HomeMy WebLinkAboutNCG240016_Monitoring Report_20220606a
MECKLENBURG COUNTY
Land Use & Environmental Services Agency
Solid Waste
May 31, 2022
DEQ Mooresville Regional Office
Attn: DEMLR Stomiwater Program
610 East Center Avenue
Suite 301
Mooresville, NC 28115
Attention: DEMLR Stormwater Program
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Subject: Discharge Monitoring Report
Mecklenburg County Compost Central — Certificate of Coverage No. NCG240016
Dear Central Files:
Please find enclosed the Discharge Monitoring Report, May 2022, for Mecklenburg County Compost Central, a
Type I facility located at 5631 West Blvd, North Carolina. If you have any questions, please contact me at 704-
634-7705 or by email at khaliem.adamsna mecklenbur countvnc gov
Sincerely,
/ -o-- vld-,-t--
Khaliem Adams
Solid Waste Environmental Specialist
Enclosed: 2022 DMR
PEOPLE • PRIDE PROGRESS • PARTNERSHIP
2145 Soule Avenue Charlotte, North Carolina 28208
www.wipeoutwaste.com
NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG240000 0
Compost Operations
Click here for instructions �, :, c
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Uoload7.otm within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR R&'bnal Off ce.
Certificate of Coverage No. NCG24 0016
Person Collecting Samples: Khaliem Adams
Facility Name: Mecklenburg County Compost Central
Laboratory Name: Pace Analytical
Facility County: Mecklenburg
Laboratory Cert. No.:
Discharge during this period:0
Yes ❑ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? 0 Yes ❑ No
If so, which Tier (I, II, or III)? Tier 2
A copy of this DMR hasbeen uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR ❑✓ Yes ❑ No
Date Uploaded: oZ 0 a zt
Analytical Monitoring Requirements for Outfalls with Industrial Activities— Benchmarks in (Red)
Parameter
Code
Parameter
Outfall2
Outfall
Outfall
Outfall
Outfall
N/A
Receiving Stream Class
N/A
Date Sample Collected MM/DD/YYYY
5/23/2022
46529
24-Hour Rainfall in inches
1.00 in
C0530
TSSin mg/L(100)
59.5
00340
Chemical Oxygen Demand (120)
80.5
31615
Fecal Coliform in colonies per 100 ml
(loon)
g800
600
Total Nitrogen in mg/L (30)
3.1
665
Total Phosphorus in mg/L (2)
2.1
400
pH in standard units (6.0-9.0)
6.82
01119
Copper, total recoverable in mg/L
(0.030)
<0.020
01051
Lead, total recoverable in mg/ L
(0.075)
<0.025
01094
Zinc, total recoverable in mg/ L
(0.126)
0.0428
Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average
005S2
Non -Polar Oil & Grease in mg/L (15)
<4.8
NCOIL
Estimated New Motor/Hydraulic Oil
Usage in gal/month
75ga1lmonth
Notes (optional):
N certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations."
or Delegated Authorized Individual
f/]i IZ z
Date
Email Address Phone Number
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ace Analytical
www.pacelabs.com
May 31, 2022
Darren Steinhilber
Mecklenburg County Solid Waste
2145 Suttle Ave
Charlotte, NC 28208
RE: Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
Dear Darren Steinhilber:
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Enclosed are the analytical results for sample(s) received by the laboratory on May 23, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
mafthew.brainard@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Khaliem Adams, Medenburg County Solid Waste
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 18
aceAnalytrcal
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CERTIFICATIONS
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
Pace Analytical Services, LLC
9800 Kinoey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Drinking Water Cert. #: 99006003
North Carolina Drinking Water Certification M 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification* 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Louisiana DoH Drinking Water #: LA029
South Carolina Laboratory ID: 99006
VirginiaNELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
South Carolina Laboratory ID: 99030
Flodda/NELAP Certification #: E87648
South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification M 40
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Comers, GA 30092
North Carolina Certification #: 381
Florida DOH Certification #: E87315
South Carolina Certification #: 98011001
Georgia DW Inorganics Certification #: 812
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 18
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SAMPLE ANALYTE COUNT
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
92605891001 OUTFALL 2 EPA 1664E
ICO
1
PASI-C
EPA 1664B
ICO
1
PASI-C
EPA 200.7
DRB
3
PASI-GA
SM 922213-2015
KDF
1
PASI-C
SM 254OD-2015
ZMC
1
PASI-A
TKN+NO3+NO2 Calculation
MA132
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.01993
KDF1
1
PASI-A
EPA 365.1 Rev 2.0 1993
SMT
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Comers, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 18
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ANALYTICAL RESULTS
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: OUTFALL 2 Lab ID: 92605891001 Collected: 05/23/2213:40 Received: 05/23/22 14:12 Matrix: Water
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L 4.8 1 05/25/22 00:30
1664 SGT HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L 4.8 1 05/25/22 00:30
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Peachtree Corners, GA
Copper
ND ug/L 20.0 1 05/24/2210:25 05/24/2215:13 7440-50-8
Lead
ND ug/L 25.0 1 05/24/2210:25 05124/2215:13 7439-92-1
Zinc
42.8 ug/L 20.0 1 05124/2210:25 05/24/2215:13 7440-66-6
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Charlotte
Fecal Coliforms
9800 CFU1100 mL 1.0 1 05/23/2217:30 05/24/22 15:34
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analytical Services - Asheville
