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HomeMy WebLinkAboutNCG240019_Monitoring Report_20220314"R�R° RECEIVED ° Z MAR. 14 7.022 0°ITN °pR°y• DENR-DEldl.tt Land Qualify Section MECKLENBURG COUNTY Mooresville Regional Off¢, Land Use & Environmental Services Agency Solid Waste March 7, 2022 DEQ Mooresville Regional Office Attn: DEMLR Stormwater Program 610 East Center Avenue Suite 301 Mooresville, NC 28115 Attention: DEMLR Stormwater Program Subject: Discharge Monitoring Report Mecklenburg County Compost Central (new) — Certificate of Coverage No. NCG240019 Dear Central Files: Please find enclosed the Discharge Monitoring Report, February 2022, for Mecklenburg County Compost Central (new), a Type I facility located at 140 Valleydale Road, North Carolina. If you have any questions, please contact me at 704-634-7705 or by email at khaliem.adamsna,mecklenbur cg ountync. og_v. Sincerely, 2a� 4� Khaliem Adams Solid Waste Environmental Specialist Enclosed: 2022 DMR PEOPLE •PRIDE PROGRESS • PARTNERSHIP 2145 Suttle Avenue Charlotte, North Carolina 28208 www.wipeoutwaste.com NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG240000 Compost Operations Click here for instructions RECEIVED MAR i a 2022 Land Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) JI516 d"fo�liiVJKWn 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG24 0019 Person Collecting Samples: Khaliem Adams Facility Name: Mecklenburg County Compost Central (new) Laboratory Name: Pace Analytical Facility County: Mecklenburg Laboratory Cert. No.: Discharge during this period: ✓❑ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ✓❑ Yes ❑ No If so, which Tier (I, II, or III)? Tier 2 A copy of this DMRhaseen ploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR 0 Yes ❑ No Date Uploaded: a aaa Analytical Monitoring Requirements for Outfalls with Industrial Activities— Benchmarks in (Red) Parameter Parameter Outfall1 Outfall Outfall Outfall Outfall Code N/A Receiving Stream Class N/A Date Sample Collected MM/DD/YYYY 02/09/2022 46529 24-Hour Rainfall in inches 0.49 in C0530 TSS in mg/L(100) <8.3 00340 Chemical Oxygen Demand (120) 140 31615 Fecal Coliform in colonies per 100 ml 4800 (1000) 600 Total Nitrogen in mg/L (30) 3.1 665 Total Phosphorus in mg/L (2) 1.9 400 pH in standard units (6.0-9.0) 6.07 Copper, total recoverable in mg/L 01119 (0.010) 0.0076 Lead, total recoverable in mg/ L 01051 (0.075) <0.0050 Zinc, total recoverable in mg/ L 01094 (0.126) 0.011 Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average 00552 Non -Polar Oil & Grease in mg/L (15) <4.9 Estimated New Motor/Hydraulic Oil NCOIL Usage in al/month 75gal/month Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false' ormation, including the ossibility of fines and imprisonment for knowing violations." � Z- Permittee or Delegated Authorized Individual Date Email Address Phone Number Jalaw Hd egPOH ZZOZ/6/Z I LO-9-1 tiZZT I t Ilepnp I (Mau) lealua:) lsodwo:) /4uno:) ginqualpalN olduueS o; pain az!naa ales I Hd I aw!1 aldwes I uopezol aldwes I aweN A4!113ej ZeAnalyfical' w .pacelabsxom February 18, 2022 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 RECEIVED MAR 14 2 21 DENR-DLIMLFs Land Quality Section Mooresville Regional OLficr Enclosed are the analytical results for sample(s) received by the laboratory on February 09, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratodes within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Y Q Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 aUuAnalytical www.pacelabs.com Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersvil le, NC 28078 North Carolina Drinking Water Certification * 37706 North Carolina Field Services Certification M 5342 North Carolina Wastewater Certification M 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #. E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification * 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 aceAnalytical Www.pacelabs.ccm SAMPLE ANALYTE COUNT Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92587282001 OUTFALL 1 EPA 1664E ICO 1 PASI-C EPA 