NCG200515_Monitoring Report_20220118

Boyer Enterprises East, LLC
see
January 12, 2022
DEQ Morrisville Regional Office
Attention: DEMLR Stormwater Program
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Subject: STORMWATER SAMPLING RESULTS
ZERO WASTE RECYCLING, INC.
301 DUPREE STREET
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
PERMIT NCG200515
Dear Sir/Madam:
Attached please find the Stormwater Discharge Monitoring Reports (DMR) and analytical
report for the sampling conducted at the above -referenced site. A stormwater sample was
collected from Outfall 001 and 002 on December 12, 2021 and analyzed for lead (Pb),
copper (Cu), zinc, (Zn), and chemical oxygen demand (COD). As indicated on the
attached DMR, all parameters were reported below or within their respective benchmark
values except for CU at Outfall 2, Zn at Outfall 1 & 2, and ZN at outfall 3. Based on these
results, a Tier One Response has been implemented at the facility and the results
documented in the facility's Stormwater Pollution Prevention Plan (SPPP). If you have any
questions or need additional information, please contact me at [phone].
Note: The sample kit was not complete during the monitoring event. A make monitoring
event will be conducted on the first qualified rain event.
Sincerely,
BOYER ENTERPRISES EAST, LLC
Paul W. Spangenberg
EH&S Compliance Director
Attachments: Cover Letter
Stormwater Discharge Monitoring Reports
Laboratory Report
127 Red Hill Church Road, Dunn, North Carolina, 28334

NCDEQ Division of Energy, Mineral and land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG2000O0
Scrap Metal
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30days ofreceiving sampling results. Mail theoriginal, signed hardcogWof the DW Wthe appropriate DEMLR Regional Office.
Certificate of Coverage No. NOG2O 0515
Person collecting samples: Chris Gossernt
Facility Name: Zero Waste Recycling, Inc.
Laboratory Name: Pace
Facility County: Meddenbteg
Laboratory Cert Na_ 12
Discharge during this period: QYes
❑No(ifrnskip tosignature and date)
Has your facility implemented mandatory Tier response actions
If so, which Tier (1,11, or 01)?
this sample period for any benchmark exceedances? ❑� Yes []No
AcopyofthisDMRhasbeenuploadedelectronicakVviahttos://edocs.deg.nc.gov/Forms/SW-DMR
Date Uploaded: 1/1222
Yes []No
Analytical Monitoring Requirements for Outfalis with LndustrialActivities—Benchmarks in (Red)
Pwanx er
Parameter
OutPae 01
Oalfa6 02
Oudall 03
Outfalf
Outfall
Code
N/A
Receiving Stream Class
C
C
C
N/A
Date Sample Collected MM/DD/YYYY
12/10/21
12f1Of21
12MG121
46529
24-Hour Rainfall in inches
0.08
0-08
0.08
CO530
TSS in r g/L (100 or 50')
00340
Chemical Oxygen Demand (120)
108
69.6
173
00552
Non -Polar Oil & Grease in mg/L (15)
Copper, teal recoverable in rrg)L
DIM io
0.0067
0.018
0.0061
0.010 FW 0.0055
Lead, total recoverable (as Ph) in
01051
nW L 0.075 FW 02220 s
0.0069
0-0071
0-0097
Zinc, total recoverable in aWL (0.126
CO034
0.145
0-156
0-102
FW 0.095 SW
Additional parameters for ou falls in drainage areas that use>55 gallons per month of pew hydraulic oil on average
Estimated New Motor/Hydraulic OR
NCOIL
Usage in gal/month
. OuUalls to erg Resource Waters (01111N1►, High Quay waters ORM, Trout waters (rr) and Primary Nursery Areas (PNA)
have a bendamrk135 emit of So mg/L, M other rater dasa6od� hmea ' k of 100 mg/L
FW (Freshvrater) SW (Sakwater)
4 Notes (optional): The sample kit was not complete. O&G and TSS were not monitored. We will conduU make monitoring on the next rain event.
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete.) am aware that there are significant penalties for submitting
false information, mclud!gg" possibility of fines and imprisonment for knowing violations."
1 /12/ 22
Signature oVermittee or Delegated Authorized Individual Date
Email Ad&15ss [e-mail] Phone Number [phone]

