WQ0018087_Monitoring - 07-2022_20220729

of.
DWR - NonDischarge Monitoring Report Submittal •4
NORTH CAROLINA
E Mranmenlcl Quaffly
Monitoring Report Submittal
..............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Permit Number#* WQ0018087
Name of Facility:* DAK Americas LLC-Cape Fear Site
Month:* July Year:* 2022
Report Information
Type* Upload Document*
GW-59 Semiannual Monitoring Well 5.61MB
Report.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1,NDAR-2,NDMLR,GW-59).
Confirmation Email Address:* [e-mail]
Name of Submitter:* Phyllis H.Simmons
Signature: �7�
2".a 9y. ii rweevre!
Date of submittal: 7/29/2022
This will be filled in automatically
Initial Review
..............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Reviewer: Gerald,Wanda

Is the project number correct?* WQ0018087
Is the monitoring report accepted?* - Yes No
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 8/16/2022

DAK Americas
July 28, 2022
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
Subject: Permit No. WQ00I 8087
Cape Fear Manufacturing Facility
Surface Disposal of Class B Residuals (Dedicated)
Brunswick County
Dear Division of Water Resources:
Enclosed please find:
1. Two copies of Compliance and Monitoring Form (GW-59) for the 6 wells
associated with the Sludge Disposal Unit.
2. Laboratory analysis for these same wells.
3. Compliance Report Form GW-59a
4. Summary of the Groundwater Monitoring Results
As shown in the summary, some of the results in the monitoring wells are above the
permit limits. However, these results remain consistent with previous results and most
results show decreases in concentration. The regional office has received this data.
No additional actions are planned at this time.
If additional information is needed, please feel free to contact either myself on 910-371-
5232 or Larry Young on 910-264-2564.
Sincerely yours,
i47 c- -,
Penny C. Mahoney
Sustainability Director
DAK Americas LLC
DAK Americas LLC • 1430 Commonwealth Drive, Suite 305• Wilmington, NC 28403
910-371-4863(Phone) • 910-371-4456(Fax)
www.dakamericas.com

GW-59A COMPLIANCE REPORT FORM Permit# k,1/Q 00 iso9 7
(Submit one each monitoring period wills GW-59 forms.)
Enter date monitoring results were due. ( 7/30/2022 ) Will this monitoring report(GW-59 and GW-59A) YES NO
be submitted after the established due date? x
2 Was any required information missing on the GW-59 report forms? YES
IF the answer to question 1 or 2 is"YES", list in the space provided below the well identification number(s)and
explain the problems encountered in obtaining the required information.
3 Are any of the monitor bells in need of repair or maintenance(damaged easing,unlocked or missing cap,missing YES NO
identification plate,area overgrown,etc.)?If the answer is "Yes", contact the Regional Office for guidance. X
4 Are any monitored constituents equal to or above the established standards? 1'XS NO
If the answer to question 4 is "NO'', skip to section 8.
If the answer to question 4 is "YES"list the affected wells individually with constituent(s)and concentration(s)
exceeding standards in the space provided below:
See attached summary of groundwater results.
5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO
same constituent(s)in the same well(s)in the last two years? X
if the answer to question 5 is 'NO", skip to section 8.
If the answer to question 5 is "YES'; list in the space provided below, each well with constituent(s)exceeding
standards, concentration(s)reported, and sample collection date for each occurrence(for the last two years).
See attached summary of groundwater results.
6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO
X
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly
located; contact the Regional Office.
7 Is the permittee implementing previously approved actions required by the Division involving this YES NO
groundwater quality problem? X
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days;an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines, and/or penalties.
The regional office has previously asked us to continue to sample per the permit.
8 The person completing this portion(GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report(Compliance Report GW-59A)is true and complete to the best of my knowledge.
7/28/2022
Signature of Permittee(or Authorized Agent) Date
G1V-59A 12/8/2003

Permit MW-2A MW-213"" MW-2C"
Parameter Limit Units Dec-16 Dec-19 Dec-21 Dec-16 12/15 Rspl Jun-17 Dec-17 Dec-18 Dec-19 Dec-20 Jun-21 Jun-22 Dec-16 Dec-17 Dec-18 Dec-19 Dec-20 Jun-21 Jun-22
Ammonia Nitrogen 1.5 mg/I 12.0 62.5 83.5 47.9 84,3 37.9 53.5 32.9 18.0 40.5
Total Dissolved Solids 500 mg/1 827 509 632 673 727 600 692 845 753 588 597 568 504 744 621
Nitrate 10 mg/1 14.3 10,8 21.2 15.5
Arsenic 0.01 mg/I 0.017 0.02 0.02 0.02 0.016
Cobalt' 6.001 mg/I 0.002 0.022 0.013 0.021 0.019
pH 5.5 - I 5.13 5.31
Permit MW-2D' MW-26 MW-3A'"'
Parameter Limit Units_ Dec-16 12/16 Rspl Jun-17 Dec-17 Dec-18 Dec-19 Jun-21 Jun-22 Dec-16 Dec-17 Dec-18 Dec-19 Dec-20 Jun•21 Dec-21 Jun-22 Jun-22
Ammonia Nitrogen 1.5 mg/I 157 12.8 96.4 142 80.5 45.8 57.3 38.8 9.5 11.0 8.5 5.5 3.3 B.4 3.3
Total Dissolved Solids 500 mg/I 678 846 532 ,
Arsenic 0.01 mg/I D.02 0.021
Cobalt` 0.001 mg/I 0,063 0.003 _ 0.005 0.004 0.003
pH 5.5 i 5.38
.New limit in 2020 permit sa Dry in December,2021 *''Background Well
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Restricted Internal Use

