NCG060412_Monitoring Report_20220413

U,Ti -
fy)vacCs Vt k �,e_ NCDEQ Division of Energy, Mineral and Land Resources
rmwater Discharge Monitoring Report (DMR) Form for NCG060000
Food and Kindred
Click here for instructions
complete, sign, scan and submit the DMR via the Stormwater NPDFS Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DFMLR Regional 0i lice.
Certificate of Coverage No. NCG06 0412
Person Collecting Samples: Madison Shoemaker
Facility Name: Amazon.com Services LLC - CLT9
Laboratory Name: Eurofins TestAmerica
Facility County: Mecklenburg
Laboratory Cert. No.: 269
Discharge during this period: [EYes ❑ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑X Yes ❑ No
If so, which Tier (I, II, or III)? Tier I
A copy of this DMR has been uploaded electronically via https://edocs,deg.nc.gov/Forms/SW-DMR ❑ Yes []No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Code
Parameter
Outfall 002
Outfall 001
Outfall
Outfall
Outfall
N/A
Receiving Stream Class
WS-IV
N/A
Date Sample Collected MM/DD/YYYY
02/23/2022
o
46529
24-Hour Rainfall in inches
0.48
u
C0530
TSS in mg/L (100 or 50*)
39
—
o
�'
CD
00400
pH in standard units (6.0— 9.0 FW,
0 E
si p
11.05
0 M
31616
Fecal Coliform per 100 ml of
N
o.N�
freshwater (if required)
N/A
m
A
61211
Enterococci per 100 ml of saltwater
a o�
(if required)
N/A
E
Chemical Oxygen Demand in mg/L
'^ �
00340
12
u
0 0
z .n
Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic
oil on average
NCOIL
Estimated New Motor/Hydraulic Oil
Usage in gal/month
N/A
00552
Non -Polar Oil & Grease in mg/L
N/A
—• ••�••� •� .,...5­a noavurce waters tvrcvv), nlgn uuauty waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of All other water classifications have a benchmark of
(Freshwater) (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, including tipjpofs`sibility of fines and imprisonment for knowing violations."
A A
n
Signature of PermittA or Delegated Authorized individual
[e-mail]
Email Address
Date
214-326-3426
Phone Number

eurofins
0
Environment Testing
America
ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-211739-1
Client Project/Site: Storm Water - Amazon Warehouses CLT9
ERM-West
1920 Main Street
Suite 300
Irvine, California 92614
Attn: Doug J Wade
Authorized for release by.-
3/8/2022 12:05:37 PM
Roxanne Cisneros, Senior Project Manager
[phone]
roxanne.cisneros@a Eurofinset.com
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The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNl requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval frorn the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Definitions/Glossary Client: ERM-West Job ID: 680-211739-1
Project/Site: Storm Water - Amazon Warehouses CLT9
Abbreviation These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah

Client: ERM-West Sample SummaryJob ID: 680-211739-1
Project/Site: Storm Water - Amazon Warehouses CLT9
Lab Sample ID Client Sample ID Matrix Collected Received
680-211739-1 CLT9_Sample_Point 02_20222302 Water 02/23/2211.07 02/24/2211:00

Case Narrative
Client: ERM-West Job ID: 680-211739-1
Project/Site: Storm Water- Amazon Warehouses CLT9
Job ID: 680-211739-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-211739-1
Comments
No additional comments.
Receipt
The sample was received on 2/24/2022 11:00 AM. Unless otherwise noted below, the sample arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 1.00 C.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
^ -f 10 Eurofins Savannah
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Client: ERM-West Client Sample Results
Project/Site: Storm Water - Amazon Warehouses CLT9
Client Sample ID: CLT9_Sample_Point 02 20222302
Date Collected: 02/23/22 11:07
Date Received: 02/24/22 11:00
[General Chemistry
Analyte Result Qualifier RL
Chemical Oxygen Demand 1;A 10
Total Suspended Solids 8.3
Job ID: 680-211739-1
Lab Sample ID: 680-211739-1
Matrix: Water
MDL Unit D Prepared Analyzed Dil Fac77
5,0 mg/L 03/04/2210:35 1
8.3 mg/L 02/24/2218:54 1
Eurofins Savannah

