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Home My WebLink AboutNCG240019_Monitoring Report Jan_20220131ea OUR. oqT„ cnao"® MECKLENBURG COUNTY Land Use & Environmental Services Agency Solid Waste January 25, 2022 DEQ Mooresville Regional Office Attn: DEMLR Stormwater Program 610 East Center Avenue Suite 301 Mooresville, NC 28115 Attention: - 1-Files pEML'4� 9pr-Mwq�ex Prh-r6'rvs RECEIVED JAN 31. 2022 DENR-DEMLR Land Quality Section Mooresville Regional Office Subject: Discharge Monitoring Report Mecklenburg County Compost Central (new) — Certificate of Coverage No. NCG240019 Dear Central Files: Please find enclosed the Discharge Monitoring Report, January 2022, for Mecklenburg County Compost Central (new), a Type I facility located at 140 Valleydale Road, North Carolina. If you have any questions, please contact me at 704-634-7705 or by email at khaliem.adamsnmecklenbur cg ountync. og_v. Sincerely, Khaliem Adams Solid Waste Environmental Specialist Enclosed: 2022 DMR PEOPLE •PRIDE PROGRESS • PARTNERSHIP 2145 Suttle Avenue Charlotte, North Carolina 28208 www.wipeoutwaste.com NCDEQ Division of Energy, Mineral and Land Resources RECEIVED Stormwater Discharge Monitoring Report (DMR) Form for NCG240000 Compost Operations Click here for instructions BAN 312022 0t:NR-DEMLR Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Re orti " &ithin 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG24 0019 Person Collecting Samples: Khaliem Adams Facility Name: Mecklenburg County Compost Central (new) Laboratory Name: Pace Analytical Facility County: Mecklenburg Laboratory Cent. No.: Discharge during this period: ✓❑ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ✓❑ Yes ❑ No If so, which Tier (l, ll, or III)? Tier 2 A copy of this DMR hasbeen uploaded electronically via https://edocs.deg.nc.gov/Forms/Sw-DMR ❑✓ Yes ❑ No Date Uploaded: U a6 aDaa Analytical Monitoring Requirements for Outfalls with Industrial Activities— Benchmarks in (Red) Parameter Parameter Outfall1 Outfall Outfall Outfall Outfall Code N/A Receiving Stream Class N/A Date Sample Collected MM/DD/YYYY 01/06/2022 46529 24-Hour Rainfall in inches 2.10 in C0530 TSSin mg/L(100) 10.5 00340 Chemical Oxygen Demand (120) 154 31615 Fecal Coliform in colonies per 100 ml 6000 (1000) 600 Total Nitrogen in mg/L (30) 3.5 665 Total Phosphorus in mg/L (2) 2.0 400 pH in standard units (6.0-9.0) 8.59 Copper, total recoverable in mg/L 01119 (0.010) 0.011 01051 Lead, total recoverable in mg/ L <0.0050 (0.075) Zinc, total recoverable in mg/ L 01094 (0.126) 0.016 Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average 00552 Non -Polar Oil & Grease in mg/L (15) <4.9 Estimated New Motor/Hydraulic Oil NCOIL Usage in al/month 75ga1/month Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false �i*rmation, including the possibility of fines and imprisonment for knowing violations." Permittee or Delegated Authorized Individual r Zrl2z Date Email Address Phone Number aaIaW Hd eglaoH ZZOZ/9/Z 65'8 OZZT t Ilellnp (mau) lealua:) isodwo:) Ajuno:) SanqualpaW aldweS o} pasty a�inap area Hd awLL aldweS ummo-i aldweS aweN Atli �ej (�15'ceAnaljtical* 1rwr.0aoalabscota January 13, 2022 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: COMPOSTCENTRAL2 Pace Project No.: 92581378 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on January 06, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, u, &,--D Matthew Brainard mafthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste CQ Pc�FG gBCR� i REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, U.C. Page 1 of 18 IaceAnalytical W pacalaba.com Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Flodda/NELAP Certification #: E87648 North Carolina Drinking Water Certification M 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 VirginiaNELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 VrginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 aceAnalyiical wwpaselabsi m SAMPLE ANALYTE COUNT Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92581378001 OUTFALL 1 EPA 1664E ICO 1 PASI-C EPA 1664E ICO 1 PASI-C EPA 200.7 Rev 4.4 1994 RDT 3 PASI-A SM 922213-2015 KDF 1 PASI-C SM 254OD-2015 ZMC 1 PASI-A TKN+NO3+NO2 Calculation DMN 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A SM 5220D-2011 JP1 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 aceAnalytical www paaetabu m ANALYTICAL RESULTS Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL 1 Lab ID: 92581378001 Collected: 01/06/22 12:20 Received: 01/06/22 14:39 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 4.9 1 01/10/22 09:23 1664 SGT HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 4.9 1 01/10/22 09:23 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville Copper 0.011 mg/L 0.0050 1 01/08/22 02:54 01/12/22 00:32 7440-50-8 Lead ND mg/L 0.0050 1 01/08/22 02:54 01/12/22 00:32 7439-92-1 Zinc 0.016 mg/L 0.010 1 01/08/22 02:54 01/12/22 00:32 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 6000 CFU/100 mL 1.0 1 01/06/22 15:49 01/07/22 14:08 u2 2640D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services - Asheville Total Suspended Solids 10.5 mg/L 4.2 1 01/07/22 22:19 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Asheville Total Nitrogen 3.5 mg/L 0.52 1 01/13/22 11:54 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.01993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 3.5 mg/L 0.50 1 01/12/2218:59 01/13/22 03:38 7727-37-9 363.2 Nitrogen, NO2/NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 ND mg/L 0.040 1 01/10/22 11:29 366.