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Home My WebLink AboutNCG240016_Monitoring Report_20211001eNBu�e u � MECKLENBURG COUNTY Z- Land Use & Environmental Services Agency o Solid Waste September 24, 2021 DEQ Mooresville Regional Office Attn: DEMLR Stormwater Program 610 East Center Avenue Suite 301 Mooresville, NC 28115 Attention: DEMLR Stormwater Program Subject: Discharge Monitoring Report Mecklenburg County Compost Central — Certificate of Coverage No. NCG240016 Dear Central Files: Please find enclosed the Discharge Monitoring Report, August 2021, for Mecklenburg County Compost Central, a Type 1 facility located at 5631 West Blvd, North Carolina. If you have any questions, please contact me at 704-634-7705 or by email at klialiem.adains@mecklenburgeountync.gov. SSi%incerely, a"It, Khaliem Adams Solid Waste Environmental Specialist Enclosed: 2021 DMR PEOPLE •PRIDE PROGRESS • PARTNERSHIP 2145 Suttle Avenue Charlotte, North Carolina 28208 www.wipeoutwaste.com NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG240000 Compost Operations Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG24 0016 Person Collecting Samples: Khaliem Adams Facility Name: Mecklenburg County Compost Central Laboratory Name: Pace Analytical Facility County: Mecklenburg Laboratory Cert. No.: Discharge during this period:❑✓ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑✓ Yes ❑ No If so, which Tier (I, II, or III)? Tier 1 A copy of this DMR ha been ploadqed electronically via https://edocs.deg.nc.gov/Forms/SW-DMR 0 Yes ❑ No Date Uploaded: �aa Analytical Monitoring Requirements for Outfalls with Industrial Activities— Benchmarks in (Red) Parameter Parameter Outfall2 Outfall Outfall Outfall Outfall Code N/A Receiving Stream Class N/A Date Sample Collected MM/DD/YYYY 08/19/2021 46529 24-Hour Rainfall in inches 0.27in C0530 TSS in mg/L(100) 3.7 00340 Chemical Oxygen Demand (120) 87.2 31615 Fecal Coliform in colonies per 100 ml 2400 (1000) 600 Total Nitrogen in mg/L (30) 2.0 665 Total Phosphorus in mg/L (2) 0.20 400 pH in standard units (6.0-9.0) 7.40 Copper, total recoverable in mg/L 01119 (0.010) 0.0056 Lead, total recoverable in mg/ L 01051 (0.075) <0.0050 Zinc, total recoverable in mg/ L 01094 (0.126) 0.010 Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average 00552 Non -Polar Oil & Grease in mg/L (15) <5.0 Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month 75ga1/month Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false infor , including the possibility of fines and imprisonment for knowing violations." 1 Signature of P#fmitttee or Delegated Authorized Individual Email Address // �ai'i c A. S�e;Ah:%w /rfcGl�'i G. S�,J Date Phone Number ,�Pv"31Y-J�-f7j J91aw Hd egPoH TZOZ/6T/8 I Ot?*L--1 LZTT I Z Ilellnp I lea}ua:) isodwo0 Aluno:) 8anqualpalN aldweS o; past 03lnaa a3ed Hd I awll aldwes I uoile3ol oldwes-F oweN Allipej Pace Analytical Semlces, LLC 15comalXical" 980OKincey Ave. Suite 100 Huntersville, NC 26078078 mnepacelailmin (704)875-9092 August 26, 2021 \j Darren Steinhilber �n Mecklenburg County Solid Waste Q 2145 Suttle Ave Charlotte, NC 28208 G ICJ RE: Project: Compost Central 1 Pace Project No.: 92556646 Dear Darren Steinhilber: Enclosed are the analytical results for sample(s) received by the laboratory on August 19, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L-C. Page 1 of 18 aceAnalytical arwarpacetabscom Project: Compost Central 1 Pace Project No.: 92556646 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification M 37706 North Carolina Field Services Certification M 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification M E87648 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 v irginia/VELAP Certification M 460221 North Carolina Wastewater Certification M 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification M 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Servces, LLC. Page 2 of 18 laceAnalyficale www.pacelabs.com SAMPLE ANALYTE COUNT Project: Compost Central 1 Pace Project No.: 92556646 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytts Reported Laboratory 92556646001 Outfall 2 EPA 1664E CJM 1 PASI-C EPA 1664E CJM 1 PASI-C EPA 200.7 Rev 4.41994 CBV 3 PASI-A SM 9222D-2006 KDF 1 PASI-C SM 254OD-2011 MJP 1 PASI-A TKN+NO3+NO2 Calculation DMN 1 PASI-A EPA 351.2 Rev 