aceftlytical,
rrrnNN�a�as
Paca Analytical Services, LLC
9800 l0ncey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 05, 2022
Chris McRae
Zero Waste Recycling, LLC
301 Dupree Street
Charlotte, NC 28208
RE: Project: STORMWATER-CHARLOTTE
Pace Project No.: 92578737
Dear Chris McRae:
Enclosed are the analytical results for samples) received by the laboratory on December 17, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions oonceming this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
Q"cc..
a` REPORT OF LABORATORY ANALYSIS
The re steal m be neproduceC. in k*
9g wffl utthe WrMM=r Aat Pa An*hCal Smioes. LLC.
Page 1 of 14

Projet# STORINYIdATER-CHARLOTTE
Pace Project No.: 92578737
Pace Analytical Services Charlotte
PawAna"cat Setvk*% LLC
9800 Kmoey Ave. Suite 100
HuntemviDe. NC 28078
(M)878-9092
South Carolina Laboratory 1D: 99M
9800 Kinney Ave. Ste 100, Huntersviile, NC 28078
North Carolina Drinking Water Certification V. 37706
North Carolina Fielki Services Certification #: 5342
North Carolina Wastewater Certification #:12
South Carorma Laboratory ID: 99006
CERTIFICATIONS
South Carona Cron #: 99006001
South Carolina Drinking Water Cert. #: 99006003
FloddalNELAP Certification #: E87627
K dudcy UST Certification #: 84
Louisiana DoH Waterr #: LA029
VffgbgaNELAP CertiTmation #: 460221
REPORT OF LABORATORY ANALYSIS
This report shad not be repraduoed, mwept in fu6,
without the written consent of Pace And Senws, LLC. Page 2 of 14

e
CeArWca!
frlarG1fL'd W rpm
PaceAn2*tiCM SeMkeS, LLC
98W ?Qrmey Ave. Suite l oo
Hurrtersvllle. NC 28078
(T0 W5-9092
SAMPLE ANALYTE COUNT
Project: STOPMMTER-CHARLOTTE
Pace Project No.: 9257873T
Analytes
Lab ID Sarsapte ID
Method Anatysts R ofted Laboratory
92578737001
OUTFALL 14
EPA 200.7 Rev 4.41994
PDT
3
PASI-C
92578737002
OUTFALL 2 11
EPA 200.7 Rev 4.41994
RDT
3
PASI-C
92578737003
OUTFALL 34
EPA 200.7 Rev 4.41994
RDT
3
PASI-C
92578737004
OUTFALL 1.2
SM 522OD-2011
JP1
1
PASI-C
92578737005
OUTFALL 2-2
SM 522OD-2011
JP1
1
PASI-C
92518137006
OUTFALL3.2
SM 5220D-2011
JP1
1
PASI-C
PASI-C = Pace Arrallltical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
TWs re fit stroll ix t W repr=h=c , excepR in fu8,
withcRA the saW 1 oorrsei I of Pace Anaiytwd Sys. L-C. Page 3 of 14

I
eAMOca1°
PaceArta"cal Services, LLC
9800 Kimey Ave. Suite 100
Huntersv91% NC 28078
[phone]
ANALYTICAL RESULTS
Project: STORNMTER-CHARLOTTE
Pace Project No.: 92578737
Sample: OUTFAL.L 14 Lab ID: 92578737001 Collected: 1211012109:00 Received: 12117121 09A8 Matrix: Water
Parameters Results Units Report Lima DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Methad: EPA 200.7 Rev 4A 1994 Preparatim ktdwd: EPA 200.7 Rev 4A 1994
Pace Analytical Services - CharWe
Copper 6.7 ug/L 5.0 1 12/28/21 04:13 01/05122 01:33 Cu
Lead 6-9 ug1L 5.0 1 12128/21 04:13 01/05/22 01:33 Pb
Zinc 145 ugfi. 10.0 1 12/28/210413 01/05/22 01:33 Zn
Date: 01/0512022 03:30 PM
REPORT OF LABORATORY ANALYSIS
This report strap not be reproduced, eaoept in fug.
wdtw3Athe written consent of Pace Analyficd Ser wams. LLC.
Page 4 of 14

