NCG060412_Monitoring Report_20220725

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NCDEQ Division of Energy, Mineral and Land Resources s°'tea
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Stormwater Discharge Monitoring Report (DMR) Form for NCG060000Q c� °3,o-7s°
Food and Kindred ®Y
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Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR Upload within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appro
Certificate of Coverage No. NCG06 0412
Person Collecting Samples: Madison Shoemaker
Facility Name:Amazon.com Services LLC - CLT9
Laboratory Name: Eurofins Test America Savannah
Facility County: Mecklenburg
Laboratory Cert. No.:269
Discharge during this period: ❑✓ Yes ❑ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? El Yes ❑ No
If so, which Tier (I, II, or III)? Tier II
A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR 0 Yes ❑ No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Parameter
Outfall001
Outfall002
Outfall
Outfall
Outfall
Code
N/A
Receiving Stream Class
WS-IV;CA
WS-IV;CA
N/A
Date Sample Collected MM/DD/YYYY
6/29/2022
6/29/2022
46529
24-Hour Rainfall in inches
0.1
0.1
C0530
TSS in mg/L ;_ `
3.3
3.9N
pH in standard units _
00400
6.8 — 8.5 SW)
7.72
10.97
Fecal Coliform per 100 ml of
31616
freshwater (if required)
N/A
N/A
Enterococci per 100 ml of saltwater
61211
(if required) �_7;,.;7,
N/A
N/A
Chemical Oxygen Demand in mg/L
00340
<5.0
<5.0
Additional parameters for outfalls in drainage areas that use >SS gallons per month of new hydraulic oil on average
Estimated New Motor/Hydraulic Oil
NCOIL
Usage in gal/month
N/A
N/A
00552
Non -Polar Oil & Grease in mg/L
N/A
N/A
Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of - All other water classifications have a benchmark of
'.'.r (Freshwater) .! (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee or Delegated Authorized Individual
[e-mail]
Email Address
Date
[phone]
Phone Number

urofins
Environment Testing
America
ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-217706-1
Client Project/Site: Storm Water - Amazon Warehouses CLT9
For:
ERM-West
1920 Main Street
Suite 300
Irvine, California 92614
Attn: Doug J Wade
Jq"& vu Ci"ros
Authorized for release by:
711812022 9:11:24 AM
Roxanne Cisneros, Senior Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
0

Definitions/Glossary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT9
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
❑ Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Job ID: 680-217706-1 --
Eurofins Savannah
Page 2 of 12 7/18/2022

Sample Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT9
Lab Sample ID Client Sample ID
680-217706-1 CLT9 Sample_Point 01_20220629
680-217706-2 CLT9_Sample_Point 02 20220629
Matrix
Water
Water
Collected Received
06/29/22 16:27 07/01 /22 11:00
06/29/22 16:12 07/01 /22 11:00
Job ID: 680-217706-1
Page 3 of 12
Eurofins Sad OWP-2

Case Narrative
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT9
Job ID: 680-217706-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-217706-1
Comments
No additional comments.
Job ID: 680-217706-1
Receipt
The samples were received on 7/1/2022 11:00 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 2.11 C.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins Savannah
Page 4 of 12 7/18/2022

Client Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT9
Job ID: 680-217706-1
Client Sample ID: CLT9_Sample_Point_01_20220629 Lab Sample ID: 680-217706-1
Date Collected: 06/29/22 16:27 Matrix: Water
Date Received: 07/01/22 11:00
General Chemistry
Analyte
Result Qualifier
RL
Total Suspended Solids
3.3
2.5
Chemical Oxygen Demand
<5.0
10
Client Sample ID: CLT9_ Sample_Point_02_20220629
Date Collected: 06/29/22 16:12
Date Received: 07/01/22 11:00
General Chemistry
Analyte
Result Qualifier
RL
Total Suspended Solids
3.9
2.5
Chemical Oxygen Demand
<5.0
10
MDL
Unit
D Prepared Analyzed Dil Fac
2.5
mg/L
07/05/2215:02 1
5.0
mg/L
07/16/2211:16 1
Lab Sample ID: 680-217706-2
Matrix: Water
MDL
Unit
D Prepared Analyzed Dil Fac
2.5
mg/L
07/05/2215:02 1
5.0
mg/L
07/16/2211:16 1
Eurofins Savannah
Page 5 of 12 7/18/2022