SUBMIT FORM ON YFLLOW PAPER ONLY
Mail original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: and 1 copy to;DIVISION OF WATER QUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:{919)733-3221
FACILITY INFORMATION Piease Print Clearly orType PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington NC 28403 County Brunswick ❑ Lagoon ❑Remediation: Infiltration Gallery
❑ Spray Field ❑Remediation:
Contact Person: Larry Young Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Down gradient/Monitoring Well#2A No. of wells to be sampled: 6 E Water Source Heat Pump ©Other:Surface Disposal Res.Sol
(fmnm Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2A Date sample collected: 06/07/22 FIELD ANALYSES: WAS
Well Depth: 13.0 ft. Well Diameter: 2.0 in. pH 6.7 units Temp. 19.0 °C DRY at
Depth to Water Level: 7.3 ft. below measuring point Screened Interval: 3.0 ft. to 13-0 ft. Spec.Cond. I.Mhos time of
sampling,
Measuring Point is 1.92 ft. above land surface Relative M.P. Elevation: 20.39 ft. Odor None check
Volume of water pumped/bailed before sampling: 12 gallons Appearance Clear here:
Samples for metals were collected unfiltered: ®YES ❑ NO and field acidified: ®YES ❑NO
LABORATORY INFORMATION
Date sample analyzed: 06/07/22-06/20/22 Laboratory Name: Envirochem Certification No. 37729
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N <0.02 mg/I Pb-Lead <0.01 mg/I
Coliform: MF Fecal 11 00ml Nitrate(NO3)as N 0.31 mg/I Zn-Zinc <0.01 mg/I
Coliform: MF Total 1100m1 Phosphorus:Total as P <0.04 mg/I
{Note: use MPN method For highly turbid samples} Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 279 mg/I Al-Aluminum mg/I Cobalt-0.001 mg/I
pH (when analyzed) 6.5 units Ba-Barium mg/I Selenium-<0.01 mg/I
TOC mg/I Ca-Calcium mg/I
Chloride 10 mgll Cd-Cadmium <0.001 mg/l
Arsenic <0.01 mgll Chromium:Total <0.01 mg/I
Grease and Oils mg/I Cu-Copper <0.01 mg/I ORGANICS:(by GC, GC/MS, HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury <0.0002 mg/I Report Attached? ❑ Yes(1) HI No(0)
Specific Conductance 1.tMhos K-Potassium mg/I VOC , method#
Total Ammonia 0.8 mgll Mg-Magnesium 2.82 mg/I _, method#
(Ammonia Nitrogen,NH3as N:Ammonia Nitrogen,Total)
Mn-Manganese mg/I , method#
TKN as N_ mg/I Ni-Nickel <0.01 mg/I , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mgtL VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,.accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DM-certified laborator . I am aware that there are significant•enalties for submitting false information,including the•ossibiii a;fines and imprisonment fo knowing violations.
Penny C. Mahoney- Director of Sustainability and Operations Supp ./. L, <` /, 7/'f/ .
Permittee(or Authorized Agent)Name and Title-Please print or type Sgnature of Permitte (or Authorized Agent) ,Date)
GW-59 Rev, 1/2007 ✓"

