WQ0033677_Monitoring - 03-2021_20210504

v••s�•Ln 4(UMLI I'1 /nVryl I UKINti: • • . { ), tr1' Y, r f�. !�{k)
COMPLIANCE REPORT FORM • Cl':''''' , ( ` ' ' f�''"- r r'r
and 1 copy to ( ,w fr U, �� r :
FACILITY INFORM Pl ase Print acarty or Type
;t
Facility Name: �� L PERMIT Number: Q©o�jdl,7Expiration Date: /aa-3)••. )
Permit Name(if different): Non Discharge ✓ UIC
r. NPDES Other
Facility Address: 50�p 7 re mean .9r e
NI Cr TYPE OF PERMITTED OPERATION BEING MONITORED
I4 r1 r...rq NC v ;`11e D�� County Ur ❑ Lagoon ❑Remediation:Infiltration Gallery
Contact Person: i( � I r ,?,S pray Field • 0 Remediation:
Telephone#:i --7L 3g4g'QD 0 Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name: Se r tri S / No.of wells to be sampled:p El Water Source;Heat Pump 0 Other:
SAMPLING INFORMATION : (from Permit) l
WELL tD NUMBER(from Permit): If WELL
Date sample collected: 3 'io - ;1 FIELD ANALYSES: WAS.
Well Depth: (1575' ft. Well Diameter: in.
DRY at
Depth to Water Level: pH 7 3 i units Temp.. i °C
Po6.� ft.below measuring point Screened Interval:.G$�ft. to�S� ft. Spec.Cond. i13' µMhos time of
Measuring Point is 3 ft.above land surface ry g Relative M.P.Elevation:'RR ft. Odor sampling,
Volume of water pumped/bailed:before sampling: 5.•(o/ gallons t° here:
Appearance Cj cil r here:.
Samples for metals were collected unfiltered: ES ❑NO and field acidified: ❑YES ❑NO
LABORATORY INFORMATION /
Date sample analyzed: P e'g5r' Sr'c)q,P , I / ` -}. 1 J9
r a°S colloidal
concentrations.
Name: (. / P(y) t-cr DJ J-r>C Certification No.
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD ' rngll I Nitrite(NO2)as N mg/I Pb-Lead
Coliform: MF Fecal /100m1 Nitrate(NO3)as N L. mg/I
Coliform:MF Total : �.� mg/I Zn-Zlnc 0 Lit p> mg/I
/100mi: Phosphorus:Total as P O. (s 5 mgil(Note: Use MPN method for highly turbid samples)
q 'Orthophosphate mg/I Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total . (0 l mg/I Al-Aluminum mg/I
pH(when analyzed) ' 7..3 units Ba-'Barium mg/I /
TOC 4 '' 7, Q ! i!
0 CND) mg/I Ca-Calcium mg/I ti 46 - t D. 10 `- /L
Chloride • (0 ki) mg/I Cd Cadmium mg/I r rr,otr ' /
cle w e BRL- f / L
Arsenip 0 • (ND� mg/I Chromium:Total mg/I T_N rl r^ l�. L
Grease and Oils
mg/I Cu-Copper 0.64 mg/I ORGANICS:; y GC,'GC/MS,HPLC)
l
Pheno
Phenol ' mg/I ' Fe-Iron 'mg/I (Specify testland.method#r ATTACH LAB REPORT.)
mg/I Hg-Mercury mg/I Report Attached? ❑• Yes(1) ❑ •No(0) 'I
Specific Conductance ((5' µMhos K..Potassium Q.(p1 ) n, /I VOC
Total Ammonia ( m /I g ,method#
9 Mg-Magnesium method#
(Ammonia Nitrogen;NH,as N;Arnmonia Mbogen;Tolaq - mg/I ��j
Mn-Manganese . mg/I V Y G ,method#
TKN as N q.20 mg/I Ni-Nickel .
mg/1 method#
For Remedfation.Systems Only(Attach b Reports): Influent Total VOCs: AA n ,�
1 ;mg/ Effluent Total VOCs:' e
i�• �:.., - .. ' ; . mg/L VOC.Removal/.
Hi . Lp.
hn, ,SC ViSC( ..� ti'2 7,242—1 r
Peimittt (or Authorized Agent)Name and Title-Please print or type i r A• Z.
$Ignalu�of erin. eq(or A rizcd Agent) (Dale)
GW=59 Rev.1/2007 � � /
L
Rt^ 11/F[
M
I
:.. . . .. , AY 0 4 2021
•
•
DWR SECTION

