average Limit:
Monthly Average: 0 0
Daily Maximum: 0
0
Daily Minimum: 0 0
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday
Discharge Monitoring g,Report-Copy Of Record(COR_NC0089958_Ver_1.0_5_2022.pdf)

f
NPDES PERMIT NO.:NC0089958 PERMIT VERSION: 1_0 PERMIT STATUS:Active
FACILITY NAME:Central Square CLASS:PC-1 COUNTY:Mecklenburg
OWNER NAME:Tgacse Central Square LLC ORC:Eric Christian Donnelly ORC CERT NUMBER: 1009608
GRADE:PC-1 ORC HAS CHANGED:No
eDMR PERIOD:05-2022(May 2022) VERSION: 1.0 STATUS:Submitted
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:06/18/2022
Electronically Certified by Eric Christian Donnelly on 2022-06-18 14:34:13.995
ORC/Certifier Signature:Eric Christian Donnelly Phone #:[phone] Date
I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.The written submission shall be made as required by part II.E.6 of the
NPDES permit.
Electronically Signed by Eric Christian Donnelly on 2022-06-18 14:35:11.437
Permittee/Submitter Signature: ***Eric Christian Donnelly Phone #:[phone] Date
Permittee Address:201 S College St Ste 1300 Charlotte NC 28244 Permit Expiration Date: 11/30/2026
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:Waypoint Analytical
CERTIFIED LAB#:402
PERSON(s)COLLECTING SAMPLES:David Morris
PARAMETER CODES
Parameter Code assistance may be obtained by visiting https://deq.nc.gov/about/divisions/water-resources/edmr/user-documentation.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:YES indicates that No Flow/Discharge occurred and,as a result,no data is reported for any parameter on the DMR for the
entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).
Discharge Monitoring Report-Copy Of Record(COR_NC0089958_Ver_1.0_5_2022.pdf)

Waypoint.. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
6/1/2022
Heric Solutions, LLC
Eric Donnelly
P.O. Box 548
Indian Trail, NC, 28079
Ref: Analytical Testing
Lab Report Number: 22-123-0024
Client Project Description: Monthly
1111 Pecan Ave.
Project Number: Permit NC0089958
Dear Eric Donnelly:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 5/3/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

V/aypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Certification Summary
Laboratory ID: WP CNC:Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
North Carolina State Program 37735 07/31/2022
North Carolina State Program 402 12/31/2022
South Carolina State Program 99012 07/31/2022
South Carolina State Program 99012 12/31/2022
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
Alabama State Program 40750 02/28/2023
Arkansas State Program 88-0650 02/07/2023
California State Program 2904 06/30/2022
Florida State Program - NELAP E871157 06/30/2022
Georgia State Program C044 02/18/2023
Georgia State Program 04015 06/30/2022
Illinois State Program -NELAP 200078 10/10/2022
Kentucky State Program 80215 06/30/2022
Kentucky State Program KY90047 12/31/2022
Louisiana State Program - NELAP LA037 12/31/2022
Louisiana State Program - NELAP 04015 06/30/2022
Mississippi State Program MS 02/11/2023
North Carolina State Program 415 12/31/2022
Pennsylvania State Program - NELAP 68-03195 05/31/2022
South Carolina State Program 84002 06/30/2022
South Carolina State Program 84002 06/30/2022
Tennessee State Program 02027 02/11/2023
Texas State Program - NELAP T104704180 09/30/2022
Virginia State Program 00106 06/30/2022
Virginia State Program - NELAP 460181 09/14/2022
Page 1 of 1 00016/22-123-0024

IA?
Waypoi nt. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-123-0024
Client Project Description: Monthly
1111 Pecan Ave.
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
89038 Monthly Aqueous 05/03/2022 13:15 05/03/2022 14:20
89038 Monthly Aqueous 05/03/2022 13:15 05/03/2022 14:20 200.8 WP MTN
89039 Monthly-8270 PAH Aqueous 05/03/2022 13:15 05/03/2022 14:20
WP MTN-Memphis,TN: Waypoint Analytical-TN, Memphis,TN

VVa'ypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 06/01/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 05/03/2022
Indian Trail , NC 28079
Report Number:22-123-0024 REPORT OF ANALYSIS
Lab No : 89038 Matrix: Aqueous
Sample ID :Monthly Sampled: 5/3/2022 13:15
Test Results Units MOL DF Date/Time By Analytical
Analyzed Method
Hardness 22.0 mg/L 10.0 1 05/18/22 09:20 CLB 2340C-2011
pH 6.09 s.u. 1 05/03/22 13:15 FLD FIELD
Temperature 24.9 C 0.1 1 05/03/22 13:15 FLD FIELD
Arsenic <5.00 pg/L 5.00 10 05/19/22 13:06 BKN 200.8
Barium 106 pg/L 10.0 10 05/19/22 13:06 BKN 200.8
Cadmium <1.00 pg/L 1.00 10 05/19/22 13:06 BKN 200.8
Chromium 24.1 u9/L 10.0 10 05/19/22 13:06 BKN 200.8
Copper <5.00 U9/L 5.00 10 05/19/22 13:06 BKN 200.8
Lead <5.00 pg/L 5.00 10 05/19/22 13:06 BKN 200.8
Mercury(Total) <0.000200 mg/L 0.000200 1 05/06/22 19:13 EDV 245.1
Nickel 6.82 pg/L 5.00 10 05/19/22 13:06 BKN 200.8
Selenium <10.0 pg/L 10.0 10 05/19/22 13:06 BKN 200.8
Zinc <200 pg/L 200 10 05/19/22 13:06 BKN 200.8
Qualifiers/ * Outside QC Limit B Analyte detected in blank
Definitions DF Dilution Factor MQL Method Quantitation Limit

fit°
Waypoi nt, 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 06/01/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 05/03/2022
Indian Trail , NC 28079
Report Number:22-123-0024 REPORT OF ANALYSIS
Lab No : 89038 Matrix: Aqueous
Sample ID :Monthly Sampled: 5/3/2022 13:15
Analytical Method: 624.1 Prep Batch(es): V18730 05/15/22 14:00
Prep Method: 624.1(Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acetone <5.00 pg/L 5.00 1 05/16/22 06:32 JLB V18731
Acrolein <5.00 pg/L 5.00 1 05/16/22 06:32 JLB V18731
Acrylonitrile <5.00 pg/L 5.00 1 05/16/22 06:32 JLB V18731
Benzene <0.500 pg/L 0.500 1 05/16/22 06:32 JLB V18731
Bromodichloromethane <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
Bromoform <3.00 pg/L 3.00 1 05/16/22 06:32 JLB V18731
Bromomethane <2.00 pg/L 2.00 1 05/16/22 06:32 JLB V18731
Carbon Tetrachloride <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
Chlorobenzene <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
Chlorodibromomethane <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
Chloroethane <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
2-Chloroethylvinyl Ether <10.0 pg/L 10.0 1 05/16/22 06:32 JLB V18731
Chloroform <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
Chloromethane <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
1,2-Dichlorobenzene <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
1,3-Dichlorobenzene <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
1,4-Dichlorobenzene <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
1,1-Dichloroethane <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
1,2-Dichloroethane 1.39 pg/L 1.00 1 05/16/22 06:32 JLB V18731
1,1-Dichloroethene <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
trans-1,2-Dichloroethene <2.00 pg/L 2.00 1 05/16/22 06:32 JLB V18731
1,2-Dichloropropane <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
Qualifiers/ * Outside QC Limit B Analyte detected in blank
Definitions DF Dilution Factor MQL Method Quantitation Limit

V�
Waypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 06/01/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 05/03/2022
Indian Trail , NC 28079
•
Report Number:22-123-0024 REPORT OF ANALYSIS
Lab No : 89038 Matrix: Aqueous
Sample ID : Monthly Sampled: 5/3/2022 13:15
Analytical Method: 624.1 Prep Batch(es): V18730 05/15/22 14:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
cis-1,3-Dichloropropene <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
trans-1,3-Dichloropropene <1.00 ug/L 1.00 1 05/16/22 06:32 JLB V18731
Ethylbenzene <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
Methylene Chloride <2.00 pg/L 2.00 1 05/16/22 06:32 JLB V18731
1,1,2,2-Tetrachloroethane <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
Tetrachloroethene <0.750 pg/L 0.750 1 05/16/22 06:32 JLB V18731
Toluene <1.00 ug/L 1.00 1 05/16/22 06:32 JLB V18731
1,1,1-Trichloroethane <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
1,1,2-Trichloroethane <0.500 hg/L 0.500 1 05/16/22 06:32 JLB V18731
Trichloroethene <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
Trichlorofluoromethane <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
1,2,3-Trichloropropane <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
1,2,4-Trimethylbenzene <0.500 pg/L 0.500 1 05/16/22 06:32 JLB V18731
Vinyl Chloride <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
o-Xylene <1.00 pg/L 1.00 1 05/16/22 06:32 JLB V18731
m,p-Xylene <2.00 pg/L 2.00 1 05/16/22 06:32 JLB V18731
Xylene(Total) <1.00 pg/L 1.00 1 05/16/22 06:32 V18731
Surrogate:4-Bromofluorobenzene 100 Limits: 74-126% 1 05/16/22 06:32 JLB V18731
Surrogate: Dibromofluoromethane 98.0 Limits: 75-127% 1 05/16/22 06:32 JLB V18731
Surrogate: 1,2-Dichloroethane-d4 96.6 Limits: 67-136% 1 05/16/22 06:32 JLB V18731
Surrogate:Toluene-d8 97.2 Limits: 70-130% 1 05/16/22 06:32 JLB V18731
Qualifiers/ * Outside QC Limit B Analyte detected in blank
Definitions DF Dilution Factor MQL Method Quantitation Limit

f
Waypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 06/01/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 05/03/2022
Indian Trail , NC 28079
Report Number:22-123-0024 REPORT OFANALYSIS
Lab No : 89038 Matrix: Aqueous
Sample ID :Monthly Sampled: 5/3/2022 13:15
Analytical Method: 625.1 Prep Batch(es): V18474 05/10/22 11:45
Prep Method: 625.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Acenaphthylene <20.0 pg/L 20.0 1 05/16/22 19:02 JMV V18916
Anthracene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Benzidine <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Benzo(a)anthracene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Benzo(a)pyrene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Benzo(b)fluoranthene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Benzo(g,h,i)perylene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Benzo(k)fluoranthene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Benzoic Acid <50.0 pg/L 50.0 1 05/16/22 19:02 JMV V18916
Benzyl alcohol <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Bis(2-Chloroethoxy)methane <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Bis(2-Chloroethyl)ether <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Bis(2-Chloroisopropyl)ether <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Bis(2-ethylhexyl)phthalate <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
4-Bromophenyl phenyl ether <20.0 pg/L 20.0 1 05/16/22 19:02 JMV V18916
Butyl benzyl phthalate <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
4-Chloro-3-methylphenol <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
2-Chloronaphthalene <20.0 pg/L 20.0 1 05/16/22 19:02 JMV V18916
2-Chlorophenol <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
4-Chlorophenyl phenyl ether <20.0 pg/L 20.0 1 05/16/22 19:02 JMV V18916
Chrysene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Qualifiers/ * Outside QC Limit B Analyte detected in blank
Definitions DF Dilution Factor MQL Method Quantitation Limit

