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HomeMy WebLinkAboutNCG240019_Monitoring Report_20220531�Ngun v Z P cARcv MECKLENBURG COUNTY Land Use & Environmental Services Agency Solid Waste May 31, 2022 DEQ Mooresville Regional Office Attn: DEMLR Stormwater Program 610 East Center Avenue Suite 301 Mooresville, NC 28115 Attention: DEMLR Stormwater Program Subject: Discharge Monitoring Report Mecklenburg County Compost Central (new) — Certificate of Coverage No. NCG240019 Dear Central Files: Please find enclosed the Discharge Monitoring Report, May 2022, for Mecklenburg County Compost Central (new), a Type I facility located at 140 Valleydale Road, North Carolina. If you have any questions, please contact me at 704-634-7705 or by email at khaliem.adams@mecklenburgcounlync.gov. Sincerely, &/ka'L A/'�— Khaliem Adams Solid Waste Environmental Specialist Enclosed: 2022 DMR PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2145 Suttle Avenue Charlotte, North Carolina 28208 www.wipeoutwaste.com NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG240000 Compost Operations Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG24 0019 Person Collecting Samples: Khaliem Adams Facility Name: Mecklenburg County Compost Central (new) Laboratory Name: Pace Analytical Facility County: Mecklenburg Laboratory Cert. No.: Discharge during this period: ✓❑ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ✓❑ Yes ❑ No If so, which Tier (1, II, or III)? Tier 2 A copy of this DMR Fyas een ploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR ❑✓ Yes []No Date Uploaded: 6 ) oZ oxx Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Code Parameter Outfall1 Outfall Outfall Outfall Outfall N/A Receiving Stream Class N/A Date Sample Collected MM/DD/YYYY 5/23/2022 46529 24-Hour Rainfall in inches 0.60 in C0530 TSSin mg/L(100) 18.6 00340 Chemical Oxygen Demand (120) 134 31615 Fecal Coliform in colonies per 100 ml 7400 (1000) 600 Total Nitrogen in mg/L (30) 3.3 665 Total Phosphorus in mg/L (2) 2.5 400 pH in standard units (6.0-9.0) 7.46 01119 Copper, total recoverable in mg/L <0.020 (0.010) 01051 Lead, total recoverable in mg/ L <0.025 (0.075) 01094 Zinc, total recoverable in mg/ L < 0.020 (0.126) Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average 00552 Non -Polar Oil & Grease NCOIL Estimated New Motor/Hydraulic Oil Usage in gal/month 75gal/month Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee or Delegated Authorized Individual Date Email Address Phone Number aaIal/U Hd egPOH ZZOZ/£Z/s 9t"L I £f7TT T Ilelin0 (mau) lealua:) lsodwo:) A}uno:) 2inqualpalN aldweS o4 past a3ma a;eQ Hd awLL aldweS ummo-1 aldweS aweN /311l3ej aceAnalytical,. www.pacelabs.com May 31, 2022 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: Compost Central 2 Pace Project No.: 92605862 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on May 23, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte • Pace Analytical Services - Peachtree Corners, GA If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard mafthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 (�Ia'cceAnalX cal www.patelabs.com CERTIFICATIONS Project: Compost Central 2 Pace Project No.: 92605862 Pace Analytical Services, LLC 9800 Kinney Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 South Carolina Certification M 99006001 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Drinking Water Cert. #: 99006003 North Carolina Drinking Water Certification #: 37706 Florida/NELAP Certification #: E87627 North Carolina Field Services Certification M 5342 Kentucky UST Certification M 84 North Carolina Wastewater Certification M 12 Louisiana DoH Drinking Water #: LA029 South Carolina Laboratory ID: 99006 VrginiaNELAP Certification M 460221 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 South Carolina Laboratory ID: 99030 Florida/NELAP Certification M E87648 South Carolina Certification M 99030001 North Carolina Drinking Water Certification M 37712 VirginiaNELAP Certification M 460222 North Carolina Wastewater Certification M 40 Pace Analytical Services Peachtree Corners 110 Technology Pkwy, Peachtree Comers, GA 30092 North Carolina Certification M 381 Florida DOH Certification M E87315 South Carolina Certification #: 98011001 Georgia DW Inorganics Certification #: 812 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 