SUBMIT FORM ON YFI I OyV PAPER ONLY
Mail original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: and 1 Co to: DIVISION OF WATER QUALITY.1NFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please Pont CreartyorType PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name{if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Dr, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington ""'"' NC 28403 County Brunswick ❑ Lagoon E Remediation: Infiltration Gallery
❑ Spray Field E Remediation:
Contact Person: Larry Young Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Down gradient/Monitoring Well#2B No. of wells to be sampled: 6 ❑ Water Source Heat Pump ©Other:Surface Disposal Res.Sol
[from Permd}
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2B Date sample collected: 06/07/22 FIELD ANALYSES: WAS
Well Depth: 13ft. Well Diameter: 2.0 in. pH 6.6 units Temp. 20.2 °C DRY at
time of
Depth to Water Level: 8.2 ft. below measuring point Screened Interval: 3 ft. to 13 ft. Spec.Cond. pMhos sampling,
Measuring Point is - _ 2.9 ft. above land surface Relative M.P. Elevation: 24 ft. Odor None check
Volume of water pumped/bailed before sampling: 12 gallons Appearance Clear here:
Samples for metals were collected unfiltered: E YES ❑ NO and field acidified: ®YES E NO
LABORATORY INFORMATION
Date sample analyzed: 06/07/22-06/13/22 Laboratory Name: Envirochem Certification No. 37729
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N 0.07 mg/I Pb-Lead <0.01 mg/I
Coliform: MF Fecal /100m1 Nitrate(NO3)as N 0.33 mg/I Zn-Zinc <0.01 mg/I
Coliform: MF Total /100m1 Phosphorus:Total as P 0.11 mg/I
(Note: use MPN method for highly turbid samplesy Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 845 mg/I Al-Aluminum mg/I Cobalt-0.013 mg/I
pH(when analyzed) 6.6 units Ba-Barium mg/I Selenium-<0.01 mg/I
TOC mg/I Ca-Calcium mg/I
Chloride 15 mg/I Cd-Cadmium <0.001 mg/I
Arsenic 0.016 mg/I Chromium:Total <0.01 mg/I
Grease and Oils mg/l Cu-Copper mg/I ORGANICS:{by GC,GC/MS, HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury <0.0002 mg/I Report Attached? ❑ Yes(1) ® No{0)
Specific Conductance µMhos K-Potassium mg/I VOC , method#
Total Ammonia 40.5 mg/I Mg-Magnesium 8.92 mg/I , method#
(Ammonia Nitrogen,NH,as N.Ammonia Nitrogen.Total)
Mn-Manganese mg/I , method#
TKN as N mg/I Ni-Nickel <0.01 mg/I , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWQ-certified laborato . I am aware that there are significant.enalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
Penny C. Mahoney-Director of Sustainability and Operations Supp I�w, ,�,I,® ,-- 2,
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of P= Ettee(or Aut ori'zed ,gent) ;Date)
GW-59 Rev. 1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: and 1 copy t0:,DIVISION OF WATER QUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington NC 28403 County Brunswick ❑ Lagoon ❑Remediation: Infiltration Gallery
` '"' ❑ Spray Field ❑Remediation:
Contact Person: Larry Young Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Down gradient/Monitoring Well#2C No. of wells to be sampled: 6 ❑ Water Source Heat Pump ©Other:Surface Disposal Res.Sol
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2C Date sample collected: 06/07/22 FIELD ANALYSES: WAS
Well Depth: 13ft. Well Diameter: 2.0 in. pH 5.31 units Temp. 19.0 °C DRY at
Mhos time of
Depth to Water Level: 7.8 ft. below measuring point Screened Interval: 3 ft. to 13 ft. Spec.Cond. a sampling,
Measuring Point is 3.05 ft. above land surface Relative M.P. Elevation: 25 ft. Odor None check
Volume of water pumped/bailed before sampling: 10 gallons Appearance Muddy here:
Samples for metals were collected unfiltered: ®YES ❑NO and field acidified: ®YES ❑NO
LABORATORY INFORMATION 37729
Date sample analyzed: 06/07/22-06/15/22 Laboratory Name: Envirochem Certification No. _
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N 0.07 mg/I Pb-Lead 0.015 mg/I
Coliform: MF Fecal 1100m1 Nitrate(NO3)as N 1.81 mg/I Zn-Zinc 0.047 mg/I
Coliform: MF Total /100m1 Phosphorus:Total as P 1.45 mg/I
(Note. Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 621 mg/I Al-Aluminum mg/I Cobalt-0.019 mg/I
pH(when analyzed) 5.1 units Ba-Barium mg/I Selenium -<0.01 mg/I
TOC mg/I Ca-Calcium mg/I
Chloride 8 mg/I Cd-Cadmium <0.001 mg/I
Arsenic <0.01 mg/I Chromium:Total 0.028 mg/I
Grease and Oils mg/I Cu-Copper 0.016 mg/I ORGANICS:(by GC,GC/MS, HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury <0.0002 mg/I Report Attached? ❑ Yes(1) ® No(0)
Specific Conductance µMhos K-Potassium mg/I VOC ,method#
Total Ammonia 0.7 mg/I Mg-Magnesium 12.9 mg/I , method#
(Ammonia Nitrogen,NH,as N:Ammonia Nitrogen,Total)
Mn-Manganese mg/I , method#
TKN as N mg/I Ni-Nickel 0.021 mg/I , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWQ-certified taboreto . I am aware that there are significant penalties for submitting false information,including the•ossibility of fines and imprisonment for knowing violations.
Penny C. Mahoney Director of Sustainability and Operations Supp ' , ,�� ti
IMMIIMMII. P., F, '
Permittee(or Authorized Agent)Name and Title-Please print or type - Signature of P- rr t ee(or Authorize*Agent) (D-te)
GW-59 Rev. 1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM and 7 copy to: 617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone]
FACILITYJNFORMAT!ON Please Print Clearly or Type PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington NC 28403 County Brunswick ❑ Lagoon ❑Remediation: Infiltration Gallery
❑ Spray Field ❑Remediation:
Contact Person: Larry Young Telephone#: [phone] ElRotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Down gradient/Monitoring Well#2D No.of wells to be sampled: 6 ❑ Water Source Heat Pump Ni Other:Surface Disposal Res.Sol
(from Perm()
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2D Date sample collected: 06/08/22 FIELD ANALYSES: WAS
Well Depth: 13 ft. Well Diameter: 2.0 in. pH 6.3 units Temp. 20.6 °C DRY at
time of
Depth to Water Level: 7.2 ft. below measuring point Screened Interval: 3 ft. to 13 ft. Spec.Cond. uMhos sampling,
Measuring Point is 3.0 ft. above land surface Relative M.P. Elevation: 22 ft. Odor None check
Volume of water pumped/bailed before sampling: 10 gallons Appearance Cloudy here:
Samples for metals were collected unfiltered: ®YES ❑ NO and field acidified: ®YES ❑NO
LABORATORY INFORMATION
Date sample analyzed: 06/08/22- 06/21/22 Laboratory Name: Envirochern Certification No. 37729
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N_ 0.07 mg/I Pb-Lead <0.01 mg/I
Coliform: MF Fecal /100m1 Nitrate(NO3)as N 0.52 mg/I Zn-Zinc 0.032 mg/I
Coliform: MF Total /100m1 Phosphorus:Total as P 0.18 mg/I
(Note, use MPN method for highly turbid samples( Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 275 mg/I Al-Aluminum mg/I Cobalt-0.003 mg/I _
pH(when analyzed) 6.6 units Ba-Barium mg/I Selenium-<0.01
TOC mg/I Ca-Calcium mg/I
Chloride 9 mg/I Cd-Cadmium <0.001 mg/I
Arsenic 0.021 mg/I Chromium:Total 0.025 mg/I
Grease and Oils mg/I Cu-Copper <0.01 mg/I ORGANICS:(by GC, GC/MS, HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury <0.0002 mg/I Report Attached? ❑ Yes(1) II No(0)
Specific Conductance µMhos K-Potassium mg/I VOC , method#
Total Ammonia 38.8 mg/I Mg-Magnesium 2.90 mg/I , method#
(Ammonia Nitrogen,Niras N,Ammonia Nitrogen,Total)
Mn-Manganese mg/I , method#
TKN as N mg/I Ni-Nickel <0.01 mg/I , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% _
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and inat the laboratory analytical data was produced using approved methods of analysis by a
DWQ-certified laborato . I am aware that there are significant penalties for submitting false information,including the possibility of fines and im risonrnent for knowing violet ons.
Penny C. Mahoney- Director of Sustainability and Operations Supp ...MIESIMIVrAlr-2
Permittee(or Authorized Agent)Name and Title-Please print or type - Sig -t,y4fi"ermittee(or Authorize•Agent),.,-- (Date)
GW-59 Rev. t/2007