Wapoint, 449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions,LLC Project Monthly
Eric Donnelly Report Date : 06/01/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :05/03/2022
Indian Trail , NC 28079
Report Number:22-123-0024 REPORT OF ANALYSIS
Lab No : 89038 Matrix: Aqueous
Sample ID : Monthly Sampled: 5/3/2022 13:15
Analytical Method: 625.1 Prep Batch(es): V18474 05/10/22 11:45
Prep Method: 625.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Dibenz(a,h)anthracene <20.0 pg/L 20.0 1 05/16/22 19:02 JMV V18916
Dibenzofuran <20.0 pg/L 20.0 1 05/16/22 19:02 JMV V18916
1,2-Dichlorobenzene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
1,3-Dichlorobenzene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
1,4-Dichlorobenzene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
3,3'-Dichlorobenzidine <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
2,4-Dichlorophenol <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Diethyl phthalate <20.0 pg/L 20.0 1 05/16/22 19:02 JMV V18916
Dimethyl phthalate <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
2,4-Dimethylphenol <20.0 pg/L 20.0 1 05/16/22 19:02 JMV V18916
Di-n-butyl phthalate <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
4,6-Dinitro-2-methylphenol <30.0 pg/L 30.0 1 05/16/22 19:02 JMV V18916
2,4-Dinitrophenol <30.0 lJ9/L 30.0 1 05/16/22 19:02 JMV V18916
2,4-Dinitrotoluene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
2,6-Dinitrotoluene <20.0 N9/L 20.0 1 05/16/22 19:02 JMV V18916
Di-n-Octyl Phthalate <10.0 u9/L 10.0 1 05/16/22 19:02 JMV V18916
Fluoranthene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Fluorene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Hexachlorobenzene <20.0 u9/L 20.0 1 05/16/22 19:02 JMV V18916
Hexachlorobutadiene <20.0 u9/L 20.0 1 05/16/22 19:02 JMV V18916
Hexachlorocyclopentadiene <20.0 pg/L 20.0 1 05/16/22 19:02 JMV V18916
Hexachloroethane <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Qualifiers/ * Outside QC Limit B Analyte detected in blank
Definitions DF Dilution Factor MQL Method Quantitation Limit

r
O
Waypoint
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 06/01/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :05/03/2022
Indian Trail , NC 28079
Report Number:22-123-0024 REPORT OF ANALYSIS
Lab No : 89038 Matrix: Aqueous
Sample ID :Monthly Sampled: 5/3/2022 13:15
Analytical Method: 625.1 Prep Batch(es): V18474 05/10/22 11:45
Prep Method: 625.1 (Prep)
Test Results Units MIL DF Date/Time By Analytical
Analyzed Batch
Indeno(1,2,3-cd)pyrene <10.0 ug/L 10.0 1 05/16/22 19:02 JMV V18916
Isophorone <10.0 ug/L 10.0 1 05/16/22 19:02 JMV V18916
1-Methylnaphthalene <10.0 ug/L 10.0 1 05/16/22 19:02 JMV V18916
2-Methylnaphthalene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
Naphthalene <10.0 ug/L 10.0 1 05/16/22 19:02 JMV V18916
Nitrobenzene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
2-Nitrophenol <10.0 ug/L 10.0 1 05/16/22 19:02 JMV V18916
4-Nitrophenol <10.0 iJg/L 10.0 1 05/16/22 19:02 JMV V18916
N-Nitrosodiphenylamine <20.0 ug/L 20.0 1 05/16/22 19:02 JMV V18916
N-Nitroso-di-n-propylamine <20.0 ug/L 20.0 1 05/16/22 19:02 JMV V18916
Pentachlorophenol <50.0 IJg/L 50.0 1 05/16/22 19:02 JMV V18916
Phenanthrene <10.0 ug/L 10.0 1 05/16/22 19:02 JMV V18916
Phenol <10.0 ug/L 10.0 1 05/16/22 19:02 JMV V18916
Pyrene <10.0 ug/L 10.0 1 05/16/22 19:02 JMV V18916
1,2,4-Trichlorobenzene <10.0 pg/L 10.0 1 05/16/22 19:02 JMV V18916
2,4,6-Trichlorophenol <20.0 ug/L 20.0 1 05/16/22 19:02 JMV V18916
Surrogate: Phenol-d5 27.5 Limits: 10-63% 1 05/16/22 19:02 JMV 625.1
Surrogate: 2-Fluorobiphenyl 65.4 Limits: 49-118% 1 05/16/22 19:02 JMV V18916
Surrogate: 2-Fluorophenol 41.6 Limits: 22-84% 1 05/16/22 19:02 JMV V18916
Surrogate: Nitrobenzene-d5 67.4 Limits: 43-123% 1 05/16/22 19:02 JMV V18916
Surrogate:4-Terphenyl-d14 83.2 Limits: 49-151% 1 05/16/22 19:02 JMV V18916
Surrogate: 2,4,6-Tribromophenol 78.2 Limits: 31-144% 1 05/16/22 19:02 JMV V18916
Qualifiers/ * Outside QC Limit B Analyte detected in blank
Definitions DF Dilution Factor MQL Method Quantitation Limit

Wa4point Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 06/01/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :05/03/2022
Indian Trail , NC 28079
Report Number :22-123-0024 REPORT OF ANALYSIS'
Lab No : 89039 Matrix: Aqueous
Sample ID : Monthly-8270 PAH Sampled: 5/3/2022 13:15
Analytical Method: 8270E Prep Batch(es): V18481 05/10/22 11:45
Prep Method: 3510C
Test Results Units MOL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <20.0 pg/L 20.0 1 05/17/22 14:36 JMV V19087
Acenaphthylene <20.0 pg/L 20.0 1 05/17/22 14:36 JMV V19087
Anthracene <10.0 Vg/L 10.0 1 05/17/22 14:36 JMV V19087
Benzo(a)anthracene <10.0 pg/L 10.0 1 05/17/22 14:36 JMV V19087
Benzo(a)pyrene <10.0 pg/L 10.0 1 05/17/22 14:36 JMV V19087
Benzo(b)fluoranthene <10.0 pg/L 10.0 1 05/17/22 14:36 JMV V19087
Benzo(g,h,i)perylene <10.0 pg/L 10.0 1 05/17/22 14:36 JMV V19087
Benzo(k)fluoranthene <10.0 pg/L 10.0 1 05/17/22 14:36 JMV V19087
Chrysene <10.0 pg/L 10.0 1 05/17/22 14:36 JMV V19087
Dibenz(a,h)anthracene <20.0 pg/L 20.0 1 05/17/22 14:36 JMV V19087
Fluoranthene <10.0 pg/L 10.0 1 05/17/22 14:36 JMV V19087
Fluorene <10.0 pg/L 10.0 1 05/17/22 14:36 JMV V19087
Indeno(1,2,3-cd)pyrene <10.0 pg/L 10.0 1 05/17/22 14:36 JMV V19087
1-Methylnaphthalene <10.0 pg/L 10.0 1 05/17/22 14:36 JMV V19087
2-Methylnaphthalene <10.0 pg/L 10.0 1 05/17/22 14:36 JMV V19087
Naphthalene <10.0 ug/L 10.0 1 05/17/22 14:36 JMV V19087
Phenanthrene <10.0 pg/L 10.0 1 05/17/22 14:36 JMV V19087
Pyrene <10.0 ug/L 10.0 1 05/17/22 14:36 JMV V19087
Surrogate: 2-Fluorobiphenyl 40.2 * Limits: 44-119% 1 05/17/22 14:36 JMV V19087
Surrogate: Nitrobenzene-d5 54.0 Limits: 44-120% 1 05/17/22 14:36 JMV V19087
Surrogate:4-Terphenyl-d14 68.4 Limits: 50-134% 1 05/17/22 14:36 JMV V19087
Qualifiers/ * Outside QC Limit B Analyte detected in blank
Definitions DF Dilution Factor MQL Method Quantitation Limit

env rortinonta,Irtc. (C64)377.6942 .rA):[phone]
P.O. Box 16414, Creenvlle, Sc 2060E 4 Craflsrntan Court, Gryer, SC 29650
Pimephales promelas 24 Hr. Acute Pass/Fail Test
EPA-821-R-02-012 Method 2000
Client: HERIC SOLUTIONS
Facility:PECAN AVE
NPDES#:NC0089958
Test Date: 04-May-22
Laboratory ID#: T61863
Test Reviewed and Approved By:
Robert W.Kelley,Ph.D. Patrick D.Timms
President QA/QC Officer
fr:ccifkiik
y'x;
AP1 Certification#E87819 SCDHEC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided s les. NCDENR Certification# 022
Wage 1 of 4

