HomeMy WebLinkAboutNCG090034_Monitoring Report_20220225STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 090000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2021
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Inolex Chemcial Co.
PERSON COLLECTING SAMPLES) Angie Young V .-14
CERTIFIED LABORATORY(S) Pace Analytical Lab # 329 7-
Lab # y
Part A: Specific Monitoring Requirements
COUNTY Mecklenburg
PHONE NO. 7t 04 ) 572-0790
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 3.
Outfall
Date
50050
No.
Sample
Collected
Total
Flow (if app.)
Total
Rainfall
pH
pH
TSS
Cadmium
Chromium
Lead
mo/dd/yr
MG
inches
Field
Lab
mg/L
mg/L
mg/L
mg/L
SW-1
02/03/2022
.24
8.37
6.3
24
< 0.003
< 0.905
< 0.075
NCDFQ nanchmark
1
6-9
6-9
100
0.003
1 0.905
0.075
Docs this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Oyes ®no
(if )es. complete Part B)
Fort SWU-247, last revised 6/12,2015
Page 1 of 2
STORM EVENT CHARACTERISTICS:
Date 2/24/2022
Total Event Precipitation (inches): .24
Event Duration (hours): (only if applicable - see pen -nit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable - see pern it.)
Mail Original and one copy to:
Division of Energy Mineral and Land Resources
Attn: Central Files
1617 Mail Service Center
Raleigit Nortli Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fine
,sand imprisonment for knowing violations."
(Signacute of
-2 46
2 Z.
(Date
Fonn S WU-247, last reWsed 6/1 1201 a
Page 2 of 2
r
P'aceAnalyical
Report of Analysis
INOLEX
12345 Steele Creek Rd
Charlotte, NC 28273
Attention: Alanna Smith
Project Name: Stormwater
Project Number: INCLEX, Inc.
Lot Number:XB03067
Date Completed: 02/20/2022
02/21/2022 3:23 PM
Approved and released by:
Project Manager I: Blaire M. Gagne
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The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel 803-791-9700 Fax:803-791-9111 www.pacelabs.com
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PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
INOLEX
Lot Number: XB03067
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 601 OD, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Pace Analytical Services, LLC (formerly Shealy Env+ronmetal Services. Inc)
106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 www pacelabs com
Page 2 of 8
PACE ANALYTICAL SERVICES, LLC
Sample Summary
INOLEX
Lot Number: XB03067
Sample Number Sample ID Matrix Date Sampled Date Received
001 SW1 Aqueous 02/03/2022 0530 02/03/2022
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services. Inc.)
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 wmv pacelabs com
Paize 1 cif S
Inorganic non-metals
Client:INOLEX Laboratory ID: XB03067-001
Description: SW1 Matrix: Aqueous
Date Sampled:02/03/2022 0530
Date Received:02103/2022
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Hexavalent C) 218.6 1 02/10/2022 1558 AAB 02/03/2022 1905 30715
1 (pH) SM 4500-H B-2011 1 02/13/2022 1602 NBW 31643
1 (TSS) SM 254OD-2011 1 02/09/2022 2210 CVR 31301
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Hexavalent Chromium
pH@20.9°C
TSS
18540-29-9 218.6 ND 1.0 ug/L 1
SM 4500-H B-20 6.3 su 1
SM 2540D-2011 24 17 mg/L 1
LOQ = Limit of QuanKation B = Detected in the method blank E = Ouantdation of compound exceeded the calibration range O = Surrogate failure
ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40`76 L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services Inc.)
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com
Page 4 of 8
ICP-MS
Client:INOLEX Laboratory ID:XB03067-001
Description: SW1 Matrix: Aqueous
Date Sampled:02/03/2022 0530
Date Received:02/03/2022
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 02/05/2022 0211 BPK 02/04/2022 0052 30723
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Cadmium
Chromium
Lead
7440-43-9 200.8 ND
7440-47-3 200.8 ND
7439-92-1 200.8 1.6
0.50 ug/L 1
5.0 ug/L 1
1.0 ug/L 1
LOO = Limn of Qua ntitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCSILCSD failure
H = Out of holding time W = Reported on wet weight basis S = MSIMSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www pacelabs.com
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lien' UPS 10 FLAKY LJ Ocher;
u�ody seal~ prchcnr on 'lie cooler?