tiI ceAna0cal*
ANALYTICAL RESULTS
Project: STORIAMTER-CHARLOTTE
Pace Project No.: 92578737
PaceAna*dcal Servtees, LLC
9800 Kincey Ave. Suite 100
Huntersviiie, NC 28078
[phone]
Sample: OUTFALL 21
Lab 0.' 92578737002
Collected: 12/1012109:30
Received: 12h7121 09:48 MatruG Water
Parameters
Results Units
Report Umit DF
Prepared Analyzed CAS No. Qua!
200.7 MET ICP
Analytical NWtod: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4.41994
Pace Analytical Services -
Charlotte
Copper
1&0 ug/L
5.0 1
122821 04:13 01/05122 01:36 Cu
Lead
7.1 uglL
5.0 1
1228121 04:13 01105122 01:36 Pb
Zinc
166 uglL
10.0 1
12128121 04:13 01/0522 01:36 Zn
Date: 01 /05/2022 03:30 PM
REPORT OF LABORATORY ANALYSIS
This report shag not be reproduced, except infus,
without De written aorrserd of Pace Analybcat Services, LLC.
Page 5 of 14

CcaAnalytica!
lr�
Pace Analytical Services, LLC
9800 Kincey Ave. suite 100
Hunters Me. NC 28078
[phone]
ANALYTICAL RESULTS
Project: STOf UAMTM-CHMLOTM
Pace Project No.: 92578737
Sample: OUTFALL 34 Lab ID: 92578737003 Collected: 12/1021 10:00 Recetwed: 1211721 09-48 Mabbr: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4.41994
Pace Ana"cal Seneiaes - Charlotte
Copper 6.1 ug1L 5.0 1 1228121 04:13 0110522 01:40 Cu
Lead 9.7 ug/L 5.0 1 121=1 04:13 01/0522 01-40 Pb
Zinc 102 ug/L 10.0 1 121=1 04:13 0110522 01*40 Zn
Date: 01 /05/2022 03:30 PM
REPORT OF LABORATORY ANALYSIS
This re fit strati nd be reproduced, except is tub.
wittnt the wi tTerr corrserrt of Paw Analytical services. LLC_
Page 6 of 14

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IcolyAr��a►°
PawAralyficah Services, LLC
98W Kmoey Ave. Suite 100
Hwdemsv!Ue, NC 28078
[phone]
QUALIFIERS
Project STGRMMTER-CHARLOTTE
Pace Project No.: 92578737
DEFINITIONS
DF - Dilution Factor, If reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated Concentration above the adjusted method detection Emit and below the adjusted reporting limit
MDL -Adjusted Method Detection Lints.
PQL - Practical Cluarititation Limit
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenyihydrazine decomposes to and cannot be separated from Azobenzene using Method 8270_ The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Corrttol Sample (ate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Dilf`enence,
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for. but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acryloniitile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Dipherrytamme using Method 8270_ The result
each analyte is a combined corrcertbatiorr. reported for
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary dgMy from the sum of the reported componerd parameters.
Pace Analytical is TNI accredited. Corm d your Pace PM for the current list of accredited analytes.
TNI - The NELAC InshI te.
SAMPLE QUALIFlERS
Sample: 92578737001
(1 ) The samples were received
outside of reams
temperature range. Anat as was completed upon client approval.
Sample: 92578737002
Ill The samples were received
outside of required
terrWdture range- Analysis was completed upon client approval.
Sample: 92578737003
Ill The samples were received
outside of required
glue range. Analysis was completed upon client approval.
Sample: 92578737004
[1l The samples were received
outside of required
temperature range. Analyses was completed upon client approval.
Sample: 92578737005
[1l The samples were received
outside of required
temperature range. Analysis was completed upon cent approval.
Sample: 92578737006
III The samples were received
outside of required
temperature range. Analysis was completed upon charm approval.
REPORT OF LABORATORY ANALYSIS
This report shag not be reprad mck in fug,
Date: 01105f2022 03:30 PM without the writs m aoresent of Pace Analyfad Services, LLC. Page 10 of 14