5aeeAnalytical www.pacelabs.com SAMPLE ANALYTE COUNT Project: Compost Central 2 Pace Project No.: 92605862 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92605862001 Outfall 1 EPA 1664B ICO 1 PASI-C EPA 1664E ICO 1 PASI-C EPA 200.7 DRB 3 PASI-GA SM 9222D-2015 KDF 1 PASI-C SM 254OD-2015 ZMC 1 PASI-A TKN+NO3+NO2 Calculation MA62 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.01993 MDW 1 PASI-A SM 5220D-2011 JP1 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte PASI-GA = Pace Analytical Services - Peachtree Comers, GA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 acenAnalyfical www.paaelabstom ANALYTICAL RESULTS Project: Compost Central 2 Pace Project No.: 92605862 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Outfall 1 Lab ID: 92605862001 Collected: 05/23/22 11:58 Received: 05/23/22 14:12 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 4.9 1 05123/22 22:45 1664 SGT HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 4.9 1 05/23/22 22:45 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Pace Analytical Services - Peachtree Corners, GA Copper ND ug/L 20.0 1 05/24/2210:25 05/24/2214:54 7440-50-8 Lead ND ug/L 25.0 1 05/24/2210:25 05/24/2214:54 7439-92-1 Zinc ND ug/L 20.0 1 05/24/2210:25 05/24/2214:54 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 7400 CFU/100 mL 1.0 1 05/23/22 17:30 05/24/22 15:34 2640D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services -Asheville Total Suspended Solids 18.6 mg1L 5.0 1 05/25/22 15:05 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Asheville Total Nitrogen 3.3 mg/L, 0.040 1 05/31/22 13:08 361.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 2.8 mg/L 0.50 1 05/25/22 19:50 05/27/22 04:39 7727-37-9 363.2 Nitrogen, NO2/NO3 pros. Analytical Method: EPA 353.2 Rev 2.01993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 0.45 mg/L 0.040 1 05/25/22 09:51 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.01993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 2.6 mg/L 0.050 1 05/24/22 21:45 05/25/22 17:16 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 134 mg/L 25.0 1 05/28/22 00:57 05/28/22 05:51 Date: 05/31/2022 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. u2 D6 Page 4 of 18 Pace Analytical Services, LLC ® a(.0c; y ica! 9800 Kincey Ave. Suite 100 www.pacefabs.com Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92605862 QC Batch: 700005 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92605862001 METHOD BLANK: 3654077 Matrix: Water Associated Lab Samples: 92605862001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 05/23/22 22:45 LABORATORY CONTROL SAMPLE: 3654078 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 32.7 82 78-114 MATRIX SPIKE SAMPLE: 3654079 92605862001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 38.6 30.9 79 78-114 SAMPLE DUPLICATE: 3654080 35717957001 Dup Parameter Units Result Result RPD Qualifiers Oil and Grease mg/L 1.1 U ND Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 Pace Analytical Services, LLC Analytical ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 trwar paaefabs ctua (704)875-9092 QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92605862 QC Batch: 700239 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92605862001 METHOD BLANK: 3655133 Matrix: Water Associated Lab Samples: 92605862001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 05/25/22 00:30 LABORATORY CONTROL SAMPLE: 3655134 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 21.1 106 64-132 MATRIX SPIKE SAMPLE: 3655135 35719177001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 6.2 19.8 34.0 140 64-132 SAMPLE DUPLICATE: 3655136 35719177002 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L 5.OU ND Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 Pace Analytical Services, LLC aftamalytical ® 9800 Kincey Ave. Suite 100 LiuHuntersville, W" pacalabs ecm NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92605862 QC Batch: 700100 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 Metals Total Laboratory: Pace Analytical Services - Peachtree Comers, GA Associated Lab Samples: 92605862001 METHOD BLANK: 3654368 Matrix: Water Associated Lab Samples: 92605862001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 20.0 05/24/2214:45 Lead ug/L' ND 25.0 05/24/2214:45 