NCG240016_Monitoring Report_20220131

a
RECEIVED
,BAN<312022
DENR-DEMLR
nand Quality SectionMECKLENBURG COUNTY sle Regional Land Use & Environmental Services Agency
Solid Waste
January 25, 2022
DEQ Mooresville Regional Office
Attn: DEMLR Stormwater Program
610 East Center Avenue
Suite 301
Mooresville, NC 28115
Attention: DEMLR Stormwater Program
Subject: Discharge Monitoring Report
Mecklenburg County Compost Central — Certificate of Coverage No. NCG240016
Dear Central Files:
Please find enclosed the Discharge Monitoring Report, December 2021, for Mecklenburg County Compost
Central, a Type I facility located at 5631 West Blvd, North Carolina. If you have any questions, please contact
me at 704-634-7705 or by email at khaliem.adams@a mecklenburucountvnc.gov.
Sincerely,
X14JIL A,�"�
Khaliem Adams
Solid Waste Environmental Specialist
Enclosed: 2021 DMR
PEOPLE •PRIDE PROGRESS • PARTNERSHIP
2145 Suttle Avenue Charlotte. North Carolina 28208
www.wipeoutwaste.com

RECEIVED
NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG240000 Ji,N 3 1022
Compost Operations
Click here for instructions
OENR-DEMLR
Land Quality Section
Mooresville Regional Office
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG24 0016
Person Collecting Samples: Khaliem Adams
Facility Name: Mecklenburg County Compost Central
Laboratory Name: Pace Analytical
Facility County: Mecklenburg
Laboratory Cert. No.:
Discharge during this period: ✓❑
Yes
❑
No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes ❑ No
If so, which Tier (I, II, or III)? Tier 2
A copy of this DMR h s be n uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR 0 Yes ❑ No
Date Uploaded: ) aW
Analytical Monitoring Requirements for Outfalls with Industrial Activities— Benchmarks in (Red)
Parameter
Parameter
Outfall2
Outfall
Outfall
Outfall
Outfall
Code
N/A
Receiving Stream Class
N/A
Date Sample Collected MM/DD/YYYY
12/21/2021
46529
24-Hour Rainfall in inches
0.88 inches
C0530
TSSin mg/L(100)
5.0
00340
Chemical Oxygen Demand (120)
204
31615
Fecal Coliform in colonies per 100 ml
6000
(1000)
600
Total Nitrogen in mg/L (30)
3.0
665
Total Phosphorus in mg/L (2)
0.50
400
pH in standard units (6.0-9.0)
8.51
Copper, total recoverable in mg/L
01119
(0.010)
0.022
01051
Lead, total recoverable in mg/L
<0.0050
(0.075)
Zinc, total recoverable in mg/ L
01094
(0.126)
0.036
Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average
00552
Non -Polar Oil & Grease in mg/L (15)
<4.9
Estimated New Motor/Hydraulic Oil
NCOIL
Usage in al/month
75gal/month
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations."
1 f V
Signature of)
or Delegated Authorized Individual
1 1%24 j7-
Date
Email Address Phone Number

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(�IaceAnalj&ale
wwapacelabs.com
January 07, 2022
Darren Steinhilber
Mecklenburg County Solid Waste
2145 Suttle Ave
Charlotte, NC 28208
RE: Project: COMPOSTCENTRAL
Pace Project No.: 92579271
Dear Darren Steinhilber:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 21, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
�,4tI/u , a3i,___Q
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Khaliem Adams, Medenburg County Solid Waste
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.L.C.
Page 1 of 18

(�Ia'ucieAnalytical
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Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification * 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification M 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Flodda/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification M 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 18

(�Ia'ouAnalytical
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Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
Lab ID Sample ID
92679271001 OUTFALL 2
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
SAMPLE ANALYTE COUNT
Method Analysts
EPA 1664B
ICO
EPA 1664E
ICO
EPA 200.7 Rev 4.4 1994
CBV
SM 9222D-2015
KDF
SM 2540D-2015
ZMC
TKN+NO3+NO2 Calculation
DMN
EPA 351.2 Rev 2.0 1993
MFO
EPA 353.2 Rev 2.0 1993
KDF1
EPA 365.1 Rev 2.0 1993
MDW
SM 5220D-2011
JP1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Reported Laboratory
1
1
3
1
1
1
1
1
1
1
PASI-C
PASI-C
PASI-A
PASI-C
PASI-A
PASI-A
PASI-A
PASI-A
PASI-A
PASI-A
Page 3 of 18