IWAna0cale
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project STORMWATER-CHARLOTTE
Pace Project No.: 92578737
Pace Analtttical Services, LLC
9800 Mcey Ave. Strife 100
Hunters Me, NC 28078
[phone]
Analytical
Lab 10
Sample to
QC Batch shod
QC Bath AnaVtical Method
Batch
92STM7001
OUTFALL 11
EPA 200.7 Rev 4.41994
668428 EPA 200.7 Rev 4.41994
668647
92578737002
OUTFALL 21
EPA 200.7 Rev 4.41994
668428 EPA 200.7 Rev 4.41994
668647
92578737003
OUTFALL 34
EPA 200.7 Rev 4.41994
668428 EPA 200.7 Rev 4.41994
668647
92678737004 OUTFALL 12
92678737005 OUTFALL 2 2
92578737006 OUTFALL 3-2
SM 522OD-2011 668366 SM 522OD-2011 668388
SM 522OD-2011 668366 SM 522OD-2011 668388
SM 522OD-2011 668366 SM 522OD-2011 668388
REPORT OF LABORATORY ANALYSIS
Th s report shut not be repa& oed, except in f C
Date: 01105/2022 03:30 PM wNund the written conce rt of Page Analytical Sues, LLC. Page 11 of 14

Document Name: Document Revised: November 15, 2021
td)tsms UPM Receipt (SCUR) Page I of 2
rDocument No,; Y Issuing Authority;
Laboratory receiving samples:
Asheville [] Eden Greenwood ❑ Huntersville Ef
Raleigh❑ Mechanicsvige❑ Atlanta[] Kemersville[]
' Client Name:
. i
Project N: WO# : 92578737
Courier: ❑Fed Ea 1 UPS ❑LISPS
El Commercial ❑Pace
❑Client
'1III"II
❑Other: —
'III II 'I'I III
Custody Seal Present? yes
❑ ❑No Seals Intact? ❑Yes
[]NO
92578737
Date/InitlaN Penan Winning Content,: ���.''. r
Packing Material: ❑gobble Wrap ❑Blabbk Bags ❑F2ane
E101her
Thermometer:
❑ IR Gun to; Qwet
❑6tue
Biological Tissue Frozen?
❑yes ❑No []N/A2f
7.T! I Typedlre:
pNi;.N
Correction Factor:
Cooler Temp: Add/Subtraa (Yj
' 1
iemP should be above keening to fi'[
- — Cooler Temp Corrected-l-C).-�--_—.
►-,.--=�--
_ _.._�_.ms
❑Samptel opt elt nnP erltada. Samples on ice, cooling process
USDA Regulated SDII I ❑ WA. agMer>mappe)
Did 1sample s originate In a quarantine zone within the United States: CA, NY, or SC (check
r,tYK QNe maps)?
Dad sarp'es vlglnafe from w
a loretgn sce (IMm eationaay,
Correa Containers Used?
.pars Ores ON. ON/A 6.
-----------------------
Sample Labels Match CDC? W ern e.
Oyes ON' ON/A 9.
Blank
COMMENTS/SAMPLE DISCREPMcy
11.
11 field Data Required? ❑yea ❑No
CLIENT NO7IFIUTION/gE50WNOA LotlD Ofi (zell4tlnera:
Person contacted:
Oate/Ume:
Project Manager SCURF Review:
Prolea Manager SRF Review:
Date:
Date:
Page 12 of 14

