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HomeMy WebLinkAboutNCG240016_Monitoring Report_20220606a MECKLENBURG COUNTY Land Use & Environmental Services Agency Solid Waste May 31, 2022 DEQ Mooresville Regional Office Attn: DEMLR Stomiwater Program 610 East Center Avenue Suite 301 Mooresville, NC 28115 Attention: DEMLR Stormwater Program o V Q asL�O2 i 0 nP Subject: Discharge Monitoring Report Mecklenburg County Compost Central — Certificate of Coverage No. NCG240016 Dear Central Files: Please find enclosed the Discharge Monitoring Report, May 2022, for Mecklenburg County Compost Central, a Type I facility located at 5631 West Blvd, North Carolina. If you have any questions, please contact me at 704- 634-7705 or by email at khaliem.adamsna mecklenbur countvnc gov Sincerely, / -o-- vld-,-t-- Khaliem Adams Solid Waste Environmental Specialist Enclosed: 2022 DMR PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2145 Soule Avenue Charlotte, North Carolina 28208 www.wipeoutwaste.com NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG240000 0 Compost Operations Click here for instructions �, :, c Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Uoload7.otm within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR R&'bnal Off ce. Certificate of Coverage No. NCG24 0016 Person Collecting Samples: Khaliem Adams Facility Name: Mecklenburg County Compost Central Laboratory Name: Pace Analytical Facility County: Mecklenburg Laboratory Cert. No.: Discharge during this period:0 Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? 0 Yes ❑ No If so, which Tier (I, II, or III)? Tier 2 A copy of this DMR hasbeen uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR ❑✓ Yes ❑ No Date Uploaded: oZ 0 a zt Analytical Monitoring Requirements for Outfalls with Industrial Activities— Benchmarks in (Red) Parameter Code Parameter Outfall2 Outfall Outfall Outfall Outfall N/A Receiving Stream Class N/A Date Sample Collected MM/DD/YYYY 5/23/2022 46529 24-Hour Rainfall in inches 1.00 in C0530 TSSin mg/L(100) 59.5 00340 Chemical Oxygen Demand (120) 80.5 31615 Fecal Coliform in colonies per 100 ml (loon) g800 600 Total Nitrogen in mg/L (30) 3.1 665 Total Phosphorus in mg/L (2) 2.1 400 pH in standard units (6.0-9.0) 6.82 01119 Copper, total recoverable in mg/L (0.030) <0.020 01051 Lead, total recoverable in mg/ L (0.075) <0.025 01094 Zinc, total recoverable in mg/ L (0.126) 0.0428 Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average 005S2 Non -Polar Oil & Grease in mg/L (15) <4.8 NCOIL Estimated New Motor/Hydraulic Oil Usage in gal/month 75ga1lmonth Notes (optional): N certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." or Delegated Authorized Individual f/]i IZ z Date Email Address Phone Number J019w Hd eglaoH ZZOZ/£Z/5 ZS*9 £Z£Z Z IlelinO lejlua:) Isodwo:) Aluno:) SinqualpaVq aldwes o� pasO a�lnad a�eQ Hd awu aldwes uolle3ol aldwes aweN Alllpel ace Analytical www.pacelabs.com May 31, 2022 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 Dear Darren Steinhilber: Pace Analytical services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on May 23, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte • Pace Analytical Services - Peachtree Corners, GA If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard mafthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Medenburg County Solid Waste REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 aceAnalytrcal wwarpacelabsaom CERTIFICATIONS Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 Pace Analytical Services, LLC 9800 Kinoey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 South Carolina Certification #: 99006001 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Drinking Water Cert. #: 99006003 North Carolina Drinking Water Certification M 37706 Florida/NELAP Certification #: E87627 North Carolina Field Services Certification* 5342 Kentucky UST Certification #: 84 North Carolina Wastewater Certification #: 12 Louisiana DoH Drinking Water #: LA029 South Carolina Laboratory ID: 99006 VirginiaNELAP Certification #: 460221 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 South Carolina Laboratory ID: 99030 Flodda/NELAP Certification #: E87648 South Carolina Certification #: 99030001 North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222 North