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ANALYTICAL RESULTS
Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: OUTFALL 2 Lab ID: 92679271001 Collected: 12/21/21 13:25 Received: 12/21/21 13:55 Matrix. Water
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L 4.9 1 12/23/21 09:15
1664 SGT HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L 4.9 1 12/23/21 09:15
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
0.022 mg/L 0.0050 1 12/30/21 15:01 01/07/22 01:25 7440-50-8
Lead
ND mg/L 0.0050 1 12/30/21 15:01 01/07/22 01:25 7439-92-1
Zinc
0.036 mg/L 0.010 1 12/30/21 15:01 01/07/22 01:25 7440-66-6
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Charlotte
Fecal Coliforms
6000 CFU/100 mL 1.0 1 12/21/21 15:54 12/22/21 14:02 u2
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analytical Services -Asheville
Total Suspended Solids
5.0 mg/L 5.0 1 12/22/21 15:52
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
Total Nitrogen
3.0 mg/L 0.52 1 01/05/22 10:17
361.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Kjeldahl, Total
2.8 mg/L 0.50 1 01/03/22 22:09 01/05/22 06:01 7727-37-9
363.2 Nitrogen, NO2/NO3 pres.
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
0.15 mg/L 0.040 1 12/28/21 13:04
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
0.50 mg/L 0.050 1 12/27/21 20:19 12/27/21 22:08 7723-14-0
6220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
204 mg/L 25.0 1 12/24/21 01:33 12/24/21 04:45
Date: 01/07/2022 03:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 667986
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1664E
Analysis Description:
1664 HEM, Oil and Grease
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92579271001
METHOD BLANK: 3499446
Matrix: Water
Associated Lab Samples: 92579271001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Oil and Grease
mg/L
ND 5.0 12/23/21 09:15
LABORATORY CONTROL SAMPLE: 3499447
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Oil and Grease
mg/L
40 33.4
84 78-114
MATRIX SPIKE SAMPLE: 3499448
35684886001 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Oil and Grease
mg/L
1.1 U 39.6
32.8 81 78-114
SAMPLE DUPLICATE: 3499449
35684884001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Oil and Grease
mg/L
1 AJ 1.5J
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /07/2022 03:17 PM without the written consent of Pace Analytical Services, I.I.C.
Page 5 of 18

11%aAnalytrcal
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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 667984
Analysis Method:
EPA 1664E
QC Batch Method: EPA 1664B
Analysis Description:
1664 SGT HEM, TPH
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92579271001
METHOD BLANK: 3499433
Matrix: Water
Associated Lab Samples: 92579271001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 5.0 12/23/21 09:15
LABORATORY CONTROL SAMPLE:
3499434
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 15.7
78 64-132
MATRIX SPIKE SAMPLE:
3499435
35684886001 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
S.OU 19.8
15.4 74 64-132
SAMPLE DUPLICATE: 3499436
35684884001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Petroleum Hydrocarbons
mg/L
S.OU ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/07/2022 03:17 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 668895
Analysis Method:
EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.41994
Analysis Description: 200.7 MET
Laboratory:
Pace
Analytical Services - Asheville
Associated Lab Samples: 92579271001
METHOD BLANK: 3503165
Matrix: Water
Associated Lab Samples: 92579271001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Copper
mg/L
ND
0.0050
01/07/22 00:01
Lead
mg/L
ND
0.0050
01/07/22 00:01
Zinc
mg/L
ND
0.010
01107/22 00:01
LABORATORY CONTROL_ SAMPLE:
3503166
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Copper
mg/L
0.5
0.54
108 85-115
Lead
mg/L
0.5
0.50
100 85-115
Zinc
mg/L
0.5
0.50
101 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3503167
3503168
MS
MSD
92578424001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc.
Conc.
Result
Result % Rec % Rec
Limits
RPD Qual
Copper
mg/L 0.14
0.5
0.5
0.67
0.68 106 107
70-130
1
Lead
mg/L ND
0.5
0.5
0.50
0.51 100 101
70-130
1
Zinc
mg/L ND
0.5
0.5
0.53
0.53 104 104
70-130
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3503169
3503170
MS
MSD
92578969001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc.
Conc.
Result
Result % Rec % Rec
Limits
RPD Qual
Copper
mg/L 88.7
0.5
0.5
0.59
0.58 100 99
70-130
1
ug/L
Lead
mg/L ND
0.5
0.5
0.49
0.49 98 98
70-130
0
Zinc
mg/L 39.8
0.5
0.5
0.54
0.53 99 98
70-130
1
ug/L
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/07/2022 03:17 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 18