1664E ICO 1 PASI-C EPA 200.7 Rev 4.4 1994 CBV 3 PASI-A SM 9222D-2015 KDF 1 PASI-C SM 254OD-2015 MA62 1 PASI-A TKN+NO3+NO2 Calculation DMN 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 SMT 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A SM 5220D-2011 JP1 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 aceAnalytical www.patelabs.com ANALYTICAL RESULTS Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL 1 Parameters Lab ID: 92587282001 Collected: 02/09/22 12:38 Results Units Report Limit DF Received: 02/09/22 14:29 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 4.8 1 02/11/22 09:21 1664 SGT HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 4.8 1 02/11/22 09:21 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville Copper 0.0076 mg/L 0.0050 1 02/12/2218:39 02/17/2211:51 7440-50-8 Lead ND mg/L 0.0050 1 02112/2218:39 02/17/22 00:00 7439-92-1 Zinc 0.011 mg/L 0.010 1 02/1212218:39 02/17/22 00:00 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 4800 CFU/100 mL 1.0 1 02/09/22 15:37 02/10/22 14:35 2540D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services -Asheville Total Suspended Solids ND mg/L 8.3 1 02/11/22 12:36 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 3.1 mg/L 0.52 1 02/16/22 14:16 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 3.1 mg/L 0.50 1 02/15/22 20:39 02/16/22 04:54 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Rev 2.01993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 ND mg/L 0.040 1 02/14/22 12:40 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.01993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 1.9 mg/L 0.050 1 02/11/22 17:03 02/11/22 20:39 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 140 mg/L 25.0 1 02/15/22 01:43 02/15/22 05:13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2022 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 18 aceAr�alytical www.pacelabs.cem QUALITY CONTROL DATA Project: • COMPOST CENTRAL 2 Pace Project No.: 92587282 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 677482 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92587282001 METHOD BLANK: 3545863 Matrix: Water Associated Lab Samples: 92587282001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 02/11/22 09:21 LABORATORY CONTROL SAMPLE: 3545864 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 32.6 82 78-114 MATRIX SPIKE SAMPLE: 3545865 92587282001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 38.5 31.8 81 78-114 SAMPLE DUPLICATE: 3545866 92587289001 Dup Parameter Units Result Result RPD Qualifiers Oil and Grease mg/L ND ND Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2022 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 (�Ia '(c ice Analytical www.pacalabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 677480 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92587282001 METHOD BLANK: 3545841 Matrix: Water Associated Lab Samples: 92587282001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 02/11/22 09:21 LABORATORY CONTROL SAMPLE: 3545842 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 15.0 75 64-132 MATRIX SPIKE SAMPLE: 3545843 92587282001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 19.2 14.6 71 64-132 SAMPLE DUPLICATE: 3545844 92587289001 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L ND ND Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2022 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 acieAnalyical www.patelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 677948 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92587282001 METHOD BLANK: 3548204 Matrix: Water Associated Lab Samples: 92587282001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper mg/L ND 0.0050 02/17/2211:12 Lead mg/L ND 0.0050 02/16/22 23:08 Zinc mg/L ND 0.010 02/16/22 23:08 LABORATORY CONTROL SAMPLE: 3548205 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/L 0.5 0.51 102 85-115 Lead mg/L 0.5 0.48 97 85-115 Zinc mg/L 0.5 0.48 96 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3548206 3548207 MS MSD 92586608001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 