Carolina Wastewater Certification M 40 Pace Analytical Services Peachtree Corners 110 Technology Pkwy, Peachtree Comers, GA 30092 North Carolina Certification #: 381 Florida DOH Certification #: E87315 South Carolina Certification #: 98011001 Georgia DW Inorganics Certification #: 812 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 aceAnalytical www.pacelabs.com SAMPLE ANALYTE COUNT Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92605891001 OUTFALL 2 EPA 1664E ICO 1 PASI-C EPA 1664B ICO 1 PASI-C EPA 200.7 DRB 3 PASI-GA SM 922213-2015 KDF 1 PASI-C SM 254OD-2015 ZMC 1 PASI-A TKN+NO3+NO2 Calculation MA132 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.01993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 SMT 1 PASI-A SM 5220D-2011 JP1 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte PASI-GA = Pace Analytical Services - Peachtree Comers, GA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 IaceAnalyNo fo www.patelabs.com ANALYTICAL RESULTS Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL 2 Lab ID: 92605891001 Collected: 05/23/2213:40 Received: 05/23/22 14:12 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Oil and Grease ND mg/L 4.8 1 05/25/22 00:30 1664 SGT HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 4.8 1 05/25/22 00:30 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Pace Analytical Services - Peachtree Corners, GA Copper ND ug/L 20.0 1 05/24/2210:25 05/24/2215:13 7440-50-8 Lead ND ug/L 25.0 1 05/24/2210:25 05124/2215:13 7439-92-1 Zinc 42.8 ug/L 20.0 1 05124/2210:25 05/24/2215:13 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 9800 CFU1100 mL 1.0 1 05/23/2217:30 05/24/22 15:34 2540D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services - Asheville Total Suspended Solids 59.5 mg/L 12.5 1 05/25/22 15:09 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 3.1 mg/L 0.040 1 05/27/2216:33 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 2.3 mg/L 0.50 1 05/24/2217:38 05/25/22 04:58 7727-37-9 353.2 Nitrogen, NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 0.78 mg/L 0.040 1 05/27/22 07:29 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 2.1 mg/L 0.060 1 05/25/22 22:28 05/27/22 00:44 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 80.5 mg/L 25.0 1 05/28/22 00:57 05/28/22 05:53 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 18 ® Pace Analytical Services, LLC a ceAnalytical 9800 Kincey Ave. Suite 100 www paaafabacam Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 QC Batch: 700238 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92605891001 METHOD BLANK: 3655127 Matrix: Water Associated Lab Samples: 92605891001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 05/25/22 00:30 LABORATORY CONTROL SAMPLE: 3655128 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 32.8 82 78-114 MATRIX SPIKE SAMPLE: 3655129 35719177001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 36.0 39.6 84.4 122 78-114 M1 SAMPLE DUPLICATE: 3655130 35719177002 Dup Parameter Units Result Result RPD Qualifiers Oil and Grease mg/L 3.6J 4.4J Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 (�Ia'neAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 700239 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92605891001 METHOD BLANK: 3655133 Matrix: Water Associated Lab Samples: 92605891001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 05/25/22 00:30 LABORATORY CONTROL SAMPLE: 3655134 Spike LCS LCS % Rec Parameter Units Conc. Result °% Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 21.1 106 64-132 MATRIX SPIKE SAMPLE: 3655135 35719177001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 6.2 19.8 34.0 140 64-132 SAMPLE DUPLICATE: 3655136 35719177002 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L 5.01.1 ND Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 ® Pace Analytical Services, LLC aceAnalXical 9800 Kincey Ave. Suite 100 vrw>wrpatelahs.i:am Huntersville. NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 QC Batch: 700100 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 Metals Total Laboratory: Pace Analytical Services - Peachtree Corners, GA Associated Lab Samples: 92605891001 METHOD BLANK: 3654368 Matrix: Water Associated Lab Samples: 92605891001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 20.0 05124/2214:45 Lead