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original:DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: •IVISION OF WATER QUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM and I copy to: 617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:WQ0018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington ""`" NC 28403 County Brunswick ❑ Lagoon ❑Remediation: Infiltration Gallery
❑ Spray Field ❑Remediation:
Contact Person: Larry Young Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Down gradient/Monitoring Well#2E No.of wells to be sampled: 6 ❑ Water Source Heat Pump ©Other:Surface Disposal Res.Sol
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#2E Date sample collected: 06/08/22 FIELD ANALYSES: WAS
Well Depth: 13 ft. Well Diameter: 2.0 in. pH 5.8 units Temp. 17.5 °C DRY at
Depth to Water Level: 7.5 ft.below measuring point Screened Interval: 3 ft. to 13 ft. Spec.Cond. µMhos time of
sampling,
Measuring Point is 3.0 ft.above land surface Relative M.P. Elevation: 23 ft. Odor None check
Volume of water pumped/bailed before sampling: 12 gallons Appearance Clear here:
Samples for metals were collected unfiltered: ®YES ❑NO and field acidified: ®YES ❑NO
LAB .EAIORIr_INFORMATION
Date sample analyzed: 06/08/22-06/21/22 Laboratory Name: Envirochem Certification No, 37729
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N 0.05 mg/I Pb-Lead <0.01 mg/I
Coliform: MF Fecal 1100m1 Nitrate(NO3)as N 0.24 mg/I Zn-Zinc 0.014 mg/I
Coliform: MF Total /100m1 Phosphorus:Total as P 0.10 mg/I
(Note, Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 272 mg/I Al-Aluminum mg/I Cobalt-0.003 mg/I
pH (when analyzed) 5.9 units Ba-Barium mg/I Selenium -<0.01 mg/I
TOC mg/I Ca-Calcium mg/I
Chloride <5 mg/I Cd-Cadmium <0.001 mg/I
Arsenic <0.01 mg/I Chromium:Total <0.01 mg/I
Grease and Oils mg/1 Cu-Copper <0.01 mg/1 ORGANICS:(by GC, GC/MS. HPLC)
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/1 Hg-Mercury <0.0002 mg/I Report Attached? ❑ Yes(1) ® No(0)
Specific Conductance µMhos K-Potassium mg/I VOC , method#
Total Ammonia 3.3 mg/I Mg-Magnesium 1.78 mg/I , method#
(Ammonia Nitrogen:NH,as N,Ammonia Nitrogen,Total) Mn-Manganese mg/1 methpd#
TKN as N mg/I Ni-Nickel <0.01 mg/I , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
1 certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWQ-certified laborato . I am aware that there are significant penalties for submitting false information,includin•the•ossibil _of fines and imprisonment for knowing violations.
Penny C. Mahoney- Director of Sustainability and Operations Supp �� ��, l 7 :���Z_
Permittee(or Authorized Agent)Name and Title-Please print or type Signiiffe of Per ee(or Authorized Agent) ',Date)
GW-59 Rev. 1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: and 1 co"to DIVISION OF WATER QUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER,RALEIGH,NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please Print Clearly orType PERMIT Number:W00018087 Expiration Date: Jan. 31, 2027
Facility Name: DAK Americas LLC, Cape Fear Site Non-Discharge UIC
Permit Name(if different): NPDES NC0000663 Other
Facility Address: 1430 Commonwealth Drive, Suite 305 TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington " '' NC 28403 County Brunswick ❑ Lagoon ❑Remediation: Infiltration Gallery
❑ Spray Field ❑Remediation:
Contact Person: Larry Young Telephone#: [phone] ❑ Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:Background/Monitoring Well# 3A No.of wells to be sampled: 6 ❑ Water Source Heat Pump g Other:Surface Disposal Res.Sol
{from Pemiil)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW#3A Date sample collected: 06/08/22 FIELD ANALYSES: WAS
Well Depth: 13.25 ft. Well Diameter: 2.0 in. pH 5.38 units Temp. 18.0 °C DRY at
time of
Depth to Water Level: 4.1 ft.below measuring point Screened Interval: 3.25 ft. to 13.3 ft. Spec.Cond. t Mhos sampling,
Measuring Point is 1.76 ft.above land surface Relative M.P. Elevation: 24.78 ft. Odor None check
Volume of water pumped/bailed before sampling: 10 gallons Appearance Clear here:
Samples for metals were collected unfiltered: ®YES ❑NO and field acidified: ®YES ❑NO
1.8B9FAJORY INFORMATION
Date sample analyzed: 06/08/22 -06/21/22 Laboratory Name: Envirochem Certification No. 37729
PARAMETERS NOTE:Values should ieflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N <0.02 mg/I Pb-Lead <0.01 mg/I
Coliform: MF Fecal /140m1 Nitrate(NO3)as N 0.23 mg/I Zn-Zinc 0.014 mgll
Coliform: MF Total 1140m1 Phosphorus:Total as P <0.04 mg/I
(Note' Use MPN method for hJghly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 101 mg/I Al-Aluminum mg11 Cobalt-<0.001 mg/I
pH (when analyzed) 5.5 units Ba-Barium _ mg/1 Selenium -<0.01 mg/I
TOG mg/I Ca-Calcium mg/I
Chloride 7 mg/I Cd-Cadmium <0.001 mg/I
Arsenic <0.01 mgll Chromium:Total <0.01 mg/I
Grease and Oils mg/I Cu-Copper 0.011 mg/I ORGANICS:(by GC, GC/MS, HPLC)
Phenol mg/I Fe-Iron_ mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury <0.0002 mg/I Report Attached? ❑ Yes(1) III No(0)
Specific Conductance uMhos K-Potassium mg/I VOC , method#
Total Ammonia <0.2 mg/I Mg-Magnesium 0.948 mg/I , method#
{Ammonia Nitrogen:NH3as N;Ammonia Nitrogen,Total} Mn-Manganese mg/I , method#
TKN as N mg/I Ni-Nickel <0.01 mg/I , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data wee produced using approved methods of analysis by a
DWQ-certified laborato . I am aware that there are si.nificant penalties for submitting false information,including the possibility c.f fines and imprisonment for knowing violations.
/.
Penny C. Mahoney- Director of Sustainability and Operations Supp �� ZA �_�-
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of ntee r Authorized Agent) f D-te)
GW-59 Rev, 1/2007 P '