Zinc ug/L ND 20.0 05/24/2214:45 LABORATORY CONTROL SAMPLE: 3654369 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 1000 1060 106 85-115 Lead ug/L 1000 1060 106 85-115 Zinc ug/L 1000 1090 109 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3654370 3654371 MS MSD 92605862001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 1000 1000 1120 1130 111 113 70-130 2 Lead ug/L ND 1000 1000 1070 1090 106 108 70-130 2 Zinc ug/L ND 1000 1000 1100 1110 109 110 70-130 1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 aceAnalytical vrmpacelab cm QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92605862 QC Batch: 700209 Analysis Method: SM 9222D-2015 QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92605862001 METHOD BLANK: 3654985 Associated Lab Samples: 92605862001 Parameter Units Fecal Coliforms CFU/100 mL SAMPLE DUPLICATE: 3654986 Parameter Fecal Coliforms Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 05/24/2215:34 92605862001 Dup Units Result Result RPD Qualifiers CFU/100 mL 7400 6000 21 u2 Paco Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 Pace Analytical Services, LLC acemalXical ® 9800 Kinney Ave. Suite 100 Yrww.pacelabs.com Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92605862 QC Batch: 700269 Analysis Method: SM 254OD-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92605862001 METHOD BLANK: 3655382 Matrix: Water Associated Lab Samples: 92605862001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 05/25/22 15:03 LABORATORY CONTROL SAMPLE: 3655383 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 228 91 90-110 SAMPLE DUPLICATE: 3656413 92605862001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 18.6 32.6 55 D6 SAMPLE DUPLICATE: 3656414 92605886001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 730 696 5 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92605862 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 700425 Analysis Method: EPA 351.2 Rev 2.01993 QC Batch Method: EPA 351.2 Rev 2.01993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92605862001 METHOD BLANK: 3656043 Matrix: Water Associated Lab Samples: 92605862001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 05/27/22 04:27 LABORATORY CONTROL SAMPLE: 3656044 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.5 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3656045 3656046 MS MSD 92605902003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 0.55 10 10 10.8 10.6 102 101 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3656047 3656048 MS MSD 92605902004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 0.65 10 10 11.5 11.4 109 108 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31 /2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (�1a'CiuMaIXical'o waw pacelaits.eam (704)875-9092 QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92605862 QC Batch: 700054 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.01993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92605862001 METHOD BLANK: 3654216 Matrix: Water Associated Lab Samples: 92605862001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.040 05/25/22 09:30 LABORATORY CONTROL SAMPLE: 3654217 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3654218 3654219 MS MSD 92605305001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 7.3 2.5 2.5 9.3 9.3 81 81 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3654220 3654221 MS MSD 92605434001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 2.2 2.5 2.5 4.4 4.4 90 90 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 IaceAnalyfical wiaiw.pacalaba.com QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92605862 QC Batch: 700258 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92605862001 METHOD BLANK: 3655348 Associated Lab Samples: 92605862001 Parameter Units Phosphorus mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 05/25/2217:08 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 3655349 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3655350 3655351 MS MSD 92605665003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.081 2.5 2.5 2.6 2.5 102 99 90-110 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3655352 3655353 MS MSD 92605665005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.093 2.5 2.5 2.6 2.6 101 102 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 