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• raWk tOp hW of b041 if PH &*or decM01900" IS
Verified and within the ex*ptance range W presurvation
Rxwgtlarm. VQA, 006M TCW, Oil and Grease, CW/8M (water) PK Wig
"Eott =- hitd b=Is to No
Pro�cR M
Wo#:92578737
PH: T'1H Duo note: 12/29/' 1
CLIENT: 924- cra to
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Page 14 of 14

C Boyer Enterprises East, LLC
a E
January 12, 2022
DEQ Morrisville Regional Office
Attention: DEMLR Stormwater Program
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Subject: STORMWATER SAMPLING RESULTS
ZERO WASTE RECYCLING, INC.
301 DUPREE STREET
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
PERMIT NCG200515
Dear Sir/Madam:
Attached please find the Stormwater Discharge Monitoring Reports (DMR) and analytical
report for the sampling conducted at the above -referenced site. A stormwater sample was
collected from Outfall 001 and 002 on December 12, 2021 and analyzed for lead (Pb),
copper (Cu), zinc, (Zn), and chemical oxygen demand (COD). As indicated on the
attached DMR, all parameters were reported below or within their respective benchmark
values except for CU at Outfall 2, Zn at Outfall 1 & 2, and ZN at outfall 3. Based on these
results, a Tier One Response has been implemented at the facility and the results
documented in the facility's Stormwater Pollution Prevention Plan (SPPP). If you have any
questions or need additional information, please contact me at [phone].
Note: The sample kit was not complete during the monitoring event. A make monitoring
event will be conducted on the first qualified rain event.
Sincerely,
BOYER ENTERPRISES EAST, LLC
Paul W. Spangenberg
EH&S Compliance Director
Attachments: Cover Letter
Stormwater Discharge Monitoring Reports
Laboratory Report
127 Red Hill Church Road, Dunn, North Carolina, 28334

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG200000
Scrap Metal
Click here for instructions
Complete, sign scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mad the original, signed had copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage Na. NCG20 0515
Person Collecting Samples Chris Gosselin
Facility Name: Zero Waste ReryckS Inc.
Laboratory Name: Pace
Facility County: Mecklenburg
Laboratory Cert. No.: 12
Discharge during this period:0
Yes
❑ No (if no. slap to signature and date)
Has your facility implemented mandatoryTra response actions
If so, which Tier (I, 11, or III)?
this sample period for any benchmark exceedances? Q Yes ❑ No
AcopyofthisDMRhasbeenuploadedefectranicaNyvfahttps://edocs.deg,nc.gov/Forms/SW-DMR
Date uploaded: 1/12122
DYes [I No
Analytical Monitoring Requirements for Outtalk vA& industrial Activities —Bendauarks in (Red)
Parameter
Parameter
Outfall01
Outfall02
Outiall03
Outfall
Outfall
Code
N/A
Receiving Stream (lass
C
C
C
N/A
Date Sample Collected MM/DD/YYYY
12/10/21
12/10/21
12/10121
46529
24-Hour Rainfall in inches
0.08
0.08
0.08
C0530
TSS in mg/L (100 or 50*)
00340
Chemical Oxygen Demand (120)
108
69.6
173
00552
Non -Polar Oil & Crease in ng/L (15)
Copper, total recoverable in mg/L
01119
0.OD67
0.018
0-MI
0.010 FW 0,005S
Lam• total recoverable (as Pb) in
OSOS1
mg/L 0.075 FW 0.220 S
0.0069
OA071
0.0097
Zinc, total recoverable in mg/L (0.126
C0034
0.145
0.156
0.102
FW 0.095 SW
Additional parameters for outtalk in drainage areas that use>55 gallons per month of new hydraulic oil on average
Estimated New Motor/Hydrauriic OR
NCOIL
Osage in gal/month
* Outface to Outstanding Resource Waters (ORWL ffgh Quality Waters (11QOr),T"xt Waters (Tr) and Primary Nursery Areas (PNA)
have a bendroarkTSS fvnit of 5o mg/L. AN otbrr waew dataifiraiaw havea bmdwak of 100 mg/L
FW (Freshwater) SW (Saltwater)
i Notes (optional): The sample k0 was not cornplete. O&G and TSS were not monitored. We will conduct make monitoring on the neM rain event.
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, inclgO.Og thevfi�sibility of fines and imprisonment for knowing violations.'
1/12/ 22
PermitteeorDelegated Authorized Individual Date
[e-mail] Phone Number (336) 4650453