2.01993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.01993 MDW 1 PASI-A SM 5220D-2011 JP1 1 PASI-A PASI-A = Pace Analytical Services -Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 eacAnalytlfcal paceiabm m ANALYTICAL RESULTS Project: Compost Central 1 Pace Project No.: 92556646 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Outfall 2 Parameters Lab ID: 92556646001 Collected: 08/19/21 11:41 Results Units Report Limit DF Received: 08/19/21 12:45 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.0 1 08/24/21 10:50 M1 1664 SGT HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 08/24/21 10:50 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville Copper 0.0056 mg/L 0.0050 1 08/25/21 12:19 08/26/21 10:29 7440-50-8 Lead ND mg/L 0.0050 1 08125/2112:19 08/26/21 10:29 7439-92-1 Zinc ND mg/L 0.010 1 08/2512112:19 08/26/21 10:29 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 922213-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Charlotte Fecal Coliforms 2400 CFU/100 mL 1.0 1 08/19/21 17:24 08/20/21 15:38 D6,u2 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Asheville Total Suspended Solids 3.7 mg/L 2.5 1 08/25/21 12:41 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Asheville Total Nitrogen 2.0 mg/L 0.52 1 08/26/21 14:41 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 2.0 mg/L 0.50 1 08/25/21 22:09 08/26/21 04:55 7727-37-9 363.2 Nitrogen, NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.01993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 ND mg/L 0.040 1 08/25/21 10:19 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.01993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus 0.20 mg/L 0.050 1 08125/2119:05 08/25/2122:43 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 87.2 mg/L 25.0 1 08/26/21 00:26 08/26/21 06:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/26/2021 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 18 Pace Analytical Services, LLC la'A.MaIXical' 9800 Kinsey Ave. Suite 100 Huntersvilie, NC 28078 wyrr�pas:elabs.eom (704)875-9092 QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92556646 QC Batch: 642347 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92556646001 METHOD BLANK: 3371321 Matrix: Water Associated Lab Samples: 92556646001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 08/24/21 10:50 LABORATORY CONTROL SAMPLE: 3371322 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 33.8 84 78-114 MATRIX SPIKE SAMPLE: 3371323 92556646001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 39.6 31.2 77 78-114 M1 SAMPLE DUPLICATE: 3371324 70184515001 Dup Parameter Units Result Result RPD Qualifiers Oil and Grease mg/L 22.3 17.9 22 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/26/2021 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 IaceAnalytical www.patelabs.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92556646 Pace Analytical Services, LLC 9800 Kincey Ave. Sulte 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 642348 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 SGT HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92556646001 METHOD BLANK: 3371325 Matrix: Water Associated Lab Samples: 92556646001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 08/24/21 10:50 LABORATORY CONTROL SAMPLE: 3371326 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 19.8 99 64-132 MATRIX SPIKE SAMPLE: 3371327 92556646001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 19.8 14.6 69 64-132 SAMPLE DUPLICATE: 3371328 70184515001 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L 9.7 8.6 12 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/26/2021 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 ' Pace Analytical Services, LLC la'.ceAnalytical � 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 www pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92556646 QC Batch: 642830 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92556646001 METHOD BLANK: 3373202 Matrix: Water Associated Lab Samples: 92556646001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper mg/L ND 0.0050 08/26/2109:31 Lead mg/L ND 0.0050 08/26/2109:31 Zinc mg/L ND 0.010 08/26/2109:31 LABORATORY CONTROL SAMPLE: 3373203 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/L 0.5 0.48 95 85-115 Lead mg/L 0.5 0.46 93 