Effluent Aquatic Toxicity Report Form -Acute Pass/Fail Date: 05/13/22
Facility HERIC SOLUTIONS-PECAN AVE NPDES# NC0089958 Pipe# 001 County Mecklenburg
Laboratory Performing Test ETT Environmental
X Comments
Signature of Operator in Responsible Charge az, av�
X W
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
North Carolina Acute Pass/Fail Toxicity Test
Collection Date: 5/3/22 Organism Tested:
Collection Time: 1315 Pimephales promelas
Test Start Date: 5/4/22
Sample Type/Duration Control 7.7 8.2
Grab Comp Duration pH Treatment 7.4 8.0
X
--_ Control Sample start end
Hardness(mg/L) 83.7 Control 8.4 9.3
Spec.Cond.(pmhos) 309 81 D.O. Treatment 9.3 9.4
Chlorine(mg/L) <0.05
Sample temp.at receipt 3.0
Mortality Replicate Mean Mortality
Treatment 1 (Control) A B C D
0% 0% 0% 0% 0%
Treatment 2(Exposure) A B C D
Concentration 90% 0% 0% 0% 0% 0%
Tested
(NOTE): If mean control mortality exceeds 10%,the test is considered invalid)
Calculate using
Arc-Sine Calculated Student's t N/A PASS X
Square Root
transformed Tabular Student's t 1.94 FAIL
data (ONE TAILED)
If the absolute value of the calculated t is less than or equal
to the absolute value of the tabular t, check PASS
If the absolute value of the calculated t is greater than the
absolute value of the tabular t, check FAIL.
If all vessels within each treatment have the same response
but the treatment two response is greater than the control, check FAIL.
DEM form AT-2(8/91)
Page 2 of 4

I
24 Hour Acute Toxicity Test
Test Method:EPA 821 R-02-012; Method 2000 Pimephales promelas
Client: HERIC PECAN AVE Sample ID:HERIC PECAN AVE Lab 1D1/: T61863
Start Date: 05/04/22 Time: 04:15 PM Set By: JC
End Date: 05/05/22 Time: 03:33 PM Ended By: JC
Test Vessel Test Solution Volume Incubator Transfer Volume Dilution Water
Fathead Minnows 500 mL plastic cup 200 mL #1 0.5 mL MHSF
Randomization pattern per SOP 'Neonates from common holding vessel ,Light: 50-100 ft-c.16 hr light/8 hr dark
TEST ORGANISMS
for Ceriodaphnia dubia Comments:
Date Removed: Between: and:
Pimephales promelas Source: ABS 5/3/22 lays old: 6 ORGANISMS HATCHED 4/28/22 1500-1630
Mysidopsis bahia Source: Days old:
Test Organisms Pre Fed by: JC Time: 2:00
MORTALITY DATA
Conc. I Initial# Cumulative Mortality Final Initial Final
Cond/ Cond/
Rep. organisms za m .n n. n n. ve I. Mun.eiy Temp D.O. pH Salini By: Temp D.O. pH Salini By:
A 10 0I
Control B 10 0 1i 4. x 3 :
D 10 0 0% 24.61 8.4 7.7 ��JC 24.8 ' 9.3 8.2 JC
A 10 0 �3 �
90.0% B 10 0 n2 t $ t" :` ,
C 10 0 4 R4
D 10 0 0% 24.8 9.3 7.4 JC 24.8 p9.4 801 jJC
A . tr tr
AT :
B
C ,
D
A 'rts ^
B '�5V S 1 A-a ,A�- 44.1ft i Z4 'h`V=L ,fir v i a^v } &,C
D I
A s mom, y c b,,. ,ivi ✓»,it` "w`°. 0,, ", '', eu
e s t:-a t `te" `> f a.4 yes
B M It.` kx p Tv
C
A ", y 'a
iii,:
D g/ec mL 1 PPT I °C I. mg/L I . .<.
C I PPT
Page 3 of 4

ETTCHALN OF CUSTODY RECORD
PO Box 15414,Greenville,SC 23506-7414
[phone], [phone] Fax[phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29550
"/WW-E•:DENVIRONMENrAL.COr.
Client: d; - - - -- -
� Z?r>4 Program Containers Preservative Parameters
Facility:
Whole C•tiiuent Te<i cin'
I
State: NPDES Acute Chronic Tmt Organisms
1 I II
1 ,
2 (Composite only) (Crab or Composite) < 5 _ v c y _ _ 5.
Z
U 9 - 2 1=H2504 c B -E - _ = G :r-
Sign,and Print below y - _ c , 2=HCL = = - _ _•a = = _ it::
the dotted line 5. i � v ''_ =' °' — G = •_ — s = =
U = = -- i = a=t,eoH o = c o = = ' •= — ? 7, N E,
r SAi�LE lD Composite Star.Date]Tine 5nmple Colicction Date Time Collected br U rn V7 Z � 7 > ,, < < U iJ t:J p 1_1-.I s — J _,y 1- Chemical Analysis&Other —6=O�hc _ _
oa
to
to I I
a I
0
4.
£O S£bl AN41.topy
bZ00-£Z�O��II�1��1I�II�111lfl��ll1i11'I1Ih suf ognlo 3 DuaH
��1 I'111IIf1111il
I f Ilii
Special instructions:
1c, /'�.-lie
Sample Custody Transfer Record !Secure Receipt Sampie
/�
Date Time elirquishedd By I Organization / Re ei' By?Organization' 1?-ea I Tame=C I Preserved?
te zzl,Cobb L /J ,,. 01 T I )_0
I i i I
1
i i I
COMPOSITE SAMPLING PROCEDURES TEiIPER-ITURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity resting the sample must first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volut 0.0 and 6.0'C.Samples must not be frozen.Use water ice in sealed bass. of sample collection(completion of compose sample).
or at minimum l sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.

•
Q
VVa point 449 Springbrook Rd,Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytital.com
Shipment Receipt Form
Customer Number:00004
Customer Name: Heric Solutions, LLC
Report Number: 22-123-0024
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: IIRT-15 2.0 C
Shipping container/cooler uncompromised? 0 Yes 0 No
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody(COC) present? 0 Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? 0 Yes 0 No
Sample containers intact? 0 Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No 0 N/A
Water- VOA vials free of headspace 0 Yes 0 No 0 N/A
Trip Blanks received with VOAs 0 Yes 0 No 0 N/A
Soil VOA method 5035—compliance criteria met O Yes 0 No 0 N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: lAngela D Overcash ! Date &Time: 05/03/2022 14:36:22

4
a
Waypoint, 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Kit ID: 181879 CHAIN-OF-CUSTODY
Initiated By: Angela Overcash ( { [ 05-03-2022
� � 3-0024
Initiated Date: 4/25/2022 I �1�1� �� � 0004
143503
Honc Solutions.LLC
Project Comment Lab Sampling Event Monthly
Company Name Company Number Client Project Manager/Contact Purchase Order Number
Heric Solutions,LLC 00004 Heric Solutions,LLC
Site Name Project Number Method of Shipment
J RUSH—Additional charges apply --._f r
lied Ex L_j UPS _ USPS
E]Special Detection Umits(s) 7 Courier 7Client Drop Off
Pecan Ave.-Monthly Date Results Needed Other
LIMS Project ID Project Manager Phone tt Project Manager Email Site/Facility ID U
980-721-2841
Grab/ if of
Date Time Sample ID Matrix Container Type Preservation Analyses
Comp Cont
ir-P5 22 / 3 j AQU 1 Plastic-SODmt Metals/Hardness
� HNQ3 Nitric
Acid
AQU 1 Plastic-1L NONE Acute Toxicity
AQU 2 Amber Glass-Liter NONE 625
AQU 2 Amber Glass-Liter NONE 827OPAH
Clear Glass Vial- HCL-
4 d AQU 3 40m1 Hydrochloric 624
° Acid
/3/} Field Re 9dingls
C-32 ,D
Date/Time J Initials 1�'� pH
Temp 79,ei Re CI Flow DO
For Laboratory Use Only Sampled by(Name
�-/J Print) Client Remarks/Comments
Ice Custody Lab Comments )414) /J/, t(S
Seals Relinquished by:(SIGNATURE) Date Time Receive:(SIGNATURE) Date Time
6;3-2'fiZZ) ' 5/3/0 Pe&
elinquish d by:(SIGNATURE) Date Time Received by:(SIGNATURE) r Date lime
Blank/Cooler Temp
- Relinquished by:(SIGNATURE) Date Time Received by:(SIGNATURE) Date Time

ETT CHAIN OF CUSTODY RECORD
enyiron Ii:,, 1" t: Page of
PG`ecx 1&4t4.Greenvi,ie,SC 2C6O&-7414��[phone], ie00)891-2325 Faic(884)877 5938
Shipping Address:4 Craftsman Ct,Greer,SC 29850
www.er�ewvrucs,.w1e.rrwt..eo,.
Client: /"'�/ /
J Vt'tz',.�� Gj .ydw Program CorttAincrs Preser4ativc Parse-let,':
Facility: - 1
Whole Effluent Tackle:,
State: IDES r: 4 I Acute Chronic Tat Orgsnians
E{ i C
r�
=
Com ns±:a orJ G. a 44 — c .. U g c
E i y) ( rob or Composite) E ' ., ej o _
U c ti _ - r y
E' 5 v `a ii2SO4 �v t -
Sign,and Print below 3 l , ° c u 2..HCt III o 2 a,2 » 5 a o :�t
i'sg the dotted line tJ • _ .t.t•OH U — _ .2 ' 3 z
0 0 °� Q o a -: = - a v
SAMPLE ID 4 Cu upas'ruSiart psis Time Sump ecilcctiuu note Time Collected b• U tf en. Z aie C 0 > � - < v J U D L�2 rn�T�'L C 3 2 Chemical Anatyaia&Other
lam' _-____
____._ CGSz e, 4141++
oloy
27.OZ-CO SG 3T1'suo)tn1oS Ptak _
f1111111(IIINI/lN1/1I/{III1111l!I(I
1Illlllllllilllll
� � _ �. .._�_._� - 1 1 I l j ; .
Special instructions:
/ ;
+!
Sample Custody Transfer Record Secure Receipt Sample
Date Time _ diminished !Organization — elt jy/Organization rea ( Temp 4C Preserved?
I
COMPOSITE SAMPLING PROCEDURES TEMPERATURE kiawrORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period, Sample temperature during collection and transport must be between For toxicity resting the sample must first be used within 36 hours
Time Proportional: I sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bans. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.