-,PaceAnalytical e
vwpacrl O
Pace Arralyocal Services, LLC
98001Gncey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
January 05, 2022
Chris McRae
Zero Waste Recycling, LLC
301 Dupree Street
Charlotte, NC 28208
RE: Project: STORMWATER-CHARLOTTE
Pace Project No.: 92578737
Dear Chris McRae:
Enclosed are the analytical results for sample(s) received by the laboratory on December 17, 2021. The results relate only
to the samples included in this report Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Endosures
REPORT OF LABORATORY ANALYSIS
ills report stem tact be rearodurm, errspt m trill,
wfthoutthecarmen.., ar PweAr9dytical Services,LLC.
Page 1 of 14

Pace Analytical Servkes, LLC
98001GnceyAve. Suite too
HuMemW le. NC 28078
[phone]
Project STORMWATER-CHARLOTTE
Pace Project No.: 92578733
Pace Analytical Services CharkA to
South Carolina Laboratory ID: 99M
9800 Kincey Ave. Ste 100. Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #:12
South Carolina Laboratory IM 99006
CERTIFICATIONS
South Carolina Certification #: 99=001
South Carolina Drinking Water Cert. #. 99M003
Flodda/NELAP Certification it E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water#: LA029
Vogb*AIELAP Cersification #: 460221
REPORT OF LABORATORY ANALYSIS
This repot sha8 rwt be mpuhmed. mwept in M.
without the written = tmnt of Paw Analytical Services, I.M. Page 2 of 14

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ANALYTICAL RESULTS
Project: STORMWATER-CHARLOTTE
Pace Project No.: 92578737
Pace Analytical Servkes, LLC
980 [0m:eyAve. Suite 100
Huntersvifle, NC 28078
[phone]
Sample: OUTFALL 21 Lab ID: 92578737002 Collected: 1211021 09:30 Rece➢ved: 12/17/21 09-48 Mahbc Water
Parameters Results un is Report Limit DF Prepared Analyzed CAS No. Qua!
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4 41994
Pace Analytical Services - Charlotte
Copper 18.0 ug/L 5.0 1 1212812104:13 0110522 01:36 Cu
Lead 7.1 ug/L 5.0 1 121282104.13 01It)5/22 01:36 Pb
Zinc 156 uglL 10.0 1 1228121 04:13 0110522 01:36 Zn
Date: 01/05/2022 03:30 PM
REPORT OF LABORATORY ANALYSIS
nft repast shag not be , except in fits,
wMxPA the wnfben co mad of PaceAm4ftal Services, U.C.
Page 5 of 14

eAnalytic�!°
PaceAne"cal Services, LLC
9800 Krncey Ave. Suite 100
Huntersviile, NC 28078
[phone]
ANALYTICAL RESULTS
Project: STORMWATER-CHARLOTTE
Pace Project No.: 92578731
Sample: OUTFALL 3-1 Lab ID: 92578737003 Collected: 12/10121 10:00 Received: 12/1712109:48 Matrix Water
Parameters Results Units Report limit DF Prepared Analyzed CAS No. Quaff
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4.41994
Pace Analytical Services - Charlotte
Copper 6.1 ug1L 5.0 1 12128/21 04:13 01/05/22 01:40 Cu
Lead 9.7 U91L 5.0 1 12/28/21 04:13 01/05/22 01:40 Pb
Zinc 102 ug1L 10.0 1 1212812104-13 01/05►22 01A0 Zn
Date: 01/05/2022 03:30 PM
REPORT OF LABORATORY ANALYSIS
This report slud rat be reproduced, except in fug,
rwfflxn t the written c w of Pace Armiy =W Services. lLC_
Page 6 of 14