85-115 Zinc mg/L 0.5 0.43 86 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3373204 3373205 MS MSD 92555994002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Copper mg/L 0.0059 0.5 0.5 0.49 0.49 97 96 70-130 1 Lead mg/L ND 0.5 0.5 0.48 0.48 97 96 70-130 1 Zinc mg/L 0.049 0.5 0.5 0.51 0.51 92 92 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3373206 3373207 MS MSD 92556646001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 0.0056 0.5 0.5 0.50 0.50 99 98 70-130 1 Lead mg/L ND 0.5 0.5 0.47 0.47 94 94 70-130 0 Zinc mg/L ND 0.5 0.5 0.46 0.45 90 89 70-130 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/26/2021 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 IJMAAnalytfcal® wrrw..parelaDs.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92556646 QC Batch: 641744 Analysis Method: SM 9222D-2006 QC Batch Method: SM 922213-2006 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92556646001 METHOD BLANK: 3368290 Associated Lab Samples: 92556646001 Parameter Units Fecal Coliforms CFU/100 mL SAMPLE DUPLICATE: 3368291 Parameter Units Fecal Coliforms CFU/100 mL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 08/20/2115:38 92556646001 Dup Result Result 2400 600 RPD Qualifiers 120 D6,u2 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/26/2021 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 ' Pace Analytical Services, LLC la'aeAnalXical'o 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 w wpnelftcom (704)875-9092 QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92556646 QC Batch: 642803 Analysis Method: SM 254OD-2011 QC Batch Method: SM 264OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92556646001 METHOD BLANK: 3373128 Matrix: Water Associated Lab Samples: 92556646001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 08/25/21 12:39 LABORATORY CONTROL SAMPLE: 3373129 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 250 100 90-110 SAMPLE DUPLICATE: 3373604 92556934001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 164 152 8 SAMPLE DUPLICATE: 3373605 92566647001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 77.3 84.7 9 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/26/2021 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 aceAnailyical afwafpat:ela5s.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92556646 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 642921 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92556646001 METHOD BLANK: 3373750 Matrix: Water Associated Lab Samples: 92556646001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Neldahl, Total mg/L ND 0.50 08/26/21 04:37 LABORATORY CONTROL SAMPLE: 3373751 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.8 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3373752 3373753 MS MSD 92556375002 Spike Spike MS MSD MS MSD °% Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 4.5 10 10 16.3 15.8 118 113 90-110 3 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3373754 3373755 MS MSD 92556397001 Spike Spike MS MSD MS MSD °% Rec Parameter Units Result Conc. Conc. Result Result % Rec °% Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 0.98 10 10 11.1 11.3 101 103 90-110 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/26/2021 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 lZeAnalyfical" www.pacoaba.egra Project: Compost Central 1 Pace Project No.: 92556646 QC Batch: 642731 QC Batch Method: EPA 353.2 Rev 2.0 1993 Associated Lab Samples: 92556646001 METHOD BLANK: 3373000 Associated Lab Samples: 92556646001 Parameter Units Nitrogen, NO2 plus NO3 mg/L QUALITY CONTROL DATA Analysis Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.040 08/25/2109:57 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 3373001 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3373002 3373003 MS MSD 92554781001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L ND 2.5 2.5 2.5 2.5 98 100 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3373004 3373005 MS MSD 92556164004 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 22.2 2.5 2.5 24.5 24.2 93 80 90-110 1 M7 Results presented on this page are in the units indicated by the "Unlis" column except where an alternate unit is preeminent to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/26/2021 04:10 PM without the written