GROUNDWATER QUALITY MONITORING: r al origins -. °lrr.i ,a ° 1tr, i..:, .;'. , yf.- i%
and 1 copy to
COMPLIANCE REPORT FORM ', i � ;+�.
FACILITY INFORMATs10L� Please F rirn Clearly or Type PERMIT Number ht•
`, f iQ�,,. xpiration Date: /9--,31-J i
Facility Name: ( q �Qr trig t Ay 1- LC!: Non-Discharge : 't/ UIC
Permit Name(if different): NPDES Other
Facility Address: 5C t'7 re"IV TYPE OF PERMITTED OPERATION BEING MONITORED
�'}�Cr^3etn 15 "1ett' NC !. Countyr� l
1 `" • r `� Ivy+�/� ❑ L• agoon ❑Remediation:Infiltration Gallery
• :i late:
, ay Field ❑Remediation:
Contact Person: C /4:.+6-•i no.'S Telephone#: -0 —(96e ❑ R• otary Distributor • ❑Land Application of Sludge
Well Location/Site Name: t7 SC P y735 fict No.of wells to be sampled: W• ater Source,Heat Pump CI Other:
SAMPLING INFORMATION . y 1; ((from aim }
❑
1 If WELL
WELL ID NUMBER(from Permit): -Date sample collected: JD-a! FIELD ANALYSES: WAS
Well Depth: tl5 ft. Well Diameter: in. •
� DRY at
�- pH �j., units Temp. C
Depth to Water Level: 31.174 ft.below measuring point Screened Interval: ? ft, toffs-ft. Spec.Cond. igy µMhos time of
'� sampling,
Measuring Point is 3 ft.above land surfac / Relative M.P.Elevation: v2l/c ft. Odor AC►1 check
Volume of water pumped/bailed before sampling: ro� gallons Appearance 5)` h�J r1 t7e�� here:
Samples for metals were collected unfiltered: EYES ❑NO and field acidified: ❑YES ❑NO tJ
LABORATORY INFORMATION _ / 1, -I
Date sample analyzed: +e y- 5� 'a �e Laboratory Name: LA..,c., r d 1 f(� L•+ 5 i } • Certification No. GQ 50
PARAMETERS NOTE:Values should reflect dissorved and colloidal concentrations.
COD mg/i Nitrite(NO2)as N mg/I Pb-Lead mg/I
Coliform: MF Fecal ' /100ml Nitrate(NO3)as N .4 f7, , mg/I Zn-Zinc 0.D 3 g mg/I
Coliform:MF Total /1001n1 Phosphorus:Total as P L 0.16 mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate
mg/I Other(SpecifX Compounds and Concentration Units):
Dissolved Solids:Total mg/I Al-Aluminum mg/I
pH(when analyzed) ' • units Ba-Barium mg/I , c1-)11 y ml ,i _ 3: L/ rj , L
TOC 0 (N D) mg/I Ca-Calcium mg/I me,9S 4 1,Oc d/L
Chloride • /0.0 mg/I Cd-Cadmium mg/I rm.f r 'ae - C (r.B� RL) /y
Arsenic 0 iV D ) mg/I Chromium:Total mg/I % V) 4, +n ' �. it / 1-
Grease and Oils mg/I Cu-Copper 0 p? mg/I ORGANIC :,Eby GC,GC/MS,HPLC)
(
Phenol mg/I Fe-Iron mg/I (Specify test and method#.ATTACH LAB REPORT.)
Sulfate mg/I Hg-Mercury mg/I Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance ' B I µMhos K-Potassium
y mg/I VOC method#
Total Ammonia <1,0 mg/I Mg-Magnesium . mg/I ,method#
(Ammonia Nitrogen;NH,as N;Arrvnonllaa Nitrogen.Total) Mn-Manganese mg/I ,method#
TKN as N .,ga mg/I Ni-Nickel mg/I . ,method#
For Remedlatlon Systems Only(Attach Lab Reports); I Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
+: p n .L,LP,crt as;rir n„n,arn •n c .r _lat,_`a. _.
•
1, d1 ,�1 Yl ..\y) a' S �^L,,�Pr . 7dteriA,a/ ��fi /• f iliY>rv� �d'�,
Perm' ee(or uthorized Agent1 Name and Title-Please print or type S gnalure of Pe Mee or Authorized Agent) ; • (Date)
GW-5 Rev.1/2007
I