Wa 4 p►oift 449 Springbrook Rd,Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
6/14/2022
Heric Solutions, LLC
Eric Donnelly
P.O. Box 548
Indian Trail, NC, 28079
Ref: Analytical Testing
Lab Report Number: 22-139-0012
Client Project Description: Bi-Monthly or Monthly
1111 Pecan Ave.
Project Number: Permit NC0089958
Dear Eric Donnelly:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 5/19/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

VVaypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Certification Summary
Laboratory ID: WP CNC:Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
North Carolina State Program 37735 07/31/2022
North Carolina State Program 402 12/31/2022
South Carolina State Program 99012 07/31/2022
South Carolina State Program 99012 12/31/2022
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
Alabama State Program 40750 02/28/2023
Arkansas State Program 88-0650 02/07/2023
California State Program 2904 06/30/2022
Florida State Program - NELAP E871157 06/30/2022
Georgia State Program C044 02/18/2023
Georgia State Program 04015 06/30/2022
Illinois State Program- NELAP 200078 10/10/2022
Kentucky State Program 80215 06/30/2022
Kentucky State Program KY90047 12/31/2022
Louisiana State Program- NELAP LA037 12/31/2022
Louisiana State Program- NELAP 04015 06/30/2023
Mississippi State Program MS 02/11/2023
North Carolina State Program 415 12/31/2022
Pennsylvania State Program - NELAP 68-03195 05/31/2023
South Carolina State Program 84002 06/30/2022
South Carolina State Program 84002 06/30/2022
Tennessee State Program 02027 02/11/2023
Texas State Program -NELAP T104704180 09/30/2022
Virginia State Program 00106 06/30/2022
Virginia State Program -NELAP 460181 09/14/2022
Page 1 of 1 00016/22-139-0012

wQ
\iVaypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-139-0012
Client Project Description: Bi-Monthly or Monthly
1111 Pecan Ave.
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
90327 Bimonthly Aqueous 05/19/2022 15:30 05/19/2022 16:30
90327 Bimonthly Aqueous 05/19/2022 15:30 05/19/2022 16:30 200.8 WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN, Memphis,TN

•
Waypoi u t V 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Client: Heric Solutions, LLC CASE NARRATIVE
Project: Bi-Monthly or Monthly
Lab Report Number: 22-139-0012
Date: 6/13/2022
Semivolatile Organic Compounds -GC/MS Method 8270E
Sample 90327 (Bimonthly)
Analyte: 4-Terphenyl-d14
QC Batch No: V19349/V19181
Surrogate recovery is below range.

to
Iaypoi nt. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly or Monthly
Eric Donnelly Report Date : 06/14/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :05/19/2022
Indian Trail , NC 28079
Report Number:22-139-0012 REPORT OF ANALYSIS
Lab No : 90327 Matrix: Aqueous
Sample ID : Bimonthly Sampled: 5/19/2022 15:30
Test Results Units MIL DF Date/Time By Analytical
Analyzed Method
pH 7.13 s.u. 1 05/19/22 15:30 FLD FIELD
Temperature 28.3 degrees C 0.1 1 05/19/22 15:30 FLD FIELD
Arsenic <0.500 pg/L 0.500 1 06/10/22 14:43 BKN 200.8
Barium 133 pg/L 1.00 1 06/10/22 14:43 BKN 200.8
Cadmium <0.100 pg/L 0.100 1 06/10/22 14:43 BKN 200.8
Chromium 1.78 pg/L 1.00 1 06/10/22 14:43 BKN 200.8
Copper 1.24 ug/L 0.500 1 06/10/22 14:43 BKN 200.8
Lead <0.500 pg/L 0.500 1 06/10/22 14:43 BKN 200.8
Mercury(Total) <0.000200 mg/L 0.000200 1 05/23/22 16:11 EDV 245.1
Nickel <0.500 pg/L 0.500 1 06/10/22 14:43 BKN 200.8
Selenium <1.00 pg/L 1.00 1 06/10/22 14:43 BKN 200.8
Zinc <20.0 u9/L 20.0 1 06/10/22 14:43 BKN 200.8
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions MQL Method Quantitation Limit

r
O
Wavpoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly or Monthly
Eric Donnelly Report Date : 06/14/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :05/19/2022
Indian Trail , NC 28079
Report Number:22-139-0012 REPORT OF ANALYSIS
Lab No : 90327 Matrix: Aqueous
Sample ID :Bimonthly Sampled: 5/19/2022 15:30
Analytical Method: 624.1 Prep Batch(es): V19472 06/01/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Benzene <0.500 pg/L 0.500 1 06/02/22 04:31 JLB V19473
Ethylbenzene <1.00 pg/L 1.00 1 06/02/22 04:31 JLB V19473
Toluene <1.00 pg/L 1.00 1 06/02/22 04:31 JLB V19473 1
o-Xylene <1.00 pg/L 1.00 1 06/02/22 04:31 JLB V19473
m,p-Xylene <2.00 pg/L 2.00 1 06/02/22 04:31 JLB V19473
Xylene(Total) <1.00 pg/L 1.00 1 06/02/22 04:31 KCC V19473
Surrogate:4-Bromofluorobenzene 101 Limits: 74-126% 1 06/02/22 04:31 JLB V19473
Surrogate: Dibromofluoromethane 104 Limits: 75-127% 1 06/02/22 04:31 JLB V19473
Surrogate: 1,2-Dichloroethane-d4 99.0 Limits: 67-136% 1 06/02/22 04:31 JLB V19473
Surrogate:Toluene-d8 93.0 Limits: 70-130% 1 06/02/22 04:31 JLB V19473
Analytical Method: 8270E Prep Batch(es): V19181 05/26/22 10:28
Prep Method: 3510C
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <20.0 pg/L 20.0 1 05/27/22 17:07 JMV V19349
Acenaphthylene <20.0 pg/L 20.0 1 05/27/22 17:07 JMV V19349
Anthracene <10.0 pg/L 10.0 1 05/27/22 17:07 JMV V19349
Benzo(a)anthracene <10.0 pg/L 10.0 1 05/27/22 17:07 JMV V19349
Benzo(a)pyrene <10.0 pg/L 10.0 1 05/27/22 17:07 JMV V19349
Benzo(b)fluoranthene <10.0 pg/L 10.0 1 05/27/22 17:07 JMV V19349
Benzo(g,h,i)perylene <10.0 pg/L 10.0 1 05/27/22 17:07 JMV V19349 1
Benzo(k)fluoranthene <10.0 pg/L 10.0 1 05/27/22 17:07 JMV V19349
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions MQL Method Quantitation Limit

y
Vtaypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions,LLC Project Bi-Monthly or Monthly
Eric Donnelly Report Date : 06/14/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :05/19/2022
Indian Trail , NC 28079
Report Number:22-139-0012 REPORT OF ANALYSIS
Lab No : 90327 Matrix: Aqueous
Sample ID : Bimonthly Sampled: 5/19/2022 15:30
Analytical Method: 8270E PrepBatches : V19181 05 26 22 10:28
Yt � ) / /
Prep Method: 3510C
Test Results Units MOL DF Date/Time By Analytical
Analyzed Batch
Chrysene <10.0 ug/L 10.0 1 05/27/22 17:07 JMV V19349
Dibenz(a,h)anthracene <20.0 pg/L 20.0 1 05/27/22 17:07 JMV V19349
Fluoranthene <10.0 pg/L 10.0 1 05/27/22 17:07 JMV V19349
Fluorene <10.0 ug/L 10.0 1 05/27/22 17:07 JMV V19349
Indeno(1,2,3-cd)pyrene <10.0 pg/L 10.0 1 05/27/22 17:07 JMV V19349
1-Methylnaphthalene <10.0 ug/L 10.0 1 05/27/22 17:07 JMV V19349
2-Methylnaphthalene <10.0 I-ig/L 10.0 1 05/27/22 17:07 JMV V19349
Naphthalene <10.0 pg/L 10.0 1 05/27/22 17:07 JMV V19349
Phenanthrene <10.0 pg/L 10.0 1 05/27/22 17:07 JMV V19349
Pyrene <10.0 pg/L 10.0 1 05/27/22 17:07 JMV V19349
Surrogate: 2-Fluorobiphenyl 55.2 Limits: 44-119% 1 05/27/22 17:07 JMV V19349
Surrogate: Nitrobenzene-d5 60.6 Limits: 44-120% 1 05/27/22 17:07 JMV V19349
Surrogate:4-Terphenyl-d14 49.8 * Limits: 50-134% 1 05/27/22 17:07 JMV V19349
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions MQL Method Quantitation Limit

•
1�1Y
WanI,oint 449 Springbrook Rd,Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:00004
Customer Name: Heric Solutions, LLC
Report Number: 22-139-0012
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: )IRT-15 1.0 C
Shipping container/cooler uncompromised? 0 Yes 0 No
Number of coolers/boxes received J 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody (COC) present? 0 Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? 0 Yes 0 No
Sample containers intact? 0 Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No 0 N/A
Water- VOA vials free of headspace 0 Yes 0 No 0 N/A
Trip Blanks received with VOAs 0 Yes 0 No 0 N/A
Soil VOA method 5035—compliance criteria met O Yes 0 No 0 N/A
High concentration container (48 hr) r Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) [ Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: lAngela D Overcash Date &Time: 05/19/2022 17:19:32 I