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 2.0 mg/L 0.050 1 01/10/22 22:53 01/11/22 22:07 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services - Asheville Chemical Oxygen Demand 154 mg/L 25.0 1 01/12/22 01:29 01/12/22 04:31 Date: 01/13/2022 11:59 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 18 aceAnalytical WWW.Pacelab&OM QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 670551 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92581378001 METHOD BLANK: 3511237 Matrix: Water Associated Lab Samples: 92581378001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 01/10/22 09:23 LABORATORY CONTROL SAMPLE: 3511238 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 33.5 84 78-114 MATRIX SPIKE SAMPLE: 3511239 92581378001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 38.5 34.3 88 78-114 SAMPLE DUPLICATE: 3511240 92581438001 Dup Parameter Units Result Result RPD Qualifiers Oil and Grease mg/L ND ND Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/13/2022 11:59 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 laCol.leAnalyfical MfYlrwpacdaba.ew QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 670547 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92581378001 METHOD BLANK: 3511160 Matrix: Water Associated Lab Samples: 92581378001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 01/10/22 09:23 LABORATORY CONTROL SAMPLE: 3511161 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 14.9 74 64-132 MATRIX SPIKE SAMPLE: 3511162 92581378001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 19.2 13.4 67 64-132 SAMPLE DUPLICATE: 3511163 92581438001 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L ND ND Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/13/2022 11:59 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 Atccice;Analyfical www pacWabs.eom QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 670557 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.41994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92581378001 METHOD BLANK: 3511510 Matrix: Water Associated Lab Samples: 92581378001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper mg/L ND 0.0050 01/11/22 22:54 Lead mg/L ND 0.0050 01/11/22 22:54 Zinc mg/L ND 0.010 01/11/22 22:54 LABORATORY CONTROL SAMPLE: 3511511 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/L 0.5 0.50 101 85-115 Lead mg/L 0.5 0.49 97 85-115 Zinc mg/L 0.5 0.47 95 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3511512 3511513 MS MSD 92579537001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 0.0060 0.5 0.5 0.52 0.52 102 103 70-130 1 Lead mg/L ND 0.5 0.5 0.49 0.50 99 100 70-130 1 Zinc mg/L 0.015 0.5 0.5 0.51 0.51 98 99 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3511514 3511515 MS MSD 92581190002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 9240 0.5 0.5 9.6 9.4 62 34 70-130 1 ug/L Lead mg/L ND 0.5 0.5 0.47 0.46 92 91 70-130 2 Zinc mg/L 236 0.5 0.5 0.72 0.71 97 96 70-130 1 ug/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/13/2022 11:59 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 (�IaceAnaiyticale www.pacelabs.cam QUALITY CONTROL DATA Project: COMPOST CENTRAL Pace Project No.: 92581378 QC Balch: 670491 Analysis Method: SM 9222D-2015 QC Batch Method: SM 922213-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHIT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92581378001 METHOD BLANK: 3510828 Associated Lab Samples: 92581378001 Parameter Fecal Coliforms SAMPLE DUPLICATE: 3510829 Parameter Fecal Coliforms Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers CFU/100 mL ND 1.0 01/0712214,08 92581392003 Dup Units Result Result RPD Qualifiers CFU/100 mL NO ND Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indlwte l by the "Units' column except where an alternate unit is presented to Me right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/131202211:59 AM without the written consent of Pace Analytical Services,LLC. Page 8 of 18 aceAnalytical arMpaCOJO corn QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 QC Batch: 670566 Analysis Method: SM 254OD-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92581378001 