GROUNDWATER QUALITY MONITORING: r'al onginal r, t11�+ r,1 1. ;tI Y +74. ;,,1, 7s {�V 1::nil
COMPLIANCE REPORT FORM and 1 copy to: (' I t; I nG r; 4 ',',
FACILITY INFQR(IAA N PleasePrinl Clearly or Type PERMlT.Number .�d
/! 0334 7�'Expiration Date: is..31 -Q�
Facility Name: �e /(jnS 1- 4-X'htl' LLC Non-Discharge : t_,.- - UIC
Permit Name(if different): _ NPDES Other
Facility Address: "'I)_h4-7 �/n' J frt'� TYPE OF PERMITTED OPERATION BEING MONITORED
rii7/.U,'Q/1_. r` NC p'��1�9 County �(
`Y� --., �c r (7X e ❑�Lgag/o ❑Remediation:Infiltration Gallery
1 :Stele: t 9.,
/')/) r pray Field ❑Remediation:
Contact Person: I I')� /-L-': , on,S Telephone#: eis:217- T1 -a.j d 0 0 Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name: (A S t_ Q t mS e No.of wells to be sampled: '3 0 Water Source Heat Pump ❑Other.
(from PempF) ,I
AMPLING INFQR N . i If WELL
WELL ID NUMBER(from Permit): -0 C Date sample collected: 3 -J 0".2 J FIELD A!QALYSES: WAS
Well Depth: IC ft. Well Diameter: In. pH biai units Temp. I °C DRY at
Depth to Water Level: 2$, time of
ft.below measuring point Screened Interval: 30 ft. toft. Spec.Cond. ' ?i(,p µMhos sampling,
:,
Measuring Point is __3 ft.above land surface Relative M.P.Elevation: 2h1 , ft. Odor ' n e n f check
Volume of water pumped/bailed:before sampling::.,�C. 3 gallons Appearance . ,),Q }r 7 i I/ CI V t.4 L\ here:
Samples for metals were oolipt U ad unfiltered: �YES ❑NO and field acidified: ❑YES ❑NO a /
Ijilii3FLATORYINFORlibgipN
/ -�fil�
Date sample analyzed: eg(e S e• Ln 2 (1es,..,I-4s. Laboratory Name: lead( -Dec P .L,�..4hC. Certification No. 1 5—O
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD mg/I Nitrite(NO2)as N mg/I Pb-Lead mg/I
Coliform:MF Fecal . /100m1 Nitrate(NO3)as N 1 Qa/ mg/I Zn-Zinc Da D 3 mg/I
Coliform:MF Total /100m1 Phosphorus:Total as P (;),RD mg/I
(Note: Use MPN method r«Mg*turbid.o;,pi s) Orthophosphate mg/I Other(Speciff Compounds and Concentration Units):
Dissolved Solids:Total 115. mg/I Al-Aluminum mg/I
pH(when analyzed) (P.A units Ba-Barium • mg/I i a PI Z-' 5.$ ri 1 L
TOC ( N ) 0 mg/I Ca Calcium mg/I p7 n .5 - �.J p I L
Chloride • 9. mg/I Cd-Cadmium mg/I /pima(el)4 C 'p—(,�i / L
Arsenic :D CND ) mg/I Chromium:Total ' mg/I T-/V,91Uc}, o?,Oa J L
Grease and Oils mg/I Cu-Copper O,OD(o" mg/1 ORGANICS:;(by GC,GC/MS,HPLC)
Phenol mg/I Fe-Iron •mg/1 (Specifytestland.method#.ATTACH LAB REPORT.)
Sulfate mg/I HgMercury
g - mg/1 Report Attached? ❑ Yes(1) ❑ No(0)
Specific Conductance ZS;
v µMhos :P 1K.-Potassium 5, t tng/i VOC ,method#Total Ammonia mg/I Mg-Magnesium .. mg/I ,method#
IAmmonle Nitrogen;N1,as N;(maenia Nitrogen:Total) Mn-Manganese mg/I ,method#
TKN as N g n O 0 mg/I Ni-Nickel mg/I ,method#
For Remedlation Systems Only( h • Oil•.day; Influent Total VOCs: 'mg/L Effluent Total,VOCs: mg/L VOC Removal%
, -. .r, 4,,, . ,r:. .... . :n.-'1..
C. 1�r1el r r 6:nn.3 ' Bia , )Pc . 1u er (1)-sol r� H-
Pe'm►ittee(or A prized Apt t)Name and Title-Please print or type Signature.f Pe Klee(or Autho ed Agent) .
CCCVVJVJJ (Date)
GW-58 Rev.1/2007
.?

