NCG060412_Monitoring Report_20211021

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG060000
Food and Kindred
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG060412
Person Collecting Samples: Darrin Paine
Facility Name: Amazon.com Services LLC - CLT9
Laboratory Name: Eurofins TestAmerica
Facility County: Mecklenburg
Laboratory Cert. No.:269
Discharge during this period:
Yes
No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? Lj Yes + No
If so, which Tier (1, 11, or III)?
A copy of this DIVIR has been uploaded electronically via https://edocs.deg. nc.gov/Forms/SW-DMR 0Yes No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities —Benchmarks in (Red)
Parameter
Parameter
Outfall002
Outfall
Outfall
Outfall
Outfall
Code
N/A
Receiving Stream Class
WS-Iv
N/A
Date Sample Collected MM/DD/YYYY
9/21/2021
46529
24-Hour Rainfall in inches
0.3
C0530
TSSin mg/L(100 or50•)
49
00400
PH in standard units (&0-9.0 FW,
7.63
6.8— 0 V)
00556
Oil & Grease in mg/L (30)
N/A
31616
l of
Fecal Coliform per 100 M,10)
N/A
freshwater (if required)1000
Enterococci per 100 ml of saltwater
61211
(if required) (500)
N/A
Chemical Oxygen Demand in mg/L
00340
(120)
47
Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average
Estimated New Motor/Hydraulic Oil
NCOIL
Usage in gal/month
N/A
00552
1 Non -Polar oil & Grease in mg/L (15)
N/A
Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L
FW (Freshwater) SW (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee or Delegated Authorized Individual
nickensaQamamn.com
Email Address
(C) �a z
Date
[phone]
Phone Number

urofins
Environment Testing
America
ANALYTICAL REPORT
Eurofins TestAmerica, Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel:[phone]
Laboratory Job ID: 680-204877-1
Laboratory SDG: 3620 Reeves Ridge Drive, Charlotte NC
28214
Client Project/Site: Storm Water - Amazon Warehouses (CLT9)
For:
ERM-Midwest Inc.
8101 North High Street
Suite 30
Columbus, Ohio 43235
Attn: Ms. Kelley Hand
lq"&A u Ccsturvs
Authorized for release by:
101412021 3:32:07 PM
Roxanne Cisneros, Senior Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
F, J

Definitions/Glossary
Client: ERM-Midwest Inc. Job ID: 680-204877-1
Project/Site: Stone Water -Amazon Warehouses (CLT9) SDG: 3620 Reeves Ridge Drive, Charlotte NC 28214
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
o Listed underthe " D` column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
oil Fac Dilution Factor
DL Detection Limit(DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis ofthe sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative/Absent
PCs Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient(Dioxin)
TNTC Too Numerous To Count
Eurofins TestAmerica, Savannah
Page 2 of 12 10/4/2021

Sample Summary
Client: ERM-Midwest Inc. Job ID: 680-204877-1
Project/Site: Storm Water - Amazon Warehouses (CLT9) SDG: 3620 Reeves Ridge Drive, Charlotte NC 28214
Lab Sample ID Client Sample ID Matrix Collected Received h
680-204877-1 CLT9 Sample Point 02_20210921 Water 09/21/21 14:19 09/23/21 10:30
Page 3 of 12 Eurofins TestAmerica, SMAiMl

Case Narrative
Client: ERM-Midwest Inc.
ProjectfSite: Storm Water -Amazon Warehouses (CLT9)
Job ID: 680-204877-1
Laboratory: Eurofins TestAmerica, Savannah
Narrative
Job ID:680-204877-1
SDG: 3620 Reeves Ridge Drive, Charlotte NC 28214
a
680-204877-1
Comments
No additional comments.
Receipt
The sample was received on 9/23/2021 10:30 AM. Unless otherwise noted below, the sample arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 0.40 C.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins TestAmerica, Savannah
Page 4 of 12 10/4/2021

Client Sample Results
Client: ERM-Midwest Inc.
Project/Site: Stone Water - Amazon Warehouses (CLT9)
Client Sample ID: CLT9_Sample_Point 02_20210921
Date Collected: 09121/21 14:19
Date Received: 09/23121 10:30
Job ID: 680-204877-1
SDG: 3620 Reeves Ridge Drive, Charlotte NC 28214
Lab Sample ID: 680-204877-1
Matrix: Water
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fae
Chemical Oxygen Demand 47 10 5.0 mg/L 10/04/21 12:52 1
Total Suspended Solids 49 13 13 mg/L 09127/21 18:16 1
Eurofins TestAmerica, Savannah
Page 5 of 12 10/4/2021