ug/L ND 25.0 05/2412214:45 Zinc ug/L ND 20.0 05/2412214:45 LABORATORY CONTROL SAMPLE: 3654369 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 1000 1060 106 85-115 Lead ug/L 1000 1060 106 85-115 Zinc ug/L 1000 1090 109 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3654370 3654371 MS MSD 92605862001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 1000 1000 1120 1130 111 113 70-130 2 Lead ug/L ND 1000 1000 1070 1090 106 108 70-130 2 Zinc ug/L ND 1000 1000 1100 1110 109 110 70-130 1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, L.I.C. Page 7 of 18 aceAnalyfical W".patelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 QC Batch: 700209 Analysis Method: SM 9222D-2015 QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92605891001 METHOD BLANK: 3654985 Associated Lab Samples: 92605891001 Matrix: Water Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 05/24/22 15:34 SAMPLE DUPLICATE: 3654986 92605862001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL 7400 6000 21 u2 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the resuiL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 Pace Analytical Services, LLC ® aceAnalytrca! 9800 Kincey Ave. Suite 100 wwwpacelabscom Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 QC Batch: 700269 Analysis Method: SM 2540D-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92605891001 METHOD BLANK: 3655382 Matrix: Water Associated Lab Samples: 92605891001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 05/25/22 15:03 LABORATORY CONTROL SAMPLE: 3655383 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 228 91 90-110 SAMPLE DUPLICATE: 3656413 92605862001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 18.6 32.6 55 D6 SAMPLE DUPLICATE: 3656414 92605886001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 730 696 5 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 aceAnalyiical www.pacofabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 QC Batch: 700152 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92605891001 METHOD BLANK: 3654672 Matrix: Water Associated Lab Samples: 92605891001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 05/25/22 04:27 LABORATORY CONTROL SAMPLE: 3654673 Spike LCS LCS °% Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3654674 3654675 MS MSD 92604736006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result e% Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.5 10 10 12.5 13.0 110 115 90-110 4 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3654676 3654677 MS MSD 92604736007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 2.4 10 10 13.1 12.5 108 101 90-110 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 ® Pace Analytical Services, LLC aLIUAnalytical 9800 Kincey Ave. Suite 100 wwx pacelabsoom Huntersville. NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 QC Batch: 700610 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.01993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92605891001 METHOD BLANK: 3657053 Matrix: Water Associated Lab Samples: 92605891001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.040 05/27/22 07:14 LABORATORY CONTROL SAMPLE: 3657054 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3657055 3657056 MS MSD 92605922001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.46 2.5 2.5 2.8 2.8 93 93 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3657057 3657058 MS MSD 92605923001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.17 2.5 2.5 2.5 2.5 95 95 90-110 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31 /2022 09:21 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 aceAnalytrca!® www.pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 700510 Analysis Method: EPA 365.1 Rev 2.01993 QC Batch Method: EPA 365.1 Rev 2.01993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92605891001 METHOD BLANK: 3656697 Matrix: Water Associated Lab Samples: 92605891001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 05/27/22 00:34 LABORATORY CONTROL SAMPLE: 3656698 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3656699 3656700 MS MSD 92605791001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.12 2.5 2.5 2.6 2.6 98 99 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3656701 3656702 MS MSD 