Environmental Chemists, Inc.
envirochem 6602 Windmill Way Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
'" 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS into rt environrnentalchemists.com
DAK Americas Date of Report: Jul 06, 2022
1205 Culbreth Drive Suite 200 Customer PO#:
Wilmington NC 28405 Customer ID: 08100044
Attention: Larry Young Report#: 2022-10354
Project ID: Monitoring Well
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-25042 Site: MW-2A 6/7/2022 6:59 AM Water Young/Simmons
Test Method Results Date Analyzed
Cobalt EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Copper EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Lead EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Magnesium EPA 200.7,Rev 4.4,1994 2.82 mg/L 06/13/2022
Nickel EPA 200.7,Rev4.4,1994 <0.01 mg/L 06/13/2022
Selenium EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Zinc EPA 200,7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Arsenic EPA 200.7,Rev.4 4,1994 <0.01 mg/L 06/13/2022
Chromium EPA 200.7,Rev.4.4,1994 <0.01 mg/L 06/13/2022
Cadmium EPA 200.8,Rev,5.4,1994 <0.001 mg/L 06/13/2022
Mercury EPA 245.1 <0.0002 mg/L 06/09/2022
Ammonia Nitrogen EPA 350.1,Rev,2 0,1993 0.8 mg/L 06/08/2022
Total Dissolved Solids (TDS) SM 2540 C-2015 279 mg/L 06/07/2022
pH SM 4500 H 8-2011 6.5 units 06/09/2022
Result estimated. Analyzed out of 15 minutes hold time.
Total Phosphorus SM 4500 P(F-H)-2011 < 0.04 mg/L 06/11/2022
Chloride SM4500 CI E-2011 10 mg/L 06/09/2022
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353 2.Rev 2 0,1993 < 0.02 mg/L 06/07/2022
Nitrate+Nitrite-Nitrogen EPA 353 2,Rev.2.0,1993 0.31 mg/L 06/09/2022
Nitrate Nitrogen Subtraclion Method 0.31 mg/L 06/13/2022
Total Nitrogen (Cale)
Total Kjeldahl Nitrogen (TKN) EPA 351.2,Rev.2 0,1993 1.3 mg/L 06/12/2022
Total Nitrogen Total N1rogen 1.3 mg/L 06/20/2022
Report 2022-10354 =o�,--. __ -- Page 1 of 3

Environmental Chemists, Inc.
envirachem, 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manta),NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
•
ANALYTICAL&CONSULTING CHEMISTS info,rrenvironmentalchemisls.com
DAK Americas Date of Report: Jul 06, 2022
1205 Culbreth Drive Suite 200 Customer PO#:
Wilmington NC 28405 Customer ID: 08100044
Attention: Larry Young Report#: 2022-10354
Project ID: Monitoring Well
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-25042A Site: MW-2A 6/7/2022 6:59 AM Water Young/Simmons
Test Method Results Date Analyzed
Cobalt EPA 200.5,Rev.5.4,1994 0.001 mg/L 06/13/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-25043 Site: MW-2B 6/7/2022 8:06 AM Water Young/Simmons
Test Method Results Date Analyzed
Cobalt EPA 200.7,Rev 4.4,1994 0.013 mg/L 06/13/2022
Copper EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Lead EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Magnesium EPA 200.7,Rev 4.4, 1994 8.92 mg/L 06/13/2022
Nickel EPA 200.7,Rev 4.4, 1994 <0.01 mg/L 06/13/2022
Selenium EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Zinc EPA 200.7,Rev 4 4, 1994 <0.01 mg/L 06/13/2022
Arsenic EPA 200.7,Rev.4.4,1994 0.016 mg/L 06/13/2022
Chromium EPA 200.7,Rev,4.4,1994 <0.01 mg/L 06/13/2022
Cadmium EPA200.0,Rev.5,4,1994 <0.001 mg/L 06/13/2022
Mercury EPA 245.1 <0.0002 mg/L 06/09/2022
Ammonia Nitrogen EPA 350.1,Rev,2.0,1993 40.5 mg/L 06/08/2022
Total Dissolved Solids (TDS) SM 2540 C-2015 845 mg/L 06/07/2022
pH SM 4500 tt B-2011 6.6 units 06/09/2022
Result estimated. Analyzed out of 15 minutes hold time.
Total Phosphorus SM 4500 P(F-H)-2011 0.11 mg/L 06/11/2022
Chloride SM4500 CI E-2011 15 mg/L 06/09/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 3532,Rev.20,1993 0.07 mg/L 06/07/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev,2.0,1993 0.40 mg/ 06/09/2022
Nitrate Nitrogen Sublfaction Method 0,33 mg/L 06/13/2022
Report 11 2022-10354 Page 2 of 3

Environmental Chemists, Inc.
envirochenl 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infolt environnientalchemists,com
DAK Americas Date of Report: Jul 06, 2022
1205 Culbreth Drive Suite 200 Customer PO #:
Wilmington NC 28405 Customer ID: 08100044
Attention: Larry Young Report#: 2022-10354
Project ID: Monitoring Well
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-25044 Site: MW-2C 6/7/2022 8:40 AM Water Young/Simmons
Test Method Results Date Analyzed
Cobalt EPA 200.7,Rev 4 4.1994 0.019 mg/L 06/13/2022
Copper EPA 200.7,Rev 4 4.1994 0.016 mg/L 06/13/2022
Lead EPA 200.7,Rev 4 4 1994 0.015 mg/L 06/13/2022
Magnesium EPA 200.7,Rev 4 4.1994 12.9 mg/L 06/15/2022
Nickel EPA 200.7,Rev 4 4,1994 0.021 mg/L 06/13/2022
Selenium EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Zinc EPA 200.7,Rev 4.4,1994 0.047 mg/L 06/13/2022
Arsenic EPA 200 7,Rev 4 4.1994 <0.01 mg/L 06/13/2022
Chromium EPA2007,Rev 44.1994 0.028 mg/L 06/13/2022
Cadmium EPA 200.9,Rev.5.4,1994 <0.001 mg/L 06/13/2022
Mercury EPA 245.1 <0.0002 mg/L 06/09/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 0.7 mg/L 06/08/2022
Total Dissolved Solids (TDS) SM 2540 C-2015 621 mg/L 06/07/2022
pH SM 4500 H B-2011 5.1 units 06/09/2022
Result estimated. Analyzed out of 15 minutes hold time.
Total Phosphorus SM 4500 P(F-H)-2011 1.45 mg/L 06/11/2022
Chloride SM4500 CI E-2011 8 mg/L 06/09/2022
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353 2,Rev.2.0,1993 0.07 mg/L 06/07/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 1.88 mg/L 06/09/2022
Nitrate Nitrogen Subtraction Method 1.81 mg/L 06/13/2022
Comment: �/
Reviewed by: ��`\' "1 ���L )C ^
Y A- '
Report* 2022.10354 Page 3 of 3