QC Sample Results
Client: ERM-Midwest Inc.
Project/Site: Stone Water -Amazon Warehouses (CLT9)
Method: 5220D-2011 - Chemical Oxygen Demand
Lab Sample ID: MB 680-687848/3
Matrix: Water
Analysis Batch:687848
Chemical Oxygen Demand
Lab Sample ID: LCS 680-687848/4
Matrix: Water
Analysis Batch: 687848
Analyte
Chemical Oxygen Demand
Job ID:680-204877-1
SDG: 3620 Reeves Ridge Drive, Charlotte NC 28214
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac
<5.0 10 5.0 mg/L 10/04/2112:52 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
50.0 44.8 mg/L 90 90-110
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-68681111
Matrix: Water
Analysis Batch: 686811
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared
Analyzed DII Fac
Total Suspended Solids <2.5
2.5 2.5 mg/L
09/27/21 18:16 1
Lab Sample ID: LCS 680.68681112
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 686811
Spike
LCS LCS
%Rec.
Analyte Added
Result Qualifier
Unit D %Rec
Limits
Total Suspended Solids 951
822
mg/L 86
80-120
Lab Sample ID: LCSD 680-686811/3
Matrix: Water
Analysis Batch: 686811
Spike
Analyte Added
Total Suspended Solids 951
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
LCSD LCSD
Result Qualifier Unit
814 mg/L
%Rec. RPD
D %Rec Limits RPD Limit
86 80-120 1 25
Eurofins TestAmerica, Savannah
Page 6 of 12 10/4/2021

QC Association Summary
Client: ERM-Midwest Inc. Job ID: 680-204877-1
Project/Site: Storm Water -Amazon Warehouses (CLT9) SDG: 3620 Reeves Ridge Drive, Charlotte NC 28214
General Chemistry
Analysis Batch: 686811
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-204877-1
CLT9_Sample_Point 02_20210921
TotaVNA
Water
SM 2540D
MB 680-686811/1
Method Blank
TotaVNA
Water
SM 2540D
LCS 680-6868112
Lab Control Sample
Total/NA
Water
SM 2540D
LCSD 680-686811/3
Lab Control Sample Dup
Total/NA
Water
SM 2540D
Analysis Batch: 687848
0
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-204877-1
CLT9_Sample_Point02_20210921
TotaVNA
Water
5220D-2011
MB 680-687848/3
Method Blank
TotaVNA
Water
5220D-2011
LCS 680-687848/4
Lab Control Sample
Total/NA
Water
5220D-2011
Eurofins TestAmerica, Savannah
Page 7 of 12 10/4/2021

Lab Chronicle
Client: ERM-Midwest Inc. Job ID: 680-204877-1
Project/Site: Stone Water -Amazon Warehouses (CLT9) SDG: 3620 Reeves Ridge Drive, Charlotte NC 28214
Client Sample ID: CLT9_Sample_Point 02_20210921 Lab Sample ID: 680-204877-1
Date Collected: 09/21/21 14:19 Matrix: Water
Date Received: 09/23/21 10:30
Batch Batch
Prep Type Type Method
oil
Run Factor
Initial
Amount
Final
Amount
Batch
Number
Prepared
or Analyzed
Analyst Lab
TotayNA Analysis 5220D-2011
1
2 mL
2 mL
687848
10/04/21 12:52
ALG TAL SAV
Instrument ID: SPC7
TctaVNA Analysis SM 25400
1
200 mL
1000 mL
686811
092721 18:16
PG TAL SAV
Instrument ID: NOEQUIP
Laboratory References:
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins TestAmerica, Savannah
Page 8 of 12 10/4/2021

Accreditation/Certification Summary
Client: ERM-Midwest Inc.
Project/Site: Storm Water - Amazon Warehouses (CLT9)
Laboratory: Eurofns TestAmerica, Savannah
The accreditations/certilications listed below are applicable to this report.
Job ID: 680-204877-1
SDG: 3620 Reeves Ridge Drive, Charlotte NC 28214
Authority Program Identification Number Explration Date
North Carolina (M/SM State 269 12-31-21
u
Eurofins TestAmerica, Savannah
Page 9 of 12 10/4/2021

Method Summary
Client: ERM-Midwest Inc. Job ID: 680-204877-1
Project/Site: Storm Water - Amazon Warehouses (CLT9) SDG: 3620 Reeves Ridge Drive, Charlotte NC 28214
Method Method Description Protocol Laboratory
5220D-2011 Chemical Oxygen Demand SM TAL SAV
SM 2540D Solids, Total Suspended (TSS) SM TAL SAV
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewater'
Laboratory References:
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
M01
Eurofins TestAmerica, Savannah
Page 10 of 12 10/4/2021

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(D
0
N
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A
N
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Eurofins TestAmerica, Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Phone. [phone] Fax [phone]
'hi-ir+nttA 9 eurofins
Chain of Custody Record `
Client Information
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Robens Danielle C
COC No
440 174105-32116 1
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Mrs Danielle Roberts
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Address
17461 Denan Ave Suite 100
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443.43- 812-0046(Tel)
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680.204877 Chain of Custody
Passible Hazard Identification
Ala,, -Hazard Flammable Skin Imlant Poison B Unknown Radiological
Sample Disposal (A lee may be assessed if samples are retained longer than 1 month)
=Ree,rn To Client In Disposal By Lab Archwe For Months
Deliverable Requested I It fit. IV. Other (specify)
5pecial InsnUCtionSrUG Requirements
Empty K4 Relinquished by Date Time M«nm of Shemar
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Login Sample Receipt Checklist
Client: ERM-Midwest Inc.
Login Number: 204877
List Number. 1
Creator: Sims, Robert D
Question
Job Number: 680-204877-1
SDG Number. 3620 Reeves Ridge Drive, Charlotte NC 28214
List Source: Eurofins TestAmerica, Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
NIA
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample botties are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4').
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
NIA
FE721
Eurofins TestAmerica, Savannah
Page 12 of 12 10/4/2021