METHOD BLANK: 3511624 Matrix: Water Associated Lab Samples: 92581378001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 01/07/22 22:08 LABORATORY CONTROL SAMPLE: 3511625 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 230 92 90-110 SAMPLE DUPLICATE: 3511626 92581524001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 234 252 7 SAMPLE DUPLICATE: 3511627 92581392001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 60.0 57.0 5 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/13/2022 11:59 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 aceArralytrcal www pacefabaccm QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 671337 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92581378001 METHOD BLANK: 3514832 Matrix: Water Associated Lab Samples: 92581378001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 01/13/22 03:30 LABORATORY CONTROL SAMPLE: 3514833 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg1L 10 10 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3514834 3514835 MS MSD 92581394001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.6 10 10 12.4 12.4 108 108 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3514836 3514837 MS MSD 92581394002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.1 10 10 12.1 11.6 111 105 90-110 5 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01113/202211:59 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 (�5a'CeAnalytical wane pstwtabLcom QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 670681 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92581378001 METHOD BLANK: 3511888 Matrix: Water Associated Lab Samples: 92581378001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.040 01/10/22 10:55 LABORATORY CONTROL SAMPLE: 3511889 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3511890 3511891 MS MSD 92580204001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.087 2.5 2.5 2.2 2.2 84 84 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3511892 3511893 MS MSD 92580204002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 1.6 2.5 2.5 4.1 4.1 98 98 90-110 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/13/2022 11:59 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 aceAnalyrcal WM.Pacelftcom QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 670940 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92581378001 METHOD BLANK: 3513053 Matrix: Water Associated Lab Samples: 92581378001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 01/11/22 21:53 LABORATORY CONTROL SAMPLE: 3513054 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3513055 3513056 MS MSD 92580426001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 2.1 2.5 2.5 4.7 4.7 101 101 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3513057 3513058 MS MSD 92580501001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 78.2 2.5 2.5 82.3 82.3 162 162 90-110 0 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 01/13/2022 11:59 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 (�Ia'neAnalytical arWW pat elebuom QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 671182 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92581378001 METHOD BLANK: 3514256 Matrix: Water Associated Lab Samples: 92581378001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 01/12/22 04:26 LABORATORY CONTROL SAMPLE: 3514257 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 766 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3514258 3514259 MS MSD 92580426001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 100 100 122 119 114 111 90-110 2 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3514260 3514261 MS MSD 92580503001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 2300 100 100 2490 2430 185 130 90-110 2 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/13/2022 11:59 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 (�IaceAnalytical www pacalabscom QUALIFIERS Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 0 1 /13/2022 11:59 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 '9 aceAnalytfcal wwiLpaeelabuom QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: COMPOST CENTRAL 2 Pace Project No.: 92581378 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Late ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92581378001 OUTFALL 1 EPA 1664E 670551 92581378001 OUTFALL 1 EPA 1664E 670547 92581378001 OUTFALL 1 EPA 200.7 Rev 4.41994 670557 EPA 200.7 Rev 4.4 1994 670585 92581378001 OUTFALL 1 SM 9222D-2015 670491 SM 9222D-2015 670494 92581378001 OUTFALL 1 SM 2540D-2015 670566 92581378001 OUTFALL 1 TKN+NO3+NO2 671532 Calculation 92581378001 OUTFALL 1 EPA 351.2 Rev 2.0 1993 671337 EPA 351.2 Rev 2.0 1993 671430 92581378001 OUTFALL 1 EPA 353.2 Rev 2.0 1993 670681 92581378001 OUTFALL 1 EPA 365.1 Rev 2.0 1993 