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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
QC Batch: 667945 Analysis Method: SM 9222D-2015
QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92579271001
METHOD BLANK: 3499121 Matrix: Water
Associated Lab Samples: 92579271001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 12/22/21 14:02
SAMPLE DUPLICATE: 3499122
92579412003 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms CFU/100 mL ND ND
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/07/2022 03:17 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 18

(�Ia'LnuAnalytical
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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 667975
Analysis Method: SM 2540D-2015
QC Batch Method: SM 254OD-2015
Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92579271001
METHOD BLANK: 3499348
Matrix: Water
Associated Lab Samples: 92579271001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 12/22/21 15:44
LABORATORY CONTROL SAMPLE: 3499349
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 246 98 90-110
SAMPLE DUPLICATE: 3499582
92578799001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
76.0 79.0 4
SAMPLE DUPLICATE: 3499583
92578953002 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
54.0 46.0 16
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/07/2022 03:17 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 18

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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 669501
Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.01993
Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92579271001
METHOD BLANK: 3505636
Matrix: Water
Associated Lab Samples: 92579271001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/L
ND 0.50
01/05/22 01:55
LABORATORY CONTROL SAMPLE: 3505637
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/L
10 9.7
97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3505640 3505641
MS MSD
92578242001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/L 79.6
10 10 92.5
98.7 129 192
90-110 7 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3506004 3506005
MS MSD
92578242002
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/L 3.1
10 10 14.6
15.7 115 126
90-110 7 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/07/2022 03:17 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 18

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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 668656
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.01993
Analysis Description: 353.2 Nitrate + Nitrite, preserved
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92579271001
METHOD BLANK: 3502028
Matrix: Water
Associated Lab Samples: 92579271001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/L
ND 0.040
12/28/21 12:33
LABORATORY CONTROL SAMPLE: 3502029
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L
2.5 2.4
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3502030 3502031
MS MSD
92578646001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 12.5
2.5 2.5 15.5
15.5 121 123
90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3502032 3502033
MS MSD
92578681001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 14.9
2.5 2.5 16.9
16.9 79 78
90-110 0 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/07/2022 03:17 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 18

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QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 668596
Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92579271001
METHOD BLANK: 3501909
Matrix: Water
Associated Lab Samples: 92579271001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Phosphorus mg/L
ND 0.050
12/27/2121:51
LABORATORY CONTROL SAMPLE: 3501910
Spike LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Phosphorus mg/L
2.5 2.5
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3501911 3501912
MS MSD
92578713001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
Phosphorus mg/L ND
2.5 2.5 2.5
2.6 100 102
90-110 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3501913 3501914
MS MSD
92578713002
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
Phosphorus mg/L ND
2.5 2.5 2.6
2.6 102 102
90-110 0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/07/2022 03:17 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 18

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 668367
Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011
Analysis Description: 6220D COD
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92579271001
METHOD BLANK: 3501144
Matrix: Water
Associated Lab Samples: 92579271001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0
12/24/21 04:41
LABORATORY CONTROL SAMPLE: 3501145
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Chemical Oxygen Demand mg/L
750 807
108 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3501146 3501147
MS MSD
92578087001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Chemical Oxygen Demand mg/L 88.8
100 100 204
204 115 115
90-110 0 M 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3501148 3501149
MS MSD
92579269003
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Chemical Oxygen Demand mg/L 69.6
100 100 187
185 118 115
90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/07/2022 03:17 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 18

(�Iaa'cuceaAnalyfical
www.pacelabs.com
QUALIFIERS
Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
u2 Colonies are too numerous to count. Actual result may be greater than reported.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/07/2022 03:17 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18

acleAnalytical
www.pacelabscom
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: COMPOST CENTRAL 1
Pace Project No.: 92579271
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92579271001
OUTFALL 2
EPA 1664B
667986
92579271001
OUTFALL 2
EPA 1664E
667984
92679271001
OUTFALL 2
EPA 200.7 Rev 4.4 1994
668895
EPA 200.7 Rev 4.4 1994
669317
92579271001
OUTFALL 2
SM 922213-2015
667945
SM 9222D-2015
667946
92579271001
OUTFALL 2
SM 254OD-2015
667975
92579271001
OUTFALL 2
TKN+NO3+NO2
669887
Calculation
92679271001
OUTFALL 2
EPA 351.2 Rev 2.01993
669501
EPA 351.2 Rev 2.0 1993
669566
92579271001
OUTFALL 2
EPA 353.2 Rev 2.01993
668656
92579271001
OUTFALL 2
EPA 365.1 Rev 2.01993
668596
EPA 365.1 Rev 2.0 1993
668643
92679271001
OUTFALL 2
SM 5220D-2011
668367
SM 5220D-2011
668389
Date: 01/07/2022 03:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 18