YL- Lij flu J N:1 2. 1fCu3tody scats were •rt iwil, were tt:ey inlart andtulbrukeit?
p. I Strip _21-952 C1110: ine Strip 11j: 14A T.sted r
Orig-inal temlicrature upon mceipt i Derivett;Corrcctedi temperature uFrur: rcc:.clipt %Sjlid Silau•Cup 1U: RSA
, IA , NA (%C NA r VA �,C NA -CIA mC
Method: J�]'i'em peraturc Blank B C41.16S M Gun ID: 5 1 R Cur, C'umcctinr Factor: tt
h".etHuil t1f cuolart: 0 Wet Ice ❑ Ice Plackc. ❑ ony kr ] None _
❑ Yes ❑ Xv [J NA if IMPerahlre of any ucu,lcr t-X=40d e.0"C, was Project Manager Nr tifi•.tl'r
PNt wAs Nod ied by, phbirc f email ; fzice'4c,-Face (cit'clr. urcr.i.
J Yes Na r NA •=. L thr- upramercial ccurriar'5 padking A.-p actachecl in, this f�mrcl? -
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7- Were sample IDs liMud ur. nil s3nlole containers'
. Was c(ACTciolt dik & timc lister, can ti:e COC?
_
WL5 tullcc(ion dare A- time JsLeJ ar) all sarlhle conl.•t t-er i?
10. D:d ali crin,ainei label information (ID. (1ale: Lirrte) %vil".1.hC COC?
1 I. 1�'etc L-URN 10 be perlbrmcd iin---d -mi Lhc ('0C.? -
12. Did :r:l SHMPiCS arrive ill tale pluper c1lil'sin?rs for cacti tea( urnVor in good condition
fllnbroken, Eels im. cre.)?
13. Wus w. gwtte snirpla volur_lc smilabte'!
14. We:c all ;a,:,llle� r C6%led within I* the hn;t ;rgrimr or 48 hours. whizhrycr eonift FrsL?_ _
5. Wcru nny sw-n les containers lli5SjD9!Mc-*5 (yirc;c one) samples Not lister; on CC}C?
❑�1.1 i 6. For VOA and RSK-17 S sampir,, wiwc bubbles (,%mn in diamcw-i)
to ally o Ibc VOA vials?
'A 17, Wcrc al] DROA--wtalsr'ru[riunr snvi3les meeived a[ u pH of <:2?
✓ N7 1 R. Were all cyanide sun pl,:s roucived at a pH > 12 arui ~»lode satnpins mucived a' a p.14 > y,
�N4I 19. Worc ai ariplicHhle N9l.+T;� kvilrlicle�pl:cnul;G7S. U606.a (=�. GJM�:l ) Samples irec (if
❑Y05i ❑Nol ON
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20. were client r=arksr'reqursts (i.e. tLqu:3tcd d'.lutions, N1'?V1SD des ignnidons, etc..,)
co.~►cctly u;trlscribud frorn the f_`OC into thu comment section in LMS?
Was tht: c ;artc ntunbrr ',istcd on the r.;lntriner lebe1? if
Sample Promervatittn (Must be completed tirlr amp sanlple(sl incorrectly pre:9ervec. or with hcadspacr.)
Srrmple(s) r+^ v►�ere received incur ec;tly rc3er wed tr d verc adjume l ar.
in sample rtit liVirtg wiIn N~ tnL ofcircl�_ one: 1121;0,1. � p, c „ NA � curdin�,iY
—.._ . H`d0_, HC'1, h,a{)l l n�:in�R ,.
Time o'}.�,r nation KA (i more than c�nr }lroser4lt;vc is nccdre. l,:r:isc t)Ole io tli_ ccrnments below.
Sample{.yl.�A .. --
_. _: err received with bubble:; : -fi mnt in diancLer.
5ampies(s) •'� _ tvW�c -coeived with TRC = 0.5 mG'l. flrig19 is If(?) trill,mere
,Ajustcd accordingly in salnpic rmcivitli vvit11 sodium L1Josu:Ja'e (Na.LSr0,) tvilh Sltcaly if):
Mt lrarcoc c labels applied by- 1111:'H _ _ I')a:c: 1r-7'01r7C22 _
Conimc:rlt.s'
Pace Analytical Services, LLC (formerly Shealy Environmental Services. Inc)
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791.9111 www pacelabs com
Page 8 of 8