Total Suspended Solids
59.5 mg/L 12.5 1 05/25/22 15:09
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
Total Nitrogen
3.1 mg/L 0.040 1 05/27/2216:33
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
2.3 mg/L 0.50 1 05/24/2217:38 05/25/22 04:58 7727-37-9
353.2 Nitrogen, NO2/NO3 pres.
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
0.78 mg/L 0.040 1 05/27/22 07:29
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
2.1 mg/L 0.060 1 05/25/22 22:28 05/27/22 00:44 7723-14-0
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
80.5 mg/L 25.0 1 05/28/22 00:57 05/28/22 05:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC.
Page 4 of 18
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Pace Analytical Services, LLC
a ceAnalytical
9800 Kincey Ave. Suite 100
www paaafabacam
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
QC Batch: 700238
Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92605891001
METHOD BLANK: 3655127
Matrix: Water
Associated Lab Samples: 92605891001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Oil and Grease
mg/L
ND 5.0 05/25/22 00:30
LABORATORY CONTROL SAMPLE: 3655128
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Oil and Grease
mg/L
40 32.8 82 78-114
MATRIX SPIKE SAMPLE: 3655129
35719177001 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
Oil and Grease
mg/L
36.0 39.6 84.4 122
78-114 M1
SAMPLE DUPLICATE: 3655130
35719177002 Dup
Parameter
Units
Result Result RPD Qualifiers
Oil and Grease
mg/L
3.6J 4.4J
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QC Batch: 700239
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1664E
Analysis Description:
1664 SGT HEM, TPH
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92605891001
METHOD BLANK: 3655133
Matrix: Water
Associated Lab Samples: 92605891001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 5.0 05/25/22 00:30
LABORATORY CONTROL SAMPLE:
3655134
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
°% Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 21.1
106 64-132
MATRIX SPIKE SAMPLE:
3655135
35719177001 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
6.2 19.8
34.0 140 64-132
SAMPLE DUPLICATE: 3655136
35719177002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Petroleum Hydrocarbons
mg/L
5.01.1 ND
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 18
®
Pace Analytical Services, LLC
aceAnalXical
9800 Kincey Ave. Suite 100
vrw>wrpatelahs.i:am
Huntersville. NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
QC Batch: 700100
Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 Metals Total
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92605891001
METHOD BLANK: 3654368
Matrix: Water
Associated Lab Samples: 92605891001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Copper
ug/L
ND 20.0 05124/2214:45
Lead
ug/L
ND 25.0 05/2412214:45
Zinc
ug/L
ND 20.0 05/2412214:45
LABORATORY CONTROL SAMPLE: 3654369
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Copper
ug/L
1000 1060 106 85-115
Lead
ug/L
1000 1060 106 85-115
Zinc
ug/L
1000 1090 109 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3654370 3654371
MS MSD
92605862001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units
Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Copper ug/L
ND
1000 1000 1120 1130 111 113
70-130 2
Lead ug/L
ND
1000 1000 1070 1090 106 108
70-130 2
Zinc ug/L
ND
1000 1000 1100 1110 109 110
70-130 1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, L.I.C.
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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
QC Batch: 700209 Analysis Method: SM 9222D-2015
QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92605891001
METHOD BLANK: 3654985
Associated Lab Samples: 92605891001
Matrix: Water
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 05/24/22 15:34
SAMPLE DUPLICATE: 3654986
92605862001 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms CFU/100 mL 7400 6000 21 u2
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the resuiL
REPORT OF LABORATORY ANALYSIS
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Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
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aceAnalytrca!