consent of Pace Analytical Services, U.C. Page 11 of 18 aceAnalyircal www.pacelabucm QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92556646 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 642698 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92556646001 METHOD BLANK: 3372910 Matrix: Water Associated Lab Samples: 92556646001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 08/25/2122:25 LABORATORY CONTROL SAMPLE: 3372911 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3372912 3372913 MS MSD 92554588001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 4.3 2.5 2.5 7.1 7.2 112 117 90-110 2 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3372914 3372915 MS MSD 92554588003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 4.7 2.5 2.5 7.3 7.4 104 109 90-110 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/26/2021 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 • Pace Analytical Services, LLC aceAnalytrcal ® 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 WM Paeebbs ctnn (704)875-9092 QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92556646 QC Batch: 642951 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92556646001 METHOD BLANK: 3373892 Matrix: Water Associated Lab Samples: 92556646001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 08/26/21 06:28 LABORATORY CONTROL SAMPLE: 3373893 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 751 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3373894 3373895 MS MSD 92556451001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 2310 100 100 2430 2560 118 245 90-110 5 M1,R1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/26/2021 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 Pace Analytical Services, LLC aceAnalyical ® 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 1s1Y pBtBl85E.CG1i1 (704)875-9092 QUALIFIERS Project: Compost Central 1 Pace Project No.: 92556646 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/26/2021 04:10 PM without the written consent of Pace Analytical Services. LLC. Page 14 of 18 IceAnalytcalo awa pacelabU= QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Compost Central 1 Pace Project No.: 92556646 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92556646001 Outfall 2 EPA 1664B 642347 92556646001 Outfall 2 EPA 1664B 642348 92656646001 Outfall 2 EPA 200.7 Rev 4.4 1994 642830 EPA 200.7 Rev 4.4 1994 642920 92556646001 Outfall 2 SM 9222D-2006 641744 SM 9222D-2006 641745 92556646001 Outfall 2 SM 254OD-2011 642803 92556646001 Outfall 2 TKN+NO3+NO2 643289 Calculation 92556646001 Outfall 2 EPA 351.2 Rev 2.0 1993 642921 EPA 351.2 Rev 2.0 1993 643080 92556646001 Outfall 2 EPA 353.2 Rev 2.0 1993 642731 92556646001 Outfall 2 EPA 365.1 Rev 2.0 1993 642698 EPA 365.1 Rev 2.0 1993 643050 92556646001 Outfall 2 SM 5220D-2011 642951 SM 5220D-2011 643092 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/26/2021 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 18 Document Name: Document Revised: October 28, 2020 - 2oAnalyfical' Sample Condition Upon Recel t(SCURI I Page I of 2 Document No.: Issuing Authority: I F-CAR{5-o33-Rev.07 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville Q/Raleigh❑ Mechanicsvllle❑ Atlanta❑ Kernersville❑ Client Name:N'CdA lik WO# : 92556646 to Lyr+ef I lei e`toig NEI II �I I III IIII Laud[L]UPS QFed Ex UPS QUSPS lent I III ❑ Commercial ❑Pace QOther. Custody Seal Present? []Yes�pf6 Seals Intact?QYes o11� /.� 646 Date/InItalsPerson Examining Contents: NISShcge�� Packing Material: ❑Bubble Wrap ❑Bubble Bags n4une ❑ Other Thermomete •��/ •j�A r.. n• �i .Z 1 A.'t3' 9 et QBlue �1 c� Correction Factor: Cooler Temp: `Z Add/Subtract (°Cj --0 , I Cooler Temp Corrected (Vfj! j USDA Regulated Soll( /A, water sample( Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps(? ❑Yes ❑No Biological Tissue Frozen? ❑Yes ❑No V/A Temp should be above freezing to 6'C ❑samples out of temp criteria. Samples on Ice, cooling process has begun Did samples originate from a foreign source (Intemationally, Comments/Discrepancy: Chain o(Custody Present? es ONO ONJA 1. Samples Arrived within Hold Time? Vfu ElNo N/A 2. Short Hold Time Analysis 1<72 hr.)