NCG060412_Monitoring Report_20220120

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG06000 <
Food and Kindred s:om y�
Click here for instructions
02'F�
Complete, sign, scan and submit the DMR via the
Permit
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the
Certificate of Coverage No. NCG06 0412
Person Collecting Samples: Madison Shoemaker
Facility Name: Amazonoom Services LLC- CLT9
Laboratory Name: Eurofins TestAmerica
Facility County: Mecklenburg -
Laboratory Cert. No.:269
Discharge during this period:0
Yes
No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? [Dyes MNo
If so, which Tier (I, II, or III)? Tier 1
A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR CYes ❑ No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Parameter
Outfall001
Outfall002
Outfall
Outfall
Outfall
Code
N/A
Receiving Stream Class
WS-IV
WS-IV
N/A
Date Sample Collected MM/DD/YYYY
12118/2021
12/18/2021
46529
24-Hour Rainfall in inches
0.42
0.42
C0530
TSS in mg/L (100 or 50*)
35
160
pH in standard units (6.0-9.0 FW,
00400
8 82
8.83
6.8 — 8.S S
00556
1 Oil & Grease in mg/L (30)
N/A
N/A
Fecal Coliform per 100 ml of
31616
freshwater (if required) (1000)
N/A
NIA
Enterococci per 100 ml of saltwater
61211
(if required 500)
N/A
N/A
Chemical Oxygen Demand in mg/L
00340
(120)
1 7
14
Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average
Estimated New Motor/Hydraulic Oil
NCOIL
Usage in gal/month
N/A
N/A
00552.
1 Non -Polar Oil & Grease in mg/L (15)
1 N/A
I N/A
* Outfalls to Outstanding Resource Waters (ORIN), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L All other water classifications have a benchmark of 100 mg/L
FW (Freshwater) SW (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee or Delegated Authorized Individual
[e-mail]
Email Address
l l $ ZZ
Date
[phone]
Phone Number

urofins
Environment Testing
America
ANALYTICAL REPORT 1%
Eurofins Southeast, Savannah ri 0 y �
5102 LaRoche Avenueoz
Savannah, GA 31404
Tel: [phone] msVP
Laboratory Job ID: 680-209202-1�
Laboratory SDG:3620 Reeves Ridge Drive, Charlotte, NC
28214
Client Project/Site: Storm Water - Amazon Warehouses CLT9
For:
ERM-West
1920 Main Street
Suite 300
Irvine, California 92614
Attn: Doug J Wade
Roxa�vtt. �S�ueras
Authorized for release by:
11412022 3:39:38 PM
Roxanne Cisneros, Senior Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the samplets) as received by the laboratory.

Definitions/Glossary
Client: ERM-West Job ID: 680-209202-1
Project/Site: Storm Water - Amazon Warehouses CLT9 SDG: 3620 Reeves Ridge Drive, Charlotte, NC 28214
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
v Listed underthe "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
oil Fee Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis ofthe sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOO Limit of Quantitation (DOD/DOE)
MCL EPA recommended"Maximum Contaminant Lever'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative/Absent
Pas Positive / Present
Pal. Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEO Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Southeast, Savannah
Page 2 of 13 1/4/2022

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Case Narrative
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT9
Job ID: 680-209202-1
Laboratory: EuroFlns Southeast, Savannah
Narrative
Job ID: 680-209202-1
SDG: 3620 Reeves Ridge Drive, Charlotte, NC 28214
a
Job Narrative
680-209202-1
Comments
No additional comments.
Receipt
The samples were received on 12/21/2021 11:35 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 1.00 C.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins Southeast, Savannah
Page 4 of 13 1/4/2022

Client Sample Results
Client: ERM-West Job ID: 680-209202-1
Project/Site: Storm Water - Amazon Warehouses CLT9 SDG: 3620 Reeves Ridge Drive, Charlotte, NC 28214
Client Sample ID: CLT9_Sample_Point 01_20211218 Lab Sample ID: 680-209202-1
Date Collected: 12118/21 15:54 Matrix: Water
Date Received: 12/21/21 11:36
General Chemistry
Analyte Result Quallfler RL MDL Unit D Prepared Analyzed oil Fac
Chemical Oxygen Demand 17 10 5.0 mg Ot/0312209:19 1
Total Suspended Solids 35 3.3 3.3 mg/L 12/22/21 16:14 1
Eurofins Southeast, Savannah
Page 5 of 13 1/4/2022