82.1 0.5 0.5 0.55 0.54 93 93 70-130 0 ug/L Lead mg/L 61.2 0.5 0.5 0.51 0.51 89 89 70-130 0 ug/L Zinc mg/L 364 0.5 0.5 0.80 0.81 88 88 70-130 0 ug/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3548208 3548209 MS MSD 92587282001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 0.0076 0.5 0.5 0.48 0.48 95 95 70-130 0 Lead mg/L ND 0.5 0.5 0.45 0.45 89 90 70-130 1 Zinc mg/L 0.011 0.5 0.5 0.46 0.46 90 90 70-130 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2022 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 (�Ia'ucnte Analytical www.pacelabscom QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 QC Batch: 677189 Analysis Method: SM 9222D-2015 QC Batch Method: SM 922213-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92587282001 METHOD BLANK: 3544413 Matrix: Water Associated Lab Samples: 92587282001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 02/10/22 14:35 SAMPLE DUPLICATE: 3544414 92587289001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL 92.0 120 26 D6 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2022 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 aceAnalyfrcal www.pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 677547 Analysis Method: SM 254OD-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92587282001 METHOD BLANK: 3546228 Matrix: Water Associated Lab Samples: 92587282001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 02/11/22 12:31 LABORATORY CONTROL SAMPLE: 3546229 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 252 101 90-110 SAMPLE DUPLICATE: 3546680 92587325001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND 50.0 SAMPLE DUPLICATE: 3546681 92586939003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 232 248 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2022 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 (�Ia'uccee Analytical www.pacolabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 678401 Analysis Method: EPA 351.2 Rev 2.01993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92587282001 METHOD BLANK: 3550184 Matrix: Water Associated Lab Samples: 92587282001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 02/16/22 04:31 LABORATORY CONTROL SAMPLE: 3550185 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.3 93 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3550186 3550187 MS MSD 92586148001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.8 10 10 10.9 10.7 92 89 90-110 3 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3550190 3550191 MS MSD 92586615001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cane. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 131 10 10 127 129 -37 -19 90-110 1 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2022 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 (�Ia'unvAnalytical arww.pacela5s.cam QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 QC Batch: 677980 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.01993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92587282001 METHOD BLANK: 3548286 Matrix: Water Associated Lab Samples: 92587282001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.040 02/14/22 12:06 LABORATORY CONTROL SAMPLE: 3548287 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3548288 3548289 MS MSD 92584755014 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L ND 2.5 2.5 2.4 2.4 95 95 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3548290 3548291 MS MSD 92584755015 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.49 2.5 2.5 2.8 2.8 93 92 90-110 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2022 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 aceAnalytical www.paceiabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 677768 Analysis Method: EPA 365.1 Rev 2.01993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92587282001 METHOD BLANK: 3547424 Matrix: Water Associated Lab Samples: 92587282001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 02/11/22 20:26 LABORATORY CONTROL SAMPLE: 3547425 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3547426 