Pace Analytical Services, LLC aceAnalytical ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 WWW pacelabs.com (704)875.9092 QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92605862 QC Batch: 701100 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92605862001 METHOD BLANK: 3659775 Matrix: Water Associated Lab Samples: 92605862001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 05/28/22 05:48 LABORATORY CONTROL SAMPLE: 3659776 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 765 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3659777 3659778 MS MSD 92604831008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 117 100 100 226 210 108 92 90-110 7 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3659779 3659780 MS MSD 92605862001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 134 100 100 235 233 101 99 90-110 1 Results presented on this page are In the units indicated by the "units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/31/2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 Pace Analytical Services, LLC ® 9800 Kincey Ave. Suite 100 (�Ia'CmleMalytical Huntersville, NC 28078 www.paceiabs.com (704)875-9092 QUALIFIERS Project: Compost Central 2 Pace Project No.: 92605862 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31 /2022 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 (�Ia'ccieAnalXical'* www.pacalabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Compost Central 2 Pace Project No.: 92605862 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92605862001 Outfall 1 EPA 1664E 700005 92605862001 Outfall 1 EPA 1664B 700239 92605862001 Outfall 1 EPA 200.7 700100 EPA 200.7 700181 92605862001 Outfall 1 SM 9222D-2015 700209 SM 9222D-2015 700212 92605862001 Outfall 1 SM 254OD-2015 700269 92605862001 Outfall 1 TKN+NO3+NO2 701347 Calculation 92605862001 Outfall 1 EPA 351.2 Rev 2.0 1993 700425 EPA 351.2 Rev 2.01993 700876 92605862001 Outfall 1 EPA 353.2 Rev 2.01993 700054 92605862001 Outfall 1 EPA 365.1 Rev 2.01993 700258 EPA 365.1 Rev 2.0 1993 700280 92605862001 Outfall 1 SM 5220D-2011 701100 SM 5220D-2011 701122 Date: 05/31/2022 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 18 /Dace mn�:un:mx Effective Date: 05/121202205/12/2022 Laboratory receiving samples: 1 Asheville ❑ Eden❑ Greenwood ❑ Huntersville 17 Raleigh[] Mechanicsville❑ Atlanta(] Kernersville❑ �n.on.n:r.an, VY (L�= �}cY PCo�'ect,�H\.[p Wul.: VZ605862 Me r k entUPS USPS ��1 Clientt �" Courier: ❑Fed Ex ❑ Commercial ❑Pace ❑Other:_ �� 62606662 Custody Seal Present? [:]yesa�jr No Sealslntact? ❑Yes DKI pate/Initials Person Examining Contents: rr Packing Material: ❑Bubble Wrap ❑Bubble Bags done El Other Biological Timgrozen?-J 13(1.2 Thermom!Vr: 'J'j'%)jpL� // ❑Yes ❑No N/A I� III Gun ID: gr-,-`(-W--t Type of Ice: []`� Wet ❑Blue ,., /�, Correction Factor: Cooler Temp: — 0 - 6 Add/Subtract (°C) Cooler Temp Corrected (`C): O USDA Regulated Soil (fSK/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC Ithprk man07 i-IYoc f1N„ []None Temp should be above freezing to VC []Samplesout of temp criteria. Samples on ice, cooling process hasbegun Did sunples originate from a foreign source (internationally, Comments/Discrepancy: Chain of Custody Present? ,--,� pares ❑No ❑N/A 1. Samples Arrived within Hold Time? es ON, ❑N/A 2. Short Hold Time Analysis(<72 hr.)? es ONNo ❑N/A 3. Rush Tom Around Time Requested? ❑Yes & No ❑N/A 4. Sufficient Volume? lyres ONO ❑N/A S. Correct Containers Used? -Pace Containers Used? I(es Qf s ONO ONO ❑N/A ❑N/A 6. Containers Intact? es ONO ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes ❑No /A S. Sample. Labels Match COC? -Includes Date/Time/ID/Analysis Matrix:--WT_ Ves ON. ❑N/A 9. Headspace In VOA Vials (>5-6mm)? Oyes ❑Na A 10. Trip Blank Present? Trip Blank Custody Seals Present? Oyes ❑Yes ONO ONO //A INN/A 11, COMMENTS/SAMPLE DISCREPANCY Held Data Required? ❑Yes j]NG Lot 10-of splitcontalners: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Date/Time: Date: Date:- - - - - Qualtrax ID: 69614 Page 1 of 2 Page 16 of 18 ,'-Pace - .......... _ _ _... � ........�.,.........,...