2 Windmill
mington
_ op ENVIRONMENTAL CHEMISTS', INCOFFICE:9 0-3 2 223IFAX910-,NC
92�24$
Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: DAK PROJECT NAME: WQ0018087 !REPORT NO: 2.2.-1°3-SU
ADDRESS: SITE:Monitoring Wells PO NO:
REPORT TO: PHONE/FAX:
J COPY TO: email:
Sampled By: --,--5;-`'/ e> � 7/�5.J�iit.,id�S SAMPLE TYPE: I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
I / l ollection a , ' I I PRESERVATION
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a E ca r E g3 c� ( Z g w ..
m U U U a Z Z = = 2 Z
DateI Time Temp y _ LT
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Transfer Relin is1 d By: Date/Time Received By: DatelTlme
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2. 'Temperature whgfi Feed°Cy: ' .&.i.9"� • Accepted: Rejected: Resample Requested:
Delivered By: ,,,,/,,.f;/�., Received By: - C ,�„M
Comments: ' ;s-� ' 7 O 3�"" Date:TURNAROUND:Time: ld Oi 4
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ENVIRONMENTAL CHEMISTS, INC fl W:9 0i13 9 2-0 22 3 1FAX910.2 5
Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION It37729 info©environmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
Client: DAK PROJECT NAME: WQ0018087 REPORT NO: Z Z.—t O 3sti
ADDRESS: SITE:Monitoring Wells PO NO:
REPORT TO: PHONE/FAX:
COPY TO: email:
Sampled By: L i.,- V°,,,.J c, f(.i mi., SAMPLE TYPE:I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
Collection a m a PRESERVATION
I- 0 m c � ca c Ow Et Sample Identification W �a o 2 `t o m a m m w 1 0 " = o ¢ w ANALYSIS REQUESTED
E E `o ° a U E V 5 m a 2 (.0 z a S r =
Date Time Temp " " V a z z = = z ~ . °
C ( _
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MW: 4 �.\ a 4-7-2r) O'O/1 p 6, fi_ 6 G •7;, �2•© 25W3 ,As.Cd,Cr,Co,Cu,Pti,Mg,Hg.Ni,Se,Zn
I C ((r) I
field pH/temp: C„ Lj I Q ,6%5-- { dp G t X
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Transfer Rell Is d By:_ Datefrme Received By: Datemme
1. l /- /, 44 /�f ,,' , _
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Temperature wh i1I ceived° C °. Accepted: ILA. Rejected: Resample Requested:
Delivered B . Received By: C_A,,,.." Date: (0)71a1� Time: 102pl ft
Comments: €} c_ [D E 7si? E3 ( , C,, t� e'7 C TURNAROUND:
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ENVIRONMENTAL CHEMISTS, INC 022g �2aIE:910-392 FAX[phone]
Analytical 8 Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: DAK PROJECT NAME:WQ0018087 REPORT NO: Z 2_—j O3S' t
ADDRESS: SITE:Monitoring Wells PO NO:
REPORT TO: PHONEIFAX:
��,F���� y 'f/ COPY TO: email:
Sampled By:f 1`t! y f�C1Jt.�' `hcr//,S ,5:41...•,.J5 SAMPLE TYPE:I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other
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Sample Identification .c' 2 5 0 m 1 w o n r o ¢ w ANALYSIS REQUESTED
E o 0 . a o `o s z 0 z n Z 4 = 18
i 1° V U _' .. z z 2 = Z p
I Date Time Temp ci _ u.
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MW: �� 727,6 � j!� �D'` G �� .1a ZS � X` As,Cd,Cr,Co,Cu,Pb,Mg,Hg,Ni,Se,Zn
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Transfer Reli qui ed By. ate/Time Received By: Date/Time1. /:IV .!. d/ /0:O/ f
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Delivered By: / Received By: ,c Date: fo "i Time: t01011'h-(
Comments: 4-) ,� q 61.a-' 1�?.1., Ge&-, D 6(F,D TURNAROUND:

Environmental Chemists, Inc.
,>i envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Sowsertown Road,Manteo,NC 27954 a 252.473.5702 Lab/Fax
5M
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infoia environmentalchemists.com
DAK Americas Date of Report: Jun 22, 2022
1205 Culbreth Drive Suite 200 Customer PO#:
Wilmington NC 28405 Customer ID: 08100044
Attention: Larry Young Report#: 2022-10531
Project ID: Monitoring Well
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-25478 Site: MW-2D 6/8/2022 9:12 AM Water Young/Simmons
Test Method Results Date Analyzed
Copper EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Lead EPA 200.7,Rev 4.4,1994 <0.01 mglL 06/13/2022
Magnesium EPA 200.7,Rev 4.4,1994 2.90mg/L 06/13/2022
Nickel EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Selenium EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Zinc EPA 200.7,Rev 4.4,1994 0.032 mg/L 06/13/2022
Arsenic EPA 200.7,Rev.4.4,1994 0.021 mg/L 06/13/2022
Chromium EPA 200.7,Rev.4.4,1994 0.025 mg/L 06/13/2022
Cadmium EPA 200.8,Rev 5.4,1994 <0.001 mg/L 06/13/2022
Mercury EPA 245.1 <0.0002 mg/L 06/09/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0, 1993 38.8 mg/L 06/08/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 275 mg/L 06/09/2022
pH SM 4500 H B-2011 6.6 units 06/09/2022
Result estimated. Analyzed out of 15 minutes hold time.
Total Phosphorus SM 4500 P{F-11)-2011 0.18 mg/L 06/17/2022
Chloride SM4500 CI E-2011 9 mg/L 06/09/2022
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2,Rev.2.0, 1993 0.07 mg/L 06/08/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.59 mg/L 06/13/2022
Nitrate Nitrogen Subtraction Method 0.52 mg/L 06/20/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-25478A Site: MW-2D 6/8/2022 9:12 AM Water Young/Simmons
Test Method Results Date Analyzed
Cobalt EPA 200.8,Rev.5 4.1994 0.003 mg/L 06/21/2022
Report#.: 2022-10531 Page 1 of 3