QC Sample Results
Client: ERM-West Job ID: 680-217706-1
Project/Site: Storm Water - Amazon Warehouses CLT9
Method: 254OD-2015 - Total Suspended Solids (Dried at 103-105°C)
FLab Sample ID: MB 680-729136/1 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729136
i Analyte
Total Suspended Solids
Lab Sample ID: LCS 680-729136/2
Matrix: Water
Analysis Batch: 729136
Analyte
Total Suspended Solids
[Lab Sample ID: LCSD 680-72913613
Matrix: Water
Analysis Batch: 729136
Analyte
Total Suspended Solids
MB MB
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
<2.5 2.5 2.5 mg/L 07/05/2215:02 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
951 908 mg/L 95 80 -120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD
Added Result Qualifier Unit
951 932 mg/L
Method: 5220D-2011 - Chemical Oxygen Demand
LLab Sample ID: MB 680-731009/3
Matrix: Water
Analysis Batch: 731009
MB MB
Analyte Result Qualifier
LChemical Oxygen Demand <5.0
Lab Sample ID: LCS 680-73100914
Matrix: Water
Analysis Batch: 731009
Spike
Analyte Added
Chemical Oxygen Demand 50.0
%Rec RPD
D %Rec Limits RPD Limit
98 80 - 220 3 25
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
10 5.0 mg/L 07/16/2211:16 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS
Result Qualifier Unit
45.9 mg/L
%Rec
D %Rec Limits
92 90 -110
Eurofins Savannah
Page 6 of 12 7/18/2022

QC Association Summary
Client: ERM-West Job ID: 680-217706-1
Project/Site: Storm Water - Amazon Warehouses CLT9
General Chem
Analysis Batch: 729136
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-217706-1
CLT9_Sample_Point_01_20220629
Total/NA
Water
2540D-2015
680-217706-2
CLT9_Sample_Point _02_20220629
Total/NA
Water
2540D-2015
MB 680-729136/1
Method Blank
Total/NA
Water
2540D-2015
LCS 680-729136/2
Lab Control Sample
Total/NA
Water
2540D-2015
LCSD 680-729136/3
Lab Control Sample Dup
Total/NA
Water
2540D-2015
Analysis Batch: 731009
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-217706-1
CLT9_Sample_Point _01_20220629
Total/NA
Water
5220D-2011
680-217706-2
CLT9_Sample_Point_02_20220629
Total/NA
Water
5220D-2011
MB 680-731009/3
Method Blank
Total/NA
Water
5220D-2011
LCS 680-731009/4
Lab Control Sample
Total/NA
Water
5220D-2011
Eurofins Savannah
Page 7 of 12 7/18/2022

Lab Chronicle
Client: ERM-West Job ID: 680-217706-1
Project/Site: Storm Water - Amazon Warehouses CLT9
Client Sample ID: CLT9_Sample_Point_01_20220629 Lab Sample ID: 680-217706-1
Date Collected: 06/29/22 16:27 Matrix: Water
Date Received: 07/01/22 11:00
Batch
Batch
Prep Type
Type
Method
Total/NA
Analysis
2540D 2015
Instrument
ID: NOEQUIP
Total/NA
Analysis
5220D-2011
L-
Instrument
ID: SPC7
Dil Initial
Final
Batch
Prepared
Run Factor Amount
Amount
Number
or Analyzed Analyst Lab
1 1000 mL
1000 mL
729136
07/05/22 15:02 PG TAL SAV
1 2 mL
2 mL
731009
07/16/22 11:16 ALG TAL SAV
Client Sample ID: CLT9_Sample_Point_02_20220629
Date Collected: 06/29/22 16:12
Date Received: 07/01/22 11:00
r-
Lab Sample ID: 680-217706-2
Matrix: Water
Batch
Batch
Dil Initial
Final
Batch
Prepared
Prep Type
Type
Method
Run Factor Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA
Analysis
2540D-2015
1 1000 mL
1000 mL
729136
07/05/22 15:02 PG TAL SAV
Instrument
ID: NOEQUIP
i
Total/NA
Analysis
5220D-2011
1 2 mL
2 mL
731009
07/16/22 11:16 ALG TAL SAV
Instrument ID: SPC7
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Page 8 of 12
Eurofins Savannah
7/18/2022