---1
447 CHAIN OF CUSTODY RECORD LAB USE ONLY
Waypoint.. PAGE ( OF / QUOTE ft TOENSURE PROPER BILLING: YES NO N/A
."*".Samples INTACT upon arrival?
.-----7
ANALYTICAL Project Name: /11,--v-e..-- Received IN ICE?
449 Springbrook Road'Charlotte,NC 28217
Phone [phone] i • Fax:[phone] Short Hold Analysis (Yes) (N ) UST Project: (Yes) (No) PROPER PRESERVATIVES Indicated?
/ 'Please ATTACH any project specific reporting(QC LEVEL I II III IV) Received WITHIN HOLDING TIMES?
Client Company Name: .., CUSTODY SEALS INTACT?
...._, provisions and/or QC Requirements
Report To/Contact Name:_ Invoice To: VOLATILES rec'd W/OUT HEADSPACE?
Reporting Address:- Address: PROPER CONTAINERS used?
TEMP' Therm ICratfrK Observed
_
_ - -
Phone: Fax(Yes)(No): Purchase Order No./Billing Reference 1
TO BE FILLED IN BY CLINT/SAMPLING PERSONNEL
Email Address: Requested Due Date J 1 Day J 2 Days -1 3 Days J 4 Days L.1 5 Days Certification: NC
EDD Type: PDF Excel Other ___ -Wetting Days" J 6-9 Days J Standard 10 days ...I R1.1:11ApW°rk MuSt Be
Other N/A kr/i/ I
Site Location Name: Samples received after 1500 will be processed next business day, I
Site Location Physical Address: Turnaround time is based on business days,excluding weekends and holidays Water Chlorinated: YES NO
(SEE REVERSE FOR TERMS&CONDITIONS REGARDING SERVICES
RENDERED BY WAYPOINT ANALYTICAL,LLC TO CUENT) Samples Iced Upon Collection: YES 7_NO
— —
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
/
REMARKS
CLIENT DATE COLLECTED (SOIL, L —
.... 1- PRESERVA-
/ ID NO.
SAMPLE DESCRIPTION COLLECTED MIUTARY WATER,OR •TYPE
HOURS SLUDGE) SEE BELOW Na
—Sla
/fa IV /
. P2-•
F 1 sf!) 3
1 149C--- g m
njr /1/12/1‘ Y —I
. CCI-- 1 lit) Yet (6.
_ .
--k----- 4-- 1
- -
I I 1111 11111111 1111 III I III 1 I 11 II 22-1349-0012
__L Hem.Solutions LLC
Eli-Aiiionthly or Monthiv I II 05-19-2022
1 7 17 58
d a 441:11&El:II d 1:I' Ilfg!i•Asti41 Iv
Sampler's Signature Sampled By(Print Name)_1)11-vi2? .,. .. /.1 C Affiliation_144,11)114f 1103=111
Upon relinquishing,this Chain of Cu y is your authorization for Waypoint Analytical to proceed with the analyses as requested above.Any changes must be
Site Arrival Time:
submitted in writing to the Waypoint Analytical Project Manager.There will be charges for any changes after analyses have been initialized.Rethnill By"itt7F- Received By iSignaluie) -1-1-5 - MihtarYllours Additional Comments
g'°12-----
.•
Site Departure Time:
Rein 'led y (Signit Reenved By(Signature) Date -- — Field Tech Fee:
IRelinquished By fignaturel Roc-F:Tived For vim(Analybcal By' Mileage:
c
memo,:of Ship/twit NOTE:ALL SAMPLI COOLERS SHOUTD BE TAPED-SHUT WITH CUSTODY SEALS FOR TRAM ATION TO THE LABORATORY, OC p No
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY
SEE REVERSE FOR
J Fed EK J UPS J Hand-delivered inini AnAlytKal Feid Service J Other_ TERMS 6 CONDITIONS
NPDES: UST: G OUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: BRWNFLD LAND ILL OTHER:
...1 NC J SC U NC .1 SC ' NC JSC UNC JSC J NC '.i SC U NC LI SC L3 NC JSC UNC a SC UNC LI SC
-I LI j L3 L3 L3 U U Li ORIGINAL
.41"A IUTA I LI IC CI irvn=r•r•nce• A ....A........... Is..."to...* taVI., .ii . 4... ...ris........-.. ........ - ...-- .,_-_..•....-- •....•_•._._,..._..,____.__ .__....._ re...- •a--Jr n--.-•

EFFLUENT ANALYTICAL REPORTS
JUNE 2022

w
Waypoint 449 Springbrook Rd,Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
7/6/2022
Heric Solutions, LLC
Eric Donnelly
P.O. Box 548
Indian Trail, NC, 28079
Ref: Analytical Testing
Lab Report Number: 22-165-0063
Client Project Description: Monthly
1111 Pecan Ave.
Project Number: Permit NC0089958
Dear Eric Donnelly:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 6/14/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

•
VVavpount 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalyti ca Isom
Certification Summary
Laboratory ID: WP CNC:Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
North Carolina State Program 37735 07/31/2022
North Carolina State Program 402 12/31/2022
South Carolina State Program 99012 07/31/2022
South Carolina State Program 99012 12/31/2022
Page 1 of 1 00016/22-165-0063

1
VVaypoi 1nt, 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-165-0063
Client Project Description: Monthly
1111 Pecan Ave.
Lab No Client Sample ID Matrix Date Collected Date Received
92159 Monthly Aqueous 06/14/2022 10:55 06/14/2022 14:00
92160 Monthly-8270 PAH Aqueous 06/14/2022 10:55 06/14/2022 14:00

Yo
VVaypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 07/06/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :06/14/2022
Indian Trail , NC 28079
Report Number:22-165-0063 REPORT OF ANALYSIS
Lab No : 92159 Matrix: Aqueous
Sample ID : Monthly Sampled: 6/14/2022 10:55
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Hardness 25.0 mg/L 10.0 1 06/23/22 11:10 CLB 2340C-2011
pH 6.23 s.u. 1 06/14/22 00:00 FLD FIELD
Temperature 24.6 C 0.1 1 06/14/22 00:00 FLD FIELD
Arsenic <0.0100 mg/L 0.0100 1 06/27/22 19:16 EDV EPA-200.7
Barium 0.0522 mg/L 0.0100 1 06/29/22 10:48 EDV EPA-200.7
Cadmium <0.0020 mg/L 0.0020 1 06/27/22 19:16 EDV EPA-200.7
Chromium <0.0050 mg/L 0.0050 1 06/29/22 10:48 EDV EPA-200.7
Copper <0.0050 mg/L 0.0050 1 06/27/22 19:16 EDV EPA-200.7
Lead <0.0060 mg/L 0.0060 1 06/27/22 19:16 EDV EPA-200.7
Mercury(Total) <0.000200 mg/L 0.000200 1 06/28/22 09:55 EDV 245.1
Nickel <0.0050 mg/L 0.0050 1 06/27/22 19:16 EDV EPA-200.7
Selenium <0.0100 mg/L 0.0100 1 06/27/22 19:16 EDV EPA-200.7 j
Zinc <0.0100 mg/L 0.0100 1 06/29/22 10:48 EDV EPA-200.7
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

F
O
Waypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 07/06/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 06/14/2022
Indian Trail , NC 28079
Report Number:22-165-0063 REPORT OF ANALYSIS
Lab No : 92159 Matrix: Aqueous
Sample ID :Monthly Sampled: 6/14/2022 10:55
Analytical Method: 624.1 Prep Batch(es): V20098 06/17/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acetone <5.00 pg/L 5.00 1 06/17/22 22:03 JLB V20101
Acrolein <5.00 pg/L 5.00 1 06/17/22 22:03 JLB V20101
Acrylonitrile <5.00 pg/L 5.00 1 06/17/22 22:03 JLB V20101
Benzene <0.500 u9/L 0.500 1 06/17/22 22:03 JLB V20101
Bromodichloromethane <1.00 l g/L 1.00 1 06/17/22 22:03 JLB V20101
Bromoform <3.00 li9/L 3.00 1 06/17/22 22:03 JLB V20101
Bromomethane <2.00 pg/L 2.00 1 06/17/22 22:03 JLB V20101
Carbon Tetrachloride <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
Chlorobenzene <1.00 li9/L 1.00 1 06/17/22 22:03 JLB V20101
Chlorodibromomethane <1.00 li9/L 1.00 1 06/17/22 22:03 JLB V20101
Chloroethane <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
2-Chloroethylvinyl Ether <10.0 pg/L 10.0 1 06/17/22 22:03 JLB V20101
Chloroform <1.00 u9/L 1.00 1 06/17/22 22:03 JLB V20101
Chloromethane <1.00 lJ9/L 1.00 1 06/17/22 22:03 ]LB V20101
1,2-Dichlorobenzene <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
1,3-Dichlorobenzene <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
1,4-Dichlorobenzene <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
1,1-Dichloroethane <1.00 u9/L 1.00 1 06/17/22 22:03 JLB V20101
1,2-Dichloroethane <1.00 u9/L 1.00 1 06/17/22 22:03 JLB V20101
1,1-Dichloroethene <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
trans-1,2-Dichloroethene <2.00 lJg/L 2.00 1 06/17/22 22:03 JLB V20101
1,2-Dichloropropane <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

vv
yy
Waypoint, 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytica l.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 07/06/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 06/14/2022
Indian Trail , NC 28079
Report Number:22-165-0063 REPORT OF ANALYSIS
Lab No : 92159 Matrix: Aqueous
Sample ID :Monthly Sampled: 6/14/2022 10:55
Analytical Method: 624.1 Prep Batch(es): V20098 06/17/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
cis-1,3-Dichloropropene <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
trans-1,3-Dichloropropene <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
Ethylbenzene <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
Methylene Chloride <2.00 pg/L 2.00 1 06/17/22 22:03 JLB V20101
1,1,2,2-Tetrachloroethane <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
Tetrachloroethene <0.750 pg/L 0.750 1 06/17/22 22:03 JLB V20101
Toluene <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
1,1,1-Trichloroethane <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
1,1,2-Trichloroethane <0.500 pg/L 0.500 1 06/17/22 22:03 JLB V20101
Trichloroethene <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
Trichlorofluoromethane <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
1,2,3-Trichloropropane <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
1,2,4-Trimethylbenzene <0.500 pg/L 0.500 1 06/17/22 22:03 JLB V20101
Vinyl Chloride <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
o-Xylene <1.00 pg/L 1.00 1 06/17/22 22:03 JLB V20101
m,p-Xylene <2.00 pg/L 2.00 1 06/17/22 22:03 JLB V20101
Xylene(Total) <1.00 pg/L 1.00 1 06/17/22 22:03 KCC V20101
Surrogate: 4-Bromofluorobenzene 101 Limits: 74-126% 1 06/17/22 22:03 JLB V20101
Surrogate: Dibromofluoromethane 101 Limits: 75-127% 1 06/17/22 22:03 JLB V20101
Surrogate: 1,2-Dichloroethane-d4 96.6 Limits: 67-136% 1 06/17/22 22:03 JLB V20101
Surrogate:Toluene-d8 114 Limits: 70-130% 1 06/17/22 22:03 JLB V20101
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