GW-59A COMPLIANCE REPORT FORM Permit # W 0 06 -30 7
(Submit one each monitoring period with GI -59 forms.)
I
Enter date monitoring results were due. _ D-DL) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
N
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Officefor guidance.
4
Are any monitored constituents equal to or above the established standards?
YES
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located, contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation
fines, and/or penalties.
g
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current G W-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report GW-59A) is true and complete to the best of my knowledge.
Signay f Permittee (or Authorized Agent) Date
l
GAN -59A 12/8/21103

WATER TECH
, - .
5 Pinewood Plaza Drive -P.O. Box 1056
Granite Falls, NC 28630
Phone[phone]-Fax [phone]
CLIENT: Case Farms Hatchery PHONE NUMBER: 828-438-6900 ext.6975
c/o Cindy McGinnis TYPE SAMPLE: n/a
Manager No. LOCATIONS: 4
SAMPLER NAME: I{���•u�C�,,
Sample Collection Information TYPE CONTAINERS
Sample Location DATE TIME TEMP. Grab! No Plastic! ANALYSIS REQUIRED
Facility Name - Composite Glass
Effluent o Grab 8 Plastic Fecal Coliform, Chloride, TDS
3/(aA�is �O Boo-5, TSS, Conductivity
NO3-N,TKN, NH3-N
Monitoring Well#3 Grab 12 Plastic! TDS Chloride, MBAS,
3rrra/z( (.3:3o a ( Glass i tt. (L, Conductivity
nrateriMa
NH3-N. NO3-N, T.P., TKNPlas
Monitoring Well#4
340/z !' 3�
Z Q Grab 12 Giassl Same As#3
1
Monitoring Well#57Jp/Z(,��f,m0 Z f o Grab 12 Glass/ Same As#3
Relinquished By: Date: Time: Recieved y; Date: Time:
67_,577/
Reiinquis By: Date: Time: Re eived Date: Time:
PRESERVATION:
Goo!4°C
/9442SO4
j J NaOH
0,HNO3
SDechlornating Agent
j J Other
SAMPLE TEMP. @ LAB(°C) off,
Chlorine Residual A- mg/I
NC CERTIFIED LAB#50