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ceAna�ytical@WNW
Pace Ana"cal Services, LLC
9800 IGnoey Ave. Suite 100
HantersviUe, NC 28078
[phone]
ANALYTICAL RESULTS
Project:: STORMWATER-CwARLOTrE
Pace Project No.: 92578737
Sample: OUTFALL 2a Lab ID: 92678737005 Collected: 1211012109.30 Received: 12/17/21 09:48 Matrix: Water
Parameters Results Unfits Report Limit DF Prepared Analyzed CAS No. Qua]
52200 COD Analytical Method: SM 522OD-2011 Preparation Method: SM 522OD-2011
Pace Analytical Sennoes - Charta#te
Chemical Oxygen Demand 69A nM#L 25.0 1 1212412101:33 1212412104:39 cod
Date: 01/05/2022 03:30 PM
REPORT OF LABORATORY ANALYSIS
nft report stw not be reproduced. except in fu8.
without ttre wnftn consent of Pace Analytical Senlcesr lJ c-
Page 8 of 14

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�eAnalytical vampcfts cm,
QUALIFIERS
Project STORMWATER-CHARLOTTE
Pace Project No.: 92578737
DEFINITIONS
DF - Dilution Factor, If reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting Omit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL -Adjusted Method Detection Limit
PQL - Practical Quanlitation Limit
Pace Analyt W Services, LLC
98W iGnceyAve. Suite 100
Huntersville, NC 28078
[phone]
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a spedliic matrix.
S - Surrogate
1.2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Medmd 8270. The result for each anayte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate far 2 Chloroe#*Anyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Ac rylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Dlphenylamine using Method 8270. The result reported for
each anayte is a combined concentration.
Reported results are not rounded uniii the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the cunwd fist of accredited anatytes.
TNI - The NEIAC Institute.
SAMPLE QUALIFIERS
Sample: 92578737001
[1 ] The samples were received outside of required ternperaature range. Analysis was comp
leted upon client approval.
Sample: 926787370132
[1 ] The samples were received outside of required temperature range. Analysis was comp
leted pleted upon client approval.
Sample: 92578737003
[1 ] The samples were received outside of required temperature range. Analysis was eampkRed upon client approval.
Sample: 92578737004
[1] The samples were received outside of required temperature range. Analysis was completed upon client approval.
Sample: 92578737005
[1 ] The samples were received outside of required temperature range. Analysis was completed upon client approval.
Sample: 92578737006
[1 ] The samples were received outside of required temperature range. Analysis was completed upon dient approval.
REPORT OF LABORATORY ANALYSIS
This report slim] riat We repro kiced, erceept in fill].
Date: 01/05/2022 03:30 PM without the wMien consent of Paw Analy ed Services, LLC. Page 10 of 14

_ ceAwlytical
x�x{axd�bsamar
PaceAna"ca! Services, LLC
9800 Kmcey Ave. Suite 100
Hunters0e, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project STORMMTER-CHARLOITE
Pace Project No.: 92578737
Analytical
Lab 10 Sample ID QC Batch Method QC Uatch Ana
tyt%a! Method Batch
92678737001
92678737002
925787337003
92678737004
92678737006
92578737006
OUTFALL 1-1
OUTFALL 2-1
OUTFALL 34
OUTFALL 1 2
OUTFALL 2 2
OUTFALL 3-2
Date: 01/05/2022 03:30 PM
EPA 200.7 Rev 4.41994 668428
EPA 200.7 Rev 4.41994 668428
EPA 200.7 Rev 4.419" 668428
SM 522OD-2011 668366
SM 522OD-2011 668366
SM 522OD-2011 668366
REPORT OF LABORATORY ANALYSIS
This repot shad rent be reproduceci, except in fill,
widmut the wften c�a lserrt of Pace Anaiykd Sues. LLC_
EPA 200.7 Rev 4.419N
668647
EPA 200.7 Rev 4.41994
668647
EPA 200.7 Rev 4.41994
668647
SM 5224D-2011
668388
SM 522OD-2011
668388
SM 522OD-2011
668388
Page 11 of 14

