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HomeMy WebLinkAboutNCG090034_Monitoring Report_20220225STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 090000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2021 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Inolex Chemcial Co. PERSON COLLECTING SAMPLES) Angie Young V .-14 CERTIFIED LABORATORY(S) Pace Analytical Lab # 329 7- Lab # y Part A: Specific Monitoring Requirements COUNTY Mecklenburg PHONE NO. 7t 04 ) 572-0790 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 3. Outfall Date 50050 No. Sample Collected Total Flow (if app.) Total Rainfall pH pH TSS Cadmium Chromium Lead mo/dd/yr MG inches Field Lab mg/L mg/L mg/L mg/L SW-1 02/03/2022 .24 8.37 6.3 24 < 0.003 < 0.905 < 0.075 NCDFQ nanchmark 1 6-9 6-9 100 0.003 1 0.905 0.075 Docs this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Oyes ®no (if )es. complete Part B) Fort SWU-247, last revised 6/12,2015 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 2/24/2022 Total Event Precipitation (inches): .24 Event Duration (hours): (only if applicable - see pen -nit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable - see pern it.) Mail Original and one copy to: Division of Energy Mineral and Land Resources Attn: Central Files 1617 Mail Service Center Raleigit Nortli Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine ,sand imprisonment for knowing violations." (Signacute of -2 46 2 Z. (Date Fonn S WU-247, last reWsed 6/1 1201 a Page 2 of 2 r P'aceAnalyical Report of Analysis INOLEX 12345 Steele Creek Rd Charlotte, NC 28273 Attention: Alanna Smith Project Name: Stormwater Project Number: INCLEX, Inc. Lot Number:XB03067 Date Completed: 02/20/2022 02/21/2022 3:23 PM Approved and released by: Project Manager I: Blaire M. Gagne r' accREo 2W joAOM TNI a %0 4'�a0/a,�baiysa .O O� s�.. Jed, The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel 803-791-9700 Fax:803-791-9111 www.pacelabs.com llagc I orb PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative INOLEX Lot Number: XB03067 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Where sampling is conducted by the client, results relate to the accuracy of the information provided, and as the samples are received. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace") Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or discussed below. Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2- dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 601 OD, VOC SM 6200 B-2011, Fecal Coliform Colilert-18. If you have any questions regarding this report, please contact the Pace Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. Pace Analytical Services, LLC (formerly Shealy Env+ronmetal Services. Inc) 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 www pacelabs com Page 2 of 8 PACE ANALYTICAL SERVICES, LLC Sample Summary INOLEX Lot Number: XB03067 Sample Number Sample ID Matrix Date Sampled Date Received 001 SW1 Aqueous 02/03/2022 0530 02/03/2022 (1 sample) Pace Analytical Services, LLC (formerly Shealy Environmental Services. Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 wmv pacelabs com Paize 1 cif S Inorganic non-metals Client:INOLEX Laboratory ID: XB03067-001 Description: SW1 Matrix: Aqueous Date Sampled:02/03/2022 0530 Date Received:02103/2022 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Hexavalent C) 218.6 1 02/10/2022 1558 AAB 02/03/2022 1905 30715 1 (pH) SM 4500-H B-2011 1 02/13/2022 1602 NBW 31643 1 (TSS) SM 254OD-2011 1 02/09/2022 2210 CVR 31301 CAS Analytical Parameter Number Method Result Q LOQ Units Run Hexavalent Chromium pH@20.9°C TSS 18540-29-9 218.6 ND 1.0 ug/L 1 SM 4500-H B-20 6.3 su 1 SM 2540D-2011 24 17 mg/L 1 LOQ = Limit of QuanKation B = Detected in the method blank E = Ouantdation of compound exceeded the calibration range O = Surrogate failure ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40`76 L = LCS/LCSD failure H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure Pace Analytical Services, LLC (formerly Shealy Environmental Services Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 8 ICP-MS Client:INOLEX Laboratory ID:XB03067-001 Description: SW1 Matrix: Aqueous Date Sampled:02/03/2022 0530 Date Received:02/03/2022 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 02/05/2022 0211 BPK 02/04/2022 0052 30723 CAS Analytical Parameter Number Method Result Q LOQ Units Run Cadmium Chromium Lead 7440-43-9 200.8 ND 7440-47-3 200.8 ND 7439-92-1 200.8 1.6 0.50 ug/L 1 5.0 ug/L 1 1.0 ug/L 1 LOO = Limn of Qua ntitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCSILCSD failure H = Out of holding time W = Reported on wet weight basis S = MSIMSD failure Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www pacelabs.com I'age 5 of R 8.10 9 09i:d woo-sgelaoed-mmm LM-L6L (£08)xed OOM-WL (£0W ZLL6Z OS 'eigwnioo;soM aniJp W{od a6elueA 9OL {•oul 'saolAieS,eluewuounu3,!leads Aliewjo1} C)'17 `saojnjaS jeoijhjeuy aoed s}uewn3oa snoeuslla3siL4j PUB ApolsnC) jo uisuC) o m rn 0 < fD m D 7 7 a (D 0 o< rD CD �r n o �Q 1 Cn( n w V C I o(:D' m o� O y w �.t `A� Slealy Er vi rorirriental Semoas.:rc. CWA ! NPOES 015i'yanmov Point Crive �'`� 4. b',rest Ceilu:r.iaia. Sold I CLrolino 29''r2 Nlil'i bor Chain of Custody Record Telephc,ne No. (;,03} 79' -8'OC Fax No. (803;1 791-91' 1 • tiw,e.she;rhrla7. �m :Rent PODOn To Cantact sort•. Y'3 Slcn -- - ^anlR hki !nclex Ancie Young x • 1 a--- .� U (3 1. t�ddress Frirldr N-3rp= 1-lvl � o, J �tU k_Vj ���,v _ .. rlerd rafamme s { . . pH. fuhrlp. M, car be tacerdbd h c'=ck t3xe;, of r cly 48U w, Zip Ccjt Telertlw�:I: ;rb. ! Fsx i�lo. + 1 rr.4 HR ( hi7.1ber D1 S:r,r w, s G:ar tti r ' J Nrrjar:l Nva-i r :j .)Utlfjl[1 ,ncle> .r_r,m �; v 1 4 j 1 pn+.:na�n•.... rJt, lPr":^rl'J��rTt=' IP � R:m�ef M ,,, I r. c'J Q. i` l I I '14TI f�iM .�� �fi�; c• L. , l oa c �c ri0 C U scnF :., � Oe3'wrFtian - ' ` XBO3067 c:anralrcm: tr each unple riav as NtE Time y% L, � � ", 4Vn:.i� on r,rw �<•�Es;• yr. 2r-• lnE r �� = l,Rstrbt 9 m y L, Ocli ; p►1r Start OD X I X X _ _ _ .• *..,�qr. rt jj � DYE l rVM57 rl Slay... _ ��"�• I � — FI:I'9r I :36'I t x t FnSh rossitte €iazarr•= 1c='Ji tii:tAc. a8l:2pir E.i; i, ti;�! ICamrranl A e'en-r•larard F ar- -n :ir. W-i Irr4tv.; II— li.-r,sir to Olzmt Dicpzv, t)y -at PaiSan Tum Aiounf Time F.egwn=a ;=•:Oi .14>:rr;,rcoa! requ..ed "or expezlite-Z TAT, QC Reculrements LT -owe 3:evivl Q=.a-43rd �_j P�01 rleF.se epee: % t. P�AnquIshe0 t. i Sjrnrs: - Jate a ,. Px- y rived 17atc Ire ' Um,; ai) ')F_te zz oy of 1 i, r»IuK;t .c3 b�/i �1 iTiM/a� 2. P.ccciv 3 S �1. 1 .1 L �n � (3� c� 3. Dedawshed by uate Tirao ?lab reac,:y r:rc-_ ec y XLC4_w=n__= Wte Time _' Note: A€! samples are r tailted for six weeks from receipt unless other �.a3 USE c 44LY €� Rece .'." rnp. ') L' Ter:r ,. Munk arrangements are made R�:eivdc On lu:• i;r:r.-k) + � ter n ica Far:k • e i ; ", C. i m D Z D r 0 D r m ;o 0 m U) r r 0 PACE ANALYTICAL SERVICES, LLC { :tient: In•�1er ��r�•fr.