�..., ...r... t���,,.,� r M41:14:19CM Effective Date: 05/121202205112/2022 *Check mark top half of box if pH and/or dechlorination is verified and Project # wO ' 926058sz within the acceptance range for preservation samples. PM: MWB Due Date: 05/31/22 _ CLIENT: 92—MECK CO **Bottom half of box is to list number of bottles ***Check all unpreserved Nitrates for chlorine f E Qal GI c N J Ir '� a G�f C7 cc & J E 0 ,n N 0. m d EN) J E 0 a �n . H N a _ ti . m V a O �' J E N v m V f.1 0Q E 0 N � M m ca fl. .J E in N *4 a m V v O Z in a J E " , am m ul E )_ v 0 0 �' Z N E Q M . W a Z Qa u E Q :_ r4 M c9 a 4c J E a r� , M to a N CL a E d �, eyi M t9 a V d' 0 N = J E o „+ NN M a Z Q J E 0 N�n N o`�i .., O > J o 'T at _ +Z. • M 10 O > -' E 0 e{ l'i > � d `0 O > J E 0 � U' > \ v M O > -J >: 0 � ch a Y (� > J c Q o Z Yz � Q r a Z uo M N :: V) E tn M H Z Mz Wnz A «: 1A J E o N N in m z V Q. J E von. N M cc a 0 E Q a ' � o a ro `C> TO c V of E N CN C .7 t] E aQl ai 1 f 2 3- 4 \N\d I N NN\ I I 6 \d I \d I I N\F \N 9 10 it 12 I------ pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time presenntion adjusted Amount of Preservative added Lot a —rtoteMiTeRve t er`� isc�cv affectins k6rth Earoiina comaiiance samniec a rnnu of this fArm will ►,e m...._ .L _ ..__.. Out of hold, incorrect preservative, out of temp, incorrect containers. Qualtrax ID: 69614 .0 11c 1.vf u, Latelina UENR Certification Office (i.e. Page 2of2 Page 17of18 CHAIN -OF -CUSTODY / Analytical Request Document (,Face- The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. S bmittina a sample via this chain of custody constitutes acknoWedament and acceotance of the Pace Terms and Conditions found at httos:1/info.02celabs.com/hubfsloas-standard4erms.odf. Section A Required Client Information: Section B Section C Required Project Information: Invoice Information: r Pane : 1 Of 1 snty Solid Waste Report To: Khaliem Adams Attention: Copy To: Company Name: ,Company: Meddenburg Co Address: 2145 Suttle Ave. ,Charlotte. NC 28208 Address: Regulatory Aaenev Email: khaliem adams enburg ntync.gov Purchase Order it: Puce Quote: :Phone: 980j314-3856 Fax Project Name: Compost Central 2 Pace Project Manager: rnatthew brainard®pacelabs-com. State ! Location Requested Due Dale: Project 0: Pace Profile It: 3207-1. NC Reauested Anal is Flltered W SAMP One Charact tA,Z. o- Sample Ids m MATFUx coos: tAh+►rip wow ow wow wT wasib pro" era P E ID os;'�°''° o r per box. wi WP 1. -) ovw oT st tx! unique Tau* 11 o $ o 8 & a V, a V COLLECTED 6 1 i p U. a Preservatives z START END r: a CL 7 Q �! 2 O 2 S 2 o, O N Z G a 1= 114 y rA ty- w Q. U A $ m z YV S Z rR H c4 ts ts (7 0 $ DATE TIME DATE TIME �- q4 ( t1121 7 xX 44 1 1 1 1 1d 3 4 5 6 -7 8 10 11: 12 CONA1TS ' DATE -. rd 'ACCEEYH IMEADDmO $AIIPLECONDmONB Metals: Cu, Pb. Zn a r -r3 eJsi�- L li-e-- 114 1 Z • V SAfiilPttt NAM£ AND SlGNA'RIRE 0 !r u� �j le a C - 2v) in c} PRINT Name of SAMPLER: n b, C, rr, SIGNATURE of SAMPLER: DATE Signed: a� 0 CM d KC Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfilling out this farm, please visit https://deg.nc.gov/about/divisions/eneruy-mineral-land- resources/enerev-mineral-land-perm its/stormwater-perm its/nodes-industrial-swlitab-4 Permit No.: Facility N County: I Inspector: Date of Inspection: Time of Inspection: J or Total Event Precipitation (inches): 0.60 '6O Vn No.: All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the petmittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: A4� Aool� (Signature ofPermittee or Designee) 1. Outfal Description: Outfall No. Structure (pipe, ditch, etc.): P//��//��Md ye—, 14 Receiving Stream: the industrial activities that opcur within the outfall drainage area: n ce d- f immn 6,4inn Page 1 of 2 S WU-242, Last modified 07/28/2017 2. Color: Describe the color of (light, medium, dark) as descriptors: _ using basic colors (red, brown, blue, etc.) and tint V1 --Rr tWi 3. Odor: Describe any distinctodorsthat the di chlorine odor, etc.): A b 0 &Z may have (i.e., smells strongly of oil, weak 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is t surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 4 5 7. Is there any foam in the stormwater discharge? 4 Yes VINO. 8. Is there an oil sheen in the stormwater discharge? OYes INo. 9. Is there evidence of erosion or deposition at the outfall? O Yes No. 10. Other Obvious Indicators of Stormwater Pollution: 0 04" , d ►'('040 fi List and describe � Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. 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