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Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
QC Batch: 700269
Analysis Method: SM 2540D-2015
QC Batch Method: SM 254OD-2015
Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92605891001
METHOD BLANK: 3655382
Matrix: Water
Associated Lab Samples: 92605891001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 05/25/22 15:03
LABORATORY CONTROL SAMPLE: 3655383
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 228 91 90-110
SAMPLE DUPLICATE: 3656413
92605862001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
18.6 32.6 55 D6
SAMPLE DUPLICATE: 3656414
92605886001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
730 696 5
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
(704)875-9092
QC Batch: 700152
Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92605891001
METHOD BLANK: 3654672
Matrix: Water
Associated Lab Samples: 92605891001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/L
ND 0.50
05/25/22 04:27
LABORATORY CONTROL SAMPLE: 3654673
Spike LCS
LCS °% Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/L
10 10
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3654674 3654675
MS MSD
92604736006
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result e% Rec % Rec
Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/L 1.5
10 10 12.5
13.0 110 115
90-110 4 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3654676 3654677
MS MSD
92604736007
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/L 2.4
10 10 13.1
12.5 108 101
90-110 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
wwx pacelabsoom
Huntersville. NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
QC Batch: 700610
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.01993
Analysis Description: 353.2 Nitrate + Nitrite, preserved
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92605891001
METHOD BLANK: 3657053
Matrix: Water
Associated Lab Samples: 92605891001
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/L
ND 0.040 05/27/22 07:14
LABORATORY CONTROL SAMPLE: 3657054
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L
2.5 2.5 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3657055
3657056
MS MSD
92605922001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.46
2.5 2.5 2.8 2.8 93 93
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3657057 3657058
MS MSD
92605923001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Cone. Result Result % Rec % Rec
Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.17
2.5 2.5 2.5 2.5 95 95
90-110 0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31 /2022 09:21 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QC Batch: 700510
Analysis Method: EPA 365.1 Rev 2.01993
QC Batch Method: EPA 365.1 Rev 2.01993
Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92605891001
METHOD BLANK: 3656697
Matrix: Water
Associated Lab Samples: 92605891001
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Phosphorus mg/L
ND 0.050 05/27/22 00:34
LABORATORY CONTROL SAMPLE: 3656698
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Phosphorus mg/L
2.5 2.5 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3656699 3656700
MS MSD
92605791001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Phosphorus mg/L 0.12
2.5 2.5 2.6 2.6 98 99
90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3656701 3656702
MS MSD
92605791002
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Phosphorus mg/L ND
2.5 2.5 2.5 2.5 99 99
90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
QC Batch: 701100
Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011
Analysis Description: 5220D COD
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92605891001
METHOD BLANK: 3659775
Matrix: Water
Associated Lab Samples: 92605891001
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0 05/28/22 05:48
LABORATORY CONTROL SAMPLE: 3659776
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L
750 765 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3659777
3659778
MS MSD
92604831008
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Chemical Oxygen Demand mg/L 117
100 100 226 210 108 92
90-110 7 R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3659779 3659780
MS MSD
92605862001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Chemical Oxygen Demand mg/L 134
100 100 235 233 101 99
90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC.
Page 13 of 18
Pace Analytical Services, LLC
(�Ia'tcceamalytical ® 9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
ww pacelftcom
(704)875-9092
QUALIFIERS
Project: COMPOST CENTRAL 1
Pace Project No.: 92605891
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyi ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acryionitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
u2 Colonies are too numerous to count. Actual result may be greater than reported.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2022 09:21 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 18
•
Pace Analytical Services, LLC
aceAnaiXical ®
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
COMPOST CENTRAL 1
Pace Project No.:
92605891
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method Batch
92606891001
OUTFALL 2
EPA 1664B
700238
92605891001
OUTFALL 2
EPA 1664B
700239
92605891001
OUTFALL 2
EPA 200.7
700100
EPA 200.7 700181
92605891001
OUTFALL 2
SM 9222D-2015
700209
SM 9222D-2015 700212
92605891001
OUTFALL 2
SM 2540D-2015
700269
92605891001
OUTFALL 2
TKN+NO3+NO2
701065
Calculation
92605891001
OUTFALL 2
EPA 351.2 Rev 2.01993
700152
EPA 351.2 Rev 2.01993 700293
92605891001
OUTFALL 2
EPA 353.2 Rev 2.01993
700610
92605891001
OUTFALL 2
EPA 365.1 Rev 2.0 1993
700510
EPA 365.1 Rev 2.01993 700846
92605891001
OUTFALL 2
SM 5220D-2011
701100
SM 5220D-2011 701122
Date: 05/31/2022 09:21 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 18
-race
Effective Date: 05/121202205/12/2022
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvilie d Raleigh❑ Mechanicsville❑ Atlanta(] Kernersville❑
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Courier:
❑Fe d Ex
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Client
Commercial
El❑
❑Pace
Other: —
II'lII
"III
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II
III
82605081
Custody Seal Present?
,�
❑Yes L"_INO
Seals Intact? Elves
�,/
Ehtvo
Date/Initials Person Examining Contents:
Packing Material:
❑Bubble Wrap
[]Bubble Bags ❑None
V Other Biological Tissu rozen??