lifirrmirscH LABS inc.
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS,NORTH CAROLINA 28630
[phone]
SAMPLE: Case Farms-Hatchery COLLECTION DATE: 3/10/2021
PERMIT#: COLLECTION TIME: 15:00
ADDRESS: Case Farms Hatchery RECEIVED DATE: 3/10/2021
RECEIVED TIME: 15:30
REPORTED: 4/8/2021
ANALYSIS
ANALYSIS EFFLUENT UNITS DATE , ANALYST
BOO 649 mg/L 3/11/21 Jdg
TSS 112 mg/L 3/12/21 jrg
NH3 45.30 mglL 3/12/21 jrg
Fecal Coliform 1020 /100mL 3/10/21 jrg
Conductivity 771 um hos/cm 3/11/21 jrg
NO3-N <0.1 mg/L 4/1/21 jdg
TKN 80.00 mg/L 4/5/21 jdg
T.Nitrogen 80.00 mg/L 4/5/21 jdg
T.Phosphorus 5.02 mg/L 4/5/21 jdg
Chloride 49 mg/L 3/12/21 lag
TDS 465 mg/L 3/11/21 lag
' ci•F : . ' '• , ", `:• .* 2.7 1•41;e'r;.,,,•-•
•
•
LOG ID: 2103-192 REPORTED BY: NC CERTIFIED LAB#50
6114,
Tony Gragg,Lab Supervisor

TEA TECH LABSlr1c.
POST OFFICE BOX 1056 • 115 PINEWOOD PLAZA DR.
GRANITE FALLS,NORTH CAROLINA 26630
[phone]
SAMPLE: Case Farms-Hatchery-MW#3 COLLECTION DATE: 3/10/2021
PERMIT#: COLLECTION TIME: 13:30
ADDRESS: Case Farms Hatchery RECEIVED DATE: 3/10/2021
RECEIVED TIME: 15:30
REPORTED: 4/8/2021
ANALYSIS
ANALYSIS RESULTS UNITS: DATE ANALYST
TDS 69 mg/L 3/11/21 lag
Conductivity 115 umhos/cm 3/11/21 jrg
NH3 <1.0 mg/L 3/12/21 jrg
Chloride 10.0 mg/L 3/12/21
Metals see attached
NO3-N <0.1 mg/L 4/1/21 jdg
TKN 4.20 mg/L 4/5/21 jdg
T.Nitrogen 4.20 mg/L 4/5/21 jdg
T. Phosphorus 0.65 mg/L 4/5/21 jdg
•
j.. - •
LOG ID: 2103-193 REPORTED BY: NCB�CERTIFIED LAB#50
f /n .
Tony Gragg,Lab Supervisor

HT M TECH LADS.Inc.
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS,NORTH CAROLINA 28630
[phone]
SAMPLE: Case Farms-Hatchery-MW#4 COLLECTION DATE: 3/10/2021
PERMIT#: COLLECTION TIME: 14:30
ADDRESS: Case Farms Hatchery RECEIVED DATE: 3/10/2021
RECEIVED TIME: 15:30
REPORTED: 4/8/2021
ANALYSIS
ANALYSIS RESULTS UNITS DATE ANALYST
TDS 50 mg/L 3/11/21 lag
Conductivity 84 umhos/cm 3/11/21 jrg
NH3 <1.0 mg/L 3/12/21 jrg
Chloride 10.0 mg/L 3/12/21 lag
Metals see attached
NO3-N <0.1 mg/L 4/1/21 jdg
TKN 2.80 mg/L 4/5/21 Jdg
T.Nitrogen 2.80 mg/L 4/5/21 jdg
T.Phosphorus <0.16 mg1L 4/5/21 jdg
- I
LOG ID: 2103-194 REPORTED BY: NCflit
CERTIFIED LAB#50
•
Tony Gragg,Lab Supervisor

TER TECH Laosi 1c.
POST OFFICE BOX 1058 • /15 PINEWOOD PLAZA DR.
GRANITE FALLS,NORTH CAROLINA 28630
[phone]
SAMPLE: Case Farms-Hatchery-MW#5 COLLECTION DATE: 3/10/2021
PERMIT#: COLLECTION TIME: 14:00
ADDRESS: Case Farms Hatchery RECEIVED DATE: 3/10/2021
RECEIVED TIME: 15:30
REPORTED: 4/8/2021
ANALYSIS
ANALYSIS RESULTS: , UNITS ; DATE ANALYST>
TDS 45 mg/L 3/11/21 lag
Conductivity 76 umhos/cm 3/11/21 jrg
NH3 <1.0 mglL 3/12/21 jrg
Chloride 9.5 mg/L 3/12/21 lag
Metals see attached
NO3-N <0.1 mg/L 4/1/21 jdg
TKN 2.00 mg/L 4/5/21 jdg
T.Nitrogen 2.00 mg/L 4/5/21 jdg
T. Phosphorus 0.20 mg/L 4/5/21 jdg
LOG ID: 2103-195 REPORTED BY: NC CERTIFIED LAB#50 TFC46.41411
Tony Gragg,Lab Supervisor