1
o
's/a4POiflt 449 Springbrook Rd, Charlotte, NC 28217
, Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 07/06/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :06/14/2022
Indian Trail , NC 28079
Report Number:22-165-0063 REPORT OF ANALYSIS
Lab No : 92159 Matrix: Aqueous
Sample ID :Monthly Sampled: 6/14/2022 10:55
Analytical Method: 625.1 Prep Batch(es): V20125 06/20/22 09:52
Prep Method: 625.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Acenaphthylene <20.0 pg/L 20.0 1 06/21/22 14:51 JMV V20315
Anthracene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Benzidine <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Benzo(a)anthracene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Benzo(a)pyrene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Benzo(b)fluoranthene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Benzo(g,h,i)perylene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Benzo(k)fluoranthene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Benzoic Acid <50.0 pg/L 50.0 1 06/21/22 14:51 JMV V20315
Benzyl alcohol <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Bis(2-Chloroethoxy)methane <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Bis(2-Chloroethyl)ether <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Bis(2-Chloroisopropyl)ether <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Bis(2-ethylhexyl)phthalate <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
4-Bromophenyl phenyl ether <20.0 pg/L 20.0 1 06/21/22 14:51 JMV V20315
Butyl benzyl phthalate <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
4-Chloro-3-methylphenol <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
2-Chloronaphthalene <20.0 pg/L 20.0 1 06/21/22 14:51 JMV V20315
2-Chlorophenol <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
4-Chlorophenyl phenyl ether <20.0 pg/L 20.0 1 06/21/22 14:51 JMV V20315
Chrysene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

v•Q
Waypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 07/06/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 06/14/2022
Indian Trail , NC 28079
Report Number:22-165-0063 REPORT OF ANALYSIS
Lab No : 92159 Matrix: Aqueous
Sample ID :Monthly Sampled: 6/14/2022 10:55
Analytical Method: 625.1 Prep Batch(es): V20125 06/20/22 09:52
Prep Method: 625.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Dibenz(a,h)anthracene <20.0 N9/L 20.0 1 06/21/22 14:51 JMV V20315
Dibenzofuran <20.0 pg/L 20.0 1 06/21/22 14:51 JMV V20315
1,2-Dichlorobenzene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
1,3-Dichlorobenzene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
1,4-Dichlorobenzene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
3,3'-Dichlorobenzidine <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
2,4-Dichlorophenol <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Diethyl phthalate <20.0 pg/L 20.0 1 06/21/22 14:51 JMV V20315
Dimethyl phthalate <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
2,4-Dimethylphenol <20.0 pg/L 20.0 1 06/21/22 14:51 JMV V20315
Di-n-butyl phthalate <10.0 u9/L 10.0 1 06/21/22 14:51 JMV V20315
4,6-Dinitro-2-methylphenol <30.0 pg/L 30.0 1 06/21/22 14:51 JMV V20315
2,4-Dinitrophenol <30.0 u9/L 30.0 1 06/21/22 14:51 JMV V20315
2,4-Dinitrotoluene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
2,6-Dinitrotoluene <20.0 N9/L 20.0 1 06/21/22 14:51 JMV V20315
Di-n-Octyl Phthalate <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Fluoranthene <10.0 u9/L 10.0 1 06/21/22 14:51 JMV V20315
Fluorene <10.0 IJ9/L 10.0 1 06/21/22 14:51 JMV V20315
Hexachlorobenzene <20.0 pg/L 20.0 1 06/21/22 14:51 JMV V20315
Hexachlorobutadiene <20.0 u9/L 20.0 1 06/21/22 14:51 JMV V20315
Hexachlorocyclopentadiene <20.0 pg/L 20.0 1 06/21/22 14:51 JMV V20315
Hexachloroethane <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

w°
WaypOint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 07/06/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 06/14/2022
Indian Trail , NC 28079
Report Number:22-165-0063 REPORT OF ANALYSIS
Lab No : 92159 Matrix: Aqueous
Sample ID :Monthly Sampled: 6/14/2022 10:55
Analytical Method: 625.1 Prep Batch(es): V20125 06/20/22 09:52
Prep Method: 625.1 (Prep)
Test Results Units MIL DF Date/Time By Analytical
Analyzed Batch
Indeno(1,2,3-cd)pyrene <10.0 ug/L 10.0 1 06/21/22 14:51 JMV V20315
Isophorone <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
1-Methylnaphthalene <10.0 lJg/L 10.0 1 06/21/22 14:51 JMV V20315
2-Methylnaphthalene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Naphthalene <10.0 ug/L 10.0 1 06/21/22 14:51 JMV V20315
Nitrobenzene <10.0 ug/L 10.0 1 06/21/22 14:51 JMV V20315
2-Nitrophenol <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
4-Nitrophenol <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
N-Nitrosodiphenylamine <20.0 pg/L 20.0 1 06/21/22 14:51 JMV V20315
N-Nitroso-di-n-propylamine <20.0 Ng/L 20.0 1 06/21/22 14:51 JMV V20315
Pentachlorophenol <50.0 ug/L 50.0 1 06/21/22 14:51 JMV V20315
Phenanthrene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Phenol <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
Pyrene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
1,2,4-Trichlorobenzene <10.0 pg/L 10.0 1 06/21/22 14:51 JMV V20315
2,4,6-Trichlorophenol <20.0 ug/L 20.0 1 06/21/22 14:51 JMV V20315
Surrogate: Phenol-d5 20.8 Limits: 10-63% 1 06/21/22 14:51 JMV 625.1
Surrogate: 2-Fluorobiphenyl 52.8 Limits:49-118% 1 06/21/22 14:51 JMV V20315
Surrogate: 2-Fluorophenol 29.2 Limits: 22-84% 1 06/21/22 14:51 JMV V20315
Surrogate: Nitrobenzene-d5 49.2 Limits: 43-123% 1 06/21/22 14:51 JMV V20315
Surrogate:4-Terphenyl-d14 68.6 Limits: 49-151% 1 06/21/22 14:51 JMV V20315
Surrogate: 2,4,6-Tribromophenol 60.1 Limits: 31-144% 1 06/21/22 14:51 JMV V20315
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

r
W
NC zsa17
f%VPoInt 449 Springbrook Rd, Charlotte,
Main 704.529.6364
ANALYTICAL www.waypointanalytital.com
00004 Project ID :
Heric Solutions, LLC Project Monthly
Eric Donnelly Report Date : 07/06/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :06/14/2022
Indian Trail , NC 28079
Report Number :22-165-0063 REPORT OF ANALYSIS
Lab No : 92160 Matrix: Aqueous
Sample ID :Monthly-8270 PAH Sampled: 6/14/2022 10:55
Analytical Method: 8270E Prep Batch(es): V20128 06/20/22 09:52
Prep Method: 3510C
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <20.0 pg/L 20.0 1 06/20/22 21:57 JMV V20346
Acenaphthylene <20.0 pg/L 20.0 1 06/20/22 21:57 JMV V20346
Anthracene <10.0 ug/L 10.0 1 06/20/22 21:57 JMV V20346
Benzo(a)anthracene <10.0 pg/L 10.0 1 06/20/22 21:57 JMV V20346
Benzo(a)pyrene <10.0 pg/L 10.0 1 06/20/22 21:57 JMV V20346
Benzo(b)fluoranthene <10.0 ug/L 10.0 1 06/20/22 21:57 JMV V20346
Benzo(g,h,i)perylene <10.0 pg/L 10.0 1 06/20/22 21:57 JMV V20346
Benzo(k)fluoranthene <10.0 iig/L 10.0 1 06/20/22 21:57 JMV V20346
Chrysene <10.0 pg/L 10.0 1 06/20/22 21:57 JMV V20346
Dibenz(a,h)anthracene <20.0 pg/L 20.0 1 06/20/22 21:57 JMV V20346
Fluoranthene <10.0 ug/L 10.0 1 06/20/22 21:57 JMV V20346
Fluorene <10.0 Ng/L 10.0 1 06/20/22 21:57 JMV V20346
Indeno(1,2,3-cd)pyrene <10.0 pg/L 10.0 1 06/20/22 21:57 JMV V20346
1-Methylnaphthalene <10.0 pg/L 10.0 1 06/20/22 21:57 JMV V20346
2-Methylnaphthalene <10.0 pg/L 10.0 1 06/20/22 21:57 JMV V20346
Naphthalene <10.0 ug/L 10.0 1 06/20/22 21:57 JMV V20346
Phenanthrene <10.0 ug/L 10.0 1 06/20/22 21:57 JMV V20346
Pyrene <10.0 ug/L 10.0 1 06/20/22 21:57 JMV V20346
Surrogate: 2-Fluorobiphenyl 59.6 Limits:44-119% 1 06/20/22 21:57 JMV V20346
Surrogate: Nitrobenzene-d5 52.0 Limits:44-120% 1 06/20/22 21:57 JMV V20346
Surrogate:4-Terphenyl-d14 57.8 Limits: 50-134% 1 06/20/22 21:57 JMV V20346
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

cnvironmcnta,Inc. (C64)377-6942 .1-A) 064)877-6930
P.O. Box 16414 Creenv lle.. SC 206066 4 Cratt;rn n Cuur,. (31ver. SC 29150
Pimephales promelas 24 Hour Acute Pass/Fail Test
EPA-821-R-02-012 Method 2000
Client: HERIC SOLUTIONS
Facility:PECAN AVE
NPDES#:NC0089958
Test Date: 15-Jun-22
Laboratory ID#: T62197 APF
Test Reviewed and Approved By:
Robert W.Kelley,Ph.D. Patrick D.Timms
President QA/QC Officer
FrS�;
Certification#E87819 SCDHEC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided s les.age 1 of 4 NCDENR Certification# 022
W

Effluent Aquatic Toxicity Report Form -Acute Pass/Fail Date: 06/28/22
Facility HERIC SOLUTIONS-PECAN AVE NPDES# NC0089958 Pipe# 001 County Mecklenburg
Laboratory Performing Test ETT Environmental
X ///n Comments
Signature of Operator in Responsible Charge a /
X f
Signature of Laboratory Supervisor MAIL ORIGINAL TO: Environmental Sciences Branch
Quality
Div.
of WaterQ a y
N.C.DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
North Carolina Acute Pass/Fail Toxicity Test
Collection Date: 6/14/22 Organism Tested:
Collection Time: 1055 Pimephales promelas
Test Start Date: 6/15/22
Sample Type/Duration Control 7.8 8.2
Grab Comp Duration pH Treatment 7.3 7.8
X -_
--_ Control Sample start end
Hardness(mg/L) 83.7 Control 7.9 7.8
Spec.Cond.(pmhos) 310 471 D.O. Treatment 8.0 7.9
Chlorine(mg/L) <0.05
Sample temp.at receipt 0.4
Mortality Replicate Mean Mortality
Treatment 1 (Control) A B C D
0% 0% 0% 0% 0%
Treatment 2(Exposure) A B C D
Concentration 90% 0% 0% 0% 0% 0%
Tested
(NOTE): If mean control mortality exceeds 10%,the test is considered invalid)
Calculate using
Arc-Sine Calculated Student's t N/A PASS X
Square Root
transformed Tabular Student's t 1.94 FAIL
data (ONE TAILED)
If the absolute value of the calculated t is less than or equal
to the absolute value of the tabular t, check PASS
If the absolute value of the calculated t is greater than the
absolute value of the tabular t, check FAIL.
If all vessels within each treatment have the same response
but the treatment two response is greater than the control, check FAIL.
DEM form AT-2(8/91)
Page 2 of 4