Accreditation/Certification Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT9
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program
North Carolina (WW/SW) State
Job ID: 680-217706-1
Identification Number Expiration Date
269 12-31-22
Eurofins Savannah
Page 9 of 12 7/18/2022

Method Summary
Client: ERM-West
Project/Site: Storm Water -Amazon Warehouses CLT9
Job ID: 680-217706-1
Method Method Description Protocol Laboratory
254OD-2015 Total Suspended Solids (Dried at 103-105°C) SM TAL SAV
5220D-2011 Chemical Oxygen Demand SM TAL SAV
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 10 of 12 7/ 18/2022

Address
Chain of Custody Record
C..'Llki0 Ak 1 `� � Reaulatory Proaram: I-1 nw f l NRnFs n RrRe M nrhpr-
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585080 acurofins
Environment Testing p
TestArnerica
TAL-8210
Client Contact
Project Manager: S 4h rN
Site Contact: tk ph % &f Kaz W
Date. Et Z.Z.--
COC No
Company Name { A - 6 j Q S }-
Tel/Email• ru-• .0 n it 1L �1 r �; �N''°
Lab Contact:
Carrier.
of COCs
Address , ct l n '-�u (
Analysis Turnaround Time
^
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m
CL
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two
m
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a.Sample
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Sampler
City/State/zip t v V 2AP
❑ CALENDAR DAYS ❑ WORiGNG DAYS
For Lab Use Only:
Walk-in Client:
Lab Sampling
Phone — V b
TAT if different from Below
❑ 2 weeks
❑ 1 week
❑ 2 days
❑ 1day
Fax
Project Name
1 %. v�i V - Mr. Jn v�
Site Ci., 9
Job / SDG No
PO# D I
Sample Identrfrcation
Sample
Date
Sample
Sample Type
Time drab)
Matrix
# of
cons
Specific Notes
L TC1-- S a m?-C, k b wl t_ 01-
�. 9- � _?Cln -u.--avak2
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680-217706 Chain of Custody
�f'i�'�a#ipi�. us¢+d: I I-] = �W 'k! >Q
ter
Possible Hazard Identification:
Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the
Comments Section d the lab is to dispose of the sample
Sample Disposal (A fee maybe assessed if samples are retain
❑ Return to Client ❑Disposal by Lab ❑Archive for
d longer than 1 month)
Months
❑ Non -Hazard ❑ Flammable ❑Skin Irritant ❑Poison 6 El unknown
Special Instructions/QC Requirements & Comments:
Custody Seals Intact: ❑ Yes No
Custody Seal No Cooler Temp (C) O s d Corr'
Therm ID No
Relinquished by
V�k4va L��VLA
Company
D
e/T• a
'�"k ILI
Rece d y ;
i IjAAAA
Company
DN
Q AZ 01a
Reli ui hed b •
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Company
D e l e
O
Received by
Company
D
elmquished by
Company
Da /Ti
Received in Laboratory by
Company
Date/Time

Cl
Login Sample Receipt Checklist
Client: ERM-West
Login Number: 217706
List Number: 1
Creator: Padayao, Abigail
Question Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Job Number: 680-217706-1
List Source: Eurofins Savannah
Eurofins Savannah
Page 12 of 12
7/ 18/2022