Laboratory receiving samples:
Asheville El EdenO Greenwood Huntersville Q• Raleigh[] Mechanicsville[] Atlanta
❑ Kernersville❑
Client Name: ..• - ' (� j�
Project R: UV7T : 92578737
Q
Cavrier. —'
—OF Ea QUPS USPS - QCOent "I'�II II'I'I'll
❑ Commercial []Pace QOther
Custody Seal Present? ❑Yes ONO s92578737
seals Ayes ❑No,/
Datellnitlahleenan Examining Contentu•/1.+•, V.,
Parking Material: ❑gobble lNra �
p ❑Bu66k sags❑dapne 0other el0foglcai Tissue Frozen?
Thermometer: ❑ ❑K/A
, []Yes No ❑' IRwnID: - t ❑wee Qekm ❑Ram
Typed la: _
_ Correction Factor:
Cooler Temp: _ Add/Subtract ('C)
Temp should he above freezing to 6'C
•—Eooler-Temp Corrected�i'C):--�.---.� -ram_ _ Y ❑Samples out of temp criteria. Samples on ice, cooling process
USDA Regulated 500 (D N/A, water sample)Otjrtlr'-
Did samples originate in a quarantine zone within the United States: NY CA, , or SC Icheck maps)? Oki sa,gJzs arigmste horn a loirien source
QYes ❑NO
Correct Containers Used?
01es
ONIA ._. '
/A 6.
-Pace Containers Used?
-❑Yn
No
❑N/A
Containers intact?
❑1'ts
CINa
N/A 7,
DtSmlved analyst: S mples Field Fhered7
of
L7Na
'
❑N/A
Sample Labels Match COC?l7yxs
_
g.
i]Na
❑N/A 9,
EE.
COMMENTS/LWPLE DISCREPANCY -
fieldOataReqvlred? Dyes ❑Np
CLIENT NDTIFICATION/RESOlU00N LO[IO Of spQl [prl[alOCTS;
Persona meted: .
Project Manager SCURF Revlew:
Project Manager SRF Review
Date/ffine:
Date;
Date,
Page 12 of 14

�t 1 "Cumertt R+eAsed; November 15. 2021
4 Sam le condithm Upon Receipt iSCUR Palo 2 of 2
.... �acaAna�ytic�l . , o�:n�tt isstrrr�Q Authartty:
i*AR-S-Q-itea�. Pace Carai#nas 4u�$tit Me-- - _.
+Check n►atk top half of box if pii and/or dedg cAnattlm is
verified and within the acceptance grange for preservation
sanwpies.
fuePtions: VOA, Colifarm,TOC, 011 and Grease, 0RO/8013 (water) 00C, LWO
"Oottoorn Wof box is to ft qwOwal botdes
IFr i jW. !'
IWO#:926787a(
P"; TO Que Date;
CLIFAT: 92— ��Wasl,s
PH AdJustment
Lqg for Preserved Samples
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1� of �
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adjusted
Aft of Presaraa�ve
added
iat A
n41q: vrhimunr Fnera is a oinrepanq ariarmag worth caragna c=p &r= samples, a copy I# tnK rwrn will tM ttat to the North carotlna DRINK certtticetlon Me (I.e.
Out of Itft *404 t pr "Vativo: out OumP, iorekR ca"84 r;,
Page 13 of 14

1 CHAIN -OF -CUSTODY J Analytical 'Request Document
The Chaffin-of-Cuslady % a IWAt DOCUMENT. AU relt:vaul *fields must be rampleted a=rately.
SaotlanA
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$=UanR eta.pr►oeyabs.Corrsthubtsdpss-stansa rent i
SaotlanC
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A AtlerRrlrt
3tat s al. Copp Ter Name
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SAMPLE 1D
4na Charaator per bax.
4b
WZ, "I, )
Sample tills roust be valqua
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