? es No N/A 3. Rush Turn Around Time Requested? ❑Yes Jyo ONJA 4. Sufficient volume? V& ON. ON/A S. Correct Containers Used? -Pace Containers Used? trres ONO ONO ❑N/A QNIA 6. Containers Intact? es Ord. N A 7. Dissolved analysis: Samples Field Filtered? Oyes ONo A B. Sample labels Match COC? -Includes Date me/ID/Anal sis Matrix: \Arr J;jt'es []No ❑N/A 9. Headspace in VOA Vials >5-6mm(? []Yes ONO N/ 10. Trip Blank Present? Trip Blank Custody Seals Present? Elves OYes [:]No ONO UKA a1A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Project Manager SCURF Review: Date: Project Manager SRF Review: Date: Field Data Required? ❑Yes ❑No •siaulinuo3 i3ammul'dwal jo ino'aApenjasajd 138JI03ul'pl04 10 3np •r1,a�tuMteunrru3e�wN �sQrr•eu[[e�ea•u�oN-au�•f»-z[eg�ae-rer�,•�u�ersrur�aAdaa•Nsa[dines•a3uettdutOa-eutlole]-tt31oN,8ullame•�ueda�3slp•e-sW�ayl�al�auay�:a3ON p 301 papp4 aApeAiasald j0lunOwV paisn(ps uollemosaid outl1 poisn(pe uoOemosaid ales 3dlasai uodn Hd aApmesud jo adAl al oldweS saldweS panaasOM ao; 301 juawlsnfpb Hd ►v�ii►►��ni� e iii►vniiiiii► pop, 1p zaa� s _ J MOM solneq jo aagwnu ;sil of s! xoq F Jley WOUOG * 8H11'a00 paiem) siOB/0»o'aseaig pue 110'301'uuOJIIO0'VOA :suopdeax3 •saidwes u014eAJosaad aoj ague] awndo= 844 uly31An pue pal)llOA s! U01MIJ014381P ao/pue Hd;) xoq;o;1ey do; >iaew 312043* a3gjo Alilen7o seullole:) aced LO'Aa?J-££O-S3-VV"3-J :/4llo4;nV 8ulnssl :•oN juawn3o0 + jaJr�fjeuya�a "� Z;o Z a ed afUS jdlaaab uodn uolilpuo3 al we5 OZOZ'8Z jagopo :paslnaa ivawnao4 :aweN 3uawn3oo CHAIN -OF -CUSTODY / Analytical Request Document Aw&ft. .w..rutueuaK The Chain -of -Custody is a LEGAL DO UMENT. All relevant fields must be completed accurately. Submitting a sample ela this chain of custody constitutes acknowledgment and acceptance of the Pace Terms and Conditions found at htips:/finfo.pacelabs.com/hubfs/pas-stand ard-terms. Section A Section B Section C Required Client Information: Required Project Information: Invoke Information: Page : 1 Of 1 Company: WleddenbuM County Solid Waste Report To: Khaliem Ads Attention: Address: 2145 Suttte Ave. Copy To: Company Name: Chartette. NC 28208 Address -� Email: khaHemodemsernoWen Purchase Order;W Pace Quote: Phone 980 3143858 JFax Proied Name: Compost Central 1 Pace Project Manager: matthew.brainard0pacelabs.com. Requested Due Date: 1projea M Pace Profile m. 3207 1 NO f a FElterod y a �(COD�' e U COLLECTED Z Prese atives s m ass watex ON 'S !� W" WT W"te woar ww .i m °+ c _ SAMPLE ID Peodud P O > a START END OJ A + z One Character per box. oO�� wl" wP ,,, 0.* x as g c m w n Sample ids must be unique odw OT Tntw TS V m- O v t n N —pp m _ o. x j v C Cl z — r ^� f� 0O c N a V � m a 0 to m o S b CL m qos -� DATE TIME DATE TIME a�= x x z z 2 O v i a cr O 1 [Y 1 total,l taw.1 t WLI total.l total,l towki fault 2. "all2 wT ? !�� l i a� r4' a► if�f a x x x x x x x .3 4 -b, 9 ' `coMrtENrs . a r�•. �r ,. �..•[ y ;Rattniati�sttEneYf AFl�tU14TtON.�'ACCttTYI.AFFtt.lA Ito N `rt�RE� 3 ' L SAtRP1E: N8 -:C �-P3.: R^` .fit.. f Y•r ^ ...M"', _DATE3.i Y. Metals! Copper. Lead. irna S",ptil:t N_ AMIE AND,SiGI&T-6, E g Z t G PRINT Name of SAMPLER: e p StGNATItRE of SAMPLER 2 a z a co 8 13 e DATE Signed: I n -� A% f ? FW- PY U t 1 C 00 `� Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfilling out thisform, please visit hgps://dea.nc.eov/about/divisions/energy-mineral-land- resources/energv-m i neral-I and -perm its/stormwater-permits/npdes-industrial-sw#tab-4 Permit No.: N/C/ l Facility Name: County: - Inspector: Kh H Date of Inspection: Time of Inspection: Total Event Precipitation (inches): C 0• a7/0 0 0/ (/�'/ All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local stone events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall escription: Outfall No. Structure (pipe, ditch, etc.): Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: V Y h 1 C Page I of 2 SWU-242, Last modified 07/28/2017 r 2. Color: Describe the color of (light, medium, dark) as descriptors: _ ing basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe ny distinct odors tha the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no soli and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? O Yes No. 8. Is there an oil sheen in the stormwater discharge? OYes O No. 9. Is there evidence of erosion or deposition at the outfall? O Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe No i 4 0 r -S Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 All ielp ll