24 Hour Acute Toxicity Test
Test Method:EPA 821 R-02-012; Method 2000 Pimephales promelas
Client: HERIC Sample ID:PECAN AVE Lab ID/7: T62197 API'
Start Date: 06/15/22 Time: 04:00 PM Set By: AM
End Date: 06/16/22 Time: 04:09 PM Ended By: JZ
Test Vessel Test Solution Volume Incubator Transfer Volume Dilution Water
Fathead Minnows 500 mL plastic cup 200 mL #1 0.5 mL MHSF
Randomization pattern per SOP 'Neonates from common holding vessel !Light: 50-100 11-c. 16 hr light/8 hr dark
TEST ORGANISMS
for Ceriodaphnia dubia Comments:
Date Removed: Between: and: FISH HATCHED ON 6/2/22 BTW 1500-1630 ET
Pimephales promelas Source: ABS lays old: 13
Mysidopsis bahia Source: Days old:
Test Organisms Pre Fed by: AM Time: 1300
MORTALITY DATA
Conc. Initial# Cumulative Mortality rin:,l Initial Final
Cond/ Cond/
Rep. organisms 24 sr a 96 m temp D.O pel Salini By: Temp D.O. pH Salini By.
A 10 0
Control B 10 0
C 10 0
D 10 0 0% 24.7 7.9 7.8 AM 24.6 7.8 8.2 JZ
A 10 0
90.0% B 10 0
C 10 0
D 10 0 0'%n 25.(1I (0 7.3 AM 24.6 7.9I 7.8 JZ
A
B
C
D I I
A
B
C
D 1
A
B
C
D 1
A
B
C
D
A
B
•
C
D C I m,:'I I I I'I'l I - `( I Ing 1 1 I Iu1i 1
Page 3 of 4

1
CHAIN OF CUSTODY RECORD
r & „ gfErg� F
PO Box 16414,Greenville,SC 29605-7414 f- o_
[phone], [phone] Fax[phone]
Shipping Address:4 Craftsman Ct,Greer,SC 296650
WWW.EYTENVIRCNMEN-AL.COM
l c .uer3 y'/a Program Container, Prescnativc Par2meters
Facility:
f f
- - - Whofc Emucr.t TDSiCir F -
State: NPDES t F
( Acute Chronic Test Organisms
Jji ,j rm
= I— — 'o o r
(Comoosiie only) (Crab or Composite) — o U
U ` O U _ J [_ a — I 7
Sign,and Print below i - = co ^ s=HCL = - °- _ 2 E s
the dotted]ire U .� U 14N0.5 ''_ ^ 3 �' • 'o 7
SAMPLE ID U C°mpotttc SL rt Date Time Sample Collection Dotc Time Collected b)• U up [j Z C U 0 U ^ - " y = t -
J _ q 6=other < U U iJ 0 _ 2 :n- _ iJ r I Z I Ch=mie_i Analysis a Other
b,`'�'�— �� ��- ion— -,--- 1----- Lob ,V ems; ZI��-
to
CD
O_
A f
•
i
Special Instructions:
'Sample Custody Transfer Record 1
Secure Receipt Sample
Date Time Relinqu led By/Organization Received By/Organization Area Temp`C Preserved?
O ilk ›i /° -/ 1� /bid
o
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONTTORIArG PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport roust be between For toxicity resrin=the sample must ft-i be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volut 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bass. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. --- Sample-may-not-be-used-after -hou from szarpie-collection.-
-
Proportional:As per instructions in NPDES permit.

'YYQ
Wapont 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:00004
Customer Name: Heric Solutions, LLC
Report Number: 22-165-0063
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: DIRT-15 1.0C
Shipping container/cooler uncompromised? # Yes 0 No
Number of coolers/boxes received J 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No # Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody(COC) present? 0 Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? 0 Yes 0 No
Sample containers intact? 0 Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? # Yes 0 No
Cooler temperature in compliance? J Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0No 0 N/A
Water- VOA vials free of 0 No 0 Yes O heads aceN/A
p
Trip Blanks received with VOAs 0 Yes # No 0 N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No J N/A
(— High concentration container (48 hr) r Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) r Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Angela D Overcash Date &Time: 06/30/2022 07:24:04

tA.0
vv CHAIN OF CUSTODY RECORD LAB USE ONLY
WaYPOint- PAGE 4.OF 1 .,,..(SIOTE 0 TOENSURE PROPER BILLING: ,.._ Samples INTACT upon arrival? YES NO NA
,e,..
ANALYTICAL Project Name: i ...‘?1:—. Ala 11111424 Received IN ICE? .."""
449 Springbrook Road•Charlotte,NC 28217 PROPER PRESERVATIVES indicated? ..""F
Phone [phone] . Fax:[phone] Short Hold Anal sis (Yes) (No) UST Projec : (Yes) (No) 1 —
*Please ATTACH any project specific reporting(QC LEVEL I II III IV) Received WITHIN HOLDING TIMES? ...••••
7".
Client Company Name: 4L . .--- provisions and/or QC Requirements CUSTODY SEALS INTACT?
Report To/Contact Name: Invoice To: VOLATILES rec d'MOUT HEADSPACE? .„/-7
Reporting Address: Address: PROPER CONTAINERS used? ---
TEMP: Therm 1Cla44 Observed E3 .C/Corr..4. 2C
Phone: Fax(Yes)(No): Purchase Order No.fBilling Reference TO BE FILLED IN BY CUENJISAMPUNG PERSONNEL
Email Address: Requested Due Date J 1 Day ...12 Days J 3 Days la 4 Days J 5 Days
u Fptirr4Npork eMiust Be Certification: NC_ SC
EDD Type: PDF__Excel Other, "Working Days" J 6-9 Days J Standard 10 clays
Ot her N/A
Site Location Name: Samples received after 15:00 will be processed next business day.
Site Location Physical Address: Turnaround time is based on business days,excluding weekends and holidays. Water Chlorinated: YES _ NO
(SEE REVERSE FOR TERMS 8 CONDITIONS REGARDING SERVICES
RENDERED BY WAYPOINT ANALYTICAL,LLC TO CLIENT) Samples Iced Upon Collection: YES NO
— -T- -'-'
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
CLIENT DATE (SOIL, _
SAMPLE DESCRIPTION COLLECTED 'MILITARY COLLECTED VVATER,OR ,TypE TIVES ifer:171/ ///.///
HOURS SWOOP SE PRESERVA-
REMARKS ID NO.
E BELOW No. SIZE
4.) Iiit7 fr
( cl)(3 //At?
Y
J
1
/WO Mil/S-
Y
Y _
11111111111111111111111111111111111111°C°°422-165-C°63
—
Herm Solutions LLC 06-14-2022
Monthly 15 40.36
I
PRESS DOWN FIRMLY-2 COPIES
.-
.7ty r...... .114_,
Samplers Signature_I
Sampled By(Print Name) i 1/1?AWLS__ Affiliation I . _.,..e, . 1111= 2111
Upon relinquishing,this Chain of Custody is your authorization for Waypoint Analytical to proceed with the analyses as requested abov-.Any changes must be
:
su d in writing to the Waypoint Analytical Project Manager There will be charges for any changes after analyses have been initialized. Sib Anival Thee
Received By:(Sfgnature) Date MtittarY/Rours Additional Comments:
c-- 6 /1"(-4, Site Departure Time:
1
Reit yi FS ) Received By:(Svnaturth Date
D// 22 Field Tech Fee:
Relinquished By'(Sae) Recta, aypoint Analyital By — Oat Mileage:
(pH I/GO 141 /Ago
Metnod of Shtpment NOTE:ALL SAMPLE COOL TAPED COOLS SHOULD BE TAP SHUT SEALS NSPO TO E LABORATORY. C roup No. / f
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COG UNTIL RECEIVED AT THE tAitilWATORY.
SEE REVERSE FOR
J Fed Ex J UPS a Hancroetivered aytxiint Anatywal Feed Service J Other__ TERMS&CONDITIONS
-----
NPDES: UST: G NDWATER, DRINKING WATER: SOLID WASTE: RCRA: ElliNNFLD LANDFILL OTHER:
Li NC,..I SC J NC USC Li NC USC s,,.1 NC USC J NC USC UNC USC UNC USC LI NC USC L--1 NC USC
t..1 - J U J J Li U U U OF,ZIGINAL

1.77' F-1!"''
CHAIN OF CUSTODY RECORD
I
O'CI 18414,Greetrnue,S'60S-7414 1
f
[phone], [phone] Fax[phone]
Shipping Addrass'4 Craftsman Ct,Greer,SC 2965E
WW' ,LTYCr+VInoMMCNTAL.COM
Client: - -
‘,/..6.4.,
C. � � Program Containers Preservative Parameters {
Facility: ' whole Err.mct Tonicity
State: \I'DES t4: ( lcnrc Chronic Tut Oreanisns
Ya'`�C: !f ii N V
(C c onnocite only) ` (Grab or Composite) <`J o 2.r2 t,7 _
li
Sign,and Print below =o -- ' HCt. = ' mac-.a = = >li <
V the dotted line 3 F U u u !i o: '2
E 4zoti `o n _� _ P. _ �
SAMPLE ID V Camposne Stan Date Time Sample Coticriian 0xM Time Collected by U ✓1 tit 2. a a. C? } j $ 2n�c < < t� CJ UJ 3 b : I .:. U = �? &
h . 6.OAu r- 7 { ? Chemical AnafysisOther
� /I � i
I _ - 4
! j
1 Henn,Solutions.LuC 06 t4 2022 --"
I Monthly 15 40 36
Speer&Instructions: — M .._._. _..,... .._-_..>._,_.._._.........u.........,t.o�....._�..�.. e !. f
Sample Custody Transfer Record I Secure Receipt Sample
--p--- 1
Date Time RelincLu seed By/Organization Received By/Oreanization i.Area Temo'C Preserved?
r- 76--/- ifr---v - 1
1 ---1- 1l
1 1
, , ,_ _ _ _ _____
____,
I__ _......_
COMPOSITE SAMPLING PROCEDUR S TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must firs:be used within 36 hours
Time Proportional: l sample each hour for 24 hours.Equal volu:0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed begs. of sample collection(completion of composite sample),
(or at minimum I sample every 4 hours over 24 hours. !Sample may not be used after 72 hours from sample collection,
[Flow Proportional:As per instructions in NPDES permit