Pace Analytical Services,LLC
aceAnalytical® 1377 South Park Drive
Kernersvllle,NC 27284
- www.pacalabs.corn
[phone]
ANALYTICAL RESULTS
Project: CASE FARMS
Pace Project No.: 92527251
Sample: CASE FARMS MW3 Lab ID: 92527251001 Collected: 03/10/21 13:30 Received: 03/11/21 10:35 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method:EPA 200,7 Rev 4.41994 Preparation Method:EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Arsenic ND mg/L 0,010 1 03/19/21 02:14 03/21/21 18:36 7440-38-2
Copper ND mg/L 0,0050 1 03/19/21 02:14 03/21/21 18:36 7440-50-8
Potassium ND mg/L 6.0 1 03/19/21 02:14 03/21/2118:36 7440-09-7
Sodium 7.8 mg/L 5.0 1 03/19/21 02:14 03/21/2118:36 7440-23-5
Zinc ND mg/L 0.010 1 03/19/21 02:14 03/21/21 18:36 7440-66-6
5310E TOC Analytical Method:SM 5310B-2011
Pace Analytical Services-Asheville
Total Organic Carbon ND mg/L 1.0 1 03/21/21 19:20 7440-44-0
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/14/2021 03:32 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 23

Pace Analytical Services,LLC
aceAnalytical® 1377 South Paris Drive
Kernersvllle,NC 27284
www.pacelaba.com [phone]
ANALYTICAL RESULTS
Project CASE FARMS
Pace Project No.: 92527251
Sample: CASE FARMS MW4 Lab ID; 92527251002 Collected: 03/10/21 14:30 Received: 03/11/21 10:35 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.41994
Pace Analytical Services-Asheville
Arsenic ND mg/L 0.010 1 03/19/21 02:14 03/21/21 18:39 7440-38-2
Copper ND mg/L 0.0050 1 03/19/21 02:14 03/21/21 18:39 7440-50-8
Potassium 5.4 mg/L 5.0 1 03/19/21 02:14 03/21/21 18:39 7440-09-7
Sodium 5A mg/L 5.0 1 03/19/21 02:14 03/21/21 18:39 7440-23-5
Zinc 0.035 mg/L 0.010 1 03/19/21 02:14 03/21/21 18:39 7440-86-6
5310B TOC Analytical Method:SM 5310B-2011
Pace Analytical Services-Asheville
Total Organic Carbon ND mg/L 1.0 1 03/21/21 19:35 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/14/2021 03:32 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 23

ace Analytical a
Pace Analytical Services,LLC
1377 South Park Drive
Kernersvllle,NC 27284
www.pacelabs.sam [phone]
ANALYTICAL RESULTS
Project: CASE FARMS
Pace Project No.: 92527251
Sample: CASE FARMS MW5 Lab ID: 92527251003 Collected: 03/10/21 14:00 Received: 03/11/21 10:35 Matrix:Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Arsenic ND mg/L 0.010 1 03/19/21 02:14 03/21/21 18:42 7440-38-2
Copper 0.0069 mg/L 0.0050 1 03/19/21 02:14 03/21/21 18:42 7440-50-8
Potassium 5.1 mg/L 5.0 1 03/19/21 02:14 03/21/21 18:42 7440-09-7
Sodium 5.8 mg/L 5.0 1 03/19/21 02:14 03/21/21 18:42 7440-23-5
Zinc 0.035 mg/L 0.010 1 03/19/21 02:14 03/21/21 18:42 7440-66-6
5310E TOC Analytical Method:SM 5310B-2011
Pace Analytical Services-Asheville
Total Organic Carbon ND mg/L 1.0 1 03/21/21 19:51 7440-44-0
•
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except In full,
Date:04/14/2021 03:32 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 23