670940 EPA 365.1 Rev 2.0 1993 671106 92681378001 OUTFALL 1 SM 5220D-2011 671182 SM 5220D-2011 671193 Date: 01 /13/2022 11:59 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 18 Document Name: Sample Condition Upon Recel t SCUR Document Revised: November Page 1 of 2 ElS2011]ace/lnalytical Issuing Authority: Pace Carolinas Quality Off Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersvilleg Raleigh[] Mechanicsville[] Atlanta[] Kernersville❑ Client Name: Project R: W0 92581378 roj N t ckLw by ui (-n C4(4 Seq L� 64 Courier: ❑!t ❑UPS ❑LISPS CTlent ❑ �pace IIIII"III I'I II I'II'll Commercial PaceYjl� I/G17.1 ❑Other._ / Custody Seal Present? ❑Yes E�Na Seats Intact? []YesqPio 1926a1378 Date/Initlak Person Examining Contents: Y� Packing Material: []Bubble Wrap ❑Bubble Bags loNone ❑' Other Biological Tissue Frozen? Thermometer o f / I []Yes []No JZN/A Type of ice: VIR Gun to: ``�O�VI Swat ❑Blue []Nam Correction Factor; Cooemp: A Su tract/('C)U Temp should be above freezing to6'C --Eoaler-Temp{onected-('C(. —r "t ❑samples ousof temp cshena. Samples on ice, cooling process Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Old samples originate from a forelgn'source (internationally, r Yes nNa -- .y.• mwar ores Una Comments/Dlstre an : Chain of Custody Present? Yes ON. N A 1. Samples Arrived within Hold Time? Myes ONO ❑N/A 2. Short Hold Time Analysis (972 hr. 7 es ❑Na N/A 3. Rush Turn Around Time Requested? Yes E314t, N/A a. SuNlclen[Volume? res No ONJA S. Correct Containers Used? -Pace Containers used? res res ❑No No ❑N/A ❑N/A 6. Containers Intact? es 0NO ONA 7. Dissolved analysis: Samples Field Filtered? CIYCS No h/A B. Sample Labels Match COC? •Includes Date me/fD/Anal is Matrfa: gyes 1 W ONO ❑N/A 9. Heads ace in VOA Vials (>5.6mm)? EIVO IOND EINM 1 10, Trip Blank Present? Trip Blank Custody Seals Present? []Yes hv,, ',;ONO QNc, ❑N/A . N/a 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of spit Containers: WENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time; Date: Date: Field Data Required? (—]Yes ❑No Page 16 of 18 Document Name: Document Revised: November IS, 2021 a Sample Condition Upon Receipt (SCUR) Page 2 of 2 2eAnMcal. • Document No.: Issuing Authority: FCAR-CS•033•Rev.08 Pace Carolinas.Quality Offirp *Check mark top half of box if pH and/or dechiorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottles Project # Wo#:92581375 PH: MI4B Due Date: Ol / 13/22 CLIENT: 92-NECK CO SUN no 01"_ UUMU ��iIYYf�f�ww�Y��a UUM fifiYYYY,�Y RAW �iYYYnun PH Adjustment log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time presenntion adjusted Amount of Preservative added Lot A Note: Whenever there is a discrepancy atrecung IVOrtn wTouna complianUe samples, a urpr v# 1,11+40 wI Ii. "Oil We sni W p.e. Out of hold, Incorrect preservathra, out of temp, incorrect containers. Page 17 of 18 8 L JO 8 L 06ed M C � as E� � 3g O v E' E� cr qaa w a _ w � C Q O � 0 � J OW l8 J CO) A2 W 9LL 4 Q = W V P C IU] r :t� sej uteNIU jam Pe as p{,�.� .�,• 4♦,Aai,A 5'-'r 1. Apoisno Gal i f a �'=.s W PaalD00a ' z `` cw� e�yo 19nplsea 0 u! dW31 i` 5y�5r��jj s: I'i¢•'975J'j Mt Aq eseei0 Ptm RO � -. GOOISMO SO4d ieiol i ML W3H•JZS Hdl d 4103 i8"d ri N)IW uQftMN ie101 y� gleiaW dui L'OOZ r x SSl JMO lwBLpaW :f v £OZSZeN I , ayi a o ~ N .I Z ` t3 `m VOSZH Paluasaidun � 81l3flIV1N00 401 dl 5 � C7 a a a H0110311031vCM3131clim cv LU 2 x Q MIS SN W O 1 (dWO3-J OVUS-0) 3dA.L31dvm C�+ 0 (Vol 01 sopoo PIPA gas) 3000 x1vix" q ¢ Q �[ 3 ' COO $ �v dot ` E � g am y #t W311 M �� •JIB � 1.'.}1 � ,�� 'Z� 1�� _� `^..—• V `M'i I ..f iq� :�� .1 . KIC EnWroomenlal Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfilling out thisform, please visit httos://deg.nc.gov/about/divisions/enerev-mineral-land- resources/enerev-mineral-land-permits/stormwater-perm its/n odes-industrial-sw#tab-4 Permit No. Facility Name: 1J Inspector: 6 Ig Date of Inspection: Time of Inspection: Total Event Precipitation (inches): 4;�' 0 t/ All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. I Structure (pipe, ditch, etc.) Receiving Stream: Page I of 2 Alec SWU-242, Last modified 07/28/2017 2. Color: Describe the color of the di (light, medium, dark) as descriptors: using basic colors (red, brown, blue, etc.) and tint hr-h-WA 3. Odor: Describ distinct odors that the ischar a may, Pave (i.e., smells strongly of il, weak chlorine odor, etc.): 1' 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 0 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there an foam in the stormwater discharge? QYYes O No. Y g 8. Is there an oil sheen in the stormwater discharge? OYes No. 0 9. Is there evidence of erosion or deposition at the outfall? O Yes d o. A) 10. Other Obvious Indicators of Stormwater Pollution: List and describe elf d f S Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 t e-1, AJ 'Riml IVV X "Juw —