3547427 MS MSD 92585633001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 9.7 2.5 2.5 12.3 11.8 102 84 90-110 4 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3547428 3547429 MS MSD 92585634001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 9.0 2.5 2.5 12.1 11.9 124 116 90-110 2 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2022 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 aceARaIj/NoI www pacelabacom QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 678255 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92587282001 METHOD BLANK: 3549648 Matrix: Water Associated Lab Samples: 92587282001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 02/15/22 05:08 LABORATORY CONTROL SAMPLE: 3549649 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 761 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3549650 3549651 MS MSD 92585910001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 67.4 100 100 172 172 105 105 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3549652 3549653 MS MSD 92585984003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 165 100 100 278 289 112 124 90-110 4 M1,R1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2022 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 aceAna lyticaI www.pacelabs.com QUALIFIERS Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2022 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 (�Ia'uce Analytical www pacelabscem QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: COMPOST CENTRAL 2 Pace Project No.: 92587282 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92587282001 OUTFALL 1 EPA 1664B 677482 92587282001 OUTFALL 1 EPA 1664E 677480 92587282001 OUTFALL 1 EPA 200.7 Rev 4.4 1994 677948 EPA 200.7 Rev 4.4 1994 677965 92587282001 OUTFALL 1 SM 922213-2015 677189 SM 9222D-2015 677190 92587282001 OUTFALL 1 SM 254OD-2015 677547 92587282001 OUTFALL 1 TKN+NO3+NO2 678778 Calculation 92687282001 OUTFALL 1 EPA 351.2 Rev 2.0 1993 678401 EPA 351.2 Rev 2.0 1993 678563 92687282001 OUTFALL 1 EPA 353.2 Rev 2.0 1993 677980 92587282001 OUTFALL 1 EPA 365.1 Rev 2.0 1993 677768 EPA 365.1 Rev 2.0 1993 677852 92587282001 OUTFALL 1 SM 5220D-2011 678255 SM 5220D-2011 678261 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2022 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 18 Document Name: Document Revlsed: November 15, 2021 on Recei t SLUR Sample Condition Up" Page 1 of 2 Document No.: Issuing Authority: aceAnalpical. F-CAR-CS-033-Rev.08 Pace Carolinas Quality 0f0ce Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville Q Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑ Client W0�# a 92:587282 MvName: ulw �l,�r, ( 0k iA I (l .2fix>I Courier: LJFedEx OUPS J CUSPS `� ❑Client ❑ Commercial []Pace ❑Other:_ II'll' II III III IIII III Custody Seal Present? // ❑Yes ❑(4o Seals Intact? ❑Yes / ❑NO 92587282 o Dale/Initlak Person Examining Contents. /✓��� —/ I cz Packing Material: �/ ❑Bubble Wrap ��]i Bubble Bags ❑None [I* Other Biological Tissue Frarlen7 Thermometerr/ ❑'1RGUn ID: (� n -`Z. �' Q1get []Blue [)Yes []No ❑N/A ❑None p(.( '_'R Type of Ica: LI � prrecUon Factor: Cooler Temp: Add/Subtract('C) Temp should be above freezing to 6'C []samples out of temp criteria. Samples on Ice, cooling process -Cooler-Temp 6orrected-(` Has USDA Regulated Soil (N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps(? Old samples originate from a In�eign source linternatlonally, mvna I —IN. IncludlneHawalland Puerto Firm?rlYes IFlNo Comments/Discrepancy: Chain of Custody Present? Yes OND ONIA 1. Samples Arrived within Hold Time? Yes ❑No ONIA 2. Short Hold Time Analysis e72 hr.)? OVes a NA 3. Rush Turn Around Time Requested; ❑Yes ®o N/A 4. Sufficient volume? iYEs ONO N/A S. Correct Containers Used? -Pace Containers Used? ' O Yes EKW ❑NO [IN. ❑N/A ❑N/A 6. Containers Intact? Yes []No N/A 7. Dissolved analysis: Samples Field Filtered? s ❑No /A B. Sample Labels Match COC? -Includes Date/rme/IO/Anal is Matrik: NOYes ONO ❑N/A 9. Heads ace in VOA Vials (>S•6mm)? Yes ❑No I/a 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes Yes ❑ o ONO ❑N/A N/A 11. COMMENTS/SAMPLE DISCREPANCY ' Lot ID of spit containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date: Date: Field Data Requlred? ❑Yes [:]No Page 16 of 18 Document Name. Condition Upon Receil Document No.: F-CAR-CS-033-Rev.08 *Check mark top half of box if pH and/or dechlorination Is Project # verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottles Document Revised: November 15, 2021 Page 2 of 2 Issuing Authority: Pace Carolinas Quali Office 9258 PM mwB Due Date: 02/16/22 CLIENT: 92—NECK CO a _ y �q, U Q Z ¢ ? a Q1 2 jai ar �j of 9( 4 v M1 aJ w d `d V !� rd ry n ZXas ai y Z y a: °� = Y id z 2 S a+ N ,,, 2 QJ $ c n c u a c L a Q C Z s ,�� si p Z '3 r c `- u `do a > Z = -' z V G � M a to 2 ^� w r x > 7s A a ai a N z a j •. c o a a c :. v a .. u is a a J a a. ° �EE m E Q 43 ¢ J %- E as M a it N x x O 7 t] O aZ a 1i CL a� a — u iv E E �Nn �i N E N N 1n N E _ N."� 6 t °: V & �•1 N ` ar r1 o, n� J E J E et J E J E O en 5 E u► E o } E U�� E $ J E 0 J E 0 :i m m m m m m m 3 w a a a i a s o>> o >> 9i in a n 1 XV Xf\ N —X 3 4 \��N \N\ I S 6 . 7 8 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative PH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added tot A Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certiflcatlon Office (i.e. Out of hold, incorrect preservattye, out of temp, Incorrect containers. Page 17 of 18 CHAIN -OF -CUSTODY I Analytical Request Document 1.0,2ceftlytal' The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. I WwActusicam Submittinn a samnle via this chain of custociv constitutes acknovAedoment and acceotance of the Pace Terms and Conditions found at httos:flinfo.oacelabs.com/hubfs/pas-standard-terms.pdf Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page: 1 Of Company: Mecklenburg County Solid Waste Report TO: Khallem Adams Attention: Address: 2145 Suttle Ave. Copy To: Company Name: Charlotte, NC 28268 Address: Rout FV' gerw--l—, Email: khatiem.adams@mar.kienburgmuntync.gov Purchase Order 0 Pace Quote: Phone: (980)314-3858 lFax- Project.Name: Compost Central 2 Pace Project Manager matthew.brainard@pwelabs.com, l Due Date: --Requested 112rojecl#: Pace Prorlie it 32o7.1 I NC i iR FRq It~ '(Y :E MATRIX CODE I 0 COLLECTED z Preservatives 00mag walef ow .8 V0 Wd9f wr Wmto walar ww 7,x ;I C Product P SAMPLE ID 5"sohd START END 0 od One Character per box. Wipe WP (A-Z, 0-9 1, Air AR w CL ul Z C tu 2 0 = M S 9 0uw OT 0 2 Sample Ids must be unique Tissw 'M X 0 0 C N 0 Z Ox -0 CL a CS 17i DATE TIME DATE TIME . 7- 0 U 0 azy b -C 7d— aIMP 1', 28 16H )q-7(�, �4' Molds: Cu, Pb. Zn -7 SAMPLWINAii -AN PRINT Name of SAMPLER: CD -L OD 0 2 Lu N 06 E M S, �,; SIGNATURE of SAMPLER: DATE Signed: 7� 0: Cj U) C � i 00 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfrlling out thisform, please visit bMs://deg.nc.izov/abouttdivisions/enerev-mineral-land- resou rces/enerev-mineral-land-perm its/stormwater-perm its/npdes-industrial-s w#tab-4 Permit No.: N/CIC,41��/ 0/ 0/ 0/ or Certificate of Cove age No.: N/C/G/J9. Facility Name: i County: Phone N . C " Inspector: Date of Inspection: oc Time of Inspection: Total Event Precipitation (inches): 0 ' 1>9 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: pjp,w t ve _,�., Outfall No. I Structure (pipe, ditch, etc.): vV `� 6 Receiving Stream: Describe the industrial activities thin occur within the outfall drainage area: V?41 fcte, IMA1,4 Pagel of 2 SWU-242, last modified 0728/2017 2. Color: Describe the color oft a disc arge using basic colors red, br wn, blue, etc.) tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct o ors that thy di charge may hav (i.e., ells strongly of oil, weak chlorine odor, etc.): 7L 1 1 — i 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? es o No. Vey 4V-e' Y 8. Is there an oil sheen in the stormwater discharge? 0Yes o.&7 V V 9. Is there evidence of erosion or deposition at the outfall? o Yes No. D 10. Other Obvious Indicators of Stormwater Pollution: List and describe NO 0�'ri,rr.� - t} dw4h-fs Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017