Analytical Environmental Services,Inc Date: 15-Mar-21 •
Client: Pace Analytical Services,Inc. Client Sample ID: CASE FARMS MW3
Project Name: 92527251 Collection Date: 3/10/2021 1:30:00 PM
Lab ID: 2103F33-001 Matrix: Aqueous
Analyses Result Reporting Qual Units BatchlD Dilution Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde BRL 311884 1 03/13/2021 17:12 RF
�'b �&/L
•
•
•
•
Qualifiers: • Vella,exceeds maximum contaminant level E Estimated(value above a uantitatioe range)
BRL Below reporting limit S Spike Recovery oulsido limits due to matrix
H Holding times for preparation or analysis exceeded Nan Set case narrative
N Analyte not NBLAC certified r Analyzed in the lab which is a deviation from the method
B Analyse detected in the associated method blank < Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Page 17 of 23
Page 4 of 10

Analytical Environmental Services,Inc Date: 15-Mar-21
Client: Pace Analytical Services,Inc. Client Sample ID: CASE FARMS MW4
Project Name: 92527251 Collection Date; 3/10/2021 2:30:00 PM
Lab ID: 2103F33-002 Matrix: Aqueous
Reporting Dilution
Analyses Result Qual Units BatchlD Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde BRL tt 311884 1 03/13/2021 17:26 RE
0. os" fill()
(J
•
Qualifiers; • Value exceeds maximum contaminant level E Estimated(value above quantitation range)
BRL Below reporting limit S Spike Recovery outside limits due to matrix
H Holding times for preparation or analysis exceeded Narr See ease narrative
N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method
II Acolyte detected in the associated method blank < Less than Result value
> Greater than Result value 1 Estimated value detected below Reporting Limit Page 18 of 23
Page 5 of 10

•
•
Analytical Environmental Services,Inc Date: I5-Mar-2l
Client: Pace Analytical Services,Inc. Client Sample ID: CASE FARMS MW5
Project Name: 92527251 Collection Date: 3/10/2021 2:00:00 PM
Lab ID: 2103F33-003 Matrix: Aqueous
Reporting Dilution
Analyses Result Qual Units BatchID Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde BRL2'7p �u3p+L 311884 1 03/13/2021 17:40 RF
D. as ���
•
Qualifiers: * Value exceeds maximum contaminant level E Estimated(value above quantitation range)
IIRL Below reporting limit S Spike Recovery outside limits duo to matrix
H Holding times for preparation or analysis exceeded Narr See case narrative
N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method
E Analyte detected in the associated method blank < Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Page 19 of 23
Page 6 of 10

Meritech, Inc.
Environmental Laboratory
t Laboratory Certiflcation No.165
Contact: Cathy Gragg Report Date: 3/17/2021
Client: Water Tech Labs, Inc
5 Pinewood Plaza Drive
Granite Falls, NC 28630 Date Sample Rcvd: 3/11/2021
Meritech Work Order # 03112178 Sample: Case Farms MW-3 Grab 3/10/21
Parameter Result Analysis Date Reporting Limit Method
MBAS (as LAS 340) <0.10 mg/L 3/11/21 0.10 mg/L SM 5540 C
Meritech Work Order## 03112179
Parameters Result
Sample: Case Farms MW-4 Grab
Analysis gate (Reporting Limit
3/10/21
Method
MBAS (as LAS 340) <1.00 mg/L 3/11/21 1.00 mg/L SM 5540 C
Meritech Work Order # 03112180 Sample: Case Farms MW-5 Grab 3/10/21
Parameters Result Analysis Date Reporting LLimitMethod
MBAS (as LAS 340) <0.10 mg/L 3/11/21 0.10 mg/L SM 5540 C
t hereby certify that f have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]