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
. 5'{ 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infora environmentalchemists.com
OAK Americas Date of Report: Jun 22, 2022
1205 Culbreth Drive Suite 200 Customer PO#:
Wilmington NC 28405 Customer ID: 08100044
Attention: Larry Young Report#: 2022-10531
Project ID: Monitoring Well
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-25479 Site: MW-2E 6/8/2022 8:38 AM Water Young/Simmons
Test Method Results Date Analyzed
Copper EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Lead EPA 200.7,Rev 4.4, 1994 <0.01 mglL 06/13/2022
Magnesium EPA 200.7,Rev4.4.1994 1.78 mg/L 06/13/2022
Nickel EPA 200.7,Rev 4.4,1994 <0.01 mglL 06/13/2022
Selenium EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Zinc EPA 200.7,Rev 4.4,1994 0.014 mg/L 06/13/2022
Arsenic EPA 200.7,Rev,4,4,1994 <0.01 mg/L 06/13/2022
Chromium EPA 200.7,Rev.4.4,1994 <0.01 mglL 06/13/2022
Cadmium EPA 200.8,Rev.5.4,1999 <0.001 mg/L 06/13/2022
Mercury EPA 245.1 <0.0002 mg/L 06/09/2022
Ammonia Nitrogen EPA 350.1,Rev,2 0,1993 3.3 mg/L 06/08/2022
Total Dissolved Solids(TDS) SM 2540 C-2015 272 mg/L 06/09/2022
pH SM 4500 H 8-2011 5.9 units 06/09/2022
Result estimated. Analyzed out of 15 minutes hold time.
Total Phosphorus SM 4500 P(F-H)•2011 0.10 mg/L 06/17/2022
Chloride SM4500 CI E-2011 < 5 mg/L 06/09/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.05 mg/L 06/08/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev,20,1993 0.29 mg/L 06/13/2022
Nitrate Nitrogen Subtraction Method 0.24 mg/L 06/20/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-25479A Site: MW-2E 6/8/2022 8:38 AM Water Young/Simmons
Test Method Results Date Analyzed
Cobalt EPA 200.8,Rev,5.4,1994 0.003 mg/L 06/21/2022
Report# 2022-10531 Page 2 of 3

Environmental Chemists, Inc.
. .eiivirocheni 6602 Windmill Way,Wilmington,NC 28405 e 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
s,n 255-A Wilmington Highway,Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infofa enviroumentalchemists.com
DAK Americas Date of Report: Jun 22, 2022
1205 Culbreth Drive Suite 200 Customer PO#:
Wilmington NC 28405 Customer ID: 08100044
Attention: Larry Young Report#: 2022.10531
Project ID: Monitoring Well
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-25480 Site: MW-3A 6/8/2022 7:59 AM Water Young/Simmons
Test Method Results Date Analyzed
Copper EPA 200 7,Rev 4.4,1994 0.011 mg/L 06/13/2022
Lead EPA 200.7.Rev 4 4,1994 <0.01 mg/L 06/13/2022
Magnesium EPA 200.7.Rev 4.4,1994 0.948 mg/L 06/13/2022
Nickel EPA 200.7.Rev 4.4,1994 <0.01 mg/L 06/13/2022
Selenium EPA 200.7,Rev 4.4, 1994 <0.01 mg/L 06/13/2022
Zinc EPA 200.7,Rev 4.4,1994 0.014 mg/L 06/13/2022
Arsenic EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Chromium EPA 200.7,Rev 4.4,1994 <0.01 mg/L 06/13/2022
Cadmium EPA 200,8,Rev 5.4,1994 <0.001 mg/L 06/13/2022
Mercury EPA 245,1 <0.0002 mg/L 06/09/2022
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 <0.2 mg/L 06/08/2022
Total Dissolved Solids(TDS) SM 2540 C.2015 101 mg/L 06/09/2022
pH SM 4500 H B-2011 5.5 units 06/09/2022
Result estimated. Analyzed out of 15 minutes hold time.
Total Phosphorus SM 4500 P(F-H)-2011 < 0.04 mg/L 06/17/2022
Chloride SM4500 CI E-2011 7 mg/L 06/09/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 06/08/2022
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev 2.0, 1993 0.23mg/L 06/13/2022
Nitrate Nitrogen Subtraction Method 0.23 mg/L 06/20/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-25480A Site: MW-3A 6/8/2022 7:59 AM Water Young/Simmons
Test Method Results Date Analyzed
Cobalt EPA 200.8,Rev.5.4,1994 <0.001 mg/L 06/21/2022
Comment: �/ ,
Reviewed by: !/ �� r),,,,
x
Report# 2022-10531 Page 3 of 3