- ERR.. Means of rec.cip:; ✓ Puce Yesl 'nj 11. were Samples ReceFptChmklist (SIRC)(ML0018C-1s) Rcv_tad:9J7Q/zu2o Issuing Auit.inrity• FaCe ENV - WCCL F:aga I ni Z SaMPIe Receipt Checklist (SIZC) Ccwl_r :nspceted by,'daw !Rv.' to 121 T,10,= (.t)r. N. XE10306? lien' UPS 10 FLAKY LJ Ocher; u�ody seal~ prchcnr on 'lie cooler? YL- Lij flu J N:1 2. 1fCu3tody scats were •rt iwil, were tt:ey inlart andtulbrukeit? p. I Strip _21-952 C1110: ine Strip 11j: 14A T.sted r Orig-inal temlicrature upon mceipt i Derivett;Corrcctedi temperature uFrur: rcc:.clipt %Sjlid Silau•Cup 1U: RSA , IA , NA (%C NA r VA �,C NA -CIA mC Method: J�]'i'em peraturc Blank B C41.16S M Gun ID: 5 1 R Cur, C'umcctinr Factor: tt h".etHuil t1f cuolart: 0 Wet Ice ❑ Ice Plackc. ❑ ony kr ] None _ ❑ Yes ❑ Xv [J NA if IMPerahlre of any ucu,lcr t-X=40d e.0"C, was Project Manager Nr tifi•.tl'r PNt wAs Nod ied by, phbirc f email ; fzice'4c,-Face (cit'clr. urcr.i. J Yes Na r NA •=. L thr- upramercial ccurriar'5 padking A.-p actachecl in, this f�mrcl? - ✓ Yez El No S. We re pmper ctts'ody prouc iures (relicryuishcdJr>rcci•:eel) fol:owed^ 7 Yes U Nal 116, Werecttplt: IUS limed <ln t{tL COC^ Y'c51 n Nu 0 Ycsl ON 0-Yes ❑\-o J Y:s iti o YeC No M Yes Ono 11C 7- Were sample IDs liMud ur. nil s3nlole containers' . Was c(ACTciolt dik & timc lister, can ti:e COC? _ WL5 tullcc(ion dare A- time JsLeJ ar) all sarlhle conl.•t t-er i? 10. D:d ali crin,ainei label information (ID. (1ale: Lirrte) %vil".1.hC COC? 1 I. 1�'etc L-URN 10 be perlbrmcd iin---d -mi Lhc ('0C.? - 12. Did :r:l SHMPiCS arrive ill tale pluper c1lil'sin?rs for cacti tea( urnVor in good condition fllnbroken, Eels im. cre.)? 13. Wus w. gwtte snirpla volur_lc smilabte'! 14. We:c all ;a,:,llle� r C6%led within I* the hn;t ;rgrimr or 48 hours. whizhrycr eonift FrsL?_ _ 5. Wcru nny sw-n les containers lli5SjD9!Mc-*5 (yirc;c one) samples Not lister; on CC}C? ❑�1.1 i 6. For VOA and RSK-17 S sampir,, wiwc bubbles (,%mn in diamcw-i) to ally o Ibc VOA vials? 'A 17, Wcrc al] DROA--wtalsr'ru[riunr snvi3les meeived a[ u pH of <:2? ✓ N7 1 R. Were all cyanide sun pl,:s roucived at a pH > 12 arui ~»lode satnpins mucived a' a p.14 > y, �N4I 19. Worc ai ariplicHhle N9l.+T;� kvilrlicle�pl:cnul;G7S. U606.a (=�. GJM�:l ) Samples irec (if ❑Y05i ❑Nol ON rt:.4111al c?ilc�rine:' 20. were client r=arksr'reqursts (i.e. tLqu:3tcd d'.lutions, N1'?V1SD des ignnidons, etc..,) co.~►cctly u;trlscribud frorn the f_`OC into thu comment section in LMS? Was tht: c ;artc ntunbrr ',istcd on the r.;lntriner lebe1? if Sample Promervatittn (Must be completed tirlr amp sanlple(sl incorrectly pre:9ervec. or with hcadspacr.) Srrmple(s) r+^ v►�ere received incur ec;tly rc3er wed tr d verc adjume l ar. in sample rtit liVirtg wiIn N~ tnL ofcircl�_ one: 1121;0,1. � p, c „ NA � curdin�,iY —.._ . H`d0_, HC'1, h,a{)l l n�:in�R ,. Time o'}.�,r nation KA (i more than c�nr }lroser4lt;vc is nccdre. l,:r:isc t)Ole io tli_ ccrnments below. Sample{.yl.�A .. -- _. _: err received with bubble:; : -fi mnt in diancLer. 5ampies(s) •'� _ tvW�c -coeived with TRC = 0.5 mG'l. flrig19 is If(?) trill,mere ,Ajustcd accordingly in salnpic rmcivitli vvit11 sodium L1Josu:Ja'e (Na.LSr0,) tvilh Sltcaly if): Mt lrarcoc c labels applied by- 1111:'H _ _ I')a:c: 1r-7'01r7C22 _ Conimc:rlt.s' Pace Analytical Services, LLC (formerly Shealy Environmental Services. Inc) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791.9111 www pacelabs com Page 8 of 8