QC Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT9
Method: 5220D-2011 - Chemical Oxygen Demand
Lab Sample ID: MB 680-709272/3
Matrix: Water
Analysis Batch: 709272
MB MB
Analyte Result Qualifier
Chemical Oxygen Demand <5.0
Lab Sample ID: LCS 680-709272/4
Matrix: Water
Analysis Batch: 709272
Spike
Analyte Added
Chemical Oxygen Demand 50.0
Lab Sample ID: 680-211739-1 MS
Matrix: Water
Analysis Batch: 709272
Analyte
Sample
Result
Sample
Qualifier
Spike
Added
Chemical Oxygen Demand
12
50.0
Lab Sample ID: 680-211739-1
MSD
Matrix: Water
Analysis Batch: 709272
Sample
Sample
Spike
Analyte
Result
Qualifier
Added
Chemical Oxygen Demand
12
50.o
Job ID: 680-211739-1
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
10 5.0 mg/L 03/04/2210:35 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS %Rec.
Result Qualifier Unit D %Rec Limits
49.9 mg/L 100 90 -110
Client Sample ID: CLT9 Sample_Point 02_20222302
Prep Type: Total/NA
MS MS %Rec.
Result Qualifier Unit D %Rec Limits
63.6 mg/L 102 90 - 110
Client Sample ID: CLT9 Sample_Point_02_20222302
Prep Type: Total/NA
MSD MSD %Rec. RPD
Result Qualifier Unit D %Rec Limits RPD Limit
61.0 mg/L 97 90-110 4 3D
ivletnoa: JM 154UL7 - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-708293/1
Matrix: Water
Client Sample ID: Method Blank
Analysis Batch: 708293
Prep Type: Total/NA
MB
MB
Analyte Result
Qualifier RL
MDL Unit D Prepared Analyzed Dil Fac
Total Suspended Solids <2.5
2.5
2.5 mg/L 02/24/22 18:54 1
Lab Sample ID: LCS 680-708293/2
Client Sample ID: Lab Control Sample
Matrix: Water
Analysis Batch: 708293
Prep Type: Total/NA
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Rec Limits
Total Suspended Solids
951
794 mg/L 83 80-120
Lab Sample ID: LCSD 680-708293/3
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Analysis Batch: 708293
Prep Type: Total/NA
Analyte
Spike
LCSD LCSD %Rec. RPD
Added
Result Qualifier Unit D %Rec Limits RPD Limit
Total Suspended Solids
951
810 mg/L 85 80-120 2 25
Eurofins Savannah

QG Associc1Aion Smrfi arrjf
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT9
General Chemistry
Analysis Batch: 708293
Job ID: 630-211739-1
Lab Sample ID
680-211739-1
Client Sample ID
Prep Type
Matrix
Method Prep Batch
CLT9_Sample_Point 02_20222302
Total/NA
Water
SM 2540D
MB 680-708293/1
Method Blank
Total/NA
Water
SM 2540D
LCS 680-708293/2
Lab Control Sample
Total/NA
Water
SM 2540D
LCSD 680-708293/3
Lab Control Sample Dup
Total/NA
Water
SM 2540D
Analysis Batch: 709272
Lab Sample ID
680-211739-1
Client Sample ID
Prep Type
Matrix
Method Prep Batch
CLT9 Sample_ Point 02_20222302
Total/NA
Water
5220D-2011
MB 680-709272/3
Method Blank
Total/NA
Water
5220D-2011
LCS 680-709272/4
Lab Control Sample
Total/NA
Water
5220D-2011
680-211739-1 MS
CLT9 Sample —Point 02_20222302
Total/NA
Water
5220D-2011
680-211739-1 MSD
CLT9_Sample_Point 02_20222302
Total/NA
Water
5220D-2011
Eurofins Savannah
D- -- 7 -f 4 1) 11/O/7(101)

Lab Chronicle
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT9
Client Sample ID: CLT9_Sample_Point 02_20222302
Date Collected: 02/23/22 11:07
Date Received: 02/24/22 11:00
Batch Batch
Prep Type Type Method Run
Total/NA Analysis 5220D-2011
Instrument ID: SPC7
Total/NA Analysis SM 2540D
Instrument ID: NOEQUIP
Dil Initial
Factor Amount
1 2 mL
Job ID: 680-211739-1
Lab Sample ID: 680-211739-1
Matrix: Water
Final Batch Prepared
Amount Number or Analyzed Analyst Lab
2 mL 709272 03/04/22 10:35 ALG TAL SAV
1 300 mL 1000 mL 708293 02/24/22 18:54 PG
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TAL SAV
Eurofins Savannah
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Accreditation/Certification Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT9
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program
North Carolina (WW/SW) State
Job ID: 680-211739-1
Identification Number Expiration Date
269 12-31-22
Eurofins Savannah
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Client: ERM-West Method Summary Job ID: 680-211739-1
Project/Site: Storm Water- Amazon Warehouses CLT9
Method
Method Description
Protocol
Laboratory
5220D-2011
Chemical Oxygen Demand
SM
TAL SAV
SM 2540D
Solids, Total Suspended (TSS)
SM
TAL SAV
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah

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Login Sample Receipt Checklist
Client: ERM-West Job Number: 680-211739-1
Login Number: 211739
List Number: 1
Creator: Padayao, Abigail
Question
List Source: Eurofins Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, inci. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4'�.
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins Savannah