Document Name: Document Revised: November 15, 2021
Sample Condition Upon Reel t (SCUR) Page 1 of 2
aceAnalytical" Document No.: Issuing Authority:
F-CAR-CS-033-Rev.08 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersvlile'Y'i Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
• Client Name: Wo# : 92579271
So�•IC �NPbrgjeclR. II'll"IIII'lll IIII'II
M�rJ bwCct Ca.,.n d-L
Courier: ❑Fed Ex LJUPS, ❑USP ❑client
❑ Commercial Peace ❑Other:_ 92579271
I.
Custody Seal Present? ❑Yes '�]No seals Intact? ❑Yes `®No
Date/Initlah Person ExaminingContents: n fG
Packing Material: []Bubble Wrap [ Wubble Bags ❑None ❑' Other Biological Tissue Frozen?
[]Yes (3No -PN/A
CL
Thermometer. I'J0 j, (]Blue ❑None
�IR Gun 10: 1 �,_ "l Type of Ice:
777 COtrection Factor:
Cooler Temp: Add/Subtract(°C) Tempshouldbe above oftemp zing
to 6°C
[]samples; out of temp craeria. Samples on i@, coaling process
Coolerfiemp-Canected-rE). c % faTie6dl
USDA Regulated $oll0NIA, water sample) - ,
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples Originate from a forelgn source (Internationally,
U...". —A m„».. al-1) nvae nNn
res Na
- -- —
Comments Dlscrepancy:
Chain of Custody Present?
yes
ONo
N/A
1.
Samples Arrived within Hold Time?
- Yes
ONO
UNIA
2.
Short Hold Time Analysis (e72 hr.)?
es
no
N/A
3.
Rush Turn Around Time Requested?
❑yes
bNo
N A
4.
Sufficient Volume? -
yes
nNo
N/A
6.
Correct Containers Used?
-Pace Containers Used?
(--]No
No
❑N/A
N/A
fi.
Containers Intact?
L!Iez
�,rres
Yes
ONO
N/A
7.
Dissolved analysis: Samples Field Filtered?
Oyes
ONO
N/A
a.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysts Matrix: Wt
9i-
ONO
❑N/A
9.
Heads ace in VDA Vials (>S.6mm)?
❑Yes
rilriaa
. NIA
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
byes
No
ONO
❑N/A
/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time;
Date:
Date:
Field Data Required? []Yes ❑No
Page 16 of 18

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4ce CHAIN -OF -CUSTODY / Analytical Request Document
,,,,,a,.nm„ The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
! Submitting a sample via this chain of custody constitutes acknowledgment and acceptance of the Pace Terms and Conditions found at httDs://info.Dacelabs.comrhubfs/nas-standard-tc*rm-. ndf
� Vig o Section C
Required Client Information: Required Project Information: Invoice Information: Pa e • 1 Of 1
Company. Mecidenb CountySolid Waste Report TV.Khallem Adams Attention:
Address: 2145 Suite Ave. Copy To: Company Name.
Charlotte. NC 28208
Emaih khalism.adam medden count e.
Purchase Order#:
Address:
Pace Quota:
Phone: 980I314-38W Fax
Requested Due Date:
Project Name: COMP031 Central 1
IPro1ect P.
Pace Project Manager, [e-mail]
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Paee Profile #: 3207_1
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Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance onfilling out thisform, please visit httos://deg.nc.aov/about/divisions/energy-mineral-land-
resources/enerev-mineral-land-uermits/stormwater-hermits/nodes-industrial-swihab-4
Permit No.: N/C/01
Facility Name: A
County: kenn
Inspector: UA
Date of Inspection:
Time of Inspection:
I a/a11,2
or Certificate of Coverage No.:
Total Event Precipitation (inches): D t D I
Phone 4 / D y—'O y --7%0
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event' is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
of Permittee or Designee)
1. Outfall Description:
Outfall No. 02 Structure (pipe, ditch, etc.):
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area: !l�
Page 1 of 2
SWU-242, Last modified 07/28/2017

2. Color: Describe the color of
(light, medium, dark) as descriptors: _
3. Odor: Des
chlorine odor, etc.):
discharge using basic colors (red, brown, blue, etc.) and tint
.PA 1 I PM
r k r AAJ �)
any di§tint odors that the discharge may have (i.e., smells strongly of oil, weak
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes gelNo.
8. Is there an oil sheen in the stormwater discharge? OYes No. 0
9. Is there evidence of erosion or deposition at the outfall? O Yes ZN..
10. Other Obvious Indicators of Stormwater Pollution:
List and describe Wo 04�f ft-i l ak's , Mbl"e' rnU_bf) <1 'A Aq's
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017

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