92605791002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.5 2.5 99 99 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 Pace Analytical Services, LLC ® aceAnalytica� 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 tYlron pacafabscom (704)875-9092 QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 QC Batch: 701100 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92605891001 METHOD BLANK: 3659775 Matrix: Water Associated Lab Samples: 92605891001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 05/28/22 05:48 LABORATORY CONTROL SAMPLE: 3659776 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 765 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3659777 3659778 MS MSD 92604831008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 117 100 100 226 210 108 92 90-110 7 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3659779 3659780 MS MSD 92605862001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 134 100 100 235 233 101 99 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 Pace Analytical Services, LLC (�Ia'tcceamalytical ® 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 ww pacelftcom (704)875-9092 QUALIFIERS Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyi ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acryionitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 • Pace Analytical Services, LLC aceAnaiXical ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: COMPOST CENTRAL 1 Pace Project No.: 92605891 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92606891001 OUTFALL 2 EPA 1664B 700238 92605891001 OUTFALL 2 EPA 1664B 700239 92605891001 OUTFALL 2 EPA 200.7 700100 EPA 200.7 700181 92605891001 OUTFALL 2 SM 9222D-2015 700209 SM 9222D-2015 700212 92605891001 OUTFALL 2 SM 2540D-2015 700269 92605891001 OUTFALL 2 TKN+NO3+NO2 701065 Calculation 92605891001 OUTFALL 2 EPA 351.2 Rev 2.01993 700152 EPA 351.2 Rev 2.01993 700293 92605891001 OUTFALL 2 EPA 353.2 Rev 2.01993 700610 92605891001 OUTFALL 2 EPA 365.1 Rev 2.0 1993 700510 EPA 365.1 Rev 2.01993 700846 92605891001 OUTFALL 2 SM 5220D-2011 701100 SM 5220D-2011 701122 Date: 05/31/2022 09:21 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 18 -race Effective Date: 05/121202205/12/2022 Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersvilie d Raleigh❑ Mechanicsville❑ Atlanta(] Kernersville❑ " e•c,k��.n4,��Yfl fn�ani-v �r�l;�l 1naS-�2••••'� • ��w�a�t Courier: ❑Fe d Ex ❑UP& ❑LISPS Client Commercial El❑ ❑Pace Other: — II'lII "III I'llll II III 82605081 Custody Seal Present? ,� ❑Yes L"_INO Seals Intact? Elves �,/ Ehtvo Date/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap []Bubble Bags ❑None V Other Biological Tissu rozen?? Thermome Ir: ID: �j���t� [-]Yes ❑No AN/A �f�- Type of Ice: 146et ❑Dlue ❑lion Correction Factor: Cooler Temp: `�' Add/Subtract(T) 0 Temp should be above freezing to 6'C []Samples out of temp criteria. Samples on ire, cooling process Cooler Temp Corrected (°rhasbegun USDA Regulated Soil ( N/A; water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC Did samples originate from a foreign source (internationally, (check maosi?oyes f1Nn :__ „r-:.._ Comments/Discrepancy: Chain of Custody Present? Wes []No ❑N/A 1. Samples Arrived within Hold Time? Dres ONO ❑N/A 2. Short Hold Time Analysis (<72 hr.)? es-❑�No ❑N/A 3. Rush Turn Around Time Requested? Elves g o ❑N/A 4. Sufficient Volume? 1QYlvs []No ❑N/A S. Correct Containers Used? -Pace Containers Used? Y� 19Ke []No ❑No ❑N/A ❑N/A 6. Containers intact? 21a, []—No ❑ q 7. Dissolved analysis: Samples Field Filtered? ❑Y ❑No N/a 8. Sample labels Match COC? -includes Date/Time/ID/Analysts Matriz:--h[_ Yes []No ❑N/A 9. Headspace In VOA Vials (>5-6mm)? ❑Yes ❑No &A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes []Yes ❑No ❑No N/A /A 11. COMMENTS/SAMPLE Lot ID of splkcontalners: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: PrajpctjylanagetSREReview:.—. -- Qualtrax ID:69614 Date/Time: Date: Date: .