Client Sample Results
Client: ERM-West Job ID: 680-209202-1
Project/Site: Storm Water -Amazon Warehouses CLT9 SDG: 3620 Reeves Ridge Drive, Charlotte, NC 28214
Client Sample ID: CLT9_ Sam ple_Point 02_20211218 Lab Sample ID: 680-209202-2
Date Collected: 12118/21 16:00 Matrix: Water
Date Received: 12121121 11:35
General Chemistry
.4nalyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac
Chemical Oxygen Demand 14 10 5.0 mg/L 01/0322 09:19 1
Total Suspended Solids 160 13 13 mgtL 12/22/21 16:14 1
Eurofins Southeast, Savannah
Page 6 of 13 1/4/2022

QC Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses CLT9
Method: 5220D-2011 - Chemical Oxygen Demand
Lab Sample ID: MB 680-701595/3
Matrix: Water
Analysis Batch: 701595
MB Me
Analyte Result Qualifier
Chemical Oxygen Demand <5.0
Lab Sample ID: LCS 680-701595/4
Matrix: Water
Analysis Batch:701595
Job ID: 680-209202-1
SDG: 3620 Reeves Ridge Drive, Charlotte, NC 28214
Client Sample ID: Method Blank
Prep Type: TotallNA
RL MDL Unit D Prepared Analyzed DII Fac
10 5.0 mg/L 01/03/22 09:19 1 �.
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Chemical Oxygen Demand 50.0 49.9 mg/L too 90-110
Method: SlI 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-70037411
Matrix: Water
Analysis Batch: 700374
Me Me
Analyte Result Qualfier
Total Suspended Solids <2.5
Lab Sample ID: LCS 680-700374/2
Matrix: Water
Analysis Batch: 700374
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
2.5 2.5 mg/L 12/22/2116*14 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Analyte
Spike
Added
LCS LCS
Result Qualifier Unit
D %Rec
%Rec.
Limits
Total Suspended Solids
951
820
mg/L
86
80-120
Lab Sample ID: LCSD 680-700374/3
Client Sample
ID: Lab Control Sample Dup
Matrix: Water
Prep Type: TotalINA
Analysis Batch: 700374
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits RPD Limit
Total Suspended Solids
951
826
mg/L
87
60-120 1 25
Eurofins Southeast, Savannah
Page 7 of 13
1 /4/2022

QC Association Summary
Client: ERM-West
Job ID: 680-209202-1
Project/Site: Storm Water
- Amazon Warehouses CLT9
SDG: 3620 Reeves Ridge Drive, Charlotte, NC 28214
General Chemistry
Analysis Batch: 700374
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-209202-1
CLT9_Sample_Point 01_20211218
TotaVNA
Water
SM 2540D
680-209202-2
CLTB_Sample_Point 02_20211218
TotaVNA
Water
SM 25400
MB 680-700374/1
Method Blank
Total/NA
Water
SM 2540D
LCS 680-700374/2
Lab Control Sample
Total/NA
Water
SM 26400
LCSD 680-70037413
Lab Control Sample Dup
TotaVNA
Water
SM 2540D
Analysis Batch: 701595
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-209202-1
CLT9_Sample_Point 01_20211218
TotaVNA
Water
522OD-2011
680-209202-2
CLT9_ Sample_ Point_02_20211218
TotaVNA
Water
5220D-2011
MB 680-70159513
Method Blank
Total/NA
Water
5220D-2011
LCS 680-70159514
Lab Control Sample
TotaVNA
Water
52200-2011
Eurofins Southeast, Savannah
Page 8 of 13 1/4/2022