02
ton,NC
: 6- ENVIRONMENTAL CHEMISTS, INC OFF 0''3 Way 2231IFAXg91039244245
AnalytiCa! Cons�lti emists NCDENR:DWQ CERTIFICATION#94 NCDHHS: DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY Z Z- I c53/
Client: DAK PROJECT NAME: WQ0018087 REPORT NO y Dll, t7 e(41$0
ADDRESS: SITE: Monitoring Wells PO NO:
REPORT TO: PHONEJFAX:
i COPY TO: email:
Sampled By:� /2, VOrl ;' %Ls /% _<�-•, . - SAMPLE TYPE: I =Influent, E=Effluent,W=Well,ST=Stream, SO=Soil, SL=Sludge, Other:
Collection a PRESERVATION
H toA c 0C r p n W o
Sample Identification Q. la.6o o In a m LYI
W a m o it w ANALYSIS REQUESTED
E o o ° ° -6 E `o _, D o = n z a = Ill 1
Date Time Temp " U V a Z z = = Z J °
LL
'`� C (P5
MW: CAL—/ �i ' Z ' ,IY6.S' �7/, 11A,) 7Gi' G -(v Z- T Z5V7 X42- As,Cd,Cr,Co,Cu,Pb,Mg,Hg,Ni,Se,Zn
,�
field pH/temp: ��Ui i G ', i X_ CI,NO2,TDS,pH -`06 �� '
J� % r ( y 1 l (0 -G ✓ J X C0•S CI.L.-2- NH3,NO3,P
i / 6 Y7�- zz_ ,i/o j�f �_�� 6 74 I f
bi ti C P
G7H—
G , o
C P
G G /n'/ 2f15c- ./9NA �yz-
C P !J !!r� P 1` /'
G G / o (l� 1 , f -(
C P
G G
Transfer Relinquished By: Date/Time Received By: Date/Time
1. f: f`� �� ! L� Z—�_ `'%2/
2. 4 i
Temperature whe eceived °C: ! , U �' Accepted: ejected: Resa a equested:
Delivered Byre L;42774:— Ce,___
Received By: Date: ZZ Time: 1 �0'- 1 9
Comments: / Jj OY: Vey L•,3 D 'z TUR AROUND:

ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Wilmington,NC 28405
OFFICE:910-392-0223 FAX [phone]
Analytical&Consulting Chemists
NCDENR:DING)CERTIFICATION#94 NCDHHS: DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: DAK PROJECT NAME: WQ0018087 REPORT NO: Z .. - /0531
ADDRESS: SITE:Monitoring Wells PO NO:
REPORT TO: PHONE/FAX:
COPY TO: email:
1f ' 1 r '`
Sampled By:/'/Grje� - /h//i4JG /,�i {//, _--),- '!_1/ZD�J< SAMPLE TYPE: I=Influent, E=Effluent,W=Well, ST=Stream, SO=Soil, SL=Sludge, Other:
Collection N PRESERVATION
w ro c [7 E _j o ,2 1 A
Sample Identification Q.0 = o - m g Z _, o p = o a w ANALYSIS REQUESTED
E .c E o t.) u) O w =
E 00 0 . u = g z z x = z J
Date Time Temp " a = ,7 o
MW: ! �o 4R %C' 5- �.� G2 9 X As,Cd,Cr,Co,Cu,Pb,Mg,Hg,Ni,Se,Zn
C 71 / _C/
field pH/temp: 62g 6G ( X CI,NO2,TDS,pH i . �27//cS
5-s // / . S l' f. G ! .D X <04`I�� NH3,NO3,P
et
%// G G / T� ti r .FJ/9/ 7L
�
C P /"
G G / //dlt ,Yd .bc7rl
C PG G //67,
f
f C P
G G 4 /---4 k,/"C. r
C P
G G
Transfer \9 Relinquished By: Date/Time Received By: Date/Time
1. ? ?^ O
2. r
Temperature when Received °C: t -Ll Accepted: Rejected: Resar>ap a quested:
Delivered By: `di' V , AJ, `( ° Received By: Date. / Time:
Comments: Ai-7/ U//row. O revqZ -Ce Q� TURNAROUND:

,.,--,-7,1,iiiiiiiiiiiiiiii,
ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Wilmington, NC 28405
OFFICE:910-392-0223 FAX [phone]
Analytical&Consulting Chemists
NCDENR: DWQ CERTIFICATION#94 NCDHHS: DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: DAK PROJECT NAME: WQ0018087 REPORT NO: Z.Z-- l 05 3 f
ADDRESS: SITE: Monitoring Wells PO NO:
REPORT TO: PHONEIFAX:
COPY TO: email:
Sampled By:L/wq yo...),4- j`9,;i��7, ,,,0„.de SAMPLE TYPE: I=Influent, E=Effluent,W=Well, ST=Stream,SO=Soil, SL=Sludge, Other:
Coll¢ction 0Cl., d PRESERVATION
� m 2 c C� c o O w n
Sample Identification m °a cD :3 0 `o a b m m w o " m o_ Lu w ANALYSIS REQUESTED
a E c _ _c E o ¢ D 0 c-} m o o w s
N 2 ¢ S
Date Time Temp E 0 D o a U a J z r Z ~ J o
N
/ C Cry-- LL
MW: .9/1 a— zZ d75 /I,C)M .., G ' , G 42. Z54680 X As,Cd,Cr,Co,Cu,Pb,Mg,Hg,Ni,Se,Zn
/��// p C W
field pH/temp: v'7S7f 1: ` p- G X A CI,NO2,TDS,pH 6a-H-I ._
_ �} o _ / C ,Lj LZ
?j�S /�. or �,`73' '� kj, �r7 G Y/ .�.a XGQ.S °[b� NH3,NO3,P
C P
C P V cad ;l
C P
G G 795e P9j 44 `z
G G , 'N .,- till-72 //C4 r---f -
C P
G G
Transfer Relinquished By: Date/Time Received By: Date/Time
1. ...--41,./LA-e L•-•-,_‘.
2. J /�;� i I I
Temperature when Receive 7C: Q ' Accepted: '� R , led: ResampI R'quested:
Delivered By: V4 Received By: �� Date: "'Ia Time:
Comments: /`�f./ f j¢,e aJ a703 /26,,q,?), S 6 67 7 TURN ROUND: