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Home My WebLink AboutNCG240019_Monitoring Report_20210813a MECKLENBURG COUNTY Land Use & Environmental Services Agency Solid Waste I% August 10, 2021 46. 9 �/l Central Files yo�a�aFy �Ca2 �Q NCDENR / DWQ 1617 Mail Service Center R"9oSPc� Raleigh, North Carolina 27699-1617 CF Attention: Central Files Subject: Discharge Monitoring Report Mecklenburg County Compost Central (new) — Certificate of Coverage No. NCG240019 Dear Central Files: Please find enclosed the Discharge Monitoring Report, July 2021, for Mecklenburg County Compost Central (new), a Type I facility located at 140 Valleydale Road, North Carolina. If you have any questions, please contact me at 704-634-7705 or by email at khaliem.adams@mecklenbur cg ountync.gov. Sincerely, Khaliem Adams Solid Waste Environmental Specialist Enclosed: 2021 DMR PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2145 Soule Avenue Charlotte, North Carolina 28208 www.wipeoutwastexom . NCDEQ Division of Energy, Mineral and Land Resources Stor(ttwjs�charge Monitoring Report (DMR) Form for NCG240000 Compost Operations Click here for instructions Complete, sign, scan 5143' e DMR via the Stormwater NPDES Permit Data Monitoring Report (DMRI Upload form within e 30 days of receiving samplirs. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG24 0019 Person Collecting Samples: Khaliem Adams Facility Name: Mecklenburg County Compost Central (new) Laboratory Name: Pace Analytical Facility County: Mecklenburg Laboratory Cert No.: Discharge during this period: ✓❑ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑✓ Yes []No If so, which Tier (I, II, or III)? Tier 1 A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR ❑✓ Yes ❑ No Date Uploaded: 10aQaI Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Parameter Outfall1 Outfall Outfall Outfall Outfall Code N/A Receiving Stream Class N/A Date Sample Collected MM/DD/YYYY 07/13/2021 46529 24-Hour Rainfall in inches 0.36 C0530 TSS in mg/L (100) 8.4 00340 Chemical Oxygen Demand (120) 112 31615 Fecal Coliform in colonies per 100 ml 2400 (1000) 600 Total Nitrogen in mg/L (30) 2.8 665 Total Phosphorus in mg/L (2) 1.8 400 pH in standard units (6.0-9.0) 8.31 Copper, total recoverable in mg/L 01119 (0.010) < 0.0050 Lead, total recoverable in mg/ L 01051 (0.075) <0.0050 Zinc, total recoverable in mg/ L 01094 (0.126) <0.010 Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average 00552 Non -Polar Oil & Grease in mg/L (15) <5.1 Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month 75 gal/month Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible forgathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Pefmittee or Delegated Authorized Individual Email Address TT J�eren.SFe rtieC/Cnc, 5o v 1,9 Date Phone Number 7k6-- ?1Y-7e-f-7 aalaw Hd egPoH TZOZ/£T/L T£'8 ZtiTT T Ilepno (mau) lealua:) isodwo:) Aluno:) SanqualpaVy aldwes o;past aalnaQ a;eQ Hd owll aldwes uolleaol aldwes aweN l4i1i3ej aceAnalytical M`II/.QaCellEfeM July 21, 2021 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: COMPOSTCENTRAL2 Pace Project No.: 92549077 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on July 13, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 1 of 18 Pace Analytical Services, LLC Analytical® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 WmPacetabLcom (704)875-9092 CERTIFICATIONS Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I_LC. Page 2 of 18 aceAnalytical awatip80181)UM SAMPLE ANALYTE COUNT Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92649077001 OUTFALL 1 EPA 16648 CJM 1 PASI-C EPA 1664E CJM 1 PASI-C EPA 200.7 Rev 4.41994 CBV 3 PASI-A SM 9222D-2006 KDF 1 PASI-C SM 254OD-2011 MJP 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.01993 MFO 1 PASI-A EPA 353.2 Rev 2.01993 HMH 1 PASI-A EPA 365.1 Rev 2.01993 KDF1 1 PASI-A SM 5220D-2011 MDW 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 aceAnalytical waive pacelabs.ccm ANALYTICAL RESULTS Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 Pace Analytical Services, LLC 9800 Kinney Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL 1 Lab ID: 92649077001 Collected: 07/13/21 11:58 Received: 07/13/21 12:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. HEM, Oil and Grease Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.1 1 07/18/21 10:38 1664 SGT HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.1 1 07/18/21 10:38 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville Copper ND mg/L 0.0050 1 07/16/21 12:20 07/20/2105:25 7440-50-8 Lead ND mg/L 0.0050 1 07/16/21 12:20 07/20/2105:25 7439-92-1 Zinc ND mg/L 0.010 1 07/16/21 12:20 07/20/2105:25 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Charlotte Fecal Coliforms 2400 CFU/100 mL 1.0 1 07/13/21 16:02 07/14/21 14:17 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 8.4 mg/L 3.3 1 07/17/21 12:41 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 2.8 mg/L 0.52 1 07/20/21 14:19 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 2.8 mg/L 0.50 1 07/16/21 23:11 07/17/21 07:22 7727-37-9 353.2 Nitrogen, NO2/NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 0.041 mg/L 0.040 1 07/16/21 09:22 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus 1.8 mg/L 0.050 1 07/15/21 13:40 07/16/2110:31 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 112 mg/L 25.0 1 07/19/21 19:13 07/19/21 23:06 Date: 07/21 /2021 08:18 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Qua[ Page 4 of 18 (�Ia'cce Analytical wwtapaselaba cam QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 634068 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92549077001 METHOD BLANK: 3330404 Matrix: Water Associated Lab Samples: 92549077001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 07/18/21 10:38 LABORATORY CONTROL SAMPLE: 3330405 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 36.8 92 78-114 MATRIX SPIKE SAMPLE: 3330406 92548613001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 36.8 90 78-114 SAMPLE DUPLICATE: 3330407 92548176001 Dup Parameter Units Result Result RPD Qualifiers Oil and Grease mg/L 25.0 23.0 8 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the resulL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21/2021 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 aceAnalytical >Irtrgfpacelat>scola QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 } Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 634070 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 SGT HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92549077001 METHOD BLANK: 3330408 Matrix: Water Associated Lab Samples: 92549077001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 07/18/21 10:38 LABORATORY CONTROL SAMPLE: 3330409 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 20.4 102 64-132 MATRIX SPIKE SAMPLE: 3330410 92548613001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 19.1 92 64-132 SAMPLE DUPLICATE: 3330411 92548176001 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L 9.6 10.8 11 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21/2021 08:18 AM without the written consent of Pace Analytical Services, LI_C. Page 6 of 18 acleAnalytical vrgaw paaeleba corn QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 633855 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92549077001 METHOD BLANK: 3329142 Matrix: Water Associated Lab Samples: 92549077001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper mg/L ND 0.0050 07/20/2103:40 Lead mg/L ND 0.0050 07/2012103:40 Zinc mg/L ND 0.010 07/20/2103:40 LABORATORY CONTROL SAMPLE: 3329143 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper mg/L 0.5 0.54 108 85-115 Lead mg/L 0.5 0.49 99 85-115 Zinc mg/L 0.5 0.48 96 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3329144 3329145 MS MSD 92548804007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Copper mg/L ND 0.5 0.5 0.49 0.52 97 103 70-130 7 Lead mg/L ND 0.5 0.5 0.45 0.48 89 96 70-130 7 Zinc mg/L 114 0.5 0.5 0.55 0.59 88 96 70-130 7 ug/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3329146 3329147 MS MSD 92548841001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qua[ Copper mg1L 35.9 0.5 0.5 0.53 0.53 98 99 70-130 1 ug/L Lead mg/L ND 0.5 0.5 0.45 0.45 89 90 70-130 1 Zinc mg/L 44.9 0.5 0.5 0.48 0.49 87 88 70-130 1 ug/L Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21/2021 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 aceAnalytical wwwpacelftcom QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 QC Batch: 633132 Analysis Method: SM 9222D-2006 QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92549077001 METHOD BLANK: 3325770 Associated Lab Samples: 92549077001 Parameter Units Fecal Coliforms CFU/100 mL SAMPLE DUPLICATE: 3325771 Parameter Fecal Coliforms Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 07114/2114:17 92549102003 Dup Units Result Result RPD Qualifiers CFU/100 mL 9.0 ND Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21/2021 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 aceArralytical www.pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 634115 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92549077001 METHOD BLANK: 3330514 Matrix: Water Associated Lab Samples: 92549077001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 07/17/21 12:38 LABORATORY CONTROL SAMPLE: 3330515 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 252 101 90-110 SAMPLE DUPLICATE: 3330516 92549427001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 264 242 9 SAMPLE DUPLICATE: 3330517 92549302001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 3.1 3.3 6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/21/2021 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 (�Ia'ucenAnalyfical www pacelabsmm QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 1 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 633979 Analysis Method: EPA 351.2 Rev 2.01993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92549077001 METHOD BLANK: 3329789 Matrix: Water Associated Lab Samples: 92549077001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 07/17/21 06:55 LABORATORY CONTROL SAMPLE: 3329790 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10.1 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3329793 3329794 MS MSD 92548282001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 17.6 10 10 32.9 30.9 153 133 90-110 6 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3330424 3330425 MS MSD 92548282002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 2.4 10 10 14.7 14.0 123 116 90-110 5 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2021 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 aceAnalyircal V1t>fir ItSU01flt1S.CarA QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 633587 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92549077001 METHOD BLANK: 3327772 Matrix: Water Associated Lab Samples: 92549077001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.040 07/16/21 09:06 LABORATORY CONTROL SAMPLE: 3327773 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3327774 3327775 MS MSD 92549004001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.049 2.5 2.5 2.4 2.4 95 95 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3327776 3327777 MS MSD 92549006001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.056 2.5 2.5 2.3 2.3 89 88 90-110 1 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21/2021 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 aceAnalylcal www pacelsba eam QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 I Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 633529 Analysis Method: EPA 365.1 Rev 2.01993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92549077001 METHOD BLANK: 3327589 Matrix: Water Associated Lab Samples: 92549077001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 07/1612110:19 LABORATORY CONTROL SAMPLE: 3327590 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3327591 3327592 MS MSD 92548626002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 6.6 2.5 2.5 9.2 9.1 104 102 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3327593 3327594 MS MSD 92548644001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.13 2.5 2.5 2.6 2.7 99 101 90-110 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21/2021 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 aceAnalyt�cal vrq� paCafabscom QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 634343 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92549077001 METHOD BLANK: 3331541 Matrix: Water Associated Lab Samples: 92549077001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 07/19/21 23:01 LABORATORY CONTROL SAMPLE: 3331542 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 762 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE. 3331545 3331546 MS MSD 92548394001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 392 100 100 482 482 91 91 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3331547 3331548 MS MSD 92548558001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 1020 100 100 1060 1070 42 47 90-110 0 M1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21/2021 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 aceAnalyfcal www P=l2b3=M QUALIFIERS Project: COMPOST CENTRAL 2 Pace Project No.: 92549077 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21/2021 08:18 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 IaceAnalytical (�ww.pacelaba.cmo QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite too Huntersville. NC 28078 (704)875-9092 Project: Pace Project No.: COMPOST CENTRAL 2 92549077 Analytical Lab ID Sample ID OC Batch Method QC Batch Analytical Method Batch 92549077001 OUTFALL1 EPA1664B 634068 92549077001 OUTFALLI EPA1664B 634070 92549077001 OUTFALL 1 EPA 200.7 Rev 4.4 1994 633855 EPA 200.7 Rev 4.4 1994 634005 92549077001 OUTFALL 1 SM 922213-2006 633132 SM 9222D-2006 633133 92549077001 OUTFALL 1 SM 254OD-2011 634115 92549077001 OUTFALL 1 TKN+NO3+NO2 634601 Calculation 92549077001 OUTFALL 1 EPA 351.2 Rev 2.0 1993 633979 EPA 351.2 Rev 2.0 1993 634094 92549077001 OUTFALL 1 EPA 353.2 Rev 2.0 1993 633587 92549077001 OUTFALL 1 EPA 365.1 Rev 2.0 1993 633529 EPA 365.1 Rev 2.0 1993 633683 92549077001 OUTFALL 1 SM 5220D-2011 634343 SM 5220D-2011 634417 Date: 07/21/2021 08:18 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 15 of 18 Document Name: page 101 c ndition U on Receli,lti,SCUR) Issuing Authorlty: nnrument No.: Pace Caroiinas Quality les: Raleigh❑ Mechanicsville Atlanta❑ I<ernersville❑ Labor receiving samp Huntersville ® - Asheville ❑ EdenO Greenwood ❑ WO# : 92549077 Client Name:�vIYlF'�p'�sei c tt. II � III III IIIIIII III III m 92549077 �,.,,rier• �_._ ❑Other: Uro�.w ❑ Commercial ❑o N �ND Seals Intact? DesDateltnitialsPerson.EnamininFGonten _..—� CustodY Seat present? ❑Yes ❑ ❑YesogONoss'@N/Aen? Bubble Wrap ❑gobble Bags None Other packing Material: ®Wet QBlue ❑None Thermometer: 92,11 Type of tee: IPGuniD: 7empshouidbeabovefreezingto6'C cooling Process Correction Factor: []Samplesout of temp uiteria. Sampies an ice, Add/Subtract VC1 0�-1--= hashegun Cooler Temp: Cooler Temp Corrected ('Cl: Did samplesoAglnatefrom aforeign source l�^t_O!R ally, USDA Regulated Soil ) (@ NIA, water sample) NY, or Sc (check Maps)?Including Hawaii and Puerto local? ❑Yes Comments/Discrepancy: Did samples originate in a quarantine tone within the United States: , ON/A 16. Correct Containers Used? QNa ON/A 19. Samole Label, Match COV COMMENTS/SAMPLE DISCREPANCY —�� Date/Time: —� Person contacted. Date: Project Manager SCURF Review: Date: praiect Manager SRF Review: Field Data Regv'red? Oyes []No Page 16 of 18 S 6 i0 L l 96ed .a•!) anwo p 101 o ino'aMen�asaid uaa jou!'p1°'! }o l(t0 •siau!ewo3 Va,jo3u! ulpa } ueda,�s!p a st asayl ianaua4M :aioN oie� 4 ,ON ayi o»uas aq !4 ^ wlo; s!MT 10 Ildo3 e'sat doves azue!tidwoj eu!tioje) yUoN Su!i�a;e A� tiN 43c, eu!! PatsnlPe Passnjp8 uopeMasaid area AM, uodn H papPe u0pemaswd able. a A01901 IUD" lsnlp� Hd an!leNasald 10 3unoWt! salduUeS panAasa d Zt tt D o O 0 0 1 7 X. 19 a g c w if to �+ b, n D t G1 b p � ; o a• d r r < < N D y3 Q 3 N G c < O 0 U` 3 's -yo O e•+ Z Q � A Sb f^ 'O W r W .yi IV ^_ D cl a r i 9 Z 9 .Di r v�y ,;;a � v i ,�- 8utnss1 � G t D cxa A 3 0 i V GI0 w D 0 r u �? m o S o N a w •+ 0 �- -► Q alms-%S110%Sl-xoqf1�l i su0�lda�x� . _.._.-----salgoq'i° iaq ue t!o'�ol'Wj0}tl°� don doves -;., ......... _ _.. .. - � �alenn) St0810�U asealD P Sal sH�1 Boa l ue pal)laan �. doh �aeLU'43ay3* �o a�uea a�ue�da��e aya uly�lM l lt uol1e+uasaad ue Hd �l xOq }° �le4 St uolleup0143aP ao/P vajoad j coa-Eso-sye�- . - •� ti aN �uawn3oa S ,► �= o auo� a we1 -.. %sla,lln'300 Request Document ratew. Analytical nubtsipas-standl Et4T. All releviint gelds must be completed accu CHAIN-Or--CUS-TOIDAL DOCUM t,,,p,.jrnto.pace1,b,.,Omr The Chaln_of.Custody Is a LECand C,,ndlgon- tund CIP once of the Pace Terms gment and 80000 Section c •consl 1c"O*l a tKIS chain -1 custody invoice 9 a sample '41 section 8 Ion. wwwulsa" SubMI ired project lao"111110 ROW COMPOM To: Adana �! 11111111 � . 1(hallem; �l R Address! . ......... client Infolvation- sol copy To: ....... paw aucle. Jobs.cm. y. Mach, P p IMaanager Avo........... ... aw urche Older paw Prof, W. 3 214S SO" P NC 282 Project lemads Fox P itc P erve'dVes st Coo Date: a 0 Zi CO 2 VATRIX CODE o"Onw," Ow C, END CL ,a P START PmdUd OR z SL 0 wilsow OL WP ol !z- 0 SAMPLE'D ve" AR 0) One Character Parbox. Aw OT U) cow is 5 sample Ids must be UniqueTnsvo OAT@ T11JSE DATE TIMEe It F tu I=- . ......................... —1 Name, of So R F. U) co 0 CO K( C. Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfilling out this form, please visit httt)s:Hdeg.ne.gov/about/divisions/enerev-mineral-land- resources/enerev-m i neral-landroermits/stormwater-permits/nodes-i nd ustrial-sw#tab-4 Permit No.: N/C/S/ 1?/j/d/j/ Ulvl or ertificate of overage N/o.:N/C/G/ 0?/ Facility Name: Me4pem ht4,mi /�ST I , /n0 l 111 e I,/ ) County: ?iAU Phone No. 70y— 770 .5� Inspector: %/ Date of Inspection: 3//LL d' Dot Time of Inspection: 1 / T011 Total Event Precipitation (inches): • 36 /0 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local stone events during the sampling period, and the permittee obtains approval from the local DEMLR Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: D �p /1 / I /� r ) Outfall No. Structure (pipe, ditch, etc.): / � /'L (� V `-14 Receiving Stream: the industrial activities that oc,within the outfall drainage area:VWC16 Page I of 2 SWU-242, Last modified 07/28/2017 2. Color: Describe the color oft a discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 1 -8 f Q r0 W n 3. Odor: Descri y distinct odors that the discharge may hav (i.e., smells strongly of oil, weak chlorine odor, etc.): { D 4. Clarity: Choose the number which best describes the clarity of the discharge, where l is clear and 5 is very cloudy: --- 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 (v 3 J 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? O Yes 0 No. No S. Is there an oil sheen in the stormwater discharge? oYes 4 - NO 9. Is there evidence of erosion or deposition at the outfall? O Yes No. 10. Other Obvious Indicators of Stormwater Pollution: L Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SwU-242, Last modified 07/28/2017