Lab Chronicle
Client: ERM-West Job ID: 680-209202-1
Project/Site: Storm Water - Amazon Warehouses CLT9 SDG: 3620 Reeves Ridge Drive, Charlotte, NC 28214
Client Sample ID: CLT9_e_Poit 0 Sampin1_20211218 Lab Sample ID: 680-209202-1
Date Collected: 12J18121 15:54 Matrix: Water
Date Received: 12121/21 11:35
Batch Batch oil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount N,,mber or Analyzed Analyst Lab
TotaVNA Analysis 522OD-2011 1 2 mL 2 mL 701595 01/0322 09:19 ALG TAL SAV
Instrument IDSPC7
TotaVNA Analysis SM 2540D 1 750 mL 1000 mL 700374 122221 16:14 PG TAL SAV
Instrument ID: NOEQUIP
Client Sample ID: CLT9_Sample_Point_02_20211218 Lab Sample ID: 680-209202-2
Date Collected: 12/18/21 16:00 Matrix: Water
Date Received: 12/21/21 11:35
Batch Batch
oil
Initial
Final
Batch
Prepared
Prep Type
Type Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA
Analysis 5220D-2011
1
2 mL
2 mL
701595
01/03/22 09:19
ALG TAL SAV
Instrument ID: SPC7
To1aVNA
Analysis SM 2540D
1
200 mL
1000 mL
700374
12/2221 16:14
PG TAL SAV
Instrument ID: NOEQUIP
Laboratory References:
TAL SAV = Eurofins Southeast, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Southeast, Savannah
Page 9 of 13 1/4/2022

Accreditation/Certification Summary
Client: ERM-West Job ID: 680-209202-1
Project/Site: Storm Water - Amazon Warehouses CLT9 SDG: 3620 Reeves Ridge Drive, Charlotte, NC 28214
Laboratory: Eurofins Southeast, Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SM State 269 12-31-22
0
Eurofins Southeast, Savannah
Page 10 of 13 1/4/2022

Method Summary
Client: ERM-West Job ID: 680-209202-1
Project/Site: Storm Water - Amazon Warehouses CLT9 SDG: 3620 Reeves Ridge Drive, Charlotte, NC 28214
Method Method Description Protocol Laboratory
5220D-2011 Chemical Oxygen Demand SM TAL SAV
SM 2540D Solids, Total Suspended (TSS) SM TAL SAV
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewatee'
Laboratory References:
TAL SAV = Eurofins Southeast, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
NO
Eurofins Southeast, Savannah
Page 11 of 13 1 /4/2022

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Eurofins TestAmerica, Savannah
5102 LaRoche Avenue
Savannah GA31404
Phone [phone] Fax. [phone]
Chain of Custody Record 1-1 • eurofins
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Client Information
Sample,rl. I.
MQ1M1{joy% hil Q r
Lab PM
Cisneros Roxanne
Cartier T2dar g"a)
CDC No
240-87330-333451
Cane Canoed,
MS Kelley Hand
Pnona 4
38' 3 j
EWail
Panne eisneros@Eurofnsetcom
Stale MOiigin
Page
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Company
ERM-Midwest Inc.
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Analysis Requested
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Address
0101 North High Street Suite 30
Due Dale Requested
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C Zn Acetate 0-AsNa02
D N=a P N2204S
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F McOH R Na25203
G hridyor 6 H2SO4
H Ascorbic And T TSPDcde®nyd.ale
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K EOTA W-PH 45
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Compliance Project AYes 4 No
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Sa�mp7le Disposal (A fee may be assessed ifsamples am retained longer than i moirdr)
l Remm To Client =Lwomil By LabArch ve For Months_
Deliverable Requested 1 II III N Other (specify)
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Login Sample Receipt Checklist
Client: ERM-West
Login Number: 209202
List Number 1
Creator: Hartley, Tyler
Question
Job Number: 680-209202-1
SDG Number: 3620 Reeves Ridge Drive, Charlotte, NC 28214
List Source: Eurofins Southeast, Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
NIA
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COG is present.
True
COG is filled out in ink and legible.
True
COG is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COG.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4').
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
NIA
Eurofins Southeast, Savannah
Page 13 of 13 1/4/2022