Y 1/Q
Waypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
7/13/2022
Heric Solutions, LLC
Eric Donnelly
P.O. Box 548
Indian Trail, NC, 28079
Ref: Analytical Testing
Lab Report Number: 22-180-0011
Client Project Description: Bi-Monthly
1111 Pecan Ave.
Project Number: Permit NC0089958
Dear Eric Donnelly:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 6/29/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

w
V/aypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
North Carolina State Program 37735 07/31/2022
North Carolina State Program 402 12/31/2022
South Carolina State Program 99012 07/31/2022
South Carolina State Program 99012 12/31/2022
Page 1 of 1 00016/22-180-0011

V/aypoi lit 449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 22-180-0011
Client Project Description: Bi-Monthly
1111 Pecan Ave.
Lab No Client Sample ID Matrix Date Collected Date Received
93220 Bimonthly EFF Aqueous 06/29/2022 10:00 06/29/2022 12:15

•
\A/aypoint 449 Springbrook Rd,Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Client: Heric Solutions, LLC CASE NARRATIVE
Project: Bi-Monthly
Lab Report Number: 22-180-0011
Date: 7/12/2022
Metals Analyses Method 200.8
Analyte: Selenium
QC Batch No: V21126/V21056
ICV failed high. Sample concentration BRL. Result not affected.
Mercury Method 245.1
Sample 93284 (130P GW-1)
Analyte: Mercury
QC Batch No: V21053/V21038
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 93284 (130P GW-1)
Analyte: Mercury
QC Batch No: V21053/V21038
Relative Percent Difference (RPD)for the duplicate analysis was outside of the allowable QC limits.

w
V/aypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 07/13/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :06/29/2022
Indian Trail , NC 28079
Report Number:22-180-0011 REPORT OF ANALYSIS
Lab No : 93220 Matrix: Aqueous
Sample ID :Bimonthly EFF Sampled: 6/29/2022 10:00
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
pH 6.15 s.u. 1 06/29/22 10:00 FLD FIELD
Temperature 24.5 C 0.1 1 06/29/22 10:00 FLD FIELD
Arsenic <1.00 pg/L 1.00 1 07/11/22 18:09 EDV 200.8
Barium 27.7 pg/L 5.00 1 07/11/22 18:09 EDV 200.8
Cadmium <1.00 pg/L 1.00 1 07/11/22 18:09 EDV 200.8
Chromium <1.00 pg/L 1.00 1 07/11/22 18:09 EDV 200.8
Copper <2.00 pg/L 2.00 1 07/11/22 18:09 EDV 200.8
Lead 1.07 pg/L 1.00 1 07/11/22 18:09 EDV 200.8
Mercury(Total) <0.000200 mg/L 0.000200 1 07/08/22 18:31 EDV 245.1
Nickel <5.00 pg/L 5.00 1 07/11/22 18:09 EDV 200.8
Selenium <5.00 pg/L 5.00 1 07/11/22 18:09 EDV 200.8
Zinc 12.9 pg/L 10.0 1 07/11/22 18:09 EDV 200.8
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

1
vv
//aypoint, 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanaiytical.com
00004 Project ID :
Heric Solutions, LLC Project Bi-Monthly
Eric Donnelly Report Date : 07/13/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received : 06/29/2022
Indian Trail , NC 28079
11
Report Number:22-180-0011 REPORT OF ANALYSIS
Lab No : 93220 Matrix: Aqueous
Sample ID : Bimonthly EFF Sampled: 6/29/2022 10:00
Analytical Method: 624.1 Prep Batch(es): V21045 07/08/22 09:00
Prep Method: 624.1 (Prep)
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Benzene <0.500 ug/L 0.500 1 07/08/22 15:01 JLB V21046
Ethylbenzene <1.00 lJg/L 1.00 1 07/08/22 15:01 JLB V21046
Toluene <1.00 pg/L 1.00 1 07/08/22 15:01 JLB V21046
o-Xylene <1.00 ug/L 1.00 1 07/08/22 15:01 JLB V21046
m,p-Xylene <2.00 Ng/L 2.00 1 07/08/22 15:01 JLB V21046
Xylene(Total) <1.00 pg/L 1.00 1 07/08/22 15:01 V21046
Surrogate:4-Bromofluorobenzene 101 Limits: 74-126% 1 07/08/22 15:01 JLB V21046
Surrogate: Dibromofluoromethane 100 Limits: 75-127% 1 07/08/22 15:01 JLB V21046
Surrogate: 1,2-Dichloroethane-d4 89.0 Limits: 67-136% 1 07/08/22 15:01 JLB V21046
Surrogate:Toluene-d8 96.6 Limits: 70-130% 1 07/08/22 15:01 JLB V21046
Analytical Method: 8270E Prep Batch(es): V20731 06/30/22 09:55
Prep Method: 3510C
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Acenaphthene <20.0 pg/L 20.0 1 06/30/22 23:04 JMV V20814
Acenaphthylene <20.0 pg/L 20.0 1 06/30/22 23:04 JMV V20814
Anthracene <10.0 pg/L 10.0 1 06/30/22 23:04 JMV V20814
Benzo(a)anthracene <10.0 pg/L 10.0 1 06/30/22 23:04 JMV V20814
Benzo(a)pyrene <10.0 iig/L 10.0 1 06/30/22 23:04 JMV V20814
Benzo(b)fluoranthene <10.0 pg/L 10.0 1 06/30/22 23:04 JMV V20814
Benzo(g,h,i)perylene <10.0 pg/L 10.0 1 06/30/22 23:04 JMV V20814
Benzo(k)fluoranthene <10.0 pg/L 10.0 1 06/30/22 23:04 JMV V20814
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

i
449 Springbrook Rd, Charlotte, NC, Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00004 Project ID :
Heric Solutions,LLC Project Bi-Monthly
Eric Donnelly Report Date : 07/13/2022
P.O. Box 548 Information : 1111 Pecan Ave. Received :06/29/2022
Indian Trail , NC 28079
Report Number:22-180-0011 REPORT OF ANALYSIS
Lab No : 93220 Matrix: Aqueous
Sample ID :Bimonthly EFF Sampled: 6/29/2022 10:00
Analytical Method: 8270E Prep Batch(es): V20731 06/30/22 09:55
Prep Method: 3510C
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Chrysene <10.0 pg/L 10.0 1 06/30/22 23:04 JMV V20814
Dibenz(a,h)anthracene <20.0 pg/L 20.0 1 06/30/22 23:04 JMV V20814
Fluoranthene <10.0 pg/L 10.0 1 06/30/22 23:04 JMV V20814
Fluorene <10.0 ug/L 10.0 1 06/30/22 23:04 JMV V20814
Indeno(1,2,3-cd)pyrene <10.0 pg/L 10.0 1 06/30/22 23:04 JMV V20814
1-Methylnaphthalene <10.0 ug/L 10.0 1 06/30/22 23:04 V20814
2-Methylnaphthalene <10.0 pg/L 10.0 1 06/30/22 23:04 JMV V20814
Naphthalene <10.0 pg/L 10.0 1 06/30/22 23:04 JMV V20814
Phenanthrene <10.0 pg/L 10.0 1 06/30/22 23:04 JMV V20814
Pyrene <10.0 pg/L 10.0 1 06/30/22 23:04 JMV V20814
Surrogate: 2-Fluorobiphenyl 74.4 Limits: 44-119% 1 06/30/22 23:04 JMV V20814
Surrogate: Nitrobenzene-d5 61.2 Limits: 44-120% 1 06/30/22 23:04 JMV V20814
Surrogate:4-Terphenyl-d14 63.8 Limits: 50-134% 1 06/30/22 23:04 JMV V20814
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

•
vv
Wa4pOiflt . 449 Springbrook Rd,Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:00004
Customer Name: Heric Solutions, LLC
Report Number: 22-180-0011
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: )IRT-15 2.0 C
Shipping container/cooler uncompromised? 0 Yes 0 No
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody(COC) present? 0 Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? 0 Yes 0 No
Sample containers intact? 0 Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No 0 N/A
Water- VOA vials free of headspace 0 Yes 0 No 0 N/A
Trip Blanks received with VOAs 0 Yes 0 No 0 N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No j N/A
High concentration container (48 hr) r Low concentration EnCore samplers (48 hr)
r High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: lAdam Crouch Date & Time: 06/29/2022 14:20:04

VVaypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529,6364
ANALYTICAL www.waypointanalytical,com
Kit ID: 184982 CHAIN-OF-CUSTODY
Initiated By: Angela Overcash
Initiated Date: 4/25/2022
I Project Comment Lab Sampling Event
I
Company Name Company Number Client Project Manager/Contact Purchase Order Number
Heric Solutions,LLC 00004 Heric Solutions,LLC
Site Name Project Number �t Method of Shipment
D RUSH—Additional charges apply �t
Fed Ex u UPS USPS
jspecial Detection limits(s) Courier f Client Drop Off
Pecan Ave.-BiMonthly Date Results Needed Other
LIMS Project ID Project Manager Phone a Project Manager Email Site/Facility ID#
980-721-2841
Grab/ n of I
Date Time Sample ID matrix Comp Cont Container Type Preservation Analyses
HNO3-Nitric
kg/..-2z v 0 G -2 , GU c 1 Plastic-250mL acid Metals l t�
I :QU 2 Amber Glass-Liter NONE 8270PAH
j 1
I
Clear Glass Vial- • HCL
AQU 3 40mL Hydrochloric 624
Acid
III 1111 Ill I I Ill11111It 1I I :C�:„
Hew;Solutions LLr 14 so
Bi MinttiN
(WO Field Readings
Date/Time 29 2. - Initials ( ''' pH 'r /.J
Temp I� Re Cl = Flow DO
For Laboratory Use Only Sampled by(Name-Print) Client Remarks/Comments
Ice Custody Lab Comments /7
(�,✓r / C
Seals Relinquished by:(SIGNATURE) Date
�� Time Received by:(SIGNATURE) Date Time
rIN y \ 6,-a a. /?/5"
elinquish d by:(SIGNATURE) Date Time Received by:(SIGNATURE) Date Time
Blank/Cooler Temp
WV t Relinquished by:(SIGNATURE) Date Time Received by:(SIGNATURE) Date Time
9...,0`C.