--- -_ Field Data Required? []Yes []No Page 1 of 2 Page 16 of 18 I-Mace r ItUhf!r,3ye.;1s Effective Date: 05112I202205/12/2022 *Check mark top half of box if pH and/or dechlorination is verified and Project # 0 ' 92-606891within the acceptance range for preservation sam les. p PM: MWB Due Date: 09/3 1/22 "Bottom half of box is to list number of bottles —ECK CO ***Check all unpreserved Nitrates for chlorine z V ei CL ea ei EE M Q d. m z as �, m c`L > v a 0 N M a. m � 'O d N d iz > am E 0 � N 06 m -- a Z a, as 4A d C _� a N �'-t Ou m Y N v a ° o U �+ 19 E � o m N v x O Z u 'A A -' E Z a m M Z oa 2 M Q Z U W .J E N N d m a o u A J E m 4 m C 5 .. '° = y c ? W � 3¢ a a, C a a `m M � N v a T .n a m` �_ �-1 (7 a y Z y N a E J E O y� {V ' !rl a N v = a = M E Q Z ryi� rl a v x NoN x 0 Ln NNN M• a 1 Z Z .s 0 Cn e a x a > -, E S M n 1 ' w 2 NN 3 N—NN\ 4 N J \ \[\ N —\\-\\F N\\d -1 6 N _N \V N�]\\\ 7 \� \ \ V N - 8 N F N 9 IO \\N\11 iz _N NN O N Z -Z.0 � V S N M Q °' � c a a a > c fa M Z S N ~ u1 ci d O O 41 W H a in E E E E E �+ E E E E a in 0 OL Qo E E M H N N ^ N Wr +... C7 t? t9 an N r" O 0 ads > > a o> 06 y M. a V, n \\FT pH Adjustment Log for Preserved Samples Sample 10 Type of Preservative pH upon receipt Date preservation adjusted Time preseration Amount of Preservative Lot # adjusted added NOW.."Irrersever tnera 6 a discrepancy affecting North Caroiiina compliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Qualtrax 1D: 69614 Page 2 of 2 Page 17 of 18 CHAIN -OF -CUSTODY 1 Analytical Request Document 4ace_ The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. I Submittino a samole via this chain of custody constitutes acknowiedament and acceptance of the Pace Terms and Conditions found at httDs://Info.Dacelabs.comthubfs/cas-standard-terms.pdf. Section A Section B Section C Required Client Information: Required Project Information: Invoice information: Page : 1 C=PanY- Mecklenburg County Solid Waste Report To: Khafiem Adams Attention: Address: 2145 Suttle Ave. Copy To: Company Name: Of 1 Charlotte, NC 28208 Address: Regulatory Agency - Email: khatiem,edams mecklenb count ov Purchase Order #: Pace Quote: Phone: 980 314-3856 JFax Project Name: Compost Central 1 Pace Project Manager matthew.brainard@pacelabs.com. Stato / Locatbn - Requested Due Date: IFroject #: Pace Prae M 3207-1 NC R uestedA►nalysts Fittenid IN UATM cm Dnrrwp water ow wow VVT wasta waw ww Product P SAMPLE ID a s°�'° � One Character per box. wroa wP (A-Z, D-91, -) Air AR Sample Ids moat be unique::>ae rs s c 3 N to G' X z c '� to COLLECTED u 0 a _Z < 0 Preservatives } START END Z C Qe N x z x U�iD x = z e+s N 2 a$'1 2 �S a t-. 0 t a c� Vj 1.- trf a� m F z 0 2 o. N �0 o� t� m tu Y Z m o m tr Y GATE TtME DATE TIME 1 Oula I X a 1 total.1 total.l 101al.1 total btal.1 totat,l total,t 2 Oudatl 2 WT sAde 13a x x x x x x x -4 5 6 T 8 9 10 12- '%0D oHft C"MEHTS _. RELtNQtlI3HED BY IAFFthtATtON NQ' Ill . DATE Tt1sE: ACt: Et�TEDBYlAFFtLlATtON DATE,- Tt/[rt Ew . 8mPLE CON)tT ow Metab: Copper. Lead. Lncco 1v 00 0, M MWPLER NAME;MM gIGNATl1RE D. w m i F- m 8 a z EE z t � p PRINT Name of SAMPLER: Gt it(/M , SIGNATURE of SAMPLER: DATE Signed: a3 NC. Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfilling out thisform, please visit https:Hdeg.ne.gov/about/divisions/enerey-mineral-land- resources/enerev-m i neral-land-oerm its/storm water-oenn its/npdes-industrial-swktab-4 Permit No.: N/C/ L Facility Name: County: Nf C Inspector: —KA Date of Inspection: Time of Inspection: 'Al l+ / � / / a/ or Ce/�ificate e ! , fl b ld-f q W Lc.n 23 / zo^ a Total Event Precipitation (inches): ' Dv in Phone No.: N/C/G/�41/O /P/ '�; u , 77 o All permits require qualitative monitoring to be performed during a "measurable storm event." A 01measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: of Permittee or Designee) 1. Outfall Description: n� Outfal] No. 02 Structure (pipe, ditch, etc.): P` V Receiving Stream: p the industrial g Aivities that occur within the outfall drainage area: Vh/ Page I of 2 SWU-242, last modified 07/282017 2. Color: Describe the color of tbp discharge u (light, medium, dark) as descriptors: I J O/C basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe y distinct odors that the disch ge may ave (i.e., smells stro gly of oil, weak chlorine odor, etc.): C� S j 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam 1n the stormwater discharge? O Yes o. /VC) 8. Is there an oil sheen 1n the stormwater discharge? OYes '/'o. 9. Is there evidence of erosion or deposition at the outfall? : es 0 No. l`� 10. Other Obvious Indicators of Stormwater Pollution: List and describe NO 04" ofldicd6fs Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017