Thermome Ir: ID:
�j���t�
[-]Yes ❑No AN/A
�f�-
Type of Ice: 146et
❑Dlue ❑lion
Correction Factor:
Cooler Temp: `�' Add/Subtract(T) 0 Temp should be above freezing to 6'C
[]Samples out of temp criteria. Samples on ire, cooling process
Cooler Temp Corrected (°rhasbegun
USDA Regulated Soil ( N/A; water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC Did samples originate from a foreign source (internationally,
(check maosi?oyes f1Nn :__ „r-:.._
Comments/Discrepancy:
Chain of Custody Present?
Wes
[]No
❑N/A
1.
Samples Arrived within Hold Time?
Dres
ONO
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
es-❑�No
❑N/A
3.
Rush Turn Around Time Requested?
Elves
g o
❑N/A
4.
Sufficient Volume?
1QYlvs
[]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
Y�
19Ke
[]No
❑No
❑N/A
❑N/A
6.
Containers intact?
21a,
[]—No
❑ q
7.
Dissolved analysis: Samples Field Filtered?
❑Y
❑No
N/a
8.
Sample labels Match COC?
-includes Date/Time/ID/Analysts Matriz:--h[_
Yes
[]No
❑N/A
9.
Headspace In VOA Vials (>5-6mm)?
❑Yes
❑No
&A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
[]Yes
❑No
❑No
N/A
/A
11.
COMMENTS/SAMPLE
Lot ID of splkcontalners:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
PrajpctjylanagetSREReview:.—. --
Qualtrax ID:69614
Date/Time:
Date:
Date: .--- -_
Field Data Required? []Yes []No
Page 1 of 2 Page 16 of 18
I-Mace
r ItUhf!r,3ye.;1s
Effective Date: 05112I202205/12/2022
*Check mark top half of box if pH and/or dechlorination is verified and Project # 0 ' 92-606891within the acceptance range for preservation sam les.
p PM: MWB Due Date: 09/3
1/22
"Bottom half of box is to list number of bottles —ECK CO
***Check all unpreserved Nitrates for chlorine
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pH Adjustment Log for Preserved Samples
Sample 10 Type of Preservative pH upon receipt Date preservation adjusted Time preseration Amount of Preservative Lot #
adjusted added
NOW.."Irrersever tnera 6 a discrepancy affecting North Caroiiina compliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax 1D: 69614 Page 2 of 2 Page 17 of 18
CHAIN -OF -CUSTODY 1 Analytical Request Document
4ace_ The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
I Submittino a samole via this chain of custody constitutes acknowiedament and acceptance of the Pace Terms and Conditions found at httDs://Info.Dacelabs.comthubfs/cas-standard-terms.pdf.
Section A Section B Section C
Required Client Information: Required Project Information: Invoice information: Page : 1
C=PanY- Mecklenburg County Solid Waste Report To: Khafiem Adams Attention:
Address: 2145 Suttle Ave. Copy To: Company Name:
Of 1
Charlotte, NC 28208
Address:
Regulatory Agency -
Email: khatiem,edams mecklenb count ov
Purchase Order #:
Pace Quote:
Phone: 980 314-3856 JFax
Project Name: Compost Central 1
Pace Project Manager matthew.brainard@pacelabs.com.
Stato / Locatbn
-
Requested Due Date:
IFroject #:
Pace Prae M 3207-1
NC
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PRINT Name of SAMPLER: Gt it(/M
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SIGNATURE of SAMPLER:
DATE Signed:
a3
NC.
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance onfilling out thisform, please visit https:Hdeg.ne.gov/about/divisions/enerey-mineral-land-
resources/enerev-m i neral-land-oerm its/storm water-oenn its/npdes-industrial-swktab-4
Permit No.: N/C/ L
Facility Name:
County: Nf C
Inspector: —KA
Date of Inspection:
Time of Inspection:
'Al
l+ / � / / a/ or Ce/�ificate
e ! , fl b ld-f q W Lc.n
23 / zo^ a
Total Event Precipitation (inches): ' Dv in
Phone
No.: N/C/G/�41/O /P/
'�; u , 77 o
All permits require qualitative monitoring to be performed during a "measurable storm event."
A 01measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
of Permittee or Designee)
1. Outfall Description: n�
Outfal] No. 02 Structure (pipe, ditch, etc.): P` V
Receiving Stream:
p the industrial g Aivities that occur within the outfall drainage area: Vh/
Page I of 2
SWU-242, last modified 07/282017
2. Color: Describe the color of tbp discharge u
(light, medium, dark) as descriptors: I J O/C
basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe y distinct odors that the disch ge may ave (i.e., smells stro gly of oil, weak
chlorine odor, etc.): C� S j
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
b. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam 1n the stormwater discharge? O Yes o.
/VC)
8. Is there an oil sheen 1n the stormwater discharge? OYes '/'o.
9. Is there evidence of erosion or deposition at the outfall? : es 0 No. l`�
10. Other Obvious Indicators of Stormwater Pollution:
List and describe NO 04" ofldicd6fs
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017